Phase II Environmental Site Assessment ii December 16, 2011

500 Kirkham Street

APN 004-049-001

Oakland, California

TABLE OF CONTENTS

ACRONYMS AND ABBREVIATIONS .................................................................................... iii

1.0 INTRODUCTION AND SCOPE OF SERVICES ......................................................... 1

2.0 BACKGROUND ............................................................................................................... 3

2.1 SITE DESCRIPTION ........................................................................................................... 3 2.2 PREVIOUS INVESTIGATIONS ............................................................................................. 3

3.0 SOIL AND GROUNDWATER INVESTIGATION ...................................................... 6

3.1 INVESTIGATION METHODS ............................................................................................... 6 3.1.1 Sampling and Analysis ............................................................................................... 6

3.1.2 Groundwater Monitoring Well Re-Development and Sampling ................................ 8

3.1.3 Data Evaluation ........................................................................................................... 9 3.2 INVESTIGATION RESULTS ............................................................................................... 10

3.2.1 Scanning for Underground Utilities .......................................................................... 10 3.2.2 Subsurface Conditions .............................................................................................. 10 3.2.3 Soil Quality ............................................................................................................... 10

3.2.4 Grab-Groundwater Quality ....................................................................................... 13 3.3 QUALITY ASSURANCE/QUALITY CONTROL (QA/QC) .................................................... 15

4.0 CONCLUSIONS AND RECOMMENDATIONS ........................................................ 17

5.0 LIMITATIONS ............................................................................................................... 19

6.0 REFERENCES ................................................................................................................ 20

TABLES

1 Soil Sample Analytical Results – TPH, VOCs, SVOCs, Pesticides, and PCBs

2 Soil Sample Analytical Results – Metals

3 Soil Sample Analytical Results – Soluble Lead

4 Grab Groundwater Sample Analytical Results – TPH and VOCs

5 Grab Groundwater Sample Analytical Results - Metals

6 Groundwater Monitoring Well Sample Analytical Results – TPH and VOCs

7 Groundwater Monitoring Well Sample Analytical Results – Metals

8 Quality Control Sample Assessment – Soil

9 Quality Control Sample Assessment – Groundwater

FIGURES

1 Site Location Map

2 Site Plan

APPENDICES

A Boring Permits

B Boring Logs

C Laboratory Analytical Reports

Phase II Environmental Site Assessment iii December 16, 2011

500 Kirkham Street

APN 004-049-001

Oakland, California

ACRONYMS AND ABBREVIATIONS

APN Assessor’s Parcel Number

BART Bay Area Rapid Transit

bgs Below Ground Surface

BTEX Benzene, toluene, ethylbenzene, and xylenes

Caltrans California Department of Transportation

CHHSL California Human Health Screening Level

DCA Dichloroethane

DCB Dichlorobenzene

DCE Dichloroethylene

DTSC Department of Toxic Substances Control

EPA United States Environmental Protection Agency

ESI Environmental Solutions, Inc.

ESL Environmental Screening Levels

LCS/LCSD Laboratory Control Spike/Laboratory Control Spike Duplicate

LUST Leaking Underground Storage Tank

MCL Maximum Contaminant Level

µg/kg Microgram per kilogram

µg/L Microgram per liter

mg/kg Milligram per kilogram

mg/L Milligram per liter

MRL Method Reporting Limit

MS/MSD Matrix Spike/Matrix Spike Duplicate

MTBE Methyl tert-Butyl Ether

ORP Oxygen Reducing Potential

PCB Polychlorinated Biphenyls

PCE Tetrachloroethylene

PID Photoionization Detector

PRG Preliminary Remedial Goals

PSI Professional Service Industries, Inc.

PVC Polyvinyl Chloride

QA/QC Quality Assurance/Quality Control

ROW Right Of Way

RPD Relative Percent Difference

RSL Regional Screening Levels (U.S. EPA)

RWQCB Regional Water Quality Control Board

SAP Sampling and Analysis Plan

STLC Soluble Threshold Limit Concentration

SVOC Semi-volatile Organic Compounds

TCA Trichloroethane

TCE Trichloroethylene

TCLP Toxicity Characteristic Leaching Procedure

TPH-d Total Petroleum Hydrocarbons as Diesel

Phase II Environmental Site Assessment iv December 16, 2011

500 Kirkham Street

APN 004-049-001

Oakland, California

TPH-g Total Petroleum Hydrocarbons as Gasoline

TPH-o Total Petroleum Hydrocarbons as Motor Oil

TTLC Total Threshold Limit Concentration

USCS Unified Soils Classification System

UST Underground Storage Tank

VCA Voluntary Cleanup Agreement

VOC Volatile Organic Compounds

WET Waste Extraction Test

Phase II Environmental Site Assessment 1 December 16, 2011

500 Kirkham Street

APN 004-049-001

Oakland, California

1.0 INTRODUCTION AND SCOPE OF SERVICES

This report presents the results of a Phase II Environmental Site Assessment performed by

Northgate Environmental Management, Inc. (Northgate) for the City of Oakland at 500 Kirkham

Street (Assessor’s Parcel Number (APN) 004-049-001) in Oakland, Alameda County, California

(the Site). The Site consists of an approximate 2.76-acre (500 feet by 250 feet) parcel of land

primarily occupied by an asphalt-paved lot utilized as a construction staging area and storage

yard. The Site is currently owned by the California Department of Transportation (Caltrans). A

Site Location Map is shown on Figure 1 and a Site Plan is shown on Figure 2.

The purpose of the investigation has been to evaluate soil and groundwater quality conditions at

the Site to evaluate possible impacts to potential redevelopment, including impacts to future

commercial or residential occupants and potential worker exposure to contaminants during

construction. A specific redevelopment plan has not been determined at this time. However, for

the purpose of this report we have assumed that redevelopment will include both residential and

commercial uses. This investigation was performed under the United States Environmental

Protection Agency (EPA) Brownfield Assessment Grant # 2B-00T18101-0 for both hazardous

substances and petroleum hydrocarbons. The work was performed in accordance with the

following documents:

Quality Assurance Project Plan, West Oakland Development Area, Oakland, California,

Northgate, September 8, 2009 (the QAPP), and

Sampling and Analysis Plan, Phase II Soil and Groundwater Investigation, 500 Kirkham

Street, APN 004-049-001, Oakland, California, Northgate, August 8, 2011 (the SAP).

According to the Phase I Environmental Site Assessment, 500 Kirkham Street, APN 004-049-

001, Oakland, California dated June 6, 2011, prepared by Northgate, the Site was occupied by

residences and commercial/industrial development (including a variety of commercial/industrial

warehouse and manufacturing operations such as clothing, canned goods, paper products, and

others) from before the 1930s through the mid-1950s. From the mid-1950s through the early

1990s, the entire Site, with the exception of the southwest quarter, was covered by an elevated

section of the Interstate 880 freeway. During this time, the southwest portion of the Site was

occupied by a chemical repackaging operation and an automotive and truck repair businesses.

The freeway was removed from the Site in the early 1990s at which time the entire Site reverted

back to commercial and industrial land use.

The Site is listed as Smilo Chemical Company on the VCP, Envirostor, CERC-NFRAP, RCRA-

SQG, and FINDS databases. The Site is also listed as J & A Truck Repair on the RCRA-SQG,


500 Kirkham Street

APN 004-049-001

Oakland, California

FINDS, HIST CORTESE, LUST, Alameda County CS, and HAZNET databases. These listings

are related to historic use, storage, and release of hazardous materials on the southwest portion of

the Site. Available information indicates that 4,700 cubic yards of contaminated soil was

excavated and removed from the southwest portion of the Site in the 1990s. Groundwater

beneath this portion of the Site reportedly contained a variety of contaminants, including

petroleum hydrocarbons and volatile organic compounds (VOCs). The Site is currently listed as

an open clean-up project undergoing site assessment on the Geotracker website maintained by

the Regional Water Quality Control Board (RWQCB) as of December 30, 1995. The

Department of Toxic Substance Control (DTSC) is listed as the lead agency for oversight.

Within the DTSC Envirostor database, the Site status is listed as inactive and requiring

evaluation as of September 3, 2010. It is understood that the City of Oakland is assisting the

current property owner, Caltrans, in assessing environmental conditions at the Site to evaluate

potential redevelopment options.

The scope of work for this investigation included the following services:

Scanning the property with a metal detecting device to evaluate the Site for the possible

presence of underground utilities;

Collecting soil samples from 16 soil borings advanced to depths of 10 to 15 feet below

ground surface (bgs) across the Site;

Collecting grab groundwater samples from nine of the boring locations;

Re-developing four on-Site groundwater monitoring wells and collecting groundwater

samples;

Selectively analyzing soil and groundwater samples for total petroleum hydrocarbons

(TPH), VOCs, semi-volatile organic compounds (SVOCs), organochlorine pesticides,

polychlorinated biphenyls (PCBs), and metals; and

Preparing this report.


500 Kirkham Street

APN 004-049-001

Oakland, California

2.0 BACKGROUND

2.1 Site Description

The Site is located at 500 Kirkham Street in Oakland, California. The Site consists of an

approximate 2.76 acre (500 feet by 250 feet) parcel of land bounded by 7th

Street on the north, 5th

Street on the south, Union Street on the east, and Kirkham Street on the west. The Site consists

of a paved lot currently used as a storage yard and staging area for a construction company. A

paved, inclined roadway previously used for truck driver training is present on the northern

portion of the Site and an office trailer is located along the western property boundary. A Bay

Area Rapid Transit (BART) right-of-way (ROW) easement transects the southwest corner of the

Site. The southwest portion of the Site situated between the BART easement and Kirkham and

5th

Streets consists of vacant land.

The Site originally consisted of bay-margin wetlands that were partially filled in between 1866

and 1890. In 1902, the Site was bisected between 7th

and 5th

Streets by Poplar Street. Land use

at that time consisted of a mix of residences and commercial/industrial activities. A railroad spur

track entered the southwestern portion of the Site from 5th

Street to serve commercial and

industrial operations that were present on the Site between 1912 and the mid-1950s. Between

the mid-1950s and 1990, the majority of the Site was covered diagonally from northwest to

southeast by an elevated section of the Nimitz (Eastshore) Freeway. The freeway was removed

and relocated about 300 feet south of the Site in the mid-1990s.

Between 1954 and 1984, the southwestern portion of the Site was occupied by Smilo Chemical

Company, a chemical repackaging business. Between 1984 and 1994, this portion of the Site

was occupied by J&A Truck Repair. The Site is currently owned and managed by Caltrans who

acquired the Site in 1994.

2.2 Previous Investigations

A soil sampling program performed in 1981 by the Alameda County Department of Health and

Safety indicated the presence of heavy metals and pesticides in shallow soil at the Site.

However, the actual sampling depths and locations were not reported. In 1992, GeoResource

Consultants collected soil samples from depths of 1 and 3 feet bgs at one location along the

southwestern corner of the Site. Organochlorine pesticides and metals were not detected above

the laboratory method reporting limits (MRLs) in either sample with the exception of lead, which

was detected in the 1-foot sample at 81 milligrams per kilogram (mg/kg). Results from a

California Waste Extraction Test (WET) analysis indicated that soluble lead concentrations did

not exceed the Soluble Threshold Limit Concentration (STLC) for lead.


500 Kirkham Street

APN 004-049-001

Oakland, California

In 1994, Environmental Solutions, Inc. (ESI) performed an investigation that included collecting

six wipe samples from interior walls and floors of the on-Site warehouse and collecting soil and

groundwater samples from 12 locations in the vicinity of an underground storage tank (UST)

present along the western Site boundary (north of the BART ROW) at that time. Borings were

drilled to depths of 4 to 13 feet bgs, with soil samples collected at 1, 5, and 8 feet bgs submitted

for chemical analysis. Analytical results indicated that soils in the vicinity of the UST were

impacted by gasoline, oil and grease, lead, acetone, BTEX (benzene, toluene, ethylbenzene, and

xylenes), and SVOCs. A WET test performed on samples near the UST, former sumps, and an

on-Site railroad spur indicated soluble lead concentrations above the STLC. Six boring locations

were drilled to approximately 10 to 13 feet bgs for collecting groundwater samples. According

to ESI, groundwater beneath the Site was impacted by petroleum hydrocarbons, metals, VOCs

and unknown compounds in the diesel and motor oil range. Heavy metals and VOCs detected in

groundwater exceeded their respective maximum contaminant levels (MCLs, the State primary

drinking water standard), established under Title 22 of the California Code of Regulations.

In 1994, Caltrans entered into a Voluntary Cleanup Agreement (VCA) with the DTSC for the

Cypress Freeway Relocation Project and East Bay Municipal Utility District Sewer Line

Realignment in Oakland and Emeryville, California. The reconstruction project covered 34

separate properties, including the 500 Kirkham Street property. The VCA was subsequently

amended twice in 1996, and once in each 1997, 1999, and 2002.

According to a Site investigation report prepared by Professional Service Industries, Inc. (PSI),

all on-Site structures were demolished in April 1995 and one approximately 2,000-gallon UST

was removed from the Site on August 30, 1995. Petroleum hydrocarbons were detected in soil

and groundwater samples collected from the UST excavation pit. Heavy metals were detected in

a composite sample collected from the excavated soil stockpile. In November 1995, the

southwest portion of the Site was over-excavated and a total of 92 confirmation samples were

collected from the excavation pit. Twenty-five chemicals were detected in the soil samples,

including PCBs, which were found at concentrations exceeding the Region 9 Preliminary

Remedial Goals (PRGs), established by the EPA. The Envirostor database record for the Site,

maintained by the DTSC, notes the completion of soil excavation to 6 feet bgs. However, it

should be noted that a formal report describing the details of this remediation work could not be

located for review. In 2000, PSI installed four monitoring wells at the Site and collected soil

samples from depths of 6.5 and 7 feet bgs. Low levels of VOCs, SVOCs, and heavy metals were

detected in the soil samples. Low levels of TPH as gasoline and diesel, VOCs, SVOCs, and

heavy metals were detected in groundwater beneath the Site. The report concluded that

groundwater monitoring should continue at the Site on a quarterly basis. However, groundwater


500 Kirkham Street

APN 004-049-001

Oakland, California

monitoring data for 2001 and beyond could not be located and it is unclear whether quarterly

groundwater monitoring ever occurred at the Site.


500 Kirkham Street

APN 004-049-001

Oakland, California

3.0 SOIL AND GROUNDWATER INVESTIGATION

3.1 Investigation Methods

3.1.1 Sampling and Analysis

Northgate performed soil and groundwater sampling at the subject Site on August 10 and 11,

2011. Field work included scanning the property with remote sensing equipment to evaluate the

Site for the possible presence of underground utilities. Subsequent to scanning, nine borings

were advanced to depths of 10 to 15 feet bgs for collecting soil and groundwater samples. Seven

additional borings were advanced to a depth of 10 feet bgs for collecting soil samples.

Approximate boring locations are shown on Figure 2. Permits for the borings were obtained

from the Alameda County Public Works Department and are presented in Appendix A.

The borings were advanced using a truck-mounted direct push GeoProbe sampling rig. During

sampling, continuous cores of subsurface materials were collected in clear acetate liners. Upon

removing the sampler from the borehole, the acetate liner containing the soil core was opened at

various intervals, and the soils were visually inspected and screened using a photoionization

detector (PID) for the possible presence of contamination. Borings were logged in the field in

accordance with the Unified Soils Classification System (USCS). Copies of the boring logs are

attached in Appendix B.

Soil samples were collected for chemical analysis at approximate depths of 1, 5, and 7-13 feet

bgs from borings B-1 through B-16. Sample intervals selected for chemical analysis were cut

from the liners, sealed with Teflon tape and plastic caps, labeled, and stored on ice in a cooler for

transport to the testing laboratory under appropriate chain-of-custody control. Soil samples

selected for VOC analysis were collected directly from a cut liner using a TerraCore™ sampler

and were immediately transferred to a pre-weighed laboratory-supplied glass vial preserved with

sodium bisulfate.

Duplicate soil samples were collected at 5 feet bgs from boring B-5 and at 1 foot bgs from

borings B-7 and B-12. Duplicate soil samples were collected immediately adjacent to the

primary sample. The laboratory was instructed to perform analysis on adjoining ends of the two

core samples.

Soil samples collected from depths of approximately 1 and 5 feet bgs were analyzed for the

following constituents:

TPH as diesel and oil (TPH-d, TPH-o) using EPA Method 8015;


500 Kirkham Street

APN 004-049-001

Oakland, California

TPH as gasoline (TPH-g) using EPA Method 8260;

VOCs using EPA Method 8260;

PCBs using EPA Method 8082;

SVOCs using EPA Method 8270; and

17 Metals using EPA 6000/7000 series.

Soil samples collected from a depth of 1 foot bgs were additionally analyzed for:

Organochlorine pesticides using EPA Method 8081.

Soil samples collected from 7-10 feet bgs were initially held pending the results of the 1 foot and

5 foot bgs samples. The following deeper samples were analyzed following receipt of the

shallow soil sample results:

The 10-foot sample from boring B-11 analyzed for TPH-g and VOCs; and

The 9-foot sample from boring B-2 and 8-foot sample from boring B-8 analyzed for

TPH-o and total lead.

Grab groundwater samples were collected at nine borings by lowering a perforated PVC casing

into the borehole and collecting groundwater samples from the casing using a peristaltic pump

with dedicated tubing. A duplicate groundwater sample was collected from boring B-12.

Groundwater samples were placed in laboratory-supplied glassware, labeled, and stored on ice in

a cooler for transport to the testing laboratory under appropriate chain-of-custody control.

Groundwater samples were analyzed for:

TPH-d and TPH-o using EPA Method 8015;

TPH-g using EPA Method 8260;

VOCs using EPA Method 8260; and

17 Metals (dissolved) using EPA 6000/7000 series.

Soil and groundwater samples were analyzed at Torrent Laboratory of Milpitas, California. All

drilling equipment was steam-cleaned or washed and rinsed prior to use at each boring location.

After completion of sampling activities, all borings were backfilled with neat cement in

accordance with the Alameda County Public Works Agency, Water Resources Section

requirements. All soil cuttings generated during this investigation were stored on the Site in a

sealed 55-gallon drum.


500 Kirkham Street

APN 004-049-001

Oakland, California

3.1.2 Groundwater Monitoring Well Re-Development and Sampling

Four groundwater monitoring wells are located on the Site. Well JA-1 is located along the

western property boundary (adjacent to Kirkham Street) and wells JA-2 through JA-4 are located

on the southern portion of the Site (immediately north of the BART ROW). An additional

unmarked well, MW-X, was also observed adjacent to well JA-4. Northgate was unable to

access well JA-1 due to a large storage container which was staged on top of the well box. The

remaining wells were assessed in the field and well construction specifications including depth,

casing diameter and material, surface completion, well security, and installed sampling

equipment were recorded. The wells were re-developed on August 10 and 11, 2011 by gentle

surging and pumping using a disposable bailer and a peristaltic pump with dedicated tubing.

Groundwater field parameters of temperature, pH, electrical conductance, dissolved oxygen, and

oxygen reducing potential (ORP) were recorded at regular intervals during re-development.

Well re-development continued until the water was relatively free of sand, silt, and turbidity and

the field parameters had stabilized to within 10 percent of previous readings. A minimum of 10

casing volumes were purged from each well during re-development. Purge water was stored on-

Site in sealed and labeled 55-gallon drums.

Wells JA-2, JA-3, and JA-4 were sampled on August 15, 2011 using a peristaltic pump with

dedicated tubing. The tubing was positioned at the approximate middle of the water column of

each well. The pumping rate was maintained to control drawdown to less than 0.3 feet. The

pumping rate was maintained below 100 milliliters per minute when collecting samples for

volatile constituent analysis. A duplicate groundwater sample was collected from well JA-4.

All samples were placed in laboratory supplied containers, labeled, and stored on ice in a cooler

for transport to the laboratory under appropriate chain-of-custody control. Samples were

analyzed at Torrent Laboratory of Milpitas, California. Each monitoring well groundwater

sample was analyzed for:

TPH-d and TPH-o using EPA Method 8015;

TPH-g using EPA Method 8260;

VOCs using EPA Method 8260; and

17 Metals using EPA 6000/7000 series.

All non-dedicated sampling equipment was decontaminated by washing with Alconox (a

laboratory-grade detergent) and rinsing with deionized water before use at each well.


500 Kirkham Street

APN 004-049-001

Oakland, California

3.1.3 Data Evaluation

Chemical test results from soil samples collected during this investigation were evaluated using

Environmental Screening Levels (ESLs) established by the California RWQCB (Screening for

Environmental Concerns at Sites with Contaminated Soil and Groundwater, Interim Final,

November 2005, Revised May 2008) and the Total Threshold Limit Concentrations (TTLCs)

established by the State of California (Title 22, California Code of Regulations).

The ESLs were developed to address environmental protection goals presented in the Water

Quality Control Plan for the San Francisco Bay Basin (Basin Plan; RWQCB, 2006), including

protection of groundwater and surface water resources, protection of human health, protection

against vapor intrusion into buildings, and other concerns. The ESLs are developed using a

tiered approach to environmental risk assessment. For site characterization studies such as the

present investigation, Tier 1 ESLs are used as a general screening guide to determine whether

additional investigation, remedial actions, or risk assessment may be required. The Tier 1 ESLs

are not regulatory cleanup standards, and the presence of a chemical at a concentration above the

Tier 1 ESL does not necessarily indicate that adverse impacts to human health or the

environment are occurring, but rather, indicate that a potential for adverse risk may exist and that

additional evaluation may be warranted. The Tier 1 ESLs are conservative, and are generally

based on an assumption of future residential land use, and the potential use of groundwater as

drinking water; assumptions that may not necessarily be applicable to a particular site.

According to the RWQCB Basin Plan, groundwater in the vicinity of the subject Site is classified

as a potential drinking water supply. This report also considers RWQCB ESLs for commercial /

industrial land use and ESLs for evaluating direct human exposure to soil for construction

workers. Based on a reduction in blood lead level benchmarks for children, the DTSC in

September 2009 lowered the established California Human Health Screening Level (CHHSL) for

lead in residential land use to 80 parts per million (ppm) and in commercial/industrial land use to

320 ppm. Those screening levels are used in place of the RWQCB ESLs for lead in soil in this

report. The TTLCs are used to define a waste as a hazardous or non-hazardous waste for landfill

disposal purposes, and do not necessarily have any relation to health risk evaluation.

Groundwater chemical test results were compared to the MCLs (the State Primary Drinking

Water Standards) established under Title 22 of the California Code of Regulations and the ESLs

for evaluating potential vapor intrusion into buildings. Where ESLs were not established, the US

EPA Regional Screening Levels (RSLs) for tap water are provided.


500 Kirkham Street

APN 004-049-001

Oakland, California

3.2 Investigation Results

3.2.1 Scanning for Underground Utilities

Scanning the boring locations with remote sensing equipment (e.g., metal detecting devices) did

not indicate the presence of underground utilities in the vicinity of the borings.

3.2.2 Subsurface Conditions

The majority of the Site is paved with an approximate 4-inch asphaltic concrete that was drilled

through prior to soil sampling each boring, with the exception of borings B-3 and B-16. Boring

B-3 was advanced along the inclined roadway in an unpaved area and boring B-16 was advanced

in the southwest corner of the Site, within a small vacant unpaved lot. Subsurface soils

encountered at the Site consisted primarily of well graded sand. Well graded sand with clay and

clayey sand were encountered in several borings at depths typically ranging from 5 to 10 feet

bgs. Groundwater was encountered in nine of the 16 borings at depths between 6.5 to 8.5 feet

bgs in borings B-1, B-4, B-8, B-11, and B-12 and at depths of 3.5 to 5.5 feet bgs in borings B-5,

B-13, and B-16.

3.2.3 Soil Quality

Soil sample analytical results are presented in Tables 1 and 2, and the laboratory analytical

reports are presented in Appendix C. As shown in Table 1, TPH-g was not detected above the

laboratory MRL in any of the soil samples collected at the Site, with the exception of the 5-foot

sample collected from boring B-3 (0.11 mg/kg) and the 6-foot sample collected from boring B-

11 (150 mg/kg). These borings were advanced at the top of the inclined roadway (B-3) and

immediately west of the office trailer, in close proximity to the location of the former on-Site

UST (B-11), respectively. The measured concentration of TPH-g from boring B-11 (150 mg/kg)

exceeds the Tier 1 and Commercial/Industrial ESLs of 83 mg/kg but does not exceed the

construction worker exposure ESL of 4,200 mg/kg for TPH-g. The 10-foot sample from boring

B-11 was analyzed for TPH-g to evaluate the vertical extent of elevated TPH-g concentrations.

The 10-foot sample did not contain TPH-g above the laboratory MRL of 0.1 mg/kg.

TPH-d was reported in five soil samples collected from the 5-6 foot depth in borings B-3, B-5,

B-11, B-12, and B-15. TPH-d concentrations range from 2.0 to 8.1 mg/kg and do not exceed

ESLs for residential or commercial land use.

TPH-o was detected above the laboratory MRLs in all but five of the samples analyzed, at

concentrations ranging from 4 to 960 mg/kg. Concentrations of TPH-o in three soil samples, the

5-foot sample from B-8 (550 mg/kg), the 1-foot sample from B-9 (720 mg/kg), and the 1-foot


500 Kirkham Street

APN 004-049-001

Oakland, California

sample from B-13 (960 mg/kg), exceed the Tier 1 ESL of 370 mg/kg for TPH-o. The elevated

concentrations of TPH-o do not exceed the commercial/industrial land use ESL of 2,500 mg/kg

or the construction worker exposure ESL of 12,000 mg/kg. As shown on Table 1, deeper soil

samples from all three borings (B-8, B-9, and B-13) did not exceed any of the regulatory

standards considered in this investigation.

VOCs were not detected above the laboratory MRLs in any of the soil samples collected at the

Site, with the exception of the 6-foot sample from B-11 which contained 1,500 micrograms per

kilogram (µg/kg) of ethylbenzene, 5,470 µg/kg of xylenes, 1,600 µg/kg of 1,3,5-

trimethylbenzene, and 4,800 µg/kg of 1,2,4-trimethylbenzene and the 1-foot sample from boring

B-14 which contained 7.7 µg/kg of xylenes and 8.9 µg/kg of 1,2,4-trimethylbenzene

The concentration of xylenes in the sample from B-11 (5,470 µg/kg) exceeds the Tier 1 and

commercial/industrial ESLs of 2,300 µg/kg but does not exceed the construction worker

exposure ESL of 420,000 µg/kg. It should be noted that, the high concentration of hydrocarbons

in the 6-foot sample from boring B-11 required dilution, which increased the MRLs for benzene

and MTBE above their respective Tier 1 and commercial/industrial land use ESLs. VOCs were

not detected above the laboratory MRLs in the 10-foot sample from boring B-11.

SVOCs, organochlorine pesticides, and PCBs were not detected above the laboratory MRLs in

any soil samples analyzed for these constituents.

Test results for metals are shown in Table 2. Antimony, beryllium, molybdenum, selenium,

silver, and thallium were not detected above the laboratory MRLs in any soil samples collected

at the Site. Cadmium was not detected above the laboratory MRLs in any soil samples with the

exception of the 1-foot sample from boring B-11, which contained 1.1 mg/kg of cadmium. The

measured concentration of cadmium does not exceed any of the regulatory standards considered

in this investigation. Barium (27 to 430 mg/kg), chromium (8.5 to 49 mg/kg), nickel (9.2 to 37

mg/kg), and zinc (9 to 130 mg/kg) were detected above the laboratory MRLs in every soil

sample analyzed, but at concentrations below their respective regulatory standards. Cobalt was

measured in 21 soil samples at concentrations ranging from 5.1 to 17 mg/kg. Copper was

measured in 23 soil samples at concentrations ranging from 5.5 to 58 mg/kg. Mercury was

measured in nine soil samples at concentrations ranging from 0.1 to 0.38 mg/kg. None of the

reported concentrations of cobalt, copper, or mercury exceed their respective regulatory

standards.

Arsenic was reported in nearly all soil samples analyzed, at concentrations ranging from 1.7 to

16 mg/kg. All measured concentrations exceed the Tier 1 and commercial/industrial ESLs of


500 Kirkham Street

APN 004-049-001

Oakland, California

0.39 mg/kg and 1.6 mg/kg, respectively. One reported concentration, 16 mg/kg measured in the

1-foot sample from boring B-11, exceeds the construction worker exposure ESL of 15 mg/kg.

Vanadium was reported in all of the soil samples analyzed at concentrations ranging from 15 to

41 mg/kg. With the exception of two soil samples, all of the measured concentrations exceed the

Tier 1 ESL of 16 mg/kg for vanadium. However, none of the reported concentrations exceed the

commercial/industrial land use or construction worker exposure ESLs of 200 mg/kg and 770

mg/kg, respectively. It should be noted that most soils throughout the San Francisco Bay Area

contain arsenic and vanadium at naturally occurring levels that are above the Tier 1 ESLs. In our

opinion, the arsenic and vanadium measured in the samples are generally representative of

naturally occurring background levels and do not represent a significant environmental concern.

Lead was reported in every sample analyzed at concentrations ranging from 2 to 130 mg/kg.

Five of the highest concentrations reported exceed the residential land use CHHSL of 80 mg/kg:

87 mg/kg (1-foot sample from B-9), 98 mg/kg (1-foot sample from B-8), 100 mg/kg (1-foot

sample from B-3), 120 mg/kg (1-foot sample from B-2), and 130 mg/kg (5-foot sample from B-

2). However, none of the reported concentrations exceed the commercial/industrial land use

CHHSL of 320 mg/kg or the construction worker ESL of 750 mg/kg. Given the increasing lead

concentration with depth in boring B-2, the 9-foot soil sample was additionally analyzed for total

lead. This sample contained 2.1 mg/kg, which is below the regulatory screening standards.

Although none of the measured concentrations of metals exceed their respective TTLCs, soil

samples with the nine highest reported concentrations of lead could potentially contain soluble

lead above the STLC of 5 milligrams per liter (mg/L) which could classify a waste as hazardous

waste based on its soluble lead content. To evaluate this potential, four soil samples (B-7-1.0

with lead at 50 mg/kg, B-8-1.0 with lead at 98 mg/kg, B-3-1.0 with lead at 100 mg/kg, and B-2-

5.0 with lead at 130 mg/kg) were additionally analyzed for soluble lead using the WET. One of

the samples (B-2-5.0) was also analyzed for soluble lead using the Toxicity Characteristic

Leaching Procedure (TCLP). Soluble lead test results are presented in Table 3. As shown in the

table, soluble lead was reported at concentrations ranging from 4.1 to 11 mg/L using the WET

and below the MRL of 0.10 mg/L using the TCLP. Lead solubility varied between soil samples

collected from the elevated roadway on the northern boundary of the Site, compared to samples

collected on the eastern half of the Site. As shown on the associated solubility graph on Table 3,

soils from the elevated roadway could potentially contain soluble lead above the STLC of 5

mg/L if the total lead concentration is 170 mg/kg or above. Alternatively, soils from the eastern

half of the Site could potentially contain soluble lead above the STLC when total lead

concentrations are 50 mg/kg or above. Soluble lead content in soil samples B-7-1.0 and B-8-1.0,

located on the eastern corner of the Site, exceed the STLC of 5.0 mg/L for lead and would be


500 Kirkham Street

APN 004-049-001

Oakland, California

classified as a California hazardous waste for landfill disposal purposes if removed from the Site.

Although soils in the elevated roadway contain higher concentrations of total lead it appears to

be in a less leachable form than lead reported in Site-wide soil.

3.2.4 Grab-Groundwater Quality

Groundwater samples were collected from borings B-1, B-4, B-5, B-8, B-9, B-11, B-12, B-13,

and B-16. Chemical test results are presented in Table 4 and 5, and laboratory analytical reports

are presented in Appendix C. As shown in Table 4, TPH-o was not detected above the

laboratory MRL in any of the groundwater samples analyzed. TPH-g was not detected in any

samples, with the exception of groundwater collected at boring B-11 (1,300 µg/L) and B-13 (51

µg/L). The laboratory report notes that the TPH-g results from B-11 do not match the reference

gasoline standard and may be due to contributions from heavy end hydrocarbons (possibly aged

gasoline) and non-fuel hydrocarbons. The 51 µg/L of TPH-g reported at B-13 is between the

laboratory method detection limit (MDL) and the method reporting limit (the MRL, or the

practical quantitation limit – PQL) and is considered “estimated” (J flagged) by the laboratory.

The measured concentration at B-11 exceeds the drinking water ESL of 100 µg/L but does not

exceed the non-drinking water ESL of 5,000 µg/L.

TPH-d was measured only in the groundwater sample from boring B-11, at a concentration of

350 µg/L. The laboratory report noted that the results for TPH-d did not match the reference

diesel pattern and may be fuel lighter than diesel. The reported concentration of TPH-d exceeds

the drinking water MCL of 100 µg/L but does not exceed the non-drinking water MCL of 2,500

µg/L.

VOCs were detected above laboratory MRLs in the groundwater samples collected from five

borings locations. Chloromethane was reported at 0.88 µg/L in groundwater from boring B-4.

Groundwater from boring B-8 contained 4.9 µg/L of chloroform and 0.35 µg/L of methylene

chloride. However, the measured concentration of methylene chloride fell between the MDL

and the PQL and is considered “estimated” (J flagged) by the laboratory. Methyl tert-butyl ether

(MTBE) was reported at 0.69 µg/L in groundwater from boring B-9. The largest suite of VOCs

were reported in groundwater collected at boring B-11 including ethylbenzene (45 µg/L),

xylenes (127 µg/L), isopropyl benzene (6.1 µg/L), n-propylbenzene (21 µg/L), 1,3,5-

trimentylbenzene (26 µg/L), 1,2,4-trimethylbenzene (52 µg/L), n-butylbenzene (4.6 µg/L), and

naphthalene (12 µg/L). The reported concentrations of chloroform, 1,2,4-trimethylbenzene, and

naphthalene exceed the RSLs of 0.19, 15, and 0.14 µg/L, respectively. None of the other

measured concentrations of VOCs in groundwater from borings B-4, B-8, B-9, or B11 exceed

their respective regulatory standards.


500 Kirkham Street

APN 004-049-001

Oakland, California

Groundwater from boring B-13 contained several chlorinated VOCs including: 48 µg/L of

tetrachloroethylene (PCE), 49 µg/L of trichloroethylene (TCE), 1.1 µg/L of vinyl chloride, 9.6

µg/L of cis-1,2-DCE, 1.5 µg/L of trans-1,2-DCE, and 0.61 µg/L of chloroform. The reported

concentrations of PCE, TCE, vinyl chloride, and cis-1,2-DCE exceed the MCLs (the State

Primary Drinking Water Standards) established under Title 22 of the California Code of

Regulations of 5, 5, 0.5, and 6 µg/L, respectively. The reported concentration of chloroform

exceeds the RSL of 0.19 µg/L. All of the detected concentrations of VOCs are well below their

respective ESLs for evaluating potential vapor intrusion into buildings established by the

RWQCB.

As shown in Table 5, with the exception of arsenic, barium, cobalt, molybdenum, nickel, and

silver, metals were not detected above the laboratory MRLs in any grab-groundwater sample

analyzed. Barium (0.022-0.19 mg/L), cobalt (0.0052-0.023 mg/L), molybdenum (0.015-0.043

mg/L), nickel (0.012-0.059 mg/L), and silver (0.0054 and 0.0056 mg/L) were reported at

concentrations below their respective MCLs, where established. Arsenic was measured above

the laboratory MRL in groundwater from two boring locations: B-9 (at 0.02 mg/L) and B 16 (at

0.01 mg/L). The reported concentration of arsenic from boring B-9 exceeds the MCL of 0.01

mg/L for arsenic.

3.2.5 Monitoring Well Groundwater Quality

Groundwater samples were collected from on-Site monitoring wells JA-2, JA-3, and JA-4 on

August 15, 2011. Chemical test results are presented in Tables 6 and 7, and laboratory analytical

results are presented in Appendix C. As shown in Table 6, TPH-d and TPH-o were not detected

above the laboratory MRLs in any of the wells. TPH-g was reported in the primary and

duplicate groundwater samples collected from well JA-4 at concentrations of 180 µg/L and 190

µg/L, respectively. The laboratory report notes that results for both the primary and duplicate

samples did not match the reference gasoline standard and the results are due to discrete peaks of

non-fuel compounds (VOCs). Both measured concentrations of TPH-g exceed the drinking

water ESL of 100 µg/L but do not exceed the non-drinking water ESL of 5,000 µg/L.


500 Kirkham Street

APN 004-049-001

Oakland, California

VOCs were not detected in groundwater sample from the monitoring wells, with the exception of

the primary and duplicate samples from well JA-4. Benzene (0.53 µg/L), 1,1-dichloroethene

(1,1-DCE – 5.2 µg/L in both samples), trans-1,2-DCE (2.6 and 2.7 µg/L), chloroform (0.53

µg/L), and 1,1,2-TCA (0.91 and 0.85 µg/L) were reported at concentrations below their

respective regulatory standards. PCE (36 and 34 µg/L), TCE (140 and 150 µg/L), cis-1,2-DCE

(160 and 170 µg/L), 1,1-DCA (46 and 45 µg/L), and vinyl chloride (2.5 µg/L in both samples)

were measured in the primary and duplicate samples at concentrations that exceed their

respective MCLs, but below their respective ESLs for vapor intrusion. The reported

concentration of chloroform in the primary sample exceeds the RSL of 0.19 µg/L. As previously

discussed, a suite of VOCs were also reported in the grab groundwater sample from boring B-13,

located upgradient of well JA-4. However, the grab groundwater sample collected from boring

B-5, located upgradient of B-13 did not contain VOCs above the laboratory MRLs. The

potential source or the full extent of VOCs in groundwater beneath the Site remains undefined.

As shown in Table 7, with the exception of barium, chromium, cobalt, and nickel, dissolved

metals were not detected above the laboratory MRLs in any monitoring well samples analyzed.

Barium was measured in all four monitoring well samples, at concentrations ranging from 0.074

to 0.17 mg/L. Chromium was only measured in the primary and duplicate samples from well

JA-4, at concentrations of 0.007 and 0.0067 mg/L, respectively. Cobalt was only measured in

the primary and duplicate samples from well JA-4, at concentrations of 0.008 and 0.0079 mg/L,

respectively. Nickel was measured in three of the four groundwater samples, from wells JA-3

and JA-4 (primary and duplicate), at concentrations of 0.036, 0.3, and 0.29 mg/L, respectively.

The reported concentrations of nickel in groundwater from well JA-4 exceed the MCL of 0.1

mg/L for nickel. None of the other measured concentrations of dissolved metals exceed their

respective MCLs.

3.3 Quality Assurance/Quality Control (QA/QC)

Soil and groundwater samples were collected following sampling protocols and QA/QC

procedures outlined in the SAP, prepared by Northgate on August 8, 2011. Chain-of-custody

forms were completed for all samples and samples were preserved according to the analytical

method requirements.

Sampling QA/QC procedures were followed with respect to equipment, field procedures, sample

containers, decontamination, storage, holding times, and field QC sampling outlined in the SAP.

All analyses were performed according to standard methods by Torrent Laboratory in Milpitas,

California. All sample holding times and preservation requirements were met. The laboratory

report noted that high concentrations of hydrocarbons in the 6-foot sample from boring B-11


500 Kirkham Street

APN 004-049-001

Oakland, California

necessitated a methanol extraction for VOCs, as opposed to analyzing from the pre-tared 5035

vials. In this case, the soil sample for methanol extraction was collected directly from the soil

liner.

Method blanks were analyzed for each analytical method performed to assess the level of

contamination introduced by the laboratory. Results of the method blank analysis were all non-

detect, with the exception of TPH-d, TPH-o, methylene chloride, and several metals that were

reported at very low-level concentrations.

Surrogate recoveries were performed by spiking selected samples with a known concentration of

a contaminant (laboratory control spike [LCS] and laboratory control spike duplicate [LCSD])

and the percent recovery was calculated to assess the accuracy of the analytical method.

Surrogate recoveries and the relative percent different (RPD) between duplicate results –

calculated to assess the precision of the data – were all within the acceptable range.

Northgate collected three duplicate soil samples: at the 5-foot depth from boring B-5, the 1-foot

depth from boring B-7, and the 1-foot depth from boring B-12. One grab groundwater duplicate

sample was collected from boring B-12. One duplicate groundwater monitoring well sample was

collected from well JA-4. Comparison of primary and duplicate sample results is shown in

Tables 8 and 9. All duplicate samples contained the same detected compounds at generally

similar concentrations. RPD values for soil duplicates were below 50% and RPD values for

groundwater duplicates were below 30%, indicating the results are acceptable.

