american environmental testing laboratory inc. · msimsd i kpd ! % i % limit , % limit . . cadmium...

American Environmental Testing Laboratory Inc. 2834 a2908 North Naomi Street, Burhank, CA 91504. DOHS NO: 1541,I.ACSDNO: I0181 Tel: (888) 288-AETI,. (818) 845-8200. Fax: (818) 845-8840. www.actlab.com

ANALYTICAL RESULTS

Telephone: (71 4)985-3434 Attn: Tom Talnall

Page: 68

S i t e

Project ID: 32486-000 Project Name: De lph i S y s t e m Corp.

~p . - ~ p~

Method: 8260B, Volatile Organic Compo~ulds by GCIMS (SW846) QC Batch No: 091505

American .. Environmental Testing Laboratory .- Inc. 2834 8~2908 North Naolni Strecl, Uurbank, CA 91504. SIOHS NO: 1541,LACSDNO: 10181 Tei: (888) 288-AETI.. (818) 845-8200 si'ax: (818) 845-8840. www.aet1nb.corn

ANALYTICAL RESULTS

Page: 6 9

Project ID: 32486-000 Project Name: Deiphi System Cor

Method: 826OB, Volatile Organic Compounds by GCIMS (SW846) QC Batch No: 091505

I Client Sainplc 1.D. Date Sampled ~ ~ ~~~ ~.. Date Prepared -~ ~ -;--- ~ .... . Preparatton Metl~od ~~ ~~ Date Aiialyzed Eaiir-~ .... - 1 . -~ - ~ - ~

09 /15 /2005 0 9 / ~ 5 / 2 0 0 5 0 9 / 1 5 / 2 0 0 5 -~- .. A - 1 Aqueous Aqueous ' ~ q u e o u s l ,. . - =EX I ue/L i ue/L

American Environmental Testing Laboratory hc. 2834&2908 Nortli Naomi Street, Rurbank, CA 91504 - DOHS NO: 1541.I.ACSDNO: 10181 Tcl: (888) 288-Awl_ . - (818) 845-8200 Fax: (818) 845-8840. www.actlab.com

ANALYTICAL RESULTS

Page: 7 0

Iiroject ID: 32486-000 ProjeclName: elp phi System cor

Method: 8260B, Volatile Organic Compounds by GCiMS (SW846) QC Batch No: 091505

American Environmental Testing Laboratory Inc. 28348~2908 North Naoini Slrczt, Rurbank, CA Y1504.DOHS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL - (818) 845-8200. Fax: (818) 845-8840 - w w w . a e t l a b . c ~ ~ n

ANALYTICAL RESULTS

Telephone: (714)985-3434 Attn: Toin Tatnali

Page: 7 1

Project ID: 3 2 4 8 6 - 0 0 0 Prqject Name: Delphi S y s t e m Carp.

. ~

- . ~- -~ ~. .. , -- .. ..-7 ~~~~ ..-.; !

American Environmental ... Testing Laboratory Inc. 28348~2908 Nonh Naorni Slrrel,Rurbaok, CA 91504. UOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL ' (818) 845-8200 Fax: (818) 845-8840. www.acilah.com

ANALYTICAL RESULTS Ordered By

Attn: Toill 'Tatnall

Page: 72

Project ID: 32486-000 Project Name: Delphi System Corp.

Oiir Lab 1.D. ---- IC..rr,."=+rrc

American Environmental Testing Laboratory .- Inc. 28348~2908 North Naonli Strcel, Burbank. CA 91504 .DOHS NO: 154l,I,ACSl)NO: 10181 Tcl: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 - www.aetIsb.com


I 500 South l

American ... Environmental Testing Laboratory Inc. 2834&2Y08 North Naomi Street. Burbank, CA 91504 .DOITS NO: 1541,LACSDNO: I0181 Tel : (888) 288-AETL - (818) 845-8200 ' F a x : (818) 845-8840 . www.aetIab.com

ANALYTICAL RESULTS Site

Telephone: (714)985-3434 Aitri: Torn Tatnall

Page: 7 4

Project ID: 3 2 4 8 6 - 0 0 0 Prqject Name: Delphi System Corp.

~ . .

Method: 8270C, Seinivolatile Organic Compounds by GCIMS (SW-846)

1 Date Prepared ~ ~~ . -- ~ c ~ & a i i o i i ~~~~ Method Date Analyzed ~~

1 U n i t s Matrix I .

I I 10 ND

--

~ P..~. Bis(2-Cl1ioroelhyl)etl1er 1 , - 10 - -~. . -. -

10 ND . --

1 Bis(2-ethyllrcxyl) phthaiat L~~~-~.. 4-Bromoplicnyl phcnyl ether 5

. ..

I ~*3!!?ih!!E-~ ~ -Cliloro-3-niethylphe11ol ND

-

I .-

.PhIn....m..!i.. e i 5 10 I ND ND

.......... r.. ..... .

4-Chloroplienyi phenyl etiicr ... ..... Chrysene

i Di-n-butyl plithalatc . . .,

Di-11-octyl piithakite (Dioctyl ester)

American Environmental Testing Laboratory Inc. -.

2834&2908 Norlli Naolni Strcct, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 'Tel: (888) 288-AETL - (818) 845-8200 Fax: (818) 8 4 5 - 8 8 4 0 . www.ae t l ab .com

AXAL,YTICAL RE-,SULTS

Page: 7 5 . Project ID: 3 2 4 8 6 - 0 0 0 Project Name: Del.phi System C

Method: 8270C, Senlivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 092005

,

-

.

Dielhyi plilhalatitz (Dietligl ester) 5

. ~

2.4-Ilinitrotoiucne

I lzxiichlorobc~~zene ~

Hexachlorobutadicne

N-Nitroso-lli-n-propyla~~ine

. . . 3-Nitroaniline

.~.. . ... ~ 4-Nitroanilinc

. ~.. ~~~- !Niliobenzenc (NBj ~~ ~ ~

4-Nitrophenol ~~~ ~ ~~ ~ -~~~

American Environmental Testing .- Laboratory .. Inc. - 28348~2908 Nor th Naomi Street, Burbank, CA 91504 .DOHS NO: i541,12ACSDNO: 10181 Trl: (888) 288-AETL.. (818) 845-8200 * Fax: (818) 845-8840. www.act1ab.com

ANALYTICAL RESULTS

Page: 76

Prqject ID: 32486-000 Project Name:

Method: 8270C, Seinivoiatile Organic Compounds by GC/MS (SW-846) QC Batch No: 092005

...

