investigation of dry ice blockage in an ultra-low temperature cascade refrigeration system using co2...

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Investigation of dry ice blockage in an ultra-low temperature cascade refrigeration system using CO 2 as a working fluid Hiroshi Yamaguchi a , Xiao-Dong Niu a, *, Kenichi Sekimoto a , Petter Neksa ˚ b a Energy Conversion Research Center, Doshisha University, Kyotanabe, Kyoto, Japan b SINTEF Energy Research, No-7465 Trondheim, Norway article info Article history: Received 6 August 2010 Received in revised form 28 October 2010 Accepted 1 November 2010 Available online 13 November 2010 Keywords: Dry ice Solid-gas flow Ultra-low temperature Refrigeration system-cascade abstract Dry ice blockage in a CO 2 -solidegas-flow-based ultra-low temperature cascade refrigera- tion system is investigated experimentally by a visualization test and a system study of the liquid CO 2 blew into an expansion tube through a Throttle needle valve. The visualization test shows that dry ice sedimentation occurs in low flow velocity and the dry ice formation makes the heat transfer behavior of CO 2 complicated. The sedimentation also occurs at low condensation temperature and low heating power input. Based on the present investigation, it is found that the present ultra-low temperature cascade refrigeration system is better to work at heating power input above 900 W and condensation temper- ature above 20 C. At suitable operating condition, the present ultra-low temperature cascade refrigeration system has been shown the capability of achieving ultra-low temperature 62 C continuously and stably. ª 2010 Elsevier Ltd and IIR. All rights reserved. Etude sur le blocage par la neige carbonique d’un syste `me frigorifique en cascade a ` tre ` s basse tempe ´ rature utilisant le CO 2 comme fluide actif Mots cle ´s : Neige carbonique ; E ´ coulement solide-gaz ; Tempe ´ rature tre `s basse ; Syste ` me frigorifique-cascade 1. Introduction CO 2 is abundant in nature and comes at low cost. As an environmentally benign fluid it has properties of zero Ozone depletion potential (ODE), low global warm potential (GWP), non-toxicity, non-flammability and inertness (ASHRAE Handbook, 2009). In addition, the thermodynamic and transport properties of CO 2 is also favorable for its using as a refrigerant in terms of its good heat transfer and large pressure drop at the critical pressure and temperature of CO 2 are 7.38 MPa (73.8 bar) and 31.1 C respectively (Liao and Zhao, 2002). Because of the above advantages, CO 2 fluid has received much attention in recent years in developing various energy conversion systems (Lorentzen, 1990, 1993, 1994; Neksa ˚ et al., 1998, 2002; Hafner et al., 1998; Liao and Zhao, 2002; Saikawa, 2004; Girotto et al., 2004; Cecchinato * Corresponding author. E-mail address: [email protected] (X.-D. Niu). www.iifiir.org available at www.sciencedirect.com journal homepage: www.elsevier.com/locate/ijrefrig international journal of refrigeration 34 (2011) 466 e475 0140-7007/$ e see front matter ª 2010 Elsevier Ltd and IIR. All rights reserved. doi:10.1016/j.ijrefrig.2010.11.001

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i n t e r n a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5

www. i ifi i r .org

ava i lab le at www.sc iencedi rec t .com

journa l homepage : www.e lsev ier . com/ loca te / i j re f r ig

Investigation of dry ice blockage in an ultra-low temperaturecascade refrigeration system using CO2 as a working fluid

Hiroshi Yamaguchi a, Xiao-Dong Niu a,*, Kenichi Sekimoto a, Petter Neksa b

aEnergy Conversion Research Center, Doshisha University, Kyotanabe, Kyoto, Japanb SINTEF Energy Research, No-7465 Trondheim, Norway

a r t i c l e i n f o

Article history:

Received 6 August 2010

Received in revised form

28 October 2010

Accepted 1 November 2010

Available online 13 November 2010

Keywords:

Dry ice

Solid-gas flow

Ultra-low temperature

Refrigeration system-cascade

* Corresponding author.E-mail address: [email protected]

