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Annual Report 2008 Department of Materials Science and Engineering

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NTNUThe Norwegian University of Science and Technology (NTNU) in Trondheim represents academic eminence in technology and the natural sciences as well as in other academic disciplines ranging from the social sciences, the arts, medicine, architecture to fine arts. Cross-disciplinary cooperation results in ideas no one else has thought of, and creative solutions that change our daily lives.

Department of Materials Science and EngineeringNorwegian University of Science and TechnologyNO-7491 Trondheim, Norway

www.ntnu.no

Ann

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Ann

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Department ofMaterials Scienceand Engineering

Table of ContentsEditorial ........................................................................................................................................................................................... 3Science stories ...................................................................................................................................................................... 5Publications in international peer review journals, books and patents ....... 15Conference proceedings, other reports and publications .............................................. 19Equipment ................................................................................................................................................................................... 21Chemistry Building II (KII)-Seminars, Energy and Materials ..................................... 24Guest lecturers ...................................................................................................................................................................... 26Staff ...................................................................................................................................................................................................... 27Graduate studies ................................................................................................................................................................. 31Dr.ing/PhD projects in progress ...................................................................................................................... 33Dr.ing/PhD projects co-supervised in other departments ............................................ 36Course program ................................................................................................................................................................... 37M.Sc. students ........................................................................................................................................................................ 39Graduated M.Sc. students with titles of their diploma works ................................... 41Extracurricular activities .......................................................................................................................................... 44

Picture on front page: Per Martin Rørvik.Photo: Lead titanate nanorods grown on strontium titanate substrates.

Annual report forDepartment of Materials Science and EngineeringNorwegian University of Science and TechnologyNO-7491 Trondheim, NorwayInternet address: http://www.ntnu.no/materialteknologi

The editor thanks✔ Brit Wenche Meland, Hilde Martinsen Nordø, Hege Knutsdatter Johnsen and

Åse Lill Salomonsen for collecting the administrative data and taking care of the process of printing the report.

✔ Skipnes kommunikasjon for printing.

NoTeS

3

From the editors

2008 have been an important year for recruitment of

new faculty members. Four new faculty members have

joined the department to strengthen our education and

research in silicon production including feedstock for

solar grade silicon, refining and recycling of metals,

high temperature corrosion and surface science and

finally nano-materials. in addition a professorship

in physical metallurgy was advertised last year and

the top candidate was just recently hired. Finally, a

professor in solar cell materials, expected to be hired

during 2009, will complete our effort to strengthen

our academic staff. the new staff will strengthen our

study programs and research activities in NtNUs

strategic areas materials, nanotechnology and energy

technology. We are much exited to see the influence of

these young and talented new faculty members in the

years to come.

Four of the new faculty members are women, which

bring the fraction of women in academic positions at

the department a significant step in the right direction.

the low fraction of female academic staff members

in natural science and technology is one of the

important challenges in academia. our new talented

female scientists are important role models for all

the excellent female students in our study programs

and we believe that this will motivate a higher fraction

of our female master students to continue with a Phd

study and to further qualify for an academic position in

the future.

the annual number of publications in peer reviewed

international journals continued to increase in 2008.

this is one of the most important strategic objectives

at NtNU and we are contributing strongly to achieve

this objective. the “working horse” in the research is

the Phd students, the post docs and scientists at the

department. We appreciate the long hours they spend

at the laboratories and the hard work they carry out.

the number of Phd awarded in 2008 was 10, which is

lower than expected, which calls for new efforts to

help the Phd students to finalise their theses in time.

2008 has also been a very successful year with

respect to new research projects. our early initiatives

to establish silicon solar cell research in Norway have

paid off in recent years and particularly last year. The

Norwegian Research Centre for Solar Cell Technology

was awarded to the four research institutions

iFe, NtNU, siNteF and Uio in February 2009. our

scientists in this field are key partners in this Centre

with an annual budget of 40 mNoK. several other

projects have also been granted, many of them are

in collaboration with siNteF and industrial partners.

Finally, basic science has also been strengthened,

particularly by the grant for a strategic University

Program (sUP), and two projects supported by the

FriNAt and FriteK programs. We acknowledge

the financial support from the research Council of

Norway and our industrial partners.

the strong growth in solar cell research has also

paved the way for addressing the need for a new

research infrastructure and state of the art labora-

tories. our vision of a new building “solbygg” are

becoming closer to realization day by day. the financial

crises has given new challenges with respect to indu-

strial support for the infrastructure, while on the

other hand we hope that this turns in favour of funding

from the government. We believe that during the next

coming months the funding for our new infrastructure

will be in place.

hydro Aluminium has been one of our key industrial

partners in the past and is certainly an important

partner also in the future. Both hydro Aluminium and

NtNU were concerned with the declining research and

education activity related to aluminium in recent years.

hydro Aluminium is strongly supporting our effort

to strengthen our aluminium activities and has given

financial support to hire two new faculty members,

one in physical metallurgy as described above and one

in aluminium electrolysis technology. Unfortunately,

we have not been able to identify candidates for the

second position. however, instead we will strengthen

the research on primary aluminium production by

hiring an adjunct professor and recruiting a young

and talented scientist, with the intention to qualify

for an academic position. We are very pleased with

the support from hydro Aluminium and their efforts

to strengthen the unique research triangle between

hydro, siNteF and NtNU. the research Council of

4

will continue their studies with a Phd degree which

will balance the fraction of foreign and domestic Phd

students at the department.

the annual report has the same outline as we have

used the last six years. the first part comprises short

reports giving an impression of the current research

conducted in the four research groups, the annual list

of publications and conference proceedings and the

laboratory infrastructure. the first part is intended to

give external readers an impression of the research

being performed. the second part, which comprises

an overview of the staff, master students and Phd

students, last years masters and Phd candidates and

their thesis’ titles and finally extracurricular activities,

is presenting a comprehensive overview of the annual

activity and is more intended for the archives.

We will like to acknowledge the scientific staff for

their contribution to this report. Particularly we would

like to acknowledge secretary Åse Lill salomonsen

and the other members of the administrative staff for

their effort.

NtNU April 2009

Tor Grande and Knut Marthinsen

From the editors

Norway has during 2009 carried out an evaluation of

research in chemistry in Norway. the electrochemistry

and inorganic chemistry groups have been evaluated

and both research groups received relatively good

scores and were recognized for their healthy research

culture. several recommendations for improvements

are suggested by the expert panel, particularly with

respect to strengthen basic science and, improve the

publication rate, particularly in high impact journals.

the implementation of the recommendations will be

initiated in near future.

excellent student recruitment to our student

programs has continued in 2008. our study program

in materials technology was recognized among the

students at NtNU to be the best master program in

technology. We believe this does not come by itself,

but reflects our continued effort to improve the quality

of our study programs, to include students in our

research activities and “the open door” policy. this is

an important recognition that we are on the right track.

this year we have also reasons to expect that a larger

fraction of the master students graduating in 2009

5

Thermodynamics is an integral part of high

temperature materials technology. For the evaluation

of process routes in synthesis of new materials,

computational thermodynamics is an essential tool,

and the importance of thermodynamic modelling in

the improvement of industrial production processes

and of materials degradation, can not be under-

estimated. As the application of thermodynamics

becomes indispensable in industries dealing with

production of bulk materials and/or energy

conversion, personnel competence in this area –

both in the scientific community and industry -

will be a cornerstone.

As such, the cross-sectorial “KmB” project

(competence project with user support) thermotech

was commenced at siNteF/NtNU in 2003, with a

projected duration of 6 years, aimed at jointly building

new- and supporting/building bridges between

established thermodynamic competence in the

different groups at siNteF materials and Chemistry

and the Faculty of science and technology at NtNU.

the overall scientific and technological goal held for

the thermotech project was to deliver new, advanced

thermodynamic modelling tools to Norwegian

industry as well as develop experimental methods

for high temperature materials technology, educate

Phd candidates and develop a strong joint research

community at siNteF and NtNU, which can serve the

industry in the field of computational thermodynamics

applied to high temperature materials technology.

the project, which had a total budget of 48.3 mNoK,

was funded by NFr, the Norwegian primary aluminium

producers, the Norwegian ferroalloy producers and

statoilhydro, and was one of the first broad KmB

consortiums at siNteF and NtNU in this field with

shared support from different industries.

the main areas in which the thermotech project has

made major scientific and technological contributions are:

•Developmentofinternationallyrenowned

ferroalloys- and solar grade silicon databases.

• Establishmentofafundamentalunderstandingof

the chemical and mechanical stability of materials in

the Al-electrolysis cell.

• Establishmentofanewmethodologyforcouplingof

thermodynamics and fluid flow in the modelling of

metallurgical processes.

•Newdataandafundamentalunderstandingof

the metal dusting – high temperature corrosion

phenomenon in the production of syngas.

For the ferroalloys industry, the database development

was mainly focused on improving the manganese and

chromium mn/Cr-Fe-si-C quaternary alloy systems,

as well as the Cr2o3/mno-sio2-Cao-Al2o3-mgo-Feo

oxide thermodynamic data in existing, commercial

databases.

With the rapidly expanding Norwegian solar cell

industry – with roots in the si metal producing

industries- the team set out to establish the

world’s best thermodynamic and kinetic database

for solar Grade silicon (soG-si) and its important

trace elements (such as P, B, Fe, ti, Al, Ca, o, C,

N). An example of boron distribution data obtained

in the project is shown to the left. the project can

successfully claim that siNteF/NtNU now holds the

world’s most complete thermodynamic database

for soG-si and its most important impurities. this

database is already in use in essentially all si

production and refining projects currently running at

siNteF/NtNU.

For the Aluminium industry, a significant contribution

by the thermotech project is the understanding

of the role of sodium (Na) in the deterioration of

electrolysis cell bottom linings. it has been shown

that Na diffuses through cathode carbon and changes

its wetting properties so that the cryolite bath can

enter the pores in cathode carbon, and react with

underlying refractory brick. if it wasn’t for sodium,

the refractories would last forever! Based on this

knowledge, the aluminium industry can now work on

solutions for reducing the Na attacks on the linings and

thus increasing the lining lifetime. this is an important

step towards cutting refractory costs and reducing

landfill of waste materials.

the “holy grail” of modelling multi-phase

metallurgical processes and reactions is to establish a

eXtrACtiVe metALLUrGY

highlights from the “thermotech” project

6

eXtrACtiVe metALLUrGY

joint treatment of thermodynamics and fluid dynamics.

to solve this computer-intensive task, the project team

used a silicon refining reactor as modelling case and

took a “module- based” approach in order to enable

the model development. modules to describe the

thermodynamics and physical properties (viscosity,

surface tension etc) of reacting species and reaction

products (gases, slags, metal phases) were developed.

these “modules” were called upon in a CFd framework

which made a simplified model description of the

multiphase flow in the refining reactor. the established

model has been used to successfully reproduce

refining data measured during industrial refining

campaigns carried out at the elkem thamshavn plant

and at the Fesil holla plant. the project has brought

the vision of developing a fully fledged tool to describe

reactive multi-phase flow significantly closer to

realisation!

reforming of natural gas to syngas (Co & h2) is the

most critical process step in gas-to-liquid conversion

processes, e.g. methanol or synfuel production.

in order to render natural gas reforming more

ecological and economical, the current and upcoming

processes seek to reduce the steam content in the

process gas while increasing the overall reforming

capacity. however, metal dusting corrosion (mdC) of

the structural material imposes a limit on optimal,

reliable, and safe syngas production under these

conditions. the work carried out in thermotech has

contributed to being able to understand and predict the

corrosion rate of materials used in high temperature,

carbon-saturated gaseous environments during

production of syngas. this knowledge is applied to

selecting new, more corrosion resistant alloys in new

and existing syngas installations. Longer material

lifetime will promote both increased safety and cost

reductions in the future.

A summary of the results dissemination include 14

Journal Publications, 58 Conference Publications and

Presentations, 34 scientific reports and memos, 7 msc

theses, 7 Phd theses, 1 Book and 1 Book Chapter, 3

Public seminars, 4 industry seminars/Workshops (at

industry premises) and 1 Popular science Article.

Gabriella Tranell

Pho

to: K

ai T

ang,

SIN

TEF

Pho

to: J

ohn

Wal

msl

ey, S

INTE

F/N

TNU

Pho

to: E

gil S

kyba

kmoe

n, S

INTE

F

7

Nanostructured ferroelectric materials

Fig. 1

SEM images of PbTiO3 nanostruktures grown on single-crystal SrTiO3 substrates by a hydrothermal method. Growth

on three different substrate orientations is shown: (a) (100)-oriented substrate, (b) (110)-oriented substrate, and (c)

(111)-oriented substrate.

Pho

to: P

er M

arti

n R

ørvi

k

Perovskite oxides are an important group of

ceramic materials with the common formula ABO3.

Several perovskites such as PbTiO3 and KNbO3 are

ferroelectric, meaning that they exhibit a spontaneous

electric polarization that can be switched by an

external electric field. Other perovskites are

multiferroic, meaning that they exhibit both

ferroelectric and ferromagnetic properties. BiFeO3 is

a multiferroic material which has gained huge interest

in the recent years because of its ferroelectric and

antiferromagnetic behaviour.

With the current trend in miniaturizing electronic

components, sensors and other technological devices,

nanostructuring of materials become increasingly

more important. Nanostructures of ferroelectric

materials are used in a variety of applications

such as non-volatile ferroelectric random access

memory, nanoelectromechanical systems, nanoscale

capacitors, advanced sensors, energy-harvesting

devices, photonic crystals and in photocatalysis. For

the wide-spread use of these applications in the future

it is desirable to fabricate the nanostructures by

cost-effective and large-area methods, which favours

chemical bottom-up methods in contrast to physical

top-down methods such as lithography. so although

controlling the growth of such nanostructures is a

challenging task it has a high impact for future use.

the inorganic materials and Ceramics research

group, headed by Professor mari-Ann einarsrud

and Professor tor Grande, has studied the growth

iNorGANiC ChemistrY

and properties of nanostructures of ferroelectric

perovskites since 2003. our main efforts have been

in synthesizing one-dimensional nanostructures of

Pbtio3 and KNbo3, and in studying finite size effects

in BiFeo3. the Phd students Per martin rørvik and

sverre magnus selbach, and post doc Guozhong Wang

have been the main contributors to this work.

For a controlled growth of Pbtio3 nanorods, we

have developed a hydrothermal synthesis method to

grow nanorods on srtio3 substrates. hydrothermal

synthesis is a relatively simple method to obtain

crystalline material at much lower temperatures

compared to other synthesis methods. in our synthesis

procedure an amorphous Pbtio3 precursor was

mixed with a surfactant and heat treated at 180 °C

in the presence of a single-crystal srtio3 substrate.

hierarchical nanostructures of Pbtio3 nanorods were

obtained by controlling the synthesis parameters (Fig.

1). the anisometric growth of the nanorods is proposed

to occur by self-assembly of cube-shaped or facetted

nanocrystals.

the domain configuration of these Pbtio3 nanorods

has been studied by transmission electron microscopy

(tem) and piezoresponse force microscopy (PFm) in

collaboration with the tem group at the department

of Physics (Professor randi holmestad) and the oxide

electronics group at the department of electronics

and telecommunications (Professor thomas tybell).

the as-synthesized nanorods were shown to have the

polarization direction in the longitudinal direction.

8

iNorGANiC ChemistrY

alumina membranes as templates in which a Pb-

ti sol was infiltrated. After subsequent drying and

annealing, and removal of the template by immersion

in Naoh, Pbtio3 nanotubes were obtained (Fig. 3). the

template-assisted method is an easy method to obtain

nanotubes of perovskite oxides, but necessitates high-

temperature treatment to crystallize the material and

typically produces polycrystalline tubes.

our group has also developed a hydrothermal

method for synthesizing orthorhombic single-

crystalline KNbo3 nanorods, by reacting Nb2o5 in

a Koh solution, using a surfactant as structure-

directing agent. high-quality KNbo3 nanorods were

only obtained in a narrow window of synthesis

parameters. the phase transition temperatures for

the orthorhombic to tetragonal and tetragonal to cubic

transitions of the nanorods were significantly lower

than that of the bulk KNbo3 materials, reflecting a

finite size or disorder effect.

A detailed study on the strong size-dependent

properties of the multiferroic compound BiFeo3 has

been conducted using X-ray diffraction and differential

scanning calorimetry. Nanoparticles with mean

diameters of 11 - 86 nm were made by calcining a

polymeric BiFeo3 precursor at various temperatures.

When the nanoparticle size decreased the polar

distortion of the unit cell decreased, the polar

displacements of Bi3+ and Fe3+ relative to the oxygen

sublattice increased, and the Néel temperature (the

onset of antiferromagnetic ordering) decreased (Fig.

4). the combination of increasing polar displacements

of cations and decreasing unit cell distortions sheds

light on the microscopic origin of finite size effects

in ferroelectric nanoparticles. Ferroelectricity

disappears at small dimensions due to loss of

cooperative ordering of cation displacements, but

polar displacements on a local scale prevail. the origin

of finite size effects is decoupling of ferroelectric

moments, hence ferroelectricity is lost through

disordering rather than a displacive process. the

decrease in the Néel temperature can be rationalized

from decreasing Fe-o-Fe angle due to increasing

displacements of Fe, and increasing Fe-o bond

lengths. Both microscopic structural changes leads

Fig. 2

Hysteresis curve measured by PFM on a single PbTiO3

nanorod.

Pho

to: P

er M

arti

n R

ørvi

k

Fig. 3

SEM image of PbTiO3 nanotubes made by a template-

assisted method.

After annealing the nanorods above the Curie

temperature (490 °C) the crystallographic orientation

changed and the polarization was found along the

radial direction. A hysteresis curve measured by PFm

is shown in Fig. 2, demonstrating the ferroelectric

nature of the nanorods.

A template-assisted method has been developed

for the preparation of Pbtio3 nanotubes, using porous

Pho

to: P

er M

arti

n R

ørvi

k

9

iNorGANiC ChemistrY

to decreasing overlap of Fe 3d eg and o 2p orbitals,

and antiferromagnetic ordering vanishes at lower

temperatures. Combined with recent observations

of increased magnetization of nanoparticles, these

are promising results with respect to the possibility

of making small multiferroic nanostructures for

technological applications.

these basic research studies have shown the ability

of relatively simple chemical methods to synthesize

nanoparticles and hierarchical nanostructures of

a technologically very important group of ceramic

materials. in our work we have also shown that the

properties of the nanostructured materials differ

from their bulk counterparts, which is important in

applications. A list of publications can be found at the

group’s homepage:

(http://www.material.ntnu.no/ceramics/publications).

Per Martin Rørvik and Sverre Magnus Selbach

Fig. 4

Size-dependent properties of BiFeO3 nano-

particles as function of the nanoparticle

diameter (d). Pseudotetragonality c/a (in red)

is a measure of the unit cell distortion along

the polar direction c. Polar displacements of

Bi and Fe along the c-axis are the origin of fer-

roelectric polarization in BiFeO3. Inset: The an-

tiferromagnetic ordering temperature TN. Pho

to: S

verr

e M

agnu

s S

elba

ch

10

Microstructure control during thermo-mechanical

processing of metals and alloys is essential to

optimize processes and taylor-make material

properties to specific applications. Key processes

are recrystallisation and grain growth, where the

evolution in microstructure and texture results from a

complex interplay between a number of material and

process parameters. In this context it is important

to have adequate simulation tools to replace time

consuming and costly experimental parametric

studies and for analyses and numerical experiments,

to explore parameter relationships which are not

easily available experimentally.

monte Carlo (mC) simulations are a powerful

and versatile computer simulation approach used

in relation to a variety of materials problems. the

mC method uses random numbers to approximate

solutions, and it is often used to solve complex

or nonlinear problems. in a recently finished Phd

work (egil Fjeldberg) 3d mC simulations were

used to investigate a number of problems related

to microstructure and texture evolution during

recrystallization and grain growth in polycrystalline

materials. in the context of grain growth and

recrystallisation, the method used is the so-called

Potts monte Carlo model, in which a microstructure

is mapped onto a 3d discrete lattice by assigning

each volume element in the lattice a crystallographic

orientation oi (i = 1:Q) so that all lattice sites within a

“grain” have the same orientation. inert particles are

incorporated by assigning clusters of sites a unique,

non-changeable index without any crystallographic

orientation. the grain boundaries are represented

only implicitly as surfaces separating neighbouring

elements of unlike orientation. the grain boundaries

may have different energies and mobilities depending

on the misorientation between the grains. due to the

computer power requirements parts of the work has

been done at the supercomputer facilities provided by

the Norwegian metacenter for computational science,

NotUr.

Fjeldberg’s Phd work is here exemplified through

the simulations on abnormal grain growth in the

presence of particles. Grain growth may be divided

into two types, normal grain growth and abnormal

grain growth (or secondary recrystallisation). during

normal grain growth, the microstructure coarsens

uniformly, and there is generally a relatively narrow

range of grain sizes and shapes, and the form of the

grain size distribution is usually independent of time.