. . . . Matrix

~~~~~~~~~ ~~~~~pp

.... . -

American Environmental Testing Laboratory .- Inc. 2834 &2908 Norlh Nao~ni Street, Burbank, CA 91504 .DOAS NO: 1541.12ACSDNO: IOl8l Tel: (888) 288-AETL - (818) 845-8200 * Fax: (818) 845-8840. www.actlab.com


1 i l,lle) Br Aldrlch i O O South Icraemer Blvd

S i t e

Telephone: (714)985-3434

Attn. To111 Tatnall

Page: 7 7

Prosect ID: 3 2 4 8 6 - 0 0 0 Project Name: De lph i System Corp.

Method: 8082, Polycl-ilorinated Bipheilyls (PCBs) by GC QC Batch No: 091605

American Environmental -- Testing ... Laboratory inc. 2834 &2908 North Naorni Street, Burbank. CA 91504 a DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 F a x : (818) 845-8840. www.actli lb.com

ANALYTICAL RESULTS Site

Telephone: (714)985-3434 Alt~i: Tom Tatt~all

Page: 78

Project ID: 32486-000 Project Name: D e Lnrii System Corp.

Method: 601017000CAM, CAM Title 22 Metals (SW-846) QC Batch No: 091605

Date Prepared Preparation Method p - ~ ~

~ . . Arsenic

~Uarium .~ . -

Cadmium -

Copper :l,ead

~~ .. .~ ' -. - . - ..~ . I Mercury (By EPA 7470) 1 o .oo1 1 0 . 002 ; ND ND

- ~~ . ~-~.. I ~ i G b d e i i u m 0 . 0 1 ! 0 . 0 5 1 ND ND - -

Nickel 7

~p prn Silver

~~ - Tlialiiuln -~ ~p~

;Vanadium --

I l inc ~~ ~ ~p~ ~~ .

American Environmental Testing Laboratory Inc. -. -. - 2814 &2908 Nortli Naomi Streel, Burbank. CA 91504. DOHS NO: 1541;LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840. www.aerlah.com

ANALYTICAL RESULTS

Ordered By

I-Iale~ & Aldrr~ii

Telephone: (714) 985-3434 Attn : Tom Tatnall

Page 7 9 Project ID: 32486-000 Project Name: Deiphi System Corp

AETL Job Number Submicced Cllenc

7~~-~~~p-~ I --.- . . I ~ ~ ~ . .

D z t e P r e p a r e d 0911612005 i 1.. . ! ~ ~p~~ ~ ~p D a t e Ana lyzed

-- - ~ Matrix I Aqueous . . QC Batch Number 091605 -1~ ~ . - - .. i

American Environmental Testing Laboratory Inc. 2834 a2908 North Naoini Street, Burbank. CA 91504 .DOHS NO: i541,LACSDNO: 1018l Tel: (888) 288-AETL. (818) 845-8200 - Fax: (818) 845-8840 * www.act lab.co~n

ANALYTICAL RESULTS

Page: 8 0 Pro'ect ID: 32486-000

Del hi S stem Cor . Method: 6010/7000CAM, CAM Title 22 Metals (SVJ-846)

Q_UALITYCONTR.OLXEPORT

QC Batch No: 091605 Sample Spiked: 34603.36 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mglL

- -- .- - S DUP RPD ! MSIMSD I KPD !

% I % Limit , % Limit

. .

Cadmium

iCobalt

Selcniuiii

QC Batch No: 091605 Sample Spiked: 34603.36 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mg1L

98 80-120

Cadmiu~n

Cobalt

American -. Environmental Testing .- Laboratory Inc. 2833 8~2908 Nortb Nao~ni Strect, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840. www.aetlab.com

- ANALYnCAI, RESULTS

Telephone: (714)985-3434 Ann: Tom Tatnall

Page: 82 Pro'ect ID: 32486-000

Method: GOlOB.LEAD, Lead, ICP QUALLTY CONTROLREPORT

QC Batch No: 091605 Sample Spiked: 34603.36 QC Prepared: 09/16/2005 QC Analyzed: 09116/2005 Units: mglL

QC Batch No: 091605 Sample Spiked: 34603.36 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mgIL

American Environmental Testing Laboratory Inc. 2834 a2908 North Naolni Strecl,Burbank, CA 91504.DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETL a (818) 845-8200 * Fax: (818) 845-8840. www.actlab.com

ANALYTiCAL RESULTS

Telephone: (714)985-3434 Attn: Tom Tatnall

I'age: 8 3 32486-000

C .+

Method: 8082, Polychloriilated Biphenyls (PCBs) by GC

QUALITYCONTROL RFLeORT QC Batch No: 091505 Sample Spiked: 091605 QC Prepared: 0911512005 QC Analyzed: 0912012005 Units: uglL

QC Batch No: 091505 Sample Spiked: 091605 QC Prepared: 09/15/2005 QC Analyzed: 0912012005 Units: ug1L

American Environmental Testing Laboratory Inc. 2834&2c)08 North Naorni Street, Burbanli, CA 91504 .DOHS NO: 1541,I.ACSDNO: 10181 Tel: (888) 288-AE'TL. (818) 845-8200 ' Fax: (818) 845-8840. www.aetlab.com

ANALYTICAL RESULTS

Telephone. (714)985-3434 Attn: Tom Talnall

Page: 8 4 32486-000

Method: 8260B, Volatile Organic Compounds by GCIMS (SW846) Q L ~ L I T Y ~ C ~ T K O I ~ . R E P O R T

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 0911512005 QC Analyzed: 0911512005 Units: uglL

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: ugll

American Environmental Testing Laboratory Inc. - 2834 8~2908 Noilh Naomi Street, Burbank, CA 91504 .DOHS N O : 1541,LACSDNO: iOi8l Tel : (888) 288-AETI,. (818) 845-8200 Fax: (818) 845-8840 www.actlab.com

ANALYTICAI, RESULTS

Ordered By S i t e

Telepho~~e. (714)985-3434 Altn: Tom Tatnall

Page: 8 5 32486-000

Method 8270C, Semivolatile Organic Compounds by GCIMS (SW-846) QUALITY CONTROL REPORT -

QC Batch No: 092005 Sample Spiked: 092005 QC Prepared: 09/2012005 QC Analyzed: 0912112005 Units: uglL

~ .... ~. , UP i MS DUP ; RPD MSIMSD , MS RPD

I I v % REC / % %Limit I %Limit

QC Batch No: 092005 Sample Spiked: 092005 QC Prepared: 0912012005 QC Analyzed: 09/21/2005 Units: uglL

American Environmental Testing ... Laboratory Inc. 2834 &2908 North Naorni Strcct,Burbank, CA 91504 .DOHS NO: 1541,I.ACSDND. 10181 Tel: (888) 288-AETI,. (818) 845-8200. Fax: (818) 845-8840 - www.act lab.com

AN.4L YTICAL RESULTS

Ordered By Maley & Aldiich

Attn: Torn Tatnall

Site

Page: 86 Prqject ID: 3 2 4 8 6 - 0 0 0 Projcct Name: Delphi System Corp.

Method: 8310, Poly~luclear Aromatic Hydrocarbons (SW-846) W A L E Y CONTROL REPORT

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 09/29/2005 Units: ug/L

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 0911612005 QC Analyzed: 09/29/2005 Units: ug/L

1 ~ . - - .- . - 1:iuorznc

~

I 1 . 0 0 0 4 1 7 4 1 75-125' ,

Phel~enthrenc -~~p . .- O . 5 0 1 0 . 4 5 . . ~ . - . . - -. .. I Pvicnc t 0 . 5 0 0 . 4 3 i 8 5 / 60-110 1

American Environmental Testing Laboratory Inc. -.

2814 a2908 North Naomi Strszt,Rurbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200. Fax: (818) 845-8840 - www.aetlah.com

ANALYTICAL RESULTS


S i t e

Page: 8 7 32486-000

Method: M8015D, TPH as Diesel and Heavy Hydrocarbons Using GCIFID QUALTY CONTROL REPORT

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 09/23/2005 Units: mglL

Analvtes cen Recov % REC , % %Limit O O Limit

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 09/23/2005 Units: mg1L