0140-7007/$ e see front matter ª 2010 Elsevdoi:10.1016/j.ijrefrig.2010.11.001

a b s t r a c t

Dry ice blockage in a CO2-solidegas-flow-based ultra-low temperature cascade refrigera-

tion system is investigated experimentally by a visualization test and a system study of the

liquid CO2 blew into an expansion tube through a Throttle needle valve. The visualization

test shows that dry ice sedimentation occurs in low flow velocity and the dry ice formation

makes the heat transfer behavior of CO2 complicated. The sedimentation also occurs

at low condensation temperature and low heating power input. Based on the present

investigation, it is found that the present ultra-low temperature cascade refrigeration

system is better to work at heating power input above 900 W and condensation temper-

ature above �20 �C. At suitable operating condition, the present ultra-low temperature

cascade refrigeration system has been shown the capability of achieving ultra-low

temperature �62 �C continuously and stably.

ª 2010 Elsevier Ltd and IIR. All rights reserved.

Etude sur le blocage par la neige carbonique d’un systemefrigorifique en cascade a tres basse temperature utilisant leCO2 comme fluide actif

Mots cles : Neige carbonique ; Ecoulement solide-gaz ; Temperature tres basse ; Systeme frigorifique-cascade

1. Introduction

CO2 is abundant in nature and comes at low cost. As an

environmentally benign fluid it has properties of zero Ozone

depletion potential (ODE), low global warm potential (GWP),

non-toxicity, non-flammability and inertness (ASHRAE

Handbook, 2009). In addition, the thermodynamic and

transport properties of CO2 is also favorable for its using as

(X.-D. Niu).ier Ltd and IIR. All rights

a refrigerant in terms of its good heat transfer and large

pressure drop at the critical pressure and temperature of CO2

are 7.38 MPa (73.8 bar) and 31.1 �C respectively (Liao and

Zhao, 2002). Because of the above advantages, CO2 fluid has

received much attention in recent years in developing

various energy conversion systems (Lorentzen, 1990, 1993,

1994; Neksa et al., 1998, 2002; Hafner et al., 1998; Liao and

Zhao, 2002; Saikawa, 2004; Girotto et al., 2004; Cecchinato

reserved.

Fig. 1 e Schematic of the CO2 cascade refrigeration system.

Fig. 2 e P-h diagram for carbon dioxide.

i n t e rn a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5 467

et al., 2005; Rieberer, 2005; Stene, 2005; Zhang et al., 2005; Kim

et al., 2004, 2009).

In 2008, a cascade refrigeration systemusing CO2 solidegas

two-phase flow is introduced by Yamaguchi et al. (2008) and it

has been shown to be able to achieve the ultra-low tempera-

ture below the CO2 triple-point temperature of �56 �C. Thesystem is comprised of two CO2 refrigeration compression

cycles (Fig. 1), and the temperature below the triple-point is

realized by an expansion process of the liquid CO2 into the

dry ice and gas mixtures in an expansion tube. The reason

designing a cascade system is due to a low condensing

temperature necessary for dry ice condensation in expanding

process. As shown in Fig. 1, this system is composed of a low

temperature cycle (LTC) and a high temperature cycle (HTC),

respectively. In HTC, CO2 is cooled to �20 �C through

a compressor, two condensers, a needle expansion valve and

an evaporator. In LTC, onemore condenser is used and cooled

by the brine from the evaporator of HTC. Through three

condensers in HTC, CO2 is cooled to below �20 �C and then

expanded into the expansion tube to achieve the dry iceegas

two-phase flow and obtain an ultra-low refrigeration

temperature below the triple point. Brine cycle connects the

evaporator of HTC and the gas cooler of LTC. The refrigeration

principle of that system is illustrated in Fig. 2. The process of

1e2 represents the liquid CO2 expansion into the two-phase

flow in the dry ice region, which is below the CO2 triple point.

The ultra-low temperature refrigeration in the system is

achieved by the CO2 dry ice sublimating and absorbing heat

from outside of the expansion tube. This process is shown

in 2e3 in Fig. 2.

