balance de masa - proceso acido citrico

8
Materials & Streams Report for ejemplo February 13, 2015 - Page 1 - 1. OVERALL PROCESS DATA Annual Operating Time 7,687.27 h Recipe Batch Time 613.27 h Recipe Cycle Time 294.75 h Number of Batches per Year 25.00 MP = Undefined

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Page 1: Balance de Masa - Proceso Acido Citrico

Materials & Streams Reportfor ejemplo

February 13, 2015

- Page 1 -

1. OVERALL PROCESS DATA

Annual Operating Time 7,687.27h

Recipe Batch Time 613.27h

Recipe Cycle Time 294.75h

Number of Batches per Year 25.00

MP = Undefined

Page 2: Balance de Masa - Proceso Acido Citrico

- Page 2 -

2.1 STARTING MATERIAL REQUIREMENTS (per Section)

Section Starting Material Active Product

AmountNeeded

(kgSin/kg

MP)

MolarYield

(%)

MassYield

(%)

GrossMassYield

(%)

Main Section (none) (none) Unknown Unknown Unknown Unknown

Sin = Section Starting Material, Aout = Section Active Product

2.2 BULK MATERIALS (Entire Process)

Material kg/yr kg/batch kg/kg MPGlucosa 15,750 630.000

Water 522,220 20,888.791

Biomass 0 0.010

Air 5,289,215 211,568.614

TOTAL 5,827,185 233,087.415

2.3 BULK MATERIALS (per Section)

SECTIONS IN: Main Branch

Main Section

Material kg/yr kg/batch kg/kg MPGlucosa 15,750 630.000

Water 522,220 20,888.791

Biomass 0 0.010

Air 5,289,215 211,568.614

TOTAL 5,827,185 233,087.415

2.4 BULK MATERIALS (per Material)

Glucosa

Procedure % Total kg/yr kg/batch kg/kg MP

Main Section (Main Branch)P-1 100.00 15,750 630.000

TOTAL 100.00 15,750 630.000

Page 3: Balance de Masa - Proceso Acido Citrico

- Page 3 -

Water

Procedure % Total kg/yr kg/batch kg/kg MP

Main Section (Main Branch)P-1 100.00 522,220 20,888.791

TOTAL 100.00 522,220 20,888.791

Biomass

Procedure % Total kg/yr kg/batch kg/kg MP

Main Section (Main Branch)P-2 100.00 0 0.010

TOTAL 100.00 0 0.010

Air

Procedure % Total kg/yr kg/batch kg/kg MP

Main Section (Main Branch)P-2 11.11 587,668 23,506.723

P-7 88.89 4,701,547 188,061.892

TOTAL 100.00 5,289,215 211,568.614

2.5 BULK MATERIALS: SECTION TOTALS (kg/batch)

Raw Material Main SectionGlucosa 630.000

Water 20,888.791

Biomass 0.010

Air 211,568.614

TOTAL 233,087.415

2.6 BULK MATERIALS: SECTION TOTALS (kg/yr)

Raw Material Main SectionGlucosa 15,750

Water 522,220

Biomass 0

Air 5,289,215

TOTAL 5,827,185

Page 4: Balance de Masa - Proceso Acido Citrico

- Page 4 -

3. STREAM DETAILS

Stream Name S-109Entrada de aire

industrNutrientes agua

Source INPUT P-7 INPUT INPUT

Destination P-7 P-3 P-1 P-1

Stream PropertiesActivity (U/ml) 0.00 0.00 0.00 0.00

Temperature (°C) 25.00 40.00 25.00 25.00

Pressure (bar) 1.01 6.01 1.01 1.01

Density (g/L) 1.18 6.66 1,509.84 994.70

Total Enthalpy (kW-h) 0.00 793.86 0.00 0.00

Specific Enthalpy (kcal/kg) 0.00 3.63 0.00 0.00

Heat Capacity (kcal/kg-°C) 0.24 0.24 0.30 1.00

Component Flowrates (kg/batch)Nitrogen 144,265.639 144,265.639 0.000 0.000

Oxygen 43,796.253 43,796.253 0.000 0.000

Glucosa 0.000 0.000 630.000 0.000

Water 0.000 0.000 0.000 20,888.791

TOTAL (kg/batch) 188,061.892 188,061.892 630.000 20,888.791

TOTAL (L/batch) 159,479,685.725 28,224,764.435 417.264 21,000.000

Stream Name S-101 S-102 S-104 S-103

Source P-1 P-6 P-6 P-4

Destination P-6 P-4 P-5 P-2

Stream PropertiesActivity (U/ml) 0.00 0.00 0.00 0.00

Temperature (°C) 25.00 25.00 25.00 25.00

Pressure (bar) 10.12 10.12 10.12 10.12

Density (g/L) 1,004.74 1,004.74 1,004.74 1,004.74

Total Enthalpy (kW-h) 0.00 0.00 0.00 0.00

Specific Enthalpy (kcal/kg) 0.00 0.00 0.00 0.00

Heat Capacity (kcal/kg-°C) 0.98 0.98 0.98 0.98

Component Flowrates (kg/batch)Glucosa 630.000 63.000 567.000 63.000

Water 20,888.791 2,088.879 18,799.912 2,088.879

TOTAL (kg/batch) 21,518.791 2,151.879 19,366.912 2,151.879

TOTAL (L/batch) 21,417.264 2,141.726 19,275.537 2,141.726

Page 5: Balance de Masa - Proceso Acido Citrico