American Environmental .... Testing Laboratory Inc. 2814 &2Y08 North Naorni Street, Burbank, CA 91504 'DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200. Fax: (818) 845-8840. www.aet1ab.com

ANALYTICAL RESULTS

Attn: Tom Tatnall

Page: 8 8 Project ID: 3 2 4 8 6 - 0 0 0 Pmiert Nnme. Deipnl Svs i rem Corp

S i t e

1 ." ,--. . - Method: M8015G, TPH as Gasoline and Light I-Iydrocarbons Using GCIFID

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: mg/L

I . ~ MSDUP MSDUP MSDUP ' s e w YG REC r0.521103

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: mg/L

I-, I % REC , % Limit . . L .- ,.. - I L . . . . . T 112 1 75-125 I

i . 1 -

American Environmental Testing Laboratory Inc. 28348~2908 Norill Naorni Slreci. Burbank, CA 91504 .DOI-1S NO: I541.1,ACSDNO: 10181 Tei: (888) 288-AETL * (818) 845-8200 * Fax: (818) 845-8840 * www.aetlab.com

ANALYTICAL mSUI,TS

Telephone: (7 14)985-3434 Attn: Tom Tat~lall

Page: 89 Project ID: 3 2 4 8 6 - 0 0 0 project NaIne: De lph i System Corp.

~p-~ ~~~

Method: (6010B.LEAD), I,ead, ICP QUALITY CONTROI,REPORT

QC Batch No: 091605-1 Sample Spiked: 34603.01 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mg/Kg

QC Batch No: 091605-1 Sample Spiked: 34603.01 QC Prepared: 09/16/2005 QC Analyzed: 0911612005 Units: mglKg

Analytes

1 Lcad

LCS ' LCS LCS 'LCSILCSD'

Recov ' % REC %Limit I

1 - ;

American Environmental Testing Laboratory Inc. 28348~2908 Nortii Naomi Street, Burbank, CA 91504.DOHS NO: 1541,I.ACSDNO: 10181 Tcl: (888) 288-AETL * (81 8 ) 845-8200 - Fax: (8 18) 845-8840 . www.act lab.com

ANALYTICAL RESULTS

Ordered By Hale) & Aldrlch

Telephone: (7 14)985-3434 Attn: Toin Tatilall

Page: 90 Project ID: 32486-000 Prnirrl N Z ~ P D e l p h i System Coru

S i t e

Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)

QC Batch No: 091605 Sample Spiked: 34602.01 QC Prepared: 0911612005 QC Analyzed: 09116/2005 Units: mg1Kg

..-., , ~p~~~~~ Cadmium r~ ~ . .~ Chromium

Cobalt 1.1 : 80-12 . . - Copper -.

I . ..I--... M o l l hiienum

Nickel .~ I Sc i r i i i i i in F.~ll . - - -. ~~~

Silver .~~ 1.05 - 105

American Environmental Testing Laboratory Inc. 28348~2908 Nortli Naomi Street, Burbank, CA 91504 .DOI-1S NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL * (818) 845-8200 - F a x : (818) 845-8840 ' wwwaet lab .com

ANALYTICAL RESULTS Page 9 1 PlOJect ID 32486-000 AETL Job Number Submrttd C l ~ e n t 1

1 ame Project Y Jelphl System Corp . I-- 34603 - I 05/15/2005 -- &A - Method: (6010B/7000CAM), CAM 'Title 22 Metals (SW-846)

QC Batch No: 091605 Sample Spiked: 34602.01 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mglKg

Selenium

Silver p~ ~~~ . .~ Thallium

Vanadium ~~ .-. 7inr

American Environmental Testing Laboratory Inc. 28348~2908 North Nao~ni Street, Burbank, CA 91504 .DOHS NO: 1541,L.ACSDNO: IOlXl Tel : (888) 288-AETL * (818) 845-8200 . Fax: (818) 845-8840 - www.aet lah.com

ANALYTICAL RESULTS


Page: 92 32486-000

Method: (60 1 0B/7000CAM), CAM Title 22 Metals (S W-846) Q U A E ~ C O N W L REPORT

QC Batch No: 091605-1 Sample Spiked: 34603.01 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mglKg

~. .

.

Lead 7 i l 80-120 1

American Environmental Testing Laboratory Inc. 28348~2908 North Naomi Street, Burbank, CA 91504. DOHS NO: 1541.LACSDNO: lOi81 Tel : (888) 288-AETL a (818) 845-8200 - Fax: (818) 845-8840 - www.act lab.com

ANALYTICAL RESULTS Page 93 Project ID 32486-000 / AETL Job Number S u b m ~ t t d C l ~ e n t p , o j e c t ~ a l n e Celpnl System Corp. 1 3 4 6 0 3 1 09/11/2005

- - - lI&A I

Method. (6010B/7000CAM), CAM litle 22 Metals (SW-846)

QC Batch No: 091605-1 Sample Spiked: 34603.01 QC Prepared: 09/16/2005 QC Analyzed: 09/16/2005 Units: mg1Kg

American Environmental Testing Laboratory Inc. 28148~2908 Nortli Naoini Street, Burhank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 - Fax: (818) 845-8840. www.aetlab.com

ANALYTICAL RESULTS

Ordered By Ilaley & Aldrlch

Telephone: (7 14)985-3434 Attn: 'Tom Tatnall

Page: 94 Project ID: 32486-000 Pvnirrt N a m e . Delphi Svstem Corp

Site

Analvtes

QUAI,IT~ CONTROI; REPORT

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 0911512005 QC Analyzed: 0911612005 Units: mgiKg

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09115/2005 QC Analyzed: 09/16/2005 Units: mglKg

American Environmental Testing Laboratory Inc. 2834 &290R North Nao~ni Street, Burbank, C A 91504 * DOllS NO: 1541, LACSDNO: 10181 Tel: (888) 288-AETL . (818) 845-8200 - Fax: (818) 845-8840 - www.aetlab.corn

ANALYTICAL RESUI,TS


Page: 9 5 32486-000

Method: (8082), Polychlorinated Biphenyls (PCBs) by GC _QUALITY CONTROL REPORT

QC Batch No: 092105 Sample Spiked: 092105 QC Prepared: 09/21/2005 QC Analyzed: 09/21/2005 Units: mglKg

P D MSMSD MI RFD 1 % % Limit ! % Limit '

QC Batch No: 092105 Sample Spiked: 092105 QC Prepared: 09/21/2005 QC Analyzed: 09/21/2005 Units: mgiKg

American Environmental Testing Laboratory Inc. 28348~2908 North Naomi Street, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL . (818) 8 4 5 - 8 2 0 0 . Fax: (818) 845-8840 . www.act lab.com

ANALYTICAL RESULTS

~ t t n l Tom Tatnall

Page: 96 Pso'ect ID: 3 2 4 8 6 - 0 0 0

Method: (8260B), Volatile Organic Coinpounds by GC/MS (SW846) QUA= CONTIZOL REPORT

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: ugiKg

. ~ .~-- Metl~yl-tert-butyl ethcr (MTBE)

Toluene (Methyl benzene) - .. .- 'frichlorodhcnc

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: uglKg

~-~~ . . . -~ .~ I-teii-but 1 sthcr (MTBE) 5 0 . 0 0 4 3 . 5 .

American Environmental Testing Laboratory Inc. 2834 &2908 North Naumi Sweet, Burbank, CA 91504.11OHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200 Fax: (818) 845-8840 . www.aetlah.com

ANALYTICAL RESL'L,TS

Site

Page: 97 32486-000

' C

Method: (8260B), Volatile Organic Compoullds by GUMS (SW846) OJALITY COINTTROL REPORT

QC Batch No: 091605 Sample Spiked: 34603.14 QC Prepared: 09/1612005 QC Analyzed: 0911612005 Units: uglKg

QC Batch No: 091605 Sample Spiked: 34603.14 QC Prepared: 09/16/2005 QC Analyzed: 0911612005 Units: uglKg

t-but I ether (MTBE) ~ . .

