inorganics data package · 2020. 12. 27. · inc. • 2425 new/holland pike • lancaster, pa...

Data Package

Contract Lab Program Data Packagefor

DuPont Environmental Remediation Sv

INORGANICS DATA PACKAGE

Christina Tidal StudyGrab Water Samples

Collected on 12/29/92, 12/30/92 by BCLLI Sample No. 1911840-1911847, 1912267-1912280

Lancaster Laboratoriesr Where quality is a science.

Lancaster Laboratories. Inc. • 2425 New/Holland Pike • Lancaster, PA 17601-5994 717-656-2301 • Fax-717-656-2681 2262 3/1/91

SR3I955U

TABLE OF CONTENTS

A. Case Narrative...............................................1

B. Sample Data.................................................. 5

C. Quality Control Data........................................ 26

D. Verification of Instrument Parameters....................... 49

E. Preparation and Run Logs.................................... 64

F. Raw Data.................................................... 9 3

1. ICP Data............................................ 94

2. Furnace Data.......................................290

3. Mercury Data....................................... 379

4. Extraction/Distillation/Digestion Logs.............384

G. Chain-of-Custody Record....................................389

AR319555

CASE NARRATIVE

AR31955&1

Lancaster LaboratoriesWhere quality is a science.

CASE NARRATIVE FOR INORGANICS

Laboratory Name: Lancaster Laboratories

SDG Number: CRT04

Date Received: 12/31/92

Analysis;All samples were digested a second time for sodium due to

the laboratory control sample being out of the control limits.

Explanatory Notes;The inappropriate error flag, % Recovery Failed,

Repeat by Standard Additions, is due to a manufacturer's(Varian) software error. The software is designed to followthe analysis protocol for USEPA Contract Laboratory ProgramILM01.0. Following this protocol, method of standard additionsis not required for samples demonstrating sample absorbance orconcentration less than 50% of the spike absorbance orconcentration; however, the Varian software prints this flag,regardless of sample absorbance or concentration, wheneverthe percent recovery is below 85% or above 115%.

Varian has been informed of this problem and hascommunicated that the problem will be resolved in a futuresoftware revision. The software is needed to operate theinstrument and to control the automatic spiking function ofthe autosampler. Since the software will not permit thiserror to be disabled, data that demonstrates this error willbe manually corrected on the raw data by the analyst.

Calibration Standards;Instrument calibration standards are prepared monthly from stock

solutions purchased from Spex or Baker chemical.Total ICP integration time is 24 seconds.

Case Narrative reviewed and approved by:Date

Susan B./ShorterQuality Assurance Specialist I

AR3I9557Lancaster Laboratories, Inc. • 2A25 New Holland Pike, Lancaster, Fft 17601-5994 • 717-656-2301 • Fax:717-656-2681

raro

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Name: LANCASTER LABORATORIES Contract: __

Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_

SOW No.: 3/90_

EPA Sample No. Lab Sample ID_BRIMT______ __1911840_____BRMTF______ __1911841_____CRMDF_______ __1912280____CRMID 1912279FBUNF________ __1912276~JASHD________ __1912270""JASHT_______ __1912269""JASHTD______ __1912272""JASHTS_______ __1912271""JSBDF________ __1912273""JSLTF________ __1912275""JSLTI________ _1912274"~MAHTF_______ __1911845""MAMTF_______ __1911843""MANHT_____ __i9ii844~"MANMT_____ _1911842"RDLOT_______ __1912267"~RDLTF_______ __1912268"~ROALT________ __1911846""ROLTF , 19 us 47"

ICP interelement corrections applied ? Yes/No YES

e ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No NO_

Comments:___THE_REPORTED_VALUE_IS_ESTIMATED_FOR_IRON_BECAUSE_OF_THE_PRESENCE_OF_

INTERFERENCE.

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.Signature; .4 • ^/,-t /•) vJ/t.C!;~t~L i Name; S/ ^ n /?.. ________

Date: TV , >.. c, : o / 5~ / 99 _______ Title ; rfu A j< 'J-u J~fS?,i/, #, ?,-s < ?Ss's ' -.rX 7~—— ^_, , ^COVER PAGE - IN IIMO2 . 1

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: LANCASTER__LABORATORIES__ Contract: _________

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_SOW No.: 3/90_

EPA Sample No. Lab Sample ID_SBMIT_______ __1912277____SBMTF 1912278

Were ICP interelement corrections applied ? Yes/No YES

Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No N0_

Comments:___THE_REPORTED_VALUE_IS_ESTIMATED_FOR_IRON_BECAUSE_OF_THE_PRESENCE_OF_

INTERFERENCE.

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.Signature; x${ .<i3u>i\. X?. XLSLCTIA ,LJ ___ Name; ••O cTa:/? /-5, Q/,?£/-";4v-

Date: /5". //'ffj _____ Title: Jut<. t<- XV_____ _, *-' COVER PAGE - IN ILMO2 . 1

SR3I9559

SAMPLE DATA

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sits

Lancaster LaboratoriesWhere quality is a science.

o<\Sample Reference List for SDG # CRT04

with a Package Type of CLPI

LabSample SampleNumber Code Client Sample Description

,.-1911840 BRIMT James Street Bridge Mid Tide Grab Water Sample' 1911841 BRMTF James street Bridge Mid Tide Filtered Grab Water1911842 MANMT Churchmans Road Mid Tide Grab Water Sample

r 0 1911843 MAMTF Churchmans Road Mid Tide Filtered Grab Waterj/i :/1911844 MANfTT Churchmans Road High Tide Grab Water Sample//\1911845 MAHTFJ Churchmans Road High Tide Filtered Grab Water

' 1911846 ROALT Churchmans Road Low Tide Grab Water Samplet_iai 184-7— ROLTF Churchmans Road Low Tide Filtered Grab Water1912267 RDLOT Churchmans Road Low Tide Grab Water Sample1912268 RDLTF Churchmans Road Low Tide Filtered Grab Water1912269 JASHT James Street Bridge High Tide Unspiked Grab Water1912270 JASHD James Street Bridge High Tide Unspiked Filtered1912271JASHTT" James street Bridge High Tide Matrix Spike Grab

\ 1912272 JASHT James Street Bridge High Tide Duplicate Grab*"' 1912273 JSBDF James Street Bridge High Tide Duplicate Filtered

1912274 JSLTI James Street Bridge Low Tide Grab Water Sample1912275 JSLTF James Street Bridge Low Tide Filtered Grab Water1912276 FBUNF Field Blank Grab Water Sample1912277 SBMIT James Street Bridge Mid Tide Grab Water Sample

•- 1912278 SBMTF_ James Street Bridge Mid Tide Filtered Grab Water1912279 CRMID Churchmans Road Mid Tide Grab Water Sample1912280 CRMDF Churchmans Road Mid Tide Filtered Grab Water

AR3I9565Larraster Laboratories, Inc. • 2425 New Holland Pike, Lancaster, FA 17601-5994 • 717-656-2301 • Fax:717-656-2681

iSro

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET

Name: LANCASTER LABORATORIES Contract:BRIMT

Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_

Matrix (soil/water): WATER Lab Sample ID: 1911840Level (low/med): LOW_ Date Received: 12/30/92

% Solids: ___0

Concentration Units (ug/L or mg/kg dry weight): UG/L_

GAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

26622.01.0

56.61.03.0

227005.05.05.0

10001.6887090.30.108.052801.0

11.0148002.06.0101

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Color Before: COLORLESS Clarity Before: CLEAR_ Texture:Color After: COLORLESS Clarity After: CLEAR_ Artifacts:

Comments:

FORM I - INILM02.1

6

flR3i9566

U.S. EPA - CLP


BRMTFLab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_


% Solids: ___0


GAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

57.022.01.045.91.03.0

226005.05.05.076.61.0885077.70.108.046601.011.0161002.06.056.9

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Color Before: COLORLESS

Color After: COLORLESSComments :

Clarity Before: CLEAR Texture:

Clarity After: CLEAR Artifacts:

FORM I - INILMO2.1

..1. 7

SR3I9567

U.S. EPA - CLP


Name: LANCASTER LABORATORIES Contract:MANMT

Lab Code: ______ Case No.: _____ SAS No.: _____ SDG No.: CRT04_


% Solids: ___0Concentration Units (ug/L or mg/kg dry weight): UG/L_

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

38722.01.061.01.03.0

131005.05.05.015901.156601480.108.028501.011.0150002.06.074.7

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Comments :

Clarity Before: CLEAR Texture:Clarity After: CLEAR Artifacts:

FORM I - INILM02.1

flR3!9568

U.S. EPA - CLP


MAMTFLab Name: LANCASTER LABORATORIES Contract:


Matrix (soil/water): WATER Lab Sample ID: 1911843__Level (low/med): LOW_ Date Received: 12/30/92

% Solids: ___0


GAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentration57.022.01.032.61.03.0

119005.05.05.01831.0

461027.00.108.027701.011.0515002.06.012.4

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Comments :



FORM I - INILMO2.1

fiR3i9569

L<ro

U.S. EPA - CLP


Name: LANCASTER LABORATORIES Contract:MANHT



% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

39222.01.0

62.61.03.0

225005.05.05.011401.0884098.40.108.046601.0

11.0172002.06.0105

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Comments :



FORM I - INILM02.1

18

U.S. EPA - CLP


Lab Name: LANCASTER LABORATORIES Contract:MAHTF

Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.

