certificate of analysis - purmed global† usp 61 (enumeration of bacteria tac, tym, and...

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Reporting Limit 10 ppm *Total CBD = CBD + CBDA x 0.877 N/D - Not Detected, B/LOQ - Below Limit of Quantification CERTIFICATE OF ANALYSIS ISO/IEC 17025:2017 ACCREDITATION #103104 Order #: 55627 Order Name: Purmed 900mg CBD Oil Tincture Batch#: B200709001 Received: 06/10/2020 Completed: 07/31/2020 PurMed Global LLC 95 NE 4th Avenue Delray Beach FL, 33483 (888) 204-9353 www.purmedglobal.com Sample N/D D9-THC 3.464% Total CBD 981.9 mg Cannabinoids per unit 981.9 mg CBD per unit 1 unit = 30 ml per unit x density (0.945) x Cannabinoid concentration Cannabinoids Test SHIMADZU INTEGRATED UPLC-PDA GSL SOP 400 PREPARED: 07/23/2020 17:41:36 UPLOADED: 07/24/2020 10:53:30 Cannabinoids LOQ weight(%) mg/g mg/unit D9-THC 10 PPM N/D N/D N/D THCA 10 PPM N/D N/D N/D CBD 10 PPM 3.464% 34.636 981.9 CBDA 20 PPM N/D N/D N/D CBDV 20 PPM N/D N/D N/D CBC 10 PPM N/D N/D N/D CBN 10 PPM N/D N/D N/D CBG 10 PPM N/D N/D N/D CBGA 20 PPM N/D N/D N/D D8-THC 10 PPM N/D N/D N/D THCV 10 PPM N/D N/D N/D TOTAL D9-THC N/D N/D N/D TOTAL CBD* 3.464% 34.636 981.9 TOTAL CANNABINOIDS 3.464% 34.636 981.9 Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director Green Scientific Labs [email protected] 1-833 TEST CBD Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data was reported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation that may result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it was taken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results with the original client of record.

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Page 1: CERTIFICATE OF ANALYSIS - PurMed Global† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella

Reporting Limit 10 ppm *Total CBD = CBD + CBDA x 0.877 N/D - Not Detected, B/LOQ - Below Limit of Quantification

CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104

Order #: 55627Order Name: Purmed 900mgCBD Oil TinctureBatch#: B200709001Received: 06/10/2020Completed: 07/31/2020

PurMed Global LLC95 NE 4th AvenueDelray Beach FL, 33483(888) 204-9353www.purmedglobal.com

Sample

N/D D9-THC

3.464% Total CBD

981.9 mg Cannabinoids per

unit

981.9 mg CBD per

unit

1 unit = 30 ml per unit x density (0.945) xCannabinoid concentration

Cannabinoids TestSHIMADZU INTEGRATED UPLC-PDAGSL SOP 400 PREPARED: 07/23/2020 17:41:36 UPLOADED: 07/24/2020 10:53:30 Cannabinoids LOQ weight(%) mg/g mg/unitD9-THC 10 PPM N/D N/D N/DTHCA 10 PPM N/D N/D N/DCBD 10 PPM 3.464% 34.636 981.9CBDA 20 PPM N/D N/D N/DCBDV 20 PPM N/D N/D N/DCBC 10 PPM N/D N/D N/DCBN 10 PPM N/D N/D N/DCBG 10 PPM N/D N/D N/DCBGA 20 PPM N/D N/D N/DD8-THC 10 PPM N/D N/D N/DTHCV 10 PPM N/D N/D N/D

TOTAL D9-THC N/D N/D N/DTOTAL CBD* 3.464% 34.636 981.9TOTAL CANNABINOIDS 3.464% 34.636 981.9

Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director

Green Scientific [email protected]

1-833 TEST CBD

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.

Page 2: CERTIFICATE OF ANALYSIS - PurMed Global† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella

PESTICIDE ANALYSIS:GSL SOP 401 PREPARED: 06/10/2020 17:02:48

N/D = Not Detected, A/LOQ = Above LOQ Level, B/LOQ = Below LOQ Level, B/LOD = Below LOD Level

CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104

Order #: 55627Order Name: Purmed 900mgCBD Oil TinctureBatch#: B200709001Received: 06/10/2020Completed: 07/31/2020

PurMed Global LLC95 NE 4th AvenueDelray Beach FL, 33483(888) 204-9353www.purmedglobal.com

GCMS-MS - Shimadzu GCMS-TQ8040

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

CAPTAN 0.700 N/D 0.003 0.001CHLORDANE 0.100 N/D 0.003 0.001CHLORFENAPYR 0.100 N/D 0.003 0.001COUMAPHOS 0.100 N/D 0.003 0.001

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

CYFLUTHRIN 2.000 N/D 0.003 0.001CYPERMETHRIN 1.000 N/D 0.003 0.001PARATHION-METHYL 0.100 N/D 0.003 0.001PENTACHLORONITROBENZENE 0.100 N/D 0.003 0.001