Northgate collected equipment blanks for VOCs and metals and a field blank for VOCs in

accordance with procedures outlines in the SAP. Contaminants were not measured above the

laboratory MRLs in any of the equipment and field blanks.

Matrix spike/matrix spike duplicate (MS/MSD) analyses were performed by the laboratory on

one of the samples submitted from this investigation. The percent recoveries for several metals,

1,4-DCB, and TPH-d were outside of laboratory control limits but were within RPD limits. The

associated LCS/LCSD percentage recoveries and RPD were within limits and corrective actions

were not required.


500 Kirkham Street

APN 004-049-001

Oakland, California

4.0 CONCLUSIONS AND RECOMMENDATIONS

Soil in the vicinity of boring B-11, located along the western property boundary, appears

to be locally impacted by TPH-g. The concentration of TPH-g at 6-feet bgs exceeds both

the Tier 1 (residential) and commercial/industrial land use ESLs. Soil in this area should

be excavated and removed off-Site or isolated beneath an engineered cap prior to

redevelopment.

Shallow soil in several locations throughout the Site (borings B-8, B-9, and B-13)

contains concentrations of TPH-o above the Tier 1 (residential land use) ESL. Shallow

soil in these areas should be excavated and removed off-Site or isolated beneath an

engineered cap prior to any residential development. Given the long industrial use of the

Site, localized areas of hydrocarbon impacted soil could be encountered elsewhere. We

recommend additional evaluation of impacted soil if encountered during Site grading

activities to evaluate appropriate management options.

Elevated concentrations of total lead were measured in soil samples collected from the

elevated roadway, located along the northern Site boundary. Although lead in these

samples from the roadway does not appear to be readily soluble, total lead concentrations

exceed the CHHSL for residential land use. The measured concentrations of lead do not

exceed the CHHSL for commercial/industrial land use. If a mixed

residential/commercial redevelopment is proposed for the Site, soil with lead above 80

mg/kg should be excavated and removed off-Site, selectively relocated to commercial

development areas of the Site or isolated beneath an engineered cap prior to any

residential development.

Soluble lead test results indicate that any soil from the main body of the Site containing

total lead greater than 50 mg/kg could potentially contain soluble lead above the STLC of

5 milligrams per liter (mg/L), which would classify the soil as a hazardous waste for off-

Site landfill disposal purposes. Any soil that will be removed from the Site should be

tested for total and soluble lead prior to off-Site disposal.

Petroleum-related VOCs are present in groundwater beneath the southwestern portion of

the Site, in close proximity to the location of a former on-Site UST. Although UST

excavation and soil remediation activities were documented, the results suggest that some

residual contamination may be present in groundwater beneath this portion of the Site.

However, the reported concentrations of petroleum-related VOCs do not exceed their

respective ESLs for vapor intrusion or the MCLs. It is our opinion that petroleum-related


500 Kirkham Street

APN 004-049-001

Oakland, California

VOCs in groundwater appear to be limited in extent and do not represent a significant

concern for potential Site redevelopment.

Chlorinated VOCs are present in groundwater beneath the southern portion of the Site, at

boring B-13 and in well JA-4, located downgradient of boring B-13. PCE, TCE, and

several breakdown products were reported at concentrations above their respective MCLs

but did not exceed their respective ESLs for vapor intrusion. In our opinion, VOCs in

groundwater are unlikely to represent a significant environmental concern, as shallow

groundwater in this area is not expected to be used for drinking water. However, the

source area and full extent of VOCs in groundwater beneath the Site have not been fully

defined, and additional investigation may be warranted. Any construction dewatering

performed at the Site will need to account for VOCs in groundwater.


500 Kirkham Street

APN 004-049-001

Oakland, California

5.0 LIMITATIONS

The purpose of a soil and groundwater quality investigation is to reasonably characterize existing

Site conditions based on the results of a limited target subsurface investigation. In performing

such a study, it is understood that a balance must be struck between a reasonable inquiry into the

Site conditions and an exhaustive analysis of each conceivable environmental characteristic. The

following paragraphs discuss the assumptions and parameters under which such an opinion is

rendered.

No investigation is thorough enough to describe all environmental conditions of interest at a

given Site. If conditions have not been identified during the study, such a finding should not

therefore be construed as a guarantee of the absence of such conditions at the Site, but rather as

the result of the services performed within the scope, limitations, and cost of the work

performed.

We are unable to report on or accurately predict events that may change the Site conditions after

the described services are performed, whether occurring naturally or caused by external forces.

We assume no responsibility for conditions we were not authorized to evaluate, or conditions not

generally recognized as predictable when services were performed.

Environmental conditions may exist at the Site that cannot be identified solely by visual

observation. Where subsurface exploratory work was performed, our professional opinions are

based in part on interpretation of data from discrete sampling locations that may not represent

actual conditions at unsampled locations.


500 Kirkham Street

APN 004-049-001

Oakland, California

6.0 REFERENCES

EPA, 1983. Interim Guidelines and Specifications for Preparing Quality Assurance Project

Plans, 1983.

EPA. 1986. Test Methods for Evaluating Solid Waste, Physical and Chemical Methods (SW-

846). Third Edition of SW-846 with Update I (pages dated September 1992), Update IIA

(pages dated August 1993), Update II (pages dated September 1994), Update IIB (pages

dated January 1995), and Update III (pages dated December 1996).

EPA, 1991. Office of Emergency and Remedial Response (OERR) Directive 9345.3-02, 1991.

Geo/Resource Consultants, Inc. 1992. Site Investigation Report – Area 8, Department of

Transportation, T.O. Number: 04-192201-01, Highway 880, Cypress Reconstruction,

Oakland, California, August 28.

Jonas & Associates, Inc. 1995. Remedial Design and Implementation Plan, Cypress Freeway

Re-Alignment, Oakland, California, September 12, 1995.

Northgate Environmental Management, Inc. 2009. Draft Quality Assurance Project Plan, West

Oakland Development Area, Oakland, California, September 8, 2009.

Northgate Environmental Management, Inc. 2011. Phase I Environmental Site Assessment, 500

Kirkham Street, APN 004-049-001, Oakland, California, June 6, 2011.

Northgate Environmental Management, Inc. 2011. Sampling and Analysis Plan, Phase II Soil

and Groundwater Investigation, 500 Kirkham Street, APN 004-049-001, Oakland,

California, August 8, 2011.

Office of the Federal Register National Archives and Records Administration, 1994. 40 Code of

Federal Regulations (CFR) Part 136, Appendix B, 1994.

Professional Service Industries, Inc. 2000. Site Investigation Report, Task Order Number 04-

192203-RJ, Contract Number 43A0012, Former J & A Truck Repair & Container

Freight Sites, Oakland, California, September 2000.

Regional Water Quality Control Board. 2008. Screening for Environmental Concerns at Sites

with Contaminated Soil and Groundwater, May 2008.


500 Kirkham Street

APN 004-049-001

Oakland, California

TABLES

TABLE 1

Soil Sample Analytical Results - TPH, VOCs, SVOCs, Pesticides, and PCBs

SVOCs PCBs

TP

H a

s G

aso

lin

e

TP

H a

s D

iese

l

TP

H a

s O

il

Ben

zen

e

To

luen

e

Eth

ylb

enze

ne

Xy

len

es

MT

BE

1,3

,5-T

rim

eth

ylb

enze

ne

1,2

,4-T

rim

eth

ylb

enze

ne

Oth

er V

OC

s

SV

OC

s

4,4

'-D

DE

4,4

'-D

DD

4,4

'-D

DT

Oth

er P

esti

cid

es

PC

Bs

mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg mg/kg µg/kg µg/kg µg/kg µg/kg mg/kg

B-1-1.0 1.0 <0.089 <10 160 <8.9 <8.9 <8.9 <13.4 <8.9 <8.9 <8.9 ND ND <9.5 <9.4 <16 ND ND

B-1-5.0 5.0 <0.081 <2 <4 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND -- -- -- -- ND

B-2-1.0 1.0 <0.092 <4.8 120 <9.2 <9.2 <9.2 <13.8 <9.2 <9.2 <9.2 ND ND <20 <20 <20 ND ND

B-2-5.0 5.0 <0.093 <4.8 160 <9.3 <9.3 <9.3 <14 <9.3 <9.3 <9.3 ND ND -- -- -- -- ND

B-2-9.0 9.0 -- -- <4 -- -- -- -- -- -- -- -- -- -- -- -- -- --

B-3-1.0 1.0 <0.084 <10 130 <8.4 <8.4 <8.4 <12.6 <8.4 <8.4 <8.4 ND ND <9.5 <9.4 <16 ND ND

B-3-5.0 5.0 0.110 1

2 2

6.8 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND -- -- -- -- ND

B-4-1.0 1.0 <0.089 <2 12 <8.9 <8.9 <8.9 <13.4 <8.9 <8.9 <8.9 ND ND <2 <2 <2 ND ND

B-4-5.0 5.0 <0.087 <2 <4 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND -- -- -- -- ND

B-5-1.0 1.0 <0.086 <2 12 <8.6 <8.6 <8.6 <12.9 <8.6 <8.6 <8.6 ND ND <2 <2 <2 ND ND

B-5-5.0 5.0 <0.076 2.4 2

4.8 <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- ND

B-5-5.0D 5.0 <0.073 <2 <4 <7.3 <7.3 <7.3 <11.0 <7.3 <7.3 <7.3 ND ND -- -- -- -- ND

B-6-1.0 1.0 <0.094 <2 4 <9.4 <9.4 <9.4 <14.1 <9.4 <9.4 <9.4 ND ND <2 <2 <2 ND ND

B-6-5.0 5.0 <0.079 <2 5.5 <7.9 <7.9 <7.9 <11.9 <7.9 <7.9 <7.9 ND ND -- -- -- -- ND

B-7-1.0 1.0 <0.100 <2 9.2 <10 <10 <10 <15.2 <10 <10 <10 ND ND <2 <2 <2 ND ND

B-7-1.0D 1.0 <0.093 <2 8.9 <9.3 <9.3 <9.3 <14.0 <9.3 <9.3 <9.3 ND -- -- -- -- -- --

B-7-5.0 5.0 <0.077 <2 5.2 <7.7 <7.7 <7.7 <11.6 <7.7 <7.7 <7.7 ND ND -- -- -- -- ND

B-8-1.0 1.0 <0.087 <2 13 <8.7 <8.7 <8.7 <13.1 <8.7 <8.7 <8.7 ND ND <2 <2 <2 ND ND

B-8-5.0 5.0 <0.078 <19 550 <7.8 <7.8 <7.8 <11.7 <7.8 <7.8 <7.8 ND ND -- -- -- -- ND

B-8-8.0 8.0 -- -- <4 -- -- -- -- -- -- -- -- -- -- -- -- -- --

B-9-1.0 1.0 <0.110 <20 720 <11 <11 <11 <16.5 <11 <11 <11 ND ND <19 <19 <32 ND ND

B-9-3.0 3.0 <0.085 <10 270 <8.5 <8.5 <8.5 <12.8 <8.5 <8.5 <8.5 ND ND -- -- -- -- ND

B-10-1.0 1.0 <0.087 <4 88 <8.7 <8.7 <87 <13.1 <8.7 <8.7 <8.7 ND ND <20 <20 <20 ND ND

B-10-5.0 5.0 <0.080 <2 6.3 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND -- -- -- -- ND

B-11-1.0 1.0 <0.082 <10 130 <8.2 <8.2 <8.2 <12.3 <8.2 <8.2 <8.2 ND ND <20 <20 <20 ND ND

B-11-6.0 6.0 150 1

8.1 2

5.2 <1,000 <1,000 1,500 5,470 <1,000 1,600 4,800 ND ND -- -- -- -- ND

B-11-10.0 10.0 <0.1 -- -- <10 <10 <10 <15 <10 <10 <10 ND -- -- -- -- -- --

B-12-1.0 1.0 <0.091 <2 29 <9.1 <9.1 <9.1 <13.7 <9.1 <9.1 <9.1 ND ND <8 <8 <8 ND ND

B-12-1.0D 1.0 <0.076 -- -- <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- --

B-12-5.0 5.0 <0.072 2.2 2

<4 <7.2 <7.2 <7.2 <10.8 <7.2 <7.2 <7.2 ND ND -- -- -- -- ND

B-13-1.0 1.0 <0.081 <20 960 <8.1 <8.1 <8.1 <12.2 <8.1 <8.1 <8.1 ND ND <19 <19 <32 ND ND

B-13-5.0 5.0 <0.076 <2 <4 <7.6 <7.6 <7.6 <11.4 <7.6 <7.6 <7.6 ND ND -- -- -- -- ND

Soil Sample ID Sample Depth

ANALYTE

Total Petroleum Hydrocarbons Volatile Organic Compounds Organochlorine Pesticides


500 Kirkham Street

APN 004-049-001

Oakland, California

1 of 2 December 16, 2011

TABLE 1

Soil Sample Analytical Results - TPH, VOCs, SVOCs, Pesticides, and PCBs

SVOCs PCBs

TP

H a

s G

aso

lin

e

TP

H a

s D

iese

l

TP

H a

s O

il

Ben

zen

e

To

luen

e

Eth

ylb

enze

ne

Xy

len

es

MT

BE

1,3

,5-T

rim

eth

ylb

enze

ne

1,2

,4-T

rim

eth

ylb

enze

ne

Oth

er V

OC

s

SV

OC

s

4,4

'-D

DE

4,4

'-D

DD

4,4

'-D

DT

Oth

er P

esti

cid

es

PC

Bs

mg/kg mg/kg mg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg µg/kg mg/kg µg/kg µg/kg µg/kg µg/kg mg/kgSoil Sample ID Sample Depth

ANALYTE

Total Petroleum Hydrocarbons Volatile Organic Compounds Organochlorine Pesticides

B-14-1.0 1.0 <0.077 <10 280 <7.7 <7.7 <7.7 7.7 <7.7 <7.7 8.9 ND ND <19 <19 <32 ND ND

B-14-5.0 5.0 <0.071 <2 14 <10 <10 <10 <15 <10 <10 <10 ND ND -- -- -- -- ND

B-15-1.0 1.0 <0.085 <10 150 <8.5 <8.5 <8.5 <12.8 <8.5 <8.5 <8.5 ND ND <20 <20 <20 ND ND

B-15-5.0 5.0 <0.077 2.6 2

6 <7.7 <7.7 <7.7 <11.6 <7.7 <7.7 <7.7 ND ND -- -- -- -- ND

B-16-1.0 1.0 <0.075 <4.8 270 <7.5 <7.5 <7.5 <11.3 <7.5 <7.5 <7.5 ND ND <9.5 <9.4 <16 ND ND

B-16-5.0 5.0 <0.092 <2 <4 <9.2 <9.2 <9.2 <13.8 <9.2 <9.2 <9.2 ND ND -- -- -- -- ND

RWQCB ESL - Tier 1 83 83 370 44 2,900 2,300 2,300 23 ne ne na na 1,700 2,400 1,700 na 0.22

RWQCB ESL - Commercial/Industrial 83 83 2,500 44 2,900 3,300 2,300 23 ne ne na na 4,000 10,000 4,000 na 0.74

RWQCB ESL - Construction Worker 4,200 4,200 12,000 12,000 650,000 210,000 420,000 2,800,000 ne ne na na 87,000 120,000 87,000 na 6.7

TTLC ne ne ne ne ne ne ne ne ne ne na na 1,000 1,000 1,000 na ne

NOTES

mg/kg: milligrams per kilogram (parts per million)

g/kg: micrograms per kilogram (parts per billion)TPH: Total Petroleum Hydrocarbons

SVOC: Semi-Volatile Organic Compound

<: Not detected at or above the indicated laboratory method reporting limit

--: Not tested

ND: Not detected above the laboratory method reporting limit; limits vary by compound

ne: Not established

na: Not applicable

ESL: Tier 1 - Environmental Screening Level for shallow soil = <10 feet deep in residential land use (RWQCB, 2008 Table A-1)

Commercial/Industrial - soil screening level for shallow soil = <10 feet deep in commercial/industrial land use (RWQCB, 2008 Table A-2)

Construction Worker - soil screening level for direct exposure of construction/trench worker (RWQCB, 2008 Table K-3)

TTLC: Total Threshold Limit Concentration for defining a waste as a hazardous waste

(1) = Does not match pattern of reference Gasoline standard.

(2) = Not typical of Diesel standard pattern (unknown hydrocarbons present)

Regulatory Standards


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 2

Soil Sample Analytical Results - Metals

An

tim

on

y

Ars

enic

Ba

riu

m

Ber

yll

ium

Ca

dm

ium

Ch

rom

ium

Co

ba

lt

Co

pp

er

Lea

d

Mer

cury

Mo

lyb

den

um

Nic

kel

Sel

eniu

m

Sil

ver

Th

all

ium

Va

na

diu

m

Zin

c

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg

B-1-1.0 1.0 <5 2.3 72 <2 <1 22 <5 12 55 <0.1 <5 9.9 <5 <1 <5 23 23

B-1-5.0 5.0 <5 2 27 <2 <1 26 6.1 <5 2.0 <0.1 <5 19 <5 <1 <5 20 11

B-2-1.0 1.0 <5 5.3 100 <2 <1 31 6.9 44 120 0.31 <5 26 <5 <1 <5 30 120

B-2-5.0 5.0 <5 6.6 190 <2 <1 21 12 40 130 0.24 <5 21 <5 <1 <5 37 130

B-2-9.0 9.0 -- -- -- -- -- -- -- -- 2.1 -- -- -- -- -- -- -- --

B-3-1.0 1.0 <5 4.2 140 <2 <1 36 8.0 29 100 0.19 <5 24 <5 <1 <5 30 99

B-3-5.0 5.0 <5 <1.7 69 <2 <1 23 <5 <5 3.0 <0.1 <5 14 <5 <1 <5 18 16

B-4-1.0 1.0 <5 2.4 67 <2 <1 31 <5 6.5 34 <0.1 <5 19 <5 <1 <5 23 35

B-4-5.0 5.0 <5 1.9 65 <2 <1 25 <5 5.6 12 <0.1 <5 12 <5 <1 <5 20 19

B-5-1.0 1.0 <5 <1.7 37 <2 <1 23 6 <5 2.1 <0.1 <5 14 <5 <1 <5 17 12

B-5-5.0 5.0 <5 1.8 28 <2 <1 45 5.4 5.5 3 <0.1 <5 31 <5 <1 <5 30 19

B-5-5.0D 5.0 <5 2.5 43 <2 <1 30 6.2 <5 2.4 <0.1 <5 29 <5 <1 <5 22 16

B-6-1.0 1.0 <5 <1.7 42 <2 <1 21 <5 <5 2.7 <0.1 <5 13 <5 <1 <5 15 14

B-6-5.0 5.0 <5 <1.7 50 <2 <1 22 <5 <5 1.9 <0.1 <5 9.2 <5 <1 <5 18 9.0

B-7-1.0 1.0 <5 <1.7 53 <2 <1 29 <5 6.8 50 0.12 <5 14 <5 <1 <5 21 130

B-7-1.0D 1.0 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

B-7-5.0 5.0 <5 <1.7 58 <2 <1 25 <5 <5 4.2 <0.1 <5 12 <5 <1 <5 16 13

B-8-1.0 1.0 <5 2.9 76 <2 <1 29 6.3 55 98 0.17 <5 19 <5 <1 <5 24 130

B-8-5.0 5.0 <5 1.8 89 <2 <1 26 <5 6.1 13 <0.1 <5 16 <5 <1 <5 19 22

B-8-8.0 8.0 -- -- -- -- -- -- -- -- 3.8 -- -- -- -- -- -- -- --

B-9-1.0 1.0 <5 4 86 <2 <1 22 6.1 22 87 0.23 <5 20 <5 <1 <5 22 73

B-9-3.0 3.0 <5 3.8 78 <2 <1 38 17 19 44 0.25 <5 24 <5 <1 <5 41 41

B-10-1.0 1.0 <5 1.7 42 <2 <1 23 <5 <5 3.5 <0.1 <5 14 <5 <1 <5 17 13

B-10-5.0 5.0 <5 2.1 47 <2 <1 37 6.7 5.9 3.1 <0.1 <5 31 <5 <1 <5 29 20

B-11-1.0 1.0 <5 16 430 <2 1.1 8.5 9.2 58 18 0.38 <5 16 <5 <1 <5 39 77

B-11-6.0 6.0 <5 4.8 42 <2 <1 30 5.3 5.7 4.3 <0.1 <5 31 <5 <1 <5 29 17

B-12-1.0 1.0 <5 1.7 42 <2 <1 24 <5 <5 2 <0.1 <5 15 <5 <1 <5 17 12

B-12-1.0D 1.0 -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- -- --

B-12-5.0 5.0 <5 2.5 46 <2 <1 44 11 6.1 3.2 <0.1 <5 33 <5 <1 <5 29 20

B-13-1.0 1.0 <5 4.3 94 <2 <1 30 7 19 53 <0.1 <5 33 <5 <1 <5 29 58

B-13-5.0 5.0 <5 2.5 55 <2 <1 49 6.2 6.7 3.5 <0.1 <5 37 <5 <1 <5 37 21

Soil Sample ID Sample Depth

ANALYTE


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 2

Soil Sample Analytical Results - Metals

An

tim

on

y

Ars

enic

Ba

riu

m

Ber

yll

ium

Ca

dm

ium

Ch

rom

ium

Co

ba

lt

Co

pp

er

Lea

d

Mer

cury

Mo

lyb

den

um

Nic

kel

Sel

eniu

m

Sil

ver

Th

all

ium

Va

na

diu

m

Zin

c

mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgSoil Sample ID Sample Depth

ANALYTE

B-14-1.0 1.0 <5 2.7 77 <2 <1 28 5.7 13 46 <0.1 <5 26 <5 <1 <5 22 47

B-14-5.0 5.0 <5 3.4 75 <2 <1 36 6.6 11 7.2 <0.1 <5 30 <5 <1 <5 31 25

B-15-1.0 1.0 <5 3.9 82 <2 <1 25 6.4 18 53 0.1 <5 24 <5 <1 <5 24 56

B-15-5.0 5.0 <5 2.2 31 <2 <1 34 <5 <5 2.4 <0.1 <5 19 <5 <1 <5 23 13

B-16-1.0 1.0 <5 2.5 58 <2 <1 24 5.1 12 41 <0.1 <5 19 <5 <1 <5 21 45

B-16-5.0 5.0 <5 2 50 <2 <1 38 6.9 5.6 3.2 <0.1 <5 29 <5 <1 <5 27 18

RWQCB ESL - Tier 1 6.3 0.39 750 4.0 1.7 750 40 230 80* 1.3 40 150 10 20 1.3 16 600

RWQCB ESL - Commercial/Industrial 40 1.6 1,500 8.0 7.4 750 80 230 320* 10 40 150 10 40 16 200 600

RWQCB ESL - Construction Worker 310 15 2,600 98 39 1,200,000 94 310,000 750 58 3,900 260 3,900 3,900 62 770 230,000

TTLC 500 500 10,000 75 100 2,500 8,000 2,500 1,000 20 3,500 2,000 100 500 700 2,400 5,000

NOTES

mg/kg: milligrams per kilogram (parts per million) ESL: Tier 1 - Environmental Screening Level for soil <10 feet deep in residential land use (RWQCB, 2008 Table A-1)

<: Not detected at or above the indicated laboratory method reporting limit * - California Human Health Screening Level for residential land use established by California EPA (September 2009)

--: Not tested Commercial/Industrial - soil screening level for soil <10 feet deep in commercial/industrial land use (RWQCB, 2008 Table A-2)

TTLC: Total Threshold Limit Concentration for defining a waste as a hazardous waste Construction Worker - soil screening level for direct exposure of construction/trench worker (RWQCB, 2008 Table K-3)



500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 3

Soil Sample Analytical Results - Soluble Lead

WET TCLP

Location Sample ID mg/kg mg/L mg/L

B-2-5.0 130 4.6 < 0.1

B-3-1.0 100 4.1 --

B-7-1.0 50 5.7 --

B-8-1.0 98 11 --

TTLC 1,000

STLC 5

NOTES

mg/kg: milligrams per kilogram (parts per million)

mg/L: Milligrams per liter (parts per million)


--: Not analyzed

TTLC/STLC: Total and Soluble Threshold Limit Concentration for defining a waste as a hazardous waste

WET: California Waste Extraction Test for defining waste as a California hazardous waste

TCLP: Toxicity Characteristic Leaching Procedure for defining waste as federal hazardous waste

Total LeadSoluble Lead

Elevated Roadway

Site-wide

4.6 4.1

5.7

11

0

1

2

3

4

5

6

7

8

9

10

11

12

13

14

0 20 40 60 80 100 120 140 160 180

Solu

ble

Le

ad (

mg/

L)

Total Lead (mg/kg)

Stockpile Samples

Site-Wide Samples


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 4

Grab Groundwater Sample Analytical Results - TPH and VOCs

RWQCB ESL

Vapor Intrusion

TPH as Gasoline µg/L <50 <50 <50 <26 <50 1,300 1

<50 <50 51 J <50 ne 100/5,000 a

TPH as Diesel µg/L <100 <100 <100 <100 <100 350 2

<100 <100 <100 <100 10,000 a

100/2,500 a

TPH as Oil µg/L <200 <200 <200 <200 <200 <200 <200 <200 <200 <200 10,000 a

100/2,500 a

Benzene µg/L <0.5 <0.5 <0.5 <0.41 <0.5 <0.5 <0.5 <0.5 <0.60 <0.5 1,800 1

Toluene µg/L <0.5 <0.5 <0.5 <0.23 <0.5 <0.5 <0.50 <0.5 <0.60 <0.5 530,000 150

Ethylbenzene µg/L <0.5 <0.5 <0.5 <0.19 <0.5 45 <0.50 <0.5 <0.60 <0.5 170,000 300

Xylenes µg/L <1.5 <1.5 <1.50 <0.4 <1.5 127 <1.5 <1.5 <1.80 <1.5 160,000 1,750

MTBE µg/L <0.5 <0.5 <0.5 <0.46 0.69 <0.5 <0.50 <0.5 <0.60 <0.5 80,000 13

Isopropyl Benzene µg/L <0.5 <0.5 <0.5 <0.34 <0.5 6.1 <0.50 <0.5 <0.60 <0.5 ne 680 b

n-Propylbenzene µg/L <0.5 <0.5 <0.5 <0.36 <0.5 21 <0.50 <0.5 <0.60 <0.5 ne 1,300 b

1,3,5-Trimethylbenzene µg/L <0.5 <0.5 <0.5 <0.24 <0.5 26 <0.50 <0.5 <0.60 <0.5 ne 370 b

1,2,4-Trimethylbenzene µg/L <0.5 <0.5 <0.5 <0.4 <0.5 52 <0.50 <0.5 <0.60 <0.5 ne 15 b

n-Butylbenzene µg/L <0.5 <0.5 <0.5 <0.39 <0.5 4.6 <0.50 <0.5 <0.60 <0.5 ne ne

Naphthalene µg/L <1 <1 <1 <0.7 <1 12 <1 <1 <1.2 <1 11,000 0.14 b

PCE µg/L <0.5 <0.5 <0.5 <0.18 <0.5 <0.5 <0.5 <0.5 48 <0.5 420 5

TCE µg/L <0.5 <0.5 <0.5 <0.46 <0.5 <0.5 <0.5 <0.5 49 <0.5 1,800 5

Vinyl Chloride µg/L <0.5 <0.5 <0.5 <0.45 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 13 0.5

cis-1,2-DCE µg/L <0.5 <0.5 <0.5 <0.4 <0.5 <0.5 <0.5 <0.5 9.6 <0.5 17,000 6

trans-1,2-DCE µg/L <0.5 <0.5 <0.5 <0.38 <0.5 <0.5 <0.5 <0.5 1.5 <0.5 19,000 10

Chloroform µg/L <0.5 <0.5 <0.5 4.9 <0.5 <0.5 <0.5 <0.5 0.61 <0.5 1,100 0.19 b

Chloromethane µg/L <0.5 0.88 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.6 <0.5 140 190 b

Methylene Chloride µg/L <5 <5 <5 0.36 J <5 <5 <5 <5 <6 <5 8,100 5

Other VOCs µg/L ND ND ND ND ND ND ND ND ND ND na na

NOTES

mg/l: Micrograms per liter (parts per billion) (1) Does not match pattern of reference Gasoline standard.

TPH: Total Petroleum Hydrocarbons (2) Not typical of Disel standard pattern (possibly fuel lighter than diesel).

<: Not detected at or above the indicated laboratory method reporting limit ESL: Vapor Intrusion - Environmental Screening Level for potential vapor intrusion into buildings

ND: Not detected above the laboratory method reporting limit; limits vary by compound (RWQCB, 2008 Table E-1)

ne: Not established MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)

na: Not applicable a: MCL not established. ESL for drinking water / non-drinking water shown instead (RWQCB, 2008)

J = Indicates an estimated value b: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA

Volatile Organic Compounds


B-5-GW MCLAnalyte

B-8-GW B-9-GW B-11-GW B-12-GW

Sample ID

B-16-GWB-13-GWB-4-GWUnits

B-1-GW B-12-GWD


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 5

Grab Groundwater Sample Analytical Results - Metals

Regulatory

Standards

Antimony mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.006

Arsenic mg/L <0.009 <0.009 <0.009 <0.009 0.020 <0.009 <0.009 <0.009 0.010 0.010

Barium mg/L 0.035 0.044 0.030 0.091 0.19 0.047 0.022 0.091 0.12 1

Beryllium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.004

Cadmium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.005

Chromium mg/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 0.05

Cobalt mg/L <0.005 <0.005 0.023 0.0052 <0.005 0.0060 0.012 0.0095 0.0057 0.011 a

Copper mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 1.3

Lead mg/L <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 <0.014 0.015

Mercury mg/L <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 <0.0002 0.002

Molybdenum mg/L 0.027 <0.009 0.023 0.015 0.016 0.030 0.040 0.043 0.022 0.18 a

Nickel mg/L 0.012 <0.009 0.033 <0.009 <0.009 <0.009 0.019 0.020 0.059 0.1

Selenium mg/L <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 <0.02 0.05

Silver mg/L <0.005 <0.005 0.0054 <0.005 <0.005 <0.005 <0.005 0.0056 <0.005 0.18 a

Thallium mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.002

Vanadium mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.18 a

Zinc mg/L <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 ne

NOTES



ne: Not established

--: Not tested

MCL: Maximum contaminant level for drinking water, California Department of Public Health (October 2008)

a: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA

MCLB-11-GW B-12-GW B-16-GW

Dissolved Metals

B-13-GW

Analyte Units

Sample ID

B-1-GW B-4-GW B-5-GW B-8-GW B-9-GW


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 6

Groundwater Monitoring Well Sample Analytical Results - TPH and VOCs

RWQCB ESL

Vapor Intrusion

TPH as Gasoline µg/L <50 <50 180 1

190 1 ne 100/5,000

a

TPH as Diesel µg/L <100 <100 <100 <100 ne 100/2,500a

TPH as Oil µg/L <200 <200 <200 <200 ne 100/2,500a

Benzene µg/L <0.50 <0.50 0.53 <0.50 1,800 1

Toluene µg/L <0.50 <0.50 <0.50 <0.50 530,000 150

Ethylbenzene µg/L <1.50 <1.50 <0.50 <1.50 170,000 300

Xylenes µg/L <0.50 <0.50 <1.50 <0.50 160,000 1,750

MTBE µg/L <0.50 <0.50 <0.50 <0.50 80,000 13

PCE µg/L <0.50 <0.50 36 34 420 5

TCE µg/L <0.50 <0.50 140 150 1,800 5

1,1-DCE µg/L <0.50 <0.50 5.2 5.2 18,000 6

cis-1,2-DCE µg/L <0.50 <0.50 160 170 17,000 6

trans-1,2-DCE µg/L <0.50 <0.50 2.6 2.7 19,000 10

1,1-DCA µg/L <0.50 <0.50 46 45 3,400 5

Vinyl Chloride µg/L <0.50 <0.50 2.5 2.5 13 0.5

Chloroform µg/L <0.50 <0.50 0.53 <0.50 1,100 0.19 b

1,1,2-TCA µg/L <0.50 <0.50 0.91 0.85 1,200 5

Other VOCs µg/L ND ND ND ND na na

NOTES

g/L: Micrograms per liter (parts per billion)TPH: Total Petroleum Hydrocarbons



na: Not applicable

ESL: Vapor Intrusion - Environmental Screening Level for potential vapor intrusion into buildings

(RWQCB, 2008 Table E-1)

(1) Not typical of Gasoline standard pattern.


a: MCL not established. ESL for drinking water / non-drinking water shown instead (RWQCB, 2008)

b: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA

MCL

Volatile Organic Compounds

JA-3 JA-4 JA-4DAnalyte Units

Sample ID Regulatory Standards

JA-2


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 7

Groundwater Monitoring Well Sample Analytical Results - Metals

Regulatory

Standards

Antimony mg/L <0.009 <0.009 <0.009 <0.009 0.006

Arsenic mg/L <0.009 <0.009 <0.009 <0.009 0.010

Barium mg/L 0.13 0.074 0.17 0.16 1

Beryllium mg/L <0.005 <0.005 <0.005 <0.005 0.004

Cadmium mg/L <0.005 <0.005 <0.005 <0.005 0.005

Chromium mg/L <0.005 <0.005 0.0070 0.0067 0.05

Cobalt mg/L <0.005 <0.005 0.0080 0.0079 0.011 a

Copper mg/L <0.009 <0.009 <0.009 <0.009 1.3

Lead mg/L <0.014 <0.014 <0.014 <0.014 0.015

Mercury mg/L <0.0002 <0.0002 <0.0002 <0.0002 0.002

Molybdenum mg/L <0.009 <0.009 <0.009 <0.009 0.18 a

Nickel mg/L <0.009 0.036 0.30 0.29 0.1

Selenium mg/L <0.02 <0.02 <0.02 <0.02 0.05

Silver mg/L <0.005 <0.005 <0.005 <0.005 0.18 a

Thallium mg/L <0.009 <0.009 <0.009 <0.009 0.002

Vanadium mg/L <0.009 <0.009 <0.009 <0.009 0.18 a

Zinc mg/L <0.009 <0.009 <0.009 <0.009 ne

NOTES



ne: Not established


a: MCL not established, value provided is the Regional Screening Level for tapwater, established by the U.S. EPA

Dissolved Metals

JA-3 JA-4 JA-4D MCL

Analyte Units

Sample ID

JA-2


500 Kirkham Street

APN 004-049-001

Oakland, California


TABLE 8

Quality Control Sample Assessment - Soil

AnalyteB-5-5.0

(mg/kg)

B-5-5.0D

(mg/kg)RPD

B-7-1.0

(mg/kg)

B-7-1.0D

(mg/kg)RPD

B-12-1.0

(mg/kg)

B-12-1.0D

(mg/kg)RPD

TPH-gasoline < 0.076 < 0.073 NA < 0.1 < 0.093 NA < 0.091 < 0.076 NA

TPH-diesel 2.4 < 2 18.2% < 2 < 2 NA -- -- NA

TPH-oil 4.8 < 4 18.2% 9.2 8.9 3.3% -- -- NA

VOCs ND ND NA ND ND NA ND ND NA

SVOCs ND ND NA -- -- NA ND ND NA

PCBs ND ND NA -- -- NA -- -- NA

Arsenic 1.8 2.5 32.6% -- -- NA -- -- NA

Barium 28 43 42.3% -- -- NA -- -- NA

Chromium 45 30 40.0% -- -- NA -- -- NA

Cobalt 5.4 6.2 13.8% -- -- NA -- -- NA

Copper 5.5 < 5 9.5% -- -- NA -- -- NA

Lead 3 2.4 22.2% -- -- NA -- -- NA

Nickel 31 29 6.7% -- -- NA -- -- NA

Vanadium 30 22 30.8% -- -- NA -- -- NA

Zinc 19 16 17.1% -- -- NA -- -- NA

Other Metals ND ND NA -- -- NA -- -- NA

NOTES:

RPD: Relative Percent Difference

mg/kg: milligrams per kilogram

NA: not applicable



--: Sample pairs not analyzed


500 Kirkham Street

APN 004-049-001

Oakland, California

1 of 1 Decmber 16, 2011

TABLE 9

Quality Control Sample Assessment - Groundwater

AnalyteB-12-GW

(µg/L)

B-12-GWD

(µg/L)RPD

JA-4

(µg/L)

JA-4D

(µg/L)RPD

TPH-gasoline < 50 < 50 NA 180 190 5.4%

TPH-diesel < 100 < 100 NA < 100 < 100 NA

TPH-oil < 200 < 200 NA < 200 < 200 NA

Benzene < 0.5 < 0.5 NA 0.53 < 0.5 5.8%

PCE < 0.5 < 0.5 NA 36 34 5.7%

TCE < 0.5 < 0.5 NA 140 150 6.9%

1,1-DCE < 0.5 < 0.5 NA 5.2 5.2 0.0%

cis-1,2-DCE < 0.5 < 0.5 NA 160 170 6.1%

trans-1,2-DCE < 0.5 < 0.5 NA 2.6 2.7 3.8%

1,1-DCA < 0.5 < 0.5 NA 46 45 2.2%

Vinyl Chloride < 0.5 < 0.5 NA 2.5 2.5 0.0%

Chloroform < 0.5 < 0.5 NA 0.53 < 0.5 5.8%

1,1,2-TCA < 0.5 < 0.5 NA 0.91 0.85 6.8%

Other VOCs ND ND NA ND ND NA

Barium -- -- NA 0.17 0.16 6.1%

Chromium -- -- NA 0.007 0.0067 4.4%

Cobalt -- -- NA 0.008 0.0079 1.3%

Nickel -- -- NA 0.3 0.29 3.4%

Other Metals ND ND NA ND ND NA

NOTES:

RPD: Relative Percent Difference

µg/L: micrograms per liter

NA: not applicable



--: Sample pairs not analyzed


500 Kirkham Street

APN 004-049-001

Oakland, California



500 Kirkham Street

APN 004-049-001

Oakland, California

FIGURES


500 Kirkham Street

APN 004-049-001

Oakland, California

APPENDIX A

BORING PERMITS

Alameda County Public Works Agency - Water Resources Well Permit

399 Elmhurst StreetHayward, CA 94544-1395

Telephone: (510)670-6633 Fax:(510)782-1939

Application Approved on: 08/04/2011 By jamesy Permit Numbers: W2011-0515Permits Valid from 08/10/2011 to 08/11/2011

Application Id: 1312327539477 City of Project Site:OaklandSite Location: 500 Kirkham St, Oakland, CAProject Start Date: 08/10/2011 Completion Date:08/11/2011Assigned Inspector: Contact Steve Miller at (510) 670-5517 or [email protected]

Applicant: Northgate Envt. Mgmt. Inc. - Anya Starovoytov Phone: 510-839-0688 x227300 F H Ogawa Plaza, Ste 510, Oakland, CA 94612

Property Owner: State of CA, Dept. of Transportation Phone: 510-286-5322111 Grand Ave, PO Box 23440, Oakland, CA 94623

Client: City of Oakland, Gopakumar Nair Phone: 510-238-6361250 F. H Ogawa Plaza, Ste 5301, Oakland, CA 94612

Total Due: $265.00Receipt Number: WR2011-0240 Total Amount Paid: $265.00

Payer Name : Northgate Paid By: CHECK PAID IN FULL

Works Requesting Permits:

Borehole(s) for Investigation-Environmental/Monitorinig Study - 16 Boreholes

Driller: Penecore - Lic #: 906899 - Method: other Work Total: $265.00

Specifications

Permit

Number

Issued Dt Expire Dt #

Boreholes

Hole Diam Max Depth

W2011-

0515

08/04/2011 11/08/2011 16 2.25 in. 20.00 ft

Specific Work Permit Conditions1. Backfill bore hole by tremie with cement grout or cement grout/sand mixture. Upper two-three feet replaced in kind or

with compacted cuttings. All cuttings remaining or unused shall be containerized and hauled off site. The containers shall

be clearly labeled to the ownership of the container and labeled hazardous or non-hazardous.

2. Boreholes shall not be left open for a period of more than 24 hours. All boreholes left open more than 24 hours will

need approval from Alameda County Public Works Agency, Water Resources Section. All boreholes shall be backfilled

according to permit destruction requirements and all concrete material and asphalt material shall be to Caltrans Spec or

County/City Codes. No borehole(s) shall be left in a manner to act as a conduit at any time.