Matrix (soil/water): WATER Lab Sample ID: 1911845_Level (low/med): LOW_ Date Received: 12/30/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentr at ion

57.022.01.0

47.21.03.0

211005.05.05.0

59.31.0833088.30.108.044401.0

11.0163002.06.0111

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FORK I - INIJLM02.1

16flR3i9571

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _____________

ROALTName: LANCASTER LABORATORIES Contract:


Matrix (soil/water): WATER Lab Sample ID: 1911846Level (low/med): LOW_ Date Received: 12/30/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration57.022.01.041.21.03.0

134005.05.05.03491.057101450.108.028501.011.0317002.06.044.1

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Color After: COLORLESS Clarity After: CLEAR_ Artifacts:Comments:

FORM I - INILMO2.1

UR3I9572

U.S. EPA - CLP


ROLTFLab Name: LANCASTER LABORATORIES Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1911847__

Level (low/med): LOW__ Date Received: 12/30/92

% Solids: ___0Concentration Units (ug/L or mg/kg dry weight): UG/L_

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentration107022.01.066.11.03.0

132005.05.05.029103.357902180.108.028301.011.0312002.06.071.0

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FORM I - INILM02.1

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U.S. EPA - CLP


RDLOTName: LANCASTER LABORATORIES__ Contract:


Matrix (soil/water): WATER Lab Sample ID: 1912267

Level (low/med): LOW_ Date Received: 12/31/92

% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

59822.01.054.11.03.0

133005.05.05.017801.55630179

0.108.027401.011.0233002.06.043.2

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Comments :



FORM I - INILM02.1

£0ftR3i957U

U.S. EPA - CLP


RDLTFLab Name: LANCASTER LABORATORIES Contract:


Matrix (soil/water): WATER Lab Sample ID: 1912268__

Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

57.022.01.0

39.51.03.0

127005.05.05.02371.05380143

0.108.026001.0

11.0246002.06.0

30.0

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Comments :


FORM I - INILM02.1

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U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _______

JASHTName: LANCASTER LABORATORIES__ Contract:

Lab Code: _____ Case No.: _____ SAS No.: ______ SDG No.: CRT04.



% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentrat i on28722.01.069.51.03.0

216005.05.05.0

12301.0856089.90.108.045201.011.0143002.06.595.8

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Comments :



FORM I - INILMO2.1

12flR3!9576

U.S. EPA - CLP


JASHDLab Name: LANCASTER LABORATORIES Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912270__Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentration57.022.02.9

51.51.03.0

219005.05.05.091.41.0862077.70.108.045201.011.0146002.06.0

82.5

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Comments :


FORM I - INILMO2.1

._£--i.

AR3I9577

L!TD

U.S. EPA - CLP


JSBDFName: LANCASTER LABORATORIES__ Contract:





CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

57.022.01.048.01.03.0

215005.05.05.01541.0854070.90.108.044101.011.0145002.06.058.1

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Comments :



FORM I - INILM02.1

AR3I9578

U.S. EPA - CLP


JSLTILab Name: LANCASTER LABORATORIES Contract:




CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6


Concentration16922.01.0

51.51.03.0

209005.05.05.09951.0

819099.70.108.060301.0

11.0173002.06.0104

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Comments :



FORM I - IN.ILM02.1

AR319579

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET __ _______

t j S L T FName: LANCASTER LABORATORIES Contract:





CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

57.022.01.0

57.51.03.0

220005.05.05.01181.0867091.60.108.046901.011.0181002.07.268.4

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Comments :



FORM I - INILM02.1

AR3I9580

U.S. EPA - CLP

1INORGANIC ANALYSES DATA SHEET

Lab Name: LANCASTER LABORATORIES Contract:

EPA SAMPLE NO.


Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumcobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration

57.022.0

r 1.0HI. 21.03.06495.05.05.07.01.01251.00.108.03111.011.07322.06.04.0

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FORK I - IN .ILMO§.1

flR3i958l

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ___

SBMITName: LANCASTER LABORATORIES Contract:





CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

20222.01.0

54.11.03.0

211005.05.05.09471.08340107

0.108.042401.0

11.0166002.06.0100

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Comments :



FORM I - INILM02.1

244R3I9582

U.S. EPA - CLP

1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _____________

Lab Name: LANCASTER LABORATORIES Contract:SBMTF

Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912278__



CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

57.022.01.0

45.51.03.0

223005.05.05.01191.0869094.20.108.049001.0

11.0161002.06.0

54.9

C

UUUBUU

UUU

U

UUBUU

UU

Q

E

M




Comments :



FORM I - INILM02.1

25

flR3i9583

Kro

U.S. EPA - CLP


CRMIDName: LANCASTER LABORATORIES__ Contract:




% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

38422.01.0

61.01.03.0

149006.55.05.022201.06280173

0.108.032501.0

11.0190002.06.0

43.2

C

UUBUU

BUU

U

UUBUU

UU

Q

E

W /

M


r

Color Before: COLORLESS Clarity Before: CLEAR_ Texture:Color After: COLORLESS Clarity After: CLEAR_ Artifacts:

Comments:

FORM I - IN' ILM02.1

3

U.S. EPA - CLP


Lab Name: LANCASTER LABORATORIES Contract:CRMDF



Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

57.022.01.0

41.21.03.0

134005.05.05.03501.05720138

0.108.027101.011.0189002.06.0

20.3

C

UUuBU'U

UUU

U

UuBUU

UU

Q

E

M


e.u



Comments :


FORM I - INILM02.1

8

QUALITY CONTROL DATA

flR319586

U.S. EPA - CLP

2AINITIAL AND CONTINUING CALIBRATION VERIFICATION


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Initial Calibration Source: LLI_______Continuing Calibration Source: LLI_______

Concentration Units: ug/L

AnalyteAluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper _____IronLeadMagnesiumManganeseMercuryNickel__ __PotassiumSeleniumSilverSodiumThalliumVanadium_ZincCyanide

Initial CalibrationTrue Found %R(1)25000.05000.050.0

5000.0500.05000.050000.05000.01000.05000.05000.020.0

25000.05000.0

2.510000.050000.0

20.0500.0

50000.040.0

2000.05000.0

24945.005156.1053.70

4983.70484.575064.6050853.005141.10994.405071.205160.3020.75

24340.005160.90

2.5410199.0051207.00

20.05507.12

50117.0042.40

2062.705142.10

99.8103.1107.499.796.9101.3101.7102.899.4101.4103.2103.897.4103.2101.6102.0102.4100.2101.4100.2106.0103,1102.8

Continuing CalibrationTrue Found %R(1) Found %R(1)

25000.05000.050.0

5000.0500.05000.050000.05000.01000.05000.05000.020.0

25000.05000.0

1.010000.050000.0

20.0500.0

50000.040.0

2000.05000.0

25222.005175.4050.67

4988.90488.665108.1050869.005199.80991.865131.905219.7020.06

24650.005209.20

0.9810289.0050953.00

20.42515.73

50659.0041.40

2057.505194.80

100.9103.5101.399.897.7102.2101.7104.099.2102.6104.4100.398.6104.298.0102.9101.9102.1103.1101.3103.5102.9103.9