Abnormal grain growth, on the other hand, refers to

the process where a few grains in the microstructure

grow at the expense of a fine grained matrix. Usually

also a bimodal grain size distribution develops,

consisting of a few large, abnormally grown grains

and a large amount of small, retained matrix grains.

Abnormal grain growth is observed in a wide variety of

polycrystalline metals and ceramics, and it may or may

not be desirable. For example, the abnormal growth of

{110} < 001 > Goss-oriented grains in transformer steel

improves magnetic permeability and loss properties.

in contrast, abnormal grain growth in copper films

used in electronic interconnects causes a bimodal

grain size distribution that is detrimental to reliability.

the avoidance of abnormal grain growth at high

temperature is generally also an important aspect of

grain size control in steels and nonferrous alloys, e.g.

aluminium.

it is generally accepted that abnormal grain growth

cannot occur in an “ideal grain assembly”, i.e. a

simple single-phase uniform grain structure with

constant and isotropic properties). most assumptions

concerning the origin of abnormal grain growth

assume some kind of advantage, as a condition for

the occurrence of abnormal growth. this advantage

is most commonly related to size, but can also be

related to texture where certain special boundaries

experience a higher mobility, or, in the case of thin

films, to surface effects. it is also well known that

second-phase particles can be used to control grain

size during normal grain growth. the use of particles

to refine grain size is important in e.g. steel making

and in the welding of certain metal alloys, including

aluminium. however, it is also common knowledge

that abnormal grain growth can develop in a matrix

pinned by particles when the pinning force somehow

is lowered. in spite of a lot of work and many efforts,

the general conditions and behaviour of abnormal

grain growth is poorly understood. in a recent work by

3d Potts monte Carlo simulations of abnormal grain growth

PhYsiCAL metALLUrGY

11

holm and co-workers at sandia National Laboratories

used a 2d Potts monte Carlo model to test whether

abnormal subgrain growth (mobility driven) could be a

possible nucleation mechanism for recrystallisation.

the present work was an extension of this previous

work to 3d and with a particular focus on the influence

of particles on mobility-driven abnormal grain growth.

the question asked, was whether mobility-driven

abnormal grain growth can be reduced or inhibited by

adding second-phase particles to the microstructure.

if this is possible, materials which are subjected to

conditions for mobility-driven grain growth and which

thus may be weakened due to abnormal grain growth,

can get considerably improved by addition of second

phase particles.

however, unfortunately the simulations did not

confirm our hypothesis. the simulation results

are exemplified by the temporal evolution of the

3d microstructure in the case of 10 vol% particles,

Figure 1. it is clearly seen that in contrast to what

one get during normal curvature driven grain growth

with particles, Zener pinning is not obtained, i.e. the

particles in this case are unable to stabilize the grain

PhYsiCAL metALLUrGY

Fig. 1

The microstruc-

ture after differ-

ent times for the

case of 10vol% of

particles. (a) Ini-

tial microstruc-

ture, (b) After

80 Monte Carlo

Steps (MCS), (c)

After 100 MCS

and (d) After 200

MCS.

Pho

to: E

gil F

jeld

berg

12

structure. instead the particles seem merly to have

a small inhibiting effect on the number of abnormal

grains, and simulations for various volume fractions

of particles, have shown that this effect has only

noticeable influence for volume fractions above 5

vol%.

however, in spite of the “negative” result this

example clearly illustrates the use of computer

simulations as a powerful tool to do numerical

experiments and test hypotheses that are not

easily, and sometimes not even possible, to do

experimentally.

Knut Marthinsen

PhYsiCAL metALLUrGY

Pho

to: E

gil F

jeld

berg

Fig. 2

Number fraction of abnormal grains versus

the vol% of particles together with the stand-

ard deviation. Two interpretations of the data

at low vol% of particles are indicated. Dotted

line: Linear trend; dashed line: Cuto in number

fraction below 5vol%.

13

New type of precipitate with belt-like morphology is

observed in Hf-containing aluminium cast alloys.

Nanobelt-like precipitates are observed in hf-

containing aluminium cast alloys after heat treatments

(Fig. 1). these nanobelt-like precipitates exhibit

straight, bent or twisted morphologies and they are

randomly distributed throughout the specimen. each

nanobelt has a uniform width along its entire length.

the nanobelt precipitates are typically 60-240 nm

wide, 10-40 nm thick and a few to several tens of

micrometers long. Quantitative compositional analysis

and hrtem investigations from one precipitate

reveal that the nanobelt precipitate has a si2hf-type

structure, which is orthorhombic.

A high density of belt-like precipitates is revealed

from microstructural observation by sem (Fig. 2). the

present nanobelt precipitate is noncoherent with the

aluminium matrix, and it is not yet clear what effect the

precipitates have on the mechanical properties.

Zhihong Jia and Lars Arnberg

Nanobelt-like precipitates in multicomponent aluminium alloys

Pho

to: Z

hiho

ng J

iaP

hoto

: Zhi

hong

Jia

Fig. 1

Low magnification bright-

field TEM (a) and HAADF

STEM (b) images from the

same alloy sample but

different areas.

Fig. 2

Back-scatter electron SEM

image of the alloy after heat

treatment. A high density of

fine HF-containing precipi-

tates (white) can be seen in

addition to eutectic Si parti-

cles (grey) and Fe-containing

particles (bright white).

PhYsiCAL metALLUrGY

14

The background of this project is the potential for

development of pure and ultra-fine grained titanium

for biomedical applications. The project is financed by

the Norwegian Research Council under the NANOMAT

program and is organized at SINTEF in Trondheim.

in recent years, commercial pure (CP) ti processed

by methods of severe plastic deformation (sPd) has

attracted growing interest among materials scientists.

this interest is based not only on the potential for

important applications such as medical implants with

better biocompatibility and no toxic alloying elements,

but also due to the potential to match and improve the

mechanical properties above that of the conventional

alloy ti-6Al-4V.

high resolution eBsd has been extensively employed

to quantitatively characterize the microstructure

evolution during sPd. it is widely known that the Kikuchi

diffraction patterns become poorer with increasing

accumulated strains and hereby residual stresses

introduced by sPd. therefore, there is no literature

characterizing the highly-strained microstructures by

means of eBsd, e.g. equal channel angular pressing

(eCAP) followed by high pressure torsion (hPt).

A removal of the residual stresses in the deformed

samples seems to be a promising approach and an

example of the corresponding structure (eBsd), is

shown in Fig.1a. the material processed by eCAP and

subsequently deformed by hPt keeps dimensions

~10mm in diameter and 0.7mm in thickness (Fig. 1b).

here, the eBsd technique reveals the cross section

structure after hPt at a position 3mm from edge. Fig.1a

shows that a bimodal - and equiaxed ultrafine grained

microstructure is obtained. the corresponding size

distribution in Fig.1c shows that there are two peaks in

grain size, i.e. around 100 nm and 700 nm respectively.

.

Yongjun Chen and Hans Jørgen Roven

Pure and ultra-fine grained titanium fabricated by sPd for biomedical applications

Pht

oto:

Yong

jun

Che

n

Fig.1 (a) High resolution EBSD orientation map of CP Ti after ECAP 4 passes route Bc at 723 K followed by HPT 5 turns at

room temperature. (b) Typical HPT samples and (c) grain size distribution of the microstructure shown in (a).

PhYsiCAL metALLUrGY

15

PUBLiCAtioNs iN iNterNAtioNAL Peer reVieW JoUrNALs , BooKs ANd PAteNts

• ElEctrochEmistry

Haarberg, G.M.; Kvalheim, E.; Wang, S.:Electrochemical behavior of dissolved Fe2O3 in molten CaCl2-KF.Journal of Iron and Steel Research International 15 (2008) 48-51.

Haas, O.-E.; Briskeby, S.T.; Kongstein, O.E.; Tsypkin, M.; Tunold, R.; Børresen, B.:Synthesis and characterisation of RuxTi1-xO2 as a catalyst support for polymer electrolyte fuel cell.Journal of New Materials for Electrochemical Systems 11 (2008) 9-14.

Jia, Z.; Graver, B.K.F.; Walmsley, J.C.; Yu, Y.; Solberg, J.K.; Nisancioglu, K.:Effect of magnesium on segregation of trace element lead and anodic activation in aluminum alloys.Journal of the Electrochemical Society 155 (2008) C1-C7.

Keppert, M.; Rakhmatullin, A.; Simko, F.; Deschamps, M.; Haarberg, G.M.; Bessada, C.:Multi-nuclear magnetic resonance study of Na3AIF6-AIPO4 molten and solidified mixtures.Magnetic Resonance in Chemistry 46 (2008) 803-810.

Larsen, M.H.; Walmsley, J.C.; Lunder, O.; Mathiesen, R.; Nisancioglu, K.:Intergranular corrosion of copper-containing AA6xxx AlMgSi aluminum alloys.Journal of the Electrochemical Society 155 (2008) C550-C556.

Mostad, E; Rolseth, S; Thonstad, J.:Electrowinning of iron from sulphate solutions.Hydrometallurgy 90 (2008) 213-220.

Nisancioglu, K.; Orazem, M.:Applications of potential theory in cathodic protection.ECS Transactions 16 (2008) 47-57.

Ofstad, A.B.; Davey, J.R.; Sunde, S.; Borup, R.L.:Carbon corrosion of a PEMFC during shut-down/start-up when using an air purge procedure.ECS Transactions 16 (2008) 1301-1311.

Seland, F.; Tunold, R.; Harrington, D.A.:Impedance study of formic acid oxidation on platinum electrodes.Electrochimica Acta 53 (2008) 6851-6864.

Svensson, A.M.; Weydahl, H.; Sunde, S.:Impedance modelling of air electrodes in alkaline media.Electrochimica Acta 53 (2008) 7483-7490.

Weydahl, H.; Möller-Holst, S.; Børresen, B.:Effect of gas composition and gas utilisation on the dynamic response of a proton exchange membrane fuel cell.Journal of Power Sources 180 (2008) 808-813.

Aarhaug, T.A.; Svensson, A.M.; Ofstad, A.B.; Sørli, J.G.H.; Couvert, H.:PEMFC degradation assessed by effluent analysis from designed experiments.ECS Transactions 16 (2008) 1687-1695.

• EXTRACTIVE METALLURGY

Cui, J.; Zhang, L.:Metallurgical recovery of metals from electronic waste: A review.Journal of Hazardous Materials 158 (2008) 228-256.

Eidem, P.A.; Tangstad, M.; Bakken, J.A.:Determination of electrical resistivity of dry coke beds.Metallurgical and Materials Transactions B - Process Metallurgy and Materials Processing Science 39 (2008) 7-15.

Kvithyld, A.; Meskers, C.E.M.; Gaal, S.; Reuter, M.; Engh, T.A.:Recycling light metals: Optimal thermal de-coating.Journal of the Minerals, Metals and Materials Society 60 (2008) 47-51.

Meskers, C.E.M.; Reuter, M.A.; Boin, U.; Kvithyld, A.:A fundamental metric for metal recycling applied to coated magnesium.Metallurgical and Materials Transactions B - Process Metallurgy and Materials Processing Science 39 (2008) 500-517.

Safarian-Dastjerdi, J.; Kolbeinsen, L.:Kinetic of carbothermic reduction of MnO from high-carbon ferromanganese slag by graphite materials.ISIJ International 48 (2008) 395-404.

Safarian-Dastjerdi, J.; Tranell, G.; Tangstad, M.; Kolbeinsen, L.; Gaal, S.; Kaczorowski, J.:Reduction kinetics of MnO from high-carbon ferro- manganese slags by carbonaceous materials in Ar and CO atmospheres.Metallurgical and Materials Transactions B - Process Metallurgy and Materials Processing Science 39 (2008) 702-712.

Zhang, L.; Ciftja, A.:Recycling of solar cell silicon scraps through filtration. Part I: Experimental investigation.Solar Energy Materials and Solar Cells 92 (2008) 1450-1461.

• INORGANIC CHEMISTRY

Jensen, M.S.; Pezzotta, M.; Zhang, Z.; Einarsrud, M.-A.; Grande, T.:Degradation of TiB2 ceramics in liquid aluminium.Journal of the European Ceramic Society 28 (2008) 3155-3164.

16

Lein, H.L.; Tezuka, T.; Grande, T.; Einarsrud, M.-A.:Asymmetric proton conducting oxide membranes and fuel cells prepared by aqueous tape casting.Solid State Ionics 179 (2008) 1146-1150.

Lioliou, M.G.; Kofina, A.N.; Paraskeva, C.A.; Klepetsanis, P.G.; Østvold, T.; Payatakes, A.C.; Koutsoukos, P.G.:Controlled precipitation of sparingly soluble phosphate salts using enzymes. I: Controlled development of solution supersaturation in situ.Crystal Growth & Design 8 (2008) 1390-1398.

Mokkelbost, T.; Kaus, I.; Haugsrud, R.; Norby, T.; Grande, T.; Einarsrud, M.-A.:High-temperature proton-conducting lanthanum ortho-niobate-based materials. Part II: Sintering properties and solubility of alkaline earth oxides.Journal of the American Ceramic Society 91 (2008) 879-886.

Ochoa-Fernandez, E.; Rønning, M.; Yu, X.; Grande, T.; Chen, D.:Compositional effects of nanocrystalline lithium zirconate on its CO2 capture properties.Industrial & Engineering Chemistry Research 47 (2008) 434-442.

Okuyucu, H.; Dahl, P.I.; Einarsrud, M.-A.:Coating of LaCoO3 thin film with sol-gel dip coating method.Journal of Nanoscience and Nanotechnology 8 (2008) 685-688.

Palcut, M.; Christensen, J.; Wiik, K.; Grande, T.:Impurity diffusion of 141Pr in LaMnO3, LaCoO3 and LaFeO3 materials.Physical Chemistry Chemical Physics 10 (2008) 6544-6552.

Pezzotta, M.; Zhang, Z.; Jensen, M.S.; Grande, T.; Einarsrud, M.-A.:Cohesive zone modeling of grain boundary microcracking induced by thermal anisotropy in titanium diboride ceramics.Computational Materials Science 43 (2008) 440-449.

Rørvik, P.M.; Almli, Å.; van Helvoort, A.; Holmestad, R.; Tybell, T.; Grande, T.; Einarsrud, M.-A.:PbTiO3 nanorod arrays grown by self-assembly of nanocrystals.Nanotechnology 19 (2008) 6 pages.

Rørvik, P.M.; Lyngdal, T.; Sæterli, R.; van Helvoort, A.; Holmestad, R.; Grande, T.; Einarsrud, M.-A.:Influence of volatile chlorides on the molten salt synthesis of ternary oxide nanorods and nanoparticles.Inorganic Chemistry 47 (2008) 3173-3181.

Sandengen, K.; Jøsang, L.O.; Kaasa, B.:Simple method for synthesis of magnesite (MgCO3).Industrial & Engineering Chemistry Research 47 (2008) 1002-1004.

Selbach, S.M.; Tybell, T.; Einarsrud, M.-A.; Grande, T.:The ferroic phase transitions of BiFeO3.Advanced Materials 20 (2008) 3692-3696.

Svarcova, S.; Wiik, K.; Tolchard, J. R; Bouwmeester, H.J.M.; Grande, T.:Structural instability of cubic perovskite BaxSrxSr1-xCo1-y

FeyO3- δ.Solid State Ionics 178 (2008) 1787-1791.

Sæterli, R.; van Helvoort, A.; Wang, G.; Rørvik, P.M.; Tanem, B.S.; Grande, T.; Einarsrud, M.-A.; Holmestad, R.:Detailed TEM characterisation of PbTiO3 nanorods.Journal of Physics, Conference Series 126 (2008) 4 pages.

Tolchard, J.R; Slater, P.R.:A high temperature powder neutron diffraction structural study of the apatite-type oxide ion conductor, La9.67Si6O26.5.Journal of Physics and Chemistry of Solids 69 (2008) 2433-2439.

Vullum, F.; Grande, T.:Oxidation driven decomposition of CeNbO4 in pure oxygen.Chemistry of Materials 20 (2008) 5434-5437.

Vullum, F.; Grande, T.:Oxygen stoichiometry and transport properties of cerium niobate.Solid State Ionics 179 (2008) 1061-1065.

Vullum, F.; Nitsche, F.; Selbach, S.M.; Grande, T.:Solid solubility and phase transitions in the system LaNb1-xTaxO4.Journal of Solid State Chemistry 181 (2008) 2580-2585.

Vullum, P.E.; Lein, H.L.; Einarsrud, M.-A.; Grande, T.; Holmestad, R.:TEM observations of rhombohedral and monoclinic domains in LaCoO3-based ceramics.Philosophical Magazine 88 (2008) 1187-1208.

Ødegård, C.; Rong, H.M.; Foosnæs, T.; Øye, H.A.:The effect of iron, aluminium and calcium in metallurgical grade silicon on the hydrogenations of silicon tetrachloride.Silicon for the Chemical and Solar Industry IX (2008) 215-224.

• PHYSICAL METALLURGY

Akhtar, S.; Arnberg, L.; Di Sabatino, M.; Dispinar, D.; Syvertsen, M.:A comparative study of porosity and pore morphology in a directionally solidified A356 alloy.International Journal of Metalcasting 3 (2008) 39-52.

Albertsen, J.Z.; Grong, Ø.; Walmsley, J.C.; Mathiesen, R.; Beek, W.J.:A model for high-temperature pitting corrosion in nickel-based alloys involving internal precipitation of carbides, oxides and graphite.Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science 39 (2008) 1258-1276.

Chen, Y.; Wang, Q.D.; Roven, H.J.; Liu, M.; Karlsen, M.; Yu, Y.; Hjelen, J.:Network-shaped fine-grained microstructure and high ductility of magnesium alloy fabricated by cyclic extrusion compression.Scripta Materialia 58 (2008) 311-314.

Chen, Y.; Wang, Q.D.; Roven, H.J.; Karlsen, M.; Yu, Y.; Liu, M.; Hjelen, J.:Microstructure evolution in magnesium alloy AZ31 during cyclic extrusion compression.Journal of Alloys and Compounds 462 (2008) 192-200.

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17

PUBLiCAtioNs iN iNterNAtioNAL Peer reVieW JoUrNALs, BooKs ANd PAteNts

Chen, Y.; Roven, H.J.; Wang, Q.D.; Liu, M.; Lin, J.:Effect of the second phase on the microstructure of magnesium alloys during cyclic extrusion compression.Materials Science Forum 584-586 (2008) 523-527.

Coco, L.; Lefevre-Schlick, F.; Bouaziz, O.; Wang, X.; Solberg, J.K.; Embury, D.:The mechanical response of compositionally graded materials.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483-484 (2008) 266-269.

Coletti, G.; Kvande, R.; Michailetchi, V.D.; Geerilings, L.J.; Arnberg, L.; Øvrelid, E.J.:Effect of iron in silicon feedstock on p- and n-type multicrystalline silicon solar cells.Journal of Applied Physics 104 (2008) 104913 (11 pages).

Di Sabatino, M.; Arnberg, L.; Apelian, D.:Progress in the understanding of fluidity of aluminium foundry alloys.International Journal of Metalcasting 2 (2008) 17-27.

Fjeldberg, E.; Marthinsen, K.:A 3D Monte Carlo simulation of the texture evolution during recrystallisation of an Al-Mg-Mn alloy.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1375-1380.

Fjeldberg, E.; Marthinsen, K.:A 3D Monte Carlo study of the effect of anisotropy on the size distribution of recrystallized grains.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1156-1162.

Forbord, B.; Hallem, H.; Røyset, J.; Marthinsen, K.:Thermal stability of Al3(Scx,Zr1-x)-dispersoids in extruded aluminium alloys.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 475 (2008) 241-248.

Gouttebroze, S.; Mo, A.; Grong, Ø.; Pedersen, K.O.; Fjær, H.:A new constitutive model for the finite element simulation of local hot forming of aluminium 6xxx alloys.Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science 39 (2008) 522-534.

Gulbrandsen-Dahl, S.; Pedersen, K.O.; Marioara, C.D.; Kolar, M.; Marthinsen, K.:Mechanical characteristics of Post-β’’ precipitates in Al-Mg-Si alloys.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1634-1639.

Grytten, F.; Holmedal, B.; Hopperstad, O.S.; Børvik, T.:Evaluation of identification methods for YLD2004-18p.International Journal of Plasticity 24 (2008) 2248-2277.

Holmedal, B.; van Houtte, P.; An, Y.:A crystal plasticity model for strain-path changes in metals.International Journal of Plasticity 24 (2008) 1360-1379.

Holmedal, B.; Skaret, P.C.; Nes, E.A.:Abrupt strain-rate changes in high-purity binary Al-Mn alloys.

Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1449-1455.

Haaland, B.Ø.; Westermann, I.; Holmedal, B.; Nes, E.A.:Microstructure and properties of as-deformed and annealed accumulated roll-bonded aluminium alloys.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1468-1473.