The feasibility study of the ultra-low temperature CO2

cascade refrigeration system has been performed by

Yamaguchi and Zhang (2009). As the dry ice sediment may

occurs to block the flow in the expansion tube and makes the

system operation failed, it is very necessary to investigate the

dry ice behaviors in the expansion tube for getting the opti-

mized system operation condition. For this aim, in the present

work, the behavior of liquid CO2 expanding into a horizontal

tube through the expansion valve is first studied by the visu-

alization test in a special open loop. Then, the dry ice sedi-

mentation effects on the cascade system are investigated at

different conditions.

The rest of the paper is organized as follows. In Sec. 2,

details of the visualization and dry ice sedimentation tests in

the cascade system are introduced. Sec. 3 is devoted to results

and discussions of the present study. A conclusion is given

in Sec. 4.

i n t e r n a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5468

2. Experiment details

2.1. Visualization test

In order to investigate the dry ice sedimentation in the

expansion tube in the CO2 cascade refrigeration system,

a special experimental set-up is built and is sketched in Fig. 3.

The experimental set-up is mainly comprised of a CO2

container, a pressure control valve, an expansion valve

(Throttle needle valve), a test section with visualization and

heating parts and an orifice flow meter. In order to get useful

information for the CO2 cascade refrigeration system (Fig. 1),

the test section is made with similar dimensions of the

expansion tube in LTC of the cascade refrigeration system.

The visualization part in the test section is a Pyrex circular

tube. The heating part in the test section is a SUS316 circular

tube rounded by sheath heater for sublimating the CO2 dry ice

particle in it. Although the loop is open one, both the visual-

ization and heating sections are set long enough so that the

solidegas flows with/without CO2 sublimation can be

observed. The visualization and heating tube has dimensions

of length 1.93 m (Visualization 0.59 m and heating 1.34 m),

thickness 0.0025m and inner diameter 0.04m. In order to keep

enough low temperature in the test section, a double cylinder

with vacuum thermal insulation structure is installed in the

test section to avoid heat transfer between the piping and the

ambient.

In the experiment, gaseliquid CO2 in the container is

pressurized into the gaseliquid separator through the pres-

sure control valve. In the separator, only liquid fluid is

Fig. 3 e Schematic of e

introduced to the expansion valve and the CO2 gas is recycled

to the container. The expansion valve is a needle-type

expansion valve with a maximum diameter of 30 mm.

Through the expansion valve, the liquid CO2 expands, and

the dry ice particles are produced by JouleeThomson effect. In

the heating section, the dry iceegas flow is heated under the

constant heat flux condition by the sheath heater so that

the dry ice sublimation occurs in the heating tube. After the

heating section, the gas CO2 flows through the orifice flow

meter and then is discharged outside. Visualization observa-

tion is achieved by using the high-speed video camera. All the

visualization tests are performed at pressure of 1.0 MPa and

temperature of �45 �C at the inlet of the tube.

2.2. Dry ice sedimentation test in CO2 cascaderefrigeration system

The performance of the CO2 cascade refrigeration system

based on the visualization results is also carried out. Here we

neglect the details of the CO2 cascade refrigeration system,

which can be referred to the work of Yamaguchi and Zhang

(2009). The performance study is based on the temperatures

and pressures measured at different positions in the system

(see Fig. 1). T-type thermocouples with an uncertainty of 0.1 �Cand pressure transmitter with an uncertainty of 0.2% are used

for the measurements. All measured data are transferred into

computer through distributor and data logger. The sample

data are obtained in every 5 s. In the pressure measurement,

each two pressures of the CO2 fluid are obtained at the inlet

(suction) and outlet (discharge) of the compressors in HTC and

LTC in the system, and for LTC they are denoted as P1 and P2

xperiment set up.

Fig. 4 e Schematic of test section of expansion tube in LTC.

i n t e rn a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5 469

and for HTC denoted as P10 and P20. In the temperature

measurement, each four temperatures of the CO2 fluid are

obtained respectively for HTC and LTC. In HTC, they are

suction temperature T10 at the compressor inlet, discharging

temperature T20 at the compressor outlet, condensing

temperature T30 at the outlet of the cooling water condenser,

and T40 at the evaporator outlet. In LTC, they are suction

temperature T1 at the compressor inlet, discharging temper-

ature T2 at the compressor outlet, condensing temperature T3

and sublimation temperature T4 before and after the expan-

sion valve (Throttle needle valve), respectively.