3. Permittee shall assume entire responsibility for all activities and uses under this permit and shall indemnify, defend

and save the Alameda County Public Works Agency, its officers, agents, and employees free and harmless from any and

all expense, cost, liability in connection with or resulting from the exercise of this Permit including, but not limited to,

properly damage, personal injury and wrongful death.

4. Applicant shall contact Steve Miller for an inspection time at (510) 670-5517 or email to [email protected] at least

five (5) working days prior to starting, once the permit has been approved. Confirm the scheduled date(s) at least 24

hours prior to drilling.

5. Copy of approved drilling permit must be on site at all times. Failure to present or show proof of the approved permit

application on site shall result in a fine of $500.00.

6. Prior to any drilling activities onto any public right-of-ways, it shall be the applicants responsibilities to contact and

Alameda County Public Works Agency - Water Resources Well Permit

coordinate a Underground Service Alert (USA), obtain encroachment permit(s), excavation permit(s) or any other permits

required for that City or to the County and follow all City or County Ordinances. It shall also be the applicants

responsibilities to provide to the Cities or to Alameda County a Traffic Safety Plan for any lane closures or detours

planned. No work shall begin until all the permits and requirements have been approved or obtained.

7. Permit is valid only for the purpose specified herein. No changes in construction procedures, as described on this

permit application. Boreholes shall not be converted to monitoring wells, without a permit application process.


500 Kirkham Street

APN 004-049-001

Oakland, California

APPENDIX B

BORING LOGS

B-1-1.0

B-1-5.0

B-1-7.0

0.1

0.0

0.0

70

90

AS

SW

SW

SC

ASPHALT (4")WELL GRADED SAND WITH GRAVEL (SW); dark yellow-brown (10YR 3/4), ~20% fine tomedium gravels, ~5% clay, ~75% fine sand, damp to moist, loose, no odorWELL GRADED SAND (SW); dark yellow-brown (10YR 4/4), trace gravels and clay, damp tomoist, loose, no odor

Same as above, clay content increases to ~10%

CLAYEY SAND (SC); dark yellow-brown (10YR 4/4), ~40% clay, ~60% fine sand, moist, mediumdense, no odor

Same as above, moisture content increases (moist to wet)

Bottom of borehole at 10.0 feet bgs.

DRILLING METHOD Geoprobe

HOLE SIZE 2.25

DRILLING CONTRACTOR PeneCore

NOTES:

AFTER DRILLING ---

AT TIME OF DRILLING ---

AT END OF DRILLING 8.50 ft

Ground ELEVATION

SURFACE CONDITIONS: Asphalt

GROUNDWATER LEVELS:

LOGGED BY A. Starovoytov CHECKED BY D. Laduzinsky

COMPLETED 8/10/11DATE STARTED 8/10/11

SA

MP

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H(f

t)

1

2

3

4

5

6

7

8

9

10

MATERIAL DESCRIPTION

PAGE 1 OF 1BORING NUMBER B-1

PROJECT NUMBER 1204.22 PROJECT LOCATION Oakland, CA

BORING LOCATIONPROJECT NAME 500 Kirkham

GE

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9/13

/11

300 Frank H. Ogawa Plaza, Suite 510Oakland, CA 94612Telephone: 510-839-0688

PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-10-1.0

B-10-5.0

B-10-9.0

0.1

0.0

0.0

50

97

AS

SW

SC

Asphalt (4")WELL GRADED SAND (SW); dark yellow-brown (10YR 3/4), moist, loose, no odor

Same as above, color changes to yellow-brown (10YR 5/4), clay content increases with depth(~10%)CLAYEY SAND (SC); dark yellow-brown (10YR 4/6), ~60% fine sand, ~40% clay, moist to wet,occasional saturated pores, dense, no odor

Same as above, moisture content increases (wet)

Sand fraction increases to ~70%, clay ~30%



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---


AT END OF DRILLING ---

Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

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DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

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L N

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EN

VIR

ON

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- O

S 1

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.22_

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RIN

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PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-11-1.0

B-11-6.0

B-11-10.0

0.1

0.0

308

275

28.6

4.9

3.3

7.3

70

100

100

100

AS

SW

CL

SW

Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark brown (10YR 3/3), ~70% fine sand, ~30% fineto coarse gravel (angular), damp, loose, no odor

SANDY CLAY WITH GRAVEL (CL); dark brown (10YR 3/3), ~60% clay (low plasticity), ~15% finesand, ~25% fine to medium angular gravels, damp no odor

WELL GRADED SAND (SW); olive (5Y 4/4), trace clay, moist, loose, strong hydrocarbon odorbetween 6' and 8.5' bgs


Same as above, occasional mottling with gray

Same as above, color changes to dark yellow-brown (10YR 4/4) with large patches of gray (2.5Y6/1), moist

Same as above, moisture increases (saturated)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

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L N

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EN

VIR

ON

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- O

S 1

204

.22_

BO

RIN

G_L

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S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-12-1.0

B-12-5.0

B-12-10.0

0.1

0.0

0.0

0.0

90

100

100

100

AS

SW

SW

SC

SW-SC

Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark brown (10YR 3/3), ~80% fine sand, ~20% fineto medium gravel, trace clay, damp, loose, no odor

WELL GRADED SAND (SW); dark yellow brown (10YR 4/6), trace clay, moist to wet, mediumdense, no odor

Same as above, clay fraction increases to 15-20%CLAYEY SAND (SC); dark yellow-brown (10YR 4/6), ~60% fine sand, ~40% clay, wet, mediumdense, no odor

Same as above, moisture increases with depth

WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/6), ~80-85% fine sand,~15-20% clay, occasional mottling, saturated, medium dense



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12





GE

NE

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L N

OR

TH

GA

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EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-13-1.0

B-13-5.0

B-13-8.0

7.3

6.8

7.0

6.8

6.4

6.0

30

100

96

100

AS

SW

SC

Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); very dark gray (10YR 3/1), ~80% fine sand, ~20%fine to medium gravel, damp, medium dense, no odor

CLAYEY SAND (SC); yellowish brown (10YR 5/6), ~60% fine sand, ~40-45% clay, damp, dense,no odor


Same as above, clay content decreases (~20%)

Same as above, clay content decreases (~15%), saturated

Same as above, color changes to light yellow brown (2.5Y 6/3), zones of gray mottling



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

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L N

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EN

VIR

ON

ME

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AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-14-1.0

B-14-5.0

B-14-7.0

1.2

0.7

0.5

90

100

AS

SC

CL

SW-SC

Asphalt (4")CLAYEY SAND (SC); dark yellow-brown (10YR 3/4), ~20% clay, ~10-15% fine to medium angulargravels, ~65% fine sand, moist, loose, no odorSANDY CLAY WITH GRAVEL (CL); dark yellow brown (10YR 4/4), ~20% fine to medium gravel(angular), ~20% fine sand, ~60% clay, damp, medium stiffness, no odor

WELL GRADED SAND WITH CLAY (SW-SC); dark yellow-brown (10YR 4/6), ~85% fine sand,~15% clay, moist to wet, loose, no odor



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

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L N

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TH

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EN

VIR

ON

ME

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AL

- O

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204

.22_

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RIN

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-15-1.0

B-15-5.0

B-15-9.0

0.7

0.5

0.0

90

100

AS

SW

CL

SC

Asphalt (4")WELL GRADED SAND (SW); dark brown (10YR 3/3), ~90% fine sand, ~5-10% fine to mediumgravels, trace clay, damp, medium dense, no odor

SANDY CLAY WITH GRAVEL (CL); dark yellow-brown (10YR 4/4), ~20% fine to coarse gravels(angular), ~15% fine sand, ~65% clay, damp, medium stiffness, no odor

CLAYEY SAND (SC); dark yellow brown (10YR 4/4), ~60% fine sand, ~40% clay, moist, mediumdense, no odor

Same as above, clay content decreases (~20%), moisture increases (wet)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

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EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

NE

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L N

OR

TH

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EN

VIR

ON

ME

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AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-16-1.0

B-16-5.0

B-16-10.0

0.0

0.0

0.0

0.0

0.0

0.0

80

100

100

100

100

SW

SC

SW-SC

WELL GRADED SAND (SW); dark yellow-brown (10YR 3/4), very fine, trace gravels (fine tomedium angular), damp, loose, no odor

Same as above, moisture content increases (moist)

Same as above, moisture content increases (wet), trace wood fragments, clay fraction increasesto ~10%CLAYEY SAND (SC); yellow-brown (10YR 5/6), ~80% fine sand, ~20% clay, moist to wet,medium dense, no odor

Same as above, moisture content increases to ~40%

Same as above, occasional gray mottles, moisture content decreases with depth (moist)

Same as above, moisture increases (wet), clay content decreases (20%)

WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/4), ~85-90% fine sand,~10-15% clay, wet, no odorSame as above, moisture increases with depth (wet to saturated)

Same as above, color changes to light olive brown (10YR 5/4)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

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EN

UM

BE

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PT

H(f

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1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

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L N

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VIR

ON

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- O

S 1

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RIN

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S.G

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-2-1.0

B-2-5.0

B-2-9.0

0.0

0.0

0.0

0.0

70

90

AS

SW

SW

Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); dark olive brown (2.5Y 3/3), ~80% fine sand, ~20%fine to medium angular gravels, damp, loose, no odorConcrete fragments

3" zone with charred wood fragments and discolored soil, no odor

WELL GRADED SAND (SW); dark brown (10YR 3/3), damp, loose, no odor

Charred wood fragments @6' bgs

Same as above, moisture content increases (moist)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION

SURFACE CONDITIONS: Bare soil

GROUNDWATER LEVELS:



SA

MP

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PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

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L N

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EN

VIR

ON

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AL

- O

S 1

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RIN

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-3-1.0

B-3-5.0

B-3-9.0

0.0

0.0

0.0

50

90

SW

WELL GRADED SAND (SW); dark olive-brown (2.5Y 3/3), ~10% fine to medium gravel, rootletspresent, damp, loose, no odor

3" zone of coarse gravel (concrete fragments)

2" zone of increased clay (~10%)

Same as above, color change to very dark brown (10YR 2/2)

Same as above, color changes to dark yellow brown (10YR 4/4), damp to moist

Same as above, clay content increases (~10%)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION

SURFACE CONDITIONS: Bare soil

GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-4-1.0

B-4-5.0

B-4-10.0

6.3

5.6

4.5

4.8

0.0

0.0

0.0

70

70

AS

SW

CL

SW-SC

Asphalt (4")WELL GRADED SAND (SW); brown (10YR 4/3), ~5% fine to medium angular gravels, damp,loose, no odor

Same as above, large pieces of charred wood debris (slight chemical odor) and coarse gravels (6"layer) and red brick fragments moisture content increases to moist

Same as above, color changes to very dark gray-brown (10YR 3/2), moist, loose, fine grainedsand, no odor

Same as above, moisture content increases (saturated), color changes to brown (10YR 4/3), noodor

Same as above, clay content increases (~10%)

LEAN CLAY WITH SAND (CL); greenish-gray (Gley1 6/5G), ~80% clay, ~20% fine sand, stiff,trace rootlets, mottling with orange, no odor

Same as above, sand fraction increases to ~25%

WELL GRADED SAND WITH CLAY (SW-SC); dark yellow brown (10YR 4/4), medium dense,wet, no odor

Same as above, occasional zones of gray mottles



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

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VIR

ON

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- O

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-5-1.0

B-5-5.0

B-5-10.0

5.3

7.7

7.5

6.6

8.1

90

AS

SW

Asphalt (4")WELL GRADED SAND (SW); dark yellow brown (10YR 3/4), ~90% fine sand, ~10% fine tomedium angular gravels, trace clay, damp, loose, no odor

Same as above, clay fraction increases to ~15%

Same as above, content increases (wet to saturated)

Same as above, occasional mottling with light gray, soil becoming more dense with depth, clay at15-20%



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

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9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-6-1.0

B-6-5.0

B-6-9.0

0.0

0.0

0.0

0.0

0.0

80

100

AS

SW

Asphalt (4")WELL GRADED SAND (SW); very dark gray-brown (10YR 3/2), ~5-10% fine to medium angulargravel, damp, slight chemical odor (possibly hydraulic fluid)

Same as above, slight hydrocarbon odor from 2.5' to 4' bgs, color changes to black (10YR 2/1)

Same as above, strong hydrocarbon odor, moisture content increases (wet to saturated)

Same as above, saturated conditions, slight organic/hydrocarbon (?) odor

Same as above, color changes to dark yellow brown (10YR 4/4)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-7-1.0

B-7-5.0

B-7-7.0

0.0

0.0

0.0

50

50

AS

SW

Asphalt (4")WELL GRADED SAND (SW); dark yellow brown (10YR 4/4), trace gravel, moist, loose, no odorVery dark soil (possibly charcoal) for ~2"

Same as above, color changes to dark brown (10YR 3/3), glass and charcoal or charred woodfragments throughout

Same as above color changes to dark yellow-brown (10YR 4/4), moisture content increases(saturated)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

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S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-8-1.0

B-8-5.0

B-8-8.0

1.7

1.2

0.0

0.7

0.0

0.0

50

70

100

100

AS

SW

CL

SW-SC

Asphalt (4")WELL GRADED SAND (SW); brown (10YR 4/3), trace fine gravels, damp, loose, no odor

3-4" zone of gravel and debris (crashed brick, concrete, charred wood, white rock (?), tilefragments

Large piece of concrete (~2" dia.)

Same as above, moisture content increases (saturated), color changes to dark yellow-brown(10YR 4/4)

Same as above, clay content increases (~10-15%)LEAN CLAY WITH SAND (CL); yellow-brown (10YR 5/6) with heavy gray mottles, ~75% clay,~25% fine sand, trace rootlets, wet, no odor

WELL GRADED SAND WITH CLAY (SW-SC); dark yellow-brown (10YR 4/6), ~90% fine sand,~10% clay, wet, medium dense, no odor

Same as above, clay fraction decreases (~5%)

Same as above, moisture content increases (saturated)



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

OG

S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG

B-9-1.0

B-9-3.0

B-9-13.0

15.7

9.9

7.5

70

33

100

AS

SW

SW

Asphalt (4")WELL GRADED SAND WITH GRAVEL (SW); very dark brown (10YR 2/2), ~80% fine sand,~20% fine to coarse gravels, trace clay, damp, loose, slight chemical odor

Same as above, concrete fragments/coarse gravel at 3.8'

No recovery. Driller reports feeling a void between 5' and 10' bgs. Some coarse gravel recovered(possibly concrete)

WELL GRADED SAND (SW); dark gray-brown (2.5Y 4/2), ~90-95% fine sand, ~5-10% clay,saturated, loose, organic odor



HOLE SIZE 2.25


NOTES:

AFTER DRILLING ---



Ground ELEVATION


GROUNDWATER LEVELS:



SA

MP

LE T

YP

EN

UM

BE

R

DE

PT

H(f

t)

1

2

3

4

5

6

7

8

9

10

11

12

13

14

15





GE

NE

RA

L N

OR

TH

GA

TE

EN

VIR

ON

ME

NT

AL

- O

S 1

204

.22_

BO

RIN

G_L

OG

S.G

PJ

9/13

/11


PID

(pp

m)

RE

CO

VE

RY

%

U.S

.C.S

.

GR

AP

HIC

LOG


500 Kirkham Street

APN 004-049-001

Oakland, California

APPENDIX C

LABORATORY ANALYTICAL REPORTS

Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350RE: 500 Kirkham

Torrent Laboratory, Inc. received 40 sample(s) on August 23, 2011 for the analyses presented in the following Report.

Dear Dennis Laduzinsky:

Work Order No.: 1108073 Rev: 1

All data for associated QC met EPA or laboratory specification(s) except where noted in the case narrative.

Torrent Laboratory, Inc. is certified by the State of California, ELAP #1991. If you have any questions regarding these test results, please feel free to contact the Project Management Team at (408)263-5258; ext 204.

DateAugust 18, 2011

Patti Sandrock

Page 1 of 260Total Page Count: 260

Date: 8/18/2011

Client: Northgate Environmental Management Inc.

Project: 500 Kirkham

Work Order: 1108073

CASE NARRATIVE

No issues encountered with the receiving, preparation, analysis or reporting of the results associated with this work order.

Note for 8260B/GCMS-GRO: Final result & PQL (Reporting limit) has been corrected for actual mass from pre-tarred 5035 VOAs for all samples except 1108073-014A. Due to high concentration of hydrocarbons, methanol extraction was performed. Sample was analyzed from liner.

Analytical Comments for method S_6010B, 1108073-002 MS/MSD, QC Analytical Batch ID 406266, Note:The % recoveries for Barium, Copper and Nickel are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.

Analytical Comments for method S_8270C, 1108073-002 MS/MSD, QC Analytical Batch ID 406315, Note:The % recoveries for 1,4-DCB are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.

Analytical Comments for method S_TPHDO, 1108073-002 MS/MSD, QC Analytical Batch ID 406315, Note:The % recoveries for TPH as Diesel are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.

Analytical Comment for Method S_8081, 1108073-002 MS/MSD, although an MS/MSD was extracted it is not reported due to the high concentration of compounds found in the parent sample (reported at a 20X dilution).

REVISIONS:

Per client request, STLC extraction and analysis for Lead was performed on sample -004A.

Note: Extraction of 50 g sample / 500g 0.2M Sodium Citrate Solution was performed according to wet extraction procedure (WET) which was rotated in a rotary shaker for 48 hours.

STLC:Extraction started on 8/23/11 @4.30 PM and ended on 8/25/[email protected] PM. Rev 1 (8/26/11)


Report prepared for: Dennis Laduzinsky

Northgate Environmental Management Inc.

Date Received: 08/23/11

Date Reported: 08/18/11

Sample Result Summary

1108073-001B-1-1.0

Parameters: PQLMDL UnitResultsDFAnalysisMethod

Arsenic mg/Kg2.31.70.28SW6010B 1

Barium mg/Kg725.01SW6010B 1Chromium mg/Kg225.00.0590SW6010B 1

Copper mg/Kg125.00.0900SW6010B 1

Lead mg/Kg551.00.043SW6010B 1Nickel mg/Kg9.95.00.0590SW6010B 1

Vanadium mg/Kg235.00.12SW6010B 1

Zinc mg/Kg235.00.59SW6010B 1

TPH as Motor Oil mg/Kg160208.33SW8015B(M) 1

1108073-002B-1-5.0




Cobalt mg/Kg6.15.00.14SW6010B 1

Lead mg/Kg2.01.00.043SW6010B 1Nickel mg/Kg195.00.0590SW6010B 1


Zinc mg/Kg115.00.59SW6010B 1







1108073-004B-3-1.0





Copper mg/Kg295.00.0900SW6010B 1Lead mg/Kg1001.00.043SW6010B 1

Nickel mg/Kg245.00.0590SW6010B 1

Vanadium mg/Kg305.00.12SW6010B 1Zinc mg/Kg995.00.59SW6010B 1

Mercury mg/Kg0.190.100.01SW7471A 1


Lead (STLC) mg/L4.10.100.0500SW6010B 1







1108073-005B-3-5.0


Barium mg/Kg695.01SW6010B 1

Chromium mg/Kg235.00.0590SW6010B 1Lead mg/Kg3.01.00.043SW6010B 1



TPH(Gasoline) ug/Kg11087158260TPH 1

TPH as Diesel mg/Kg2.02.00.759SW8015B(M) 1TPH as Motor Oil mg/Kg6.84.01.65SW8015B(M) 1

1108073-007B-10-1.0







TPH as Motor Oil mg/Kg888.03.33SW8015B(M) 1







1108073-008B-10-5.0





Copper mg/Kg5.95.00.0900SW6010B 1Lead mg/Kg3.11.00.043SW6010B 1



TPH as Motor Oil mg/Kg6.34.01.65SW8015B(M) 1

1108073-010B-12-1.0




Lead mg/Kg2.01.00.043SW6010B 1

Nickel mg/Kg155.00.0590SW6010B 1Vanadium mg/Kg175.00.12SW6010B 1

Zinc mg/Kg125.00.59SW6010B 1








1108073-011B-12-5.0




Cobalt mg/Kg115.00.14SW6010B 1




TPH as Diesel mg/Kg2.22.00.759SW8015B(M) 1







1108073-013B-11-1.0


Arsenic mg/Kg161.70.28SW6010B 1

Barium mg/Kg4305.01SW6010B 1Cadmium mg/Kg1.11.00.0590SW6010B 1

Chromium mg/Kg8.55.00.0590SW6010B 1

Cobalt mg/Kg9.25.00.14SW6010B 1Copper mg/Kg585.00.0900SW6010B 1

Lead mg/Kg181.00.043SW6010B 1


Zinc mg/Kg775.00.59SW6010B 1









1108073-014B-11-6.0








Ethyl Benzene ug/Kg1500100086SW8260B 100m,p-Xylene ug/Kg48001000190SW8260B 100

o-Xylene ug/Kg67050066SW8260B 100

1,3,5-Trimethylbenzene ug/Kg16001000110SW8260B 1001,2,4-Trimethylbenzene ug/Kg48001000110SW8260B 100

TPH(Gasoline) ug/Kg1500001000017008260TPH 100



1108073-015B-11-10.0


All compounds were non-detectable for this sample.







1108073-016B-14-1.0








m,p-Xylene ug/Kg7.77.71.4SW8260B 11,2,4-Trimethylbenzene ug/Kg8.97.70.84SW8260B 1








1108073-017B-14-5.0





Copper mg/Kg115.00.0900SW6010B 1Lead mg/Kg7.21.00.043SW6010B 1










1108073-019B-15-1.0










1108073-020B-15-5.0















1108073-022B-9-1.0
















1108073-023B-9-3.0










1108073-025B-5-1.0






Zinc mg/Kg125.00.59SW6010B 1








1108073-026B-5-5.0
















1108073-028B-13-1.0









1108073-029B-13-5.0


Arsenic mg/Kg2.51.70.28SW6010B 1Barium mg/Kg555.01SW6010B 1

Chromium mg/Kg495.00.0590SW6010B 1

Cobalt mg/Kg6.25.00.14SW6010B 1Copper mg/Kg6.75.00.0900SW6010B 1

Lead mg/Kg3.51.00.043SW6010B 1


Zinc mg/Kg215.00.59SW6010B 1







1108073-031B-12-1.0 D



1108073-032B-5-5.0 D







Zinc mg/Kg165.00.59SW6010B 1

1108073-033B-1-GW


Barium (Dissolved) mg/L0.0350.0090.002SW6010B 1Molybdenum (Dissolved) mg/L0.0270.0090.002SW6010B 1

Nickel (Dissolved) mg/L0.0120.0090.002SW6010B 1







1108073-034B-12-GW


Barium (Dissolved) mg/L0.0220.0090.002SW6010B 1

Cobalt (Dissolved) mg/L0.0120.0050.002SW6010B 1Molybdenum (Dissolved) mg/L0.0400.0090.002SW6010B 1


1108073-035B-12-GWD









1108073-036B-11-GW


Ethyl Benzene ug/L450.500.15SW8260B 1

m,p-Xylene ug/L1101.00.20SW8260B 1o-Xylene ug/L170.500.13SW8260B 1

Isopropyl Benzene ug/L6.10.500.28SW8260B 1

n-Propylbenzene ug/L210.500.30SW8260B 11,3,5-Trimethylbenzene ug/L260.500.20SW8260B 1

1,2,4-Trimethylbenzene ug/L520.500.33SW8260B 1

n-Butylbenzene ug/L4.60.500.32SW8260B 1Naphthalene ug/L121.00.57SW8260B 1

TPH(Gasoline) ug/L130050228260TPH 1

TPH as Diesel (SG) mg/L0.350.100.0400SW8015B(M) 1


Cobalt (Dissolved) mg/L0.00600.0050.002SW6010B 1

Molybdenum (Dissolved) mg/L0.0300.0090.002SW6010B 1

1108073-037B-9-GW


MTBE ug/L0.690.500.38SW8260B 1

Arsenic (Dissolved) mg/L0.0200.0090.005SW6010B 1

Barium (Dissolved) mg/L0.190.0090.002SW6010B 1Molybdenum (Dissolved) mg/L0.0160.0090.002SW6010B 1







1108073-038B-13-GW


Vinyl Chloride ug/L1.10.600.44SW8260B 1.19

trans-1,2-Dichloroethene ug/L1.50.600.37SW8260B 1.19cis-1,2-Dichloroethene ug/L9.60.600.39SW8260B 1.19

Chloroform ug/L0.610.600.35SW8260B 1.19

Trichloroethylene ug/L490.600.45SW8260B 1.19Tetrachloroethylene ug/L480.600.18SW8260B 1.19

TPH(Gasoline) ug/L5160268260TPH 1.19

Barium (Dissolved) mg/L0.0910.0090.002SW6010B 1Cobalt (Dissolved) mg/L0.00950.0050.002SW6010B 1


Nickel (Dissolved) mg/L0.0200.0090.002SW6010B 1Silver (Dissolved) mg/L0.00560.0050.002SW6010B 1

1108073-039B-5-GW



Cobalt (Dissolved) mg/L0.0230.0050.002SW6010B 1Molybdenum (Dissolved) mg/L0.0230.0090.002SW6010B 1


Silver (Dissolved) mg/L0.00540.0050.002SW6010B 1

1108073-040Equip BLANK




SAMPLE RESULTS

Report prepared for: Date Reported: 08/18/11Date Received: 08/23/11

Northgate Environmental Management Inc.Dennis Laduzinsky

Client Sample ID:

Date/Time Sampled:

Project Number:

Project Name/Location:

08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:

Lab Sample ID: 1108073-001A

Tag Number: 500 Kirkham

Parameters: PrepBatch

AnalyticalBatch

UnitLabQualifier

ResultsPQLMDLDFDateAnalyzed

PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.3Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg72Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg22Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg12Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg55Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg9.9Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg23Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg23Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/KgNDMercury 08/16/11 0.01 0.10 33921


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 7.9 40 340120SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 7.3 40 340120SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 22 40 340120SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 6.3 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 8.4 40 340120SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 7.2 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 12 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 9.5 40 340120SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 8.5 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 11 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 9.4 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 31 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 16 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 21 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 12 100 340120SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 8.0 40 340120SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 200 400 340120SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 200 2000 340120SW8081A 8/16/11 406314%121TCMX (S) 08/16/11 52.5 139 340120SW8081A 8/16/11 406314S %142DCBP (S) 08/16/11 50.2 139 340120

Reporting limits increased due to the nature of the sample matrix (dark color extract). Surrogate recovery of DCBP is bias high possibly due to the dilution made on the sample; recovery of second surrogate supports data quality.

NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%102TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324S %117DCBP (S) 08/17/11 55.1 113 34001

Surrogate recovery of DCPB is bias high; recovery of second surrogate supports data quality. Sample is ND.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 3.9 8.9 NA1SW8260B NA 406301ug/KgNDChloromethane 08/15/11 4.1 8.9 NA1SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 2.4 8.9 NA1SW8260B NA 406301ug/KgNDBromomethane 08/15/11 4.2 8.9 NA1SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 2.6 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgNDFreon 113 08/15/11 3.3 8.9 NA1SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 1.8 45 NA1SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.99 8.9 NA1SW8260B NA 406301ug/KgNDMTBE 08/15/11 2.3 8.9 NA1SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 18 45 NA1SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDETBE 08/15/11 2.1 8.9 NA1SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 2.0 8.9 NA1SW8260B NA 406301ug/KgNDChloroform 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDBenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDTAME 08/15/11 1.8 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 1.7 8.9 NA1SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 3.5 8.9 NA1SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 2.0 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 1.2 8.9 NA1SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 0.99 8.9 NA1SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDToluene 08/15/11 0.87 8.9 NA1SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 1.8 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 1.6 8.9 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.77 8.9 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.7 8.9 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.76 8.9 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.59 4.5 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.68 8.9 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.7 8.9 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.1 8.9 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.7 8.9 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 8.9 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 3.0 8.9 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.4 8.9 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.97 8.9 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.5 8.9 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.9 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.9 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.2 8.9 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.8 8.9 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.3 8.9 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.9 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.5 8.9 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.6 8.9 NA1SW8260B NA 406301%95.0(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%93.8(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%117(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 200 198 337420SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 33.3 100 337420SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 37.2 100 337420SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 39.0 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 20.1 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 21.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 35.1 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 20.7 100 337420SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 42.0 100 337420SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 28.2 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 14.1 100 337420SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 16.0 100 337420SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 17.4 198 337420SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 15.9 198 337420SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 40.2 2000 337420SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 1700 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 17.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 22.2 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 31.5 100 337420SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 27.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 19.8 100 337420SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 30.9 100 337420SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 24.0 100 337420SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 8.40 100 337420SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 28.8 100 337420SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 36.6 100 337420SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 18.0 990 337420SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 21.0 100 337420


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 35.7 100 337420SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 32.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 25.8 100 337420SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 26.0 100 337420SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 21.0 100 337420SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 29.1 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 9.00 990 337420SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 23.7 100 337420SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 8.10 100 337420SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 36.0 100 337420SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 35.4 100 337420SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 30.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 24.3 100 337420SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 20.1 100 337420SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 33.0 100 337420SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 24.6 990 337420SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 30.6 100 337420SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 30.9 990 337420SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 42.9 100 337420SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 40.1 100 337420SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 32.7 510 337420SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 40.1 198 337420SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 113 990 337420SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 44.5 100 337420SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 27.0 100 337420SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 45.3 100 337420SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 46.2 100 337420SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 53.4 100 337420SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 25.2 100 337420


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:301204.22500 KirkhamB-1-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 41.7 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 40.2 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 51.3 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 40.8 100 337420SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 39.6 100 337420SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 45.9 100 337420SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 45.6 100 337420SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337420SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337420SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337420SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337420SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337420

D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).

NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH NA 406301ug/KgNDTPH(Gasoline) 08/15/11 15 89 NA18260TPH NA 406301%45.0(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 3.83 10 33981SW8015B(M) 8/16/11 406319mg/Kg160TPH as Motor Oil 08/17/11 8.33 20 33981SW8015B(M) 8/16/11 406319mg/Kg79.8Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.0Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg27Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg26Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.1Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg19Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg11Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%82.2TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%81.2DCBP (S) 08/17/11 55.1 113 34001


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.70 8.1 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.69 8.1 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.54 4.1 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.62 8.1 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.0 8.1 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.96 8.1 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.4 8.1 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.91 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.7 8.1 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.88 8.1 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 8.1 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.1 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 8.1 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.8 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.1 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.4 8.1 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.1 8.1 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.7 8.1 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.3 8.1 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.3 8.1 NA1SW8260B NA 406328%76.5(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%90.9(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%92.6(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 0.660 0.653 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 0.110 0.330 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 0.123 0.330 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 0.129 0.330 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 0.0663 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 0.0713 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 0.116 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 0.0683 0.330 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 0.139 0.330 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 0.0931 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.0465 0.330 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.0528 0.330 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.0574 0.653 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.0525 0.653 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 0.133 6.59 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 5.59 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.0584 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 0.0733 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 0.104 0.330 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 0.0901 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.0653 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 0.102 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 0.0792 0.330 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.0277 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 0.0950 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 0.121 0.330 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.0594 3.27 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 0.118 0.330 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 0.106 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 0.0851 0.330 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 0.0858 0.330 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 0.0693 0.330 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 0.0960 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.0297 3.27 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 0.0782 0.330 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.0267 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 0.119 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 0.117 0.330 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 0.0990 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 0.0802 0.330 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 0.0663 0.330 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 0.109 0.330 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 0.0812 3.27 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 0.101 0.330 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 0.102 3.27 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 0.142 0.330 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 0.132 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 0.108 1.68 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 0.132 0.653 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 0.374 3.27 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 0.147 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 0.0891 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 0.149 0.330 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 0.152 0.330 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 0.176 0.330 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 0.0832 0.330 33741SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 0.138 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 0.133 0.330 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 8:351204.22500 KirkhamB-1-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 0.169 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 0.135 0.330 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 0.131 0.330 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 0.151 0.330 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 0.150 0.330 33741SW8270C 8/14/11 406315%57.22,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%69.72-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%59.12-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%65.8Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%68.2Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315%66.1p-Terphenyl-d14 (S) 08/15/11 18 137 33741


NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 81 342518260TPH 8/15/11 406328%82.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/KgNDTPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg110Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:151204.22500 KirkhamB-3-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/25/11 406447mg/L4.1Lead (STLC) 08/26/11 0.0500 0.10 34961


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg4.2Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg140Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg36Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg8.0Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg29Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg100Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg24Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg30Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg99Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/Kg0.19Mercury 08/16/11 0.01 0.10 33921


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:151204.22500 KirkhamB-3-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 7.9 40 340120SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 7.3 40 340120SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 22 40 340120SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 8.8 40 340120SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 6.3 40 340120SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 8.4 40 340120SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 7.2 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 12 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 9.5 40 340120SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 8.5 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 11 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 9.4 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 31 40 340120SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 16 40 340120SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 21 40 340120SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 9.8 40 340120SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 12 100 340120SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 8.0 40 340120SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 200 400 340120SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 200 2000 340120SW8081A 8/16/11 406314%90.1TCMX (S) 08/16/11 52.5 139 340120SW8081A 8/16/11 406314%92.0DCBP (S) 08/16/11 50.2 139 340120

Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:151204.22500 KirkhamB-3-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8082 8/16/11 406324mg/KgNDAroclor1016 08/17/11 0.0230 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1221 08/17/11 0.0920 0.20 34001SW8082 8/16/11 406324mg/KgNDAroclor1232 08/17/11 0.0460 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1242 08/17/11 0.0430 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1248 08/17/11 0.0360 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1254 08/17/11 0.0240 0.10 34001SW8082 8/16/11 406324mg/KgNDAroclor1260 08/17/11 0.0270 0.10 34001SW8082 8/16/11 406324%91.3TCMX (S) 08/17/11 50.4 136 34001SW8082 8/16/11 406324%105DCBP (S) 08/17/11 55.1 113 34001


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:151204.22500 KirkhamB-3-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:151204.22500 KirkhamB-3-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:201204.22500 KirkhamB-3-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/KgNDArsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg69Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.0Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg18Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg16Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:201204.22500 KirkhamB-3-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:201204.22500 KirkhamB-3-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/15/11 406328x ug/Kg110TPH(Gasoline) 08/15/11 15 87 342518260TPH 8/15/11 406328%125(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251

x - Does not match pattern of reference Gasoline standard. Hydrocarbons in the range of C5-C12 quantified as Gasoline.NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319x mg/Kg2.0TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg6.8TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg121Pentacosane (S) 08/17/11 59.7 129 33981

x-Not typical of Diesel standard pattern (unknown hydrocarbons present).NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg1.7Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg42Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDCobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.5Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg13Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%107TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%109DCBP (S) 08/16/11 50.2 139 340110

Reporting limits increased due to the nature of the sample matrix (dark color extract). Toxaphene reported to the MDL.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 10.0 9.90 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 1.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 1.86 5.00 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 1.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 1.08 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 1.76 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 2.10 5.00 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 1.41 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.705 5.00 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.800 5.00 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.870 9.90 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.795 9.90 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 2.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 84.8 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.885 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 1.37 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.990 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 1.55 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.420 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 1.44 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 1.83 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.900 49.5 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 1.05 5.00 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 1.79 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 1.60 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 1.29 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 1.30 5.00 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 1.05 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 1.46 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.450 49.5 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 1.19 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 1.77 5.00 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 1.65 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 1.23 49.5 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 1.53 5.00 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 1.55 49.5 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 2.15 5.00 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 1.64 25.5 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 2.01 9.90 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 5.67 49.5 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 2.23 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 1.35 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 2.27 5.00 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 2.31 5.00 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 2.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 1.26 5.00 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:501204.22500 KirkhamB-10-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 2.09 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 2.57 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 2.04 5.00 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 1.98 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 2.30 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315S %1062,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%1062-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%82.82-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%93.4Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%82.1Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 33741

D - Surrogates not recoverable due to prep of the sample. Reporting limits increased due to the nature of the sample matrix (viscous and dark color extract).

NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 1.53 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg88TPH as Motor Oil 08/17/11 3.33 8.0 33981SW8015B(M) 8/16/11 406319mg/Kg84.5Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:551204.22500 KirkhamB-10-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.1Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg47Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg37Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.7Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg5.9Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.1Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg31Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:551204.22500 KirkhamB-10-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:551204.22500 KirkhamB-10-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg6.3TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg123Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 1.8 8.0 34014SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 1.6 8.0 34014SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 1.5 8.0 34014SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 2.0 8.0 34014SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 4.4 8.0 34014SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 1.8 8.0 34014SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 1.3 8.0 34014SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 1.7 8.0 34014SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 1.4 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 2.4 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 1.9 8.0 34014SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 1.7 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 2.3 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 1.9 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 6.1 8.0 34014SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 3.2 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 4.1 8.0 34014SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 2.0 8.0 34014SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 2.5 20 34014SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 1.6 8.0 34014SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 40 80 34014SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 40 400 34014SW8081A 8/16/11 406314%107TCMX (S) 08/16/11 52.5 139 34014SW8081A 8/16/11 406314%105DCBP (S) 08/16/11 50.2 139 34014



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 10.0 9.90 33741SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 1.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 1.86 5.00 33741SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 1.95 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 1.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 1.08 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 1.76 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 1.04 5.00 33741SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 2.10 5.00 33741SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 1.41 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 0.705 5.00 33741SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 0.800 5.00 33741SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 0.870 9.90 33741SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 0.795 9.90 33741SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 2.01 99.9 33741SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 84.8 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 0.885 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 1.11 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 1.58 5.00 33741SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 1.37 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 0.990 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 1.55 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 1.20 5.00 33741SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 0.420 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 1.44 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 1.83 5.00 33741SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 0.900 49.5 33741SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 1.05 5.00 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 1.79 5.00 33741SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 1.60 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 1.29 5.00 33741SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 1.30 5.00 33741SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 1.05 5.00 33741SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 1.46 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 0.450 49.5 33741SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 1.19 5.00 33741SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 0.405 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 1.80 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 1.77 5.00 33741SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 1.50 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 1.22 5.00 33741SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 1.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 1.65 5.00 33741SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 1.23 49.5 33741SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 1.53 5.00 33741SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 1.55 49.5 33741SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 2.15 5.00 33741SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 1.64 25.5 33741SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 2.01 9.90 33741SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 5.67 49.5 33741SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 2.23 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 1.35 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 2.27 5.00 33741SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 2.31 5.00 33741SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 2.67 5.00 33741SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 1.26 5.00 33741


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 2.09 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 2.01 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 2.57 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 2.04 5.00 33741SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 1.98 5.00 33741SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 2.30 5.00 33741SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 2.28 5.00 33741SW8270C 8/14/11 406315%1002,4,6-Tribromophenol (S) 08/15/11 19 122 33741SW8270C 8/14/11 406315%1022-Fluorobiphenyl (S) 08/15/11 30 115 33741SW8270C 8/14/11 406315%79.92-Fluorophenol (S) 08/15/11 25 121 33741SW8270C 8/14/11 406315%89.1Nitrobenzene-d5 (S) 08/15/11 23 120 33741SW8270C 8/14/11 406315%75.3Phenol-d6 (S) 08/15/11 24 113 33741SW8270C 8/14/11 406315S,D %-29.9p-Terphenyl-d14 (S) 08/15/11 18 137 33741


NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg29TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg86.6Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:501204.22500 KirkhamB-12-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg2.5Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg46Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg44Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg11Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg6.1Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg3.2Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg33Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg29Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg20Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:501204.22500 KirkhamB-12-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:501204.22500 KirkhamB-12-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319x mg/Kg2.2TPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/KgNDTPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg97.4Pentacosane (S) 08/17/11 59.7 129 33981



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg16Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg430Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/Kg1.1Cadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg8.5Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg9.2Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg58Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg18Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg16Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg39Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg77Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/Kg0.38Mercury 08/16/11 0.01 0.10 33921


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%93.9TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%87.1DCBP (S) 08/16/11 50.2 139 340110



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDPyridine 08/15/11 100 99.0 337410SW8270C 8/14/11 406315mg/KgNDN-Nitrosdimethylamine 08/15/11 16.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDAniline 08/15/11 18.6 50.0 337410SW8270C 8/14/11 406315mg/KgNDPhenol 08/15/11 19.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-chloroethyl) ether 08/15/11 10.4 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Chlorophenol 08/15/11 19.5 50.0 337410SW8270C 8/14/11 406315mg/KgND1,3-Dichlorobenzene 08/15/11 11.1 50.0 337410SW8270C 8/14/11 406315mg/KgND1,4-Dichlorobenzene 08/15/11 10.1 999 337410SW8270C 8/14/11 406315mg/KgNDBenzyl Alcohol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2-Dichlorobenzene 08/15/11 10.8 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Methylphenol (o-Cresol) 08/15/11 17.6 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-chloroisopropyl)ether 08/15/11 10.4 50.0 337410SW8270C 8/14/11 406315mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/15/11 21.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDN-nitroso-di-n-propylamine 08/15/11 14.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachloroethane 08/15/11 7.05 50.0 337410SW8270C 8/14/11 406315mg/KgNDNitrobenzene 08/15/11 8.00 50.0 337410SW8270C 8/14/11 406315mg/KgNDIsophorone 08/15/11 8.70 99.0 337410SW8270C 8/14/11 406315mg/KgND2-Nitrophenol 08/15/11 7.95 99.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dimethylphenol 08/15/11 20.1 999 337410SW8270C 8/14/11 406315mg/KgNDBenzoic Acid 08/15/11 848 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-Chloroethoxy)methane 08/15/11 8.85 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dichlorophenol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2,4-Trichlorobenzene 08/15/11 11.1 50.0 337410SW8270C 8/14/11 406315mg/KgND2,6-Dichlorophenol 08/15/11 15.8 50.0 337410SW8270C 8/14/11 406315mg/KgNDNaphthalene 08/15/11 13.7 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chloroaniline 08/15/11 15.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachloro-1,3-butadiene 08/15/11 9.90 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chloro-3-methylphenol 08/15/11 15.5 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Methylnaphthalene 08/15/11 12.0 50.0 337410SW8270C 8/14/11 406315mg/KgND1-Methylnaphthalene 08/15/11 12.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDHexachlorocyclopentadiene 08/15/11 4.20 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4,6-Trichlorophenol 08/15/11 14.4 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4,5-Trichlorophenol 08/15/11 18.3 50.0 337410SW8270C 8/14/11 406315mg/KgND2-Chloronaphthalene 08/15/11 9.00 495 337410SW8270C 8/14/11 406315mg/KgND2-Nitroaniline 08/15/11 10.5 50.0 337410


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDimethyl phthalate 08/15/11 17.9 50.0 337410SW8270C 8/14/11 406315mg/KgND1,3-Dinitrobenzene 08/15/11 16.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDAcenaphthylene 08/15/11 12.9 50.0 337410SW8270C 8/14/11 406315mg/KgND2,6-Dinitrotoluene 08/15/11 4.05 50.0 337410SW8270C 8/14/11 406315mg/KgND1,2-Dinitrobenzene 08/15/11 13.0 50.0 337410SW8270C 8/14/11 406315mg/KgND3-Nitroaniline 08/15/11 10.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDAcenaphthene 08/15/11 14.6 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dinitrophenol 08/15/11 4.50 495 337410SW8270C 8/14/11 406315mg/KgND4-Nitrophenol 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDibenzofuran 08/15/11 11.9 50.0 337410SW8270C 8/14/11 406315mg/KgND2,4-Dinitrotoluene 08/15/11 4.05 50.0 337410SW8270C 8/14/11 406315mg/KgND2,3,5,6-Tetrachlorophenol 08/15/11 18.0 50.0 337410SW8270C 8/14/11 406315mg/KgND2,3,4,6-Tetrachlorophenol 08/15/11 18.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDDiethylphthalate 08/15/11 17.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDFluorene 08/15/11 15.0 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Chlorophenyl phenyl ether 08/15/11 12.2 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Nitroaniline 08/15/11 12.2 50.0 337410SW8270C 8/14/11 406315mg/KgND4,6-Dinitro-2-methylphenol 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDiphenylamine 08/15/11 10.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDAzobenzene 08/15/11 16.5 50.0 337410SW8270C 8/14/11 406315mg/KgND4-Bromophenyl phenyl ether 08/15/11 12.3 495 337410SW8270C 8/14/11 406315mg/KgNDHexachlorobenzene 08/15/11 15.3 50.0 337410SW8270C 8/14/11 406315mg/KgNDPentachlorophenol 08/15/11 15.5 495 337410SW8270C 8/14/11 406315mg/KgNDPhenanthrene 08/15/11 21.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDAnthracene 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDCarbazole 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDDi-n-butylphthalate 08/15/11 16.4 255 337410SW8270C 8/14/11 406315mg/KgNDFluoranthene 08/15/11 20.1 99.0 337410SW8270C 8/14/11 406315mg/KgNDBenzidine 08/15/11 56.7 495 337410SW8270C 8/14/11 406315mg/KgNDPyrene 08/15/11 22.3 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzyl butyl phthalate 08/15/11 13.5 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenz[a]anthracene 08/15/11 22.7 50.0 337410SW8270C 8/14/11 406315mg/KgND3,3'-Dichlorobenzidine 08/15/11 23.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDChrysene 08/15/11 26.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDBis(2-Ethylhexyl)phthalate 08/15/11 12.6 50.0 337410


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:501204.22500 KirkhamB-11-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/14/11 406315mg/KgNDDi-n-octyl phthalate 08/15/11 20.9 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[b]fluoranthene 08/15/11 20.1 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[k]fluoranthene 08/15/11 25.7 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[a]pyrene 08/15/11 20.4 50.0 337410SW8270C 8/14/11 406315mg/KgNDIndeno[1,2,3-cd]pyrene 08/15/11 19.8 50.0 337410SW8270C 8/14/11 406315mg/KgNDDibenz[a,h]anthracene 08/15/11 23.0 50.0 337410SW8270C 8/14/11 406315mg/KgNDBenzo[g,h,i]perylene 08/15/11 22.8 50.0 337410SW8270C 8/14/11 406315mg/KgND1,4-Dinitrobenzene 08/15/11 22.8 50.0 337410SW8270C 8/14/11 406315S,D %0.0002,4,6-Tribromophenol (S) 08/15/11 19 122 337410SW8270C 8/14/11 406315S,D %0.0002-Fluorobiphenyl (S) 08/15/11 30 115 337410SW8270C 8/14/11 406315S,D %0.0002-Fluorophenol (S) 08/15/11 25 121 337410SW8270C 8/14/11 406315S,D %0.000Nitrobenzene-d5 (S) 08/15/11 23 120 337410SW8270C 8/14/11 406315S,D %0.000Phenol-d6 (S) 08/15/11 24 113 337410SW8270C 8/14/11 406315S,D %0.000p-Terphenyl-d14 (S) 08/15/11 18 137 337410


NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/15/11 406328ug/KgNDTPH(Gasoline) 08/15/11 14 82 342518260TPH 8/15/11 406328S %43.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 34251

S-Surrogate recovery out of limit.Matrix effect suspected. Sample analyzed twice with similar results.NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:551204.22500 KirkhamB-11-6.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:551204.22500 KirkhamB-11-6.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDDichlorodifluoromethane 08/15/11 440 1000 NA100SW8260B NA 406301ug/KgNDChloromethane 08/15/11 460 1000 NA100SW8260B NA 406301ug/KgNDVinyl Chloride 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgNDBromomethane 08/15/11 470 1000 NA100SW8260B NA 406301ug/KgNDTrichlorofluoromethane 08/15/11 290 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloroethene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDFreon 113 08/15/11 370 1000 NA100SW8260B NA 406301ug/KgNDMethylene Chloride 08/15/11 200 5000 NA100SW8260B NA 406301ug/KgNDtrans-1,2-Dichloroethene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDMTBE 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgNDtert-Butanol 08/15/11 2100 5000 NA100SW8260B NA 406301ug/KgNDDiisopropyl ether (DIPE) 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloroethane 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgNDETBE 08/15/11 240 1000 NA100SW8260B NA 406301ug/KgNDcis-1,2-Dichloroethene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgND2,2-Dichloropropane 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDBromochloromethane 08/15/11 230 1000 NA100SW8260B NA 406301ug/KgNDChloroform 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDCarbon Tetrachloride 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgND1,1,1-Trichloroethane 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1-Dichloropropene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDBenzene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDTAME 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichloroethane 08/15/11 190 1000 NA100SW8260B NA 406301ug/KgNDTrichloroethylene 08/15/11 390 1000 NA100SW8260B NA 406301ug/KgNDDibromomethane 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichloropropane 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgNDBromodichloromethane 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDcis-1,3-Dichloropropene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDToluene 08/15/11 98 1000 NA100SW8260B NA 406301ug/KgNDTetrachloroethylene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgNDtrans-1,3-Dichloropropene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1,2-Trichloroethane 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgNDDibromochloromethane 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgND1,3-Dichloropropane 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgND1,2-Dibromoethane 08/15/11 170 1000 NA100


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:551204.22500 KirkhamB-11-6.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/Kg1500Ethyl Benzene 08/15/11 86 1000 NA100SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 420 1000 NA100SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 86 1000 NA100SW8260B NA 406301ug/Kg4800m,p-Xylene 08/15/11 190 1000 NA100SW8260B NA 406301ug/Kg670o-Xylene 08/15/11 66 500 NA100SW8260B NA 406301ug/KgNDStyrene 08/15/11 77 1000 NA100SW8260B NA 406301ug/KgNDBromoform 08/15/11 190 1000 NA100SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 140 1000 NA100SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 120 1000 NA100SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 300 1000 NA100SW8260B NA 406301ug/Kg16001,3,5-Trimethylbenzene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 330 1000 NA100SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 140 1000 NA100SW8260B NA 406301ug/Kg48001,2,4-Trimethylbenzene 08/15/11 110 1000 NA100SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 160 1000 NA100SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 180 1000 NA100SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 150 1000 NA100SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 220 1000 NA100SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 130 1000 NA100SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 420 1000 NA100SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 260 1000 NA100SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 210 1000 NA100SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 280 1000 NA100SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 290 1000 NA100SW8260B NA 406301%103(S) Dibromofluoromethane 08/15/11 59.8 148 NA100SW8260B NA 406301%72.8(S) Toluene-d8 08/15/11 55.2 133 NA100SW8260B NA 406301%89.1(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA100


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:551204.22500 KirkhamB-11-6.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:551204.22500 KirkhamB-11-6.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH NA 406301x ug/Kg150000TPH(Gasoline) 08/15/11 1700 10000 NA1008260TPH NA 406301%82.7(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA100

x - Does not match pattern of reference Gasoline standard. Result is elevated due to contribution from heavy end hydrocarbons (possibly aged gasoline) and non-fuel light hydrocarbons to the C5-C12 range quantified as Gasoline.

NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:001204.22500 KirkhamB-11-10.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406411ug/KgNDDichlorodifluoromethane 08/24/11 4.4 10 NA1SW8260B NA 406411ug/KgNDChloromethane 08/24/11 4.6 10 NA1SW8260B NA 406411ug/KgNDVinyl Chloride 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgNDBromomethane 08/24/11 4.7 10 NA1SW8260B NA 406411ug/KgNDTrichlorofluoromethane 08/24/11 2.9 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloroethene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDFreon 113 08/24/11 3.7 10 NA1SW8260B NA 406411ug/KgNDMethylene Chloride 08/24/11 2.0 50 NA1SW8260B NA 406411ug/KgNDtrans-1,2-Dichloroethene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDMTBE 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgNDtert-Butanol 08/24/11 21 50 NA1SW8260B NA 406411ug/KgNDDiisopropyl ether (DIPE) 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloroethane 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgNDETBE 08/24/11 2.4 10 NA1SW8260B NA 406411ug/KgNDcis-1,2-Dichloroethene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgND2,2-Dichloropropane 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDBromochloromethane 08/24/11 2.3 10 NA1SW8260B NA 406411ug/KgNDChloroform 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDCarbon Tetrachloride 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgND1,1,1-Trichloroethane 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1-Dichloropropene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDBenzene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDTAME 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgND1,2-Dichloroethane 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDTrichloroethylene 08/24/11 3.9 10 NA1SW8260B NA 406411ug/KgNDDibromomethane 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,2-Dichloropropane 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgNDBromodichloromethane 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDcis-1,3-Dichloropropene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDToluene 08/24/11 0.98 10 NA1SW8260B NA 406411ug/KgNDTetrachloroethylene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgNDtrans-1,3-Dichloropropene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1,2-Trichloroethane 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgNDDibromochloromethane 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgND1,3-Dichloropropane 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgND1,2-Dibromoethane 08/24/11 1.7 10 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:001204.22500 KirkhamB-11-10.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406411ug/KgNDEthyl Benzene 08/24/11 0.86 10 NA1SW8260B NA 406411ug/KgNDChlorobenzene 08/24/11 4.2 10 NA1SW8260B NA 406411ug/KgND1,1,1,2-Tetrachloroethane 08/24/11 0.86 10 NA1SW8260B NA 406411ug/KgNDm,p-Xylene 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDo-Xylene 08/24/11 0.66 5.0 NA1SW8260B NA 406411ug/KgNDStyrene 08/24/11 0.77 10 NA1SW8260B NA 406411ug/KgNDBromoform 08/24/11 1.9 10 NA1SW8260B NA 406411ug/KgNDIsopropyl Benzene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgNDn-Propylbenzene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgNDBromobenzene 08/24/11 1.2 10 NA1SW8260B NA 406411ug/KgND1,1,2,2-Tetrachloroethane 08/24/11 3.0 10 NA1SW8260B NA 406411ug/KgND1,3,5-Trimethylbenzene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgND1,2,3-Trichloropropane 08/24/11 3.3 10 NA1SW8260B NA 406411ug/KgND4-Chlorotoluene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgND2-Chlorotoluene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgNDtert-Butylbenzene 08/24/11 1.4 10 NA1SW8260B NA 406411ug/KgND1,2,4-Trimethylbenzene 08/24/11 1.1 10 NA1SW8260B NA 406411ug/KgNDsec-Butyl Benzene 08/24/11 1.6 10 NA1SW8260B NA 406411ug/KgNDp-Isopropyltoluene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgND1,3-Dichlorobenzene 08/24/11 1.8 10 NA1SW8260B NA 406411ug/KgND1,4-Dichlorobenzene 08/24/11 1.5 10 NA1SW8260B NA 406411ug/KgNDn-Butylbenzene 08/24/11 2.2 10 NA1SW8260B NA 406411ug/KgND1,2-Dichlorobenzene 08/24/11 1.3 10 NA1SW8260B NA 406411ug/KgND1,2-Dibromo-3-Chloropropane 08/24/11 4.2 10 NA1SW8260B NA 406411ug/KgNDHexachlorobutadiene 08/24/11 2.6 10 NA1SW8260B NA 406411ug/KgND1,2,4-Trichlorobenzene 08/24/11 2.1 10 NA1SW8260B NA 406411ug/KgNDNaphthalene 08/24/11 2.8 10 NA1SW8260B NA 406411ug/KgND1,2,3-Trichlorobenzene 08/24/11 2.9 10 NA1SW8260B NA 406411%87.9(S) Dibromofluoromethane 08/24/11 59.8 148 NA1SW8260B NA 406411%90.4(S) Toluene-d8 08/24/11 55.2 133 NA1SW8260B NA 406411%94.1(S) 4-Bromofluorobenzene 08/24/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:001204.22500 KirkhamB-11-10.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 15 80 340140SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 44 80 340140SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 18 80 340140SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 13 80 340140SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 14 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 24 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 17 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 23 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 19 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 61 80 340140SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 32 80 340140SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 41 80 340140SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 20 80 340140SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 25 200 340140SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 16 80 340140SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 400 800 340140SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 400 4000 340140SW8081A 8/16/11 406314S,D %0.000TCMX (S) 08/16/11 52.5 139 340140SW8081A 8/16/11 406314S,D %0.000DCBP (S) 08/16/11 50.2 139 340140

D - Surrogates not recoverable due to dilution of the sample. Reporting limits increased due to the nature of the sample matrix (dark color extract).NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.66 7.7 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.2 7.7 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.66 7.7 NA1SW8260B NA 406328ug/Kg7.7m,p-Xylene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.51 3.9 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.59 7.7 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.5 7.7 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 0.95 7.7 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 0.91 7.7 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.7 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.87 7.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.7 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/Kg8.91,2,4-Trimethylbenzene 08/15/11 0.84 7.7 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.7 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.7 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.7 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.7 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.7 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.7 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.7 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.7 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.2 7.7 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.7 NA1SW8260B NA 406328%86.3(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%99.6(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%76.2(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:501204.22500 KirkhamB-14-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:551204.22500 KirkhamB-14-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg3.4Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg75Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg36Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.6Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg11Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg7.2Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg30Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg31Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg25Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:551204.22500 KirkhamB-14-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:551204.22500 KirkhamB-14-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.86 10 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 4.2 10 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.86 10 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.9 10 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.66 5.0 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.77 10 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.9 10 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.2 10 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.0 10 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 3.3 10 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.4 10 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.1 10 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.6 10 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.8 10 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.5 10 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 2.2 10 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.3 10 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.2 10 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.6 10 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.1 10 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.8 10 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.9 10 NA1SW8260B NA 406328%78.8(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%88.3(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%91.1(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:551204.22500 KirkhamB-14-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:551204.22500 KirkhamB-14-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg14TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg105Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/Kg0.10Mercury 08/16/11 0.01 0.10 33921


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 11 20 340110SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 4.4 20 340110SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 3.2 20 340110SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 4.2 20 340110SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 3.6 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 5.9 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 4.8 20 340110SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 4.3 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 5.7 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 4.7 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 15 20 340110SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 8.1 20 340110SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 10 20 340110SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 4.9 20 340110SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 6.2 50 340110SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 4.0 20 340110SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 100 200 340110SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 100 100 340110SW8081A 8/16/11 406314%100TCMX (S) 08/16/11 52.5 139 340110SW8081A 8/16/11 406314%96.5DCBP (S) 08/16/11 50.2 139 340110



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406328ug/KgNDEthyl Benzene 08/15/11 0.73 8.5 NA1SW8260B NA 406328ug/KgNDChlorobenzene 08/15/11 3.6 8.5 NA1SW8260B NA 406328ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.73 8.5 NA1SW8260B NA 406328ug/KgNDm,p-Xylene 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDo-Xylene 08/15/11 0.56 4.3 NA1SW8260B NA 406328ug/KgNDStyrene 08/15/11 0.65 8.5 NA1SW8260B NA 406328ug/KgNDBromoform 08/15/11 1.6 8.5 NA1SW8260B NA 406328ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgNDn-Propylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgNDBromobenzene 08/15/11 1.0 8.5 NA1SW8260B NA 406328ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.6 8.5 NA1SW8260B NA 406328ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.96 8.5 NA1SW8260B NA 406328ug/KgND1,2,3-Trichloropropane 08/15/11 2.8 8.5 NA1SW8260B NA 406328ug/KgND4-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgND2-Chlorotoluene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgNDtert-Butylbenzene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.92 8.5 NA1SW8260B NA 406328ug/KgNDsec-Butyl Benzene 08/15/11 1.4 8.5 NA1SW8260B NA 406328ug/KgNDp-Isopropyltoluene 08/15/11 1.2 8.5 NA1SW8260B NA 406328ug/KgND1,3-Dichlorobenzene 08/15/11 1.5 8.5 NA1SW8260B NA 406328ug/KgND1,4-Dichlorobenzene 08/15/11 1.3 8.5 NA1SW8260B NA 406328ug/KgNDn-Butylbenzene 08/15/11 1.9 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dichlorobenzene 08/15/11 1.1 8.5 NA1SW8260B NA 406328ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.6 8.5 NA1SW8260B NA 406328ug/KgNDHexachlorobutadiene 08/15/11 2.2 8.5 NA1SW8260B NA 406328ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.8 8.5 NA1SW8260B NA 406328ug/KgNDNaphthalene 08/15/11 2.4 8.5 NA1SW8260B NA 406328ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.4 8.5 NA1SW8260B NA 406328%83.3(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406328%102(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406328%72.9(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:401204.22500 KirkhamB-15-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:451204.22500 KirkhamB-15-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:451204.22500 KirkhamB-15-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:451204.22500 KirkhamB-15-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.66 7.7 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.2 7.7 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.66 7.7 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.51 3.9 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.59 7.7 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.5 7.7 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.95 7.7 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.91 7.7 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.3 7.7 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.87 7.7 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.6 7.7 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.84 7.7 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.3 7.7 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.7 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.4 7.7 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.2 7.7 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.7 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.0 7.7 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.3 7.7 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.0 7.7 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.7 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.2 7.7 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.2 7.7 NA1SW8260B NA 406301%101(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%87.3(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%102(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:451204.22500 KirkhamB-15-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 13:451204.22500 KirkhamB-15-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:101204.22500 KirkhamB-9-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/Kg0.23Mercury 08/16/11 0.01 0.10 33921


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:101204.22500 KirkhamB-9-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:101204.22500 KirkhamB-9-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.95 11 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 4.6 11 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.94 11 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.73 5.5 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.84 11 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 2.1 11 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 1.3 11 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.3 11 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 3.7 11 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.7 11 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.2 11 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.8 11 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 2.0 11 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.6 11 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 2.4 11 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 1.4 11 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.7 11 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 2.8 11 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.3 11 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 3.1 11 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 3.2 11 NA1SW8260B NA 406301%95.4(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%96.7(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%129(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:101204.22500 KirkhamB-9-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:101204.22500 KirkhamB-9-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:151204.22500 KirkhamB-9-3.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/Kg3.8Arsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg78Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg38Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg17Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/Kg19Copper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg44Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg24Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg41Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg41Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406269mg/Kg0.25Mercury 08/16/11 0.01 0.10 33921


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:151204.22500 KirkhamB-9-3.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 15:151204.22500 KirkhamB-9-3.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:051204.22500 KirkhamB-5-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406266mg/KgNDAntimony 08/16/11 0.20 5.0 33881SW6010B 8/15/11 406266mg/KgNDArsenic 08/16/11 0.28 1.7 33881SW6010B 8/15/11 406266mg/Kg37Barium 08/16/11 1 5.0 33881SW6010B 8/15/11 406266mg/KgNDBeryllium 08/16/11 0.0840 2.0 33881SW6010B 8/15/11 406266mg/KgNDCadmium 08/16/11 0.0590 1.0 33881SW6010B 8/15/11 406266mg/Kg23Chromium 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg6.0Cobalt 08/16/11 0.14 5.0 33881SW6010B 8/15/11 406266mg/KgNDCopper 08/16/11 0.0900 5.0 33881SW6010B 8/15/11 406266mg/Kg2.1Lead 08/16/11 0.043 1.0 33881SW6010B 8/15/11 406266mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/Kg14Nickel 08/16/11 0.0590 5.0 33881SW6010B 8/15/11 406266mg/KgNDSelenium 08/16/11 0.29 5.0 33881SW6010B 8/15/11 406266mg/KgNDSilver 08/16/11 1.0 1.0 33881SW6010B 8/15/11 406266mg/KgNDThallium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg17Vanadium 08/16/11 0.12 5.0 33881SW6010B 8/15/11 406266mg/Kg12Zinc 08/16/11 0.59 5.0 33881


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:051204.22500 KirkhamB-5-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/16/11 406314ug/KgNDalpha-BHC 08/16/11 0.44 2.0 34011SW8081A 8/16/11 406314ug/KgNDgamma-BHC 08/16/11 0.40 2.0 34011SW8081A 8/16/11 406314ug/KgNDbeta-BHC 08/16/11 0.36 2.0 34011SW8081A 8/16/11 406314ug/KgNDdelta-BHC 08/16/11 0.49 2.0 34011SW8081A 8/16/11 406314ug/KgNDHeptachlor 08/16/11 1.1 2.0 34011SW8081A 8/16/11 406314ug/KgNDAldrin 08/16/11 0.44 2.0 34011SW8081A 8/16/11 406314ug/KgNDHeptachlor epoxide 08/16/11 0.32 2.0 34011SW8081A 8/16/11 406314ug/KgNDgamma-Chlordane 08/16/11 0.42 2.0 34011SW8081A 8/16/11 406314ug/KgNDalpha-Chlordane 08/16/11 0.36 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan I 08/16/11 0.59 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDE 08/16/11 0.48 2.0 34011SW8081A 8/16/11 406314ug/KgNDDieldrin 08/16/11 0.43 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin 08/16/11 0.57 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDD 08/16/11 0.47 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan II 08/16/11 1.5 2.0 34011SW8081A 8/16/11 406314ug/KgND4,4'-DDT 08/16/11 0.81 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin aldehyde 08/16/11 1.0 2.0 34011SW8081A 8/16/11 406314ug/KgNDEndosulfan sulfate 08/16/11 0.49 2.0 34011SW8081A 8/16/11 406314ug/KgNDMethoxychlor 08/16/11 0.62 5.0 34011SW8081A 8/16/11 406314ug/KgNDEndrin Ketone 08/16/11 0.40 2.0 34011SW8081A 8/16/11 406314ug/KgNDChlordane 08/16/11 10 20 34011SW8081A 8/16/11 406314ug/KgNDToxaphene 08/16/11 10 100 34011SW8081A 8/16/11 406314%63.9TCMX (S) 08/16/11 52.5 139 34011SW8081A 8/16/11 406314%58.7DCBP (S) 08/16/11 50.2 139 34011


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:051204.22500 KirkhamB-5-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:051204.22500 KirkhamB-5-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406319mg/KgNDTPH as Diesel 08/17/11 0.759 2.0 33981SW8015B(M) 8/16/11 406319mg/Kg12TPH as Motor Oil 08/17/11 1.65 4.0 33981SW8015B(M) 8/16/11 406319mg/Kg108Pentacosane (S) 08/17/11 59.7 129 33981


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-13-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-13-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-13-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:301204.22500 KirkhamB-13-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:301204.22500 KirkhamB-13-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:301204.22500 KirkhamB-13-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 10:401204.22500 KirkhamB-12-1.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891SW6010B 8/15/11 406267mg/Kg2.5Arsenic 08/16/11 0.28 1.7 33891SW6010B 8/15/11 406267mg/Kg43Barium 08/16/11 1 5.0 33891SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891SW6010B 8/15/11 406267mg/Kg30Chromium 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg6.2Cobalt 08/16/11 0.14 5.0 33891SW6010B 8/15/11 406267mg/KgNDCopper 08/16/11 0.0900 5.0 33891SW6010B 8/15/11 406267mg/Kg2.4Lead 08/16/11 0.043 1.0 33891SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/Kg29Nickel 08/16/11 0.0590 5.0 33891SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg22Vanadium 08/16/11 0.12 5.0 33891SW6010B 8/15/11 406267mg/Kg16Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406301ug/KgNDEthyl Benzene 08/15/11 0.63 7.3 NA1SW8260B NA 406301ug/KgNDChlorobenzene 08/15/11 3.1 7.3 NA1SW8260B NA 406301ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.63 7.3 NA1SW8260B NA 406301ug/KgNDm,p-Xylene 08/15/11 1.4 7.3 NA1SW8260B NA 406301ug/KgNDo-Xylene 08/15/11 0.48 3.7 NA1SW8260B NA 406301ug/KgNDStyrene 08/15/11 0.56 7.3 NA1SW8260B NA 406301ug/KgNDBromoform 08/15/11 1.4 7.3 NA1SW8260B NA 406301ug/KgNDIsopropyl Benzene 08/15/11 0.91 7.3 NA1SW8260B NA 406301ug/KgNDn-Propylbenzene 08/15/11 1.0 7.3 NA1SW8260B NA 406301ug/KgNDBromobenzene 08/15/11 0.87 7.3 NA1SW8260B NA 406301ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 2.2 7.3 NA1SW8260B NA 406301ug/KgND1,3,5-Trimethylbenzene 08/15/11 0.82 7.3 NA1SW8260B NA 406301ug/KgND1,2,3-Trichloropropane 08/15/11 2.4 7.3 NA1SW8260B NA 406301ug/KgND4-Chlorotoluene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgND2-Chlorotoluene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgNDtert-Butylbenzene 08/15/11 1.0 7.3 NA1SW8260B NA 406301ug/KgND1,2,4-Trimethylbenzene 08/15/11 0.79 7.3 NA1SW8260B NA 406301ug/KgNDsec-Butyl Benzene 08/15/11 1.2 7.3 NA1SW8260B NA 406301ug/KgNDp-Isopropyltoluene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgND1,3-Dichlorobenzene 08/15/11 1.3 7.3 NA1SW8260B NA 406301ug/KgND1,4-Dichlorobenzene 08/15/11 1.1 7.3 NA1SW8260B NA 406301ug/KgNDn-Butylbenzene 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dichlorobenzene 08/15/11 0.96 7.3 NA1SW8260B NA 406301ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.1 7.3 NA1SW8260B NA 406301ug/KgNDHexachlorobutadiene 08/15/11 1.9 7.3 NA1SW8260B NA 406301ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.6 7.3 NA1SW8260B NA 406301ug/KgNDNaphthalene 08/15/11 2.1 7.3 NA1SW8260B NA 406301ug/KgND1,2,3-Trichlorobenzene 08/15/11 2.1 7.3 NA1SW8260B NA 406301%101(S) Dibromofluoromethane 08/15/11 59.8 148 NA1SW8260B NA 406301%81.7(S) Toluene-d8 08/15/11 55.2 133 NA1SW8260B NA 406301%98.3(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:101204.22500 KirkhamB-5-5.0 D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:451204.22500 KirkhamB-1-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LNDMTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:451204.22500 KirkhamB-1-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%90.0(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%91.5(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%90.6(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:451204.22500 KirkhamB-1-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/17/11 406320ug/LNDTPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%80.2(S) 4-Bromofluorobenzene 08/17/11 34 114 34221


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:451204.22500 KirkhamB-1-GW

WaterSample Matrix:

Lab Sample ID: 1108073-033B



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%79.5Pentacosane (S) 08/17/11 57.9 125 34021


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 9:451204.22500 KirkhamB-1-GW

WaterSample Matrix:

Lab Sample ID: 1108073-033C



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.035Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.027Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.012Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7470A 8/12/11 406238mg/LNDMercury 08/15/11 0.00005 0.0002 33651


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:001204.22500 KirkhamB-12-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:001204.22500 KirkhamB-12-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.022Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.012Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.040Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.019Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 11:001204.22500 KirkhamB-12-GWD

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:101204.22500 KirkhamB-11-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:101204.22500 KirkhamB-11-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.14 0.50 NA1SW8260B NA 406320ug/L45Ethyl Benzene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.10 0.50 NA1SW8260B NA 406320ug/L110m,p-Xylene 08/17/11 0.20 1.0 NA1SW8260B NA 406320ug/L17o-Xylene 08/17/11 0.13 0.50 NA1SW8260B NA 406320ug/LNDStyrene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDBromoform 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/L6.1Isopropyl Benzene 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/L21n-Propylbenzene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/L261,3,5-Trimethylbenzene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.59 1.0 NA1SW8260B NA 406320ug/L521,2,4-Trimethylbenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.24 0.50 NA1SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.25 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/L4.6n-Butylbenzene 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.39 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.45 1.0 NA1SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.22 0.50 NA1SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.48 1.0 NA1SW8260B NA 406320ug/L12Naphthalene 08/17/11 0.57 1.0 NA1SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.52 1.0 NA1SW8260B NA 406320%93.5(S) Dibromofluoromethane 08/17/11 61.2 131 NA1SW8260B NA 406320%92.1(S) Toluene-d8 08/17/11 75.1 127 NA1SW8260B NA 406320%90.1(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:101204.22500 KirkhamB-11-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/17/11 406320x ug/L1300TPH(Gasoline) 08/17/11 22 50 342218260TPH 8/17/11 406320%83.2(S) 4-Bromofluorobenzene 08/17/11 34 114 34221

x - Does not match pattern of reference Gasoline standard. Result is elevated due to contribution from heavy end hydrocarbons (possibly aged gasoline) and non-fuel light hydrocarbons to the C5-C12 range quantified as Gasoline.

NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:101204.22500 KirkhamB-11-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406321x mg/L0.35TPH as Diesel (SG) 08/17/11 0.0400 0.10 34021SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021SW8015B(M) 8/16/11 406321%82.1Pentacosane (S) 08/17/11 57.9 125 34021

x- Not typical of Diesel standard pattern (possibly fuel lighter than diesel)NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 12:101204.22500 KirkhamB-11-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.047Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.0060Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.030Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-9-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.41 0.50 NA1SW8260B NA 406320ug/LNDVinyl Chloride 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.18 5.0 NA1SW8260B NA 406320ug/LNDtrans-1,2-Dichloroethene 08/17/11 0.31 0.50 NA1SW8260B NA 406320ug/L0.69MTBE 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.5 5.0 NA1SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.36 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDETBE 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDcis-1,2-Dichloroethene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.34 0.50 NA1SW8260B NA 406320ug/LNDChloroform 08/17/11 0.29 0.50 NA1SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.26 0.50 NA1SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.40 0.50 NA1SW8260B NA 406320ug/LNDBenzene 08/17/11 0.33 0.50 NA1SW8260B NA 406320ug/LNDTAME 08/17/11 0.32 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.28 0.50 NA1SW8260B NA 406320ug/LNDTrichloroethylene 08/17/11 0.38 0.50 NA1SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.37 0.50 NA1SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.23 0.50 NA1SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.30 0.50 NA1SW8260B NA 406320ug/LNDToluene 08/17/11 0.19 0.50 NA1SW8260B NA 406320ug/LNDTetrachloroethylene 08/17/11 0.15 0.50 NA1SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.20 0.50 NA1SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.21 0.50 NA1SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.18 0.50 NA1SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.19 0.50 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-9-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:251204.22500 KirkhamB-9-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/L0.020Arsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.19Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.016Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 17:151204.22500 KirkhamB-13-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDDichlorodifluoromethane 08/17/11 0.48 0.60 NA1.19SW8260B NA 406320ug/LNDChloromethane 08/17/11 0.48 0.60 NA1.19SW8260B NA 406320ug/L1.1Vinyl Chloride 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromomethane 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDTrichlorofluoromethane 08/17/11 0.40 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloroethene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDFreon 113 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDMethylene Chloride 08/17/11 0.21 6.0 NA1.19SW8260B NA 406320ug/L1.5trans-1,2-Dichloroethene 08/17/11 0.37 0.60 NA1.19SW8260B NA 406320ug/LNDMTBE 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDtert-Butanol 08/17/11 1.8 6.0 NA1.19SW8260B NA 406320ug/LNDDiisopropyl ether (DIPE) 08/17/11 0.43 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloroethane 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDETBE 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/L9.6cis-1,2-Dichloroethene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LND2,2-Dichloropropane 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromochloromethane 08/17/11 0.41 0.60 NA1.19SW8260B NA 406320ug/L0.61Chloroform 08/17/11 0.35 0.60 NA1.19SW8260B NA 406320ug/LNDCarbon Tetrachloride 08/17/11 0.32 0.60 NA1.19SW8260B NA 406320ug/LND1,1,1-Trichloroethane 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,1-Dichloropropene 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/LNDBenzene 08/17/11 0.40 0.60 NA1.19SW8260B NA 406320ug/LNDTAME 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichloroethane 08/17/11 0.33 0.60 NA1.19SW8260B NA 406320ug/L49Trichloroethylene 08/17/11 0.45 0.60 NA1.19SW8260B NA 406320ug/LNDDibromomethane 08/17/11 0.25 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichloropropane 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDBromodichloromethane 08/17/11 0.27 0.60 NA1.19SW8260B NA 406320ug/LNDcis-1,3-Dichloropropene 08/17/11 0.36 0.60 NA1.19SW8260B NA 406320ug/LNDToluene 08/17/11 0.23 0.60 NA1.19SW8260B NA 406320ug/L48Tetrachloroethylene 08/17/11 0.18 0.60 NA1.19SW8260B NA 406320ug/LNDtrans-1,3-Dichloropropene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LND1,1,2-Trichloroethane 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LNDDibromochloromethane 08/17/11 0.26 0.60 NA1.19SW8260B NA 406320ug/LND1,3-Dichloropropane 08/17/11 0.21 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dibromoethane 08/17/11 0.23 0.60 NA1.19


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 17:151204.22500 KirkhamB-13-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406320ug/LNDChlorobenzene 08/17/11 0.17 0.60 NA1.19SW8260B NA 406320ug/LNDEthyl Benzene 08/17/11 0.18 0.60 NA1.19SW8260B NA 406320ug/LND1,1,1,2-Tetrachloroethane 08/17/11 0.12 0.60 NA1.19SW8260B NA 406320ug/LNDm,p-Xylene 08/17/11 0.24 1.2 NA1.19SW8260B NA 406320ug/LNDo-Xylene 08/17/11 0.15 0.60 NA1.19SW8260B NA 406320ug/LNDStyrene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LNDBromoform 08/17/11 0.54 1.2 NA1.19SW8260B NA 406320ug/LNDIsopropyl Benzene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LNDBromobenzene 08/17/11 0.46 0.60 NA1.19SW8260B NA 406320ug/LND1,1,2,2-Tetrachloroethane 08/17/11 0.30 0.60 NA1.19SW8260B NA 406320ug/LNDn-Propylbenzene 08/17/11 0.35 0.60 NA1.19SW8260B NA 406320ug/LND2-Chlorotoluene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LND1,3,5-Trimethylbenzene 08/17/11 0.24 0.60 NA1.19SW8260B NA 406320ug/LND4-Chlorotoluene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LNDtert-Butylbenzene 08/17/11 0.34 0.60 NA1.19SW8260B NA 406320ug/LND1,2,3-Trichloropropane 08/17/11 0.70 1.2 NA1.19SW8260B NA 406320ug/LND1,2,4-Trimethylbenzene 08/17/11 0.39 0.60 NA1.19SW8260B NA 406320ug/LNDsec-Butyl Benzene 08/17/11 0.29 0.60 NA1.19SW8260B NA 406320ug/LNDp-Isopropyltoluene 08/17/11 0.29 0.60 NA1.19SW8260B NA 406320ug/LND1,3-Dichlorobenzene 08/17/11 0.37 0.60 NA1.19SW8260B NA 406320ug/LND1,4-Dichlorobenzene 08/17/11 0.44 0.60 NA1.19SW8260B NA 406320ug/LNDn-Butylbenzene 08/17/11 0.38 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dichlorobenzene 08/17/11 0.47 0.60 NA1.19SW8260B NA 406320ug/LND1,2-Dibromo-3-Chloropropane 08/17/11 0.53 1.2 NA1.19SW8260B NA 406320ug/LNDHexachlorobutadiene 08/17/11 0.26 0.60 NA1.19SW8260B NA 406320ug/LND1,2,4-Trichlorobenzene 08/17/11 0.58 1.2 NA1.19SW8260B NA 406320ug/LNDNaphthalene 08/17/11 0.68 1.2 NA1.19SW8260B NA 406320ug/LND1,2,3-Trichlorobenzene 08/17/11 0.62 1.2 NA1.19SW8260B NA 406320%92.7(S) Dibromofluoromethane 08/17/11 61.2 131 NA1.19SW8260B NA 406320%90.9(S) Toluene-d8 08/17/11 75.1 127 NA1.19SW8260B NA 406320%89.0(S) 4-Bromofluorobenzene 08/17/11 64.1 120 NA1.19

Reporting limits were raised due to sediment in all VOAs.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 17:151204.22500 KirkhamB-13-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. 8260TPH 8/17/11 406320J ug/L51TPH(Gasoline) 08/17/11 26 60 34221.198260TPH 8/17/11 406320%74.1(S) 4-Bromofluorobenzene 08/17/11 34 114 34221.19

Raised reporting limit - see comment for 8260B analysis.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 17:151204.22500 KirkhamB-13-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 17:151204.22500 KirkhamB-13-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.091Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.0095Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.043Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.020Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/L0.0056Silver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:551204.22500 KirkhamB-5-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:551204.22500 KirkhamB-5-GW

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771SW6010B 8/12/11 406242mg/L0.030Barium (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/L0.023Cobalt (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771SW6010B 8/12/11 406242mg/L0.023Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/L0.033Nickel (Dissolved) 08/15/11 0.002 0.009 33771SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771SW6010B 8/12/11 406242mg/L0.0054Silver (Dissolved) 08/15/11 0.002 0.005 33771SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/10/11 / 16:451204.22500 KirkhamEquip BLANK

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:

SW7470AAnalytical Method:

Prep Date:

Analyzed Date:

08/12/11 Prep Batch:

Analytical Batch:

406238

mg/L

08/15/11

33657470A1108073Water

ParametersMethodBlankConc.