Jia, Z.; Arnberg, L.:Nanobelts in multicomponent aluminium alloys.Applied Physics Letters 93 (2008) 093115 (3 pages).

Jia, Z.; Arnberg, L.; Åsholt, P.; Barlas, B.; Iveland, T.:TEM investigations of aluminum precipitate in eutectic Si of A356 based alloys.Proceedings of the 14th European Microscopy Congress 2 (2008) 435-436.

Jia, Z.; Forbord, B.; Røyset, J.; Solberg, J.K.:Effect of heat treatments on hardening of Al-Zr-Sc alloys.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 141-147.

Jia, Z.; Hu, G.; Forbord, B.; Solberg, J.K.:Enhancement of recrystallization resistance of Al-Zr-Mn by two-step precipitation annealing.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483-484 (2008) 195-198.

Karlsen, M.; Hjelen, J.; Grong, Ø.; Rørvik, G.; Chiron, R.; Schubert, U.; Nilsen, E.:SEM/EBSD based in situ studies of deformation induced phase transformations in supermartensitic stainless steels.Materials Science and Technology 24 (2008) 64-72.

Kolar, M.; Gulbrandsen-Dahl, S.; Pedersen, K.O.; Marthinsen, K.:The effect of deformation on the aging response of an Al-Mg-Si alloy.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 1619-1624.

Kvande, R.; Geerlings, L.J.; Coletti, G.; Arnberg, L.; Di Sabatino, M.; Øvrelid, E.J.; Swanson, C.C.:Distribution of iron in multicrystalline silicon ingots.Journal of Applied Physics 104 (2008) 064905 (9 pages).

Li, Y.; Dons, A.L.; Furu, T.; Arnberg, L.:Decomposition of a Mn-saturated solid solution in an AA3xxx alloy during the cooling process after homogenization.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 986-992.

Li, Y.; Furu, T.; Dons, A.L.; Marthinsen, K.; Arnberg, L.:Factors influencing the precipitation behaviour of Mn-containing dispersoids during homogenization of AA3xxx aluminium alloys.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 929-935.

Lin, J.; Wang, Q.; Peng, L.; Roven, H.J.:Study on deformation behavior and strain homogeneity during cyclic extrusion and compression.Journal of Materials Science 43 (2008) 6920-6924.

18

Liu, M.; Roven, H.J.; Murashkin, M.; Valiev, R.Z.:Deformation twins and stacking faults in an AA5182 Al-Mg alloy processed by high pressure torsion.Materials Science Forum 579 (2008) 147-154.

Liu, M.; Roven, H.J.; Ungar, T.; Balogh, L.; Murashkin, M.; Valiev, R.Z.:Effects of Mg in nanostructured Al-Mg alloys subjected to severe plastic deformation.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 835-841.

Liu, M.; Roven, H.J.; Ungar, T.; Balogh, L.; Murashkin, M.; Valiev, R.Z.:Grain boundary structure and deformation defects in nanostructured Al–Mg alloys processed by high pressure torsion.Materials Science Forum 584-586 (2008) 528-534.

Liu, M.; Roven, H.J.; Yu, Y.; Werenskiold, J.C.:Deformation structures in 6082 aluminium alloy after severe plastic deformation by equal-channel angular pressing.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483–484 (2008) 59-63.

Myhr, O.R.; Grong, Ø.:Utilizing a predictive tool for designing welded aluminum components.Welding Journal 87 (2008) 36-39.

Nijs, O.C.J.; Holmedal, B.; Friis, J.; Nes, E.A.:Sub-structure strengthening and work hardening of an ultra-fine grained aluminium-magnesium alloy.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483-484 (2008) 51-53.

Pedersen, K.O.; Roven, H.J.; Lademo, O.-G.; Hopperstad, O.S.:Strength and ductility of aluminium alloy AA7030.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 473 (2008) 81-89.

Roven, H.J.; Liu, M.; Werenskiold, J.C.:Dynamic precipitation during severe plastic deformation of an Al–Mg–Si aluminium alloy.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483-484 (2008) 54-58.

Røyset, J.; Ryum, N.; Bettella, D.; Tocco, A.; Jia, Z.; Solberg, J.K.; Reiso, O.:On the addition of precipitation- and work-hardening in an Al-Sc alloy.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 483-484 (2008) 175-178.

Schaffer, P.; Mathiesen, R.; Arnberg, L.; Di Sabatino, M.; Snigirev, A.: In situ investigation of spinodal decomposition in hypermonotectic Al–Bi and Al–Bi–Zn alloys.New Journal of Physics 10 (2008) 16 pages.

Starink, M.J.; Wang, S.C.; Qiao, X.G.; Gao, N.; Roven, H.J.; Langdon, T.G.:Shear deformation and texture evolution in Al alloys processed for one pass by ECAP.Materials Science Forum 584-586 (2008) 679-684.

Stokkan, G; Ryningen, B.; Lohne, O.:Microstructures in multicrystalline silicon wafers for solar cells.Silicon for the Chemical and Solar Industry IX (2008) 113-119.

Szczygiel, P.; Roven, H.J.; Reiso, O.:Annealing of Al-Si alloys after equal-channel angular pressing.Materials Science & Engineering A - Structural Materials: Properties, Microstructure and Processing 493 (2008) 202-206.

Tangen, S.; Furu, T.; Auran, L.; Nes, E.A.:On the effect of supersaturation and dispersoids on the microstructure development after extrusion of AlMn-alloys.Proceedings of the 11th International Conference on Aluminium Alloys (2008) 607-613.

Timelli, G.; Lohne, O.; Arnberg, L.; Laukli, H.I.:Effect of solution heat treatments on the microstructure and mechanical properties of a die-cast AlSi7MgMn alloy.Metallurgical and Materials Transactions A - Physical Metallurgy and Materials Science 39 (2008 ) 1747-1758.

Werenskiold, J.C.; Auran, L.; Roven, H.J.; Ryum, N.; Reiso, O.:Screw extruder for continuous extrusion of materials with high viscosity.Patent number WO 2008/063076 A1 (2008).

Wu, Y.; Han, W.; Zhou, S.X.; Lototsky, M.V.; Solberg, J.K.; Yartys, V.:Microstructure and hydrogenation behaviour of ball-milled and melt-spun Mg-10Ni-2Mm alloys.Journal of Alloys and Compounds 466 (2008) 176-181.

Yu, Y.; Nilsen, T.A.; Raanes, M.P.; Hjelen, J.; Solberg, J.K.:Characterization of morphology and microstructure of different kinds of materials at NTNU Mater Sci EM Lab.Proceedings of the 14th European Microscopy Congress 2 (2008) 513-514.

PUBLiCAtioNs iN reFereed JoUrNALs ANd BooKs

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19

CoNFereNCe ProCeediNGs, other rePorts ANd PUBLiCAtioNs

Akhtar, S.; Timelli, G.; Bonollo, F.; Arnberg, L.; Di Sabatino, M.:A comparative study of defects and mechanical properties in high pressure die cast and gravity die cast aluminium alloys.Proceedings of the 4th International Conference High Tech Die Casting (CD) (2008) 19 pages.

Borup, R.L.; Davey, J.R.; Xu, H.; Ofstad, A.B.; Garzon, F.; Pivovar, B.:PEM fuel cell durability.Annual Progress Report (2008) 957-961.

Ciftja, A.; Engh, T.A.; Tangstad, M.:Refining and recycling of silicon: A review.NTNU Report (2008). 40 pages.

Ciftja, A.; Engh, T.A.; Tangstad, M.; Kvithyld, A.:Recycling of silicon scrap by filtration.Proceedings of the 18th Workshop on Crystalline Silicon Solar Cells & Modules: Materials and Processes (2008) 101-104.

Ciftja, A.; Engh, T.A.; Tangstad, M.; Kvithyld, A.:Recycling of solar cell silicon scrap by filtration.Proceedings of the 23rd European Photovoltaic Solar Energy Conference (2008) 1274-1277.

Ciftja, A.; Tangstad, M.; Engh, T.A.:Wettability of silicon with refractory materials: A review.NTNU Report (2008). 37 pages.

Ciftja, A.; Øvrelid, E.J.; Tangstad, M.; Engh, T.A.:Settling of solid particles in molten silicon as a refining step from metallurgical grade to solar grade silicon.Proceedings of the 3rd Nordic Symposium for Young Scientists in Metallurgy (2008) 77-81.

Cui, J.; Forssberg, E.; Manouchehri, H.-R.; Roven, H.J.:Recovery of metals from shredded television scrap.Proceedings of the XXIV International Mineral Processing Congress 3 (2008) 3461-3468.

Dalaker, H.:Addition to “Effective distribution coefficients of boron in solar grade multicrystalline silicon”: a discussion of the samples from the liquid phase.SINTEF Report A8200 (2008). 6 pages.

Dalaker, H.:Light microscopy.Translation of J. K. Solberg’s “Lysmikroskopi” (2008). 101 pages.

Dalaker, H.:The solubility of carbon in liquid silicon.SINTEF Report A6363 (2008). 22 pages.

Dalaker, H.:The solubility of nitrogen in liquid silicon equilibrated with silicon nitride.SINTEF Report A8201 (2008). 26 pages.

Dalaker, H.:Time and temperature dependency of the solubility of carbon in liquid silicon the effect of boron content.SINTEF Report A9820 (2008). 35 pages.

Dalaker, H.; Tangstad, M.:The solubility of carbon in liquid silicon and its dependence on the boron levels.Proceedings of the 18th Workshop on Crystalline Silicon Solar Cells & Modules: Materials and Processes (2008) 117-120.

Dalaker, H.; Tangstad, M.:Time and temperature of the solubility of carbon in liquid silicon.Proceedings of the 23rd European Photovoltaic Solar Energy Conference (2008) 1250-1252.

Espelund, A.W.:Bondejern i Norge.Arketype forlag (2008). 176 pages.

Espelund, A.W.:Jernvinne-mannen Halvard Bakås.Roser i skrinn jord - Halvard Bakås, Hessdalen og Arbeiderbevegelsen (2008) 150-153.

Espelund, A.W.:The mechanism of bloomery iron production.The Introduction of Iron in Eurasia (2008) 33-42.

Espelund, A.W.:Åmdals Verk 1691-1945, Deutsche Ausgabe.Vest-Telemark Museum (2008). 27 pages.

Espelund, A.W.:Åmdals Verk 1691-1945, English version.Vest-Telemark Museum (2008). 27 pages.

Espelund, A.W.; Morten, Ø.; Kyvik, G.; Grini, V.; Nordrum, F.S.; Bastiansen, B.:Åmdals Verk 1691-1945.Vest-Telemark Museum (2008). 27 pages.

Frosta, O.E.; Foosnæs, T.; Øye, H.A.; Linga, H.:Modelling of anode thermal cracking behaviour.Light Metals (2008) 923-927.

Giri, R.; Solberg, J.K.:Microstructural and mechanical properties of pulsed plasma nitrided duplex stainless steel.Proceedings of the Materials Science & Technology Conference and Exhibition (CD) (2008) 1493-1501.

20

Ibrahiem, M.O.; Foosnæs, T.; Øye, H.A.:Properties of pitch and furan-based TiB2-C cathodes.Light Metals (2008) 1013-1018.

Larsen, T.; Randhol, P.; Lioliou, M.; Jøsang, L.O.; Østvold, T.:Kinetics of CaCO3 scale formation during core flooding.Proceedings of the 9th International Conference on Oilfield Scale (2008) 12 pages.

Mönks, F.J.; Ypenburg, I.H.; Ystenes, M.:Begavede barn. En veiledning for foreldre og pedagoger.Abstrakt forlag (2008). 105 pages.

Ratvik, A.P.; Støre, A.; Solheim, A.; Foosnæs, T.:The effect of current density on cathode expansion during start-up.Light Metals (2008) 973-978.

Roven, H.J.; Hansen, G.H.:China and “The Hydro Way”: An interview with Carl Lewin, Senior Engineer, Hydro Aluminium.Making it in China (2008) 185-195.

Ryningen, B.; Stokkan, G.; Lohne, O.; Modanese, C.:Growth of dislocation clusters in directionally solidified multicrystalline silicon.Proceedings of the 23rd European Photovoltaic Solar Energy Conference (2008) 4 pages.

Wiik, K.:Et pulver for framtiden.Universitetsavisa (2008). 25.01.2008.

Ystenes, M.:Slike barn finnes - og de trenger denne boken.Begavede barn. En veiledning for foreldre og pedagoger (2008) 7-13.

Øye, H.A.:ISO standards for testing of cathode materials.Light Metals (2008) 937-948.

Øye, H.A.; Brekken, H.; Foosnæs, T.; Nygård, L.:Silicon for the Chemical and Solar Industry IX.Tapir Akademisk Forlag (2008). 283 pages.

CoNFereNCe ProCeediNGs, other rePorts ANd PUBLiCAtioNs

21

ElEctrochEmistry

Electrochemical equipment:

Potentiostates, frequency analysers and sweep

generators.

Electrochemical quartz crystal microbalance and an

electrochemical quartz crystal nanobalance.

Digital Acquisition system for FFT ac voltammetry.

Surface characterisation:

Electrochemical STM/AFM microscopy for performing in

situ combined electrochemical and surface studies.

Adsorption measurements:

A volumetric PCT (Pressure Composition Temperature)

equipment for measurements of hydrogen adsorption in

hydride forming materials.

Miscellaneous:

Preparative equipment, vacuum systems, glove boxes,

test rigs.

EXTRACTIVE METALLURGY

Furnaces

• Cruciblefurnace,capacity140kgaluminium;withgas

purging unit etc. for metal refinery studies.

• Inductionfurnace,capacity200kgofsteel,Eloterm.

• Inductionfurnace,capacity20kgofsteel,ASEA.

• Vacuuminductionfurnace,capacity2kgofsteel,Balzer.

• Plasmapilotfacility/furnace,capacity30kg/hand

plasma temperatures up to ~ 3000°C.

• Electro-meltingfurnace,one-phasecurrent,forpilot

production of metals.

• Smallinductionfurnaceupto3600°C.

Water model

• Lasermethodsappliedtofollowfluidflowandgas

bubbleflowbehaviourinlight-transparentmodels

representing industrial processes.

• Pilotscalegasinjections(inwater).

Miscellaneous

• Hightemperaturemicroscopeforwettabilitystudies;

sessile drop method.

• 10-15differentvertical‘versatile’furnaces,

temperatures up to 1600°C.

• ThermoGravimetricAnalyzerwithmassspectrometer.

• Vacuum/inertgasfacilityformeasurementsofdiffusion

constants, up to 1200°C.

• Instrumentsforsolubilitymeasurements.

INORGANIC CHEMISTRY

Materials characterization:

• Thermobalancesequippedfor

- Vapour pressure measurements by boiling point and

Knudsen effusion method for use up to 2200°C.

- High temperature gravimetric analysis (max. 2200°C)

in controlled atmosphere.

• Calorimeters

- Calvet type reaction calorimeters (max. 1120°C).

- Differential scanning calorimeter (Perkin-Elmer DSC-

2) for use up to 727°C.

- DTA/Reaction calorimeter (max 1200°C).

- TGA/DTA/DSC for use up to 1600°C.

• Viscometers

- Precision viscometers for determination of the

viscosity of molten salts, metals and hydrocarbons at

high temperatures and pressures.

• Equipmentforthemeasurementofthermalconductivity

and thermal diffusivity by the hot strip method of solids

or liquids up to 700°C (R and D Carbon).

• Equipmentforthemeasurementofthermalconductivity

of bricks and powders up to 1200°C.

• HitatchiS-3400NvariablepressureSEMequippedwith

INCA Energy EDS system and EBSD.

• Reichert-JungMeF3Aopticalmicroscopeformetaland

mineralogical applications equipped with computerized

image analysis system.

• Porosimeters

- Carlo Erba 2000 WS, (pore radius: 0.004-7.5 mm),

Macropore 120 (pore radius: 7.5-600 mm).

- Micromeritics TRISTAR 3000, (pore diameter: 3.5-

2100 Å).

• Rapoporttestapparatus(RandDCarbon).

• Rammability(RandDCarbon).

• AirPermeability(RandDCarbon).

• SpecificElectricalResistance(RandDCarbon).

• Sodiumresistancetestequipment(carbon).

• Abrasiontester.

eQUiPmeNt

22

• LloydLR100KMaterialsTestingMachine.Yieldand

strength tests up to 1000°C.

• Equipmentformechanicalcharacteri¬zationofbending

strength, E-modulus, fracture toughness and creep up

to 1100°C under controlled atmosphere.

• Equipmentformechanical3-pointbendingofgels(100g

load cell).

• Thermaldilationmeasurementsincontrolled

atmosphere up to 1450°C.

• LECOTC-436OxygenandNitrogenDeterminator.

• MicromeriticsAccuPyc1330Pycnometer.

• HaakeVT550viscometersystem.

• Instron5543Mechanicaltestingequipmentforball-on-

ring testing method, with 5N, 100N and 1kN load cells.

• Spray coater: Sono-Tek ExactaCoat FC, xyz tabletop

ultrasonic spray system with combined heat/vacuum plate.

• KSVLMX2Dipcoaterformultiplevesseldipcoating

applications.

Production of carbon materials

• Pilotplantscaleformixinganode,cathodeorramming

paste including sigma-mixer and vibration press.

Production of ceramic materials

• Spraypyrolysisunitforlargescaleproductionof

ceramic powders.

• Spraydryer.

• Coldisostaticpress(FlowAutoclaveSystems).

• Uniaxialpress.

• TapeCaster(RichardE.Mistler).

• CARVERModel#12-12HHydraulicLaboratoryPress.

Spectroscopy

• BrukerIFS66vFourierTransformInfrared

Spectrometer (4500 100 cm-1). IR microscope.

• Cary5,UV-VIS-NIRSpectrometer(57000-333cm-1).

X-ray diffraction equipment

• BrukerD8ADVANCEX-raydiffractometer.

- Cu Kα X-ray tube, variable divergence slit assembly.

- Theta/theta base goniometer, automatic sample

changer,rotatingreflectionsamplestage.

- Variable antiscatter slit assembly, scintillation

detector.

- VANTEC-I 1D detector with large active area.

- TC-Wide Range low/high temperature chamber,

rotating ceramic sample stage.

• SiemensD5005powderX-raydiffractometer,unitA.

- Primary monochromator (quartz)

- Cu Kα X-ray tube, automatic antiscatter slit,

scintillation detector.

• SiemensD5005powderX-raydiffractometer,unitB.

- Secondary monochromator (graphite), autom.

antiscatter and divergence slit, Göbel mirror system,

high temp. system HTK 15, pos. sensitive and

scintillation detector, grazing incidence attachment,

sample changer 40 pos, capillary sample holder.

• BrukerD8FocusX-raydiffractometer.

- Cu Kα X-ray tube, variable divergence slit assembly.

- Theta/theta base goniometer, automatic sample

changer,rotatingreflectionsamplestage.

- Solid state LynxEye(TM) detector and scintillation

detector.

Catalysis

• ReactorforZiegler-Nattapolymerizationwith

continuousgasflowmeasurements.

• Reactorsforproductionofdimethyldichlorosilaneand

trichlorosilane both with computerized on-line gas

chromatographs for continuous analysis. One of the

reactors can be pressurized up to 4 bars.

PHYSICAL METALLURGY

Metallography

• Specimen preparation and light optical laboratory

Traditional specimen preparation equipment for cutting,

embedding, grinding and mechanical polishing, Struers

RotoPol-31 automatic grinding and polishing machine,

Struers Lectropol-5 electropolisher, Struers Tenopol-5

for TEM thin foil preparation, 4 optical microscopes

attached with digital cameras (Leica MeF4, Leitz MM6,

Leitz Metalloplan, Zeiss Axiovert 25), Matuzawa DVK-1S

microhardness tester (0.5 – 10 kg), Leica VMHT MOT

micro hardness tester (1g – 2000g, anno 2003).

• Scanning electron microscope (SEM) laboratory

Zeiss SUPRA 55VP (LVFESEM, 2006), Hitachi S-4300SE

(FESEM, 2002), Zeiss, Ultra 55LE, FESEM (2007), Jeol

840 (1989). 3 SEMs are equipped with EDS and EBSD.

The laboratory have in-situ sub-stage systems for EBSD

tensile and thermo mechanical experiments (heating,

and cooling down to -60 °C).

• Electron probe microanalyzer (EPMA)

Jeol JXA-8500F field emission gun hyperprobe with

5 wavelength dispersive spectrometers, special

crystals for light element analysis, EDS, and

cathodoluminescence system (2006). Chemical analysis

of submicron volumes.

• Focused Ion Beam

FEI, FIB 200 (2008). While the SEM uses a focused

beam of electrons to image the sample in the chamber,

eQUiPmeNt

23

a FIB instead uses a focused beam of gallium. Focused

ion beam, also known as “FIB”, is a technique used

particularly in the semiconductor and materials science

fields for site-specific analysis, deposition, and specimen

preparation for SEM and TEM samples.