The details of the test section of the expansion tube in LTC

with temperature and pressure measuring positions is

sketched in Fig. 4. The test section is a copper-made hori-

zontal circular tube, which has an internal diameter of 0.04 m

and outer diameter of 0.045m. The length of the test section is

5.0 m. The inlet pipe and outlet pipe have a thickness of

0.0015 m and an outer diameter of 0.01588 m and 0.02222 m,

respectively. The heater used to heat the tube is silicon rubber

type heater with good water proof. The heater can be used in

a low-temperature environment until �80 �C.In the experiment, HTC is started first and cools the brine

of second subsystem. After the brine is fully cooled, the heater

rounded in the expansion tube in LTC is started to preheat the

tube. When the expansion tube in LTC reaches the prescribed

temperature, LTC is started. Then the two machine systems

should be made to operate simultaneously. The stable state of

the system operation is judged by observing whether T1 and

T4 in LTC converge into a confined range. In the present work,

pressure and temperature become steady around 3 h later

from starting working HTC and LTC. After that, average

pressure and temperature during 26-min period are adopted.

Fig. 5 e Pictures of CO2 solidegas two phase flows achieved

from liquid CO2 expansion throughout CO2 triple point.

(black region represents dry ice particles and white region

represents CO2 gas phase; pictures are taken at 13500 fps

by high-speed camera).

3. Results and discussions

3.1. Visualization test

The visualization test is carried out at the two opening

conditions of 15 mm and 10 mm of expansion valve (corre-

sponding high and low inlet flow velocities of 2.5 m/s and

0.78 m/s, respectively) with heat input 1200W. Fig. 5(a) and (b)

show the pictures of the solidegas two phase fluids at two

respective opening conditions of 15 mm and 10 mm of the

expansion valve taken by a high-speed camera with 13500 fps.

In Fig. 5, black and white regions represent the dry ice parti-

cles and CO2 gas, respectively. The dry iceegas two phase flow

in the expansion tube can be justified examining the

measured pressure inside the visualization section. At the

opening conditions of 15 mm and 10 mm, the measured

pressures near the inlet of the expansion tube are 0.163 MPa

and 0.186 MPa, respectively. Both values are below the triple-

point pressure of CO2. Since the expansion process through

the needle valve to the test section is adiabatic by the Jou-

leeThomson effect, it is confirmed that there is no liquid

existing inside the test section.

The particle distribution is almost uniform at the expan-

sion valve condition of 15 mm (Fig. 5(a)). At this high flow

velocity, the flow is considered to be turbulent and thus

helping the uniform distribution of the dry ice formation in

Fig. 7 e The calculated Nusselt number of CO2 flow at the

inner wall varying along the test section at different flow

velocities.

i n t e r n a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5470

the expansion tube. From the visualization results, the

diameters of most dry ice particles are estimated about

1.0 mm. By taking average of 100 sample particles, the mean

particle size is measured to be 1.023 mm. When the opening

condition of the needle valve is reduced to 10mm, as shown in

Fig. 5(b), it is observed that a sedimentation phenomenon

occurs and larger particles form in the expansion tube. The

opening size of the needle valve has an important effect to the

dry ice sedimentation. With the JouleeThomson effect, high

concentration and large size of the dry ice particles are

expected to form after the needle valve at small opening size.

This is because the small opening size causes the low flow

speed after the needle valve. As a consequence, the small-size

dry ice particles more easily collide and stick with each other

to form large-size particles inside the expansion tube and the

inlet tube connected to the needle valve. On the other hand,

the movement of large-size particles is more difficult to

overcome the drag forces inside the fluid and on the tube wall

than at high flow speed.

The effects of the flow velocity on the dry iceegas flow

behavior and the heat transfer characteristics can be

demonstrated quantitatively Figs. 6 and 7, respectively, which

show themeasured inner-wall temperature TW and calculated

Nusselt numberNu (¼Qw/plL(Tw�Tb), Qw is the input heat flux,

l the thermal conductivity of CO2 gas, L the heating length of

the test section, Tb the bulk temperature evaluated based on

the inlet temperature and the input heat flux Qw ) of CO2 flow

varying along the test section at different flow velocities. In

order to identify the range of the dry iceegas two phase flow

region, the CO2 triple-point temperature line Ttr is also plotted.