PQL MDL Lab

Qualifier

0.00005 0.0002Mercury 0.00007

Work Order:

Matrix:

Units:

Prep Method:

SW8270CAnalytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406315

mg/Kg

08/15/11

33743545_BNA1108073Soil


PQL MDL Lab

Qualifier

0.660 0.653Pyridine ND0.110 0.330N-Nitrosdimethylamine ND0.123 0.330Aniline ND0.129 0.330Phenol ND0.0683 0.330Bis(2-chloroethyl) ether ND0.129 0.3302-Chlorophenol ND

0.0733 0.3301,3-Dichlorobenzene ND0.0663 6.591,4-Dichlorobenzene ND0.104 0.330Benzyl Alcohol ND

0.0713 0.3301,2-Dichlorobenzene ND0.116 0.3302-Methylphenol (o-Cresol) ND0.0683 0.330Bis(2-chloroisopropyl)ether ND0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND0.0931 0.330N-nitroso-di-n-propylamine ND0.0465 0.330Hexachloroethane ND0.0528 0.330Nitrobenzene ND0.0574 0.653Isophorone ND0.0525 0.6532-Nitrophenol ND0.133 6.592,4-Dimethylphenol ND5.59 0.330Benzoic Acid ND

0.0584 0.330Bis(2-Chloroethoxy)methane ND0.104 0.3302,4-Dichlorophenol ND0.0733 0.3301,2,4-Trichlorobenzene ND0.104 0.3302,6-Dichlorophenol ND0.0901 0.330Naphthalene ND0.0990 0.3304-Chloroaniline ND0.0653 0.330Hexachloro-1,3-butadiene ND0.102 0.3304-Chloro-3-methylphenol ND0.0792 0.3302-Methylnaphthalene ND0.0792 0.3301-Methylnaphthalene ND0.0277 0.330Hexachlorocyclopentadiene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406315

mg/Kg

08/15/11

33743545_BNA1108073Soil


PQL MDL Lab

Qualifier

0.0950 0.3302,4,6-Trichlorophenol ND0.121 0.3302,4,5-Trichlorophenol ND

0.0594 3.272-Chloronaphthalene ND0.0693 0.3302-Nitroaniline ND0.118 0.330Dimethyl phthalate ND0.106 0.3301,3-Dinitrobenzene ND

0.0851 0.330Acenaphthylene ND0.0267 0.3302,6-Dinitrotoluene ND0.0858 0.3301,2-Dinitrobenzene ND0.0693 0.3303-Nitroaniline ND0.0960 0.330Acenaphthene ND0.0297 3.272,4-Dinitrophenol ND0.0663 0.3304-Nitrophenol ND0.0782 0.330Dibenzofuran ND0.0267 0.3302,4-Dinitrotoluene ND0.119 0.3302,3,5,6-Tetrachlorophenol ND0.119 0.3302,3,4,6-Tetrachlorophenol ND0.117 0.330Diethylphthalate ND0.0990 0.330Fluorene ND0.0802 0.3304-Chlorophenyl phenyl ether ND0.0802 0.3304-Nitroaniline ND0.0663 0.3304,6-Dinitro-2-methylphenol ND0.0663 0.330Diphenylamine ND0.109 0.330Azobenzene ND

0.0812 3.274-Bromophenyl phenyl ether ND0.101 0.330Hexachlorobenzene ND0.102 3.27Pentachlorophenol ND0.142 0.330Phenanthrene ND0.132 0.330Anthracene ND0.132 0.330Carbazole ND0.108 1.68Di-n-butylphthalate ND0.132 0.653Fluoranthene ND0.374 3.27Benzidine ND0.147 0.330Pyrene ND0.0891 0.330Benzyl butyl phthalate ND0.149 0.330Benz[a]anthracene ND0.152 0.3303,3'-Dichlorobenzidine ND0.176 0.330Chrysene ND

0.0832 0.330Bis(2-Ethylhexyl)phthalate ND0.138 0.330Di-n-octyl phthalate ND0.133 0.330Benzo[b]fluoranthene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406315

mg/Kg

08/15/11

33743545_BNA1108073Soil


PQL MDL Lab

Qualifier

0.169 0.330Benzo[k]fluoranthene ND0.135 0.330Benzo[a]pyrene ND0.131 0.330Indeno[1,2,3-cd]pyrene ND0.151 0.330Dibenz[a,h]anthracene ND0.150 0.330Benzo[g,h,i]perylene ND0.150 0.3301,4-Dinitrobenzene ND

2,4,6-Tribromophenol (S) 33.52-Fluorobiphenyl (S) 52.02-Fluorophenol (S) 55.2Nitrobenzene-d5 (S) 50.7Phenol-d6 (S) 60.4p-Terphenyl-d14 (S) 85.4

Work Order:

Matrix:

Units:

Prep Method:

SW6010BAnalytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406242

mg/Kg

08/15/11

337730051108073Water


PQL MDL Lab

Qualifier

0.004 0.009Antimony (Dissolved) ND0.005 0.009Arsenic (Dissolved) ND0.002 0.009Barium (Dissolved) ND0.002 0.005Beryllium (Dissolved) ND0.001 0.005Cadmium (Dissolved) ND0.002 0.005Chromium (Dissolved) ND0.002 0.005Cobalt (Dissolved) ND0.003 0.009Copper (Dissolved) 0.003570.005 0.014Lead (Dissolved) ND0.002 0.009Molybdenum (Dissolved) ND0.002 0.009Nickel (Dissolved) ND0.004 0.02Selenium (Dissolved) ND0.002 0.005Silver (Dissolved) ND0.004 0.009Thallium (dissolved) ND0.004 0.009Vanadium (Dissolved) ND0.002 0.009Zinc (dissolved) ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108073Soil


PQL MDL Lab

Qualifier

0.660 0.653Pyridine ND0.110 0.330N-Nitrosdimethylamine ND0.123 0.330Aniline ND0.129 0.330Phenol ND0.0683 0.330Bis(2-chloroethyl) ether ND0.129 0.3302-Chlorophenol ND

0.0733 0.3301,3-Dichlorobenzene ND0.0663 6.591,4-Dichlorobenzene ND0.104 0.330Benzyl Alcohol ND

0.0713 0.3301,2-Dichlorobenzene ND0.116 0.3302-Methylphenol (o-Cresol) ND0.0683 0.330Bis(2-chloroisopropyl)ether ND0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND0.0931 0.330N-nitroso-di-n-propylamine ND0.0465 0.330Hexachloroethane ND0.0528 0.330Nitrobenzene ND0.0574 0.653Isophorone ND0.0525 0.6532-Nitrophenol ND0.133 6.592,4-Dimethylphenol ND5.59 0.330Benzoic Acid ND

0.0584 0.330Bis(2-Chloroethoxy)methane ND0.104 0.3302,4-Dichlorophenol ND0.0733 0.3301,2,4-Trichlorobenzene ND0.104 0.3302,6-Dichlorophenol ND0.0901 0.330Naphthalene ND0.0990 0.3304-Chloroaniline ND0.0653 0.330Hexachloro-1,3-butadiene ND0.102 0.3304-Chloro-3-methylphenol ND0.0792 0.3302-Methylnaphthalene ND0.0792 0.3301-Methylnaphthalene ND0.0277 0.330Hexachlorocyclopentadiene ND0.0950 0.3302,4,6-Trichlorophenol ND0.121 0.3302,4,5-Trichlorophenol ND

0.0594 3.272-Chloronaphthalene ND0.0693 0.3302-Nitroaniline ND0.118 0.330Dimethyl phthalate ND0.106 0.3301,3-Dinitrobenzene ND

0.0851 0.330Acenaphthylene ND0.0267 0.3302,6-Dinitrotoluene ND0.0858 0.3301,2-Dinitrobenzene ND0.0693 0.3303-Nitroaniline ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108073Soil


PQL MDL Lab

Qualifier

0.0960 0.330Acenaphthene ND0.0297 3.272,4-Dinitrophenol ND0.0663 0.3304-Nitrophenol ND0.0782 0.330Dibenzofuran ND0.0267 0.3302,4-Dinitrotoluene ND0.119 0.3302,3,5,6-Tetrachlorophenol ND0.119 0.3302,3,4,6-Tetrachlorophenol ND0.117 0.330Diethylphthalate ND0.0990 0.330Fluorene ND0.0802 0.3304-Chlorophenyl phenyl ether ND0.0802 0.3304-Nitroaniline ND0.0663 0.3304,6-Dinitro-2-methylphenol ND0.0663 0.330Diphenylamine ND0.109 0.330Azobenzene ND

0.0812 3.274-Bromophenyl phenyl ether ND0.101 0.330Hexachlorobenzene ND0.102 3.27Pentachlorophenol ND0.142 0.330Phenanthrene ND0.132 0.330Anthracene ND0.132 0.330Carbazole ND0.108 1.68Di-n-butylphthalate ND0.132 0.653Fluoranthene ND0.374 3.27Benzidine ND0.147 0.330Pyrene ND0.0891 0.330Benzyl butyl phthalate ND0.149 0.330Benz[a]anthracene ND0.152 0.3303,3'-Dichlorobenzidine ND0.176 0.330Chrysene ND

0.0832 0.330Bis(2-Ethylhexyl)phthalate ND0.138 0.330Di-n-octyl phthalate ND0.133 0.330Benzo[b]fluoranthene ND0.169 0.330Benzo[k]fluoranthene ND0.135 0.330Benzo[a]pyrene ND0.131 0.330Indeno[1,2,3-cd]pyrene ND0.151 0.330Dibenz[a,h]anthracene ND0.150 0.330Benzo[g,h,i]perylene ND0.150 0.3301,4-Dinitrobenzene ND

2,4,6-Tribromophenol (S) 33.32-Fluorobiphenyl (S) 46.72-Fluorophenol (S) 59.8Nitrobenzene-d5 (S) 48.5


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108073Soil


PQL MDL Lab

Qualifier

Phenol-d6 (S) 60.6p-Terphenyl-d14 (S) 89.6

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406266

mg/Kg

08/16/11

338830501108073Soil


PQL MDL Lab

Qualifier

0.20 5.0Antimony 0.350.28 1.7Arsenic 0.28

1 5.0Barium 1.10.0840 2.0Beryllium ND0.059 1.0Cadmium ND0.059 5.0Chromium 0.330.14 5.0Cobalt ND

0.090 5.0Copper 0.180.043 1.0Lead 0.340.059 5.0Molybdenum 0.120.059 5.0Nickel 0.150.29 5.0Selenium ND1.0 1.0Silver ND0.12 5.0Thallium ND0.12 5.0Vanadium 0.140.59 5.0Zinc 0.88


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406267

mg/Kg

08/16/11

338930501108073Soil


PQL MDL Lab

Qualifier

0.20 5.0Antimony 0.350.28 1.7Arsenic 0.28

1 5.0Barium 1.10.0840 2.0Beryllium ND0.059 1.0Cadmium ND0.059 5.0Chromium 0.330.14 5.0Cobalt ND

0.090 5.0Copper 0.180.043 1.0Lead 0.340.059 5.0Molybdenum 0.120.059 5.0Nickel 0.150.29 5.0Selenium ND1.0 1.0Silver ND0.12 5.0Thallium ND0.12 5.0Vanadium 0.140.59 5.0Zinc 0.88

Work Order:

Matrix:

Units:

Prep Method:

7471ABAnalytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406269

mg/Kg

08/16/11

339274711108073Soil


PQL MDL Lab

Qualifier

0.01 0.10Mercury ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406270

mg/Kg

08/16/11

339374711108073Soil


PQL MDL Lab

Qualifier

0.01 0.10Mercury ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:

SW8015B(M)Analytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406298

mg/Kg

08/16/11

33983545_TPH1108073Soil


PQL MDL Lab

Qualifier

0.758 2.0TPH as Diesel 1.41.78 4.0TPH as Motor Oil 2.5

Pentacosane (S) 110

Work Order:

Matrix:

Units:

Prep Method:

SW8082Analytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406324

mg/Kg

08/17/11

34003545_PCB1108073Soil


PQL MDL Lab

Qualifier

0.0230 0.10Aroclor1016 ND0.0920 0.20Aroclor1221 ND0.0460 0.10Aroclor1232 ND0.0430 0.10Aroclor1242 ND0.0360 0.10Aroclor1248 ND0.0240 0.10Aroclor1254 ND0.0270 0.10Aroclor1260 ND

TCMX (S) 74.9DCBP (S) 71.6


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406314

ug/Kg

08/16/11

34013545_OCP1108073Soil


PQL MDL Lab

Qualifier

0.44 2.0alpha-BHC ND0.40 2.0gamma-BHC ND0.36 2.0beta-BHC ND0.49 2.0delta-BHC ND1.1 2.0Heptachlor ND0.44 2.0Aldrin ND0.32 2.0Heptachlor epoxide ND0.42 2.0gamma-Chlordane ND0.36 2.0alpha-Chlordane ND0.59 2.0Endosulfan I ND0.48 2.04,4'-DDE ND0.43 2.0Dieldrin ND0.57 2.0Endrin ND0.47 2.04,4'-DDD ND1.5 2.0Endosulfan II ND0.81 2.04,4'-DDT ND1.0 2.0Endrin aldehyde ND0.49 2.0Endosulfan sulfate ND0.62 5.0Methoxychlor ND0.40 2.0Endrin Ketone ND10 20Chlordane ND10 100Toxaphene ND

TCMX (S) 86.4DCBP (S) 77.1


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406314

ug/Kg

08/16/11

34013545_OCP1108073Soil


PQL MDL Lab

Qualifier

0.44 2.0alpha-BHC ND0.40 2.0gamma-BHC ND0.36 2.0beta-BHC ND0.49 2.0delta-BHC ND1.1 2.0Heptachlor ND0.44 2.0Aldrin ND0.32 2.0Heptachlor epoxide ND0.42 2.0gamma-Chlordane ND0.36 2.0alpha-Chlordane ND0.59 2.0Endosulfan I ND0.48 2.04,4'-DDE ND0.43 2.0Dieldrin ND0.57 2.0Endrin ND0.47 2.04,4'-DDD ND1.5 2.0Endosulfan II ND0.81 2.04,4'-DDT ND1.0 2.0Endrin aldehyde ND0.49 2.0Endosulfan sulfate ND0.62 5.0Methoxychlor ND0.40 2.0Endrin Ketone ND10 20Chlordane ND10 100Toxaphene ND

TCMX (S) 76.8DCBP (S) 72.8

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108073Water


PQL MDL Lab

Qualifier

0.0440 0.10TPH as Diesel (SG) ND0.0920 0.20TPH as Motor Oil (SG) ND

Pentacosane (S) 51.7 S


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108073Water


PQL MDL Lab

Qualifier

0.0440 0.10TPH as Diesel (SG) ND0.0920 0.20TPH as Motor Oil (SG) 0.13

Pentacosane (S) 75.1

Work Order:

Matrix:

Units:

Prep Method:

8260TPHAnalytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

406301

ug/Kg

08/15/11

341350351108073Soil


PQL MDL Lab

Qualifier

17 100TPH(Gasoline) ND(S) 4-Bromofluorobenzene 97.7

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406325

mg/Kg

08/18/11

34183545_TPH1108073Soil


PQL MDL Lab

Qualifier

0.758 2.0TPH as Diesel 1.21.78 4.0TPH as Motor Oil 3.3

Pentacosane (S) 111


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406326

mg/Kg

08/18/11

34193545_PCB1108073Soil


PQL MDL Lab

Qualifier

0.0230 0.10Aroclor1016 ND0.0920 0.20Aroclor1221 ND0.0460 0.10Aroclor1232 ND0.0430 0.10Aroclor1242 ND0.0360 0.10Aroclor1248 ND0.0240 0.10Aroclor1254 ND0.0270 0.10Aroclor1260 ND

TCMX (S) 99.1DCBP (S) 113

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406320

ug/L

08/17/11

342250301108073Water


PQL MDL Lab

Qualifier


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406328

ug/Kg

08/15/11

342550351108073Soil


PQL MDL Lab

Qualifier



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406330

ug/Kg

08/18/11

342750351108073Soil


PQL MDL Lab

Qualifier


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406411

ug/Kg

08/24/11

348050351108073Soil


PQL MDL Lab

Qualifier


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406447

mg/Kg

08/26/11

3496WET/3010B1108073Soil


PQL MDL Lab

Qualifier

0.0500 0.10Lead (STLC) ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406301

ug/Kg

08/15/11

NANA1108073Soil


PQL MDL Lab

Qualifier

4.4 10Dichlorodifluoromethane ND4.6 10Chloromethane ND2.6 10Vinyl Chloride ND4.7 10Bromomethane ND2.9 10Trichlorofluoromethane ND1.5 101,1-Dichloroethene ND3.7 10Freon 113 ND2.0 50Methylene Chloride ND1.1 10trans-1,2-Dichloroethene ND2.6 10MTBE ND21 50tert-Butanol ND2.2 10Diisopropyl ether (DIPE) ND1.3 101,1-Dichloroethane ND2.4 10ETBE ND1.8 10cis-1,2-Dichloroethene ND1.2 102,2-Dichloropropane ND2.3 10Bromochloromethane ND1.2 10Chloroform ND1.6 10Carbon Tetrachloride ND1.2 101,1,1-Trichloroethane ND1.4 101,1-Dichloropropene ND1.5 10Benzene ND2.1 10TAME ND1.9 101,2-Dichloroethane ND3.9 10Trichloroethylene ND2.2 10Dibromomethane ND1.3 101,2-Dichloropropane ND1.1 10Bromodichloromethane ND1.4 10cis-1,3-Dichloropropene ND0.98 10Toluene ND1.8 10Tetrachloroethylene ND1.2 10trans-1,3-Dichloropropene ND1.8 101,1,2-Trichloroethane ND1.1 10Dibromochloromethane ND2.1 101,3-Dichloropropane ND1.7 101,2-Dibromoethane ND0.86 10Ethyl Benzene ND4.2 10Chlorobenzene ND0.86 101,1,1,2-Tetrachloroethane ND1.9 10m,p-Xylene ND0.66 5.0o-Xylene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406301

ug/Kg

08/15/11

NANA1108073Soil


PQL MDL Lab

Qualifier

0.77 10Styrene ND1.9 10Bromoform ND1.2 10Isopropyl Benzene ND1.4 10n-Propylbenzene ND1.2 10Bromobenzene ND3.0 101,1,2,2-Tetrachloroethane ND1.1 101,3,5-Trimethylbenzene ND3.3 101,2,3-Trichloropropane ND1.6 104-Chlorotoluene ND1.6 102-Chlorotoluene ND1.4 10tert-Butylbenzene ND1.1 101,2,4-Trimethylbenzene ND1.6 10sec-Butyl Benzene ND1.5 10p-Isopropyltoluene ND1.8 101,3-Dichlorobenzene ND1.5 101,4-Dichlorobenzene ND2.2 10n-Butylbenzene ND1.3 101,2-Dichlorobenzene ND4.2 101,2-Dibromo-3-Chloropropane ND2.6 10Hexachlorobutadiene ND2.1 101,2,4-Trichlorobenzene ND2.8 10Naphthalene ND2.9 101,2,3-Trichlorobenzene ND

(S) Dibromofluoromethane 77.1(S) Toluene-d8 82.7(S) 4-Bromofluorobenzene 89.9


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406320

ug/L

08/17/11

NANA1108073Water


PQL MDL Lab

Qualifier

0.41 0.50Dichlorodifluoromethane ND0.41 0.50Chloromethane ND0.37 0.50Vinyl Chloride ND0.37 0.50Bromomethane ND0.34 0.50Trichlorofluoromethane ND0.29 0.501,1-Dichloroethene ND0.38 0.50Freon 113 ND0.18 5.0Methylene Chloride ND0.31 0.50trans-1,2-Dichloroethene ND0.38 0.50MTBE ND1.5 5.0tert-Butanol ND0.36 0.50Diisopropyl ether (DIPE) ND0.28 0.501,1-Dichloroethane ND0.40 0.50ETBE ND0.33 0.50cis-1,2-Dichloroethene ND0.37 0.502,2-Dichloropropane ND0.34 0.50Bromochloromethane ND0.29 0.50Chloroform ND0.26 0.50Carbon Tetrachloride ND0.32 0.501,1,1-Trichloroethane ND0.40 0.501,1-Dichloropropene ND0.33 0.50Benzene ND0.32 0.50TAME ND0.28 0.501,2-Dichloroethane ND0.38 0.50Trichloroethylene ND0.21 0.50Dibromomethane ND0.37 0.501,2-Dichloropropane ND0.23 0.50Bromodichloromethane ND0.30 0.50cis-1,3-Dichloropropene ND0.19 0.50Toluene ND0.15 0.50Tetrachloroethylene ND0.20 0.50trans-1,3-Dichloropropene ND0.20 0.501,1,2-Trichloroethane ND0.21 0.50Dibromochloromethane ND0.18 0.501,3-Dichloropropane ND0.19 0.501,2-Dibromoethane ND0.14 0.50Chlorobenzene ND0.15 0.50Ethyl Benzene ND0.10 0.501,1,1,2-Tetrachloroethane ND0.20 1.0m,p-Xylene ND0.13 0.50o-Xylene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406320

ug/L

08/17/11

NANA1108073Water


PQL MDL Lab

Qualifier

0.20 0.50Styrene ND0.45 1.0Bromoform ND0.28 0.50Isopropyl Benzene ND0.39 0.50Bromobenzene ND0.26 0.501,1,2,2-Tetrachloroethane ND0.30 0.50n-Propylbenzene ND0.33 0.502-Chlorotoluene ND0.20 0.501,3,5-Trimethylbenzene ND0.32 0.504-Chlorotoluene ND0.29 0.50tert-Butylbenzene ND0.59 1.01,2,3-Trichloropropane ND0.33 0.501,2,4-Trimethylbenzene ND0.24 0.50sec-Butyl Benzene ND0.25 0.50p-Isopropyltoluene ND0.31 0.501,3-Dichlorobenzene ND0.37 0.501,4-Dichlorobenzene ND0.32 0.50n-Butylbenzene ND0.39 0.501,2-Dichlorobenzene ND0.45 1.01,2-Dibromo-3-Chloropropane ND0.22 0.50Hexachlorobutadiene ND0.48 1.01,2,4-Trichlorobenzene ND0.57 1.0Naphthalene ND0.52 1.01,2,3-Trichlorobenzene ND100 100Ethanol ND TIC



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406328

ug/Kg

08/15/11

NANA1108073Soil


PQL MDL Lab

Qualifier



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406330

ug/Kg

08/18/11

NANA1108073Soil


PQL MDL Lab

Qualifier



LCS/LCSD Summary ReportRaw values are used in quality control assessment.

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40623808/15/11

mg/L

7470A 3365

Water

1108073

Parameters MDL PQL MethodBlankConc.

SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.0002 0.0150.00005 0.188 0,80 - 120Mercury 106 1060.00007

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40631508/15/11

mg/Kg

3545_BNA 3374

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.33 1.6670.129 14.2 3016 - 98.6Phenol 53.7 46.7ND

0.33 1.6670.129 13.6 3012.9 - 91.32-Chlorophenol 48.7 42.5ND

0.33 0.8330.0663 16.2 3021.9 - 79.81,4-Dichlorobenzene 54.0 45.9ND

0.33 1.6670.0931 16.2 3015.5 - 116N-nitroso-di-n-propylamine 55.8 47.5ND

0.33 0.8330.0733 13.6 3031.7 - 85.11,2,4-Trichlorobenzene 49.3 43.1ND

0.33 1.6670.102 14.8 3023.8 - 1164-Chloro-3-methylphenol 43.9 37.9ND

0.33 0.8330.0964 12.9 3029.1 - 94.8Acenaphthene 49.5 43.5ND

0.33 1.6670.0663 9.91 3010.4 - 1314-Nitrophenol 76.6 69.6ND

0.33 0.8330.0267 14.4 3030.8 - 1242,4-Dinitrotoluene 69.2 59.8ND

0.33 1.6670.102 12.9 3019.9 - 133Pentachlorophenol 72.9 64.0ND

0.33 0.8330.147 4.39 3034.2 - 127Pyrene 75.3 72.0ND

50 24 - 113Phenol-d6 (S) 67.1 58.0ND

50 25 - 1212-Fluorophenol (S) 49.3 42.2ND

50 19 - 1222,4,6-Tribromophenol (S) 63.9 51.2ND

25 23 - 120Nitrobenzene-d5 (S) 57.8 51.1ND

25 30 - 1152-Fluorobiphenyl (S) 56.0 47.9ND

25 18 - 137p-Terphenyl-d14 (S) 53.3 49.9ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40624208/15/11

mg/Kg

3005 3377

Water

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.009 10.004 0.269 0,80 - 120Antimony (Dissolved) 91.2 91.1ND

0.009 10.005 0.293 0,80 - 120Arsenic (Dissolved) 94.3 94.2ND

0.009 10.002 0.411 0,80 - 120Barium (Dissolved) 96.7 96.6ND

0.005 10.002 3.12 2080 - 120Beryllium (Dissolved) 97.9 95.0ND

0.005 10.001 0.221 2080 - 120Cadmium (Dissolved) 97.3 97.2ND

0.005 10.002 0.0737 2080 - 120Chromium (Dissolved) 96.6 97.1ND

0.005 10.002 0.711 2080 - 120Cobalt (Dissolved) 98.3 97.3ND

0.009 10.003 0.295 2080 - 120Copper (Dissolved) 97.2 96.70.00357

0.014 10.005 0.0753 2080 - 120Lead (Dissolved) 95.2 94.9ND

0.009 10.002 0.169 2080 - 120Molybdenum (Dissolved) 97.5 96.8ND

0.009 10.002 0.334 2080 - 120Nickel (Dissolved) 97.6 97.7ND

0.02 10.004 1.45 2080 - 120Selenium (Dissolved) 95.5 94.6ND

0.005 10.002 0.582 2080 - 120Silver (Dissolved) 94.7 94.4ND

0.009 10.004 0.0323 2080 - 120Thallium (dissolved) 95.4 95.0ND

0.009 10.004 0.169 2080 - 120Vanadium (Dissolved) 96.7 96.8ND

0.009 10.002 1.28 2080 - 120Zinc (dissolved) 99.1 97.8ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40631608/16/11

mg/Kg

3545_BNA 3385

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.33 1.6670.129 20.3 3016 - 98.6Phenol 40.3 49.5ND

0.33 1.6670.129 19.2 3012.9 - 91.32-Chlorophenol 36.9 44.8ND





0.33 0.8330.0964 21.8 3029.1 - 94.8Acenaphthene 38.1 47.3ND

0.33 1.6670.0663 7.93 3010.4 - 1314-Nitrophenol 56.0 60.9ND



0.33 0.8330.147 16.8 3034.2 - 127Pyrene 59.5 70.5ND

50 24 - 113Phenol-d6 (S) 54.0 64.1ND





25 18 - 137p-Terphenyl-d14 (S) 47.4 53.4ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40626608/16/11

mg/Kg

3050 3388

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

5.0 500.20 1.27 3030.7 - 130Antimony 96.1 97.30.35

1.7 500.28 1.21 3071 - 121Arsenic 96.8 95.60.28

5.0 501 3.03 3070.2 - 130Barium 102 99.01.1

2.0 500.0840 1.52 3073.3 - 115Beryllium 95.1 93.6ND

1.0 500.059 2.75 3068.7 - 110Cadmium 98.4 95.7ND

5.0 500.059 1.60 3076 - 116Chromium 99.5 97.90.33

5.0 500.14 1.75 3057.4 - 122Cobalt 101 99.3ND

5.0 500.090 1.06 3074.8 - 119Copper 104 1030.18

1.0 500.13 0.0206 3067.9 - 118Lead 97.3 97.30.34

5.0 500.059 0.101 3062.9 - 123Molybdenum 98.7 98.80.12

5.0 500.059 2.35 3061.5 - 122Nickel 100 97.70.15

5.0 500.29 1.58 3062 - 111Selenium 93.7 92.2ND

1.0 501.0 2.03 3081.1 - 109Silver 96.7 94.8ND

5.0 500.12 0.214 3039.2 - 125Thallium 93.2 93.4ND

5.0 500.12 1.61 3065.8 - 122Vanadium 101 99.40.14

5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40626708/16/11

mg/Kg

3050 3389

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

5.0 500.20 1.07 3030.7 - 130Antimony 96.1 95.10.35

1.7 500.28 3.03 3071 - 121Arsenic 96.8 93.90.28

5.0 501 2.35 3070.2 - 130Barium 102 99.61.1

2.0 500.0840 1.35 3073.3 - 115Beryllium 95.1 96.3ND

1.0 500.059 2.07 3068.7 - 110Cadmium 98.4 96.4ND

5.0 500.059 1.63 3076 - 116Chromium 99.5 97.90.33

5.0 500.14 2.36 3057.4 - 122Cobalt 101 98.6ND

5.0 500.090 2.14 3074.8 - 119Copper 104 1020.18

1.0 500.13 0.784 3067.9 - 118Lead 97.3 96.50.34

5.0 500.059 0.936 3062.9 - 123Molybdenum 98.7 97.80.12

5.0 500.059 2.15 3061.5 - 122Nickel 100 97.90.15

5.0 500.29 4.36 3062 - 111Selenium 93.7 89.7ND

1.0 501.0 2.22 3081.1 - 109Silver 96.7 94.6ND

5.0 500.12 0.226 3039.2 - 125Thallium 93.2 93.0ND

5.0 500.12 1.89 3065.8 - 122Vanadium 101 99.10.14

5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88

Work Order:

Matrix:

Units:

Prep Method:

7471BAnalytical Method:

Prep Date:

Analyzed Date:


Analytical Batch:

40626908/16/11

mg/Kg

7471 3392

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 1.250.01 8.13 30,80.5 - 133Mercury 101 110ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40627008/16/11

mg/Kg

7471 3393

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 1.250.01 6.58 30,80.5 - 133Mercury 109 116ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40629808/16/11

mg/Kg

3545_TPH 3398

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2 33.330.758 2.45 3052.7 - 115TPH as Diesel 89.7 87.51.4

200 59.7 - 129Pentacosane (S) 96.7 1232.5

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632408/17/11

mg/Kg

3545_PCB 3400

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0230 4.95 3055.6 - 135Aroclor1016 94.2 99.0ND

0.10 0.50.0270 7.26 3065.6 - 132Aroclor1260 89.1 95.8ND

1.5 68.9 - 123TCMX (S) 103 101ND

1.5 69.5 - 119DCBP (S) 108 117ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40631408/16/11

ug/Kg

3545_OCP 3401

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2.0 200.40 1.09 3056.9 - 120gamma-BHC 84.6 83.7ND

2.0 201.1 0.0815 3063.6 - 117Heptachlor 96.3 96.4ND

2.0 200.44 0.997 3053 - 123Aldrin 87.3 86.4ND

2.0 200.43 0.827 3044 - 130Dieldrin 84.7 85.4ND

2.0 200.57 2.96 3044.1 - 121Endrin 100 97.5ND

2.0 200.81 1.01 3052.8 - 1344,4'-DDT 107 105ND

2100 52.5 - 139TCMX (S) 89.8 88.8ND

2100 50.2 - 139DCBP (S) 87.8 83.5ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632108/17/11

mg/L

3510_TPHSG 3402

Water

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0440 2.00 30,34.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND

100 57.9 - 125Pentacosane (S) 79.6 73.0ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40630108/15/11

ug/Kg

5035 3413

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

100 100017 2.25 3048.2 - 132TPH(Gasoline) 91.4 93.5ND

50 57 - 127(S) 4-Bromofluorobenzene 89.7 92.897.7

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632508/18/11

mg/Kg

3545_TPH 3418

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2 33.330.758 0.871 3052.7 - 115TPH as Diesel 87.1 87.81.2

100 59.7 - 129Pentacosane (S) 96.8 98.13.3

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632608/18/11

mg/Kg

3545_PCB 3419

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0230 4.27 3055.6 - 135Aroclor1016 92.7 88.8ND

0.10 0.50.0270 4.66 3065.6 - 132Aroclor1260 89.6 85.5ND

0.25 68.9 - 123TCMX (S) 91.7 83.8ND

0.250 69.5 - 119DCBP (S) 107 98.6ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632008/17/11

ug/L

5030 3422

Water

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

50 227.2722 0.686 3052.4 - 127TPH(Gasoline) 83.3 82.7ND

11.36 58.4 - 133(S) 4-Bromofluorobenzene 81.0 81.479.7

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632808/15/11

ug/Kg

5035 3425

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

100 100017 9.94 3048.2 - 132TPH(Gasoline) 94.3 85.3ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40633008/18/11

ug/Kg

5035 3427

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

100 100017 12.1 3048.2 - 132TPH(Gasoline) 93.1 105ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40641108/24/11

ug/Kg

5035 3480

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

100 100017 4.88 3048.2 - 132TPH(Gasoline) 90.0 85.8ND




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40644708/26/11

mg/L

WET/3010B 3496

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 100.0500 2.49 2080 - 120Lead (STLC) 87.0 89.2ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40630108/15/11

ug/Kg

NA NA

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

10 501.5 18.3 3053.7 - 1391,1-Dichloroethene 90.6 75.4ND

10 501.5 11.5 3066.5 - 135Benzene 91.5 81.6ND

10 503.9 20.3 3057.5 - 150Trichloroethylene 99.7 81.4ND

10 500.98 17.3 3056.8 - 134Toluene 102 85.4ND

10 504.2 14.0 3057.4 - 134Chlorobenzene 90.6 78.7ND

50 59.8 - 148(S) Dibromofluoromethane 73.5 88.3ND

50 55.2 - 133(S) Toluene-d8 86.9 89.4ND

50 55.8 - 141(S) 4-Bromofluorobenzene 92.8 99.0ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40632008/17/11

ug/L

NA NA

Water

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.50 17.040.29 12.2 3061.4 - 1291,1-Dichloroethene 95.6 84.6ND

0.50 17.040.33 11.8 3066.9 - 140Benzene 101 89.7ND

0.50 17.040.38 18.6 3069.3 - 144Trichloroethylene 109 90.5ND

0.50 17.040.19 5.87 3076.6 - 123Toluene 98.1 92.4ND

0.50 17.040.14 7.45 3073.9 - 137Chlorobenzene 99.0 92.1ND

11.36 61.2 - 131(S) Dibromofluoromethane 91.5 89.5ND

11.36 75.1 - 127(S) Toluene-d8 93.8 92.0ND

11.36 64.1 - 120(S) 4-Bromofluorobenzene 93.0 90.2ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40632808/15/11

ug/Kg

NA NA

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

10 501.5 27.3 3053.7 - 1391,1-Dichloroethene 82.3 108ND

10 501.5 19.9 3066.5 - 135Benzene 93.5 114ND

10 503.9 4.48 3057.5 - 150Trichloroethylene 115 121ND

10 500.98 2.81 3056.8 - 134Toluene 110 113ND

10 504.2 3.55 3057.4 - 134Chlorobenzene 107 111ND


50 55.2 - 133(S) Toluene-d8 88.8 88.5ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40633008/18/11

ug/Kg

NA NA

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier


10 501.5 1.67 3066.5 - 135Benzene 90.7 89.3ND


10 500.98 5.34 3056.8 - 134Toluene 101 95.6ND



50 55.2 - 133(S) Toluene-d8 86.3 86.0ND




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40641108/24/11

ug/Kg

NA NA

Soil

1108073


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

10 501.5 1.97 3053.7 - 1391,1-Dichloroethene 81.5 83.0

10 501.5 2.77 3066.5 - 135Benzene 86.4 84.0

10 503.9 6.04 3057.5 - 150Trichloroethylene 90.0 84.7

10 500.98 10.9 3056.8 - 134Toluene 96.5 86.6

10 504.2 10.7 3057.4 - 134Chlorobenzene 89.5 80.5

50 59.8 - 148(S) Dibromofluoromethane 80.9 80.6

50 55.2 - 133(S) Toluene-d8 90.0 90.8

50 55.8 - 141(S) 4-Bromofluorobenzene 93.4 90.8


MS/MSD Summary ReportRaw values are used in quality control assessment.

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:

Prep Method: 08/12/11

1108073-037CSpiked Sample:

Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW7470A 40623808/15/11

mg/L

33657470A

Water

Parameters MDL PQL SampleConc.

SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

0.015 75 - 1250.00005 0.0002 10.4 20Mercury 104 1180.00009

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40624208/15/11

mg/Kg

33773005

Water


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1 75 - 1250.004 0.009 0.504 20Antimony (Dissolved) 91.1 91.30.001 75 - 1250.005 0.009 1.21 20Arsenic (Dissolved) 91.3 92.00.001 80 - 1200.002 0.009 1.66 20Barium (Dissolved) 92.8 90.70.04561 80 - 1200.002 0.005 6.28 20Beryllium (Dissolved) 87.6 93.501 75 - 1250.001 0.005 2.28 20Cadmium (Dissolved) 93.2 90.80.001 75 - 1250.002 0.005 1.65 20Chromium (Dissolved) 93.1 91.40.001 75 - 1250.002 0.005 1.95 20Cobalt (Dissolved) 92.5 91.10.001 75 - 1250.003 0.009 0.753 20Copper (Dissolved) 93.5 93.20.001 75 - 1250.005 0.014 0.452 20Lead (Dissolved) 87.9 88.20.001 75 - 1250.002 0.009 0.579 20Molybdenum (Dissolved) 92.1 92.40.0301 75 - 1250.002 0.009 2.39 20Nickel (Dissolved) 93.0 90.70.001 75 - 1250.004 0.02 0.460 20Selenium (Dissolved) 91.0 91.30.001 75 - 1250.002 0.005 1.75 20Silver (Dissolved) 90.8 89.30.001 75 - 1250.004 0.009 0.203 20Thallium (dissolved) 86.1 85.60.001 75 - 1250.004 0.009 1.21 20Vanadium (Dissolved) 93.3 91.80.001 75 - 1250.002 0.009 0.0990 20Zinc (dissolved) 92.8 92.80.00



Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:


1108073-002ASpiked Sample:

Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40626608/16/11

mg/Kg

33883050

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

50 30.7 - 1300.20 5.0 0.196 30Antimony 86.6 86.80.0050 71 - 1210.28 1.7 1.76 30Arsenic 91.5 89.80.04050 70.2 - 1301 S5.0 0.324 30Barium 130 1310.5550 73.3 - 1150.0840 2.0 7.05 30Beryllium 93.3 86.70.0050 68.7 - 1100.059 1.0 3.35 30Cadmium 95.7 92.60.0050 76 - 1160.059 S5.0 0.698 30Chromium 136 1350.5150 57.4 - 1220.14 5.0 1.39 30Cobalt 97.4 95.50.1250 74.8 - 1190.090 5.0 0.634 30Copper 110 1110.0050 67.9 - 1180.13 1.0 4.07 30Lead 96.2 92.00.04050 62.9 - 1230.059 5.0 3.08 30Molybdenum 93.9 91.10.0050 61.5 - 1220.059 S5.0 2.32 30Nickel 123 1190.3850 62 - 1110.29 5.0 2.38 30Selenium 88.1 86.00.0050 81.1 - 1091.0 1.0 0.538 30Silver 93.2 92.70.0050 39.2 - 1250.12 5.0 6.01 30Thallium 84.6 79.70.0050 65.8 - 1220.12 5.0 1.75 30Vanadium 121 1180.4050 59.9 - 1220.59 5.0 0.628 30Zinc 105 1060.22

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

7471B 40626908/16/11

mg/Kg

33927471

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1.25 60 - 1400.01 0.10 1.20 30Mercury 109 1100.00017



Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:

Prep Method: NA


Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8260B 40630108/15/11

ug/Kg

NANA

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

38 53.7 - 1391.2 7.6 6.13 301,1-Dichloroethene 83.5 88.7038 66.5 - 1351.1 7.6 6.15 30Benzene 84.1 89.5038 57.5 - 1502.9 7.6 0.498 30Trichloroethylene 88.2 88.6038 56.8 - 1340.75 7.6 4.02 30Toluene 85.7 89.2038 57.4 - 1343.2 7.6 0.242 30Chlorobenzene 91.1 90.8038 59.8 - 148(S) Dibromofluoromethane 95.3 10138 55.2 - 133(S) Toluene-d8 85.4 87.738 55.8 - 141(S) 4-Bromofluorobenzene 96.8 97.3

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8270C 40631508/15/11

mg/Kg

33743545_BNA

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1.667 16 - 98.60.129 0.33 30.2 30Phenol 50.9 68.70.0001.667 12.9 - 91.30.129 0.33 30.3 302-Chlorophenol 56.0 76.30.0000.833 21.9 - 79.80.0663 S0.33 32.2 301,4-Dichlorobenzene 59.3 82.10.0001.667 15.5 - 1160.0931 0.33 24.8 30N-Nitroso-di-n-propylamine 24.2 31.00.0000.833 31.7 - 85.10.0733 0.33 34.2 301,2,4-Trichlorobenzene 57.0 80.40.0001.667 23.8 - 1160.102 0.33 30.3 304-Chloro-3-methylphenol 48.2 65.50.0000.833 29.1 - 94.80.0964 0.33 33.7 30Acenaphthene 64.0 90.00.0001.667 10.4 - 1310.0663 0.33 3.46 304-Nitrophenol 68.7 71.30.0000.833 30.8 - 1240.0267 0.33 17.4 302,4-Dinitrotoluene 53.7 63.80.0001.667 19.9 - 1330.102 0.33 19.3 30Pentachlorophenol 72.2 87.40.0000.833 34.2 - 1270.147 0.33 14.2 30Pyrene 109 1260.000

50 24 - 113Phenol-d6 (S) 65.8 91.950 25 - 1212-Fluorophenol (S) 51.0 71.250 19 - 1222,4,6-Tribromophenol (S) 62.2 85.625 23 - 120Nitrobenzene-d5 (S) 60.8 86.425 30 - 1152-Fluorobiphenyl (S) 66.2 95.725 18 - 137p-Terphenyl-d14 (S) 69.7 72.7



Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8015B(M) 40631908/17/11

mg/Kg

33983545_TPH

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

33.33 50.3 - 1253.8 S10 10.3 30TPH as Diesel 23.0 20.54.6511100 57.9 - 125Pentacosane (S) 90.3 86.2

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8082 40632408/17/11

mg/Kg

34003545_PCB

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1 55.6 - 1350.0230 0.10 1.86 30Aroclor1016 103 10100.5 65.6 - 1320.0270 0.10 2.68 30Aroclor1260 98.6 96.00.0031.5 50.4 - 136TCMX (S) 98.2 99.41.5 69.5 - 119DCBP (S) 112 112

Work Order: 1108073

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40644708/26/11

mg/L

3496WET/3010B

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

10 75 - 1250.0500 0.10 0.390 20Lead (STLC) 86.4 87.10.414


Laboratory Qualifiers and Definitions

Method Detection Limit (MDL) - the minimum concentration of a substance that can be measured and reported with a 99% confidence that the analyte concentration is greater than zero

Matrix Spike (MS/MSD) - Client sample spiked with identical concentrations of target analyte (s). The spiking occurs prior to the sample preparation and analysis. They are used to document the precision and bias of a method in a given sample matrix.