LCMS-MS - Shimadzu LCMS-8060

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

ABAMECTIN B1A 0.100 N/D 0.005 0.001ACEPHATE 0.100 N/D 0.001 0.001ACEQUINOCYL 0.100 N/D 0.001 0.001ACETAMIPRID 0.100 N/D 0.005 0.001ALDICARB 0.100 N/D 0.005 0.001AZOXYSTROBIN 0.100 N/D 0.001 0.001BIFENAZATE 0.100 N/D 0.005 0.001BIFENTHRIN 3.000 N/D 0.005 0.001BOSCALID 0.100 N/D 0.005 0.001CARBARYL 0.500 N/D 0.003 0.001CARBOFURAN 0.100 N/D 0.001 0.001CHLORANTRANILIPROLE 10.000 N/D 0.005 0.005CHLORPYRIFOS 0.100 N/D 0.001 0.001CLOFENTEZINE 0.100 N/D 0.001 0.001DAMINOZIDE 0.100 N/D 0.005 0.001DIAZINON 0.100 N/D 0.001 0.001DICHLORVOS 0.100 N/D 0.005 0.001DIMETHOATE 0.100 N/D 0.001 0.001DIMETHOMORPH 2.000 N/D 0.005 0.001ETHOPROPHOS 0.100 N/D 0.001 0.001ETOFENPROX 0.100 N/D 0.001 0.001ETOXAZOLE 0.100 N/D 0.010 0.005FENHEXAMID 0.100 N/D 0.005 0.001FENOXYCARB 0.100 N/D 0.005 0.001FENPYROXIMATE 0.100 N/D 0.001 0.001FIPRONIL 0.100 N/D 0.003 0.001FLONICAMID 0.100 N/D 0.025 0.010FLUDIOXONIL 0.100 N/D 0.003 0.001HEXYTHIAZOX 0.100 N/D 0.005 0.001IMAZALIL 0.100 N/D 0.005 0.001

Pesticide Action Level(ppm)

Results(ppm)

LOQ(ppm)

LOD(ppm)

IMIDACLOPRID 5.000 N/D 0.005 0.001KRESOXIM-METHYL 0.100 N/D 0.010 0.005MALATHION 0.500 N/D 0.005 0.001METALAXYL 2.000 N/D 0.001 0.001METHIOCARB 0.100 N/D 0.005 0.001METHOMYL 1.000 N/D 0.001 0.001MEVINPHOS 0.100 N/D 0.001 0.001MYCLOBUTANIL 0.100 N/D 0.005 0.001NALED 0.100 N/D 0.005 0.001OXAMYL 0.500 N/D 0.001 0.001PACLOBUTRAZOL 0.100 N/D 0.005 0.001PERMETHRINS 0.500 N/D 0.005 0.001PHOSMET 0.100 N/D 0.005 0.001PIPERONYLBUTOXIDE

3.000 N/D 0.001 0.001

PRALLETHRIN 0.100 N/D 0.005 0.005PROPICONAZOLE 0.100 N/D 0.010 0.005PROPOXUR 0.100 N/D 0.001 0.001PYRETHRINS(PYRETHRIN I)

0.500 N/D 0.005 0.005

PYRIDABEN 0.100 N/D 0.005 0.001SPINETORAM 0.100 N/D 0.001 0.001SPINOSAD 0.100 N/D 0.001 0.001SPIROMESIFEN 0.100 N/D 0.005 0.001SPIROTETRAMAT 0.100 N/D 0.001 0.001SPIROXAMINE 0.100 N/D 0.001 0.001TEBUCONAZOLE 0.100 N/D 0.005 0.001THIACLOPRID 0.100 N/D 0.001 0.001THIAMETHOXAM 5.000 N/D 0.001 0.001TRIFLOXYSTROBIN 0.100 N/D 0.001 0.001

Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director

Green Scientific [email protected]

1-833 TEST CBD

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.

Page 3: CERTIFICATE OF ANALYSIS - PurMed Global† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella

CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104

Order #: 55627Order Name: Purmed 900mgCBD Oil TinctureBatch#: B200709001Received: 06/10/2020Completed: 07/31/2020

PurMed Global LLC95 NE 4th AvenueDelray Beach FL, 33483(888) 204-9353www.purmedglobal.com

RESIDUAL SOLVENTS:Headspace GCMS - Shimadzu GCMS QP2020 with HS20

GSL SOP 405Prepared: 06/10/2020 16:54:42

Residual Solvent Action Level (ppm) Results (ppm) LOQ (ppm) LOD (ppm)1,1-DICHLOROETHENE 8 N/D 0.63 0.631,2- DICHLOROETHANE 2 N/D 0.12 0.02ACETONE 5,000 N/D 140 20ACETONITRILE 410 N/D 25 1BENZENE 1 N/D 1 0.5BUTANE 5,000 N/D 50 10CHLOROFORM 1 N/D 1 0.5CIS 1,2-DICHLOROETHENE 5 N/D 0.73 0.18ETHANOL 5,000 N/D 140 20ETHYL ACETATE 5,000 N/D 140 20ETHYL ETHER 5,000 N/D 140 20ETHYLENE OXIDE 1 N/D 0 0ISOPROPYL ALCOHOL 5,000 N/D 140 20METHANOL 3,000 N/D 100 20METHYLENE CHLORIDE 125 N/D 0.15 0.15N-HEPTANE 5,000 N/D 140 20N-HEXANE 290 N/D 18 10PENTANE 5,000 N/D 140 20PROPANE 5,000 N/D 20 1TOLUENE 890 N/D 53 1TRANS 1,2-DICHLOROETHENE 5 N/D 0.73 0.18TRICHLOROETHENE 1 N/D 1 0.5XYLENES 150 N/D 130 20

Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director

Green Scientific [email protected]

1-833 TEST CBD

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.