24998.005104.0051.03

4997.90483.715073.4050512.005157.10989.925112.105155.9020.53

24327.005163.90

0.9810188.0050599.00

19.38509.63

49024.0042.20

2066.905140.90

100.0102.1102.1100.096.7101.5101.0103.199.0102.2103.1102.697.3103.398.0101.9101.296.9101.998.0105.5103.3102.8

M

f-PFPPP_PiFPP~CVPPFPPFPP~NR

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IN

ILM02.1

-•;•« £7flR3l9587

U.S. EPA - CLP




Initial Calibration Source: LLI_______

Continuing Calibration Source: LLI_______


AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalcium^ChromiumMpalt,_ppperTironLeadMagnesiumManganeseMercuryNickel.. ___PotassiumSelenium_SilverSodiumThalliumVanadiumZincCyanide _

Initial CalibrationTrue Found %R(1)

40.0 42.80

————

107.0


25000.05000.0

50.05000.0500.0

—— 5000.050000.05000.01000.05000.05000.0

20.025000.05000.0

1.010000.050000.0

20.0500.0

50000.040.0

2000.05000.0

25342.005213.1049.25

5106.80490.495136.3051833.005116.801008.505175.005219.9020.20

24898.005224.50

0.9610310.0051559.00

18.70512.85

50334.0043.40

2115.005199.00

101.4104.398.5

102.198.1

102.7103.7102.3100.8103.5104.4101.099.6104.596.0

T03.1103.193.5

102.6100.7108.5105.8104.0

25843.005270.7050.37

4989.70498.53

"5206.4050588.005347.50991.175257.705325.2020.79

24644.005309.30

0.9410485.0050670.00

19.14525.05

49960.0043.80

2068.605286.00

103.4105.4100.799.899.7

104.1101.2107.099.1

105.2106.5104.098.6

106.294.0

104.8101.395.7

105.099.9

109.5103.4105.7

M

P~PFPPP~PPPP~PFPPCVPPFPPFPPNR

(l) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115


ILM02.1

SR3I9588

U.S. EPA - CLP


Lab Name: LANCASTER LABORATORIES__ Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Initial Calibration Source: LLI_______



Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobalt __CopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide



50.0

5000.0

___ 20.0

20.0

40.0

48.72

5291.30

___ 21.07

20.30

43.70

_ _ _ — _ — _

97.4

105.8

105.4

101.5

109.2

48.20

___ 21.28

20.72

42.00

_96.4

106.4

103.6

105.0

M

NRNRFNRNRNRNR

39FNKNRNRNRNRFNRNRFNRNRNR

»



ILMO2.1

HR3I9589

U.S. EPA - CLP



Lab Code: ____ Case No.: ____ SAS No.: _______ SDG No.: CRT04_Initial Calibration Source: LLI_______



Analyte

AluminumAntimonyArsenic _BariumBerylliumCadmiumCalciumChromium•bait•bperxronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide _

Initial CalibrationTrue Found %R ( 1 )

20.0 20.67

————

103.4


20.0

40.0

19.64

41.50

98.2

103.8

18.99

————

95.0

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRFNRNRNR



ILM02 . 1

AR3I9590

U.S. EPA - CLP




Initial Calibration Source: LLI_______Continuing Calibration Source: LLI_______


Analyte

AluminumAntimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide



20.0 20.26

————

101.3

————

20.44

————

102.2

M

NRNRNRNRNRNRNRNR|mNWNRNRNRNRNRNRFNRNRNRNRNRNR



ILM02.1

HR31959I

U.S. EPA - CLP

2BCRDL STANDARD FOR AA AND ICP

Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_

AA CRDL Standard Source: LLI________

ICP CRDL Standard Source: LLI_______


Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium^ alt| K>erITonLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

CRDL £

True

10.0

3.0

0.2

5.0

10.0

Standard fc

Found

11.37

2.66

0.16

4.92

11.90

>r AA

%R

113.7

88.7

80.0

98.4

119.0

True

100.0

100.0

CRDL StarInitialFound

105.16

109.69

idard i%R

105.2

109.7

:or ICPFina]

Found

97.64

105.35

L%R

97.6

105.4

o,\vFORM II (PART 2) - IN

ILMO2.1

' "32HR3I9592

U.S. EPA - CLP

26CRDL STANDARD FOR AA AND ICP



AA CRDL Standard Source: LLI________

ICP CRDL Standard Source: LLI


Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

CRDL £

True

5.0

10.0

Standard fcFound

4.87

10.40

>r AA

%R

97.4

104.0

True

120.0

10.010.0

50.0

30.0

80.0

20.0

40.0


119.13

8.889.02

50.09

30.93

70.37

18.63

40.32

idard 1%R

99.3

88.890.2

100.2

103.1

88.0

93.2

100.8

:or ICPFina]

Found

129.60

8.879.92

50.54

31.78

72.26

20.79

41.91

%R

108.0

88.799.2....

4101 .•™

105.9

90.3

104.0

104.8


• ILM02.1

IT' 33

SR3I9593

U.S. EPA - CLP

2BCRDL STANDARD FOR AA AND ICP



AA CRDL Standard Source:ICP CRDL Standard Source: LLI


AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium^ •alt^ HBerronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

CRDL £

True

Standard fc

Found

ar AA

%R True

20.0


19.72

idard J

%R

98.6

for ICPFina]

Found

22.58

L%R

112.9

j \ • FORM II (PART 2) - IN

VO ILMO2.1

*•*._?•

. , . 24AR3I959I*-

U.S. EPA - CLP

3BLANKS



Preparation Blank Matrix (soil/water): WATERPreparation Blank Concentration Units (ug/L or mg/kg): UG/L_

AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_ _____PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

InitialCalib.Blank(ug/L) C

57.022.01.34.01.03.0

-73.5——— 5.0 ——

5.08.2

-44.41.0

-80.71.00.18.0

132.01.0

11.065.02.06.04.0

UUBUUUBUUBBUBUUUuuuuuuu

Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

-77.922.01.0

24.01.03.0

239.15-.05.0

10.4-40.11.0

93.31.00.18.0

282.31.0

11.065.02.0

12.24.0

BUUBUUBUUBBUBUUuBUuuuBU

-62.122.01.0

34.31.03.0

278.15.05,05.1

-43.81.0

88.52.50.18.0

395.21.0

11.065.02~rQr=

(16.6\ J

BUUBUUBUUBBUBBUUBUUU

$U

-84.722.01.0

67.81.03.0

629.2——— • 5.0"

11.55.0

-46.31.0

241.81.00.1

-10.6734.0r.o11.0

___ 65 . 0_

28.44.0

BUUBUUBUBUBUBUUBBUUU

BU

Prepa-rationBlank C57.00022.0001.0004.0001.0003.000

-60.400——— 5.000

5.0005.000

-38.9001.000

-78.3001.0000.100

-12.500169.500

1.00011.00065.0002.0006.0004.000

UUUUUUBUUuBUBUUBBUUuuuu

M

P——PFPPP

APPFPPCVPPFPPFPPNR

FORM III - INILM02.1

,... 25

AR3I9595

U.S. EPA - CLP

3BLANKS


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Preparation Blank Matrix (soil/water): ____

Preparation Blank Concentration Units (ug/L or mg/kg):

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumkcium^VomiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide


-2.8 B


1 C 2 C 3 C

57.022.01.0

63.91.03.0

933.75.09.59.7

-35.21.0

600.43.00.18.0

621.01.0

11.065.0-2.030.04.0

UUUBUUBUBBBUBBUUBUUUBBU

-1.0

5.0

1.0

1.0

-2.8

B

U

U

U

B

1.0

-1.2

1.0

-3.3

U

B

U

B

Prepa-rationBlank C M



AR3I9596

U.S. EPA - CLP

3BLANKS


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Preparation Blank Matrix (soil/water): ____

Preparation Blank Concentration Units (ug/L or mg/kg): ____

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel ______PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide


1.0 U


1 C 2 C 3 C

1.0

-2.5

U

B

1.0

-4.0

U

B

1.0 U


NRNRNRNRNRNR,,

NlPNRNRNRNRNRNRNRNRF "~NRNRFNRNRNR


AR3I9597

U.S. EPA - CLP

3BLANKS



Preparation Blank Matrix (soil/water): ____Preparation Blank Concentration Units (ug/L or mg/kg):

Analyte

AluminumAntimonyArsenicBariumBeryllium^gdmiumBlcium^BromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. ______PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

InitialCalib.Blank(ug/L) c


1 C 2 C 3 C

1.0 U


NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNR


U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 4725-PE51 GF_ Method: F_

start Date: 01/04/93 End Date: 01/04/93

EPASampleNo.