American Environmental Testing Laboratory Inc. 2834 8~2008 North Naomi StrccL, Burbank, CA 91504. I>ORS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL . (818) 845-8200. Fax: (818) 845-8840 - www.aerlab.com

ANALYTICAI, RESULTS

Ordered By Hale) gi Aldr~ch

Telephone: (714)985-3434 Attil: Tom Tatllall

Page: 98 Project ID: 3 2 4 8 6 - 0 0 0 prnicr+ N Z ~ P . De.lpRi Svs tern Corp

S i t e

Method: (8270C), Semivolatile Organic Compoullds by GCIMS (SW-846) QUALITJ CONTROL REPORT

QC Batch No 091505 Sample Splked: 34603.02 QC Prepared: 0911512005 QC Analyzed: 0911612005 Unlts: mglKg

QC Batch No: 091505 Sample Spiked: 34603.02 QC Prepared: 0911512005 QC Analyzed: 0911612005 Units: mglKg

American Environmental Testing .... Laboratory Inc. 2834 &2908 North Naoini Strcct, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL . (818) 845-8200 -Fax : (818) 845-8840. www.aet1ab.com

ANALY'I'ICAL RESULTS

Ordered By 1 tlaley & Aldricli

Si t e

Telephone: (714)985-3434 Attn: Tom Tah~all

Page: 9 9 Pro'ect ID: 32486-000

Method: (831 O), Polynuclear Aromatic Hydrocarbons (SW-846) Q1JALITY COKTROL REPORT

QC Batch No: 091505 Sample Spiked: 32603.33 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: rnglKg

QC Batch No: 091505 Sample Spiked: 32603.33 QC Prepared: 09/15/2005 QC Analyzed: 09/15/2005 Units: mglKg

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burhank. CA 91 504. DOIFIS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL - (818) 845-8200 Fax : (818) 845-8840 - www.ast lah.com

AKAI.,YTICAL RESULTS

Ordered By 1 Hdley & Ald~icli

Telephone: (7 14)985-3434 Attn: Toin Tatnall

Site

Page: 100 32486-000

Method: (M8015D), TPH as Diesel and Heavy Hydrocarbons Using GCIFID QUALITY CONTROL REPORT

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 0911612005 Units: mglKg

D

I lmit a imit

QC Batch No: 091505 Sample Spiked: 091505 QC Prepared: 09/15/2005 QC Analyzed: 0911612005 Units: mglKg

American Environmental Testing Laboratory Inc. 28349i2908 North Naomi Strczt,Rurbailk, CA 91504 -DOHS NO: 1541,LACSDNO: 10181 T r l : (888) 288-AETL. (818) 845-8200 * F a x : (818) 845-8840 * www.act iab.corn

ANALYTICAL i%SULTS

O r d e r e d By Hale) & Aldr~ch

S i t e

Telephone: (7 14)985-3434 Atln: To111 Tatnall

Page 1 0 1 Project ID. 32486-000 1 AETL ~ o b N u m b e r Submitted Clrent Project Name Deiph- System Corp. I 34603 - -- i 09/15/2005 1 lh&A -

Method: (MSOlSG), TPM as Gasoline and Light Hydrocarbons Usiilg GCIFID QUALITY CONTROL REPORT

QC Batch No: 091505 Sample Spiked: 34603.29 QC Prepared: 0911512005 QC Analyzed: 09/15/2005 Units: mg/Kg

QC Batch No: 091505 Sample Spiked: 34603.29 QC Prepared: 09115/2005 QC Analyzed: 09115/2005 Units: mg1Kg

American Environmental Testing Laboratory Inc. 2834&2908 Nortli Naonli Slrecl, Burbank, CA 91504 -DOHS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 - www.aet1ab.com

Data Qualifiers and Descriptors

Data Qualifier:

* -

B:

D:

E :

H:

J :

M:

S6:

SX:

X :

In the QC section, sample results have been taken directly fiom the ICP reading. No preparation factor has been applied.

Analyte was present in the Method Rlailk.

Result is fioln a diluted analysis.

Result is beyond calibratio~l limits and is estimated.

Analysis was perfovmed over the allowed holding time due to circumstances which were beyond laboratory control.

Analyte was detected . However, the analyte concentration is an estimated value, which is between the Method Detection Iimit (MDL) and the Practical Quantitation Limit (PQL).

Matrix spike recovery is outside control limits due to matrix interference. Laboratory Control Sample recovery was acceptable.

Surl-ogate recovery is outside control limits due to matrix interference.

The analysis o r the sanlple required a dilution such that the surrogate concentration was diluted below the method acceptance criteria.

Results represent LCS and LCSD data.

%Limi: Percent acceptable limits

YORE(:: Percent recovery.

C:on.L: Acceptable Control Limits

Concc: Added concent~atio~i to tlre sample.

LCS: Laboratory Control Sample

MDL: Method Detection Lin~it is a statistically derived number which is specific for each instriunent, each method, and each compound. It indicates a distinctively detectable qual~tity with 99% probability.

MS Matrlx Sp~lce

MS Dl: Matr~x Sp~ke Duplicate

American Environmental Testing Laboratory Inc. 2834 &2908 North Naolni Strecl, Burbank. CA 91504-DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 'Fax: (818) 845-8840. www.aetlab.coin


ND: Analyte was not detected in the sample at or above MDL.

PQL: Practical Quantitation Limit or ML (Minimum Level as per RWQCB) is the miilirnnm concentl-ation that be quantified with inore than 99% confidence. Taking into account all aspects of the entire analytical iiistrumentation and practice.

Recov: Recovered concentralion in ihe sample.

RPD: Relative Perccnt Difference

American Environmental Testing ..... Laboratory ... Inc. 2834 &2908 North Naomi S11,eel. RurhanL, CA 91504 DOHS NO: 1541,LACSDN Tc l : (888) 288-AETL (818) 845-8200. Fax: (818) 845-8840. www.aei l

':1CT 0 5 2905

f, .'.~ ~ ~ . . ::,.4- Ordered Bv

Telephone: (714) 985-3434

Attention: Tom Tatnall


Site: 1201 N. Magnolia Avenue

Anaheim, CA 92801

Znclosed please find results of analyses of 2 water and 3 soj.1 samples which were analyzed as specified on the attached chain of custody. If there are any questions, please do not hesitate to call.

Checked By: a Approved By: Cyrus Razmara, Ph.D.

Laboratory Director

American Environmental Testing Laboratory Inc. 2814 North Naomi Street Burbank, CA 91504 a DOHS NO: 1541. LACSD NO: 10181

CHAIN OF CUSTODY RECORD a 3 c ,~.,, d ~ q j r - 4 '"i " -3 L: *,-, \'# k?

American Environmental Testing .- Laboratory Inc. 28148~2908 North Naoini S:ree:,Burbailk, CA 91504*DOHS NO: 1541,L.ACSI)NQ 10181 Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840 - www.aetlab.com

ANALYTICAL RESULTS S i t e

Teiephoi~e (71 4)985-3434 Aflll Torn Tatnall

Page: 2

Project ID: 32486-000 Project Name: Delphi Sys tem Corp.

Method: (8260B), Volatile Organic Compou~lds by GCIMS (SW846)

i Cl~lorofor~ii (Tiichloiomelhane) 8

~.~ .... Dibromomethilne -- ~- I -2-Dichlorobenzeae