Matrix - the component or substrate that contains the analyte of interest (e.g., - groundwater, sediment, soil, waste water, etc)

Laboratory Control Sample (LCS ad LCSD) - A known matrix spiked with compounds representative of the target analyte(s). This is used to document laboratory performance.

Duplicate - a field sample and/or laboratory QC sample prepared in duplicate following all of the same processes and procedures used on the original sample (sample duplicate, LCSD, MSD)

Blank (Method/Preparation Blank) -MB/PB - An analyte-free matrix to which all reagents are added in the same volumes/proportions as used in sample processing. The method blank is used to document contamination resulting from the analytical process.

Practical Quantitation Limit (PQL) - a laboratory determined value at 2 to 5 times above the MDL that can be reproduced in a manner that results in a 99% confidence level that the result is both accurate and precise. PQLs reflect all preparation factors and/or dilution factors that have been applied to the sample during the preparation and/or analytical processes.

Precision (%RPD) - The agreement among a set of replicate/duplicate measurements without regard to known value of the replicates

Surrogate (S) or (Surr) - An organic compound which is similar to the target analyte(s) in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples. Surrogates are used in most organic analysis to demonstrate matrix compatibility with the chosen method of analysis

Tentatively Identified Compound (TIC) - A compound not contained within the analytical calibration standards but present in the GCMS library of defined compounds. When the library is searched for an unknown compound, it can frequently give a tentative identification to the compound based on retention time and primary and secondary ion match. TICs are reported as estimates and are candidates for further investigation.

Units: the unit of measure used to express the reported result - mg/L and mg/Kg (equivalent to PPM - parts per million in liquid and solid), ug/L and ug/Kg (equivalent to PPB - parts per billion in liquid and solid), ug/m3, mg.m3, ppbv and ppmv (all units of measure for reporting concentrations in air), % ( equivalent to 10000 ppm or 1,000,000 ppb), ug/Wipe ( concentration found on the surface of a single Wipe usually taken over a 100cm2 surface)

B - Indicates when the anlayte is found in the associated method or preparation blank D - Surrogate is not recoverable due to the necessary dilution of the sampleE - Indicates the reportable value is outside of the calibration range of the instrument but within the linear range of the instrument (unless otherwise noted) Values reported with an E qualifier should be considered as estimated.H- Indicates that the recommended holding time for the analyte or compound has been exceededJ- Indicates a value between the method MDL and PQL and that the reported concentration should be considered as estimated rather the quantitative NA - Not AnalyzedN/A - Not ApplicableNR - Not recoverable - a matrix spike concentration is not recoverable due to a concentration within the original sample that is greater than four times the spike concentration addedR- The % RPD between a duplicate set of samples is outside of the absolute values established by laboratory control chartsS- Spike recovery is outside of established method and/or laboratory control limits. Further explanation of the use of this qualifier should be included within a case narrative

X -Used to indicate that a value based on pattern identification is within the pattern range but not typical of the pattern found in standards. Further explanation may or may not be provided within the sample footnote and/or the case narrative.

DEFINITIONS:

Accuracy/Bias (% Recovery) - The closeness of agreement between an observed value and an accepted reference value.

LABORATORY QUALIFIERS:


pH Adjusted by: pH Checked by:

°C6

Yes

Yes

Yes

Temperature:

Water-pH acceptable upon receipt?

Water-VOA vials have zero headspace?

Container/Temp Blank temperature in compliance?

All samples received within holding time?

Sample Preservation and Hold Time (HT) Information

YesSamples containers intact?

Yes

Yes

Not Present

Yes

Sufficient sample volume for indicated test?

Samples in proper container/bottle?

Custody seals intact on shipping container/cooler?

Shipping Container/Cooler In Good Condition?

Sample Receipt Information

Yes

Yes

Yes

Not Present

Chain of custody agrees with sample labels?

Chain of custody signed when relinquished and received?

Chain of custody present?

Custody seals intact on sample bottles?

Chain of Custody (COC) Information

Checklist Completed By: NG

Carrier Name: First Courier

Physically Logged By: NG

Received By: NG

Date and Time Received: 8/23/2011 14:15

Work Order No.: 1108073

Project Name: 500 Kirkham

Client Name: Northgate Environmental Management Inc.

Sample Receipt Checklist


Login Summary Report

Report Due Date:

5 day TAT! Received 32 soils and 8 waters @ 6'C. Dissolved metals for GW samples. Silica gel cleanup for all waters.Pretarred voas for 8260.Sample 031A received only 3 voas no liner client informed. Per client request from 08/23/2011 additional analysis added: 004 (WET/TCLP Pb) and 015(TPH-G and VOC)on 3 day RUSH TAT. Due 08/26/2011. Only STLC Pb on 004 per client, not enough sample.

14:15

8/23/2011

Northgate Environmental Management Inc.TL5143

500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25

1108073Work Order # :

SubbedRequestedTests

TestOn Hold

SampleOn Hold

ScheduledDisposal

MatrixCollection Date/Time

Client Sample ID

WO Sample ID

B-1-1.01108073-001A Soil 02/06/1208/10/11 8:30S_6010BCAM17S_7471BHGS_TPHDOS_8082PCBS_8081AOCPS_8270FullS_GCMS-GROS_8260Full

Sample Note: Pretarred voas for 8260 for soil samples. Use this sample for MS/MSD for all analyses.B-1-5.01108073-002A Soil 02/06/1208/10/11 8:35

S_6010BCAM17S_8082PCBS_TPHDOS_8260FullS_GCMS-GROS_8270FullS_7471BHG

B-1-7.01108073-003A Soil 02/06/12 On-Hold08/10/11 8:40Hold Samples

B-3-1.01108073-004A Soil 02/06/1208/10/11 9:15S_6010B(STLC)S_8081AOCPS_8270FullS_7471BHGS_GCMS-GROS_8260FullS_8082PCBS_TPHDOS_6010BCAM17

Sample Note: Per client request from 08/23/2011 add STLC Lead on sample 004. 3 day TAT RUSH Due 08/26/2011.B-3-5.01108073-005A Soil 02/06/1208/10/11 9:20

S_6010BCAM17



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_GCMS-GROS_8260FullS_8270FullS_TPHDOS_8082PCBS_7471BHG


B-10-1.01108073-007A Soil 02/06/1208/10/11 9:50S_6010BCAM17S_8082PCBS_7471BHGS_TPHDOS_8270FullS_GCMS-GROS_8260FullS_8081AOCP

B-10-5.01108073-008A Soil 02/06/1208/10/11 9:55S_6010BCAM17S_8270FullS_7471BHGS_GCMS-GROS_8260FullS_TPHDOS_8082PCB


B-12-1.01108073-010A Soil 02/06/1208/10/11 10:40S_6010BCAM17S_GCMS-GROS_8260FullS_8270FullS_8081AOCPS_8082PCB



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_TPHDOS_7471BHG

B-12-5.01108073-011A Soil 02/06/1208/10/11 10:50S_6010BCAM17S_GCMS-GROS_7471BHGS_8082PCBS_8260FullS_8270FullS_TPHDO


B-11-1.01108073-013A Soil 02/06/1208/10/11 11:50S_6010BCAM17S_8081AOCPS_8082PCBS_7471BHGS_GCMS-GROS_8260FullS_TPHDOS_8270Full

B-11-6.01108073-014A Soil 02/06/1208/10/11 11:55S_6010BCAM17S_7471BHGS_8260FullS_GCMS-GROS_8082PCBS_8270FullS_TPHDO

B-11-10.01108073-015A Soil 02/06/1208/10/11 12:00S_GCMS-GROS_8260Full

Sample Note: Per client request added TPH-Gas and VOCs on sample 015A. HOLDING TIME IS UP on 08/24/2011. 3 day TAT Due 08/26/2011



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

B-14-1.01108073-016A Soil 02/06/1208/10/11 12:50S_6010BCAM17S_7471BHGS_TPHDOS_8270FullS_8081AOCPS_GCMS-GROS_8260FullS_8082PCB

B-14-5.01108073-017A Soil 02/06/1208/10/11 12:55S_6010BCAM17S_7471BHGS_TPHDOS_GCMS-GROS_8260FullS_8082PCBS_8270Full


B-15-1.01108073-019A Soil 02/06/1208/10/11 13:40S_6010BCAM17S_GCMS-GROS_8260FullS_8081AOCPS_8082PCBS_8270FullS_TPHDOS_7471BHG

B-15-5.01108073-020A Soil 02/06/1208/10/11 13:45S_6010BCAM17S_8260FullS_7471BHGS_8082PCBS_GCMS-GRO



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_8270FullS_TPHDO


B-9-1.01108073-022A Soil 02/06/1208/10/11 15:10S_7471BHGS_8081AOCPS_8082PCBS_6010BCAM17S_8260FullS_GCMS-GROS_TPHDOS_8270Full

B-9-3.01108073-023A Soil 02/06/1208/10/11 15:15S_7471BHGS_6010BCAM17S_8260FullS_GCMS-GROS_8082PCBS_8270FullS_TPHDO


B-5-1.01108073-025A Soil 02/06/1208/10/11 16:05S_7471BHGS_TPHDOS_8081AOCPS_8082PCBS_8270FullS_6010BCAM17S_8260FullS_GCMS-GRO

B-5-5.01108073-026A Soil 02/06/1208/10/11 16:10S_7471BHG



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_8270FullS_8082PCBS_TPHDOS_8260FullS_GCMS-GROS_6010BCAM17


B-13-1.01108073-028A Soil 02/06/1208/10/11 16:25S_7471BHGS_6010BCAM17S_8260FullS_GCMS-GROS_8081AOCPS_TPHDOS_8082PCBS_8270Full

B-13-5.01108073-029A Soil 02/06/1208/10/11 16:30S_6010BCAM17S_8270FullS_8260FullS_GCMS-GROS_7471BHGS_8082PCBS_TPHDO


B-12-1.0 D1108073-031A Soil 02/06/1208/10/11 10:40S_GCMS-GROS_8260Full

Sample Note: Received only 3 pretarred voas no liner.B-5-5.0 D1108073-032A Soil 02/06/1208/10/11 16:10

S_6010BCAM17S_7471BHG



Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_8260FullS_GCMS-GROS_TPHDOS_8082PCBS_8270Full

B-1-GW1108073-033A Water 09/24/1108/10/11 9:45W_8260FullW_GCMS-GRO

B-1-GW1108073-033B Water 09/24/1108/10/11 9:45W_TPHDOSG

B-1-GW1108073-033C Water 09/24/1108/10/11 9:45W_D6010BCAM17W_D7470AHG




B-12-GWD1108073-035A Water 09/24/1108/10/11 11:00W_8260FullW_GCMS-GRO

B-12-GWD1108073-035B Water 09/24/1108/10/11 11:00W_TPHDOSG






Report Due Date:


14:15

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID


Sample Note: 4 vaos unpreservedB-9-GW1108073-037B Water 09/24/1108/10/11 16:25

W_TPHDOSGB-9-GW1108073-037C Water 09/24/1108/10/11 16:25

W_D6010BCAM17W_D7470AHG


Sample Note: For GW one voa unpreservedB-13-GW1108073-038B Water 09/24/1108/10/11 17:15






Equip BLANK1108073-040A Water 09/24/1108/10/11 16:45W_8260Full


of 260Total Page Count: 260

Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350

RE: 500 Kirkham

Torrent Laboratory, Inc. received sample(s) on August 23, 2011 for the analyses presented in the following Report.

Dear Anya Starovoytov:

Work Order No.: 1108084 Rev: 2



Date

August 26, 2011

Patti Sandrock


Date: 8/26/2011



Work Order: 1108084

CASE NARRATIVE


Note for 8260B/GCMS-GRO: Final results and PQL (Reporting Limit) have been corrected for actual mass from pre-tarred 5035 VOAs.

Analytical Comments for method S_6010B, 1108084-008 MS/MSD, QC Analytical Batch ID 406288, Note:The % recoveries for Copper and Lead are outside of laboratory control limits but are within % RPD limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.

REVISIONS:

Per client request, Lead and TPH analysis was performed on samples 006 and 009 and additional STLC and TCLP extraction and analysis was performed on samples 004, 008, 010. Due to insufficeint remaining sample mass for -004, only STLC was performed per client instruction.

Note: Extraction of 100 g sample / 2000g TCLP Fluid # 1 was performed according to Toxicity Characteristic Leaching Procedure (TCLP) which was rotated in a rotary shaker for 18 hours.

TCLP:Extraction started on 8/23/11 @4.30 PM and ended on 8/24/11 @10.30 AM

__________

Note: Extraction of 50 g sample / 500g 0.2M Sodium Citrate Solution was performed according to wet extraction procedure (WET) which was rotated in a rotary shaker for 48 hours. STLC:Extraction started on 8/23/11 @4.30 PM and ended on 8/25/[email protected] PM.

Rev 1 (8/26/11)

Report revised to revise above comment to include information regarding limited mass for TCLP analysis on sample 004.

Report revised to release data for samples 006 and 009 from "hold" status.

Rev 2 (9/7/11)


Report prepared for: Anya Starovoytov





1108084-001B-4-1.0





Copper mg/Kg6.55.00.0900SW6010B 1

Lead mg/Kg341.00.043SW6010B 1



Zinc mg/Kg355.00.59SW6010B 1


1108084-002B-4-5.0





Copper mg/Kg5.65.00.0900SW6010B 1

Lead mg/Kg121.00.043SW6010B 1



Zinc mg/Kg195.00.59SW6010B 1







1108084-004B-8-1.0







Lead mg/Kg981.00.043SW6010B 1



Zinc mg/Kg1305.00.59SW6010B 1



Lead (STLC) mg/L110.100.0500SW6010B 1







1108084-005B-8-5.0





Copper mg/Kg6.15.00.0900SW6010B 1

Lead mg/Kg131.00.043SW6010B 1



Zinc mg/Kg225.00.59SW6010B 1


1108084-006B-8-8.0


Lead mg/Kg3.81.00.043SW6010B 1







1108084-007B-2-1.0







Lead mg/Kg1201.00.043SW6010B 1



Zinc mg/Kg1205.00.59SW6010B 1









1108084-008B-2-5.0







Lead mg/Kg1301.00.043SW6010B 1



Zinc mg/Kg1305.00.59SW6010B 1



Lead (STLC) mg/L4.60.100.0500SW6010B 1

1108084-009B-2-9.0


Lead mg/Kg2.11.00.043SW6010B 1







1108084-010B-7-1.0




Copper mg/Kg6.85.00.0900SW6010B 1

Lead mg/Kg501.00.043SW6010B 1



Zinc mg/Kg1305.00.59SW6010B 1



Lead (STLC) mg/L5.70.100.0500SW6010B 1

1108084-011B-7-5.0




Lead mg/Kg4.21.00.043SW6010B 1



Zinc mg/Kg135.00.59SW6010B 1








1108084-013B-6-1.0




Lead mg/Kg2.71.00.043SW6010B 1



Zinc mg/Kg145.00.59SW6010B 1


1108084-014B-6-5.0




Lead mg/Kg1.91.00.043SW6010B 1

Nickel mg/Kg9.25.00.0590SW6010B 1


Zinc mg/Kg9.05.00.59SW6010B 1








1108084-016B-16-1.0







Lead mg/Kg411.00.043SW6010B 1



Zinc mg/Kg455.00.59SW6010B 1


1108084-017B-16-5.0






Copper mg/Kg5.65.00.0900SW6010B 1

Lead mg/Kg3.21.00.043SW6010B 1



Zinc mg/Kg185.00.59SW6010B 1







1108084-019B-7-1.0D



1108084-020B-4-GW


Chloromethane ug/L0.880.500.41SW8260B 1


1108084-021B-8-GW


Methylene Chloride ug/L0.366.10.21SW8260B 1.22

Chloroform ug/L4.90.610.36SW8260B 1.22










1108084-022B-16-GW


Arsenic (Dissolved) mg/L0.0100.0090.005SW6010B 1





1108084-023FB



1108084-024IDW





Lead mg/Kg3.01.00.043SW6010B 1



Zinc mg/Kg185.00.59SW6010B 1


1108084-025EQUIP BLANK




SAMPLE RESULTS


Northgate Environmental Management Inc.Anya Starovoytov

Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 3.9 8.9 NA1

SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.1 8.9 NA1

SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.4 8.9 NA1

SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.2 8.9 NA1

SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 2.6 8.9 NA1

SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.4 8.9 NA1

SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.3 8.9 NA1

SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 1.8 8.9 NA1

SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 0.99 8.9 NA1

SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.3 8.9 NA1

SW8260B NA 406253ug/KgNDtert-Butanol 08/15/11 18 45 NA1

SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 1.9 8.9 NA1

SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.1 8.9 NA1

SW8260B NA 406253ug/KgNDETBE 08/15/11 2.1 8.9 NA1

SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.6 8.9 NA1

SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.1 8.9 NA1

SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.0 8.9 NA1

SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.1 8.9 NA1

SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.4 8.9 NA1

SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.1 8.9 NA1

SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.3 8.9 NA1

SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.3 8.9 NA1

SW8260B NA 406253ug/KgNDTAME 08/15/11 1.8 8.9 NA1


SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 3.5 8.9 NA1

SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.0 8.9 NA1


SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 0.99 8.9 NA1

SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.0 8.9 NA1

SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.3 8.9 NA1

SW8260B NA 406253ug/KgNDToluene 08/15/11 0.87 8.9 NA1

SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.6 8.9 NA1

SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.0 8.9 NA1


SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.0 8.9 NA1



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.6 8.9 NA1

SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.77 8.9 NA1

SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 3.7 8.9 NA1

SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.76 8.9 NA1

SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.6 8.9 NA1

SW8260B NA 406253ug/KgNDo-Xylene 08/15/11 0.59 4.5 NA1

SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.68 8.9 NA1

SW8260B NA 406253ug/KgNDBromoform 08/15/11 1.7 8.9 NA1

SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.1 8.9 NA1

SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.3 8.9 NA1

SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.1 8.9 NA1


SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.0 8.9 NA1

SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.0 8.9 NA1

SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.4 8.9 NA1


SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.3 8.9 NA1


SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.5 8.9 NA1

SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.3 8.9 NA1

SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.6 8.9 NA1


SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 1.9 8.9 NA1


SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 3.8 8.9 NA1

SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.3 8.9 NA1

SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 1.9 8.9 NA1

SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.5 8.9 NA1


SW8260B NA 406253%93.1(S) Dibromofluoromethane 08/15/11 59.8 148 NA1

SW8260B NA 406253%83.6(S) Toluene-d8 08/15/11 55.2 133 NA1

SW8260B NA 406253%97.0(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/15/11 406267mg/KgNDAntimony 08/16/11 0.20 5.0 33891

SW6010B 8/15/11 406267mg/Kg2.4Arsenic 08/16/11 0.28 1.7 33891

SW6010B 8/15/11 406267mg/Kg67Barium 08/16/11 1 5.0 33891

SW6010B 8/15/11 406267mg/KgNDBeryllium 08/16/11 0.0840 2.0 33891

SW6010B 8/15/11 406267mg/KgNDCadmium 08/16/11 0.0590 1.0 33891

SW6010B 8/15/11 406267mg/Kg31Chromium 08/16/11 0.0590 5.0 33891

SW6010B 8/15/11 406267mg/KgNDCobalt 08/16/11 0.14 5.0 33891

SW6010B 8/15/11 406267mg/Kg6.5Copper 08/16/11 0.0900 5.0 33891

SW6010B 8/15/11 406267mg/Kg34Lead 08/16/11 0.043 1.0 33891

SW6010B 8/15/11 406267mg/KgNDMolybdenum 08/16/11 0.0590 5.0 33891

SW6010B 8/15/11 406267mg/Kg19Nickel 08/16/11 0.0590 5.0 33891

SW6010B 8/15/11 406267mg/KgNDSelenium 08/16/11 0.29 5.0 33891

SW6010B 8/15/11 406267mg/KgNDSilver 08/16/11 1.0 1.0 33891

SW6010B 8/15/11 406267mg/KgNDThallium 08/16/11 0.12 5.0 33891

SW6010B 8/15/11 406267mg/Kg23Vanadium 08/16/11 0.12 5.0 33891

SW6010B 8/15/11 406267mg/Kg35Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 0.44 2.0 34201

SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 0.40 2.0 34201

SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 0.36 2.0 34201

SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 0.49 2.0 34201

SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 1.1 2.0 34201

SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 0.44 2.0 34201

SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 0.32 2.0 34201

SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 0.42 2.0 34201

SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 0.36 2.0 34201

SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 0.59 2.0 34201

SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201

SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 0.43 2.0 34201

SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 0.57 2.0 34201

SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201

SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 1.5 2.0 34201

SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201

SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 1.0 2.0 34201

SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 0.49 2.0 34201

SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 0.62 5.0 34201

SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 0.40 2.0 34201

SW8081A 8/18/11 406333ug/KgNDChlordane 08/18/11 10 20 34201

SW8081A 8/18/11 406333ug/KgNDToxaphene 08/18/11 10 100 34201

SW8081A 8/18/11 406333%98.2TCMX (S) 08/18/11 52.5 139 34201

SW8081A 8/18/11 406333%88.6DCBP (S) 08/18/11 50.2 139 34201


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8082 8/18/11 406326mg/KgNDAroclor1016 08/18/11 0.0230 0.10 34191







SW8082 8/18/11 406326%95.6TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%104DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 0.660 0.653 33851

SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 0.110 0.330 33851

SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 0.123 0.330 33851

SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 0.129 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 0.0683 0.330 33851

SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 0.129 0.330 33851

SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 0.0733 0.330 33851


SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 0.104 0.330 33851


SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 0.116 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 0.0683 0.330 33851

SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 0.139 0.330 33851

SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 0.0931 0.330 33851

SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 0.0465 0.330 33851

SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 0.0528 0.330 33851

SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 0.0574 0.653 33851

SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 0.0525 0.653 33851

SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 0.133 6.59 33851

SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 5.59 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 0.0584 0.330 33851

SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 0.104 0.330 33851

SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 0.0733 0.330 33851


SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 0.0901 0.330 33851

SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 0.0990 0.330 33851

SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 0.0653 0.330 33851

SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 0.102 0.330 33851

SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 0.0792 0.330 33851


SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 0.0277 0.330 33851

SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 0.0950 0.330 33851


SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 0.0594 3.27 33851

SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 0.0693 0.330 33851

SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 0.118 0.330 33851


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 0.106 0.330 33851

SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 0.0851 0.330 33851

SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 0.0267 0.330 33851



SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 0.0960 0.330 33851

SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 0.0297 3.27 33851


SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 0.0782 0.330 33851


SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 0.119 0.330 33851


SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 0.117 0.330 33851

SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 0.0990 0.330 33851

SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 0.0802 0.330 33851


SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 0.0663 0.330 33851

SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 0.0663 0.330 33851

SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 0.109 0.330 33851

SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 0.0812 3.27 33851

SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 0.101 0.330 33851

SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 0.102 3.27 33851

SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 0.142 0.330 33851

SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 0.132 0.330 33851

SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 0.132 0.330 33851

SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 0.108 1.68 33851

SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 0.132 0.653 33851

SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 0.374 3.27 33851

SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 0.147 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 0.0891 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 0.149 0.330 33851

SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 0.152 0.330 33851

SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 0.176 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 0.0832 0.330 33851

SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 0.138 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 0.133 0.330 33851


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:15

1204.22

500 Kirkham

B-4-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 0.169 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 0.135 0.330 33851

SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 0.131 0.330 33851

SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 0.151 0.330 33851

SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 0.150 0.330 33851


SW8270C 8/15/11 406316%45.52,4,6-Tribromophenol (S) 08/16/11 19 122 33851

SW8270C 8/15/11 406316%51.82-Fluorobiphenyl (S) 08/16/11 30 115 33851

SW8270C 8/15/11 406316%56.92-Fluorophenol (S) 08/16/11 25 121 33851

SW8270C 8/15/11 406316%51.3Nitrobenzene-d5 (S) 08/16/11 23 120 33851

SW8270C 8/15/11 406316%61.5Phenol-d6 (S) 08/16/11 24 113 33851

SW8270C 8/15/11 406316%48.7p-Terphenyl-d14 (S) 08/16/11 18 137 33851


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH NA 406253ug/KgNDTPH(Gasoline) 08/15/11 15 89 NA1

8260TPH NA 406253%96.4(S) 4-Bromofluorobenzene 08/15/11 43.9 127 NA1


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 0.759 2.0 34181

SW8015B(M) 8/18/11 406325mg/Kg12TPH as Motor Oil 08/18/11 1.65 4.0 34181

SW8015B(M) 8/18/11 406325mg/Kg114Pentacosane (S) 08/18/11 59.7 129 34181


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:20

1204.22

500 Kirkham

B-4-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:20

1204.22

500 Kirkham

B-4-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/15/11 406267mg/Kg1.9Arsenic 08/16/11 0.28 1.7 33891

SW6010B 8/15/11 406267mg/Kg65Barium 08/16/11 1 5.0 33891





SW6010B 8/15/11 406267mg/Kg5.6Copper 08/16/11 0.0900 5.0 33891

SW6010B 8/15/11 406267mg/Kg12Lead 08/16/11 0.043 1.0 33891


SW6010B 8/15/11 406267mg/Kg12Nickel 08/16/11 0.0590 5.0 33891





SW6010B 8/15/11 406267mg/Kg19Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%90.6TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%83.1DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:20

1204.22

500 Kirkham

B-4-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:20

1204.22

500 Kirkham

B-4-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8270C 8/15/11 406316%66.0Phenol-d6 (S) 08/16/11 24 113 33851



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW8015B(M) 8/18/11 406325mg/KgNDTPH as Motor Oil 08/18/11 1.65 4.0 34181



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/25/11 406447mg/L11Lead (STLC) 08/26/11 0.0500 0.10 34961


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/15/11 406267mg/Kg2.9Arsenic 08/16/11 0.28 1.7 33891

SW6010B 8/15/11 406267mg/Kg76Barium 08/16/11 1 5.0 33891




SW6010B 8/15/11 406267mg/Kg6.3Cobalt 08/16/11 0.14 5.0 33891

SW6010B 8/15/11 406267mg/Kg55Copper 08/16/11 0.0900 5.0 33891

SW6010B 8/15/11 406267mg/Kg98Lead 08/16/11 0.043 1.0 33891


SW6010B 8/15/11 406267mg/Kg19Nickel 08/16/11 0.0590 5.0 33891





SW6010B 8/15/11 406267mg/Kg130Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406270mg/Kg0.17Mercury 08/16/11 0.01 0.10 33931


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201



SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201


SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201







SW8081A 8/18/11 406333%99.2TCMX (S) 08/18/11 52.5 139 34201

SW8081A 8/18/11 406333%94.3DCBP (S) 08/18/11 50.2 139 34201


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%93.4TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%97.6DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 100 99.0 338510







SW8270C 8/15/11 406316mg/KgND1,4-Dichlorobenzene 08/16/11 10.1 999 338510











SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 20.1 999 338510

SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 848 50.0 338510














SW8270C 8/15/11 406316mg/KgND2-Chloronaphthalene 08/16/11 9.00 495 338510



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 17.9 50.0 338510







SW8270C 8/15/11 406316mg/KgND2,4-Dinitrophenol 08/16/11 4.50 495 338510













SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 12.3 495 338510


SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 15.5 495 338510




SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 16.4 255 338510


SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 56.7 495 338510








SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 8:55

1204.22

500 Kirkham

B-8-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 20.9 50.0 338510








SW8270C 8/15/11 406316S,D %0.0002,4,6-Tribromophenol (S) 08/16/11 19 122 338510

SW8270C 8/15/11 406316S,D %0.0002-Fluorobiphenyl (S) 08/16/11 30 115 338510

SW8270C 8/15/11 406316S,D %0.0002-Fluorophenol (S) 08/16/11 25 121 338510

SW8270C 8/15/11 406316S,D %0.000Nitrobenzene-d5 (S) 08/16/11 23 120 338510

SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510

SW8270C 8/15/11 406316S,D %0.000p-Terphenyl-d14 (S) 08/16/11 18 137 338510


NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod
































SW8260B NA 406253%106(S) 4-Bromofluorobenzene 08/15/11 55.8 141 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/15/11 406267mg/Kg1.8Arsenic 08/16/11 0.28 1.7 33891

SW6010B 8/15/11 406267mg/Kg89Barium 08/16/11 1 5.0 33891





SW6010B 8/15/11 406267mg/Kg6.1Copper 08/16/11 0.0900 5.0 33891

SW6010B 8/15/11 406267mg/Kg13Lead 08/16/11 0.043 1.0 33891


SW6010B 8/15/11 406267mg/Kg16Nickel 08/16/11 0.0590 5.0 33891





SW6010B 8/15/11 406267mg/Kg22Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%81.8TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%78.5DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDPyridine 08/16/11 250 248 338525

SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 41.6 125 338525

SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 46.5 125 338525

SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 48.8 125 338525

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 25.9 125 338525

SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 48.8 125 338525



SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 39.4 125 338525


SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 43.9 125 338525

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 25.9 125 338525

SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 52.5 125 338525

SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 35.3 125 338525

SW8270C 8/15/11 406316mg/KgNDHexachloroethane 08/16/11 17.6 125 338525

SW8270C 8/15/11 406316mg/KgNDNitrobenzene 08/16/11 20.0 125 338525

SW8270C 8/15/11 406316mg/KgNDIsophorone 08/16/11 21.8 248 338525

SW8270C 8/15/11 406316mg/KgND2-Nitrophenol 08/16/11 19.9 248 338525


SW8270C 8/15/11 406316mg/KgNDBenzoic Acid 08/16/11 2120 125 338525

SW8270C 8/15/11 406316mg/KgNDBis(2-Chloroethoxy)methane 08/16/11 22.1 125 338525

SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 39.4 125 338525

SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 27.8 125 338525


SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 34.1 125 338525

SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 37.5 125 338525

SW8270C 8/15/11 406316mg/KgNDHexachloro-1,3-butadiene 08/16/11 24.8 125 338525

SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 38.6 125 338525

SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 30.0 125 338525


SW8270C 8/15/11 406316mg/KgNDHexachlorocyclopentadiene 08/16/11 10.5 125 338525

SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 36.0 125 338525



SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 26.3 125 338525


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 44.6 125 338525

SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 40.0 125 338525

SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 32.3 125 338525

SW8270C 8/15/11 406316mg/KgND2,6-Dinitrotoluene 08/16/11 10.1 125 338525



SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 36.4 125 338525



SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 29.6 125 338525


SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 45.0 125 338525


SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 44.3 125 338525

SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 37.5 125 338525

SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 30.4 125 338525


SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 25.1 125 338525

SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 25.1 125 338525

SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 41.3 125 338525


SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 38.3 125 338525


SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 53.6 125 338525

SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 50.2 125 338525

SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 50.2 125 338525


SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 50.1 248 338525

SW8270C 8/15/11 406316mg/KgNDBenzidine 08/16/11 142 1240 338525

SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 55.6 125 338525

SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 33.8 125 338525

SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 56.6 125 338525

SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 57.8 125 338525

SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 66.8 125 338525

SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 31.5 125 338525


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:00

1204.22

500 Kirkham

B-8-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 52.1 125 338525

SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 50.3 125 338525

SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 64.1 125 338525

SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 51.0 125 338525

SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 49.5 125 338525

SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 57.4 125 338525

SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 57.0 125 338525






SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338525



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/18/11 406325mg/KgNDTPH as Diesel 08/18/11 7.36 19 34184

SW8015B(M) 8/18/11 406325mg/Kg550TPH as Motor Oil 08/18/11 16.0 38 34184

SW8015B(M) 8/18/11 406325mg/Kg91.4Pentacosane (S) 08/18/11 59.7 129 34184


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:05

1204.22

500 Kirkham

B-8-8.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/24/11 406410mg/Kg3.8Lead 08/24/11 0.043 1.0 34791


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/15/11 406267mg/Kg5.3Arsenic 08/16/11 0.28 1.7 33891

SW6010B 8/15/11 406267mg/Kg100Barium 08/16/11 1 5.0 33891




SW6010B 8/15/11 406267mg/Kg6.9Cobalt 08/16/11 0.14 5.0 33891

SW6010B 8/15/11 406267mg/Kg44Copper 08/16/11 0.0900 5.0 33891

SW6010B 8/15/11 406267mg/Kg120Lead 08/16/11 0.043 1.0 33891


SW6010B 8/15/11 406267mg/Kg26Nickel 08/16/11 0.0590 5.0 33891





SW6010B 8/15/11 406267mg/Kg120Zinc 08/16/11 0.59 5.0 33891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406270mg/Kg0.31Mercury 08/16/11 0.01 0.10 33931


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 4.4 20 342010

SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 4.0 20 342010

SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 3.6 20 342010

SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 4.9 20 342010

SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 11 20 342010

SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 4.4 20 342010

SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 3.2 20 342010

SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 4.2 20 342010

SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 3.6 20 342010

SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 5.9 20 342010

SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 4.8 20 342010

SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 4.3 20 342010

SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 5.7 20 342010

SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 4.7 20 342010

SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 15 20 342010

SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 8.1 20 342010

SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 10 20 342010

SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 4.9 20 342010

SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 6.2 50 342010

SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 4.0 20 342010



SW8081A 8/18/11 406333%91.5TCMX (S) 08/18/11 52.5 139 342010

SW8081A 8/18/11 406333%90.0DCBP (S) 08/18/11 50.2 139 342010



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%88.5TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%94.6DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 33.3 100 338520

SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 37.2 100 338520

SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 39.0 100 338520

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 20.7 100 338520

SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 39.0 100 338520



SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 31.5 100 338520


SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 35.1 100 338520

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 20.7 100 338520

SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 42.0 100 338520

SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 28.2 100 338520









SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 22.2 100 338520


SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 27.3 100 338520

SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 30.0 100 338520


SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 30.9 100 338520









SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 35.7 100 338520


SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 25.8 100 338520




SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 29.1 100 338520



SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 23.7 100 338520




SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 35.4 100 338520

SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 30.0 100 338520

SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 24.3 100 338520


SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 20.1 100 338520

SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 20.1 100 338520

SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 33.0 100 338520


SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 30.6 100 338520


SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 42.9 100 338520

SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 40.1 100 338520

SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 40.1 100 338520


SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 40.1 198 338520


SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 44.5 100 338520

SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 27.0 100 338520

SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 45.3 100 338520

SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 46.2 100 338520

SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 53.4 100 338520

SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 25.2 100 338520


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:15

1204.22

500 Kirkham

B-2-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 41.7 100 338520

SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 40.2 100 338520

SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 51.3 100 338520

SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 40.8 100 338520

SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 39.6 100 338520

SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 45.9 100 338520

SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 45.6 100 338520






SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338520



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-2-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-2-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/25/11 406447mg/L4.6Lead (STLC) 08/26/11 0.0500 0.10 34961


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/24/11 406421mg/LNDLead (TCLP) 08/25/11 0.05 0.10 34891


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/16/11 406288mg/Kg6.6Arsenic 08/17/11 0.28 1.7 34051

SW6010B 8/16/11 406288mg/Kg190Barium 08/17/11 1 5.0 34051




SW6010B 8/16/11 406288mg/Kg12Cobalt 08/17/11 0.14 5.0 34051

SW6010B 8/16/11 406288mg/Kg40Copper 08/17/11 0.0900 5.0 34051

SW6010B 8/16/11 406288mg/Kg130Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg21Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg130Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406270mg/Kg0.24Mercury 08/16/11 0.01 0.10 33931


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-2-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%87.0TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%100DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-2-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-2-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod













SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:25

1204.22

500 Kirkham

B-2-9.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/24/11 406410mg/Kg2.1Lead 08/24/11 0.043 1.0 34791


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406253ug/KgNDDichlorodifluoromethane 08/15/11 4.5 10 NA1

SW8260B NA 406253ug/KgNDChloromethane 08/15/11 4.7 10 NA1

SW8260B NA 406253ug/KgNDVinyl Chloride 08/15/11 2.7 10 NA1

SW8260B NA 406253ug/KgNDBromomethane 08/15/11 4.8 10 NA1

SW8260B NA 406253ug/KgNDTrichlorofluoromethane 08/15/11 3.0 10 NA1

SW8260B NA 406253ug/KgND1,1-Dichloroethene 08/15/11 1.6 10 NA1

SW8260B NA 406253ug/KgNDFreon 113 08/15/11 3.8 10 NA1

SW8260B NA 406253ug/KgNDMethylene Chloride 08/15/11 2.0 10 NA1

SW8260B NA 406253ug/KgNDtrans-1,2-Dichloroethene 08/15/11 1.1 10 NA1

SW8260B NA 406253ug/KgNDMTBE 08/15/11 2.7 10 NA1


SW8260B NA 406253ug/KgNDDiisopropyl ether (DIPE) 08/15/11 2.3 10 NA1

SW8260B NA 406253ug/KgND1,1-Dichloroethane 08/15/11 1.3 10 NA1

SW8260B NA 406253ug/KgNDETBE 08/15/11 2.5 10 NA1

SW8260B NA 406253ug/KgNDcis-1,2-Dichloroethene 08/15/11 1.8 10 NA1

SW8260B NA 406253ug/KgND2,2-Dichloropropane 08/15/11 1.3 10 NA1

SW8260B NA 406253ug/KgNDBromochloromethane 08/15/11 2.4 10 NA1

SW8260B NA 406253ug/KgNDChloroform 08/15/11 1.3 10 NA1

SW8260B NA 406253ug/KgNDCarbon Tetrachloride 08/15/11 1.7 10 NA1

SW8260B NA 406253ug/KgND1,1,1-Trichloroethane 08/15/11 1.3 10 NA1

SW8260B NA 406253ug/KgND1,1-Dichloropropene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgNDBenzene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgNDTAME 08/15/11 2.1 10 NA1

SW8260B NA 406253ug/KgND1,2-Dichloroethane 08/15/11 2.0 10 NA1

SW8260B NA 406253ug/KgNDTrichloroethylene 08/15/11 4.0 10 NA1

SW8260B NA 406253ug/KgNDDibromomethane 08/15/11 2.3 10 NA1


SW8260B NA 406253ug/KgNDBromodichloromethane 08/15/11 1.2 10 NA1

SW8260B NA 406253ug/KgND2-Chloroethyl vinyl ether 08/15/11 4.6 10 NA1

SW8260B NA 406253ug/KgNDcis-1,3-Dichloropropene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgNDToluene 08/15/11 1.0 10 NA1