ROLTFACCVCCBRDLOTRDLOTARDLTFRDLTFAJASHTJASHTAJASHDJASHDAJASHT SZZZZZZCCVCCBJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCVCCBSBMTFSBMTFACRMIDCRMIDACRMDF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

16531657170217071712171617211726173117361741174517511755180018051810181518201825183018351840184518501855185919041909191419191924

% R

(84 . 7,- — -

89.1

85.3

85.9s~* \

/81vO( /

84.6

93.7

89.6

85.5

105.5

78.2

(83. £

AL

>fg

-

SB

»=

AS

'

BABECDCACRC0

Ar

Cu

lal

FE

•ytpB

:es

MGMNHGNIK SE

XXXXXXXXXXXX

XXXXXXXXXXXXXX

XXX

AGNATLV

=

zN

1

cN

-

FORM XIV - IN ILM02.1

~" 84

SR3I9599

U.S. EPA - CLP

14ANALYSIS RUN LOG

Name: LANCASTER LABORATORIES Contract:

Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04.

Instrument ID Number: 4725-PE51 GF_ Method: F_

Start Date: 01/04/93 End Date: 01/04/93

EPASampleNo.

CRMDFASBMITSBMITACCVCCB

•=

D/F

1.001.001.001.001.00

Time

19291934193919441948

% R

90.2

35.5

AL

-->SB

L-

AS

''-BA

P

BECDCACRC0

ArCU

\a]

FE

Lyt

PB

;es

MG

s

MNHGNIK SE

X

XX

AGNATL

V ZNCN


"" 85flR319600

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

soS5S15S25S40S50ICVICBCRACCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ

D/F

1.001.001.001.001.001.001.001.001.001.001.0010.0010.0010.0010.005.005.005.005.0010.0010.001.001.001.001.001.001.0010.0010.0010.0010.001.00

Time

22362241224522502255230023052310231423192324232923342339234423492354235900040009001400180023002800330038004300470052005701020107

% R ALSBAS

—

BABECDCACRCO

ArCU

laiFE

-ytpB

:e£MGMNHGNIK SE

XXXXXXXXXXX

XX

AGNATLV

--'

ZN

-

Iv

CN

->


QR31960I

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_



EPASampleNo.

ZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZSBMTFSBMTFASBMITSBMITAIzzzzzz•EZZZ

WB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

011201170121012601310135014001450150015502000205021002150219

% R

^ __

/ " ~\(_103y4NX— - ~ //£3 yX.

' —— '-"

ALSBASBABECDCACRCO

Ar

CU

laJ

FE

Ly1

PB

:es

MG

s

MNHGNIK SE

XX

XXXX

XX

AGNATLV ZNCN

FORM XIV - IN ILMO2.1

87

^319602

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 3812-V40Z GF_ Method: F_


EPASampleNo.

SOsioS25S50S75S100ICVICBCRACRAACCVCCBPBWPBWALCSWLCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001,001.001.001.001.001.001.001.001.001.001.001.001.00

Time

145315001506151315201526153215391545155215581604161116171623163016361643164916561702170917151721

% R

108.5

133.1

113.9

108.3

111.0

ALSBASBABECDCACRC0

Ar

CU

mJ

FE

-ytpB

:es

MG

«

MNHGNIK SEAGNATL

XXXXXXXXX

XXXXXXXXXXXXXX

V zN

1

CN

f|

*


• ;_•;_" es6R319603

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No. :CRT04_

Instrument ID Number: 2803-V400 GF_ Method: F_Start Date: 01/04/93 End Date: 01/05/93

EPASampleNo.

SOS10S25S50S75S100ICVICBCRACRAAIccvLCCB•ezzz•ezzzMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTACCVCCBROLTFROLTFARDLOTRDLOTARDLTFRDLTFAJASHTJASHTA

D/F

1.001.001.001.001.001.001.001.001.001.001.001.005.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

20192025203220392045205220582104211021172123213021362143214921562202220922152221222822342241224722532300230623132319232523312338

•

% R

••==*•— (118.6)\ _ '112.7

112.2

107.9

106.1

104.9

110.5

106.0

ALSBASBABECDCACRCO

Arcu

laJFE

LytpB

:esMGMNHGNIK SEAGNATL

XXXXXXXXX

XX

XXXXXXXXXXXXXXXXXX

V zNcN


flR3!960t4

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: 2803-V400 GF_ Method: F_Start Date: 01/04/93 End Date: 01/05/93

EPASampleNo.

JASHDJASHDACCVCCBJASHT SZZZZZZJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFACCVCCBFBUNFFBUNFASBMTFSBMTFACRMIDCRMIDACRMDFCRMDFASBMITSBMITACCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

2344235123570004001000160023002900350042004800550101010801140121012701340140014701530200020602130219022602320239

% R

109.4

108.6

111.9

114.0^

(123 0\_S

— VOO A_ e107.9

113.6

111.9-

- T

ALSBASBABECDCACRCO

Ar

CU

ia]

FE

Lyt

PB

;es

MGMNHGNIK SEAGNATL

XXXXX

XXXXXXXXXXXXXXXXXXXXXX

V zN

<

1

cN

FORM XIV - IN . ILMO2.1

SO

AR3I9605

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: _______ SAS No.: _____ SDG No.:CRT04_

Instrument ID Number: 3998-V20 AA Method: CV


EPASampleNo.

SOSO. 2SO. 5Sl.OS2.5S5.0ICVICBCRACCVICCBLfiBW^KW•|MTT?RMTFMANMTMAMTFMANHTMAHTFROALTROLTFCCVCCBRDLOTRDLTFJASHTJASHDJASHT SJASHT DJSBDFJSLTIJSLTF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

09050906090809090911091209140915091709180920092109230924092609270929093009320933093509360938093909410942094409450947094809500951

% R ALSBASBA

BECDCACRCO

Al

CU

iaJFE

LytpB

;esMGMNHG

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

NIK SEAGNATLV ZNCN


SI

3R3I9606

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: 3998-V20 AA Method: CVStart Date: 01/06/93 End Date: 01/06/93

EPASampleNo.

FBUNFCCVCCBSBMITSBMTFCRMIDCRMDFZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

095309540956095709591000100210031005100610081009101110121014

% R ALSBASBABECDCACRCO

ArcU

iaJFE

-ytpB

;esMGMNHG

XXXXXXX

XX

NIK SEAGNATLV ZN

1

CN


SR3I9607

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: _____ SAS .No. : _____ SDG No.:CRT04_

Instrument ID Number: 2360-ICP1100_ Method: P_


<1.

EPASampleNo.

SOSSSSSICVICBICSAICSABCRICCVUp v.•F•BCSWJASHT -JASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCV•GCB vv%>MAMTFMANHTMAHTFROALTROLTFRDLOTRDLTF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

19001904190819121915191819211925193019341939194319481952195720012006201020152020202420292033203820422047205120562101210521102114

% R ALSBASBA

XX

XXXX

XXXXX

XXXXXXXXXXXXXXX

BECDCA

X

XXXXX

XXXXX

XXXXXXXXXXXXXXX

cRcoX

X

XXXXXXXXXX

XXXXXXXXXXXXXXX

Ar

cu

ia]

FE

LylpB

;es

MG

X

XXXXX

XXXXX

XXXXXXXXXXXXXXX

MNHG

NIK

X

X

XXXX

XXXXX

XXXXXXXXXXXXXXX

sEAGNATLV

X

X

XXXXXXXXXX

XXXXXXXXXXXXXXX

zNcN


U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 2360-ICP1100_ Method: P_


EPASampleNo.