American Environmental Testing Laboratory .- - Inc. 2834 8 ~ 2 9 0 8 Nol-ti1 Naonri Street, Burbank, CA 91504eDOHS NO: 154I,L,ACSDNO: 10181 Tel : (888) 2 8 8 - A E T L (818) 845-X200 - Fax: (818) 845-8840 . www.ac t l ab .co rn

ANALYTICAL RESULTS

Page: 3

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: D e l p h i System Corp.

Method: (8260B), Volatile Orgaiiic Compounds by GC/MS (SW846) QC Batch No: 092005

---- ~p~~~~ ---- Isopropyibenzene ~

p-Isopropyltoli~ene

Naplrtlialene ~~. ... .

11-Propyibcnzene : ?*\,?.'~",,

American -. Environmental Testing Laboratory Inc. 28148~2908 North Naomi Street, Rui-bank. CA 91504.DOtIS NO: 1541.LACSDNO: 10181 Tcl: (888) 288-AETL * (818) 845-8200. Pax: (818) 845-8840 - www.aetlab.com

ANALYTICAL E S U L T S

Page: 4

Project 1D: 3 2 4 8 6 - 0 0 0 Project Name: Delphi System Corp.

Method: (8260B), Volatile Organic Compou~lds by GCIMS (SW846) QC Batch No: 092005

American Environmental Testing Laboratory Inc. 2834 a 2 9 0 8 Nonli Naorni Slrzzt,Rusbank, CA 91504 .DOIIS NO: 1541,LACSDNO: lOl81 Tcl : (888) 288-AETL - (818) 845-8200 - Fan: (818) 845-8840 www.aerlab.com

ANALYTICAL RESULTS Ordered By I H,!Ie) & Aldr~ch

Telephone: (714)985-3434 Attn: Tom Tat~lall

Page: 5

I'roject ID: 3 2 4 8 6 - 0 0 0 Prqject Name: Delphi Syscem Corp.

Method: (M8015G), TPH as Gasoline and Light Hydrocaxbons Using GCIFID QC Batch No: 091905

American - Environmental ...... Testing Laboratory Inc. 2834 &290X North Naolni Strect, Burbank, CA 91504 .DOI-IS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL - (8 18) 845-8200 - Fax: (818) 845-8840. www.ae1lab.com

AKALYTICAL RESULTS Ordered B y

00 Soiith Kraemer Blvd

S i t e


Page: 6

Project ID: 32486-000 Project Name: De lph i Sys tem Corp.

Method: (M8015D), TPII as Diesel and Heavy Hydrocarbons Using GCIFID QC Batch No: 091905

American Environmental .. ...... Testing Laboratory fnc. 2834 &2908 Nor111 Naorni Strccl, Burhank, CA 91504 .DOHS NO: l541,I.ACSDNO: I0181 Tc l : (888) 2 8 8 - A E T L . ( 8 IS) 845-8200 Fax: (818) 845-8840 . www.act lab.com

ANALYTICAL RESULTS Ordered By Site

00 South Kraemer Blvd.

Telephone: (714)985-3434 Attn: Torn Tatr~all

Page: 7

32486-000

Method: (83 10); Polynuclear Aromatic Hydrocarbons (SW-846)

....

Aceiiaplithyiene

American Environmental Testing Laboratory Inc. -. ..

2834 &2908 North Naomi Sireei,i3ul%ank, CA 91504.1)OIIS NO: 1541,LACSDNO: 10181 l 'e l : (888) 288-AETL - (818) 845-8200. Fax: (81 8) 845-8840 a www.aetlab.coin

- ANALYTICAL RESTJLTS

Page: 8

Project ID: 32486-000 Project ?*T 1 a~ne: Delphi Systen Corp.

Method: (83 lo), Polynuclear Aromatic Hydrocarbons (SW-846)

American Environmental Testing Laboratory Inc. 2834 a2908 Norih Uaomi StreeLBurbank, CA 91504 e11OHS NO: iS41,LACSDNO: 10181 Tel: (888) 288-AETL ' (818) 845-8200 * Fax : (818) 845.8840 - www.ac t i ab .com


I Halc) R: Aldrich 500 South Icraemer Blvd.

Telephone: (714)985-3434 Attn: lorn Tatiiali

S i t e

Page: 9


Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 091905

.~ Date Sampled --

I Azobenzenc Bcnzidine

--

Benzo(b)fluoranth

Beliroic Acid

-. . l~is(2-~hloroethox~)1ne~lia"~

American Environmental Testing Laboratory Inc. 2834 &2908 North Naorni Street, Ruibank, CA 91504 .DOHS NO: 1541.1,ACSDNO: 10181 T e l : (888) 288-AETI- ' (818) 845-8200 * Fax: (818) 8 4 5 - 8 8 4 0 . www.aet lah.corn

ANALYTICAL RESULTS

Page: 1 0

Pso'ect ID: 32486-000

Method: (8270C), Semivolatile Organic Compounds by GUMS (SW-846)

- - - 1 0.25 1 0 . 5 0 1

2-Methylnaphthalene

4-Nitroaniline Nilrobei~zenc (NR)

American Environmental -. Testing Laboratory Inc. 2834 a2908 North Naolni Street, Rorbaiik, CA 91504 .DOIHS NO: 1541,LACSDNV: 10181 Tel: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840 ' www.aetlab.com

ANALYTICAT, RESIJLTS

Page: 11

Project ID: 3 2 4 8 6 - 0 0 0 Project Narne: Delphi System Corp .

Method: (8270C), Semivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 091905

American Environmental Testing Laboratory Inc. .. .... 2834 8~2908 North Naomi Street, Burbani

American Environmental Testing .. Laboratory Inc. 2834 &2908 Norlii Naon~i Street, Burhank, CA 91504*DOHS NO: 1541,LACSDNO: 1018l Tcl: (888) 288-AETL. (818) 845-8200 - Fax: (818) 845-8840 ' www.aetiah.com

ANALYTICAL RESULTS Ordered B y

I Hale) & A i d i i ~ h 500 5outh Kiaemer Blvd

Site

Suite 370 I I Telephone: (714)985-3434 Attn: Torn Tah~all

Page: 13

Project ID: 32486-300 Project Name: D e l p h i system Corp.

Method: (8082): Polychlorinated Biphenyls (PCBs) by GC QC Batch No: 091905

Dale Sampled

Arocior-1260 (PCB-1260) -

American Environmental Testing Laboratory Inc. 2834 &2908 North Naorni Street, Burbank, CA 91504 -DOl lS NO: 1541,LACSDNO: 10181 Tcl : (888) 288-AETI, * (818) 8 4 5 - 8 2 0 0 . Fax: (818) 845-8840 www.ael lab.com

ANALYTICAL RESULTS S i t e

0 Soutli Kracrner Blvd.

Telephone: (714)985-3434 Attn: To111 Tatnall

Page: 1 4

Project ID: 32486-000 Project Name: Delphi sys tern Corp.

. ~

Units . -. . . --

Dilution Factor

-. - ~ - - , ~~.. . . .. - . Aroclor-1232 (I'CB-I 232) 0 .04 -~ ~~~ ...... ~-~~ ---. ~ ~ Aroclor- 1242 (PCB-1242)

~..... ~- Aroclor-1248 (PCB-1248)

-. .. hroclor-1254 ( ~ ~ F 2 5 4 ) . 0 . 10 -. Aroclor-1260 (I'CB-1260) ND

....~ - -- ... . - Aroclor- 1262 (PCB- 1262) 0 .04

... . .~ 0 . 0 4 0 .10 Aroclor-I268 (PCB-1268) 1 ND

Our Lab I.D. Surrogates

34b34.113 31(~34.00 i R e c . i R e c .

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Svcel, Burbank, CA 91504.DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL . (818) 845-8200 ' Fax : (818) 845-8840 www.aetlab.com

ANALYTICAL RESULTS

00 South I

American Environmental Testing Laboratory ...... Inc. 2834 8 ~ 2 9 0 8 North Naorni Street, Burhank, CA 9 1504. DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AEYL (818) 8 4 5 - 8 2 0 0 . Fax: (818) 845-8840 - www.aet lab.com


I Haley & Aidrlch 500 South Kraerner Blvd.

I Suite 370

I Telephone: (714)985-3434 Alln: Tom Tatnali

Page: 1 6

Project ID: 32486-300 Project Naine: Delphi systern Corp.

Method: 8260B, Volatile Organic Coillpounds by GCIMS (SW846) QC Batch No: 092005

1 Preparation ]Method Date Analyzcd