- Page 5 -

Stream Name Preinoculoentrada de aire

inoculoVenteo

inoculaciónInoculo

industrial

Source INPUT INPUT P-2 P-2

Destination P-2 P-2 OUTPUT P-3

Stream PropertiesActivity (U/ml) 0.00 0.00 0.00 0.00

Temperature (°C) 25.00 25.00 25.00 25.00

Pressure (bar) 1.01 1.01 1.01 1.01

Density (g/L) 1,050.00 1.18 1.18 995.22

Total Enthalpy (kW-h) 0.00 0.00 1.98 0.00

Specific Enthalpy (kcal/kg) 0.00 0.00 0.07 0.00

Heat Capacity (kcal/kg-°C) 1.00 0.24 0.24 1.00

Component Flowrates (kg/batch)Biomass 0.010 0.000 0.000 20.908

Carb. Dioxide 0.000 0.000 59.858 0.000

Nitrogen 0.000 18,032.427 18,034.366 0.000

Oxygen 0.000 5,474.296 5,434.425 0.000

Water 0.000 0.000 0.000 2,111.591

TOTAL (kg/batch) 0.010 23,506.723 23,528.648 2,132.499

TOTAL (L/batch) 0.010 19,934,100.972 19,938,585.181 2,142.745

Stream Name S-106 Salida industrial Cosecha medio agotado

Source P-5 P-3 P-3 P-9

Destination P-3 OUTPUT P-9 OUTPUT

Stream PropertiesActivity (U/ml) 0.00 0.00 0.00 0.00

Temperature (°C) 25.00 25.00 25.00 25.14

Pressure (bar) 10.12 1.01 1.01 1.01

Density (g/L) 1,004.74 1.18 995.22 994.66

Total Enthalpy (kW-h) 0.00 17.85 0.00 3.28

Specific Enthalpy (kcal/kg) 0.00 0.08 0.00 0.14

Heat Capacity (kcal/kg-°C) 0.98 0.24 1.00 1.00

Component Flowrates (kg/batch)Biomass 0.000 0.000 208.988 2.090

Carb. Dioxide 0.000 538.714 0.000 0.000

Nitrogen 0.000 144,285.023 0.000 0.000

Oxygen 0.000 43,438.008 0.000 0.000

Glucosa 567.000 0.000 0.000 0.000

Water 18,799.912 0.000 21,115.913 19,939.900

TOTAL (kg/batch) 19,366.912 188,261.745 21,324.901 19,941.990

TOTAL (L/batch) 19,275.537 159,522,186.264 21,427.368 20,049.090

Page 6: Balance de Masa - Proceso Acido Citrico

- Page 6 -

Stream Name biomasa S-117 residual

Source P-9 P-11 P-8

Destination P-11 P-8 OUTPUT

Stream PropertiesActivity (U/ml) 0.00 0.00 0.00

Temperature (°C) 25.14 25.00 40.00

Pressure (bar) 1.01 1.01 1.01

Density (g/L) 1,002.56 994.92 989.47

Total Enthalpy (kW-h) 0.23 0.00 24.07

Specific Enthalpy (kcal/kg) 0.14 0.00 14.97

Heat Capacity (kcal/kg-°C) 1.00 1.00 1.00

Component Flowrates (kg/batch)Biomass 206.898 5.653 5.653

Citric Acid 0.000 120.747 120.747

residuos 0.000 80.498 80.498

Water 1,176.013 1,176.013 1,176.013

TOTAL (kg/batch) 1,382.911 1,382.911 1,382.911

TOTAL (L/batch) 1,379.381 1,389.974 1,397.627

Page 7: Balance de Masa - Proceso Acido Citrico

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4. OVERALL COMPONENT BALANCE (kg/batch)

COMPONENT INITIAL INPUT OUTPUT FINAL IN-OUTBiomass 0.000 0.010 7.743 0.000 - 7.733

Carb. Dioxide 0.000 0.000 598.572 0.020 - 598.592

Nitrogen 48.179 162,298.066 162,319.388 26.856 0.000

Citric Acid 0.000 0.000 120.747 0.000 - 120.747

Oxygen 14.626 49,270.548 48,872.433 8.140 404.602

residuos 0.000 0.000 80.498 0.000 - 80.498

Glucosa 0.000 630.000 0.000 0.000 630.000

Water 0.000 20,888.791 21,115.913 0.000 - 227.122

TOTAL 62.805 233,087.415 233,115.294 35.016 0.090

Page 8: Balance de Masa - Proceso Acido Citrico

- Page 8 -

5. EQUIPMENT CONTENTS

V-101

Procedure Operation Time (in h) Volume (in L)P-1 START 0.000 0.000

P-1 CHARGE-1 (Charge) 0.917 417.264

P-1 CHARGE-2 (Charge) 4.167 21,417.264

P-1 AGITATE-1 (Agitation) 5.167 21,417.264

P-1 TRANSFER-OUT-1 (Transfer Out) 7.417 0.000

SFR-101

Procedure Operation Time (in h) Volume (in L)P-2 START 11.417 0.000

P-2 CHARGE-1 (Charge) 11.917 0.010

P-2 TRANSFER-IN-1 (Transfer In) 12.517 2,141.736

P-2FERMENT-1 (Batch Stoich.Fermentation)

300.517 2,142.745

P-2 TRANSFER-OUT-1 (Transfer Out) 303.767 0.000

FR-101

Procedure Operation Time (in h) Volume (in L)P-3 START 304.517 0.000

P-3 TRANSFER-IN-1 (Transfer In) 305.767 2,142.745

P-3 TRANSFER-IN-2 (Transfer In) 308.017 21,418.283

P-3FERMENT-1 (Batch Stoich.Fermentation)

596.017 21,427.368

P-3 TRANSFER-OUT-1 (Transfer Out) 599.267 0.000