• Transmission electron microscope

Jeol JEM-2010 (1994) with LaB6 filament equipped with

STEM, EDS and Gatan GIF imaging filter.

• Specimen preparation laboratory for electron microscope

Agar, Turbo carbon coater.

Edwards, Sputtercoater S150B (Au, Pt, W).

JEOL, JEE-4X evaporator.

Fishione, Plasma cleaner, model 1020.

Iontech, Ionetcher SEM sample.

Iontech, Ionetcher TEM sample.

• X-ray diffraction

Siemens D5000 X-ray diffractometer equipped with Euler

cradle for texture measurements.

• Furnace laboratory

5 salt bath furnaces (250°C-590°C), 5 oil bath furnaces

(50°C-250°C),9fluidbedfurnaces(0°C-600°C),2muffle

furnaces (0°C-800°C, 0°C-1300°C), 2 air circulation

furnaces (0°C-650°C), one with large chamber

(Multitherm S250/65A, 450mm×450mm×600mm, anno

2003).

Mechanical testing

MTS 810 universal testing machine (10 tons), MTS 880

universal testing machine (10 tons) equipped with 250°C

furnace chamber and MTS Teststar control units, shear

tester, bend tester, compression tools, formability

tools, fatigue and fracture grips, high rate tensile grips,

ordinary extensometers and clip gauges for room

temperature testing, laser speckle analyzer, dynamic

speckle correlation strain analyses.

Metal forming

60 and 100 tons hydraulic presses, equal channel

angular pressing tools, hydroforming tools, Marciniak

formability tester (used also in MTS 880), ASAME

equipment for automatic 3-dimensional strain analysis and

measurements. Hot torsion machine, two cold rolling mills.

Casting

• Small scale solidification laboratory

3 resistor furnaces (max 1000°C), reometer, Podfa filter

for analysing melt quality, Bridgeman furnace (ferro

alloys), Seiko differential scanning calorimeter (-150°C -

600°C).

• Casting laboratory

ASEA 3830 Hz induction furnace (6.5 liters, max 1700°C),

Balzer VSG10 3830Hz vacuum induction furnace (1-2

liters, max 2000°C), induction melt spinner for rapid

solidification (5cm3), Marco arc melt spinner for rapid

solidification (100cm3).

Welding

(SINTEF but used by Department of Materials Science and

Engineering).

Hyperbaric welding equipment, ABB welding robot

station, Smitweld TCS 1405 resistor weld simulator,

2 high frequency induction generators (6kW, 12kW),

medium frequency generator (50kW), IRC (Instrumented

Restrained Cracking) jig, Satoh jig for welding prestrained

specimens, Ströhlein TCD (Thermal Conductivity

Detection) instrument for hydrogen measurement,

mercury based hydrogen analysis apparatus.

Wear testing

Pin on disk -, pin on ring - and pin on plate machines,

Struers Microwave abrasive testing machine, water jet

erosion machine.

Pressing

ABB hot isostatic press (2000 bar, 2000°C), ABB cold

isostatic press (6000 bar), Thermal Technology Inc.

hydraulic hot axial press (200kPa).

Solar silicon

Clean room class 10000, Crystalox DS 250 Bridgeman

furnace for directional solidification of (solar cell) silicon,

saw for cutting silicon ingots, Jandel four points probe

for resistivity measurements, Leo Gieken instrument

for measurement of lifetime of minority charge carriers,

PVScan 6000 instrument for measurement of dislocation

densities and detection of grain boundaries, GTSolar LBIC

(Light Beam Induced Current) measuring device.

eQUiPmeNt

24

Speaker Topic

January 18 Dr. Ulrich Bünger and Dr. Reinhold Wurster, Ludwig-Bölkow-Systemtechnik (GmbH), München-Ottobrunn, Germany.

Motivation and strategic activities required in the development of hydrogen & fuel cells for the world market.

February 1 PhD student Sverre Magnus Selbach, Department of Materials Science and Engineering, NTNU.

Order, symmetry and phase transitions in a multiferroic perovskite.

February 8 Professor, Dr.philos. Otto Lohne, Department of Materials Science and Engineering, NTNU.

Solar cells - Technology, opportunities and challenges.

February 15 Research Scientist, PhD Ingeborg Kaus, SINTEF Materials and Chemistry.

Added value technologies for solar cells.

February 22 Dr. Gery R. Stafford, National Institute of Standards and Technology (NIST), Gaithersburg, Maryland, USA.

In situ stress and nanogravimetric measurements during underpotential metal deposition.

February 29 PhD student Rajorshi Basu, Department of Materials Science and Engineering, NTNU.

Oxidation properties of a MAX phase based composite.

March 7 Project Manager, Dr.ing. Børre Tore Børresen, StatoilHydro, Norway.

The R&D project: “New energy carriers and biotechnology” in StatoilHydro.

March 28 PhD Julian Tolchard, Department of Materials Science and Engineering, NTNU.

Cation diffusion in LaGaO3, a molecular dynamics study.

April 4 PhD student Anawati, Department of Materials Science and Engineering, NTNU.

Characterization of the effect of Cu on activation of AlPb model alloy.

April 11 Associate Professor, Dr.ing. Magnus Rønning, Department of Chemical Engineering, NTNU.

In situ characterisation of catalysts for fuel production and energy conversion.

April 18 PhD student Francesco Madaro, Department of Materials Science and Engineering, NTNU.

Synthesis of alkali niobate templates for textured KNN piezoelectrics.

April 20 Professor Adolf Kisza, Faculty of Chemistry, University of Wroclaw, Wroclaw, Poland.

An equivalent circuit approach to electrochemical methods.

May 20 Professor Pierre Millet, University Paris-Sud 11, Orsay Cedex, France.

Highlights from research and development on hydrogen technology within University Paris-Sud 11.

May 29 Professor Dr. Tatiana Stromnova, the Lomonosov State Academy of Fine Chemical Technology (MITHT), Moscow, Russia.

Polynuclear carboxylate-palladium complexes as precursors for fuel cell catalysts.

May 30 Chief Technology Officer, Dr.ing. Lars Ole Valøen, Miljø Innovasjon AS, Herøya Forskningspark, Porsgrunn, Norway.

Challenges facing the Li-ion battery technology when entering the automotive market.

ChemistrY BUiLdiNG ii (Kii)–semiNArs, eNerGY ANd mAteriALsDepartment of Materials Science and EngineeringFridays 12.30 in KII (Chemistry building II)Seminar leader: Reidar Tunold

25

June 3 Principal Research Scientist Alberto Gonzalez, Teck Cominco Metals Ltd., Vancouver, Canada.

Advances in zinc electrowinning.

October 10 Professor, Dr.ing. Tor Grande, Department of Materials Science and Engineering, NTNU.

Cation diffusion in perovskite materials.

October 17 Associate Professor, PhD Fride Vullum, Department of Materials Science and Engineering, NTNU.

Synthesis and characterization of lithium ion nanobatteries and lithium battery nanoelectrode arrays.

October 24 Research Scientist, Dr.ing. Magnus Thomassen, SINTEF Materials and Chemistry.

Designed experimental approach for screening of PEMFC performance and durability.

November 7 Professor, PhD Kemal Nisancioglu, Department of Materials Science and Engineering, NTNU.

Effect of lead (Pb) segregation on electrochemistry and corrosion of aluminum alloys.

November 14 Chief Scientist Asbjørn Solheim, SINTEF Materials and Chemistry.

Deterioration of the bottom lining in aluminium reduction cells - chemical equilibria at 1100 K.

November 21 PhD student Stein Trygve Briskeby, Department of Materials Science and Engineering, NTNU.

Characterization of electrocatalysts for fuel cells.

November 28 PhD Edita Garskaite, Department of Materials Science and Engineering, NTNU.

Thin film deposition for PV solar cell applications.

December 5 PhD Evanthia Stefanidaki, Department of Materials Science and Engineering, NTNU.

Value added products based on ceramic nano-sized powders.

ChemistrY BUiLdiNG ii (Kii)–semiNArs, eNerGY ANd mAteriALs

26

Speaker Topic

January 18 Dr. Ulrich Bünger and Dr. Reinhold Wurster, Ludwig-Bölkow-Systemtechnik (GmbH), München-Ottobrunn, Germany.

Motivation and strategic activities required in the development of hydrogen & fuel cells for the world market.

February 11 Dr. Marie-Isabelle Baraton, Department of Ceramics (SPCTS, UMR CNRS), University of Limoges, Limoges Cedex, France.

Contribution of FTIR spectroscopy to nanoscience and nanotechnology.

February 22 Dr. Gery R. Stafford, National Institute of Standards and Technology (NIST), Gaithersburg, Maryland, USA.

In situ stress and nanogravimetric measurements during underpotential metal deposition.

April 29 Professor Adolf Kisza, Faculty of Chemistry, University of Wroclaw, Wroclaw, Poland.

An equivalent circuit approach to electrochemical methods.

May 20 Professor Pierre Millet, University Paris-Sud 11, Orsay Cedex, France.

Highlights from research and development on hydrogen technology within University Paris-Sud 11.

May 29 Professor Dr. Tatiana Stromnova, the Lomonosov State Academy of Fine Chemical Technology (MITHT), Moscow, Russia.

Polynuclear carboxylate-palladium complexes as precursors for fuel cell catalysts.

May 29 Principal Research Scientist Alberto Gonzalez, Teck Com-inco Metals Ltd., Vancouver, Canada.

Advances in zink electrowinning.

September 12 Kimon Symeonidis, Metals Processing Institute, Worcester Polytechnic Institute, Worcester, USA.

Controlled diffusion solidification - mechanisms and principles.

GUest LeCtUrers

27

stAFF

SCIENTIFIC STAFF

Professor, PhD Lars Arnberg

Professor emeritus Jon Arne Bakken

Associate Professor emeritus, Dr.ing. Dagfinn Bratland

Professor, Dr.ing. Mari-Ann Einarsrud,

50 % position from January 1 to June 30, 2008 and

80 % position from July 1 to December 31, 2008

Professor emeritus, Dr.ing. Thorvald Abel Engh

Adjunct Professor, PhD Olaf Engler

Professor emeritus Arne Wang Espelund

Professor, Dr.ing. Trygve Foosnæs

Professor, Dr.ing. Tor Grande

Professor, Dr.ing. Øystein Grong

Professor, Dr.scient. Jarle Hjelen

Professor emeritus, Dr.techn. Jan Lützow Holm

Associate Professor, Dr.scient. Bjørn Holmedal, (40 %)

Professor, Dr.ing. Geir Martin Haarberg

Adjunct Professor, Dr.ing. Ola Jensrud

Adjunct Professor, Dr.ing. Harald Justnes

Professor, Dr.ing. Leiv Kolbeinsen

Associate Professor, Dr.ing. Hilde Lea Lein,

from August 1, 2008

Professor, Dr.philos. Otto Lohne

Professor, Dr.ing. Knut Marthinsen

Adjunct Professor, PhD Mohammed M’Hamdi,

from August 9, 2008

Professor emeritus, M.Sc.Eng. Ketil Motzfeldt

Professor emeritus, PhD Erik Nes

Professor, PhD Kemal Nisancioglu

Professor emeritus Sverre Olsen

Adjunct Professor, Dr.ing. Knut Arne Paulsen

Adjunct Professor, Dr.techn. Oddvin Reiso

Adjunct Professor, Dr.ing. Christian Rosenkilde

Professor emeritus, Dr.techn. Terkel Rosenqvist

Professor, Dr.techn. Hans Jørgen Roven

Professor emeritus, Dr.techn. Nils Ryum

Associate Professor, PhD Frode Seland

Professor, Dr.philos Jan Ketil Solberg

Professor emeritus, Dr.ing. Åsmund Sterten

Professor, Dr.techn. Svein Sunde

Adjunct Professor, Dr.ing. Morten Sørlie

Professor, Dr.ing. Merete Tangstad

Professor emeritus, Dr.techn. Jomar Thonstad

Professor emeritus Reidar Tunold

Professor emeritus Johan Kristian Tuset

Adjunct Professor, Dr.ing. Halvard Tveit

Associate Professor, PhD Fride Vullum,

from September 17, 2008

Professor, Dr.ing. Kjell Wiik

Adjunct Professor, PhD Volodymyr Yartys

Professor, Dr.ing. Martin Ystenes

Professor, Dr.techn. Terje Østvold

Adjunct Associate Professor, Dr.ing. Eivind Johannes

Øvrelid, from July 1, 2008

Professor emeritus, Dr.techn. Harald Arnljot Øye

TECHNICAL STAFF

Senior Engineer Elin Harboe Albertsen, from April 1, 2008

Senior Engineer Jan Arve Baatnes

Chief Engineer Wilhelm Dall

Engineer Fritz Helgemo

Senior Engineer Harald Holm, from June 1, 2008

Chief Engineer Eli Beate Jakobsen

Engineer Solveig Louise Sørli Jonassen,

(50 %) from December 1, 2008

Senior Engineer Torild Krogstad

Chief Engineer Elin Nilsen, to September 1, 2008

Senior Engineer Tor Arild Nilsen

Senior Engineer Svein Arne Pedersen, (50 %)

from March 3, 2008

Senior Engineer Kjell Røkke

Chief Engineer Morten Raanes

Senior Engineer Pål Skaret

Engineer Odd Steinar Strømsli

Senior Engineer May Grete Sætran,

(50 %) from October 6, 2008

Chief Engineer Pål Ulseth

Engineer Gunn Torill Wikdahl

Chief Engineer Yingda Yu

ADMINISTRATIVE STAFF

Executive Officer Martha Bjerknes

Executive Officer Elsa Mari Florhaug

Head of Administration Trond Einar Hagen

Office Apprentice Hege Knutsdatter Johnsen,

from November 24, 2008

Executive Officer Unni Keiseraas

Higher Executive Officer Brit Wenche Meland

Executive Officer Hilde Martinsen Nordø

Secretary Åse Lill Salomonsen

28

stAFF

RESEARCH SCIENTISTS

PhD Snorre Fjeldbo, to September 15, 2008

PhD Zhihong Jia

PhD Paul Schaffer

Dr.ing. Gaute Stokkan

PhD Shuihua Tang, from June 11, 2008

PhD Mikhail Tsypkin

PhD Fride Vullum, from May 1 to September 16, 2008

GUEST PROFESSORS/RESEARCHERS

Nadia Cheroudi, from April 1 to June 30, 2008

Associate Professor, Dr.ing. Hallstein Hemmer,

from August 1, 2008

M.Sc. Jinbao Lin, to September, 2008

PhD Pietrzyk Stanislaw,

from August 4 to September 30, 2008

M.Sc. Zhipeng Zeng, from October 1, 2008

POST DOCTORAL FELLOWS

PhD Martin Bellmann

PhD Dmitry Bokach, from January 24, 2008

PhD Yongjun Chen

PhD Snorre Fjeldbo, from September 16, 2008

PhD Edita Garskaite

PhD Rajiv Giri

PhD José Luis Gómez, from February 25, 2008

Dr.ing. Sverre Gulbrandsen-Dahl, (50 %)

Dr.ing. Hilde Lea Lein, to July 31, 2008

PhD Manping Liu

PhD Raymond Longbottom, to August 28, 2008

PhD Jafar Safarian-Dastjerdi

PhD Evanthia Stefanidaki, from February 1, 2008

PhD Julian Tolchard

PhD Fride Vullum, to April 30, 2008

PhD Boyan Yuan

SCIENTIFIC ASSISTANTS

Leiv Olav Jøsang

Rune Christian Kjøsnes, to December 17, 2008

Stephen Lobo, from October 1, 2008

Natasha Rajan, from May 1 to August 31, 2008

Ruth Astrid Strøm, (10 %) from September 1, 2008

Benjamin Topinka, from May 1, 2008

Kira Turkova, (30%)

DEPARTMENT SCHOLARSHIP HOLDERS

Per Kristian Dahlstrøm, from August 11, 2008

Morten Karlsen

Lars-Erik Owe

Sverre Magnus Selbach

Xiangjun Zuo, to September 1, 2008

Cecilie Ødegård, to August 5, 2008

EXTERNAL SCHOLARSHIP HOLDERS WITH TEACHING DUTIES

Sarina Bao

Stein Trygve Briskeby

Jirang Cui

Halvor Dalaker

Mahdi Darab, from June 2, 2008

Per Anders Eidem, to September 15, 2008

Egil Fjeldberg

Nils Håvard Giskeødegård

Sidsel Meli Hanetho

Fredrik Haakonsen

Liudmila Igorevna Ilyukhina

Morten Sundheim Jensen, to September 6, 2008

Lina M. Jonasson, to September 19, 2008

Kenji Kawaguchi

Eirin Kvalheim

Ingrid Anne Lervik, to November 8, 2008

Francesco Madaro

Chiara Modanese

Peyman Mohseni, from August 26, 2008

Erlend Fjøsne Nordstrand

Axel Baumann Ofstad

Silje Rodahl, to June 13, 2008

Espen Rudberg, to March 23, 2008

Birgit Ryningen, to June 30, 2008

Per Martin Rørvik

Dmitry Slizowskiy

Sapthagireesh Subbarayan, from September 10, 2008

Guttorm Ernst Syvertsen, from March 3, 2008

Yufeng Wang, to June 30, 2008

Sophie Beatrice Weber, from June 23, 2008

Øyvind Østrem

EXTERNAL SCHOLARSHIP HOLDERS

Shahid Akhtar

Anawati

Rajorshi Basu, to August 27, 2008

Marte Bjørnsdotter

Yacine Boulfrad, from October 6, 2008

29

Arjan Ciftja

Pierre Delaleau

Jørgen Furu

Hasan Güleryüz, from February 11, 2008

Mehdi Kadkhodabeigi, from April 17, 2008

Maulid Kivambe, from December 1, 2008

Ole Sigmund Kjos

Michal Kolar

Michal Ksiazek, from August 27, 2008

Köksal Kurt, from February 18, 2008

Piotr Ochal, from February 13, 2008

Stian Seim

Esma Senel, from October 27, 2008

Maneesh C. Srivastava, to October 10, 2008

Juan Tan, from March 15, 2008

Kati Tschöpe

Zhaohui Wang

Saijun Xiao

Dongju Zhao

UNDERGRADUATE ASSISTANTS

Spring semester

Vegar Andersen

Michel Brunes Berg

Olav Kigen Bjering

Ingvild Brynjulfsen

Per Kristian Dahlstrøm

Kjersti Meldahl Eide

Espen Erdal

Siri Albertsen Fagerbekk

Jalal Fahadi

Chriss T. R. L. Grimholt

Ragnhild Helene Gulbrandsen

Kjell Inge Halten

Jens Kristian Holmen

Tor Johansen

Halvor Kjærås

Hans Fredrik Nyvold Kvitvang

Eva Landsem

Anders Langva

Ingunn Ramdal

Håvard Reitan

Solveig Rørkjær

Anna Synnøve Ødegård Røstad

Trine Vibeke Salvesen

Aslak Skjeldestad

Kjetil Skjeldestad

Elisabeth Slevolden

Helga Wiig Stangeland

Hanne Kristine Sørgård

Jan Gregor Høydahl Sørli

Morten Tjelta

Knut Omdal Tveito

Birgitte Bårli Vågenes

Espen Tjønneland Wefring

Heidi T. Østby

Vegar Øygarden

Fall semester

Patrick Alknes

Olav Kigen Bjering

Ingvild Brynjulfsen

Andreas Egholm

Kjersti Meldal Eide

Nina Enaasen

Espen Erdal

Chriss T. R. L. Grimholt

Silje Aamodt Haga

Kjell Inge Halten

Alexander Hammersgård

Jens Kristian Holmen

Katja Ekroll Jahren

Joakim Johnsen

Halvor Kjærås

Hans Fredrik Nyvold Kvitvang

Eva Landsem

Ørjan Fossmark Lohne

Erica Marley

Thea Ragna Storesund Mohn

Rolf Heilemann Myhre

Håvard Johnsen Reitan

Solveig Rørkjær

Anna Synnøve Ødegaard Røstad

Trine Vibeke Salvesen

Kjetil Skjeldestad

Lilian Sola Strand

Tor Olav Løveng Sunde

Morten Tjelta

Espen Tjønneland Wefring

Vegar Øygarden

SUMMER STUDENTS

Olav Kigen Bjering

Thomas Brynjulfsen

Sindre Bunkholt

Asle Fredriksen

Astrid Bjørnetun Haugen

Katja Ekroll Jahren

Steinar Jørstad

Fenar Kamlow

stAFF

30

Lone Sjursen Kleveland

Amund Nordli Løvik

Miriam Mekki

Rune Nilsen

Urd Sæther Olden

Malin Sletnes

Jon Strand

Tor Olav Løveng Sunde

Jørgen Svendby

Marit Takla

Paul Tandberg

Morten Tjelta

Vegard Øygarden

APPRENTICE

Jon Michael Love, from August, 2008

Ekrem Yerlikaya, to June, 2008

DEPARTMENT MANAGEMENT

Merethe Falstad/Sigrid Lædre

Trygve Foosnæs

Tor Grande (head)

Øystein Grong

Trond Einar Hagen

Fredrik Haakonsen

Geir Martin Haarberg

Eli Beate Jakobsen

Leiv Kolbeinsen

Ørjan Fossmark Lohne

Knut Marthinsen (deputy head)

Pål Ulseth

ADVISORY BOARD

Lars Arnberg

Mari-Ann Einarsrud

Merethe Falstad/Sigrid Lædre

Trond Einar Hagen (Secretary)

Odd Sture Hopperstad

Fredrik Haakonsen/Lars Erik Owe

Ørjan Fossmark Lohne

Brit Wenche Meland

Kemal Nisancioglu

Aud Nina Wærnes (chair)

SUBSTITUTES

Geir Martin Haarberg

Leiv Kolbeinsen

Kjell Wiik

stAFF

31

During 2008, 72 Dr.ing./PhD students have worked at Department of Materials Science and Engineering.