~A

4-Chiorotolue

i 1~2-Dibro1no-3-ci1loropropane (DBCP) Dibron~ociiloromethane

~ . - ..... ~~ h-Dibromoelhnne (EDB)

',T' 2834 &2908 North Naolni Strcet, Burhank, CA 91504. UOHS NO: 1541.1aACSDNO: 10181

3bg$i,# Tel: (888) 288-AETL. (818) 845-8200 - Pax: (818) 815-8840. www.aet lab.com

Page: 1 7

1'ro.jecl ID: 3 2 4 8 6 - 0 0 0 Project Name: Delphi System Corp.

Method: 8260B, Volatile Organic Compounds by GCIMS (SW846) QC Batch No: 092005

American Environmental Testing Laboratory Inc. -. - 2834 &2908 Nortii Naoini Stl.ect, Burbank, CA 91504 .DOHS NO: l541,LACSDNO: 10181 Tel: (888) 288-AETL * (818) 845-8200 -Fax : (818) 845-8840. www.aetlah.conr

ANALYTICAL RESIJLTS

Page: 18


Method: 8260B, Volatile Organic Compounds by GCiMS (SW846) QC Batch No: 092005

I Date Satnpled ~~~~~ ~~~ ~. , . ~~~ ~-~~~~ 1 Date Prepared ..... -~ . . ~

Preparation Method I 5 0 3 0 ~ 503(

American .- Environmental Testing L m Inc. 2834 &2908 North Nao~ni Srrcct. Rurbank, CA 91504. DOHS NO: 1541,IACSDNO: 10181 Tel: (888) 288-AETL.. (818) 845-8200 Fax: (81 8) 845-8840. www.aet1ab.com

ANALYTICAT, RESIJLTS

Telephone: (714)985-3434 Attn: Tom Tatliall

Page: 1 9

Project ID: 32486-090 : AETL job Number' submitted Ciient I'roject Name: De lph i System Corp. 4634 09/16/200

Method: M8015G, TPH as Gasoline and Light Hydrocarbons Using GCIFIU

~-

. .

American -. Environmental ... Testing .. Laboratory Inc. 2834 8~2908 North Naoini Strect, Burbank, CA 91504 .DOHS NO: 1541,1,ACSDNO: 10181 l 'cl: (888) 288-AE'rLs (818) 845-8200 - F a x : (818) 845-8840 - www.actlab.com

ANALYTICAL RESULTS

'Telephone: (714)985-3434 Attn: Tom latnall

Page: 2 0

Project ID: 32436-000 Project Narne: oclphi Sysi.ern Corp.

Method: M8015U, TPIi as Uiesei and I-lcavy Hydrocarbons Using GCIFID QC Batch No: 091605

Date Sampled - . - Date Prepared

i $ ~ j ~ Z i o n ,- ~~ Method .. . Date ~ n a l ~ z e d -~ ~ Matrix ~~p~~ .

American -- Environmental Testing Laboratory Inc. 2834 8~2908 Nortlr Nao~ni Street, Burbank. CA 91504 'DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETI,. (818) 845-8200. Fax: (818) 845-8840 - wwwact lab .com

ANALYTICAI, RESIJLTS

00 South Icraemer Bivd.


Page: 2 1

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: D e l p h i System Corp.

.

Method: 8310, Polyiiuclear Aromatic Hydrocarbons (SW-846) QC Batch No: 091605

28148~2908 Nortli Naoini Street. Burbank. CA 91504 IIOMS NO: IS41,LACSDNO: 10181 Tcl : (888) 288-AETL * (818) 845-8200 . Fax: (818) 845-8840 * www.aetlab.com


I Hale\ K: Aldr~ch 0 0 South Kraeiuer Blvd.


Site

1201 N Magnol~a Avenue Anaheim, CA 92801

Page: 22

Project ID: 3 2 4 8 6 - 0 0 0 Project Name: D e l p h i Sys tem Corp . !

..........

Method: 8270C, Semivolatile Organic Compouilds by GCIMS (SW-846) QC Batch No: 092005

........... --

...........

............ -

....

. . ......... - Rsilzo(ii)anthracene ...............

Benzo(b)iluoranthe~~c ... 13enzo(g,h,i)pcrylenc

Benzo(k)fluoranthciie - .............

Bcnzoic Acid nenzyi Alcohol

2-Cliloronaphihaiene .

4-Chlorophenyl phenyl ethcr ..................... ..

American Environmental Testing Laboratory ... . Inc. 2834 8~2908 Nol-lh Naomi Stmcc. Burhank, CA 91504 .DOHS NO: 1541,LACSDNO: 101X1 Trl: (888) 288-AETL - (818) 845-8200 ' Fax: (818) 845-8840. www.aetlab.com

ANAI,YTICAL RESULTS

Page: 2 3

Prqject ID: 32486-000 Project Narne: Delphi S y s t e m Corp.

Method: 8270C, Semivolatile Organic Coinpounds by GCIMS (SW-846) QC Batch No: 092005

American - Environmental Testing Laboratory Inc. .- 28348~2908 Nol.th Naorni Strcct, Burbank , CA 91504 .DOAS NO: 1541,I,ACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 ' Fax: (818) 845-8840 - www.aetlab.com

ANALYTICAL RESULTS

Page: 2 4

Project ID: 32486-000 D e i hi S stem Cor .

Method: 8270C; Seinivolatile Organic Compounds by GCIMS (SW-846) QC Batch No: 092005

American - Environmental Testing Laboratory .... Inc. 2834 a2908 North Naomi Streci. Burbank, CA 91504 .DOEIS NO: 1541,IBCSDNO: 10181 l'el: (888) 288-AE'rL (818) 845-8200. Fax: (818) 845-8840. www.actlab.com

ANA1,YTICAL KESU1,TS Ordered By Site

I'elepiione: (714)985-3434 Attn: Tom Tatnall

Page: 2 5

Project ID: 32486-000 Project Name: De Lphi S y s t e n Carp.

Dale Analyzed Matrix Units

~roc~or-1242 ( ~ ~ i i - 1 2 4 2 ) p~

Aroclor-I248 (I'CB-1248)

Aroclor-1254 (PCB-1254) zoclor-1260 (PCB-1260)

American Environmental Testing Laboratory Inc. 2814 &2908 North Naomi Stl-cct, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL . (81 8) 845-8200 - Fax: (81 8) 845-8840 * www.act1ab.com


Hale) & Aldr~ch 500 South Icraemer Dl ld

S i t e

Telephone: (714)985-3434 Attn: To111 Tatnall

32486-000

Method: 601017000CAM, CAM Title 22 Metals (SW-846)

!-- --

Arsenic

. -p~~ .. ....

Cadmium Chrornium --- ~. ~- Cobalt

- . i'haiiii~ni

~~ ~~ ~ ~~ ~ ~~ .. Varrddiuin 7inr

American Environmental Testing Laboratory Inc. -- -- 2834 8~2908 Nortli Naorni Street, Burbank, CA 91504 .DOHS NO: 1541.I.ACSDNO: 10181 Tei: (888) 288-AETL.. (818) 845-8200. Fax: (818) 845-8840. www.aetlah.corn

ANALYTICAL RESULTS

Ordered By Hale\ R: Aldrich

5 0 0 South Kraerner Blvd. :Suite 370 1 ' I Brea. CA 92821-6723

Telephone: (714)985-3434 Attii: Tom Tatnall

S l t e

11201 N Magnol~a Avenue

Page: 27 Project ID: 32486-000 ProjectName: Delphi. System Corp.

Method: 6010/7000CAM, CAM Title 22 Metals (SW-846) QUALITY CONTROL REPORT

QC Batch No: 092005 Sample Spiked: 34634.05 QC Prepared: 0912012005 QC Analyzed: 0912012005 Units: mglL

Copper

QC Batch No: 092005 Sample Spiked: 34634.05 QC Prepared: 0912012005 QC Analyzed: 09/2012005 Units: mglL

American Environmental - Testing Laboratory Inc. - 2834 8~2908 North Naomi Street, Burbank. CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tcl: (888) 288-AETL (818) 845-8200 - Fax: (818) 845-8840. www.aetiah.corn

ANALYTICAL RESULTS Page: 2 8

32486-000 Project ID:

QC Batch No: 092005 Sample Spiked: 34634.05 QC Prepared: 0912012005 QC Analyzed: 0912012005 Units: mglL

~p~~ .

T~ -, -~

cs ' LCS I- LCS ILEILCSE] , ~ - ~ -~

Concen Recov 1 % REC i %Limit 1 i i 1 i ... -- . 4- 0.011 0.01' 94 80-120

~~. -- 1 ---A -; ---- .I ~+--i 1.00 1.00 100 [ 80-120 i , j I

