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Presented to: International Aircraft Materials Fire Test Forum By: Steve Rehn Date: 6/11/2020 Federal Aviation Administration Relationship Between 3-D Printed Materials and Flammability

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  • Presented to: International Aircraft Materials Fire

    Test Forum

    By: Steve Rehn

    Date: 6/11/2020

    Federal AviationAdministration

    Relationship Between 3-D

    Printed Materials and

    Flammability

  • 2Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Introduction

    • 3D printing introduces all

    new variables in material

    construction

    • Variables include:

    – Printing orientation

    – Infill percentage

    – Raster angle

    – Layer thickness

    – Raster width

  • 3Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Test Plan

    • Determine worst case scenario for each

    variable in flammability testing in order to

    simplify future testing

    • Vary printing parameters in several different

    materials and sample thicknesses

    • Test using vertical Bunsen Burner

    • Analyze test results to determine how future

    testing can be simplified and reduced

  • 4Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Calculating Infill Percentage

    • Infill percentage calculated from Insight program material

    estimate

    • Create toolpath of single layer

    • Delete outer contours to only calculate infill

    • Divide material used by material used in solid sample to get

    infill %

    Sparse: 0.100 in3 material Solid: 0.435 in3 material

    ൗ0.100 0.435 = 23.0%

  • 5Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Print Infill Patterns

    • Tested with Ultem Support (PES) and Ultem

    9085 (PEI) materials

    • Several infill patterns and percentages

    • Tested infill by itself and with solid outer

    layers

  • 6Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Print Infill Patterns

    Hexagonal

    (29.7%)

    Hexagram

    (32.4%)

    Permeable

    Triangular (32.4%)

    Sparse

    (23.0%)Sparse DD

    (44.8%)

  • 7Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Infill Only

    • PES Material

    • 0.060” sample thickness

    • Every sample tested burned

    until chamber filled with

    smoke and put out fire

  • 8Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill with Solid Outer Layers

    • Tested 0.10” thickness

    • 2 solid outer layers, rest is hollow infill

    – On 0.10”, 2 solid layers, 6 infill, 2 solid layers

    • Two materials – Ultem Support (PES) and

    Ultem 9085 (PEI)

    • 12-second vertical Bunsen burner for both

    materials, 60s VBB for Ultem 9085

  • 9Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem Support

    • 8 samples per

    infill pattern

  • 10Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem Support

    218.8

    87.268.6

    27.8

    49.1

    14.9

    9.4

    1

    10

    100

    1000

    20% 30% 40% 50% 60% 70% 80% 90% 100%

    Flam

    e Ti

    me

    (s)

    -lo

    g sc

    ale

    Infill Percentage (%)

    0.10" PES Infill Percentage 12 s VBB Flame Time (log scale)

  • 11Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem Support

    • Good correlation

    between infill

    percentage and test

    results

    • Less infill % causes

    more burning

    0

    5

    10

    15

    20

    25

    30

    35

    40

    45

    0

    0.1

    0.2

    0.3

    0.4

    0.5

    0.6

    0.7

    0.8

    20% 30% 40% 50% 60% 70% 80% 90% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage (%)

    0.10" PES Infill Percentage 12 s VBB Results

    Avg. Burn Length Avg Flame Time

  • 12Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085 (PEI)

    • Same layer configuration – 2 solid outer layers, 6 inner infill

    layers (0.10 inch thickness)

    – 12-second test, 4 samples per infill pattern

    0

    0.5

    1

    1.5

    2

    2.5

    3

    0

    0.05

    0.1

    0.15

    0.2

    0.25

    0.3

    0.35

    0% 20% 40% 60% 80% 100%

    Flam

    e T

    ime

    (s)

    Bu

    rn L

    en

    gth

    (in

    )

    Infill Percentage

    Ultem 9085 0.10" Infill Percentage 12s VBB

    Burn Length Flame Time

    0

    0.5

    1

    1.5

    2

    2.5

    3

    0

    0.05

    0.1

    0.15

    0.2

    0.25

    0.3

    0.35

    0% 20% 40% 60% 80% 100%

    Flame Tim

    e (s)

    Bu

    rn L

    en

    gth

    (in

    )

    Infill Percentage

    Ultem 9085 0.10" Infill Percentage 12s VBB Avg.

    Average Burn Length Average Flame Time

  • 13Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Same layer configuration – 2 solid outer layers, 6 inner infill

    layers (0.10 inch thickness)

    – 60-second test, 5 samples per infill pattern

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    0

    0.2

    0.4

    0.6

    0.8

    1

    1.2

    1.4

    1.6

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.10" Infill Percentage 60s VBB

    Burn Length Flame Time

    0.0

    0.5

    1.0

    1.5

    2.0

    2.5

    3.0

    3.5

    0.0

    0.2

    0.4

    0.6

    0.8

    1.0

    1.2

    1.4

    1.6

    0% 20% 40% 60% 80% 100%

    Flame Tim

    e (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.10" Infill Percentage 60s VBB Avg.