JASHDJSBDFJSLTICCVCCB 1-7 ."VJSLTF -(FBUNFISBMITSBMTFCRMIDCRMDFICSAICSABCRICCVICCB \,T>,4' '

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

2119212421282133213721422146215121562200220522092214221922232228

% R ALSBASBA

XXXXXXXXXXXXX

XX

BECDCA

XXXXXXXXXXXXX

XX

cRCO

XXXXXXXXXXXXXXXX

Ar

CU

laJ

FE

-ytpB

:es

MG

XXXXXXXXXXXXX

XX

MNHGNIK

XXXXXXXXXXXXX

XX

sEAGNATLV

XXXXXXXXXXXXXXXX

zN

<

cN


70

AR3I9609

oro

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

soSSSsSICVICBICSAICSABCRICVVW*TTCSWJASHTJASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCVCCBMAMTFMANHTMAHTFROALTROLTFRDLOTRDLTF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

21372145214821532156215822012205221022142219222422282233223722422246225122552300230423092313231823232327233223362341234523502354

•

% R AL

X

XXXXX

XXXXX

XXXXXXXXXXXXXXX

sB

X

X

XXXXXXXXXX

XXXXXXXXXXXXXXX

AsBABE

X

X

XXXXXXXXXX

XXXXXXXXXXXXXXX

cD

XX

XXXXXXXXXX

XXXXXXXXXXXXXXX

cAcRc0

Ar

cuXX

XXXXXXXXXX

XXXXXXXXXXXXXXX

laJ

FE

XX

XXXX

XXXXX

XXXXXXXXXXXXXXX

•ytpB

;esMG

5

MN

XX

XXXXXXXXXX

XXXXXXXXXXXXXXX

HGNIXX

XXXXXXXXXX

XXXXXXXXXXXXXXX

K sEAG

X

X

XXXXXXXXXX

XXXXXXXXXXXXXXX

NATLV zN

XX

XXXXXXXXXX

XXXXXXXXXXXXXXX

cN

71

R3I9610

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

JASHDJSBDFJSLTICCVCCBJSLTFFBUNFSBMITSBMTFCRMIDCRMDFICSAICSABCRICCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

2359000400080013001800220027003100360041004500500055005901040109

% R AL

XXXXXXXXXXXXX

XX

SB

XXXXXXXXXXXXXXXX

ASBABE

XXXXXXXXXXXXXXXX

cD

XXXXXXXXXXXXXXXX

cAcRco

Ar

CU

XXXXXXXXXXXXXXXX

laJ

FE

XXXXXXXXXXXXX

XX

-ytpB

;es

MGMN

XXXXXXXXXXXXXXXX

HGNI

XXXXXXXXXXXXXXXX

K sEAG

XXXXXXXXXXXXXXXX

NATL

,

V

-

zN

XXXXXXXXXXXxa _

I1X

cN

>


HR3I96

IBs

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: 3144-ICP61__ Method: P_


EPASampleNo.

SOsSSSslevICBICSAICSABCRI«£CVKVzzzzTcvCCBPBWLCSWJASHTJASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCVCCBMAMTFMANHTMAHTFROALT

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.0025.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.00

Time

10011006101010141017102010231027103210371041104610511056110011051110111411191124112911331138114311471152115712021206121112161221

% R ALSBASBABECDCACR

XX

XXXXXXX

XXXXX

XXXXXXXXXXXX

co

Ar

CU

laJ

FE

-ytPB

:es

MGMNHGNIK SEAGNATL

V ZNCN


73

flR3196(2

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 3144-ICP61__ Method: P_


EPASampleNo.

ROLTFRDLOTRDLTFJASHDJSBDFJSLTICCVCCBJSLTFFBUNFSBMITSBMTFCRMIDCRMDFICSAICSABCRICCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

1225123012351240124412491254125913031308131313181322132713321337134113461351

% R ALSBASBABECDCACR

XXXXXXXXXXXXXXXXXXX

c0

Ar

CU

ia]

FE

-ytpB

;es

MGMNHGNIK SEAG

NATL

V ZN

<

I

cN


' 74

SR3I9613

KHD

U.S. EPA - CLP

14ANALYSIS RUN LOG

Name: LANCASTER LABORATORIES__ Contract:


Instrument ID Number: 3144-ICP61__ Method: P_Start Date: 01/08/93 End Date: 01/08/93

EPASampleNo.

SOSSSSSICVICBICSAICSABCRI.CCV•PV*TcswJASHDZZZZZZJASHT DJASHT SJASHD LRDLOTRDLTFJASHTCCVCCBJSBDFJSLTIJSLTFFBUNFSBMITSBMTFCRMID

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

01120118012201260129013201350140014401490154015802030208021302170222022702310236024102460250025503000305030903140319032403280333

% R ALSBASBABECDCACRC0

AT

CU

ia]FE

LytPB

;esMG

;

MNHGNIK SEAGNA

X

X

XXXX

XXXXX

XXXXXXXXXXXXXXX

TL

V ZNCN


75

U.S. EPA - CLP

14ANALYSIS RUN LOG

Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_

Instrument ID Number: 3144-ICP61__ Method: P_


EPASampleNo.

CRMDFBRIMTBRMTFCCVCCBMANMTMAMTFMANHTMAHTFROALTROLTFICSAICSABCRICCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

0338034303470352035704020406041104160421042504300435044004440449

% R ALSBASBABECDCACRC0

Ar

CU

ia]

FE

-ytpB

:es

MG

5

MNHGNIK SEAGNA

XXXXXXXXXXXXX

XX

TLV ZNCN

>


SR3I96I5

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

SOS10S20S40S60S80ICV-,ICCRACCVCCB wj-jLEBW•HA•BWTCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCB V>\;MAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTAROLTF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

15071511151615201524152915341538154215471551155616001605160916141618162316271632163616411645164916541658170317071712171617201725

% R

102.8

96.1

107.1

__ 105.1

100.9

101.1

94.6.-

-f71*,8'85.8

Analytes

ALSBAS


BABECDCACRCOCUFEPBMGMNHGNIK SEAGNATLV ZNCN


,.. ' 77

3R3I9616

U.S. EPA - CLP

14ANALYSIS RUN LOG


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 4724-PE51 GF_ Method: F_


EPASampleNo.

ROLTFACCV _CCB *>\)RDLOTRDLOTARDLTFRDLTFAJASHTJASHTAJASHDJASHDAJASHT SZZZZZZCCVCCB UOJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCV ,CCB -\SBMTFSBMTFACRMIDCRMIDACRMDF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

17291734173817421747175117551800180418081813181718221826183118351839184418481853185719021907191119161920192419291933193819431947

% R

93.1

108.8

91.0

101.3— "*>

f 76. )6\ _ /

92.8

94.0

88.7

94.2

87.4

93.6

89.4

ALSBAS

XXXXXXXXXXXX

XXXXXXXXXXXXXXXXXXX

BABECDCACRCO

Ar

CU

laJ

FE

•ytpB

:es

MGMNHGNIK SEAGNATLV

•

ZN

*

CN


ftR3196i7

U.S. EPA - CLP

14ANALYSIS RUN LOG





EPASampleNo.

CRMDFASBMITSBMITAZZZZZZZZZZZZCCVCCB vl J

r=

D/F

1.001.001.001.001.001.001.00

Time

1952195620002005200920142018

% R

93.9

93.7

ALSBAS

XXX

XX

BA

BECDCACRCO

Ar

CU

ia]

FE

iy1

PB

:es

MG

;

MNHGNIK SEAGNATLV ZNCN


„... 78

AR3I96I8

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: 3812-V40Z GF_ Method: F_Start Date: 01/04/93 End Date: 01/04/93

EPASampleNo.

SOS5S10S25S40S50ICVICBCRACRAACCVCCBPBWPBWALCSWLCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCBMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTA

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

10131019102610331040104610521059110511121118112411311138114411511157120412101217122312301236124312491256130213091315132213281335

% R

101.2

103.8

89.2__ _ ,_

'82.9,. _ •"92.8

>8"l7)DCL--89.5

85.3

,-81.7v x

AL

/'

SBASBABECDCACRC0

Ar

CU

laJ

FE

-ytpB

XXXXXXXXX

XXXXXXXXXXXXXXXXXXXXXX

:e£

MGMNHGNIK SEAGNATLV ZN

t

CN

»


-' 80

SR3196I9

U.S. EPA - CLP

, 14ANALYSIS RUN LOG


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 3812-V40Z GF_ Method: F_


EPASampleNo.