~~~ -. -- -- I i 1.00 j 1.01' 101 , 80-120 I

, -

American Environmental - Testing Laboratory -- Inc. 2834 8~2908 North Naomi Street, Burbank, CA 91504 .DOHS NO: I541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200. Pax: (818) 845-8840 - www.aeilah.com

- ANALYTICAL, RESlJLTS

Ordered By Hale) 6r Aldl~cl i 500 South Iirdemer Blvd Suite 370

Site

1201 h Maqnolld Avenue

Telephone: (714)985-3434 Alln: Tom Tatnall

Page: 29 Pro'ect ID: 3 2 4 8 6 - 0 0 0

Method: 8082, Polychlorinated Biphenyls (PCBs) by GC QUALITY CONTIIOLPEPORT

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 09/21/2005 Units: uglL

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 09/21/2005 Units: uglL

, -

American Environmental Testing Laboratory Inc. 2814 &2908 Nor111 Naorni Street, Burbank, CA 91504 .DOFIS NO: 1541.LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840 - www.ae1lab.com

- ANALYTICAL RESU1,TS

Ordered By I-laleb & Aidi~ch 500 South I

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Strcct, Busbank. CA 91504 .DOHS NO: 1541,I,ACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840 . www.aetIab.com

ANALYTICAL RESIJLTS

Ordered By I{alc\ & Ald~ lch

YjOO South I

American Environmental .-.- Testing Laboratory Inc. 2814&2Y08 North Naomi Streer. Burbank, CA 91501 .DOHS NO: 1541,LACSDNO: 10181 Tel : (888) 288-AETI.. (818) 845-8200 * Fax: (818) 845-8840 * www.aet lah.com

ANALYTICAL RESIJLTS

South Kraeiner Blvd.

Telephone: (714)985-3434 Attn: Torn Tatnall

Site

Page: 32 Pro'ect ID: 32486-000

' PL co r . Method: 83 10, Polynuclear Aromatic Hydrocarbons (SW-846)

Q U A L I a CONTROL REKORT

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 09/16/2005 QC Analyzed: 0912912005 Units: uglL

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 0911612005 QC Analyzed: 09/29/2005 Units: ug1L

Iiznzo(b)iluoranll,eii ~~~

Benzo(k)iluoranthenc

.. llibcnzo(a,l~)aniliracciie --~-~p~~

Fluoranthcne

lndcno(l,2,3-cd)pyrc11e

Phcnanthrenc .. .

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Streei.Burhank. CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL * (818) 845-8200. Fax: (818) 845-8840 * www.aetlab.com

ANALYTICAL RESULTS

O r d e r e d By Hale\ & Aldr~ch

Bred. CA 92821-6723

Telephone (714)985-3434 Attn Torn Tatnall

S i t e

Page: 3 3 Project ID: 32486-000 projectName: D e l p h i Sys tern Corp.

Method M8015D, TPH as Diesel and Heavy Hydrocarbons Using GCIFIU QUALITY CObJTROL R E P O )

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 0911612005 QC Analyzed: 09/23/2005 Units: mg/L

QC Batch No: 091605 Sample Spiked: 091605 QC Prepared: 0911612005 QC Analyzed: 0912312005 Units: mglL

American -. Environmental Testing Laboratory Inc. .. 28348~2908 no ill^ Naomi Strcet, Burbank, CA 91504 .DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL. (818) 845-8200 Fax: (818) 845-8840. www.aetlab.com

- ANALYTICAL RESU1,TS

Ordered By 'Hale\ & Aldrlch -00 South Kraemrr UlvJ.

Telephone: (7 14)985-3434 Attn: Tom Tatnall

Page: 3 4 Project ID: 3 2 4 8 6 - 0 0 0

D e l h i S scern Cora.

Method. M8015G, TPI-I as Gasoline and Light Iiydrocarbons Using GCIFID QUALITY CON'TROL REPORT

QC Batch No: 091905 Sample Spiked: 091905 QC Prepared: 0911912005 QC Analyzed: 0911912005 Units: mglL

American Environmental - Testing Laboratory Inc. 2834 8 ~ 2 9 0 8 Nortii Naomi Streel, Burhailk, CA 91504 * DOHS NO: 1541.LACSDNO. 10181 Tcl : (888) 288-AETL . (818) 8 4 5 - 8 2 0 0 . Fax: (818) 845-8840 . www.ac t l ab .com

ANALYTICAL RESULTS

Ordered By

Att11: Tom Tatnall

Site

Page: 3 5 Project ID: 32486-300

Dei hi S stern Coi . Method: (60lOB/7000CAM), CAM Title 22 Metals (SW-846)

QUALITY CONTROL REPORT -

QC Batch No: 092005-1 Sample Spiked: 34634.01 QC Prepared: 09120/2005 QC Analyzed: 0912012005 Units: mglKg

.~ .. . . ... Chromium

Cobell

Vanadium ~~

1 1.11 1.00

QC Batch No: 092005-1 Sample Spiked: 34634.01 QC Prepared: Q912012005 QC Analyzed: 09/2012005 Units: mg/Kg

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Street, Burhank, CA 91504 .DOHS NO: i541,LACSDNO. IOSXl Tel: (888) 288-AETL. (818) 845-8200. Fax: (818) 845-8840. www.actlah.corn

ANA4LYTICAL RESULTS Page: 36 Project ID: 32486-000 Pro'ect Name: Delphj. System Corp.

