organic chemistry intro to lab

21
ORGANIC CHM 250 lab-what to expect? By : Dr. Robert D. Craig, Ph.D

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Introductory course in the principles of organic chemistry and the derivation of these principles from a study of the properties, preparations, and interrelationships of the important classes of organic compounds

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Page 1: Organic chemistry intro to lab

ORGANIC CHM 250 lab-what to expect?By : Dr. Robert D. Craig, Ph.D

Page 2: Organic chemistry intro to lab

In the past-1980’s

• Large text books• Needed to memorize “Reactions of functional

groups and mechanism”

Page 3: Organic chemistry intro to lab

Chemials you are dealing with

• Are ofcourse-are Acids –Bases or Organic!• They have high vapour pressures• They are Flammable

Page 4: Organic chemistry intro to lab

Safety in a car

Page 6: Organic chemistry intro to lab

lab coats

• Can be taken off if something spills on You

Page 7: Organic chemistry intro to lab

Accidents could be from some else

Page 8: Organic chemistry intro to lab

Just like a drunken driver

• You are not always the cause-some other lab

Page 9: Organic chemistry intro to lab

Most organic molecules are tearing agents-leave lab when feeling dizzy!

Page 10: Organic chemistry intro to lab

Also –No contact lens!!

Page 11: Organic chemistry intro to lab

No flip flops –when warmer!!

• Proper footwear is imperative-sneakers OK!

Page 12: Organic chemistry intro to lab

The labs are cold-be prepared

Page 13: Organic chemistry intro to lab

Water flow simulates air flow

Page 14: Organic chemistry intro to lab

When Some has an accident . .

• Hold out a stick . . . .

Page 15: Organic chemistry intro to lab

Get the instructor . .know locationof showers

Page 16: Organic chemistry intro to lab

Need to work in pairs

• You can not see Yourself!

Page 17: Organic chemistry intro to lab

Lastly –respect for others

Page 18: Organic chemistry intro to lab

Assignments will look like this

Week 2 : 2/6/2012 Prelab Questions: Due 2/6/2012 at the start of the class:• Please watch required video-download sample lab-• Define what is a crystal?• Write an expanded outline for the seven-step process

of crystallization.• *This will be included in the lab report

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• This technique is used for obtaining a compound in pure solid form of well-defined geometrically shaped crystals. This process of crystallization can be used for the purification of a compound only when the compound and the impurities present in it differ considerably in their solubilities in any particular solvent

Page 21: Organic chemistry intro to lab

Digimelt apparatus

Chapter 4: Melting point- Please watch required video in portal

• 3.) (3 sentences) Why are melting points

recorded?• Review operation of “Digimelt apparatus”*This will be included in the lab report