As shown in Fig. 6, with the flow velocity increasing, that is,

the opening condition of the expansion valve becoming larger,

the increasing rate of the wall temperature reduces. By

comparing with the triple-point temperature, it is found that

the region of the dry iceegas flow near the inlet of the test

section increases along the test section with the inlet flow

velocity increasing. The heat transfer behavior of the flow in

this dry iceegas region becomes complicated as shown in

Fig. 6 e The measured temperature of CO2 flow at the inner

wall varying along the test section at different flow

velocities.

Fig. 7. In this region, the Nusselt number has a rapid decrease

and follows a slightly quick rising and reducing. After this

region, the flow becomes pure gas flow as the dry ice particles

have sublimated, and the Nusselt number gently decreases to

a constant value.

Increasing the heat input is expected to reduce the dry

iceegas flow region by increasing the dry ice particle subli-

mation. This can be seen in Fig. 8 by plotting the Nusselt

number variation along the test section at different input heat

fluxes (Qw ¼ 464.2, 1393, 2321, 3249 and 4117 [W/m2]) and the

fixed inlet flow velocity of 1.755 m/s. As shown in Fig. 8, the

Nusselt number increases in the inlet region of the test section

but the rapid varying range of it reduces, implying the dry

iceegas two-phase flow region reduces. On the other hand,

Fig. 8 e The calculated Nusselt number of CO2 flow at the

inner wall varying along the test section at different input

heat fluxes.

Fig. 10 e Behavior of measured condensing and local

pressures in test section at expansion valve opening

10 mm, condensing temperature L20 �C and heat input

900 W.

i n t e rn a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5 471

increasing the input heat fluxes, the Nusselt number does not

change in the gas flow region because the inner wall

temperature also increases.

3.2. Dry ice sedimentation test in CO2 cascaderefrigeration system

The behavior of dry ice blockage phenomenon in the test

section of the cascade system can be detected by examining

the suction and discharge pressures before and after the

compressor, condensing pressure before the expansion valve

and pressures in the test section in LTC varying with the time.

In the following, results based on two typical conditions, at

which dry ice sedimentation and blockage occur in the

expansion tube in LTC of the cascade system, are presented.

The suction and discharge pressure behaviors before and

after the compressor in LTC at the expansion valve opening in

10mm, the condensing temperature of�20 �C and the heating

power input 900 W are described in Fig. 9. As shown in Fig. 9,

the discharge pressure has a sudden rise while the suction

pressure slightly decreases during the time of 120e180 min.

The change of the discharge and suction pressures is caused

by the dry ice accumulating in a large amount in the inlet

small tube right after the expansion valve (Fig. 4) and blocking

the liquid CO2 flowing. With the time going longer, due to the

dry ice particles accumulated in the inlet small tube blew into

the expansion tube, the discharge pressure decreases. This

finding can be confirmed in Fig. 10, which shows the behavior

of measured condensing pressure and those at four position

along the test section (see Fig. 4) in the time period of

120e200 min for the expansion valve opening in 10 mm, the

condensing temperature of �20 �C and the heating power

input 900 W. As shown in Fig. 10, the condensing pressure

rises remarkably in the time range of 150e170 min and

decreases suddenly after, and the local pressures P1, P2, P3 and

P4 at four positions of the test section vary slightly within the

operation time, indicating clearly that the blockage of dry ice

Fig. 9 e Measured suction and discharge pressures in LTC

vary with time (the expansion valve opening in 10 mm, the

condensing temperature of L20 �C and the heating power

input 900 W).

occurs in the inlet small tube right after the expansion valve

and this blockage disappears when the dry ice particles are

blew into the expansion tube. It may argue that the blockage

of this test occurs inside the expansion valve. Since the CO2

flow in the test loop is found continuously running, this

argument is eliminated because the system operation will

breakdown otherwise.