10 students have been awarded the degree Dr.ing./PhD.

Per Anders Eidem: Electrical resistivity of coke beds.Doctoral thesis 2008:279, IMT-report 2008:104. October 2008.

Major subject: Extractive metallurgy.Dr. lecture: Theeffectsofzinkandalkaliesontheheat-andmassflowintheferromanganesefurnace.Thesis advisor: Professor, Dr.ing. Merete Tangstad.Co-supervisor: Senior Scientist Magne Runde, SINTEF Energy Research, Trondheim, Norway.Examination committee: Professor Paulo von Krüger, Universidade Federal de Ouro Preto, Ouro Preto-MG, Brazil.

Dr.ing. Jan Anders Sæter, RDM, Mo i Rana, Norway.Professor, Dr.ing. Øystein Grong (chair).

Lina M. Jonasson: Electrochemical formation of nanostructures in cryolitic melts.Doctoral thesis 2008:242, IMT-report 2008:102. August 2008.

Major subject: Inorganic chemistry.Dr. lecture: Carbon nanocompounds - Fundamental properties and practical applications.Thesis advisor: Professor, Dr.ing. Trygve Foosnæs.Co-supervisor: Professor emeritus, Dr.techn. Harald A. Øye.Examination committee: Professor Rolf W. Berg, Department of Chemistry, Technical University of Denmark, Lyngby,

Denmark. Chief Engineer Halvor Kvande, Hydro Aluminium AS, Oslo, Norway.Professor, Dr.ing. Martin Ystenes (chair).

Rannveig Kvande: Incorporation of impurities during directional solidification of multicrystalline silicon for solar cells.Doctoral thesis 2008:71, IMT-report 2008:98. February 2008.

Major subject: Physical metallurgy.Dr. lecture: Challenges in the production of carbothermically reduced silicon.Thesis advisor: Professor, PhD Lars Arnberg.Co-supervisor: Professor, Dr.philos. Otto Lohne.Examination committee: Professor, Dr. Hans Joachim Möller, Institute for Experimental Physics, TU Bergakademie,

Freiberg, Germany.VP R&D, Dr.ing. Øyvind Nielsen, NorSun AS, Oslo, Norway.Professor, Dr.ing. Merete Tangstad (chair).

Viktor Myrvågnes: Incorporation of impurities during directional solidification of multicrystalline silicon for solar cells.Doctoral thesis 2008:71, IMT-report 2008:98. February 2008

Major subject: Physical metallurgy.Dr. lecture: Challenges in the production of carbothermically reduced silicon.Thesis advisor: Professor, PhD Lars Arnberg.Co-supervisor: Professor, Dr.philos. Otto Lohne.Examination committee: Professor, Dr. Hans Joachim Möller, Institute for Experimental Physics, TU Bergakademie,

Freiberg, Germany.VP R&D, Dr.ing. Øyvind Nielsen, NorSun AS, Oslo, Norway.Professor, Dr.ing. Merete Tangstad (chair).

Birgit Ryningen: Formation and growth of crystal defects in directionally solidified multicrystalline silicon for solar cells.Doctoral thesis 2008:103. October 2008.

Major subject: Physical metallurgy.Dr. lecture: Solar cell wafer cutting technologies.Thesis advisor: Professor, Dr.philos. Otto Lohne.Co-supervisor: Professor, PhD Lars Arnberg.

GrAdUAte stUdiesDr.ing./PhD Degrees

32

GrAdUAte stUdies

Examination committee: Professor, Torbjörn Carlberg, Department of Natural Sciences, Engineering and Mathematics, Mid-Sweden University, Sundsvall, Sweden.Dr.ing. Katrin Nord-Varhaug, Technology Department, REC Scanwafer AS, Porsgrunn, Norway.Professor, Dr.philos. Jan Ketil Solberg (chair).

Per Martin Rørvik: Synthesis of ferroelectric nanostructures.

Doctoral thesis 2008:321, IMT-report 2008:106. October 2008.Major subject: Inorganic chemistry.Dr. lecture: Nanostructured materials for high efficiency photovoltaics.Thesis advisor: Professor, Dr.ing. Mari-Ann Einarsrud.Co-supervisor: Professor Dr.ing. Tor Grande.

Professor Thomas Tybell, Department of Electronics and Telecommunications, NTNU, Norway.Examination committee: Professor Nava Setter, Ceramics Laboratory of the Swiss Federal Institute of Technology,

Lausanne, Switzerland.Associate professor, Dr.scient. Ola Nilsen, Department of Chemistry, University of Oslo, Oslo, Norway.Associate Professor, Dr.ing. Jens-Petter Andreassen, Department of Chemical Engineering, NTNU (chair).

Espen Sandnes: The anode process on carbon in chloride-oxide melts.Doctoral thesis 2008:120.

Major subject: Electrochemistry.Dr. lecture: Electrodeposition of metals from room temperature ionic liquids.Thesis advisor: Professor, Dr.ing. Geir Martin Haarberg.Co-supervisor: Professor emeritus Reidar Tunold.

Professor Adolf Kisza, Faculty of Chemistry, University of Wroclaw, Wroclaw, Poland.Examination committee: Professor Pierre Taxil, Universitè Paul-Sabatier, Toulouse, France.

Professor Masatsugu Morimitsu, Doshisha University, Kyoto, Japan.Professor, PhD Kemal Nisancioglu (chair).

Przemyslaw Szczygiel: Characterization of recycle-like Al-Si alloys processed by severe plastic deformation.Doctoral thesis 2008:277, IMT-report 2008:105. November 2008.

Major subject: Physical metallurgy.Dr. lecture: Materialflowpathsinthemetalrecyclingmarketwithspecialemphasisonaluminiumalloys

- status and trends.Thesis advisor: Professor, Dr.techn. Hans Jørgen Roven.Examination committee: Professor, Dr. Marco J. Starink, Materials Research Group, School of Engineering Sciences,

University of Southampton, United Kingdom.Professor, Dr. Maria Richert, Department of Structure & Mechanics of Solids, Faculty of Non-ferrous Metals, AGH University of Science and Technology, Krakow, Poland.Senior Metallurgist, Dr.ing. Ola Jensrud, Raufoss Technology & Industrial Management, Raufoss, Norway.Professor, Dr.ing. Knut Marthinsen (chair).

Kristin Vasshaug: The influence of the formation and dissolution of aluminium carbide on the cathode wear in aluminium electrolysis cells.Doctoral thesis 2008:106, IMT-report 2008:99. March 2008.

Major subject: Electrochemistry.Dr. lecture: Future challenges in the production of solar grade silicon: Comparision of electrochemical

methods with current industrial practices.Thesis advisor: Professor, Dr.ing. Geir Martin Haarberg.Co-supervisor: Professor, Dr.ing. Trygve Foosnæs.Examination committee: Professor Donald R. Sadoway, Department of Materials Science and Engineering,

Massachusetts Institute of Technology, Cambridge, Massachusetts, USA.Chief Engineer Halvor Kvande, Hydro Aluminium AS, Oslo, Norway.Adjunct Professor Knut Arne Paulsen (chair).

Torjus Åkre: Electrowinning of cobalt from chloride solutions: Anode deposition of cobalt oxide on DSA®.Doctoral thesis 2008:172, IMT-report 2008:101. April 2008.

Major subject: Electrochemistry.Dr. lecture: Electrochemical methods for wastewater treatment.

33

GrAdUAte stUdies

Thesis advisor: Professor, Dr.ing. Geir Martin Haarberg.Co-supervisor: Research Scientist Sarbjyot Haarberg, SINTEF Marintek, Trondheim, Norway.Examination committee: Professor Olof Forsen, Helsinki University of Technology, Espoo, Finland.

Dr. Alberto Gonzalez, Applied Research and Technology Group, Teck Cominco Metals Ltd., Vancouver, Canada.Professor emeritus Reidar Tunold (chair).

Dr.ing./PhD projects in progress

Name and Title Thesis advisor

Madhubabu Abburi Electrochemical texturization of Si-wafers. Kemal Nisancioglu

Shahid Akhtar Hydrogen porosity in aluminum castings. Lars Arnberg

Anawati Effect of trace elements on the electrochemistry and corrosion of aluminium alloys. Kemal Nisancioglu

Sarina Bao Purification of aluminum through filtration. Merete Tangstad

Marte Bjørnsdotter Effect of surface conditions on hydrogen uptake during cathodic protection of steel in seawater. Kemal Nisancioglu

Yacine Boulfrad Investigation of the edge zone of multichrystalline silicon ingots for solar cells. Eivind J. Øvrelid

Stein Trygve Briskeby Electrocatalysts of noble metals supported on carbon nanofibres. Svein Sunde

Arjan Ciftja Recycling to feedstock of photo voltaic silicon scrap by removal of inclusions; effect of refractory materials and wettabilities.

Merete Tangstad

Jirang Cui Recovery of metals from electronic wastes. Hans Jørgen Roven

Per Kristian Dahlstrøm Electrooxidation of small organic molecules. Frode Seland

Halvor Dalaker Thermodynamics of solar cell silicon in the high temperature area. Merete Tangstad

Mahdi Darab Synthesis and durability enhancement of CNT based MEAs for PEMFC. Svein Sunde

Pierre Delaleau Equiaxed dendrite growth in aluminium alloys. Lars Arnberg

Ole-Kristian Eide IR and NMR spectroscopy of catalyst for olefin polymerization. Martin Ystenes

Tomas Laugsand Erlien Cold bonding mechanisms in aluminium alloys. Øystein Grong

Egil Fjeldberg Modelling and simulation of nano- and microstructure in Al-alloys. Knut Marthinsen

Odd Einar Frosta Modeling of baked anodes. Trygve Foosnæs

Jørgen Furu Remelting and recycling of aluminum scraps. Knut Marthinsen

Nils Håvard Giskeødegård Adhesion of organic functional groups on aluminium. Kemal Nisancioglu

Brit K. F. Graver Electrochemical activation of aluminium by surface segregation of trace elements indium, tin and lead.

Kemal Nisancioglu

Hasan Güleryüz Investigation of the mechanisms governing the deposition of sol particles on a substrate. Mari-Ann Einarsrud

34

Harald Görner Development of an AlF3 active filter for Al. Lars Arnberg

Sidsel Meli Hanetho Coating and surface modification of multiphase pipelines. Mari-Ann Einarsrud

Raimo Helenius High pressure die casting of light metals. Otto Lohne

Fredrik Haakonsen Optimizing of Strømhard austenitic manganese steel. Jan Ketil Solberg

Liudmila Ilyukhina Rational design of mixed oxide catalysts for PEM water electrolysis. Svein Sunde

Morten Sundheim Jensen Chemical degradation, wetting and electrochemical properties of polycrystalline TiB2 inert cathodes. Tor Grande

Mehdi Kadkhodabeigi Modeling of tap hole phenomenon in ferroalloys production furnaces. Halvard Tveit

Morten Karlsen Thermo-mechanical in-situ investigations using the EBSD. Jarle Hjelen

Kenji Kawaguchi Electrocatalysis and novel functions of IrO2-based electrodes. Geir Martin Haarberg

Ole Sigmund Kjos Electrochemical production of titanium from molten salts. Geir Martin Haarberg

Michal Kolar Deformation and precipitation in Al-Mg-Si-(Cu) alloys. Knut Marthinsen

Michal Ksiazek Thermal conductivity in ores. Merete Tangstad

Köksal Kurt Effect of thermomechanical treatment on trace element segregation and electrochemical activation of commercial and model aluminium alloys.

Kemal Nisancioglu

Eirin Kvalheim Electrode kinetics of anode processes on candidate inert anode materials for oxygen evolution during electrowinning in molten salts.

Geir Martin Haarberg

Magnus Hurlen Larsen Effect of composition and thermomechanical processing on the intergranular corrosion of AA6000 aluminium alloys.

Kemal Nisancioglu

Sten Yngve Larsen Novel carbon materials in electrometallurgical applications. Trygve Foosnæs

Ingrid Anne Lervik Electrocatalyst for PEM water electrolysis. Svein Sunde

Anders Sunde Lilleby MathematicalmodellingofmaterialflowduringextrusionandjoiningofaluminiumbasedontheHYMEN bonding method.

Øystein Grong

Jan Lindgård Alkali Silica Reactions (ASR) - performance based testing concept. Harald Justnes

Francesco Madaro Synthesis of textured piezo- and ferroelectric materials by chemical and ceramic techniques. Tor Grande

Chiara Modanese Investigation of new Si solar cells feedstock. Lars Arnberg

Peyman Mohseni Brittle and ductile fracture of arctic steels. Jan Ketil Solberg

Erlend Fjøsne Nordstrand Effects of non-metallic inclusions on the transformation behaviour of steel. Øystein Grong

Piotr Ochal Core-shell electrocatalysts for oxidation of small organic molecules. Svein Sunde

Axel Baumann Ofstad Increasing the lifetime of PEM fuel cells - a fundamental study of degradation mechanisms. Svein Sunde

GrAdUAte stUdies

35

Morten Andreas Onsrud Production and characterization of carbon cones. Trygve Foosnæs

Lars-Erik Owe Oxide electrocatalysts for the oxygen evolution reaction during water electrolysis. Svein Sunde

Ove Bjørn Paulsen Sealing of high temperature membrane reactors. Tor Grande

Andrey Poletaev Nanostructured hydrides of aluminium and magnesium for hydrogen storage. Jan Ketil Solberg

Silje Rodahl Chromate-free pre-treatment of aluminium for organic coating. Kemal Nisancioglu

Magnus Rotan Phase composition, microstructure and resistance to attrition of alumina-based supports for Fischer-Tropsch catalysts.

Tor Grande

Espen Andre Rudberg Oxygen exchange on functional oxide membranes. Kemal Nisancioglu

Stein Rørvik Migration effects in prebaked anodes. Trygve Foosnæs

Stian Seim Slag properties and phase relations in the Ti-industry. Leiv Kolbeinsen

Sverre Magnus Selbach Size and strain effects in ferroelectric and piezoelectric materials. Tor Grande

Esma Senel Effect of trace elements on surface properties of aluminium alloys. Kemal Nisancioglu

Dmitry Slizowskiy Use of waste materials for ferromanganese production. Merete Tangstad

Karl Gunnar Solheim Theeffectofmicrostructureonthepropertiesof13%Crflowlinesinoperation. Jan Ketil Solberg

Isac Sorin Metal powder project - “metal printing process”.

Lars Arnberg

Maneesh C. Srivastava High pressure die casting of aluminium and magnesium alloys. Otto Lohne

Guttorm Ernst Syvertsen Synthesis and characterisation of nanostructured fuel cells based on proton conductors. Tor Grande

Juan Tan Effect of trace elements tin and indium on aluminium model alloy. Kemal Nisancioglu

Kati Tschöpe FEM modelling of degradation of cathode lining in Hall-Heroult cells. Tor Grande

Yufeng Wang Purification of aluminum through electromagnetic field. Merete Tangstad

Zhaohui Wang Mathematical models for degradation of cathode lining in Hall-Heroult cells. Tor Grande

Sophie Beatrice Weber Ceramic thermal barrier coatings. Mari-Ann Einarsrud

Saijun Xiao Gas anode for metal electrowinning. Geir Martin Haarberg

Dongju Zhao Processing, properties and performance in use of direct reduced iron pellets containing added material to control steel structure.

Leiv Kolbeinsen

Xiangjun Zuo Recycling of the electronic waste. Hans Jørgen Roven

Cecilie Ødegård Conversion of silicon tetrachloride to trichlorosilane. Trygve Foosnæs

Øyvind Østrem Cathode wear in industrial aluminium electrolysis cells. Christian Rosenkilde

GrAdUAte stUdies

36

Dr.ing./PhD projects co-supervised in other departments

Name and Title Thesis advisor

Dag Herman Andersen Thermo-electrical-mechanical models for anode carbon cracking. Zhiliang Zhang (Department of

Structural Engineering, NTNU) and Trygve Foosnæs

Eleni Arvaniti Soil stabilization and waterproofing of concrete constructions. Alkiviades Payatakes (Department

of Chemical Engineering, University of Patras, Patras, Greece) and Terje Østvold

Jinbao Lin SPD by CEC of magnesium alloys. Qudong Wang (Shanghai Jiao Tong

University, China) and Hans Jørgen Roven

Efstathios Ntafalias Investigation on the possibility to control water permeability of concrete. Petros G. Koutsoukos (FORTH-

ICEHT and Department of Chemical Engineering, University of Patras, Patras, Greece) and Terje Østvold

Maria Psarrou Protecting soil from water erosion through precipitation of calcium phosphate. Alkiviades Payatakes (Department

of Chemical Engineering, University of Patras, Patras, Greece) and Terje Østvold

Peter Schmidt Hollow castings produced by LPDC. Jürgen Bast (T. U. Bergakademie,

Freiberg, Germany) and Lars Arnberg

Ragnhild Kjæstad Sæterli Electronic structure of thermoelectric materials - TEM studies at the nanos-cale.

Randi Holmestad (Department of Physics, NTNU) and Knut Marthinsen

Zhipeng Zeng Study on the ECAP process for commercially pure titanium. Stefan Jonsson (Department of

Materials Science and Engineering, KTH, Stockholm, Sweden) and Hans Jørgen Roven

Ida Westermann Mechanical properties of 7xxx alloys - effect of precipitates and elements in solid solution, strain, strain path and strain rate.

Odd Sture Hopperstad (Department of Structural Engineering, NTNU), Bjørn Holmedal and Knut Marthinsen

GrAdUAte stUdies

37

Descriptions of the courses offered at the Department of Materials Science and Engineering are included in the

University Course Catalogue that can be obtained from Student and Academic Section, NTNU. The present survey

lists the courses given by our scientific staff.

