7.459 7.439 7.424 7.404 7.320 7.289 7.274 7.246 7.224 7 ... · injection date sample name: 18 feb...
TRANSCRIPT
7.4
59 7
.439
7.4
24 7
.404
7.3
20 7
.289
7.2
74 7
.246
7.2
24 7
.172
7.1
51 7
.131
6.9
90 6
.955
6.9
34 5
.109
3.6
10 3
.578
3.4
75 3
.442
3.3
50 2
.987
2.9
70 2
.501
2.2
58
1.1
22 1
.105
-0.0
03
1.02
6.04
3.08
2.00 1.96 1.00 1.03
3.02
0.08
8 6 4 2 0 PPM
DATE: Mon Feb 18 04:45:50 2019
Nuts - $pdata
10
DMSO, F1: 400.132 F2: 1.000 SW1: 8224 OF1: 2469.1 PTS1d: 65536 EX: zg30 PW: 15.0 usec PD: 1.0 sec NA: 8 LB: 0.0
MedKoo Biosciences www.medkoo.com [email protected]
MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]
Injection Date Sample Name
: 18 Feb 19: 133865-89-1
Acq. Method : D:\METHODS\2-POS-15MIN.M Analysis Method : D:\METHODS\2-POS-15MIN.M Sample Info : Easy-Access Method: '2-POS-15MIN' Method Info : Mobile Phase : A:water(0.01%TFA) B:ACN(0.01%TFA)
GGradientTime 0 7.5 15B % 5 95 95Flow Rate :1ml/minColumn :SUNFIRE, 150*4.6mm,3.5umColumn Temperature:45C,MS POS150-1500
min*2 4 6 8 10 12 14
mAU
0
200
400
600
*DAD1 A, Sig=214,4 Ref=off
4.93
0
min*2 4 6 8 10 12 14
mAU
0
20
40
60
*DAD1 B, Sig=254,4 Ref=off
4.93
1
Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 4.93 0.03 1962.66 852.36 100.00
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 4.93 0.03 181.40 80.82 100.00
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]
: 18 Feb 19 Injection Date Sample Name : 133865-89-1
Acq. Method : D:\METHODS\1-POS-3MIN.M Analysis Method : D:\METHODS\1-POS-3MIN.M Sample Info : Easy-Access Method: '1-POS-3MIN' Method Info : Mobile Phase : A:water(0.01%TFA) B:ACN(0.01%TFA)
Gradient:5%B for 0.2min,increase to 95%B within 1.5min,95%B for 1.5min,back to 5%Bwithin 0.01min
Flow Rate :2ml/minColumn :Sunfire, 50*4.6mm,3.5umColumn Temperature:50C
min0.5 1 1.5 2 2.5
mV
-0.1
-0.05
0
0.05
ADC1 A, ELSD
min*0.5 1 1.5 2 2.5
mAU
0200400600
*DAD1 A, Sig=214,4 Ref=off
1.45
4
min*0.5 1 1.5 2 2.5
mAU
02040
*DAD1 B, Sig=254,4 Ref=off
1.45
4
min0.5 1 1.5 2 2.50
50000100000150000200000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 70
1.45
0
<<<< POSITIVE SPECTRA >>>>
1400 m/z200 400 600 800 1000 1200
05000
10000150002000025000300003500040000
Ret. Time: 1.45 ES-API Positive
325
.2
215
.1
304
.1 3
03.1
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected] MedKoo Biosciences Quality control data www.medkoo.com; [email protected]