SW8260B NA 406253ug/KgNDTetrachloroethylene 08/15/11 1.9 10 NA1

SW8260B NA 406253ug/KgNDtrans-1,3-Dichloropropene 08/15/11 1.2 10 NA1

SW8260B NA 406253ug/KgND1,1,2-Trichloroethane 08/15/11 1.9 10 NA1

SW8260B NA 406253ug/KgNDDibromochloromethane 08/15/11 1.2 10 NA1



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406253ug/KgND1,2-Dibromoethane 08/15/11 1.8 10 NA1

SW8260B NA 406253ug/KgNDEthyl Benzene 08/15/11 0.89 10 NA1

SW8260B NA 406253ug/KgNDChlorobenzene 08/15/11 4.3 10 NA1

SW8260B NA 406253ug/KgND1,1,1,2-Tetrachloroethane 08/15/11 0.88 10 NA1

SW8260B NA 406253ug/KgNDm,p-Xylene 08/15/11 1.9 10 NA1


SW8260B NA 406253ug/KgNDStyrene 08/15/11 0.79 10 NA1

SW8260B NA 406253ug/KgNDBromoform 08/15/11 2.0 10 NA1

SW8260B NA 406253ug/KgNDIsopropyl Benzene 08/15/11 1.3 10 NA1

SW8260B NA 406253ug/KgNDn-Propylbenzene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgNDBromobenzene 08/15/11 1.2 10 NA1

SW8260B NA 406253ug/KgND1,1,2,2-Tetrachloroethane 08/15/11 3.1 10 NA1

SW8260B NA 406253ug/KgND1,3,5-Trimethylbenzene 08/15/11 1.2 10 NA1

SW8260B NA 406253ug/KgND1,2,3-Trichloropropane 08/15/11 3.4 10 NA1

SW8260B NA 406253ug/KgND4-Chlorotoluene 08/15/11 1.6 10 NA1

SW8260B NA 406253ug/KgND2-Chlorotoluene 08/15/11 1.6 10 NA1

SW8260B NA 406253ug/KgNDtert-Butylbenzene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgND1,2,4-Trimethylbenzene 08/15/11 1.1 10 NA1

SW8260B NA 406253ug/KgNDsec-Butyl Benzene 08/15/11 1.7 10 NA1

SW8260B NA 406253ug/KgNDp-Isopropyltoluene 08/15/11 1.5 10 NA1

SW8260B NA 406253ug/KgND1,3-Dichlorobenzene 08/15/11 1.8 10 NA1


SW8260B NA 406253ug/KgNDn-Butylbenzene 08/15/11 2.3 10 NA1


SW8260B NA 406253ug/KgND1,2-Dibromo-3-Chloropropane 08/15/11 4.4 10 NA1

SW8260B NA 406253ug/KgNDHexachlorobutadiene 08/15/11 2.6 10 NA1

SW8260B NA 406253ug/KgND1,2,4-Trichlorobenzene 08/15/11 2.2 10 NA1

SW8260B NA 406253ug/KgNDNaphthalene 08/15/11 2.9 10 NA1

SW8260B NA 406253ug/KgND1,2,3-Trichlorobenzene 08/15/11 3.0 10 NA1





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/25/11 406447mg/L5.7Lead (STLC) 08/26/11 0.0500 0.10 34961


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/16/11 406288mg/KgNDArsenic 08/17/11 0.28 1.7 34051

SW6010B 8/16/11 406288mg/Kg53Barium 08/17/11 1 5.0 34051





SW6010B 8/16/11 406288mg/Kg6.8Copper 08/17/11 0.0900 5.0 34051

SW6010B 8/16/11 406288mg/Kg50Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg14Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg130Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7471A 8/15/11 406270mg/Kg0.12Mercury 08/16/11 0.01 0.10 33931


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201



SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201


SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201







SW8081A 8/18/11 406333%85.0TCMX (S) 08/18/11 52.5 139 34201

SW8081A 8/18/11 406333%58.9DCBP (S) 08/18/11 50.2 139 34201



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%87.2TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%87.9DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod













SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW8015B(M) 8/18/11 406325mg/Kg9.2TPH as Motor Oil 08/18/11 1.65 4.0 34181



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:35

1204.22

500 Kirkham

B-7-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:35

1204.22

500 Kirkham

B-7-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW6010B 8/16/11 406288mg/Kg58Barium 08/17/11 1 5.0 34051





SW6010B 8/16/11 406288mg/KgNDCopper 08/17/11 0.0900 5.0 34051

SW6010B 8/16/11 406288mg/Kg4.2Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg12Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg13Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%67.8TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326S %52.5DCBP (S) 08/18/11 55.1 113 34191

Surrogate recovery of DCBP is bias low possibly due to matrix effects; recovery of second surrogate supports data quality.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:35

1204.22

500 Kirkham

B-7-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:35

1204.22

500 Kirkham

B-7-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8270C 8/15/11 406316%77.2Phenol-d6 (S) 08/16/11 24 113 33851



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW6010B 8/16/11 406288mg/Kg42Barium 08/17/11 1 5.0 34051






SW6010B 8/16/11 406288mg/Kg2.7Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg13Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg14Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 0.48 2.0 34201



SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 0.47 2.0 34201


SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 0.81 2.0 34201







SW8081A 8/18/11 406333%87.6TCMX (S) 08/18/11 52.5 139 34201

SW8081A 8/18/11 406333%70.0DCBP (S) 08/18/11 50.2 139 34201


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%87.9TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%87.7DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:55

1204.22

500 Kirkham

B-6-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8270C 8/15/11 406316%80.5Phenol-d6 (S) 08/16/11 24 113 33851



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 11:00

1204.22

500 Kirkham

B-6-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 11:00

1204.22

500 Kirkham

B-6-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW6010B 8/16/11 406288mg/Kg50Barium 08/17/11 1 5.0 34051






SW6010B 8/16/11 406288mg/Kg1.9Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg9.2Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg9.0Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%133TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%79.2DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 11:00

1204.22

500 Kirkham

B-6-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 11:00

1204.22

500 Kirkham

B-6-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8270C 8/15/11 406316%71.5Phenol-d6 (S) 08/16/11 24 113 33851



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/16/11 406288mg/Kg2.5Arsenic 08/17/11 0.28 1.7 34051

SW6010B 8/16/11 406288mg/Kg58Barium 08/17/11 1 5.0 34051




SW6010B 8/16/11 406288mg/Kg5.1Cobalt 08/17/11 0.14 5.0 34051

SW6010B 8/16/11 406288mg/Kg12Copper 08/17/11 0.0900 5.0 34051

SW6010B 8/16/11 406288mg/Kg41Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg19Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg45Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8081A 8/18/11 406333ug/KgNDalpha-BHC 08/18/11 8.8 40 342020

SW8081A 8/18/11 406333ug/KgNDgamma-BHC 08/18/11 7.9 40 342020

SW8081A 8/18/11 406333ug/KgNDbeta-BHC 08/18/11 7.3 40 342020

SW8081A 8/18/11 406333ug/KgNDdelta-BHC 08/18/11 9.8 40 342020

SW8081A 8/18/11 406333ug/KgNDHeptachlor 08/18/11 22 40 342020

SW8081A 8/18/11 406333ug/KgNDAldrin 08/18/11 8.8 40 342020

SW8081A 8/18/11 406333ug/KgNDHeptachlor epoxide 08/18/11 6.3 40 342020

SW8081A 8/18/11 406333ug/KgNDgamma-Chlordane 08/18/11 8.4 40 342020

SW8081A 8/18/11 406333ug/KgNDalpha-Chlordane 08/18/11 7.2 40 342020

SW8081A 8/18/11 406333ug/KgNDEndosulfan I 08/18/11 12 40 342020

SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 9.5 40 342020

SW8081A 8/18/11 406333ug/KgNDDieldrin 08/18/11 8.5 40 342020

SW8081A 8/18/11 406333ug/KgNDEndrin 08/18/11 11 40 342020

SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 9.4 40 342020

SW8081A 8/18/11 406333ug/KgNDEndosulfan II 08/18/11 31 40 342020

SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 16 40 342020

SW8081A 8/18/11 406333ug/KgNDEndrin aldehyde 08/18/11 21 40 342020

SW8081A 8/18/11 406333ug/KgNDEndosulfan sulfate 08/18/11 9.8 40 342020

SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 12 100 342020

SW8081A 8/18/11 406333ug/KgNDEndrin Ketone 08/18/11 8.0 40 342020



SW8081A 8/18/11 406333%112TCMX (S) 08/18/11 52.5 139 342020

SW8081A 8/18/11 406333%107DCBP (S) 08/18/11 50.2 139 342020



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%93.6TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%99.6DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW8270C 8/15/11 406316mg/KgNDN-Nitrosdimethylamine 08/16/11 167 500 338510

SW8270C 8/15/11 406316mg/KgNDAniline 08/16/11 186 500 338510

SW8270C 8/15/11 406316mg/KgNDPhenol 08/16/11 195 500 338510

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroethyl) ether 08/16/11 104 500 338510

SW8270C 8/15/11 406316mg/KgND2-Chlorophenol 08/16/11 195 500 338510

SW8270C 8/15/11 406316mg/KgND1,3-Dichlorobenzene 08/16/11 111 500 338510


SW8270C 8/15/11 406316mg/KgNDBenzyl Alcohol 08/16/11 158 500 338510


SW8270C 8/15/11 406316mg/KgND2-Methylphenol (o-Cresol) 08/16/11 176 500 338510

SW8270C 8/15/11 406316mg/KgNDBis(2-chloroisopropyl)ether 08/16/11 104 500 338510

SW8270C 8/15/11 406316mg/KgND3-/4-Methylphenol (p-/m-Cresol) 08/16/11 210 500 338510

SW8270C 8/15/11 406316mg/KgNDN-nitroso-di-n-propylamine 08/16/11 141 500 338510





SW8270C 8/15/11 406316mg/KgND2,4-Dimethylphenol 08/16/11 201 9990 338510



SW8270C 8/15/11 406316mg/KgND2,4-Dichlorophenol 08/16/11 158 500 338510

SW8270C 8/15/11 406316mg/KgND1,2,4-Trichlorobenzene 08/16/11 111 500 338510

SW8270C 8/15/11 406316mg/KgND2,6-Dichlorophenol 08/16/11 158 500 338510

SW8270C 8/15/11 406316mg/KgNDNaphthalene 08/16/11 137 500 338510

SW8270C 8/15/11 406316mg/KgND4-Chloroaniline 08/16/11 150 500 338510


SW8270C 8/15/11 406316mg/KgND4-Chloro-3-methylphenol 08/16/11 155 500 338510

SW8270C 8/15/11 406316mg/KgND2-Methylnaphthalene 08/16/11 120 500 338510

SW8270C 8/15/11 406316mg/KgND1-Methylnaphthalene 08/16/11 120 500 338510


SW8270C 8/15/11 406316mg/KgND2,4,6-Trichlorophenol 08/16/11 144 500 338510

SW8270C 8/15/11 406316mg/KgND2,4,5-Trichlorophenol 08/16/11 183 500 338510


SW8270C 8/15/11 406316mg/KgND2-Nitroaniline 08/16/11 105 500 338510


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDimethyl phthalate 08/16/11 179 500 338510

SW8270C 8/15/11 406316mg/KgND1,3-Dinitrobenzene 08/16/11 160 500 338510

SW8270C 8/15/11 406316mg/KgNDAcenaphthylene 08/16/11 129 500 338510




SW8270C 8/15/11 406316mg/KgNDAcenaphthene 08/16/11 146 500 338510


SW8270C 8/15/11 406316mg/KgND4-Nitrophenol 08/16/11 101 500 338510

SW8270C 8/15/11 406316mg/KgNDDibenzofuran 08/16/11 119 500 338510


SW8270C 8/15/11 406316mg/KgND2,3,5,6-Tetrachlorophenol 08/16/11 180 500 338510

SW8270C 8/15/11 406316mg/KgND2,3,4,6-Tetrachlorophenol 08/16/11 180 500 338510

SW8270C 8/15/11 406316mg/KgNDDiethylphthalate 08/16/11 177 500 338510

SW8270C 8/15/11 406316mg/KgNDFluorene 08/16/11 150 500 338510

SW8270C 8/15/11 406316mg/KgND4-Chlorophenyl phenyl ether 08/16/11 122 500 338510


SW8270C 8/15/11 406316mg/KgND4,6-Dinitro-2-methylphenol 08/16/11 101 500 338510

SW8270C 8/15/11 406316mg/KgNDDiphenylamine 08/16/11 101 500 338510

SW8270C 8/15/11 406316mg/KgNDAzobenzene 08/16/11 165 500 338510

SW8270C 8/15/11 406316mg/KgND4-Bromophenyl phenyl ether 08/16/11 123 4950 338510

SW8270C 8/15/11 406316mg/KgNDHexachlorobenzene 08/16/11 153 500 338510

SW8270C 8/15/11 406316mg/KgNDPentachlorophenol 08/16/11 155 4950 338510

SW8270C 8/15/11 406316mg/KgNDPhenanthrene 08/16/11 215 500 338510

SW8270C 8/15/11 406316mg/KgNDAnthracene 08/16/11 201 500 338510

SW8270C 8/15/11 406316mg/KgNDCarbazole 08/16/11 201 500 338510

SW8270C 8/15/11 406316mg/KgNDDi-n-butylphthalate 08/16/11 164 2550 338510

SW8270C 8/15/11 406316mg/KgNDFluoranthene 08/16/11 201 990 338510


SW8270C 8/15/11 406316mg/KgNDPyrene 08/16/11 223 500 338510

SW8270C 8/15/11 406316mg/KgNDBenzyl butyl phthalate 08/16/11 135 500 338510

SW8270C 8/15/11 406316mg/KgNDBenz[a]anthracene 08/16/11 227 500 338510

SW8270C 8/15/11 406316mg/KgND3,3'-Dichlorobenzidine 08/16/11 231 500 338510

SW8270C 8/15/11 406316mg/KgNDChrysene 08/16/11 267 500 338510

SW8270C 8/15/11 406316mg/KgNDBis(2-Ethylhexyl)phthalate 08/16/11 126 500 338510


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:05

1204.22

500 Kirkham

B-16-1.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8270C 8/15/11 406316mg/KgNDDi-n-octyl phthalate 08/16/11 209 500 338510

SW8270C 8/15/11 406316mg/KgNDBenzo[b]fluoranthene 08/16/11 201 500 338510

SW8270C 8/15/11 406316mg/KgNDBenzo[k]fluoranthene 08/16/11 257 500 338510

SW8270C 8/15/11 406316mg/KgNDBenzo[a]pyrene 08/16/11 204 500 338510

SW8270C 8/15/11 406316mg/KgNDIndeno[1,2,3-cd]pyrene 08/16/11 198 500 338510

SW8270C 8/15/11 406316mg/KgNDDibenz[a,h]anthracene 08/16/11 230 500 338510

SW8270C 8/15/11 406316mg/KgNDBenzo[g,h,i]perylene 08/16/11 228 500 338510






SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:10

1204.22

500 Kirkham

B-16-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:10

1204.22

500 Kirkham

B-16-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/16/11 406288mg/Kg2.0Arsenic 08/17/11 0.28 1.7 34051

SW6010B 8/16/11 406288mg/Kg50Barium 08/17/11 1 5.0 34051




SW6010B 8/16/11 406288mg/Kg6.9Cobalt 08/17/11 0.14 5.0 34051

SW6010B 8/16/11 406288mg/Kg5.6Copper 08/17/11 0.0900 5.0 34051

SW6010B 8/16/11 406288mg/Kg3.2Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg29Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg18Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod








SW8082 8/18/11 406326%81.8TCMX (S) 08/18/11 50.4 136 34191

SW8082 8/18/11 406326%83.2DCBP (S) 08/18/11 55.1 113 34191


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:10

1204.22

500 Kirkham

B-16-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:10

1204.22

500 Kirkham

B-16-5.0

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod













SW8270C 8/15/11 406316S,D %0.000Phenol-d6 (S) 08/16/11 24 113 338510



NOTE:


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 10:30

1204.22

500 Kirkham

B-7-1.0D

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-4-GW

GroundwaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.41 0.50 NA1

SW8260B NA 406300ug/L0.88Chloromethane 08/16/11 0.41 0.50 NA1

SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.37 0.50 NA1

SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.37 0.50 NA1

SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.34 0.50 NA1

SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.29 0.50 NA1

SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.38 0.50 NA1

SW8260B NA 406300ug/LNDMethylene Chloride 08/16/11 0.18 5.0 NA1

SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.31 0.50 NA1

SW8260B NA 406300ug/LNDMTBE 08/16/11 0.38 0.50 NA1

SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.5 5.0 NA1

SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.36 0.50 NA1

SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.28 0.50 NA1

SW8260B NA 406300ug/LNDETBE 08/16/11 0.40 0.50 NA1

SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.33 0.50 NA1

SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.37 0.50 NA1

SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.34 0.50 NA1

SW8260B NA 406300ug/LNDChloroform 08/16/11 0.29 0.50 NA1

SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.26 0.50 NA1

SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.32 0.50 NA1

SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.40 0.50 NA1

SW8260B NA 406300ug/LNDBenzene 08/16/11 0.33 0.50 NA1

SW8260B NA 406300ug/LNDTAME 08/16/11 0.32 0.50 NA1


SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.38 0.50 NA1

SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.21 0.50 NA1


SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.23 0.50 NA1

SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.30 0.50 NA1

SW8260B NA 406300ug/LNDToluene 08/16/11 0.19 0.50 NA1

SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.15 0.50 NA1

SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.20 0.50 NA1


SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.21 0.50 NA1


SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.19 0.50 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-4-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.14 0.50 NA1

SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.15 0.50 NA1

SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.10 0.50 NA1

SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.20 1.0 NA1

SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.13 0.50 NA1

SW8260B NA 406300ug/LNDStyrene 08/16/11 0.20 0.50 NA1

SW8260B NA 406300ug/LNDBromoform 08/16/11 0.45 1.0 NA1

SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.28 0.50 NA1

SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.39 0.50 NA1


SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.30 0.50 NA1

SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.33 0.50 NA1

SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.20 0.50 NA1


SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.29 0.50 NA1

SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.59 1.0 NA1


SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.24 0.50 NA1

SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.25 0.50 NA1

SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.31 0.50 NA1


SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.32 0.50 NA1


SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.45 1.0 NA1

SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.22 0.50 NA1

SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.48 1.0 NA1

SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.57 1.0 NA1






SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-4-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 22 50 NA1

8260TPH NA 406300%71.1(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-4-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW8015B(M) 8/16/11 406321mg/LNDTPH as Diesel (SG) 08/17/11 0.0400 0.10 34021

SW8015B(M) 8/16/11 406321mg/LNDTPH as Motor Oil (SG) 08/17/11 0.0900 0.20 34021

SW8015B(M) 8/16/11 406321%82.2Pentacosane (S) 08/17/11 57.9 125 34021


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-4-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW6010B 8/12/11 406242mg/LNDAntimony (Dissolved) 08/15/11 0.004 0.009 33771

SW6010B 8/12/11 406242mg/LNDArsenic (Dissolved) 08/15/11 0.005 0.009 33771

SW6010B 8/12/11 406242mg/L0.044Barium (Dissolved) 08/15/11 0.002 0.009 33771

SW6010B 8/12/11 406242mg/LNDBeryllium (Dissolved) 08/15/11 0.002 0.005 33771

SW6010B 8/12/11 406242mg/LNDCadmium (Dissolved) 08/15/11 0.001 0.005 33771

SW6010B 8/12/11 406242mg/LNDChromium (Dissolved) 08/15/11 0.002 0.005 33771

SW6010B 8/12/11 406242mg/LNDCobalt (Dissolved) 08/15/11 0.002 0.005 33771

SW6010B 8/12/11 406242mg/LNDCopper (Dissolved) 08/15/11 0.003 0.009 33771

SW6010B 8/12/11 406242mg/LNDLead (Dissolved) 08/15/11 0.005 0.014 33771

SW6010B 8/12/11 406242mg/LNDMolybdenum (Dissolved) 08/15/11 0.002 0.009 33771

SW6010B 8/12/11 406242mg/LNDNickel (Dissolved) 08/15/11 0.002 0.009 33771

SW6010B 8/12/11 406242mg/LNDSelenium (Dissolved) 08/15/11 0.004 0.02 33771

SW6010B 8/12/11 406242mg/LNDSilver (Dissolved) 08/15/11 0.002 0.005 33771

SW6010B 8/12/11 406242mg/LNDThallium (dissolved) 08/15/11 0.004 0.009 33771

SW6010B 8/12/11 406242mg/LNDVanadium (Dissolved) 08/15/11 0.004 0.009 33771

SW6010B 8/12/11 406242mg/LNDZinc (dissolved) 08/15/11 0.002 0.009 33771


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-8-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8260B NA 406300ug/LNDDichlorodifluoromethane 08/16/11 0.50 0.61 NA1.22

SW8260B NA 406300ug/LNDChloromethane 08/16/11 0.50 0.61 NA1.22

SW8260B NA 406300ug/LNDVinyl Chloride 08/16/11 0.45 0.61 NA1.22

SW8260B NA 406300ug/LNDBromomethane 08/16/11 0.46 0.61 NA1.22

SW8260B NA 406300ug/LNDTrichlorofluoromethane 08/16/11 0.42 0.61 NA1.22

SW8260B NA 406300ug/LND1,1-Dichloroethene 08/16/11 0.35 0.61 NA1.22

SW8260B NA 406300ug/LNDFreon 113 08/16/11 0.46 0.61 NA1.22

SW8260B NA 406300J ug/L0.36Methylene Chloride 08/16/11 0.21 6.1 NA1.22

SW8260B NA 406300ug/LNDtrans-1,2-Dichloroethene 08/16/11 0.38 0.61 NA1.22

SW8260B NA 406300ug/LNDMTBE 08/16/11 0.46 0.61 NA1.22

SW8260B NA 406300ug/LNDtert-Butanol 08/16/11 1.8 6.1 NA1.22

SW8260B NA 406300ug/LNDDiisopropyl ether (DIPE) 08/16/11 0.44 0.61 NA1.22

SW8260B NA 406300ug/LND1,1-Dichloroethane 08/16/11 0.34 0.61 NA1.22

SW8260B NA 406300ug/LNDETBE 08/16/11 0.48 0.61 NA1.22

SW8260B NA 406300ug/LNDcis-1,2-Dichloroethene 08/16/11 0.40 0.61 NA1.22

SW8260B NA 406300ug/LND2,2-Dichloropropane 08/16/11 0.46 0.61 NA1.22

SW8260B NA 406300ug/LNDBromochloromethane 08/16/11 0.42 0.61 NA1.22

SW8260B NA 406300ug/L4.9Chloroform 08/16/11 0.36 0.61 NA1.22

SW8260B NA 406300ug/LNDCarbon Tetrachloride 08/16/11 0.32 0.61 NA1.22

SW8260B NA 406300ug/LND1,1,1-Trichloroethane 08/16/11 0.39 0.61 NA1.22

SW8260B NA 406300ug/LND1,1-Dichloropropene 08/16/11 0.48 0.61 NA1.22

SW8260B NA 406300ug/LNDBenzene 08/16/11 0.41 0.61 NA1.22

SW8260B NA 406300ug/LNDTAME 08/16/11 0.39 0.61 NA1.22

SW8260B NA 406300ug/LND1,2-Dichloroethane 08/16/11 0.34 0.61 NA1.22

SW8260B NA 406300ug/LNDTrichloroethylene 08/16/11 0.46 0.61 NA1.22

SW8260B NA 406300ug/LNDDibromomethane 08/16/11 0.26 0.61 NA1.22


SW8260B NA 406300ug/LNDBromodichloromethane 08/16/11 0.28 0.61 NA1.22

SW8260B NA 406300ug/LNDcis-1,3-Dichloropropene 08/16/11 0.37 0.61 NA1.22

SW8260B NA 406300ug/LNDToluene 08/16/11 0.23 0.61 NA1.22

SW8260B NA 406300ug/LNDTetrachloroethylene 08/16/11 0.18 0.61 NA1.22

SW8260B NA 406300ug/LNDtrans-1,3-Dichloropropene 08/16/11 0.25 0.61 NA1.22

SW8260B NA 406300ug/LND1,1,2-Trichloroethane 08/16/11 0.25 0.61 NA1.22

SW8260B NA 406300ug/LNDDibromochloromethane 08/16/11 0.26 0.61 NA1.22



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-8-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. SW8260B NA 406300ug/LND1,2-Dibromoethane 08/16/11 0.24 0.61 NA1.22

SW8260B NA 406300ug/LNDChlorobenzene 08/16/11 0.17 0.61 NA1.22

SW8260B NA 406300ug/LNDEthyl Benzene 08/16/11 0.19 0.61 NA1.22

SW8260B NA 406300ug/LND1,1,1,2-Tetrachloroethane 08/16/11 0.12 0.61 NA1.22

SW8260B NA 406300ug/LNDm,p-Xylene 08/16/11 0.24 1.2 NA1.22

SW8260B NA 406300ug/LNDo-Xylene 08/16/11 0.16 0.61 NA1.22

SW8260B NA 406300ug/LNDStyrene 08/16/11 0.24 0.61 NA1.22

SW8260B NA 406300ug/LNDBromoform 08/16/11 0.55 1.2 NA1.22

SW8260B NA 406300ug/LNDIsopropyl Benzene 08/16/11 0.34 0.61 NA1.22

SW8260B NA 406300ug/LNDBromobenzene 08/16/11 0.48 0.61 NA1.22

SW8260B NA 406300ug/LND1,1,2,2-Tetrachloroethane 08/16/11 0.31 0.61 NA1.22

SW8260B NA 406300ug/LNDn-Propylbenzene 08/16/11 0.36 0.61 NA1.22

SW8260B NA 406300ug/LND2-Chlorotoluene 08/16/11 0.40 0.61 NA1.22

SW8260B NA 406300ug/LND1,3,5-Trimethylbenzene 08/16/11 0.24 0.61 NA1.22

SW8260B NA 406300ug/LND4-Chlorotoluene 08/16/11 0.40 0.61 NA1.22

SW8260B NA 406300ug/LNDtert-Butylbenzene 08/16/11 0.35 0.61 NA1.22

SW8260B NA 406300ug/LND1,2,3-Trichloropropane 08/16/11 0.72 1.2 NA1.22

SW8260B NA 406300ug/LND1,2,4-Trimethylbenzene 08/16/11 0.40 0.61 NA1.22

SW8260B NA 406300ug/LNDsec-Butyl Benzene 08/16/11 0.30 0.61 NA1.22

SW8260B NA 406300ug/LNDp-Isopropyltoluene 08/16/11 0.30 0.61 NA1.22

SW8260B NA 406300ug/LND1,3-Dichlorobenzene 08/16/11 0.38 0.61 NA1.22


SW8260B NA 406300ug/LNDn-Butylbenzene 08/16/11 0.39 0.61 NA1.22


SW8260B NA 406300ug/LND1,2-Dibromo-3-Chloropropane 08/16/11 0.55 1.2 NA1.22

SW8260B NA 406300ug/LNDHexachlorobutadiene 08/16/11 0.27 0.61 NA1.22

SW8260B NA 406300ug/LND1,2,4-Trichlorobenzene 08/16/11 0.59 1.2 NA1.22

SW8260B NA 406300ug/LNDNaphthalene 08/16/11 0.70 1.2 NA1.22

SW8260B NA 406300ug/LND1,2,3-Trichlorobenzene 08/16/11 0.64 1.2 NA1.22

SW8260B NA 406300%94.7(S) Dibromofluoromethane 08/16/11 61.2 131 NA1.22

SW8260B NA 406300%92.1(S) Toluene-d8 08/16/11 75.1 127 NA1.22

SW8260B NA 406300%92.5(S) 4-Bromofluorobenzene 08/16/11 64.1 120 NA1.22

Reporting limits were raised due to sediment in all VOAs.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-8-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

The results shown below are reported using their MDL. 8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 26 61 NA1.22

8260TPH NA 406300%71.1(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1.22

Raised reporting limit - see comment for 8260B analysis.NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-8-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 9:20

1204.22

500 Kirkham

B-8-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod







SW6010B 8/12/11 406242mg/L0.0052Cobalt (Dissolved) 08/15/11 0.002 0.005 33771



SW6010B 8/12/11 406242mg/L0.015Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771








AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:30

1204.22

500 Kirkham

B-16-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW8260B NA 406300ug/LNDChloromethane 08/16/11 0.41 0.50 NA1




































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:30

1204.22

500 Kirkham

B-16-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:30

1204.22

500 Kirkham

B-16-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH NA 406300ug/LNDTPH(Gasoline) 08/16/11 22 50 NA1

8260TPH NA 406300%68.7(S) 4-Bromofluorobenzene 08/16/11 34 114 NA1


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:30

1204.22

500 Kirkham

B-16-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 12:30

1204.22

500 Kirkham

B-16-GW





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


SW6010B 8/12/11 406242mg/L0.010Arsenic (Dissolved) 08/15/11 0.005 0.009 33771








SW6010B 8/12/11 406242mg/L0.022Molybdenum (Dissolved) 08/15/11 0.002 0.009 33771

SW6010B 8/12/11 406242mg/L0.059Nickel (Dissolved) 08/15/11 0.002 0.009 33771







AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 13:00

1204.22

500 Kirkham

FB





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 13:15

1204.22

500 Kirkham

IDW

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW6010B 8/16/11 406288mg/Kg39Barium 08/17/11 1 5.0 34051




SW6010B 8/16/11 406288mg/Kg5.5Cobalt 08/17/11 0.14 5.0 34051


SW6010B 8/16/11 406288mg/Kg3.0Lead 08/17/11 0.043 1.0 34051


SW6010B 8/16/11 406288mg/Kg25Nickel 08/17/11 0.0590 5.0 34051





SW6010B 8/16/11 406288mg/Kg18Zinc 08/17/11 0.59 5.0 34051


AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 13:15

1204.22

500 Kirkham

IDW

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod











SW8081A 8/18/11 406333ug/KgND4,4'-DDE 08/18/11 1.9 8.0 34204



SW8081A 8/18/11 406333ug/KgND4,4'-DDD 08/18/11 1.9 8.0 34204


SW8081A 8/18/11 406333ug/KgND4,4'-DDT 08/18/11 3.2 8.0 34204



SW8081A 8/18/11 406333ug/KgNDMethoxychlor 08/18/11 2.5 20 34204




SW8081A 8/18/11 406333%85.0TCMX (S) 08/18/11 52.5 139 34204

SW8081A 8/18/11 406333%73.5DCBP (S) 08/18/11 50.2 139 34204



AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 13:15

1204.22

500 Kirkham

IDW

SoilSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/11/11 / 13:22

1204.22

500 Kirkham

EQUIP BLANK





AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW6010B 8/12/11 406242mg/LNDBarium (Dissolved) 08/15/11 0.002 0.009 33771















AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406238

mg/L

08/15/11

33657470A1108084

Water


PQL MDL Lab

Qualifier

0.00005 0.0002Mercury 0.00007

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406242

mg/Kg

08/15/11

337730051108084

Water


PQL MDL Lab

Qualifier

0.004 0.009Antimony (Dissolved) ND

0.005 0.009Arsenic (Dissolved) ND

0.002 0.009Barium (Dissolved) ND

0.002 0.005Beryllium (Dissolved) ND

0.001 0.005Cadmium (Dissolved) ND

0.002 0.005Chromium (Dissolved) ND

0.002 0.005Cobalt (Dissolved) ND

0.003 0.009Copper (Dissolved) 0.00357

0.005 0.014Lead (Dissolved) ND

0.002 0.009Molybdenum (Dissolved) ND

0.002 0.009Nickel (Dissolved) ND

0.004 0.02Selenium (Dissolved) ND

0.002 0.005Silver (Dissolved) ND

0.004 0.009Thallium (dissolved) ND

0.004 0.009Vanadium (Dissolved) ND

0.002 0.009Zinc (dissolved) ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108084

Soil


PQL MDL Lab

Qualifier

0.660 0.653Pyridine ND

0.110 0.330N-Nitrosdimethylamine ND

0.123 0.330Aniline ND

0.129 0.330Phenol ND

0.0683 0.330Bis(2-chloroethyl) ether ND

0.129 0.3302-Chlorophenol ND

0.0733 0.3301,3-Dichlorobenzene ND


0.104 0.330Benzyl Alcohol ND


0.116 0.3302-Methylphenol (o-Cresol) ND

0.0683 0.330Bis(2-chloroisopropyl)ether ND

0.139 0.3303-/4-Methylphenol (p-/m-Cresol) ND

0.0931 0.330N-nitroso-di-n-propylamine ND

0.0465 0.330Hexachloroethane ND

0.0528 0.330Nitrobenzene ND

0.0574 0.653Isophorone ND

0.0525 0.6532-Nitrophenol ND

0.133 6.592,4-Dimethylphenol ND

5.59 0.330Benzoic Acid ND

0.0584 0.330Bis(2-Chloroethoxy)methane ND

0.104 0.3302,4-Dichlorophenol ND

0.0733 0.3301,2,4-Trichlorobenzene ND

0.104 0.3302,6-Dichlorophenol ND

0.0901 0.330Naphthalene ND

0.0990 0.3304-Chloroaniline ND

0.0653 0.330Hexachloro-1,3-butadiene ND

0.102 0.3304-Chloro-3-methylphenol ND

0.0792 0.3302-Methylnaphthalene ND

0.0792 0.3301-Methylnaphthalene ND

0.0277 0.330Hexachlorocyclopentadiene ND

0.0950 0.3302,4,6-Trichlorophenol ND

0.121 0.3302,4,5-Trichlorophenol ND

0.0594 3.272-Chloronaphthalene ND

0.0693 0.3302-Nitroaniline ND

0.118 0.330Dimethyl phthalate ND

0.106 0.3301,3-Dinitrobenzene ND

0.0851 0.330Acenaphthylene ND

0.0267 0.3302,6-Dinitrotoluene ND




MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108084

Soil


PQL MDL Lab

Qualifier

0.0960 0.330Acenaphthene ND

0.0297 3.272,4-Dinitrophenol ND

0.0663 0.3304-Nitrophenol ND

0.0782 0.330Dibenzofuran ND

0.0267 0.3302,4-Dinitrotoluene ND

0.119 0.3302,3,5,6-Tetrachlorophenol ND

0.119 0.3302,3,4,6-Tetrachlorophenol ND

0.117 0.330Diethylphthalate ND

0.0990 0.330Fluorene ND

0.0802 0.3304-Chlorophenyl phenyl ether ND


0.0663 0.3304,6-Dinitro-2-methylphenol ND

0.0663 0.330Diphenylamine ND

0.109 0.330Azobenzene ND

0.0812 3.274-Bromophenyl phenyl ether ND

0.101 0.330Hexachlorobenzene ND

0.102 3.27Pentachlorophenol ND

0.142 0.330Phenanthrene ND

0.132 0.330Anthracene ND

0.132 0.330Carbazole ND

0.108 1.68Di-n-butylphthalate ND

0.132 0.653Fluoranthene ND

0.374 3.27Benzidine ND

0.147 0.330Pyrene ND

0.0891 0.330Benzyl butyl phthalate ND

0.149 0.330Benz[a]anthracene ND

0.152 0.3303,3'-Dichlorobenzidine ND

0.176 0.330Chrysene ND

0.0832 0.330Bis(2-Ethylhexyl)phthalate ND

0.138 0.330Di-n-octyl phthalate ND

0.133 0.330Benzo[b]fluoranthene ND

0.169 0.330Benzo[k]fluoranthene ND

0.135 0.330Benzo[a]pyrene ND

0.131 0.330Indeno[1,2,3-cd]pyrene ND

0.151 0.330Dibenz[a,h]anthracene ND

0.150 0.330Benzo[g,h,i]perylene ND


2,4,6-Tribromophenol (S) 33.3

2-Fluorobiphenyl (S) 46.7

2-Fluorophenol (S) 59.8

Nitrobenzene-d5 (S) 48.5


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406316

mg/Kg

08/16/11

33853545_BNA1108084

Soil


PQL MDL Lab

Qualifier

Phenol-d6 (S) 60.6

p-Terphenyl-d14 (S) 89.6

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406267

mg/Kg

08/16/11

338930501108084

Soil


PQL MDL Lab

Qualifier

0.20 5.0Antimony 0.35

0.28 1.7Arsenic 0.28

1 5.0Barium 1.1

0.0840 2.0Beryllium ND

0.059 1.0Cadmium ND

0.059 5.0Chromium 0.33

0.14 5.0Cobalt ND

0.090 5.0Copper 0.18

0.043 1.0Lead 0.34

0.059 5.0Molybdenum 0.12

0.059 5.0Nickel 0.15

0.29 5.0Selenium ND

1.0 1.0Silver ND

0.12 5.0Thallium ND

0.12 5.0Vanadium 0.14

0.59 5.0Zinc 0.88

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406270

mg/Kg

08/16/11

339374711108084

Soil


PQL MDL Lab

Qualifier

0.01 0.10Mercury ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108084

Water


PQL MDL Lab

Qualifier

0.0440 0.10TPH as Diesel (SG) ND

0.0920 0.20TPH as Motor Oil (SG) ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108084