Course no. Semester:Spring=S

Autumn=A

TitleCredits in parenthesis

Lectures and exercise coordinators Passed/ Started

TMT4106 S General Chemistry (7.5) M. Ystenes 369/308

TMT4110 S General Chemistry (7.5) T. Grande 179/174

TMT4120 S General Chemistry 2 (7.5) T. Foosnæs 78/78

TMT4130 S Inorganic Chemistry (7.5) H. L. Lein, T. Grande 79/78

TMT4140 S Applied Thermodynamics (7.5) T. Østvold, T. Haug-Warberg 3/1

TMT4150 S Refractories (7.5) K. Wiik 13/11

TMT4165 S Materials- and Electro Chemistry, proj. (7.5) K. Wiik 21/21

TMT4175 S Materials Technology 2 (7.5) Ø. Grong, K. Marthinsen, O. Lohne 21/21

TMT4206 S Fluid and Heat Transfer, Intr. Course (7.5) M. Tangstad, R. Kristoffersen, H. F. Svendsen

19/15

TMT4210 S Material and Process Modelling (7.5) K. Marthinsen 38/38

TMT4215 S Casting (7.5) L. Arnberg 27/18

TMT4225 S Mechanical Properties of Eng. Mat. 2 (7.5) Ø. Grong, K. Marthinsen, H. J. Roven 3/3

TMT4230 S Metallurgical Engineering (7.5) J. A. Bakken 1/1

TMT4240 S Microstructure and properties of Metals (7.5) J. K. Solberg 21/18

TMT4245 S Functional Materials (7.5) H. L. Lein 16/12

TMT4250 S Electrochemistry, basic course (7.5) G. M. Haarberg 45/40

TMT4260 S Phase Transformations in Metals (7.5) K. Marthinsen, Ø. Grong 5/5

TMT4265 S MaterialsTechn.-Forming Light Metals (7.5) H. J. Roven, O. Jensrud, O. Reiso 5/5

TMT4275 S Thermodynamics and Phasediagrams (7.5) L. Kolbeinsen 16/16

TMT4285 S Hydrogen Techn., Fuel/Solar Cells (7.5) S. Sunde 53/47

TMT4310 S Electrocatalysis and Energy Techn. (7.5) F. Seland 12/8

TMT4315 S Electrochemical Engineering (7.5) K. Nisancioglu 5/5

TMT4500 S Materials Technology, special project (15.0) 4/4

TMT4851 S Experts in Team (7.5) T. Foosnæs 18/18

TMT4900 S Master thesis, Spec. in Materials Chemistry and Energy Techn. (30.0)

17/17

TMT4905 S Master thesis, Materials Techn. (30.0) 17/16

TMT5100 S Electrolysis of Light Metals 2 (7.5) K. A. Paulsen 7/7

TMT4100 A General Chemistry (7.5) M. Ystenes 315/256

TMT4115 A General Chemistry 1 (7.5) T. Foosnæs 86/86

TMT4145 A Ceramic Engineering (7.5) M-A. Einarsrud 27/27

TMT4155 A Heterogen Equilibria/Phase Diagrams (7.5) T. Grande 54/46

TMT4170 A Materials Technology 1 (7.5) H. J. Roven, M. Tangstad 28/26

TMT4185 A Materials Technology (7.5) J. Hjelen, L. Arnberg 77/72

TMT4190 A Applied Materials Technology (7.5) O. Lohne, K. H. Holthe 24/24

TMT4222 A Mechanical Properties of Metals 1 (7.5) B. Holmedal 24/21

CoUrse ProGrAm

38

TMT4240 A Microstructure and Properties of Metals (7.5) J. K. Solberg 28/27

TMT4253 A Electrochemical Process- and Energy Technology (7.5)

F. Seland 19/18

TMT4255 A Corrosion and Corrosion Protection (7.5) K. Nisancioglu, R. Johnsen 30/29

TMT4280 A Extractive Metallurgy (7.5) L. Kolbeinsen 3/3

TMT4292 A Materials- and Surface Chemistry (7.5) S. Sunde, K. Wiik 25/24

TMT4305 A Electrometallurgy (7.5) M. Tangstad, H. Tveit 7/7

TMT4320 A Nanomaterials (7.5) F. Vullum 49/44

TMT4325 A Refining and Recycling of Metals (7.5) E. Øvrelid 10/10

TMT4500 A Materials Technology, special project (15.0) K.Wiik, T. Foosnæs, H.J. Roven, S. Sunde, R. Johnsen

32/32

TMT4505 A Materials Technology, special course (7.5) Several teachers at the department 37/37

TMT5500 A Process Metallurgy and Electrolysis, special project (15.0)

T. Østvold, T. Foosnæs 6/5

TMT5505 A Process Metallurgy and Electrolysis, special course (7.5)

Several teachers at the department 6/6

MT8100 S Transport Phenomena (7.5) K. Nisancioglu 6/6

MT8102 S Corrosion and Surface Technology (7.5) K. Nisancioglu 1/1

MT8103 S Semiconductor Electrochemistry (7.5) S. Sunde 7/7

MT8104 S Electrolysis of Light Metals 1 (7.5) K. A. Paulsen, G. M. Haarberg 4/4

MT8105 S Electrochemical Energy Technology (7.5) F. Seland 1/1

MT8201 S Advanced Electrometallurgy (7.5) M. Tangstad, H. Tveit 4/4

MT8205 S Metallurgical Modelling of Welding Ø. Grong 2/2

MT8206 S Iron and Steel Metallurgy (7.5) Ø. Grong 1/1

MT8207 S Electron Microscopy (7.5) J. K. Solberg 14/12

MT8209 S Failure Analysis of Metals (7.5) J. K. Solberg 1/1

MT8300 S Electrolysis of Light Metals 2 (7.5) K. A. Paulsen 2/2

MT8301 S Carbon Materials Technology (7.5) M. Sørlie 6/6

MT8305 S Cement Semestry (7.5) H. Justnes 1/1

MT8306 S Advanced Ceramics Processing (7.5) M.-A. Einarsrud 8/7

MT8308 S Advanced Solid State Chemistry (7.5) T. Grande 5/5

MT8205 A Metallurgical Modelling of Welding (7.5) Ø. Grong 1/1

MT8210 A Advanced Solidification Metallurgy (7.5) L. Arnberg 6/6

MT8213 A Modelling and Simulation of Microstructure and Properties (7.5)

K. Marthinsen 1/1

MT8215 A Dislocation Theory Applied to Thermo-Mechanical Treatments (7.5)

B. Holmedal 3/3

MT8217 A Kinetics of Metallurgical Reactions (7.5) L. Kolbeinsen 3/3

MT8300 A Electrolysis of Light Metals 2 (7.5) K. A. Paulsen 2/2

MT8307 A Thermodynamics of Metals (7.5) T. Grande 5/5

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39

Master of Science in Materials Technology (5 years)Autumn semester

3rd year

Eirik Belland

Tor Arne Buberg

Jens Erik Davidsen

Sofie Drågen

Solveig Egtvedt

Jan Gaute Frydendahl

Preben Kjos Gabrielsen

Aleksander Rise Gallala

Anne-Jorunn Hausken

Ruth Oftedal Herikstad

Håkon Trygve Strøm Jørgensen

Steinar Jørstad

Bjarte Åstveit Nygård

Petter Ottesen

Jonas Hovde Pedersen

Mads Reiten

Trine Viveke Salvesen

4th year

Vegard Andersen

Svein Prestrud Astad

Olav Kigen Bjering

Lars-Petter Bjørkeng

Tor Henning Bjørnå

Kristian Karlsen Brende

Thomas Brynjulfsen

Sindre Bunkholt

Kristian Nyborg Dahl

Ørjan Aronsen Ellingsen

Ann Leni Haugstad

Steinar Lauvdal

Amund Nordli Løvik

Ingeborg Johannesen Odland

Eirik Andersen Rotevatn

Magnus Skjellerudsveen

Gunstein Skomedal

Hans Magne Torseth

Phung Hieu Dinh Tran

Knut Omdal Tveito

5th year

Patrick Alknes

Elena Bai (student from Italy)

Ingvild Brynjulfsen

Andreas Egholm

Terje Hals

Morten Ro Helsem

Katja Ekroll Jahren

Fenar Kamlow

Kristoffer Kløgetvedt

Ørjan Fossmark Lohne

Christoffer Vikne Moen

Rune Nilsen

Trygve Ottemo Nordby

Thomas Odd

Richard Hagvåg Ringstad

Boots Christoffer Demez Rosario

Yngve Rønning

Erling Gjestvang Schrøder

Vaseeharan Sivaneesan

Knut Erik Snilsberg

Marte Aadland Sørensen

Graduated Master of Technology studentsSpring semester

Elin Christine Andersen

Kristoffer Brinchmann

Thien Thanh Nguyen Cao

Torbjørn Engebretsen

Hans Ove Tinnan Hagen

Tore Helland

Tor Johansen

Elise Tverberg Nordnes

Dag Rønningen

Elisabeth Slevolden

Helga Wiig Stangeland

Stian Strømstad

Guttorm Ernst Syvertsen

Mario Kokolakis Søfferud

Håvard Vingsand

Master of Science in Chemistry and Biotechnology, Specialization in Materials Chemistry and Energy TechnologyAutumn semester

3rd year

Inga Askestad

Inger Marie Bjørnevik

Marthe Emilie Melandsø Buan

Kai Erik Ekstrøm

Jarl Erik Morsund Flatøy

Ragnhild Helene Gulbrandsen

Håkon A Holm Gundersen

Lise Jemblie

Sigrid Lædre

Håvard Mølnås

Anita Reksten

Kristian Grøtta Skorpen

Halfdan Kristoffer Småbråten

Camilla Sommerseth

Øyvind Sunde Sortland

Mari Lovise Torp

Magnus Weberg

Espen Tjønneland Wefring

Ole Jørgen Østensen

Åsne Århus

4th year

Henrik Klitgaard Bostad

Tone Beate Heiaas Bukholm

Torbjørn Cederløv

Ingelin Clausen Endsjø

Helle Ervik Fossheim

Mette Grorud

Øystein Grøtting

Victoria Leivestad

Knut Åge Meland

Urd Sæther Olden

Solveig Rørkjær

Marianne Charlotte Simonsen

Ragne Marie Skarra

Ingrid Stamnes

Jørgen Svendby

Henrik Åsheim

m.sc. stUdeNts

40

m.sC. stUdeNts

5th year

Hanne Flåten Andersen

Astrid Bakken

Marianne Elisabeth Berg

Kristin Bergum

Torunn Kringlen Ervik

Carl Eik Lie Foss

Silje Aamot Haga

Astri Bjørnetun Haugen

Caroline Ramstad

Malin Sletnes

Tor Olav Løveng Sunde

Paul Bragelien Tandberg

Morten Tjelta

Mari Voldsund

Vegar Øygarden

Graduated Master of Technology students Spring semester

Maren Bjørnstad

Aleksander R. M. Brandtzæg

Per Kristian Dahlstrøm

Tine Eikevik

Merethe Falstad

Asle Fredriksen

Magnus Torleif Rune P. Halvorsen

Caroline Holme

Kristine Uberg Nærland

Morten Andreas Onsrud

Øystein Edland Pedersen

Ingunn Ramdal

Aslak Skjeldestad

Ida Svanberg

Camilla Skotnes Wollan

Michelle Cecilia Ystad

Heidi Therese Østby

Master of Technology in Materials Technology (2 years)(Master Programme in Materials

Technology for Engineers)

Autumn semester

1st year

Anders Welde Gjennes (part time)

Line Sunde Lilleby

Svein Arne Pedersen (part time)

Zeinab Sharifi

2nd year

Aws Yonis Faisal

Anita Hansen

Per Fredrik Rosenqvist

Graduated Master of Technology students

Spring semester

Torje Mathisen

Master of Science Program in Light Metals Production Autumn semester

1st year

Andrews Adjei (Ghana)

Joseph Prince Armoo (Ghana)

Thomas Hartmut Ludwig (Germany)

2nd year

Mohsen Dehghan-Niri (Iran)

Yohannes Addis Desta (Ethiopia)

Tone Eilertsen (Norway)

Finnur Flosason (Iceland)

Alex Luyima (Uganda)

Emmanuel Nyankson (Ghana)

Graduated Master of Technology students

Spring semester

Benjamin Agyei-Tuffour (Ghana)

Wondowsen Abebe Aregawi (Ethiopia)

Jens Fladerer (Germany)

Samuel Senanu (Ghana)

Chunming Tan (China)

Eric Barimah Twum (Ghana)

Michael Yanney (Ghana)

Master of Science Program in Silicon and Ferroalloy ProductionAutumn semester

1st year

Stephen Caesar Lobo (Canada)

Foreign guest students at Department of Material Science and EngineeringSpring and autumn semester

Oliver Baptiste Gabriel Astruz

(France)

Ayke Augustin (Germany)

Elena Bai (Italy)

Thiemo Brüggemann (Germany)

Wu Chen (China)

Mehdi Patrice Djame Cherfaoui

(France)

Hèlène Clogenson (France)

Jaroslava Davidova (Czech Republic)

Franziska Dietel (Germany)

Amèlie Dieudionne (France)

Christian Fink Elkjær (Denmark)

Petit Florent (France)

Mohammad Haj Mohammadian

Baghban (Iran)

Thomas Huger (France)

Christian Junglewitz (Germany)

Dong-Ho Kim (South Korea)

Moojun Kim (South Korea)

Simon Klein (Germany)

Carina Kreutner (Germany)

Joon Kwon (South Korea)

Apolline Leclerc (France)

Guillaume Majeau-Bettez (Canada)

Bastien Mercenier (Belgium)

Bjørn Duus Mikkelsen (Denmark)

Amaury Laine (France)

Yun Joo Nam (Republic of Corea)

Martin Repka (Czech Republic)

Hari Kishor Sah (Nepal)

Sebastino Scacchetti (Italy)

Veronica Schiavon (Italy)

Marco Tommaselli (Italy)

Adeline Vincent (France)

Seongjin Yu (South Korea)

Tina Zscherpe (Germany)

Haitao Zhou (China)

41

GrAdUAted m.sC. stUdeNts With titLes oF their diPLomA WorKs

ElEctrochEmistryName and title Supervisor and examiner

Per Kristian Dahlstrøm Verification of a new conseptfor electrochemical hydrogen compression.

Supervisor: Associate Professor Frode Seland.Examiner: Dr.ing. Magnus Thomassen, SINTEF, Trondheim.

Torbjørn Engebretsen Supply of dissolved oxygen by water electrolysis in Lake Biwa.

Supervisor: Professor Geir Martin Haarberg.Examiner: Professor emertitus Reidar Tunold.

Merethe Falstad Corrosion inhibiting coating on steel – Longterm characteristic on zinc-rich coating on steel with varying surface finish.

Supervisor: Professor Kemal Nisancioglu.Examiner: Associate Professor Håvard Karoliussen, Sør-Trøndelag University College.

Ingunn Ramdal Sea water battery with long lifetime.

Supervisor: Professor Kemal Nisancioglu.Examiner: Associate Professor Håvard Karoliussen, Sør-Trøndelag University College.

Camilla Skotnes Wollan Study of anodic chlorine evolution on titanium- and titanium based anodes.

Supervisor: Associate professor Frode Seland.Examiner: Dr.ing. Magnus Thomassen, SINTEF, Trondheim.

Michelle Cecilia Ystad Electrochemical impedance spectroscopy on organic coatings.

Supervisor: Professor Svein Sunde.Examiner: Dr.ing. Astrid Bjørgum, SINTEF, Trondheim.

EXTRACTIVE METALLRUGYName and title Supervisor and examiner

Hans Ove Tinnan Hagen Boron removal form molten sililscon by slag refining.

Supervisor: Professor Merete Tangstad.Examiner: Dr.ing. Gabriella Tranell, SINTEF, Trondheim.

INORGANIC CHEMISTRYName and title Supervisor and examiner

Aleksander Richard Merkesvik Brandtzæg Anodes made from coke calcined under anode baking furnace conditions, a quality and economical evaluation.

Supervisor: Professor Trygve Foosnæs.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

Morten Andreas Onsrud Production and characterization of carbon nanocones.

Supervisor: Professor Trygve Foosnæs.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

Aslak Skjeldestad Production, characterization and application of conical carbon nanostructuresin carbon anodes.

Supervisor: Professor Trygve Foosnæs.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

Guttorm Ernst Syvertsen Development and testing of anode- and cathode materials intended for SOFCs based on proton conducting electrolytes.

Supervisor: Professor Kjell Wiik.Examiner: Professor Truls Nordby, University of Oslo, Oslo.

PHYSICAL METALLURGYName and title Supervisor and examiner

Antonio Alvaro Structure development in a martensitic stainless steel and its effects on toughness.

Supervisor: Professor Jan Ketil Solberg.Examined at theUniverità Politecnica delle Marche, Italy.

Ayke Augustin Plastic deformation in ultrafine grained aluminium alloys processed by ECAP-I.

Supervisor: Professor Hans Jørgen Roven.Examined at the TU-Freiberg, Germany.

42

Mads Aursand Characterization and performance assessment of refurbished Renè 80 gas turbine blades.

Supervisor: Professor Jan Ketil Solberg.Examined at the Department of Engineering Design and Materials.

Maren Bjørnstad Investigation of the detrimental effect of nickel on the sulfide stress cracking resistance of low alloy steels.

Supervisor: Professor Jan Ketil Solberg.Examiner: Siv.ing. Bjørn Borchgrevink, Oslo.

Kristoffer Brinchmann Joint for high modulus composite rods.

Supervisor: Professor Andreas Echtermeyer, Department of Engineering Design and Materials. Examined at the Department of Engineering Design and Materials.

Thanh Thien Nguyen Cao Biofilm formation on stainless steel.

Supervisor: Professor Kemal Nisancioglu.Examiner: Associate Professor Håvard Karoliussen, Sør-Trøndelag University College.

Tine Christin Eikevik Removal of silicon carbid in liquid silicon for solarcell purpose.

Supervisor: Professor Øystein Grong.Examiner: Associate Professor Hallstein Hemmer, Sør-Trøndelag University College.

Tore Helland Experimenantal and numeral study on the nano-mechanical properties of polymer particles.

Supervisor: Professor Zhilang Zhang, Department of Structural Engineering. Examined at the Department of Structural Engineering.

Tor Johansen Properties of coatings and pulseplasma nitrided surfaces ex-posed to corrosion and wear.

Supervisor: Professor Roy Johnsen, Department of Engi-neering Design and Materials. Examined at the Department of Engineering Design and Materials.

Torje Mathisen Physical-metallurgical investigation of steel for arctic contruc-tion purpose.

Supervisor: Professor Hans Jørgen Roven.Examiner: Dr.ing. Marianne Videm, Force Technology, Trondheim.

Elise Tverberg Nordnes Metal-composite interface for offshore-oil and gas risers.

Supervisor: Associate Professor Nils Petter Vedvik, De-partment of Engineering Design and Materials. Examined at the Department of Engineering Design and Materials.

Kristine Uberg Nærland Investigation of the causes for red zone in multicrystallization silicon.

Supervisor: Professor Lars Arnberg.Examiner: Dr.ing. Ragnar Fagerberg, SINTEF, Trondheim.

Øystein Edland Pedersen How to minimalize the use of solvent based adhesives for cor-rosion protection with rubber polymers in order to reduce the strain on health and environment.

Supervisor: Professor Jan Ketil Solberg.Examiner: Dr.ing. Ragnar Gjengedal, Corus Packaging, Bergen.

Dag Rønningen Failure analysis of cold deformed super duplex stainless steel.

Supervisor: Professor Christian Thaulow, Department of Engineering Design and Materials. Examined at the Department of Engineering Design and Materials.

Elisabeth Slevolden Characterization of phases and corrosion products in nickel based alloys exposed to high temperature corrosion.

Supervisor: Professor Øystein Grong.Examiner: Associate Professor Hallstein Hemmer, Sør-Trøndelag University College.

Helga Wiig Stangeland Cathodic protection in cold climate –current density require-ments of calcareous deposits.

Supervisor: Professor Roy Johnsen, Department of Engi-neering Design and Materials. Examined at the Department of Engineering Design and Materials.

Stian Strømstad Brittle fracture in arctic steels.

Supervisor: Professor Christian Thaulow, Department of Engineering Design and Materials. Examined at the Department of Engineering Design and Materials.

GrAdUAted m.sC. stUdeNts With titLes oF their diPLomA WorKs

43

GrAdUAted m.sC. stUdeNts With titLes oF their diPLomA WorKs

Ida Svanberg Translation elements and swiv subsea use.

Supervisor: Professor Roy Johnsen, Department of Engi-neering Design and Materials. Examined at the Department of Engineering Design and Materials.

Mario Kokolakis Søfferud High-speed EBSD and characterization of supermartensitic stainless steel deformed in-situ in the SEM.

Supervisor: Professor Jarle Hjelen.Examiner: Dr.ing Gustav Heiberg, DnV, Høvik.

Håvard Vingsand Corrosion properties of nickel alloys in chlorinated seawater.

Supervisor: Professor Roy Johnsen, Department of Engi-neering Design and Materials. Examined at the Department of Engineering Design and Materials.

MASTER OF SCIENCE PROGRAMME IN LIGHT METALS PRODUCTIONName and title Supervisor and examiner

Benjamin Agyei Tuffour Refining of solar grade silicon by directional solidification using the accelerated crucible rotation technique (ACRT).

Supervisor: Professor Trygve Foosnæs.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

Wondowsen Abebe Aregawi The production of titanium-nickel alloys by electrodeoxidation of mixed oxides.

Supervisor: Professor Geir Martin Haarberg.Examiner: Professor emeritus Jomar Thonstad.

Jens Fladerer Electrodeoxidation of mixed oxides in molten salts to produce aluminium alloys.

Supervisor: Professor Geir Martin Haarberg.Examiner: Professor Douglas Inman, Imperial College London, United Kingdom.

Samuel Senanu Optimizing the back side contact material of silicon solar cells.

Supervisor: Professor Otto Lohne.Examiner: Professor emeritus Nils Ryum.

Chungmin Tan Models for degradation of refractory lining in aluminium electrolysis cells.

Supervisor: Professor Tor Grande.Examiner: Dr.ing. Eirik Hagen, Hydro Aluminium, Porsgrunn.

Eric Barimah Twum Electrodeoxidation of metals of titanium and nickel in CaCl2 melts for the production of titanium metal and titanium-nickel alloys.

Supervisor: Professor Geir Martin Haarberg.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

Michael Yanney Electrical resistivity of prebaked anodes as function of temperature.

Supervisor: Professor Trygve Foosnæs.Examiner: Dr.ing. Arne Petter Ratvik, SINTEF, Trondheim.

44

eXtrACUrriCULAr ACtiVities, Honours, Participation in Courses, Conferences, Lectures and Study Visits

Shahid Akhtar

MaGma, SINTEF, Oslo, Norway, February 29, 2008.

Meeting.

Casting Solidification group, NTNU seminar, Edsåsdalen,

Sweden, April 3-4, 2008.

4th International Conference on High Tech Die Casting,

Brescia, Italy, April 9-10, 2008.