    Average Burn Length Average Flame Time

  • 14Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only – 0.06 inch thickness

    • Same tests as completed by Airbus

    – Have not reconciled infill % calculation yet

  • 15Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only, 0.06 inch thickness

    – 12-second test, 4 samples per infill pattern

    0

    2

    4

    6

    8

    10

    12

    14

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    4

    4.5

    5

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.06" Infill Only 12s VBB

    Burn Length Flame Time

    0

    2

    4

    6

    8

    10

    12

    14

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    4

    4.5

    5

    0% 20% 40% 60% 80% 100%

    Flame Tim

    e (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.06" Infill Only 12s VBB Avg.

    Average Burn Length Average Flame Time

  • 16Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only, 0.06 inch thickness

    – 60-second test, 5 samples per infill pattern

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    4

    4.5

    5

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.06" Infill Only 60s VBB

    Burn Length Flame Time

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    0

    0.5

    1

    1.5

    2

    2.5

    3

    3.5

    4

    4.5

    5

    0% 20% 40% 60% 80% 100%

    Flame Tim

    e (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.06" Infill Only 60s VBB Avg.

    Average Burn Length Average Flame Time

  • 17Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only, 0.20 inch thickness

    – 12-second test, 4 samples per infill pattern

    0.00

    0.20

    0.40

    0.60

    0.80

    1.00

    1.20

    0.00

    0.05

    0.10

    0.15

    0.20

    0.25

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.20" Infill Only 12s VBB

    Burn Length Flame Time

    0.00

    0.20

    0.40

    0.60

    0.80

    1.00

    1.20

    0.00

    0.05

    0.10

    0.15

    0.20

    0.25

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.20" Infill Only 12s VBB Avg.

    Average Burn Length Average Flame Time

  • 18Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only, 0.20 inch thickness

    – 60-second test, 5 samples per infill pattern

    0.00

    0.50

    1.00

    1.50

    2.00

    2.50

    0.00

    0.20

    0.40

    0.60

    0.80

    1.00

    1.20

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.20" Infill Only 60s VBB Avg.

    Average Burn Length Average Flame Time

    0.00

    0.50

    1.00

    1.50

    2.00

    2.50

    0.00

    0.20

    0.40

    0.60

    0.80

    1.00

    1.20

    0% 20% 40% 60% 80% 100%

    Flam

    e Ti

    me

    (s)

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 0.20" Infill Only 60s VBB

    Burn Length Flame Time

  • 19Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem 9085

    • Infill only, 0.06 inch vs. 0.20 inch thickness

    0.00

    0.50

    1.00

    1.50

    2.00

    2.50

    3.00

    3.50

    4.00

    0% 20% 40% 60% 80% 100%

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem 9085 Varying Thickness 12s VBB

    0.06 inch 0.20 inch

    0.00

    0.50

    1.00

    1.50

    2.00

    2.50

    3.00

    3.50

    4.00

    4.50

    0% 20% 40% 60% 80% 100%B

    urn

    Len

    gth

    (in

    )

    Infill Percentage

    Ultem 9085 Varying Thickness 60s VBB

    0.06 inch 0.20 inch

  • 20Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Varying Infill – Ultem Support

    • Infill w/ solid outer layers, 0.10 inch vs. 0.25 inch thickness

    – 12-second VBB

    0

    0.1

    0.2

    0.3

    0.4

    0.5

    0.6

    0.7

    0.8

    0% 20% 40% 60% 80% 100%

    Bu

    rn L

    engt

    h (

    in)

    Infill Percentage

    Ultem Support Varying Thickness 12s VBB

    0.10 inch 0.25 inch

    0

    5

    10

    15

    20

    25

    30

    35

    40

    45

    0% 20% 40% 60% 80% 100%Fl

    ame

    Tim

    e (s

    )

    Infill Percentage

    Ultem Support Varying Thickness 12s VBB

    0.10 inch 0.25 inch

  • 21Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Additive Manufacturing VBB AC

    • Began writing advisory circular for vertical

    Bunsen burner testing of 3D printed

    materials

    – Details most severe case for each variable in order

    to reduce/simplify testing

    – For example, lower infill % is more severe than

    higher infill %, therefore testing lower infill

    substantiates higher infill.

    – Will have separate section for PEI-based materials

    – Can discuss further in task group meeting

  • 22Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Conclusion

    • Less infill percentage is more severe case

    than more infill

    • Agrees with Airbus test results using Ultem

    9085

    – Have not made direct comparison yet because of

    infill percentage calculation

    • Thinner samples is more severe than thicker

    • Next parameter to test

    – Raster angle?

    – Raster width?

  • 23Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Contact:Steven Rehn

    Federal Aviation Administration

    William J. Hughes Technical Center

    Fire Safety Branch, Bldg. 203

    Atlantic City Int’l Airport, NJ 08405

    (609) 485-5587

    [email protected]

    Questions?

  • 24Additive Manufacturing Fire Testing6/11/2020 Federal Aviation

    Administration

    Ground Rules for Webinars and Zoom Meetings

    Everyone PLEASE go on mute

    Zoom meeting Ground Rules:

    Use raised hand feature (under participants button) to ask a question

    A panelist will call on participant to ask their question, as time permits

    Once question has been answered, click raised hand to “un-raise”