ROLTFROLTFACCVCCBRDLOTRDLOTARDLTFRDLTFAJASHTJASHTA

I JASHDtASHDAKHT S•zzzzIccvCCBJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCVCCBSBMTFSBMTFACRMIDCRMIDA

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

13411348135414001407141314201427143314401446145314591506151215191525153215381545155115581605161216181625163116381644165116571704

% R

88.2

91.6

86.1

88.6-r>

x84 ;'jw( — -'"

86.3-———— T-s

,84.9^ — ---••"'90.2

85.7

102.8

85.9

97.4

AL

t

SBASBABECDCACRCO

ArcU

laJ

FE

Lyi

PB

XXXXXXXXXXXXX

XXXXXXXXXXXXXXXXXX

:es

MG

3

MNHGNIK SEAGNATLV ZNCN


81

HR3I9620

U.S. EPA - CLP

14ANALYSIS RUN LOG



Instrument ID Number: 3812-V40Z GF_ Method: F_Start Date: 01/04/93 End Date: 01/04/93

EPASampleNo.

CRMDFCRMDFASBMITSBMITAZZZZZZZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.00

Time

17111718172417311737174417501757

% R

93.9

93.0

ALSBASBABECDCACRC0

Ar

CU

ial

FE

-ytpB

XXXX

XX

;es

MG

i

MNHGNIK SEAGNATLV ZN

-<

1

cN


'82

&R319621

U.S. EPA - CLP

14ANALYSIS RUN LOG

ame: LANCASTER LABORATORIES__ Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 4725-PE51 GF_ Method: F_


EPASampleNo.

soS5S15S25S40S50ICVICBCRACCVCCBIPBW•LAV"WSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCBMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTAROLTF

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

14171422142614311436144014461450145515001505150915151519152515291535153915441549155415591604160916141618162316281633163816431648

•

% R

105.4

113.5-x—— ' -•

/ ''84.8'^ ^86.2

91.1

. y*2.TJ—/89.7

85.6x- 82/2

V^'-

ALSBASBA

BECDCACRCO

Arcu

laJFE

LylpB

:es

MG

5

MNHGNIK SE


AGNATLV ZNCN


83

flR3J9622

U.S. EPA - CLP

4ICP INTERFERENCE CHECK SAMPLE


Lab Code: _____ Case No.: _____ SAS No: _____ SDG No.: CRT04_

ICP ID Number: 2360-ICP1100 ICS Source: LLI _____


TrueSol. Sol.

Analyte A AB

AluminumAntimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSelenium_SilverSodiumThalliumVanadiumZinc

0

500000

0

500000

0

500

_500000

500

_500000

500

Initial FoundSol. Sol.A AB %R

11

_484640

-2

_500700

11

478.9

_484840.0

443.6

_501250.0

478.7

95.8

_97.0

88.7

100.2

95.7

Final FoundSol. Sol.A AB %R

6

_486500

0

_503570

9

491.6

_503680.0

452.4

_520080.0

493.8

98.3

100.7

90.5

104.0

98.8

FORM IV - IN

ILMO2.1

AR3I9623

U.S. EPA - CLP



Lab Code: _____ Case No.: _____ SAS No: _____ SDG No.: CRT04_

ICP ID Number: 2360-ICP1100 ICS Source: LLI


TrueSol. Sol.

Analyte A AB

AluminumAntimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltpopper•ronPeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadium_Zinc

500000

00

0200000

0

0

0

0

_500000

5001000

500200000

500

1000

1000

1000


_490050

028

8186430

-13

-40

-38

-8

_491950.0

454.6918.8

480.2187170.0

453.9

857.8

961.1

933.8

_98.4

90.991.9

96.093.6

90.8

85.8

96.1

93.4


_497770

030

7188780

-14

-39

-41

-9

_509010.0

470.5953.8

502.5193190.0

468.8

888.6

993.9

959.9

101.8

94.195.4

100.596.6

93.8

88.9

99.4

96.0

FORM IV - IN

ILMO2.1

U.S. EPA - CLP



Lab Code: _____ Case No. : _____ SAS No: _____ SDG No. : CRT04_

ICP ID Number: 3144-ICP61 ICS Source: LLI


TrueSol. Sol.

Analyte A AB

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

0 500


73 525.0 105.0


73 532.0 106.4

FORM IV - IN

ILMO2.1

AR319625

U.S. EPA - CLP

5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY

JASHT SName: LANCASTER LABORATORIES Contract:


Matrix (soil/water): WATER_ Level (low/med): LOW_

% Solids for Sample: _0.0Concentration Units (ug/L or mg/kg dry weight): UG/L_

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperJLron»d _____•gnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

ControlLimit%R

75-12575-12575-12575-12575-12575-125

75-12575-12575-12575-12575-125

75-12575-12575-125

75-12575-125

75-12575-12575-125

Spiked SampleResult (SSR)

2390.0000464.100040.1500

1893.200046.720046.9300

189.5900463.5700240.66002053.000016.1400

560.37000.9500

474.5600

9.000045.2100

59.7000477.8300573.1600

CSample

Result (SR)

286.520022.00001.000069.52001.00003.0000

5.00005.00005.0000

1234.60001.0000

89.91000.10008.0000

1.000011.0000

2.00006.480095.8200

C

UUBUU

UUU

U

UU

UU

UB

SpikeAdded (SA)

2000.00500.0040.00

2000.0050.0050.00

200.00500.00250.001000.0020.00

500.001.00

500.00

10.0050.00

50.00500.00500.00

%R

105.292.8100.491.293.493.9

94.892.796.381.880.7

94.195.094.9

90.090.4

119.494.395.5

Q M

PPFPPPNRPPPPFNRPCVPNRFPNRFPPNR

Comments:

FORM V (Part 1) - IN ILM02.1

42

U.S. EPA - CLP

6 EPA SAMPLE NO.DUPLICATES

JASHT DLab Name: LANCASTER LABORATORIES__ Contract:


Matrix (soil/water) : WATER . Level (low/med) : _LOW____

% Solids for Sample: ___0 % Solids for Duplicate: ___0



ControlLimit200.0

5000.0

5000.0

5000.0

20.0

Sample (S)

286.520022.00001.000069.52001.00003.0000

21555.00005.00005.00005.0000

1234.60001.0000

8562.700089.91000.10008.0000

4520.60001.000011.0000

14311.00002.00006.480095.8200

C

UUBUU

UUU

U

UuBUU

UB

Duplicate (D)

323.140022.00001.000068.66001.00003.0000

21360.00005.00005.00005.0000

1209.90001.1000

8451.300089.07000.10008.0000

4435.80001.000011.0000

15610.00002.00007.560084.2800

C

UUBUU

UUU

B

UUBUU

UB

RPD

12.0

1.2

0.9

2.0200.01.30.9

1.9

8.7

15.412.8

Q M


FORM VI - INILM02.1

AR3I9627

U.S. EPA - CLP

7LABORATORY CONTROL SAMPLE



Solid LCS Source: __________

Aqueous LCS Source: LLI________

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltfcpoer_____PbnjBeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Aqueous (ug/L)True Found %R

2000.0500.040.0

2000.050.050.0

4000.0200.0500.0250.01000.020.0

2000.0500.01.0

500.04000.010.050.0

50.0500.0500.0

1979.60527.7641.68

2103.8052.4053.98

4663.60208.63524.37274.241061.4018.80

2074.30542.040.93

537.574671.60

9.3854.32

50.60540.39552.03

99.0105.6104.2105.2104.8108.0116.6104.3104.9109.7106.194.0103.7108.493.0107.5116.893.8108. 6_

101.2108.1110.4

Solid (mg/kg)True Found C Limits %R

—

—

FORM VII - INILM02.1

U.S. EPA - CLP

7LABORATORY CONTROL SAMPLE



Solid LCS Source: __________

Aqueous LCS Source: LLI_______

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_i ______PotassiumSeleniumSilver ______SodiumThalliumVanadiumZincCyanide

Aqueous (ug/L)True Found %R

4000.0 4202.90 105.1

Solid (mg/kg)True Found C Limits %R

—

31

FORM VII - INILM02.1

„ 45AR3I9629

Kfo

U.S. EPA - CLP

8STANDARD ADDITION RESULTS

Cab Name:

Lab Code:

LANCASTER LABORATORIES

Case No. :

Contract :

SAS No. : SDG No. :CRT04


EPASampleNo.