Water


PQL MDL Lab

Qualifier


0.0920 0.20TPH as Motor Oil (SG) 0.13


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406288

mg/Kg

08/17/11

340530501108084

Soil


PQL MDL Lab

Qualifier

0.20 5.0Antimony 0.30

0.28 1.7Arsenic ND

1 5.0Barium 1.1


0.059 1.0Cadmium ND

0.059 5.0Chromium 0.35

0.14 5.0Cobalt ND

0.090 5.0Copper 0.25

0.043 1.0Lead 0.25


0.059 5.0Nickel 0.12

0.29 5.0Selenium ND

1.0 1.0Silver ND

0.12 5.0Thallium ND

0.12 5.0Vanadium 0.12

0.59 5.0Zinc 0.85


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406300

ug/L

08/16/11

341450301108084

Water


PQL MDL Lab

Qualifier

22 50TPH(Gasoline) ND

(S) 4-Bromofluorobenzene 90.2

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406253

ug/Kg

08/15/11

341750351108084

Soil


PQL MDL Lab

Qualifier


(S) 4-Bromofluorobenzene 101

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406325

mg/Kg

08/18/11

34183545_TPH1108084

Soil


PQL MDL Lab

Qualifier

0.758 2.0TPH as Diesel 1.2

1.78 4.0TPH as Motor Oil 3.3

Pentacosane (S) 111


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406326

mg/Kg

08/18/11

34193545_PCB1108084

Soil


PQL MDL Lab

Qualifier

0.0230 0.10Aroclor1016 ND

0.0920 0.20Aroclor1221 ND

0.0460 0.10Aroclor1232 ND

0.0430 0.10Aroclor1242 ND

0.0360 0.10Aroclor1248 ND

0.0240 0.10Aroclor1254 ND

0.0270 0.10Aroclor1260 ND

TCMX (S) 99.1

DCBP (S) 113


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406333

ug/Kg

08/18/11

34203545_OCP1108084

Soil


PQL MDL Lab

Qualifier

0.44 2.0alpha-BHC ND

0.40 2.0gamma-BHC ND

0.36 2.0beta-BHC ND

0.49 2.0delta-BHC ND

1.1 2.0Heptachlor ND

0.44 2.0Aldrin ND

0.32 2.0Heptachlor epoxide ND

0.42 2.0gamma-Chlordane ND

0.36 2.0alpha-Chlordane ND

0.59 2.0Endosulfan I ND

0.48 2.04,4'-DDE ND

0.43 2.0Dieldrin ND

0.57 2.0Endrin ND

0.47 2.04,4'-DDD ND

1.5 2.0Endosulfan II ND

0.81 2.04,4'-DDT ND

1.0 2.0Endrin aldehyde ND

0.49 2.0Endosulfan sulfate ND

0.62 5.0Methoxychlor ND

0.40 2.0Endrin Ketone ND

10 20Chlordane ND

10 100Toxaphene ND

TCMX (S) 100

DCBP (S) 101


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406410

mg/Kg

08/24/11

347930501108084

Soil


PQL MDL Lab

Qualifier

0.20 5.0Antimony ND

0.28 1.7Arsenic ND

1 5.0Barium 1.8


0.059 1.0Cadmium ND

0.059 5.0Chromium 0.14

0.14 5.0Cobalt ND

0.090 5.0Copper 0.96

0.043 1.0Lead 0.25


0.059 5.0Nickel 0.095

0.29 5.0Selenium ND

1.0 1.0Silver ND

0.12 5.0Thallium 0.60

0.12 5.0Vanadium ND

0.59 5.0Zinc 1.2

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406421

mg/L

08/25/11

34891311/3010B1108084

Soil


PQL MDL Lab

Qualifier

0.0500 0.10Lead (TCLP) ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406448

mg/Kg

08/25/11

34943545_TPH1108084

Soil


PQL MDL Lab

Qualifier

0.758 2.0TPH as Diesel 1.7

1.78 4.0TPH as Motor Oil 2.8

Pentacosane (S) 120


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406447

mg/Kg

08/26/11

3496WET/3010B1108084

Soil


PQL MDL Lab

Qualifier

0.0500 0.10Lead (STLC) ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406253

ug/Kg

08/15/11

NANA1108084

Soil


PQL MDL Lab

Qualifier

4.4 10Dichlorodifluoromethane ND

4.6 10Chloromethane ND

2.6 10Vinyl Chloride ND

4.7 10Bromomethane ND

2.9 10Trichlorofluoromethane ND

1.5 101,1-Dichloroethene ND

3.7 10Freon 113 ND

2.0 50Methylene Chloride ND

1.1 10trans-1,2-Dichloroethene ND

2.6 10MTBE ND

21 50tert-Butanol ND

2.2 10Diisopropyl ether (DIPE) ND

1.3 101,1-Dichloroethane ND

2.4 10ETBE ND

1.8 10cis-1,2-Dichloroethene ND

1.2 102,2-Dichloropropane ND

2.3 10Bromochloromethane ND

1.2 10Chloroform ND

1.6 10Carbon Tetrachloride ND

1.2 101,1,1-Trichloroethane ND

1.4 101,1-Dichloropropene ND

1.5 10Benzene ND

2.1 10TAME ND

1.9 101,2-Dichloroethane ND

3.9 10Trichloroethylene ND

2.2 10Dibromomethane ND


1.1 10Bromodichloromethane ND

1.4 10cis-1,3-Dichloropropene ND

0.98 10Toluene ND

1.8 10Tetrachloroethylene ND

1.2 10trans-1,3-Dichloropropene ND

1.8 101,1,2-Trichloroethane ND

1.1 10Dibromochloromethane ND


1.7 101,2-Dibromoethane ND

0.86 10Ethyl Benzene ND

4.2 10Chlorobenzene ND

0.86 101,1,1,2-Tetrachloroethane ND

1.9 10m,p-Xylene ND

0.66 5.0o-Xylene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406253

ug/Kg

08/15/11

NANA1108084

Soil


PQL MDL Lab

Qualifier

0.77 10Styrene ND

1.9 10Bromoform ND

1.2 10Isopropyl Benzene ND

1.4 10n-Propylbenzene ND

1.2 10Bromobenzene ND

3.0 101,1,2,2-Tetrachloroethane ND

1.1 101,3,5-Trimethylbenzene ND

3.3 101,2,3-Trichloropropane ND

1.6 104-Chlorotoluene ND

1.6 102-Chlorotoluene ND

1.4 10tert-Butylbenzene ND

1.1 101,2,4-Trimethylbenzene ND

1.6 10sec-Butyl Benzene ND

1.5 10p-Isopropyltoluene ND

1.8 101,3-Dichlorobenzene ND


2.2 10n-Butylbenzene ND


4.2 101,2-Dibromo-3-Chloropropane ND

2.6 10Hexachlorobutadiene ND

2.1 101,2,4-Trichlorobenzene ND

2.8 10Naphthalene ND

2.9 101,2,3-Trichlorobenzene ND

(S) Dibromofluoromethane 92.9

(S) Toluene-d8 86.1



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406300

ug/L

08/16/11

NANA1108084

Water


PQL MDL Lab

Qualifier

0.41 0.50Dichlorodifluoromethane ND

0.41 0.50Chloromethane ND

0.37 0.50Vinyl Chloride ND

0.37 0.50Bromomethane ND

0.34 0.50Trichlorofluoromethane ND

0.29 0.501,1-Dichloroethene ND

0.38 0.50Freon 113 ND

0.18 5.0Methylene Chloride 0.22

0.31 0.50trans-1,2-Dichloroethene ND

0.38 0.50MTBE ND

1.5 5.0tert-Butanol ND

0.36 0.50Diisopropyl ether (DIPE) ND

0.28 0.501,1-Dichloroethane ND

0.40 0.50ETBE ND

0.33 0.50cis-1,2-Dichloroethene ND

0.37 0.502,2-Dichloropropane ND

0.34 0.50Bromochloromethane ND

0.29 0.50Chloroform ND

0.26 0.50Carbon Tetrachloride ND

0.32 0.501,1,1-Trichloroethane ND

0.40 0.501,1-Dichloropropene ND

0.33 0.50Benzene ND

0.32 0.50TAME ND


0.38 0.50Trichloroethylene ND

0.21 0.50Dibromomethane ND


0.23 0.50Bromodichloromethane ND

0.30 0.50cis-1,3-Dichloropropene ND

0.19 0.50Toluene ND

0.15 0.50Tetrachloroethylene ND

0.20 0.50trans-1,3-Dichloropropene ND


0.21 0.50Dibromochloromethane ND


0.19 0.501,2-Dibromoethane ND

0.14 0.50Chlorobenzene ND

0.15 0.50Ethyl Benzene ND

0.10 0.501,1,1,2-Tetrachloroethane ND

0.20 1.0m,p-Xylene ND

0.13 0.50o-Xylene ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406300

ug/L

08/16/11

NANA1108084

Water


PQL MDL Lab

Qualifier

0.20 0.50Styrene ND

0.45 1.0Bromoform ND

0.28 0.50Isopropyl Benzene ND

0.39 0.50Bromobenzene ND


0.30 0.50n-Propylbenzene ND

0.33 0.502-Chlorotoluene ND

0.20 0.501,3,5-Trimethylbenzene ND


0.29 0.50tert-Butylbenzene ND

0.59 1.01,2,3-Trichloropropane ND


0.24 0.50sec-Butyl Benzene ND

0.25 0.50p-Isopropyltoluene ND



0.32 0.50n-Butylbenzene ND


0.45 1.01,2-Dibromo-3-Chloropropane ND

0.22 0.50Hexachlorobutadiene ND




100 100Ethanol ND TIC


(S) Toluene-d8 92.1




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40623808/15/11

mg/L

7470A 3365

Water

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.0002 0.0150.00005 0.188 2080 - 120Mercury 106 1060.00007

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40624208/15/11

mg/Kg

3005 3377

Water

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.009 10.004 0.269 2080 - 120Antimony (Dissolved) 91.2 91.1ND

0.009 10.005 0.293 2080 - 120Arsenic (Dissolved) 94.3 94.2ND

0.009 10.002 0.411 2080 - 120Barium (Dissolved) 96.7 96.6ND





0.009 10.003 0.295 2080 - 120Copper (Dissolved) 97.2 96.70.00357





0.005 10.002 0.582 2080 - 120Silver (Dissolved) 94.7 94.4ND






Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40631608/16/11

mg/Kg

3545_BNA 3385

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.33 1.6670.129 20.3 3016 - 98.6Phenol 40.3 49.5ND

0.33 1.6670.129 19.2 3012.9 - 91.32-Chlorophenol 36.9 44.8ND





0.33 0.8330.0964 21.8 3029.1 - 94.8Acenaphthene 38.1 47.3ND

0.33 1.6670.0663 7.93 3010.4 - 1314-Nitrophenol 56.0 60.9ND



0.33 0.8330.147 16.8 3034.2 - 127Pyrene 59.5 70.5ND

50 24 - 113Phenol-d6 (S) 54.0 64.1ND





25 18 - 137p-Terphenyl-d14 (S) 47.4 53.4ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40626708/16/11

mg/Kg

3050 3389

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

5.0 500.20 1.07 3030.7 - 130Antimony 96.1 95.10.35

1.7 500.28 3.03 3071 - 121Arsenic 96.8 93.90.28

5.0 501 2.35 3070.2 - 130Barium 102 99.61.1

2.0 500.0840 1.35 3073.3 - 115Beryllium 95.1 96.3ND

1.0 500.059 2.07 3068.7 - 110Cadmium 98.4 96.4ND

5.0 500.059 1.63 3076 - 116Chromium 99.5 97.90.33

5.0 500.14 2.36 3057.4 - 122Cobalt 101 98.6ND

5.0 500.090 2.14 3074.8 - 119Copper 104 1020.18

1.0 500.13 0.784 3067.9 - 118Lead 97.3 96.50.34

5.0 500.059 0.936 3062.9 - 123Molybdenum 98.7 97.80.12

5.0 500.059 2.15 3061.5 - 122Nickel 100 97.90.15

5.0 500.29 4.36 3062 - 111Selenium 93.7 89.7ND

1.0 501.0 2.22 3081.1 - 109Silver 96.7 94.6ND

5.0 500.12 0.226 3039.2 - 125Thallium 93.2 93.0ND

5.0 500.12 1.89 3065.8 - 122Vanadium 101 99.10.14

5.0 500.59 3.08 3059.9 - 122Zinc 122 1180.88

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40627008/16/11

mg/Kg

7471 3393

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 1.250.01 6.58 3080.5 - 133Mercury 109 116ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632108/17/11

mg/L

3510_TPHSG 3402

Water

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0440 2.00 3034.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND

100 57.9 - 125Pentacosane (S) 79.6 73.0ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40628808/17/11

mg/Kg

3050 3405

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

5 500.2 1.79 3030.7 - 130Antimony 97.13 98.90.30

1.7 500.28 1.66 3071 - 121Arsenic 96.33 97.9ND

5 501.1 4.59 3070.2 - 130Barium 103.4 98.41.1

2 500.084 3.66 3073.3 - 115Beryllium 98.33 94.8ND

1 500.059 5.40 3068.7 - 110Cadmium 99.51 94.3ND

5 500.059 4.69 3076 - 116Chromium 104.2 99.20.35

5 500.14 5.72 3057.4 - 122Cobalt 101.8 96.3ND

5 500.09 4.58 3074.8 - 119Copper 104.2 99.30.25

1 500.13 0.996 3067.9 - 118Lead 97.89 98.90.25

5 500.059 1.51 3062.9 - 123Molybdenum 98.92 1000.060

5 500.059 5.44 3061.5 - 122Nickel 101.7 96.60.12

5 500.29 2.56 3062 - 111Selenium 91.96 94.4ND

1 501 4.38 3081.1 - 109Silver 98.56 94.4ND

5 500.12 1.50 3039.2 - 125Thallium 92.93 94.3ND

5 500.12 5.40 3065.8 - 122Vanadium 103.9 98.50.12

5 500.59 5.37 3059.9 - 122Zinc 100 94.80.85

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40630008/16/11

ug/L

5030 3414

Water

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

50 227.2722 21.5 3052.4 - 127TPH(Gasoline) 114 92.1ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40625308/15/11

ug/Kg

5035 3417

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

100 100017 2.25 3048.2 - 132TPH(Gasoline) 91.4 93.5ND

50 57 - 127(S) 4-Bromofluorobenzene 89.7 92.8101



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632508/18/11

mg/Kg

3545_TPH 3418

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2 33.330.758 0.871 3052.7 - 115TPH as Diesel 87.1 87.81.2

100 59.7 - 129Pentacosane (S) 96.8 98.13.3

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632608/18/11

mg/Kg

3545_PCB 3419

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0230 4.27 3055.6 - 135Aroclor1016 92.7 88.8ND

0.10 0.50.0270 4.66 3065.6 - 132Aroclor1260 89.6 85.5ND

0.25 68.9 - 123TCMX (S) 91.7 83.8ND

0.250 69.5 - 119DCBP (S) 107 98.6ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40633308/18/11

ug/Kg

3545_OCP 3420

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2.0 200.40 9.23 3056.9 - 120gamma-BHC 74.9 68.3ND

2.0 201.1 10.9 3063.6 - 117Heptachlor 76.4 68.5ND

2.0 200.44 0.805 3053 - 123Aldrin 78.4 79.1ND

2.0 200.43 8.92 3044 - 130Dieldrin 76.7 70.2ND

2.0 200.57 12.2 3044.1 - 121Endrin 75.3 66.6ND

2.0 200.81 10.4 3052.8 - 1344,4'-DDT 81.3 73.3ND

350 52.5 - 139TCMX (S) 76.3 70.7ND

350 50.2 - 139DCBP (S) 75.7 68.4ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40641008/24/11

mg/Kg

3050 3479

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

5.0 500.20 0.719 3030.7 - 130Antimony 98.4 99.1ND

1.7 500.28 0.802 3071 - 121Arsenic 99.3 100ND

5.0 501 0.939 3070.2 - 130Barium 106 1071.8

2.0 500.0840 3.41 3073.3 - 115Beryllium 101 97.6ND

1.0 500.059 1.60 3068.7 - 110Cadmium 99.2 101ND

5.0 500.059 1.61 3076 - 116Chromium 105 1070.14

5.0 500.14 1.92 3057.4 - 122Cobalt 103 105ND

5.0 500.090 1.03 3074.8 - 119Copper 106 1070.96

1.0 500.13 0.695 3067.9 - 118Lead 101 1000.25

5.0 500.059 2.26 3062.9 - 123Molybdenum 105 1070.17

5.0 500.059 2.93 3061.5 - 122Nickel 101 1040.095

5.0 500.29 0.118 3062 - 111Selenium 93.3 93.2ND

1.0 501.0 0.587 3081.1 - 109Silver 102 103ND

5.0 500.12 3.75 3039.2 - 125Thallium 94.1 97.70.60

5.0 500.12 1.04 3065.8 - 122Vanadium 105 106ND

5.0 500.59 0.292 3059.9 - 122Zinc 103 1031.2

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40642108/25/11

mg/L

1311/3010B 3489

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 100.0500 0.343 2080 - 120Lead (TCLP) 99.4 99.1ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40644808/25/11

mg/Kg

3545_TPH 3494

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

2 33.330.758 2.84 3052.7 - 125TPH as Diesel 85.8 83.41.7

100 59.7 - 129Pentacosane (S) 127 1262.8



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40644708/26/11

mg/L

WET/3010B 3496

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 100.0500 2.49 2080 - 120Lead (STLC) 87.0 89.2ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40625308/15/11

ug/Kg

NA NA

Soil

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier


10 501.5 0.170 3066.5 - 135Benzene 82.5 82.5ND


10 500.98 0.730 3056.8 - 134Toluene 88.1 87.4ND



50 55.2 - 133(S) Toluene-d8 87.9 87.4ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40630008/16/11

ug/L

NA NA

Water

1108084


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.50 17.040.29 14.7 3061.4 - 1291,1-Dichloroethene 87.0 101ND

0.50 17.040.33 8.61 3066.9 - 140Benzene 93.2 102ND

0.50 17.040.38 8.38 3069.3 - 144Trichloroethylene 99.4 108ND

0.50 17.040.19 8.26 3076.6 - 123Toluene 95.3 103ND

0.50 17.040.14 8.04 3073.9 - 137Chlorobenzene 97.0 105ND

11.36 61.2 - 131(S) Dibromofluoromethane 88.9 103ND

11.36 75.1 - 127(S) Toluene-d8 92.0 104ND




Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:

Prep Method: NA


Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8260B 40625308/15/11

ug/Kg

NANA

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

50 53.7 - 1391.5 10 1.47 301,1-Dichloroethene 92.0 90.60

50 66.5 - 1351.5 10 0.523 30Benzene 91.5 92.00

50 57.5 - 1503.9 10 1.26 30Trichloroethylene 88.1 89.20

50 56.8 - 1340.98 10 5.59 30Toluene 91.2 96.40

50 57.4 - 1344.2 10 5.90 30Chlorobenzene 94.1 99.80

50 59.8 - 148(S) Dibromofluoromethane 84.2 91.9

50 55.2 - 133(S) Toluene-d8 86.2 87.8

50 55.8 - 141(S) 4-Bromofluorobenzene 94.0 102

Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40626708/16/11

mg/Kg

33893050

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

50 30.7 - 1300.20 5.0 2.94 30Antimony 92.0 89.30.00

50 71 - 1210.28 1.7 2.37 30Arsenic 92.7 90.40.048

50 70.2 - 1301 5.0 3.47 30Barium 108 1161.3

50 73.3 - 1150.0840 2.0 1.06 30Beryllium 94.1 93.10.00

50 68.7 - 1100.059 1.0 0.659 30Cadmium 92.9 92.30.00

50 76 - 1160.059 5.0 1.94 30Chromium 96.7 1000.61

50 57.4 - 1220.14 5.0 6.75 30Cobalt 98.7 1060.00

50 74.8 - 1190.090 5.0 6.54 30Copper 98.3 1060.13

50 67.9 - 1180.13 1.0 25.4 30Lead 115 73.50.69

50 62.9 - 1230.059 5.0 2.15 30Molybdenum 92.3 90.30.00

50 61.5 - 1220.059 5.0 0.310 30Nickel 91.1 91.40.38

50 62 - 1110.29 5.0 0.560 30Selenium 89.5 89.00.00

50 81.1 - 1091.0 1.0 5.99 30Silver 92.4 98.10.00

50 39.2 - 1250.12 5.0 2.64 30Thallium 83.6 81.40.00

50 65.8 - 1220.12 5.0 8.74 30Vanadium 91.7 1050.47

50 59.9 - 1220.59 5.0 4.06 30Zinc 96.7 90.40.69



Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

7471B 40627008/16/11

mg/Kg

33937471

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1.25 60 - 1400.01 0.10 8.29 30Mercury 114 1050.00057

Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40628808/17/11

mg/Kg

34053050

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

50 30.7 - 1300.20 5.0 4.24 30Antimony 88.6 84.90.00

50 71 - 1210.28 1.7 3.04 30Arsenic 93.9 90.80.13

50 70.2 - 1301 5.0 3.08 30Barium 81.2 95.43.8

50 73.3 - 1150.0840 2.0 4.92 30Beryllium 98.2 93.50.00

50 68.7 - 1100.059 1.0 2.04 30Cadmium 98.1 96.10.00

50 76 - 1160.059 5.0 2.93 30Chromium 92.9 89.10.42

50 57.4 - 1220.14 5.0 13.5 30Cobalt 104 87.80.24

50 74.8 - 1190.090 S5.0 23.1 30Copper 155 1070.79

50 67.9 - 1180.13 S1.0 0.000 30Lead 3.80 4.002.6

50 62.9 - 1230.059 5.0 0.771 30Molybdenum 91.2 90.50.00

50 61.5 - 1220.059 5.0 6.72 30Nickel 98.7 89.90.41

50 62 - 1110.29 5.0 0.815 30Selenium 92.4 91.70.00

50 81.1 - 1091.0 1.0 3.10 30Silver 94.3 97.30.00

50 39.2 - 1250.12 5.0 0.185 30Thallium 81.2 81.40.00

50 65.8 - 1220.12 5.0 2.30 30Vanadium 105 1010.75

50 59.9 - 1220.59 5.0 2.96 30Zinc 82.9 93.32.6

Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40642108/25/11

mg/L

34891311/3010B

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

10 75 - 1250.0500 0.10 0.964 20Lead (TCLP) 93.9 94.80.000



Work Order: 1108084

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8015B(M) 40644808/25/11

mg/Kg

34943545_TPH

Soil


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

33.33 50.3 - 1250.76 2.0 1.78 30TPH as Diesel 78.4 79.828.2966

100 57.9 - 125Pentacosane (S) 116 121
















DEFINITIONS:





°C5

Yes

Yes

Yes

Temperature:







Yes

Yes

Not Present

Yes






Yes

Yes

Yes

Not Present









Received By: NK








Report Due Date:

5 Day TAT!! Received 20 soils and 5 waters @ 5'C. Dissolved metals analysis for Waters samples. SG clean up on all waters.Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.

16:35

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

B-4-1.01108084-001A Soil 02/07/1208/11/11 8:15S_6010BCAM17S_7471BHGEn_8260FullS_8081AOCPS_8082PCBS_TPHDOS_8270FullS_GCMS-GRO

Sample Note: Pretarred voas for 8260, TPHg. Use for MS/MSD.

B-4-5.01108084-002A Soil 02/07/1208/11/11 8:20S_6010BCAM17S_TPHDOS_8082PCBS_8270FullEn_8260FullS_GCMS-GROS_7471BHG

B-4-101108084-003A Soil 02/07/12 On-Hold08/11/11 8:25Hold Samples

Sample Note:

B-8-1.01108084-004A Soil 02/07/1208/11/11 8:55S_6010B(STLC)S_7471BHGS_GCMS-GROS_TPHDOS_8270FullS_8082PCBS_8081AOCPEn_8260FullS_6010BCAM17

Sample Note: Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both. Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011



Report Due Date:


16:35

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

B-8-5.01108084-005A Soil 02/07/1208/11/11 9:00S_6010BCAM17S_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GROS_7471BHG

B-8-8.01108084-006A Soil 02/07/1208/11/11 9:05S_6010BCAM17S_TPHDO

Sample Note: Sample 004 amd 010 for Lead STLC. Sample 008 for STLC and TCLP Lead. Sample 009 and 006 off Hold, added total Lead on both and TPH-oil(watch the hloding time). Added per client on 08/23/2011. 3 day RUSH TAT Due 08/26/2011.B-2-1.01108084-007A Soil 02/07/1208/11/11 9:15

S_6010BCAM17En_8260FullS_GCMS-GROS_7471BHGS_TPHDOS_8270FullS_8082PCBS_8081AOCP

B-2-5.01108084-008A Soil 02/07/1208/11/11 9:20S_6010B(STLC)S_7471BHGS_6010B(TCLP)S_6010BCAM17S_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GRO

B-2-9.01108084-009A Soil 02/07/1208/11/11 9:25S_6010BCAM17



Report Due Date:


16:35

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_TPHDOB-7-1.01108084-010A Soil 02/07/1208/11/11 10:30

S_6010B(STLC)S_7471BHGS_GCMS-GROS_6010BCAM17En_8260FullS_8270FullS_8082PCBS_TPHDOS_8081AOCP

B-7-5.01108084-011A Soil 02/07/1208/11/11 10:35S_7471BHGS_TPHDOS_8082PCBS_8270FullS_6010BCAM17En_8260FullS_GCMS-GRO

B-7-7.01108084-012A Soil 02/07/1208/11/11 10:40Hold Samples

B-6-1.01108084-013A Soil 02/07/1208/11/11 10:55S_7471BHGS_8082PCBS_TPHDOS_8270FullS_8081AOCPS_6010BCAM17S_GCMS-GROEn_8260Full

B-6-5.01108084-014A Soil 02/07/1208/11/11 11:00S_7471BHGEn_8260FullS_8270Full



Report Due Date:


16:35

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

S_TPHDOS_8082PCBS_6010BCAM17S_GCMS-GRO


B-16-1.01108084-016A Soil 02/07/1208/11/11 12:05S_7471BHGS_6010BCAM17En_8260FullS_8082PCBS_8270FullS_TPHDOS_8081AOCPS_GCMS-GRO

B-16-5.01108084-017A Soil 02/07/1208/11/11 12:10S_7471BHGS_8270FullS_8082PCBS_TPHDOEn_8260FullS_GCMS-GROS_6010BCAM17


B-7-1.0D1108084-019A Soil 02/07/1208/11/11 10:30S_GCMS-GROEn_8260FullS_TPHDO

B-4-GW1108084-020A Water 09/25/1108/11/11 9:20W_GCMS-GROW_8260Full

Sample Note:

B-4-GW1108084-020B Water 09/25/1108/11/11 9:20



Report Due Date:


16:35

8/23/2011


500 Kirkham

1204.22

8/26/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

3 day:25



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID



Sample Note: Dissolved metals analysis for all waters samples. SG clean up on all waters.



Sample Note: Dissolved metals analysis for all waters samples. SG clean up on all waters.





FB1108084-023A Water 09/25/1108/11/11 13:00W_8260Full

IDW1108084-024A Soil 09/25/1108/11/11 13:15S_7471BHGS_TPHDOS_8081AOCPS_GCMS-GROS_6010BCAM17

EQUIP BLANK1108084-025A Water 09/25/1108/11/11 13:22W_D6010BCAM17W_D7470AHG


Northgate Environmental Management Inc.300 Frank H. Ogawa Plaza, Suite 510Oakland, California 94612Tel: 5108390688Fax: (510) 839-4350

RE: 500 Kirkham

Torrent Laboratory, Inc. received 7 sample(s) on August 15, 2011 for the analyses presented in the following Report.

Dear Dennis Laduzinsky:




Date

August 22, 2011

G.Gueorguieva

Sr. Project Manager


Date: 8/22/2011



Work Order: 1108103

CASE NARRATIVE


Analytical Comments for method W_D7470A, 1108103-002C MS/MSD, QC Analytical Batch ID 406291, Note:The % recoveries for Mercury are outside of laboratory control limits. The associated LCS/LCSD % recoveries and % RPD are within limits. No corrective action required.







1108103-001JA-2



1108103-002JA-3










1108103-003JA-4


Vinyl Chloride ug/L2.50.500.37SW8260B 1

1,1-Dichloroethene ug/L5.20.500.29SW8260B 1

trans-1,2-Dichloroethene ug/L2.60.500.31SW8260B 1

1,1-Dichloroethane ug/L460.500.28SW8260B 1

Chloroform ug/L0.530.500.29SW8260B 1

Benzene ug/L0.530.500.33SW8260B 1

Tetrachloroethylene ug/L360.500.15SW8260B 1

1,1,2-Trichloroethane ug/L0.910.500.20SW8260B 1


cis-1,2-Dichloroethene ug/L1602.21.4SW8260B 4.4

Trichloroethylene ug/L1402.21.7SW8260B 4.4


Chromium (Dissolved) mg/L0.00700.0050.002SW6010B 1









1108103-004JA-4D


Vinyl Chloride ug/L2.50.500.37SW8260B 1

1,1-Dichloroethene ug/L5.20.500.29SW8260B 1

trans-1,2-Dichloroethene ug/L2.70.500.31SW8260B 1

1,1-Dichloroethane ug/L450.500.28SW8260B 1

Tetrachloroethylene ug/L340.500.15SW8260B 1

1,1,2-Trichloroethane ug/L0.850.500.20SW8260B 1


cis-1,2-Dichloroethene ug/L1702.21.4SW8260B 4.4

Trichloroethylene ug/L1502.21.7SW8260B 4.4


Chromium (Dissolved) mg/L0.00670.0050.002SW6010B 1



1108103-005Equipment Blank



1108103-006TB080911 #4



1108103-007TB080911 #3




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 11:15

1204.22

500 Kirkham

JA-2

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 11:15

1204.22

500 Kirkham

JA-2

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





























SW8260B NA 406355%103(S) Dibromofluoromethane 08/19/11 61.2 131 NA1




SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 11:15

1204.22

500 Kirkham

JA-2

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/19/11 406355ug/LNDTPH(Gasoline) 08/19/11 22 50 34441

8260TPH 8/19/11 406355%83.4(S) 4-Bromofluorobenzene 08/19/11 34 114 34441


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 11:15

1204.22

500 Kirkham

JA-2

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 11:15

1204.22

500 Kirkham

JA-2

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


















AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

SW7470A 8/16/11 406291mg/LNDMercury (Dissolved) 08/17/11 0.00005 0.0002 34091


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 12:45

1204.22

500 Kirkham

JA-3

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 12:45

1204.22

500 Kirkham

JA-3

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod


















AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW8260B NA 406355ug/L2.5Vinyl Chloride 08/19/11 0.37 0.50 NA1



SW8260B NA 406355ug/L5.21,1-Dichloroethene 08/19/11 0.29 0.50 NA1



SW8260B NA 406355ug/L2.6trans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1




SW8260B NA 406355ug/L461,1-Dichloroethane 08/19/11 0.28 0.50 NA1




SW8260B NA 406355ug/L0.53Chloroform 08/19/11 0.29 0.50 NA1




SW8260B NA 406355ug/L0.53Benzene 08/19/11 0.33 0.50 NA1








SW8260B NA 406355ug/L36Tetrachloroethylene 08/19/11 0.15 0.50 NA1


SW8260B NA 406355ug/L0.911,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1







SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






























SW8260B NA 406363ug/L160cis-1,2-Dichloroethene 08/22/11 1.4 2.2 NA4.4

SW8260B NA 406363ug/L140Trichloroethylene 08/22/11 1.7 2.2 NA4.4





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/19/11 406355x ug/L180TPH(Gasoline) 08/19/11 22 50 34441


x-Not typical of Gasoline standard pattern. Result due to discrete peaks of non-fuel compounds (see 8260 results).NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






SW6010B 8/16/11 406289mg/L0.0070Chromium (Dissolved) 08/18/11 0.002 0.005 34061












AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4D

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SW8260B NA 406355ug/L2.5Vinyl Chloride 08/19/11 0.37 0.50 NA1



SW8260B NA 406355ug/L5.21,1-Dichloroethene 08/19/11 0.29 0.50 NA1



SW8260B NA 406355ug/L2.7trans-1,2-Dichloroethene 08/19/11 0.31 0.50 NA1




SW8260B NA 406355ug/L451,1-Dichloroethane 08/19/11 0.28 0.50 NA1
















SW8260B NA 406355ug/L34Tetrachloroethylene 08/19/11 0.15 0.50 NA1


SW8260B NA 406355ug/L0.851,1,2-Trichloroethane 08/19/11 0.20 0.50 NA1







SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4D

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






























SW8260B NA 406363ug/L170cis-1,2-Dichloroethene 08/22/11 1.4 2.2 NA4.4

SW8260B NA 406363ug/L150Trichloroethylene 08/22/11 1.7 2.2 NA4.4





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4D

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod

8260TPH 8/19/11 406355x ug/L190TPH(Gasoline) 08/19/11 22 50 34441


x-Not typical of Gasoline standard pattern. Result due to discrete peaks of non-fuel compounds (see 8260 results).NOTE:


SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4D

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod





SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 14:20

1204.22

500 Kirkham

JA-4D

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






SW6010B 8/16/11 406289mg/L0.0067Chromium (Dissolved) 08/18/11 0.002 0.005 34061












AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod



SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/15/11 / 10:00

1204.22

500 Kirkham

Equipment Blank

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/09/11 /

1204.22

500 Kirkham

TB080911 #4

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































SAMPLE RESULTS



Client Sample ID:

Date/Time Sampled:

Project Number:


08/09/11 /

1204.22

500 Kirkham

TB080911 #3

WaterSample Matrix:




AnalyticalBatch

UnitLabQualifier


PrepDate

AnalysisMethod






































MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108103

Water


PQL MDL Lab

Qualifier


0.0920 0.20TPH as Motor Oil (SG) ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406321

mg/L

08/17/11

34023510_TPHSG1108103

Water


PQL MDL Lab

Qualifier


0.0920 0.20TPH as Motor Oil (SG) 0.13


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406289

mg/Kg

08/18/11

340630051108103

Water


PQL MDL Lab

Qualifier

0.004 0.009Antimony (Dissolved) ND

0.005 0.009Arsenic (Dissolved) ND

0.002 0.009Barium (Dissolved) ND

0.002 0.005Beryllium (Dissolved) ND

0.001 0.005Cadmium (Dissolved) ND

0.002 0.005Chromium (Dissolved) ND

0.002 0.005Cobalt (Dissolved) ND

0.003 0.009Copper (Dissolved) ND

0.005 0.014Lead (Dissolved) ND

0.002 0.009Molybdenum (Dissolved) ND

0.002 0.009Nickel (Dissolved) ND

0.004 0.02Selenium (Dissolved) ND

0.002 0.005Silver (Dissolved) 0.00255

0.004 0.009Thallium (dissolved) ND

0.004 0.009Vanadium (Dissolved) ND

0.002 0.009Zinc (dissolved) ND


MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406291

mg/L

08/17/11

34097470A1108103

Water


PQL MDL Lab

Qualifier

0.00005 0.0002Mercury (Dissolved) ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406362

ug/L

08/19/11

344450301108103

Water


PQL MDL Lab

Qualifier



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

406355

ug/L

08/19/11

345050301108103

Water


PQL MDL Lab

Qualifier




MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

ug/L

NA1108103

Water


PQL MDL Lab

Qualifier







0.38 0.50Freon 113 ND

0.18 5.0Methylene Chloride ND


0.38 0.50MTBE ND




0.40 0.50ETBE ND








0.33 0.50Benzene ND

0.32 0.50TAME ND







0.19 0.50Toluene ND













MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

ug/L

NA1108103

Water


PQL MDL Lab

Qualifier

0.20 0.50Styrene ND

























(S) Toluene-d8 93.3



MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406363

ug/L

08/22/11

NANA1108103

Water


PQL MDL Lab

Qualifier







0.38 0.50Freon 113 ND

0.18 5.0Methylene Chloride ND


0.38 0.50MTBE ND




0.40 0.50ETBE ND








0.33 0.50Benzene ND

0.32 0.50TAME ND







0.19 0.50Toluene ND













MB Summary Report

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

406363

ug/L

08/22/11

NANA1108103

Water


PQL MDL Lab

Qualifier

0.20 0.50Styrene ND

























(S) Toluene-d8 90.3




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40632108/17/11

mg/L

3510_TPHSG 3402

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.10 10.0440 2.00 0,34.5 - 95.6TPH as Diesel (SG) 51.6 52.7ND

100 57.9 - 125Pentacosane (S) 79.6 73.0ND

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40628908/18/11

mg/Kg

3005 3406

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.009 10.004 0.195 0,80 - 120Antimony (Dissolved) 88.5 89.0ND

0.009 10.005 1.71 0,80 - 120Arsenic (Dissolved) 89.9 91.4ND

0.009 10.002 0.739 0,80 - 120Barium (Dissolved) 91.0 91.5ND





0.009 10.003 0.951 2080 - 120Copper (Dissolved) 91.2 91.7ND





0.005 10.002 0.114 2080 - 120Silver (Dissolved) 89.4 90.00.00255




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40629108/17/11

mg/L

7470A 3409

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

0.0002 0.0150.00005 14.1 0,80 - 120Mercury (Dissolved) 110 98.4ND



Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40636208/19/11

ug/L

5030 3444

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

50 227.2722 10.2 3052.4 - 127TPH(Gasoline) 98.2 109ND


Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:


Analytical Batch:

40635508/19/11

ug/L

5030 3450

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier

50 227.2722 52.4 - 127TPH(Gasoline) 81.8ND

11.36 58.4 - 133(S) 4-Bromofluorobenzene 89.487.3

Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

ug/L

NA

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier


0.50 17.040.33 2.97 3066.9 - 140Benzene 90.5 93.1ND

0.50 17.040.38 1.31 3069.3 - 144Trichloroethylene 101 103ND

0.50 17.040.19 1.10 3076.6 - 123Toluene 92.9 93.7ND



11.36 75.1 - 127(S) Toluene-d8 89.5 91.2ND




Work Order:

Matrix:

Units:

Prep Method:


Prep Date:

Analyzed Date:

NA Prep Batch:

Analytical Batch:

40636308/22/11

ug/L

NA NA

Water

1108103


SpikeConc.

LCS %Recovery

LCSD %Recovery

LCS/LCSD% RPD

%Recovery

Limits% RPDLimits

LabQualifier


0.50 17.040.33 8.18 3066.9 - 140Benzene 86.8 94.3ND

0.50 17.040.38 9.08 3069.3 - 144Trichloroethylene 87.7 95.8ND

0.50 17.040.19 9.09 3076.6 - 123Toluene 86.8 95.1ND



11.36 75.1 - 127(S) Toluene-d8 89.1 89.3ND




Work Order: 1108103

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW6010B 40628908/18/11

mg/Kg

34063005

Water


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

1 75 - 1250.004 0.009 0.669 20Antimony (Dissolved) 88.4 88.20.00

1 75 - 1250.005 0.009 1.22 20Arsenic (Dissolved) 87.1 87.80.00

1 80 - 1200.002 0.009 1.84 20Barium (Dissolved) 86.4 84.30.127

1 80 - 1200.002 0.005 0.460 20Beryllium (Dissolved) 92.7 93.30

1 75 - 1250.001 0.005 2.17 20Cadmium (Dissolved) 86.1 83.90.00

1 75 - 1250.002 0.005 2.16 20Chromium (Dissolved) 89.8 87.90.00

1 75 - 1250.002 0.005 0.274 20Cobalt (Dissolved) 86.0 85.50.00

1 75 - 1250.003 0.009 2.62 20Copper (Dissolved) 92.6 90.50.00

1 75 - 1250.005 0.014 1.08 20Lead (Dissolved) 85.9 84.80.00

1 75 - 1250.002 0.009 0.595 20Molybdenum (Dissolved) 92.8 92.40.00

1 75 - 1250.002 0.009 0.0476 20Nickel (Dissolved) 85.9 85.70.00

1 75 - 1250.004 0.02 0.157 20Selenium (Dissolved) 91.1 90.70.00

1 75 - 1250.002 0.005 2.93 20Silver (Dissolved) 90.5 88.20.00

1 75 - 1250.004 0.009 0.602 20Thallium (dissolved) 81.6 81.20.00

1 75 - 1250.004 0.009 1.91 20Vanadium (Dissolved) 89.3 87.10.00

1 75 - 1250.002 0.009 3.54 20Zinc (dissolved) 87.3 84.80.00

Work Order: 1108103

Analyzed Date:

Prep Date:

Matrix:



Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW7470A 40629108/17/11

mg/L

34097470A

Water


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

0.015 75 - 1250.00005 S,R0.0002 28.4 20Mercury (Dissolved) 52.3 69.3-0.00001



Work Order: 1108103

Analyzed Date:

Prep Date:

Matrix:

Prep Method: NA


Analytical Method:

Prep Batch:

Units:

Analytical Batch:

SW8260B 40636308/22/11

ug/L

NANA

Water


SpikeConc.

MS %Recovery

MSD %Recovery

MS/MSD% RPD

%Recovery

Limits

% RPDLimits

LabQualifier

17.04 61.4 - 1290.29 0.50 2.88 301,1-Dichloroethene 112 1150

17.04 66.9 - 1400.33 0.50 4.26 30Benzene 103 1080

17.04 69.3 - 1440.38 0.50 0.213 30Trichloroethylene 107 1070

17.04 76.6 - 1230.19 0.50 0.594 30Toluene 106 1050

17.04 73.9 - 1370.14 0.50 0.115 30Chlorobenzene 102 1020

11.36 61.2 - 131(S) Dibromofluoromethane 85.7 89.4

11.36 75.1 - 127(S) Toluene-d8 89.8 87.2

11.36 64.1 - 120(S) 4-Bromofluorobenzene 84.2 82.7
















DEFINITIONS:





°C4

Yes

Yes

Yes

Temperature:







Yes

Yes

Not Present

Yes






Yes

Yes

Yes

Not Present









Received By: NG








Report Due Date:

On 08/15/2011, 7 samples received on 5 day TAT.

16:15

8/15/2011


500 Kirkham

1204.22

8/22/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

5+ day:0



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

JA-21108103-001A Water 09/29/1108/15/11 11:15W_GCMS-GROW_8260Full

Sample Note: TPH-D/O Silica Gel clean up on all samples. Dissolved Metals CAM 17 on all samples. Use JA-2(sample 001) for MS/MSD. VOAs for JA-4 and JA-4D are unpreserved. Watch for the holding time on samples 006 and 007.JA-21108103-001B Water 09/29/1108/15/11 11:15

W_TPHDOSGJA-21108103-001C Water 09/29/1108/15/11 11:15

W_D7470AHGW_D6010BCAM17


JA-31108103-002B Water 09/29/1108/15/11 12:45W_TPHDOSG

JA-31108103-002C Water 09/29/1108/15/11 12:45W_D7470AHGW_D6010BCAM17


JA-41108103-003B Water 09/29/1108/15/11 14:20W_TPHDOSG

JA-41108103-003C Water 09/29/1108/15/11 14:20W_D7470AHGW_D6010BCAM17

JA-4D1108103-004A Water 09/29/1108/15/11 14:20W_GCMS-GROW_8260Full

JA-4D1108103-004B Water 09/29/1108/15/11 14:20W_TPHDOSG

JA-4D1108103-004C Water 09/29/1108/15/11 14:20W_D7470AHGW_D6010BCAM17

Equipment Blank1108103-005A Water 09/29/1108/15/11 10:00W_GCMS-GROW_8260Full



Report Due Date:

On 08/15/2011, 7 samples received on 5 day TAT.

16:15

8/15/2011


500 Kirkham

1204.22

8/22/2011

TAT Requested:

Date Received:

Time Received:

QC Level:

Project Name:

Project # :

Comments:

Client ID:

5+ day:0



TestOn Hold

SampleOn Hold

ScheduledDisposal


Client Sample ID

WO Sample ID

TB080911 #41108103-006A Water 09/29/1108/09/11W_8260Full

TB080911 #31108103-007A Water 09/29/1108/09/11W_8260Full


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