Fig. 11 displays the suction and discharge pressure

behaviors before and after the compressor in LTC at the

expansion valve opening in 15 mm, the condensing temper-

ature of �25 �C and the heating power input 1200 W. In this

figure, both of the suction and discharge pressures are

Fig. 11 e Measured suction and discharge pressures in LTC

vary with time (the expansion valve opening in 15 mm, the

condensing temperature of L25 �C and the heating power

input 1200 W).

Fig. 12 e Behavior of measured condensing and local

pressures in test section at expansion valve opening

15 mm, condensing temperature L25 �C and heat input

1200 W.

Fig. 13 e Variations of local pressure and wall temperature with

times. (a) Expansion valve opening in 15 mm. (b) Expansion va

i n t e r n a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5472

observed to slightly decrease in the time period of

120e150 min, suggesting that the dry ice particles partly

sediment on the wall of the expansion tube and change the

CO2 solidegas two-phase flow behaviors inside it. This can

also be confirmed by measuring condensing pressure and

those at four positions along the test section. Fig. 12 shows the

behavior of measured condensing pressure and those at four

position along the test section (see Fig. 4) in the time period of

120e150 min for the expansion valve opening in 15 mm, the

condensing temperature of �25 �C and the heating power

input 1200W. As shown in Fig. 12, the local pressures P1, P2, P3and P4 have a sequential rapid rise and decrease, and the

condensing pressure varies little within the plotted operation

time. This observation illustrates that the sedimentation of

dry ice occurs on the wall of the expansion tube and was blew

to downstream gradually by accompanying sublimation

processes. When all the dry ice particles sublimated, the local

pressures go down.

The detailed dry ice sedimentation inside the test section

can be illuminated in Fig. 13 with displaying the variations of

local pressures and temperatures at four typical blocking

times at the expansion valve opening in 15 mm, the

condensing temperature of �25 �C and the heating power

input 1200 W. The measured positions of pressures and

the dry ice sedimentation inside the test section at different

lve opening in 10 mm.

Expansion valve opening in 15mm Expansion valve opening in 10mm

Heat input [W]

P1[M

Pa]

T3T3T3

=-15=-20=-25

600 900 1200 1500 18000.35

0.4

0.45

0.5

0.55

0.6

Heat input [W]

P1[M

Pa]

T3T3T3

=-15=-20=-25

600 900 1200 1500 18000.35

0.4

0.45

0.5

0.55

0.6a b

Fig. 14 e Variations of measured evaporating pressure of LTC with heat input at three condensation temperatures and two

expansion valve opening.

i n t e rn a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5 473

temperatures are also given in the illuminated figures. The

sedimentation of dry ice first appears in the inlet region of the

test section, and then gradually moves to downstream with

the time going. Before the dry ice sediment point, the pressure

and temperature rise due to the flow entrapped. The large

temperature variation near the outlet of the test section

observed in the figure is mainly due to the flow rapidly

shrinking to the tube connected to the compressor.

Fig. 14(a) and (b) plot the variations of the measured steady

state suction pressure P1 in LTC with the heating power input

at three condensing temperatures T3 of �15 �C, �20 �Cand�25 �C for two opening conditions of 10mmand 15mmof

the expansion valve, respectively. It is found in both Fig. 14(a)

and (b) that, except at low heating power input of 900 W, the

suction pressure generally decreases with the condensing

temperature and the heating power input decreasing. At the

heating power input of 900 W, the suction pressure at

condensing temperature of T3 ¼ �25 �C increases for the

expansion valve opening in 15 mm (Fig. 14(a)), implying the

sedimentation of dry ice may occurs to partly block the flow.

For the expansion valve opening in 10 mm as shown in Fig. 11

(b), due to the serious blockage phenomenon occurring in the

inlet of the expansion tube at the heating power input of

900 W, the evaporating pressure cannot be measured.

Fig. 15 e Variations of measured CO2 pressures of HTC and

LTC with time. Temperature at HTC. Temperature at LTC.