'= ——•=

An

—

—

0 ADDABS

1 ADDCON ABS

2 ADDCON ABS

3 ADDCON ABS

FinalCone. r Q

—

—

—

—

_

FORM VIII - IN ILMO2.1

II ' 46

flR3i9630

U.S. EPA - CLP

9 EPA SAMPLE NO.ICP SERIAL DILUTION

JASHD LLab Name: LANCASTER LABORATORIES Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Level (low/med): LOW_


AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Initial SampleResult (I)

14642.00

C

SerialDilutionResult (S)

14806.50

C

B

%Differ-ence

l.i

Q M

P

FORM IX - INILM02.1

„...: 47SR3I963

U.S. EPA - CLP

9 EPA SAMPLE NO.ICP SERIAL DILUTION

JASHT LName: LANCASTER LABORATORIES Contract:


Matrix (soil/water): WATER Level (low/med): LOW_


Analyte


Initial SampleResult (I)

286.5222.00

69.521.003.00

21555.005.005.005.00

1234.60

8562.7089.91

8.004520.60

11.00

6.4895.82

C

U

BUU

UUU

UB

U

B

SerialDilutionResult (S)

285.00110.00

128.705.00

15.0022371.00

25.0025.0025.00

1052.50

8545.5090.75

40.005509.00

55.00

30.00256.55

C

UU

BUUBUUU

B

UB

U

U

%Differ-ence

100.0

85.1

3.8

14.7

0.20.9

21.9

100.0167.7

Q

E

M

PP

PPPPPPPP

PP

PP

P

PP

FORM IX - INILM02.1

. C8

HR3I9632

VERIFICATION OF INSTRUMENT PARAMETERS

43f • •*

SR3I9633

U.S. EPA - CLP

10Instrument Detection Limits (Quarterly)



ICP ID Number: 2360-ICP1100 Date: 10/15/92

Flame AA ID Number : __________

Furnace AA ID Number :

Comments:


Wave-length(nm)

308.22206.84

493.41313.04226.50317.93

228.62324.75259.94

279.08257.61

231.60766.49

328.07

292.40213.86

Back-ground

CRDL(ug/L)

200601020055

50001050251003

5000150.240

5000510

5000105020

IDL(ug/L)

57.022.0

4.01.03.0

23.0

5.05.07.0

45.01.0

8.0132.0

11.0

6.04.0

M

PPNRPPP .PNRPPPNRPPNRPPNRPNRNRPP

FORM X - IN ILMO2.1

HR3I963U

U.S. EPA - CLP


Lab Name: LANCASTER LABORATORIES__ Contract: _________


ICP ID Number: 3144-ICP61_ Date: 10/15/92

Flame AA ID Number : 3998-V20_AA_

Furnace AA ID Number :

Comments:

Analyte


Wave-length(nm)

267.72

253.65

589.59

Back-ground

CRDL(ug/L)

200601020055

5000105025100

35000

150.240

5000510

5000105020

IDL(ug/L)

5.0

0.1

65.0

M

NRNRNRNRNRNRNRPNRNRNRNRNRNRCVNRNRNRNRPNRNRNR

FORM X - IN ILM02.1

51

SR319635

U.S. EPA - CLP



Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: __________ Date: 10/15/92

Flame AA ID Number : _____________Furnace AA ID Number : 2803-V400 GF

Analyte


Wave-length(nm)

276.80

Back-ground

BD

CRDL(ug/L)

200601020055

50001050251003

5000150.240

5000510

5000105020

IDL(ug/L)

2.0

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNR

Comments:

FORM X - IN ILMO2.1

&R319636

U.S. EPA - CLP




ICP ID Number: __________ Date: 10/15/92


Furnace AA ID Number : 3812-V40Z GF

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganesfeMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Wave-length(nm)

283.30

276.80

Back-ground

BZ

BZ

CRDL(ug/L)

200601020055

50001050251003

5000150.240

5000510

5000105020

IDL(ug/L)

1.0

1.0

M

NRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNRNRNRFNRNR

Comments:

FORM X - IN ILMO2.1

8R319637

U.S. EPA - CLP


ame: LANCASTER LABORATORIES Contract:


ICP ID Number: __________ Date: 10/15/92

Flame AA ID Number : _________

Furnace AA ID Number : 4724-PE51 GF

Analyte


Wave-length(nm)

193.70

Back-ground

BZ

CRDL(ug/L)

200601020055

5000105025100

35000150.240

5000510

5000105020

IDL(ug/L)

1.0

M

NRNRFNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNR

Comments:

FORM X - IN ILMO2.1

54

flR3i9638

U.S. EPA - CLP



Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: __________ Date: 10/15/92


Furnace AA ID Number : 4725-PE51 GF

Analyte


Wave-length(nm)

196.00

Back-ground

BZ

CRDL(ug/L)

200601020055

50001050251003

5000150.240

5000510

5000105020

IDL(ug/L)

1.0

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNR

Comments:

FORM X - IN ILM02.1

...... 55

&R319639

ram

U.S. EPA - CLP

11AICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04.ICP ID Number: 2360-ICP1100 Date: 01/15/92

AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalcium ______ChromiumCobaltCopperIroniead•gnesiumHnganeseMercuryNickel.. _____PotassiumSeleniumSilverSodiumThallium_Vanadium_Zinc

Wave-length(nm)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __

231.60766.49196.03328.07589.59377.57292.40213.86

Ir

Al

0.0000000-0.0000120-0.00711200.00000000.0000000-0.00003900.00000000.00000000.00000000.00000000.0000000-0.00098300.0000000

_0. 0005890

0.00001000.00000000.00021300.00000000.00000000.00067900.00000000.0000350

iterelement C

Ca

0.0001640"0. 00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000320-0.00001100.0000890

_0.0000000_

0.00000000.00021400.00001700.00001700.0000000-0.00024200.00000000.0000000

Correction I

Fe

0.00000000.0001220-0.0071120-0.00003200.00000000.0000710-0.00001700.0000050-0.00000400.00001100.00000000.00000000.0002080

_0. 0000460

0.00008100.00000000.00004200.00006300.00000000.0000460-0.00003000.0001160

?actors for

Mg

0.00023400.00000000.00000000.00000000.00000000.00000900.00039600.0000080-0.00000200.00000000.0000600-0.00001900.0000000

_0. 0000280

0.0000000-0.0000270-0.00008100.00000000.00000000.00001100.00000000.0000380

••

BE_

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000-0.0031410_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

Comments:

FORM XI (Part 1) - IN ILM02.1

U.S. EPA - CLP

11AICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)


Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: 3144-ICP61_ Date: 01/15/92

AnalyteAluminum_Antimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobalt _____Copper _____IronLeadMagnesiumManganeseMercuryNickel _____PotassiumSelenium__SilverSodium _____ThalliumVanadium_Zinc

Wave-length(nra)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08

_257.61 __

231.60766.49196.03328.07589.59377.57292.40213.86

Interelement Correction Factors for :

Al Ca Fe Mg C0_0.00000000.00000000.00023100.00000000.00000000.00000000.0000150-0.00002400.00000000.00000000.0000000-0.00059000.0000000

_0. 0000000

0.00000000.00000000.00007700.00000000.00000000.00001300.00000000.0000000

0.00002000.0000000-0.00001200.00000000.00000000.00000000.0000000-0.00002400.00000000.00000000.00000000.00000000.0000000_0.0000000_

0.0000000-0.0000150-0.00002900.00000000.0000000-0.00010400.00000000.0000000

0.0000270-0.0022600-0.00258000.00000000.00000000.0002430-0.0003870-0.00034500.0000000-0.00015000.00000000.00011000.0001330-0.0000150

-0.00003900.00000000.0002430-0.00019500.0000000-0.0000320-0.00002800.0001050

0.00004800.00000000.00000000.00000000.00000000.00000000.00000000.00004200.00000000.00000000.00004900.00000000.0000000

_0. 0000320

0.00000000.0000000-0.00005700.00000000.0000000-0.00011400.00000000.0000290

-0.0167000-0.0000510-0.00211000.00000000.00000000.00006000.0000110-0.00048200.0000000-0.00114000.0000430-0.0008890-0.000366_f_0.000000