Method: (6010B/7000CAM), CAM Title 22 Metals (SW-846)

QC Batch No: 092005-1 Sample Spiked: 34634.01 QC Prepared: 09/20/2005 QC Analyzed: 09/20/2005 Units: mg/Kg

American Environmental Testing Laboratory -- Inc. 2834 &2908 North Ni~omi Slrezl, Burbank. CA 9 1504. DOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL * (818) 845-8200 - Fax: (818) 845-8840 * www.aetlah.com

ANALYTICAT, RESULTS

S i t e

0 South Kraerner BIsd.

~ t t n l Torn Tatnal l

Page: 37 Project ID: 3 2 4 8 6 - 0 0 0

Dcl hi S stem Cora.

Method: (8082), Polychlori~lated Biphenyls (PCBs) by GC QUAL1T.Y C L N T R O L m R T

QC Batch No: 091905 Sample Spiked: 091905 QC Prepared: 0911912005 QC Analyzed: 09120/2005 Units: mgiKg

QC Batch No: 091905 Sample Spiked: 091905 QC Prepared: 0911912005 QC Analyzed: 09/20/2005 Units: mg1Kg

American Environmental Testing Laboratory Inc. 2814 a2908 North Naolni Slreet,Burbank, CA 91504eDOHS NO: 1541,LACSDNO: 10181 Tel: (888) 288-AETL (818) 845-8200. Fax: (818) 845-8840 ' www.aetlah.com

ANALYTICAL RESU1,TS

Ordered By Hdleq & AIdr~ch 500 South I

American -- Environmental Testing Laboratory Inc. 2834 a2908 North Naomi Strcct, Burbonk, CA 9 I504 a DOHS NO: 1541,LACSDNO. 10181 Tel: (888) 288-APTL . (818) 845-8200. Fax: (818) 845-8840. www.aet Iab.com

ANALYTICAL RESGLTS

O r d e r e d By Itidle\ & Aid~rcli

0 South I

American Environmental Testing - Laboratory Inc. 2834&290X North Naolni Street, Burhank, CA 91504.DOHS NO: 1541,LACSUNO: 10181 Tel : (888) 288-AETL. (818) 845-8200 'Fan: (818) 8 4 5 - 8 8 4 0 . www.aetlab.co1n

ANALYTICAL NSULTS

Ordered By 1&1Ie\ 8L Aldiicl~

Site

~ t t n ; Tom Tatnail

Page: 4 0 Project ID: 32486-000 project Name: De lph i S y s t e m Corp.

Method: (831 O), Polynuclea Aromatic FIydrocarbons (SW-846)

- QI~ALU:YC~NTR~L~REPO~:~ QC Batch No: 091905 Sample Spiked: 091905 QC Prepared: 09/19/2005 QC Analyzed: 0911912005 Units: mglKg

QC Batch No: 091905 Sample Spiked: 091905 QC Prepared: 09/19/2005 QC Analyzed: 09/19/2005 Units: mg/Kg

American Environmental Testing Laboratory Inc. 2834 (1.2908 North Naomi Stieer. Burbank. CA 91504. DOHS NO: 1541.I.ACSDNO: 10181 Tel: (888) 288-AETL - (818) 845-8200 ' Fan: (818) 845-8840. www.aetlab.com

ANALYTICAL RESULTS

~ t t n l Tom Talnall

Page: 4 1 Ptoject ID: 32406-000 projectNarne: Delp!li System Corp.

Method: (M8015D), TPH as Diesel and Heavy IJydrocarbons Using GCIFID QIJALITY_CQNTROL REPORT

QC Batch No: 091905 Sample Spiked: 34634.03 QC Prepared: 09/19/2005 QC Analyzed: 09/19/2005 Units: mg/Kg

Analytes

TPII 7- 1)aev-I 1CI 3-I 77) C Result Concen Recov : % REC Concen 1 Recov % REC O h % Limit % Limit , I 0 .0 500.00 ' 380.00 i 76 500.00 i 415.00 1 83 8.8 75-125 QC Batch No: 091905 Sample Spiked: 34634.03 QC Prepared: 09/19/2005 QC Analyzed: 09/19/2005 Units: mglKg

American Environmental Testing .... Laboratory Inc. 2834 &2908 Nortii Naomi Slreel. Burbank, CA 91504. DOI-1S NO: 1541.1dACSDNO: 10181 Tcl: (888) 288-AEI'L a (818) 845-8200. Fox: (818) 845-8840 . www.aetIab.com

ANALYTICAL RESULTS

Ordered By ilaley & Aidrich 500 South [

American Environmental Testing Laboratory Inc. 2834 8~2908 North Naomi Strret, Burbank. CA 91504 .DOHS NO: 1541,I.ACSDNO: I0181 Tcl: (888) 288-AETL. (818) 845-8200. Fan: (818) 845-8840 www.aetlab.com


Data Qualifier:

1;. In tile QC section, sample results have been talcen directly from the ICP reading. No preparation factor has been applied.

B: Analyte was present in tlie Method Blank.

D: Result is from a diluted analysis.

E: Result is beyond calibratio~l limits and is estimated.

H: Ailalysis was perfol-med over the allowed holding time due to circulnsta~lces which were beyond laboratory contsol.

J : Analytc was detected . However, the analyte concenWation is an estimated value, which is between the Method Detection Liiilit (MDL) and the Practical Quantitatio~~ Limit (PQL).

M: Matsix spike recovery is outside control liluits due to matsix iilterference. Laboratory Control Sample recovery was acceptable.

S6: Surrogate recovery is outside contsol limits due to matrix interference

S8: The analysis of the sample required a dilution such that tile surrogate concentration was diluted below the nietliod acceptance criteria.

X. Results reprcsellt LCS and LCSD data

Definition:

%Limi: Percelit acceptable limits.

%REC: Percent recovery.

C0r.L: Acceptable Control Limits

Conce: Added co~lce~riration to the sanlple.

LCS. Laboratory Co~ltrol Sample

MDL: Method Detection Limit is a statistically derived number which is specific for each instrument, each method, and eacli compound. It indicates a disti~lctively detectable quantity with 99% probability.

American - Environmental Testing Laboratory Inc. .. 2834&2908 North Naorni Strezt,Burbank. CA YI504.DONS NO: 1541,LACSDNO: I0181 Tel: (888) 288-AETL (818) 845-8200. Pax: (818) 845-8840 ' www.astlab.com


ND Analyie was not detected ill the sainple at or above MDL

PQL: Practical Quai~titation Limit or ML (Minimum Level as per RWQCB) is the minimum coilceniraiion that can be quantified wiih inore thail 99% confidence. Taking into account all aspects of the entire a~~alytical i~~s t ru~ne~~ta t ion arid practice.

Recov: Recovered concentration in the sanlple

RPD: Relative Percent Diflerence

american environmental testing laboratory inc. · msimsd i kpd ! % i % limit , % limit . . cadmium...

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