Nadia Project General Assembly Meeting, Helsinki,

Finland, June 11, 2008.

2nd International Conference on Advanced Solidification

Processes, Graz, Austria, June 17-20, 2008.

International Summer School on High Integrity Casting,

Processing Fundamentals, Worcester Polytechnic

Institute, Worcester, USA, July 28 - August 1, 2008.

Meeting with MaGma, SINTEF, Aachen, Germany, August

27, 2008.

Teksid Aluminium, Torino, Italy, September 12 - December

14, 2008. Experimental activities.

University of Padova, Vicenza, Italy, November 22, 2008.

Project presentation.

Elin Harboe Albertsen

Course in “Helse-, miljø- og sikkerhetsarbeid”,

Trondheim, Norway, April 7, 8, 9 and 25, 2008.

Arbeidsmiljøkongressen, Bergen, Norway, October 15-17,

2008.

Lars Arnberg

Lars Arnberg is an Affiliate Professor at the Department

of Mechanical Engineering, Worcester Polytechnic

Institute, USA. He is the leader of the Strategic University

program Light Metals Technology.

Project meeting FONDAL, Paris, France, February 25-26,

2008.

Research Group Seminar, Edsåsdalen, Sweden, April 3-4,

2008.

High Tech Die Casting International Conference, Brescia,

Italy, April 9-10, 2008.

14th International Conference on Crystal Growth and

Crystal Technology, Sendai, Japan, May 21-24, 2008.

General Assembly Meeting, EU project NADIA, Helsinki,

Finland, June 11-13, 2008.

International Conference on Advanced Solidification

Processes, Graaz, Austria, June 17-20, 2008.

International Summer School on High-Intergrity Die

Castings: Processing Fundamentals, Worcester, United

Kingdom, July 28 - August 1, 2008.

Work package meeting EU-project NADIA, Aachen,

Germany, August 27, 2008.

International Summer School on Process Modelling,

Freiberg, Germany, August 28-29, 2008.

14th International Metallurgy and Materials Congress,

Istanbul, Turkey, October 16-18, 2008.

TEKSID, Carmagnola, Italy, November 26, 2008. Study

visit.

Management Scientific Committee, EU-project NADIA,

Padova, Italy, November 27, 2008.

University of Padova, Vicenza, Italy, November 28, 2008.

Visit.

Martin Bellmann

Scientific group seminar, Edsåsdalen, Sweden, April

3-4, 2008. Presentation on: “How to inhibit dislocation

multiplication in multi-crystalline Si?”.

User group meeting, Fraunhofer Institut fuer Integrierte

Systeme und Bauelementetechnologie, Erlangen,

Germany, April 14-18, 2008. Course in: “CrysVun++ for

modelling in crystal growth”.

NTNU, Trondheim, Norway, May 26, 2008. Presentation on:

“Impurity segregation in mc-silicon - Numerical study”.

45

Multiphase Flow Workshop, Dresden, Germany, June 24-

26, 2008.

Solar World Innovations, Freiberg, Germany, June 27,

2008. Presentation on: “The PV-Solar Cell Materials

Gemini Centre - The unifying organisational structure

for PV materials Research and Education at SINTEF and

NTNU”.

23rd European Photovoltaic Solar Energy Conference,

Valencia, Spain, September 1-5, 2008.

Norwegian - German Group Seminar on Solar Cell

Materials, NTNU, Trondheim, Norway, September 15-17,

2008. Presentation on: “Modelling of solidification in a

Bridgman laboratory furnace and related applications”.

Marte Bjørnsdotter

EUROCORR 2008, Edinburgh, Scotland, September 7-11,

2008.

Dmitry Bokach

COST Action 543: Course on Sustainable Production

and Energy: Catalysis by Nanomaterials, Catalytic

Microreactors, University of Oulu, Oulu, Finland, June 2-6,

2008.

Norwegian Hydrogen Seminar 2008, Bergen, Norway,

September 25-26, 2008. Poster on: “High-temperature

fuel cells operating with organic fuels”.

Stein Trygve Briskeby

5th Funmat meeting, Oslo, Norway, June 5, 2008.

59th Annual Meeting of the International Society of

Electrochemistry, Seville, Spain, September 7-12, 2008.

Poster on: “Particle size effects on electrochemically

degraded electrocatalysts.”

Norwegian Hydrogen Seminar 2008, Bergen, Norway,

September 25-26, 2008. Poster on: “Effect of chloride on

the stability of electrocatalysts for fuel cells”.

Yongjun Chen

Completed a special study financed by the TSA – Materials

entitled:InvestigateinfluenceofECAPonprecipitation

behaviour of dispersoids in aluminium alloy AA3003. Very

promising new results obtained.

The NMS (Norwegian Metallurgical Society) Summer

Meeting, Trondheim, Norway, May 21-22, 2008.

Presentation on: “Nanostructured commercial pure Ti

fabricated by severe plastic deformation”.

The 4th International Conference on Nanomaterials

by SPD (nanoSPD4), Goslar, Germany, August 18-22,

2008. Presentation on: “Effect of the second phase on

the microstructure of magnesium alloys during cyclic

extrusion compression”.

School of Engineering Sciences, University of

Southampton, United Kingdom, October 15 - November 16,

2008. Research visit, Financed by MOBILITY FELLOWSHIP

2008 at NTNU.

Mari-Ann Einarsrud

Thin film seminar, SINTEF Materials and Chemistry,

Trondheim, Norway, January 16, 2008. Presentation on:

“Thin film activities at Department of Materials Science

and engineering, NTNU”.

3rd NTNU NanoLab user meeting, Trondheim, Norway,

March 6, 2008.

FUNMAT meeting, Oslo, Norway, June 3-4, 2008.

1st Nanotechnology@NTNU, Trondheim, Norway,

September 11-12, 2008.

Washington Mills, Orkanger, Norway, November 7, 2008.

Study visit.

Arne Espelund

Kulturhistorisk Museum (KHM), Oslo, Norway, May 14,

2008. Introductory lecture at meeting on the provenance

of iron.

Buskerud and Nord-Østerdalen in Hedmark, Norway, 4

days in August and two days in September, 2008. Field trip

with the responsible archaeologists and representatives

from Kulturhistorisk Museum (KHM).

Àgordo, Italy, September 12-16, 2008. Guided a delegation

from the city Røros, including representatives from the

State Antiquarian and Røros secondary school.

Conference on Early Iron in Europe - Prehistoric, Roman

and Medieval Iron Production, Hüttenberg, Kärnten,

Austria, September 8-12, 2008. Presentation on: “Roman

age iron blooms in Norway and their origin”. Poster on:

“Ironmaking by Norsemen in Canada around year 1000?”.

eXtrACUrriCULAr ACtiVities

46

10th Conference on Social and Community Psychology,

Department of Psychology, Dragvoll, NTNU, Trondheim,

Norway, November 6-7, 2008. Special invited speaker.

Lecture on: ”Science before science”.

Trygve Foosnæs

Hydro Aluminium AS, Sunndalsøra, Norway, February

14, 2008. Excursion with 4th year students in “Experts in

Team”.

FESIL Holla Metall, Kyrksæterøra, Norway, March 5, 2008.

Excursion with 4th year students in “Experts in Team”.

The 137th TMS Annual Meeting, New Orleans, LA, USA,

March 9-13, 2008.

Hydro Aluminium AS, Sunndalsøra, Norway, April 24,

2008. Excursion with 1st year chemistry students.

Hydro Aluminium AS, Sunndalsøra, Norway, May 9, 2008.

Presentation of: “Experts in Team” student project on

cathode production.

Fundamentals of Aluminium Production, Trondheim,

Norway, May 13-23, 2008. Presentation on: “Fundamentals

of carbon”, “Raw materials”, “Carbon process”, “Anode

quality characteristics” and “Anode performance in

reduction cells”.

Hydro Aluminium AS, Sunndalsøra, Norway, May 21, 2008.

Excursion with course participants in “Fundamentals and

their application in aluminium production”.

27th International Course on Process Metallurgy of

Aluminium, Trondheim, Norway, May 26-30, 2008.

Presentation on: “Improvement of the potroom work

environment”.

Silicon for the Chemical and Solar Industries, Holmen

Fjordhotell, Asker, Norway, June 23-26, 2008.

ROMA Junior Program Seminar, Sunndalsøra, Norway,

June 30 - July 1, 2008.

Hydro Aluminium AS, Oslo, Norway, August 14, 2008.

Research discussions.

Researchers’ Night, NTNU, Trondheim, Norway,

September 28, 2008. Co-organizer and two demonstration

lectures.

Hydro Network, Banska Stiavnica, Slovak Republic,

September 30 - October 2, 2008.

Lectures during high school visits in Norway:

• Selbu,February8,2008.Demonstrationlecture.

• Byåsen,February12,2008.“Whatisscienceandwhy

is it important?”

• Markaplassenungdomsskole,March27,2008.

Demonstration lecture.

• Steinkjer,April1,2008.“StudiesatNTandDMSC”.

• Ørlandungdomsskole,April21,2008.Demonstration

lecture.

• Utleiraungdomsskole,June12,2008.Demonstration

lecture.

• Årdal,September26,2008.“StudiesatNTand

DMSC”.

• Fredrikstad,October15,2008.“StudiesatNTand

DMSC”.

• OleVig,December2,2008.“StudiesatNTandDMSC”.

Edita Garskaite

MRS 2008 Fall Meeting, Boston, USA, December 1-5, 2008.

Poster on: “Optically active thin films deposition by sol-gel

dip-coating on Si substrates”.

Rajiv Giri

PETROMAKS Seminar, April 24- 25, 2008, Oslo, Norway.

Presentation on: “Investigations on microstructural and

mechanical properties of pulse plasma treated metal

surfaces”.

Metallurgisk sommermøte 2008, Trondheim, Norway, May

21-22, 2008. Presentation on: “Pulsed plasma treatment

of stainless steel”.

Materials Science & Technology Conference & Exhibition,

David L. Lawrence Convention Center Pittsburgh,

Pennsylvania, USA, October 5-9, 2008. Presentation on:

“Microstructure and mechanical properties of pulsed

plasma nitrided duplex stainless steel”.

Tor Grande

Tor Grande is the head of the department and he is a

board member of NTNU Nanolab. He is currently NTNUs

representative in the steering committee in the research

consortium FUNMAT between NTNU, UiO, SINTEF and

IFE.

University of Oslo, Chemistry department, External

examiner PhD defense Marius Widerøe, January 11, 2008.

eXtrACUrriCULAr ACtiVities

47

Zing Solid State Chemistry conference 2008, Cancun,

Mexico, March 10-14, 2008. Lecture on: “Ferroelasticity of

Sr and Ca substituted LaCoO3-based perovskites”.

Strategy seminar, Faculty of Natural Science and

Technology, NTNU, Hell, Norway, April 24-25, 2008.

Meeting FUNMAT steering committee, Trondheim,

Norway, May 8, 2008.

Department seminar, Stiklestad, Norway, May 15-16, 2008.

Lecture on: “Velkommen og presentasjon av formålet med

seminaret”.

FUMAT meeting, June 4-5, 2008.

Project meeting, Effpower AB, Gothenburg, Sweden,

August 29, 2008.

Electroceramics XI, Manchester, England, September,

1-3, 2008. Lecture on: “The ferroic phase transitions of

BiFeO3 and finite size effects of nano-crystalline BiFeO3”.

Advisory Board meeting: “Presentation of Electroceramic

XII in Trondheim, June 13-17, 2010”.

NFR Evaluation, Trondheim, Norway, September 4, 2008.

Lecture on: “Presentation of the Department of Materials

Science and Engineering, NTNU”.

NTNU Nanolab seminar, Trondheim, Norway, September

11-12, 2008.

Thermotech seminar, Trondheim, Norway, November 12-

13, 2008. Lecture on: “Stability of materials, macroscopic

and microscopic aspects”.

Materials Science and Technology 2008 (MT&S08),

Pittsburgh, USA, October 6-9, 2008. Invited lecture on:

“Cation diffusion in perovskites”. Lecture on: “The ferroic

phase transitions of BiFeO3 and finite size effects of nano-

crystalline BiFeO3”.

Seminar - Nyskaping og utvikling av Midt-Norge,

Trondheim, Norway, November 4, 2008.

Board meeting NTNU Nanolab, Trondheim, Norway,

December 2, 2008.

Imperial College, London, United Kingdom, December 10,

2008. External examiner PhD defense Robert Packer.

Geir Martin Haarberg

ULCOS project meeting, Aveiro, Portugal, January 17-18,

2008.

Bo Håkansson Seminar; KTH, Stockholm, Sweden,

January 30, 2008.

1st Round Table on Titanium Production by Electrolysis,

Cologne, Germany, March 2-4, 2008.

1st International Round Table on Titanium Production

in Molten Salts, Cologne, Germany, March 2-4, 2008.

Presentation on: “Electrochemical behaviour of dissolved

titanium species in molten salts”.

ISE Spring Meeting, Foz do Iguaco, Brazil, March 16-20,

2008. Presentation on: “The supply of dissolved oxygen by

electrolysis in Lake Biwa”.

ULCOS project meeting, Paris, France, April 10-11, 2008.

KTH, Stockholm, Sweden, April 18, 2008. PhD defence,

opponent.

4th Asian Conference of Crystal Growth and Crystal

Technology (CGCT-4), Sendai, Japan, May 19-24, 2008.

Presentation on: “Electrochemical refining of silicon in

molten salts”.

Hokkaido University, Sapporo, Japan, May 26-28, 2008.

Study visit and presentation.

Foxy project meeting, Kiev, Ukraine, June 16-17, 2008.

Presentation.

ULCOS project meeting, Metz, France, July 10-11, 2008.

Molten Salts Discussion Group, Nottingham, United

Kingdom, July 15, 2008. Presentation on: “Electrochemical

behaviour of Fe (III) in molten NaCl-FeCl3”.

University of Cambridge, London, United Kingdom, July

22, 2008. PhD defence, opponent.

Doshisha University, Japan, August - December, 2008.

Visiting professor.

214th Meeting of the Electrochemical Society, Fall Meeting,

Honolulu, Hawaii, USA, October 12-17, 2008. Presentation

on: “Diffusion kinetics for the electrochemical reduction of

eXtrACUrriCULAr ACtiVities

48

eXtrACUrriCULAr ACtiVities

Fe (III) species in molten NaCl-FeCl3”. Session chairman.

MS8, Kobe, Japan, October 19-23, 2008. Presentation on:

“Electrochemical deoxidation of mixed metal oxides in

molten calcium chloride to produce aluminium-scandium

alloys” and “Estimation of current efficiency and energy

consumption in Hall-Heroult cell based on the electronic

conduction in cryolite alumina melts”. Session chairman.

The IUMRS International Conference in Asia 2008,

Nagoya, Japan, December 9-13, 2008. Presentation on:

“Electrorefining of silicon in molten chlorides”.

Liudmila Ilyukhina

European Forum on Electrochemical Promotion of

Catalysis (Efepoc), Ciudad Real, Spain, May 26-30, 2008.

The Second Training Course on Basics and Applications of

Catalysis (Heterogeneous and Homogeneous).

XII International Scientific Conference “High-Tech

in Chemical Engineering 2008”, Volgograd, Russia,

September 9-11, 2008. Presentation on: “Rational design of

mixed oxide catalysts for polymer electrolyte membrane

(PEM) water electrolysis”.

Norwegian Hydrogen Seminar 2008, Bergen, Norway,

September 25-26, 2008. Poster on: “Photoelectrochemical

characterisation of oxide electrocatalysts”.

Zhihong Jia

FONDAL project meeting, Trondheim, Norway, February

25-26, 2008. Lecture on: “Microstructure study of family

III-3, III-4 and family II-5 cast alloys”.

Hydro Aluminium, Sunndalsøra, Norway, May 22, 2008.

Lecture on: “Experimental progress on the current

FONDAL project”.

FONDAL project meeting, Lillehammer, Norway, May 28-

29, 2008. Lecture on: “On development of aluminium cast

alloys for elevated temperature applications”.

The 14th European Microscopy Congress, Aachen,

Germany, September 1-5, 2008. Lecture on: “TEM

investigations of aluminum precipitate in eutectic Si of

A356 based alloys”.

11th International Conference on Aluminium Alloys,

Aachen, Germany, September 22-26, 2008. Lecture on:

“Effect of heat treatments on hardening of Al-Zr-Sc

alloys”.

Institut de Chimie et Materiaux Paris-Est (ICMPE), CNRS,

Paris, France, October 5 - November 31, 2008. Visit.

Hilde Lea Lein

3rd NanoLab User Meeting. Royal Garden, Trondheim,

Norway, March 6, 2008.

Sono-Tek Corporation, Milton, New York, USA, May 8,

2008. Visit.

Materials Science & Technology 2008 Conference &

Exhibition, Pittsburg, USA, October 5-10, 2008. Lecture

on: “Proton conducting solid oxide fuel cells with the novel

LaNbO4 electrolyte”.

Manping Liu

Co-Mentor of a PhD student (Jinbao Lin) from SJTU on

Mechanical behavior and strengthening mechanism of

ultrafine grained Mg alloys fabricated by severe plastic

deformation (SPD).

The NMS (Norwegian Metallurgical Society) Summer

Meeting, Trondheim, Norway, May 21-22, 2008.

Presentation on: “Characterization of nanostructured Al-

Mg alloys using high-resolution electron microscopy”.

Recent developments in the processing and applications

of structural metals and alloys, Como Lake, Italy, June

22-25, 2008. Presentation on: “Nanostructures and

microhardness in Al and Al-Mg alloys subjected to severe

plastic deformation”.

The 4th International Conference on Nanomaterials

by SPD (nanoSPD4), Goslar, Germany, August 18-22,

2008. Presentation on: “Grain boundary structure and

deformation defects in nanostructured Al–Mg alloys

processed by high pressure torsion”.

International Conference on Aluminium Alloys (ICAA 11),

Aachen, Germany, September 22-26, 2008. Presentation

on: “Effects of Mg in nanostructured Al-Mg alloys

subjected to severe plastic deformation”.

Department of Materials Science and Engineering,

Shanghai Jiao Tong University, China, November 3-9, 2008.

Project meetings.

2008 MRS Fall Meeting, Boston, MA, USA, December 1-5,

2008. Presentation on: “Formation of nanostructures in

Al-Mg alloys subjected to severe plastic deformation”.

49

Knut Marthinsen

Knut Marthinsen is deputy head at the Department of

Materials Science and Engineering, and a member of the

Board of Research and PhD education at the Faculty of

Natural Sciences and Technology, NTNU.

He is member of the International Committee for the Joint

International Conferences on Recrystallization and Grain

Growth (ReX&GG), the International Committee for the

International Conferences of Aluminium Alloys (ICAA) and

he is also Topics coordinator for the Aluminium Alloys

session and a member of the Executive Committee for

Thermec’2009, Berlin, Germany (August 25-29, 2009).

Knut Marthinsen is member (NTNU’s representative) in the

Steering Committee for the BIP NFR projects “Nucleation

Control for Optimized properties” and RIRA (Remelting and

Inclusion Refining of Aluminium) and the NFR KMB project

“Defect Engineering for Crystalline Silicon Solar Cells”.

Participation in International Convergent Beam Electron

Diffraction (CBED) Workshop, NTNU/Skistua, Trondheim,

Norway, May 29-30, 2008.

Hydro Al R&D Bonn, Germany, July 8-9, 2008. Visit.

11th International Conference on Aluminium Alloys (ICAA11),

September 22-26, 2008. Presentation on: “A 3D Monte

Carlo study of the effect of anisotropy and particles on the

size distribution of grains after recrystallization and grain

growth”.

Referee for several renowned international journals with a

peer review system.

Kemal Nisancioglu

Member of evaluation committees for two academic

positions in corrosion at the Royal Institute of Technology,

Stockholm, Sweden.

University of Birmingham, United Kingdom, March, 2008.

PhD thesis defence committee Rob Winsley.

Department of Materials Science and Engineering, NTNU,

Trondheim, Norway, April 30, 2008. PhD thesis defence

committee Espen Sandnes.

213th Meeting of the Electrochemical Society, Phoenix, USA,

May 18-22, 2008. Invited paper: “Comparison of alternating

and direct current relaxation techniques”. Contributed

paper: “Determination of oxygen exchange and diffusion

coefficients of MIEC perovskites by asymptotic analysis of

relaxation data”.

Department of Materials and Metallurgical Engineering,

Istanbul Technical University, Istanbul, Turkey, June 16,

2008. Esma Senel’s MSc thesis defence and visit.

Gordon Research Conference on Aqueous Corrosion, New

London, USA, July 20-25, 2008.

Hydro - NTNU seminars, Trondheim, Norway, August 26 and

September 16, 2008.

59th Meeting of International Society of Electrochemistry,

Seville, Spain, September 7-12, 2008. Keynote lecture on:

“Effect of low melting point trace element segregation on

electrochemistry and corrosion of aluminum alloys”.