0.00049700.00000000.00109000.00000000.00000000.00016100.00001300.0000000

I

Comments:

FORM XI (Part 1) - IN . ILM02.1

, ..' 57

AR3I96M

Ml N,

U.S. EPA - CLP

11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)


Lab Code: ______ Case No.: ______ SAS No.: .______ SDG No.: CRT04_


Analyte

Aluminum_AntimonyArsenic _BariumBerylliumCadmium _____CalciumChromiumCobalt __CopperIronLeadknesium^ pganeseSrcuryNickelPotassiumSelenium_SilverSodium ______ThalliumVanadium_Zinc

Wave-length(ran)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __

231.60766.49196.03328.07589.59377.57292.40213.86

Ir

CO_

0.0001860-0.0038310-0.00308000.00000000.00000000.00003200.0000000-0.00007600.00000000.00005700.00008100.0002700-0.0018810_0. 0000000

0.00155900.00000000.00059900.00001200.00000000.00013300.00000000.0000000

iterelement C

CR_

0.00024500.00701100.00095000.00000000.0000180-0.00001200.00091400.00000000.00007500.00000000.0001150-0.0010390-0.0007860_0.0000000_

0.00000000.0000000-0.00029800.00004200.0000000-0.0007970-0.00222400.0000620

Correction I

CU_

0.0000420-0.00001500.00001800.00000000.00000000.00001200.0000000-0.00001500.00000000.00000000.0000000-0.00001100.0000000-0.0000770

0.00000000.00013300.00043800.00007400.00000000.0000000-0.00006400.0043410

"•actors for

K _

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0001870

_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

••

MN_

0.0013450-0.0001910-0.00041300.00000000.00000000.00000000.0003530-0.00112400.00000000.00003900.00089800.0000920-0.0080910_0. 0000000

0.00000000.00000000.00027500.00013400.0000000-0.0002470-0.00017600.0000000

Comments:

FORM XI (Part 2) - IN / ILMO2.1

U.S. EPA - CLP





AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryn J.W.NCSXPotassiumSeleniumSilverSodiumThalliumVanadium_Zinc

Wave-length(nm)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __

231.60766.49196.03328.07589.59377.57292.40213.86

Ir

M0_

0.00895500.00488900.00107200.00001200.00001900.00013700.0007860-0.0012330-0.00173200.00068900.0003620-0.0019300-0.0215500-0.0001860

-0.00266000.00189500.00010700.00064000.00048830.00000000.00000000.0000000

iterelement C

s*_0.01054400.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000_0.0000000_

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

Correction I

SR_

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0001940

_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00237400.00000000.0000000

actors forTI_

0.00248100.0011430-0.00001200.0000000-0.00003500.00029200.00071400.00017100.00170600.00031400.00024200.0003340-0.0036750_0. 0000430

0.00000000.0002270-0.00032700.0002520-0.0049410-0.05503000.00031400.0000360

"••

V _

0.0228200-0.00177100.00551000.00000000.0029800-0.00001500.0008280-0.08807000.00003000.00006200.0002960-0.0003050-0.000324*-0.000150

-0.00045600.00026700.00020300.00029100.0007290-0.00423800.00000000.0002510

I

Comments:

FORM XI (Part 2) - IN ILMO2.1

U.S. EPA - CLP


Name: LANCASTER LABORATORIES__ Contract:

Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: 3144-ICP61_ Date: 01/15/92

AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmium _Calcium _ChromiumCobalt _____Copper _____IronLead•jnesiumHganeseMercuryNickel_> _____PotassiumSelenium_Silver ____SodiumThallium_Vanadium_Zinc

Wave-length(nm)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08

_257.61 __

231.60766.49196.03328.07589.59377.57292.40213.86

Ir

CR_

-0.00007800.00824000.00098200.00000000.00000000.00000000.00065200.0000000-0.00011000.00014400.0000490-0.0011200-0.0004700_0. 0000130

-0.00003800.0000150-0.00022900.00000000.0000000-0.0006260-0.00305000.0000000

vterelement C

CU_

-0.00001600.00000000.00001400.00000000.00000000.00000000.00003400.0000300-0.00001900.00000000.0000000-0.00004600.0000000-0.0001000_

0.00000000.00000000.00019800.00000000.0000000-0.0002620-0.00006000.0027800

Correction I

MN_

0.0006990-0.0000670-0.00014000.00000000.00000000.00000000.00018400.00097100.00000000.0000530-0.00014200.0000640-0.0081200_0. 0000000

-0.00031200.00005800.00024500.00011700.0000520-0.0002250-0.00016100.0000200

?actors for

MO_

0.01280000.00286000.00130000.0000000-0.00007800.00012300.0004250-0.00205000.00002300.00053700.0001470-0.00282200.0002440-0.0002920

-0.00224000.00156000.00022700.00000000.00324000.0006520-0.0026200-0.0000730

••

NI_

0.0000950-0.00060000.00004200.00000000.00000000.00027200.00000000.00005400.00038800.00004600.00000000.0002870-0.0008810_0. 0000000

0.00000000.0000290-0.00001600.00000000.00000000.05404000.00002000.0032600

Comments:


60

U.S. EPA - CLP




ICP ID Number: 3144-ICP61_ Date: 01/15/92


Wave-length

(nm)

308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08257.61

231.60766.49196.03328.07589.59377.57292.40213.86

Ir

V

-0.0153400-0.00360000.00669200.00000000.0022540-0.00001400.00041800.00559000.0000140-0.00003300.0002220-0.00024100.0005090-0.0001510

-0.00031000.00010100.0003280-0.00016400.0000000-0.00053700.0000000-0.0064500

it er element CCorrection I actors for •*

— I.Comments:


61

AR3196I*5

U.S. EPA - CLP

12ICP LINEAR RANGES (QUARTERLY)




Comments:

Analyte


Integ.Time(sec. )

6.006.006.006.006.006.006.006.006.006.006.006.006.006.00

6.006.006.006.006.006.006.006.00

Concentration(ug/L)

600000.0200000.0200000.0100000.010000.0100000.0600000.0100000.0100000.0100000.0250000.0100000.0800000.0100000.0

100000.0900000.0200000.050000.0900000.0200000.0100000.0100000.0

M

ppppppppppppppNRPPPPPPPP

FORM XII - IN ILM02.1

62

U.S. EPA - CLP

12ICP LINEAR RANGES (QUARTERLY)




Analyte


Integ .Time(sec. )

6.006.006.006.006.006.006.006.006.006.006.006.006.006.00

6.006.006.006.006.006.006.006.00

Concentration(ug/L)

600000.0200000.0200000.0100000.010000.0100000.0600000.0100000.0100000.0100000.0250000.0100000.0800000.0100000.0

100000.0900000.0200000.050000.0900000.0200000.0100000.0100000.0

M

ppppppppppppppNRPPPPPPPP

Comments:

FORM XII - IN ILM02.1

SR3I96U7

PREPARATION AND RUN LOGS

64

U.S. EPA - CLP

13PREPARATION LOG


Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04.

Method: P

EPASampleNo.

BRIMTBRMTFCRMDFCRMIDFBUNFJASHDJASHTJASHT DJASHT SJSBDFJSLTFJSLTILCSWMAHTFMAMTFMANHTMANMTPBWRDLOTRDLTFROALTROLTFSBMITSBMTF

PreparationDate

12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92

Weight(gram)

Volume(mL)

100100100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILM02.1

65

oro

U.S. EPA - CLP

13PREPARATION LOG

Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_

Method: P

EPASampleNo.


PreparationDate

01/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/93

Weight(gram)

Volume(mL)

100100100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILMO2.1

66

U.S. EPA - CLP

13PREPARATION LOG

Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_

Method: F

EPASampleNo.


PreparationDate

12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92

Weight(gram)

Volume(mL)

100100100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILM02.1

raro N

U.S. EPA - CLP

13PREPARATION LOG


Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_

Method: CV

EPASampleNo.


PreparationDate

12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92

Weight(gram)

Volume(mL)100100100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILMO2.1

C8

SR3I9652

RAW DATA

""• 93

AR319653

inorganics data package · 2020. 12. 27. · inc. • 2425 new/holland pike • lancaster, pa...

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