Page 4: CERTIFICATE OF ANALYSIS - PurMed Global† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella

CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104

Order #: 55627Order Name: Purmed 900mgCBD Oil TinctureBatch#: B200709001Received: 06/10/2020Completed: 07/31/2020

PurMed Global LLC95 NE 4th AvenueDelray Beach FL, 33483(888) 204-9353www.purmedglobal.com

Microbial Analysis:PCR - Agilent AriaMX

Microbial Analysis GSL SOP 406 Uploaded: 06/15/2020 09:32:25

Test Test MethodUsed Device Used LOD Allowable Criteria Actual

Result Pass/Fail

STEC E.COLI* USP 61/62† ARIAMX PCR 1 CFU/G** DETECT/NOT DETECTEDNOT

DETECTEDPASS

SALMONELLA* USP 61/62† ARIAMX PCR 1 CFU/G** DETECT/NOT DETECTEDNOT

DETECTEDPASS

YEAST AND MOLD USP 61/62† ARIAMX PCR CFU/G BY SAMPLE TYPE** 10,000 CFU/GNOT

DETECTEDPASS

TOTAL AEROBIC BACTERIA USP 61/62† ARIAMX PCR CFU/G BY SAMPLE TYPE** 100,000 CFU/GNOT

DETECTEDPASS

COLIFORM USP 61/62† ARIAMX PCR CFU/G BY SAMPLE TYPE** 1,000 CFU/GNOT

DETECTEDPASS

ENTEROBACTERIACEAE USP 61/62† ARIAMX PCR CFU/G BY SAMPLE TYPE** 1,000 CFU/GNOT

DETECTEDPASS

† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella run as Multiplex ** CFU/g Calculation based on Select Category Type Gummy MIP/Extract Flower matrix

Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director

Green Scientific [email protected]

1-833 TEST CBD

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.

Page 5: CERTIFICATE OF ANALYSIS - PurMed Global† USP 61 (enumeration of bacteria TAC, TYM, and ENT/Coliform), USP 62 (identifying specific species E.coli Aspergillus etc) * STEC and Salmonella

CERTIFICATE OF ANALYSISISO/IEC 17025:2017 ACCREDITATION #103104

Order #: 55627Order Name: Purmed 900mgCBD Oil TinctureBatch#: B200709001Received: 06/10/2020Completed: 07/31/2020

PurMed Global LLC95 NE 4th AvenueDelray Beach FL, 33483(888) 204-9353www.purmedglobal.com

Mycotoxin Analysis:LC-MS - Shimadzu LCMS-8060GSL SOP 401 Uploaded: 06/11/2020 11:34:04

Analyte Action Lvl (ppb) Results (ppb)AFLATOXIN B1 20 N/DAFLATOXIN B2 20 N/DAFLATOXIN G1 20 N/DAFLATOXIN G2 20 N/DOCHRATOXIN A 20 N/D

LOQ is 1ppb, LOD is 1ppb

Heavy Metals Analysis:ICP-MS - Shimadzu ICPMS-2030GSL SOP 403 Uploaded: 06/12/2020 17:50:04

Metal Action Level (ppb) Result (ppb)ARSENIC (AS) 200 B/LOQCADMIUM (CD) 200 B/LOQMERCURY (HG) 100 B/LOQLEAD (PB) 500 B/LOQ

Lower Limit of Quantitation (LOQ) is 75 ppb

Water Activity:HD-3A Water Activity Meter - GSL SOP 407 Uploaded: 06/11/2020 16:14:06

Water0.78

Filth and Foreign Materials Analysis:Microscope - Amscope Simul-Focal Trinocular Stereo Zoom Microscope - GSL SOP 409 Uploaded: 06/11/2020 15:44:55

Pass: No Foreign Materials Detected

Dr. Andrew Hall, Ph.D.,Chief Scientific Officer Ben Witten, MS, MT., Lab Director

Green Scientific [email protected]

1-833 TEST CBD

Green Scientific Labs uses its best efforts to deliver high quality results and to verify that the data contained therein are based on sound scientific judgment and levels listed are guidelines only and all data wasreported based on standard laboratory procedures and deviations. However Green Scientific Labs makes no warranties or claims to that effect and further shall not be liable for any damage or misrepresentation thatmay result from the use or misuse of the data contained herein in any way. Further, Green Scientific Labs makes no claims regarding representations of the analyzed sample to the larger batch from which it wastaken. Data and information in this report are intended solely for the individual(s) for whom samples were submitted and as part of our strict confidentiality policy, Green Scientific Labs can only discuss results withthe original client of record.