214th Meeting of the Electrochemical Society, Honolulu,

Hawaii, USA, October 12-17, 2008. Invited paper:

“Applications of potential theory in cathodic protection”.

XI International Corrosion Symposium (KORSEM08), Izmir,

Turkey, October 22-25, 2008. Member, International Advisory

Board. Keynote talks: “Relevance of copper and silicon in

intercrystalline corrosion of AA6000-series aluminium alloys”

and “Significance of hydrogen evolution in cathodic protection

of steel in seawater”. Contributed paper: “Activation of

aluminium alloys by low melting point trace elements”.

Lars-Erik Owe

59th Annual Meeting of the International Society of

Electrochemistry, Seville, Spain, September 7-12, 2008.

Poster on: “Oxide catalysts for the oxygen evolution

reaction”.

Norwegian Hydrogen Seminar 2008, Bergen, Norway,

September 25-26, 2008. Poster on: “Oxide catalysts for the

oxygen evolution reaction”.

Hans Jørgen Roven

Hans Jørgen Roven is Head of the Strategic Area Materials

at NTNU and vice-dean at the Faculty of Natural Science

and Technology. He is also professor in physical metallurgy

and responsible for the severe plastic deformation (SPD)

nanostructuring group at the DMSE.

Member of the www.nanospd.org promoting international

research collaboration on bulk nanostructured materials

and Head of FORMLAB, the forming, new forming technology

and mechanical testing laboratories at the DMSE.

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50

eXtrACUrriCULAr ACtiVities

Officially appointed Guest professor to the Shanghai Jiao

Tong University in China for the period May 2007 - May

2010.

Peer-reviewer to the Engineering and Physical Sciences

Research Council U.K. (EPSRC), Natural Sciences and

Engineering Research Council of Canada (NSERC) and

Italian Research Council (CIVR/CINECA).

Det Norske Veritas - NTNU Meeting, Trondheim, Norway,

January 15-16, 2008. Lecture on: “New light alloys”.

Nanomat Seminar NTNU - SINTEF, Trondheim, Norway,

February 4, 2008. Lecture on: “Plans and projects at

NTNU - New Materials”.

AluRenameeting#5,Oslo,Norway,February14,2008.

Royal Institute of Technology, Materials Science and

Engineering, Stockholm, Sweden, March 6-7, 2008. Visit

and project meeting.

Royal Institute of Technology, Materials Science and

Engineering, Stockholm, Sweden, March 26-27, 2008. Visit

and project meeting.

The Hydro-Day at NTNU - SINTEF, Lerchendal Gård,

Trondheim, Norway, April 10-11, 2008. Lecture on: “A brief

status of Materials at NTNU”.

Innovation Norway, Special Project Evaluation Committee

Meeting, Oslo, Norway, May 6, 2008.

Elkem - NTNU Meeting, Trondheim, Norway, May 13, 2008.

Lecture on: “Strategic Area Materials at NTNU”.

Norwegian Metallurgical Society Meeting, Trondheim,

Norway, May 21-22, 2008. Lecture on: “Bulk

nanostructured metals by severe plastic deformation

(SPD)”.

Chalmers University of Technology, Goethenburg, Sweden,

June 12-13, 2008. PhD Defense Committee.

International Conference in honor of Professor Enrico

Evangelista 70th year’s birthday: Recent Developments

in the Processing and Applications of Structural Metals

and Alloys, Como, Italy, June 22-25, 2008. Lecture on:

“Nanostructures and microhardness in Al and Al-Mg

alloys subjected to SPD”.

NanoSPD 4 International Conference, Goslar, Germany,

August 18-22, 2008. Lecture on: “Grain boundary

structure and deformation defects in nanostructured Al-

Mg alloys processed by high pressure torsion”.

Organizing Internal Hydro - NTNU - SINTEF Strategy

Seminar on Aluminium Technology, Kvilhaugen Gård,

Trondheim, Norway, August 25-26, 2008.

Directors and Deans Meeting NTNU - SINTEF, Lerchendal

Gård, Trondheim, Norway, September 15, 2008.

ICAA11 International Conference, Aachen, Germany,

September 22-26, 2008. Lecture on: “Effects of Mg in

nanostructured Al-Mg alloys subjected to severe plastic

deformation”.

Norwegian Titanium meeting, Trondheim, Norway,

October 27, 2008.

Materials Forum (talk 27-2008), Shanghai Jiao Tong

University, China, November 5, 2008. Invited lecture on:

“Bulk nanostructured light metals produced by severe

plastic deformation”.

Part of official Norwegian Ministry Delegation to China

visiting Fudan University, Norwegian Consul General

in Shanghai, Polar Research Institute of China ((PRIC)

and the Shanghai Jiao Tong University, Shanghai, China,

November 6-8, 2008.

MRS Fall Meeting, Boston, USA, December 1-3, 2008.

Lecture on: “Formation of nanostructures in Al-Mg alloys

subjected to severe plastic deformation”.

MIT, Boston, USA, December 2, 2008. Visit.

Purdue University, Center for Materials processing

and tribology; Lafayette, Indiana, USA, December 4,

2008. Invited lecture on: “Bulk nano-structured metals

produced by SPD”.

PhD Defense own candidate Przemyslaw Szczygiel,

Trondheim, Norway, December 16, 2008.

Per Martin Rørvik

Thin film seminar, NTNU-SINTEF, Oslo, Norway, January

16, 2008.

3rd NTNU NanoLab User Meeting, Trondheim, Norway,

March 6, 2008. Lecture on: “Template-free hydrothermal

51

synthesis of PbTiO3 nanorod arrays”.

Zing Conference on Solid State Chemistry, Cancun,

Mexico, March 10-13, 2008. Poster on: “Hydrothermal

synthesis of PbTiO3 nanorod arrays”.

Electroceramics XI, Manchester, United Kingdom, August

31 - September 3, 2008. Lecture on: “Template-free

hydrothermal synthesis of PbTiO3 nanorod arrays”.

1st Nanotechnology@NTNU Symposium, Trondheim,

Norway, September 11-12, 2008. Poster on: “Hydrothermal

synthesis of PbTiO3 nanorod arrays”.

Veeco Scandinavian Conference & Users Meeting -

Developments in Atomic Force Microscopy for advanced

imaging techniques, Trondheim, Norway, October 30-31,

2008. Poster on: “Piezoresponse force microscopy studies

of single PbTiO3 nanorods”.

Frode Seland

Seminar in the memory of Bo Håkansson, Royal Institute

of Technology (KTH), Stockholm, Sweden, January 30,

2008. Invited talk.

Final meeting in EU-project FURIM, HyGear, Arnhem, The

Netherlands, March 12, 2008.

Joint Seminar and Workshops, Hydrogen and Fuel cells,

StatoilHydro, SINTEF, NTNU and Tsinghua University,

NTNU, Trondheim, Norway, April 15, 2008.

“Pedagogisk Utviklingsprogram”, NTNU, Trondheim,

Norway.

Sverre Magnus Selbach

Thin film seminar, SINTEF and NTNU, Oslo, Norway, ,

January 16, 2008.

3rd NTNU NanoLab user meeting, Trondheim, Norway,

March 6, 2008. Lecture on: “Size-dependent properties of

multiferroic nanoparticles”.

Zing Solid State Chemistry Conference 2008, Cancun,

Mexico, March 10-13, 2008. Poster on: “Size-dependent

properties of BiFeO3 nanoparticles”.

Professor Ram Seshadri’s group, Materials Research

Laboratory, University of California, Santa Barbara, USA,

September 2 - December 12, 2008. Research stay.

Quantum Design, San Diego, USA, November 23-26, 2008.

Experiments and study visit, host: Application Chemist,

PhD James O’Brien.

Materials Research Society Fall Meeting, November 30 -

December 5, 2008. Lecture on: “Ferroic phase transitions

in BiFe1-xMnxO3, 0 ≤ x ≤ 0.3”.

Argonne National Laboratory, Argonne, USA, December

5-6, 2008. Study visit and experimental work, host:

Professor Valeri Petkov at Central Michigan University.

Jan Ketil Solberg

Meeting between DnV and NTNU regarding future

cooperation, Trondheim, Norway, January 15, 2008.

Project meeting in SUP project “Materials and Structural

Integrity” (StatoilHydro/NTNU), Trondheim, Norway,

February 2, 2008.

Project meetings in BIP project “An integrated process

for hydrogen production and separation” (StatoilHydro,

SINTEF, IFE, NTNU), Rotvoll, Trondheim, Norway, March 4,

April 27 and September 9, 2008.

Seminar in ISP project, Brekstad, Norway, March 26,

2008. Presentation on: “Ductile-to-brittle transition

temperature”.

“Hydrodagen”, NTNU, Trondheim, Norway, April 10, 2008.

NORSTORE 2008, International Conference on “Integration

of Advanced H Storage Materials and Systems into the

Hydrogen Society”, Moscow, Russia, May 26-30, 2008.

Presentation on: “Synthesis and characterization of

H-storage alloys”.

Project meetings in BIP project “Pulsed plasma

surface treatment for wear and corrosion protection of

superalloys and stainless steel valves, pumps and pipes”

(MOTech Plasma, NTNU), Trondheim, Norway, June 30 and

December 10, 2008.

Meeting with Kverneland Group regarding future

cooperation, Trondheim, Norway, August 29, 2008.

Project meeting in “OptiWeld” (TubeFuse, AMR, NTNU),

Trondheim, Norway, October 1, 2008.

Annual meeting at Norsk Metallografisk Forening (25 year

anniversary), Oslo, Norway, November 6-7, 2008.

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52

eXtrACUrriCULAr ACtiVities

Meeting between Posco (Korea), SINTEF, Elkem and

NTNU regarding future cooperation, Trondheim, Norway,

December 16, 2008.

Svein Sunde

MITHT, Moscow, Russia, April 5, 2008. Lecture on:

“Electrocatalysts for water electrolysis”.

Network meeting on carbon materials, The Research

Council of Norway, Oslo, Norway, August 28, 2008.

Lecture on: “Carbon nanofibres as electrocatalyst

supports for fuel cells”.

Jomar Thonstad

Aluminium Smelting Course, Barran Abbas, Iran, January,

23-24, 2008. Lectured (together with Harald Øye). Visited

two aluminium plants, one in Iran (Almadhi) and one in

Dubai (Dubai Aluminium).

TMS Annual Meeting, New Orleans, USA, March 9-13,

2008. Served as session co-chairman, Aluminum

reduction, Inert anodes.

Slovak Technical University, Bratislava, Slovak Republic,

April 22 and July 10, 2008. Project meetings.

University of Leuven, Belgium, June 12-13, 2008.

Opponent, PhD thesis.

IUPAC Conference on Solid State Chemistry, Bratislava,

Slovak Republic, July 6-11, 2008. Presented paper on:

“Inert anodes for aluminium electrolysis”. Co-authored

paper on: “Transference numbers in cryolite-based

melts”.

Norwegian Silicon Refinery, Moss, Norway, August 28,

2008. Visit.

Kronos Titan, Fredrikstad, Norway, August 29, 2008. Visit.

International Society of Electrochemistry, Annual

Meeting, Sevilla, Spain, September 7-12, 2008. Lecture on:

“Electrowinning of iron from sulphate solutions”.

Julian Tolchard

2nd International Conference on Functional Materials and

Devices 2008, Kuala Lumpur, Malaysia, June 16-19, 2008.

Invited presentation: “Choosing the right components:

Compatibility of the proton conductors BaZrO3, SrCeO3

and LaNbO4”.

NTNU Nanolab: 1st Nanotechnology@NTNU, Trondheim,

Norway, September 11-12, 2008. Poster on: “Choosing the

right components: the solid state chemistry of BaZrO3 and

SrCeO3 to potential partner oxides”.

Researchers Night, NTNU, Trondheim, Norway,

September 26, 2008.

Mikhail Tsypkin

MITHT, Moscow, Russia, April 5, 2008. Lecture on:

“Catalyst development for high temperature PEMFC”.

SNBL ESRF, Grenoble, France, October 29 - November 3,

2008. Experiment 01-01-777: “In situ XAS study of carbon-

supported core-shell electrocatalysts for oxidation of

small organic molecules”.

Fride Vullum

Lecture on Nanotechnology for high school chemistry

teachers in Sør-Trøndelag, Trondheim, Norway, April 23,

2008. Lecture on: “Liten ® Mindre ® Minst ® Nano –

Fremtidens teknologi”.

Lecture on Nanotechnology for high school chemistry

teachers in Nord-Trøndelag, Levanger, Norway, May 3,

2008.

International Conference on Materials Science &

Technology, Pittsburgh, Pennsylvania, USA, October 6-9,

2008. Lecture on: “Synthesis and characterization of

Ce1-x-y/2Lax-y/2CayNbO4 thin film membranes”.

Scandinavian Conference & Users Meeting -

Developments in Atomic Force Microscopy for advanced

imaging techniques, Trondheim, Norway, October 30-31,

2008. Invited lecture on: “From atoms to microspheres -

An introduction to AFM”.

Kjell Wiik

COST-539, Workshop: Electroceramics from nanopowders

produced by innovative methods (ELENA), Leysin,

Switzerland, January 30-31, 2008. Lecture on: “Production

of complex proton conducting oxide powders by spray

pyrolysis”.

Membrane work group meeting at Fuel Cells and Solid

State Chemistry Department, Risø National Laboratory

for Sustainable Energy, Technical University of Denmark,

Risø, Denmark, October 31, 2008. Lecture on: “Mass

transport in perovskites. Part I”.

53

Membrane work group meeting at Fuel Cells and Solid

State Chemistry Department, Risø National Laboratory

for Sustainable Energy, Technical University of Denmark,

Risø, Denmark, December 12, 2008. Lecture on: “Mass

transport in perovskites. Part II”.

The 5th National FUNMAT meeting, Oslo, Norway. June 5,

2008. Lecture on: “Spray pyrolysis and the production of

submicron complex oxide powders”.

Gunn Torill Wikdahl

Diffrac Plus Advance Method Development Course: X-Ray

Diffracetion, Villa Martin, Spain, April 7-11, 2008.

The 15th Norwegian X-ray Conference, Kristiansand,

Norway, September 8-10, 2008.

BRUKER User Meeting, Stockholm, Sweden, September

29-30 and October 1, 2008.

Terje Østvold

Project and board meetings related to “Sand Stabilisation

and Water Proofing of Tunnels”. This project is operated

by the spin-off company Impermeable AS where Terje

Østvold is the manager.

Cooperation with SINTEF Petroleum Research. Project

meetings and reporting on running projects. A series of

meetings during the year at Statoil Rotvoll and Stjørdal,

Norway.

Project meetings, Radcon Scandinavia, Oslo, Norway,

January 4, April 11-13, August 14-17, October 3-5 and

December 28, 2008. Board meetings, Trondheim, Norway,

April 9, 2008.

19th International Oil Field Chemistry Symposium, Geilo,

Norway, March 9-12, 2008. Project meeting with Dond.

Member of committee and session chairman. Paper on:

“CaCO3 scale formation: Visual observations in 2D model

pore networks and precipitation kinetics during core

flooding”.

Svalbard with Sintef Petroleum Research, April 15-18,

2008. Study visit.

Bologna, Modena, Italy, May 6, 2008. Meeting with Radcon

Italia and Kerakoll.

University of Bergen. Bergen, Norway, May 14-16, 2008.

Project meetings.

SPE 9th International Conference on Oilfield Scale,

Aberdeen, United Kingdom, May 28-29, 2008. Paper on:

“Kinetics of CaCO3scaleformationduringcoreflooding”.

Terje Østvold is a member of the TEKNA Oil field

chemistry symposium board. Meetings in Oslo, May 29 and

October 15, 2008.

ICE/HT-FORTH and University of Patras, Patras, Greece,

June 9 - July 7, 2008. Guidance of 3 PhD students and one

Postdoctor at the Department of Chemical Engineering,

University of Patras, Greece. Study visit.

International MultiScale course. 1: Heriopt-Watt

University, Edinburgh, United Kingdom, August 10-12,

2008. 2: Exprogroup (Petrotech ASA), Haugesund, Norway,

September 15-18, 2008.

Gas Hydrates - Operational Treatment and Future

Scenarios, Bergen, Norway, October 12-22, 2008. Paper

on: “Thermodynamic hydrate inhibitors. Consequences for

carbonate scale formation during oil and gas recovery in

pH stabilized systems”.

Rio de Janeiro, Brazil, October 29 – November 15, 2008.

Study visit and consulting with the oil and gas research

institution Petrobras.

The Federal University Fluminense, Rio de Janeiro, Brazil,

October 30-31, 2008. Courses on mineral scale prediction.

The focus was on evaluation of new gas field developments

with respect to the possible scale problems that could

occur when these fields experience formation water

breakthrough.

Hotel Copacabana Merlin, Rio de Janeiro, Brazil,

November 3-7, 2008. Courses for Petrobras on mineral

scale prediction. The focus was on evaluation of new gas

field developments with respect to the possible scale

problems that could occur when these fields experience

formation water breakthrough.

Buenos Aires, Argentina, November 12-13, 2008. Meetings

with Celta Industrias, Dir. Carlos Luengo.

Study visit Argentina to oil and gas industry and research

institutions, November 15-30, 2008.

Neuquen, Argentina, November 20-21, 2008. Meetings

with Petrobras

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eXtrACUrriCULAr ACtiVities

Harald A. Øye

Harald A. Øye is chairman of the technical committee

ISO/TC 226 (Materials for the Production of Primary

Aluminium).

Irianian Smelter Course 2008, Almahdy Aluminium,

Bandar-Abbas, Iran, January 23-24, 2008. Lectures on:

“Fundamentals of aluminium electrolysis (Principles

and environmental concerns)”, “Cathode materials”,

Cathode construction”, “Cell autopsy manual”, “How to

obtain long-lived cathodes”, “ISO standardization work

and testing of cathodes and ramming paste”, “Carbon

materials testing at the Norwegian University of Science

and Technology and SINTEF”, “Spent potlining treatment”

and “3D modelling of thermal and sodium expansion in an

aluminium reduction cell”.

Dubal, Dubai, January 29, 2008. Plant visit.

TMS 2008 Annual Meeting, New Orleans, LA, USA, March

9-13, 2008. Lecture on: “ISO standards of testing of

cathode materials”.

Fundamentals of Aluminium Production 2008, Trondheim,

Norway, May 13-23, 2008. Chairman.

27th International Course on Process Metallurgy of

Aluminium, Trondheim, Norway, May 26-30, 2008.

Chairman and lectures on: “The principles of aluminium

electrolysis” and “How to obtain long-lived cells”.

ISO Chairman Conference, Geneva, Switzerland, June 5-6,

2008.

Silicon for the Chemical and Solar Industry IX, Oslo,

Norway, June 23-26, 2008. Chairman.

3rd China Silicon Conference, Kunming, China, September

24-27, 2008

Molten Salt Discussion Group, London, United Kingdom,

December, 2008. Lecture on: “Pyrohydrolysis of solium

fluoridecontainingsilicateslagfromspentpotlining”.

Table of ContentsEditorial ........................................................................................................................................................................................... 3Science stories ...................................................................................................................................................................... 5Publications in international peer review journals, books and patents ....... 15Conference proceedings, other reports and publications .............................................. 19Equipment ................................................................................................................................................................................... 21Chemistry Building II (KII)-Seminars, Energy and Materials ..................................... 24Guest lecturers ...................................................................................................................................................................... 26Staff ...................................................................................................................................................................................................... 27Graduate studies ................................................................................................................................................................. 31Dr.ing/PhD projects in progress ...................................................................................................................... 33Dr.ing/PhD projects co-supervised in other departments ............................................ 36Course program ................................................................................................................................................................... 37M.Sc. students ........................................................................................................................................................................ 39Graduated M.Sc. students with titles of their diploma works ................................... 41Extracurricular activities .......................................................................................................................................... 44

Picture on front page: Per Martin Rørvik.Photo: Lead titanate nanorods grown on strontium titanate substrates.

Annual report forDepartment of Materials Science and EngineeringNorwegian University of Science and TechnologyNO-7491 Trondheim, NorwayInternet address: http://www.ntnu.no/materialteknologi

The editor thanks✔ Brit Wenche Meland, Hilde Martinsen Nordø, Hege Knutsdatter Johnsen and

Åse Lill Salomonsen for collecting the administrative data and taking care of the process of printing the report.

✔ Skipnes kommunikasjon for printing.

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NTNUThe Norwegian University of Science and Technology (NTNU) in Trondheim represents academic eminence in technology and the natural sciences as well as in other academic disciplines ranging from the social sciences, the arts, medicine, architecture to fine arts. Cross-disciplinary cooperation results in ideas no one else has thought of, and creative solutions that change our daily lives.

Department of Materials Science and EngineeringNorwegian University of Science and TechnologyNO-7491 Trondheim, Norway

www.ntnu.no

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Department ofMaterials Scienceand Engineering