3.3. Performance of the CO2 cascade refrigeration systemat an optimized operating condition

Based on the above investigations, it is found that the present

ultra-low temperature cascade refrigeration system is better

to work at heating power input above 900W and condensation

temperature above �20 �C. Fig. 15 shows the measured

suction and discharge pressures in HTC and LTC varying with

time at the heating power input of 1000 W and the opening of

the expansion valve of 15 mm, and Fig. 16 plots the measured

suction, discharge and condensing temperatures in HTC and

LTC varying with time at the same conditions. As shown in

Figs. 15 and 16, the measured pressures and temperatures

quickly reach in a certain value range after started, and it

takes about 180 min for the suction and discharge tempera-

tures to become stable. In HTC, the discharge pressure is

P20 ¼ 6.60 MPa, the discharge temperature is T20 ¼ 136 �C, thecondensing temperature is T30 ¼ 25.1 �C, the suction pressure

is P10 ¼ 1.65 MPa and the suction temperature is T10 ¼ �15 �C.The oscillation of the discharge pressures and temperatures

shown in Figs. 15 and 16 aremainly due to the automatic valve

opening and closing in cooling tower side leading the

temperature variations of cooling water in the heat

exchangers. By comparing the P-h diagram shown in Fig. 2, it is

confirmed that, in HTC, the CO2 fluid state is of gas state at the

compressor inlet and outlet, of supercritical state at the outlet

of the condensers, and of liquid-gas two-phase state at the

inlet of the evaporator. In LTC, the discharge pressure is

P2 ¼ 2.20 MPa, the discharge temperature is T2 ¼ 136 �C, the

Fig. 16 e Variations of measured temperatures with time.

i n t e r n a t i o n a l j o u r n a l o f r e f r i g e r a t i o n 3 4 ( 2 0 1 1 ) 4 6 6e4 7 5474

condensing temperature is T3 ¼ �17 �C, the evaporator outlet

temperature is �62 �C, and the suction pressure and temper-

ature of the compressor are P1 ¼ 0.36 MPa and T1 ¼ �30 �C,respectively. Based on P-h diagram in Fig. 2 again, the CO2 fluid

state is confirmed to be of gas state at the compressor inlet

and outlet, of liquid state at the inlet of the expansion valve

and of solidegas two-phase state at the inlet of the test

section. Based on Figs. 15 and 16, it is certain that the CO2

cascade refrigeration system could continuously and stably

realize the dry ice-solid two phase flow and an ultra-low

temperature of �62 �C in the expansion tube.

4. Conclusions

Dry ice blockage in a CO2-solidegas-flow-based ultra-low

temperature cascade refrigeration system is investigated

experimentally by a visualization test and a system study of

the liquid CO2 blew into an expansion tube through a Throttle

needle valve. The visualization test shows that dry ice sedi-

mentation occurs in low flow velocity and the dry ice forma-

tionmakes the heat transfer behavior of CO2 complicated. The

investigation with the cascade system to simulate the dry

iceegas two-phase flow through the expansion valve shows

that the dry ice flow blockage in the expansion tube has the

following characteristics:

Dry ice blockage occurs in the small inlet tube right after

the expansion valve at lowmass flow rates, low condensation

temperature and low heating power input. When the mass

flow rate increases, blockage occurs in the expansion tubes

due to the dry ice particles partly accumulating on the wall of

the expansion tube. Based on the system performance

investigation, the blockage in the small inlet tube may be

eliminated by adding a heater on that or increasing the

opening conditions, and the blockage in the expansion tube

can be avoided by increasing the input heat fluxes and the

opening condition of the expansion valve as well.

Moreover, it is found that the present ultra-low tempera-

ture cascade refrigeration system is better to work at heating

power input above 900 W and condensation temperature

above �20 �C. At a suitable operating condition, the present

ultra-low temperature cascade refrigeration system has

been shown the capability of achieving ultra-low tempera-

ture �62 �C continuously and stably.

Acknowledgements

This study was supported by the Academic Frontier Research

Project on ‘Next Generation Zero-emission Energy Conversion

System’ of Ministry of Education, Culture, Sports, Science and

Technology., and forms a part of the CREATIV project, per-

formed under the strategic Norwegian research program

RENERGI. The author(s) acknowledge the partners: Danfoss,

FHL, Hydro Aluminium, John Bean Technology, Norske Skog,

REMA1000, Systemair, TINE, and the Research Council of

Norway (195182/S60) for their support.

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