faculty of · faculty of chemical engineering uitm shah alam 40450, shah alam, selangor h a j a t u...

FACULTY OF

CHEMICAL ENGINEERING

UiTM SHAH ALAM

40450, SHAH ALAM,

SELANGOR

H A J A T U N R A B A N I A H M A D R A Z I F

03-55436549 (O) [email protected]

LIST OF INSTRUMENTS

1. THERMOGRAPHIC ANALYZER ( TGA )

2. DIFFERENTIAL SCANNING CALORIMETER ( DSC )

3. ATOMIC ABSORPTION SPECTROMETRY ( AAS )

4. INDUCTIVELY COUPLED PLASMA ( ICP-OES )

5. BOMB CALORIMETER

6. ELEMENTAL ANALYZER ( CHNS-O )

7. FOURIER TRANSFORM INFRA RED ( FTIR )

8. X-RAY DIFFRACTOMETER ( XRD )

9. X-RAY FLOURESCENCE SPECTROMETER SYSTEM ( XRF )

10. GAS CHROMATOGRAPHY MASS SPECTROMETER ( GCMS )

11. GAS CHROMATOGRAPHY ( GC )

12. HIGH PERFORMANCE LIQUID CHROMATOGRAPHY ( HPLC )

13. ULTRAVIOLET VISIBLE SPECTROPHOTOMETER ( UV-Vis )

14. MERCURY POROSIMETER

15. MICROPORE SURFACE AREA ( BET )

16. PARTICLE SIZE ANALYZER

17. CONTACT ANGLE GONIOMETER

18. TEMPERATURE PROGRAMMED DESOPRTION, REDUCTION AND OXIDATION

( TPDRO )

19. CHEMBET PULSAR TPR/TPD/TPO & PULSE CHEMISORBTION

20. SPRAY DYER ( LAB SCALE )

21. SPRAY DRYER ( INDUSTRIAL SCALE )

22. UNIVERSAL TENSILE MACHINE

23. LAB SCALE INTERNAL MIXER & MINI TWIN SCREW EXTRUDER

24. VISCOMETER

25. RHEOMETER

26. COMPACT CLOUD & POUR POINT

27. LABORATORY OVEN

28. FURNACE

29. PH METER

30. SOXHLET EXTRACTION

WORK FLOW OF CHARGING INSTRUMENT

WORK FLOW OF CHARGING INSTRUMENT

Applicant

Dean

Science Officer

Science Officer

Applicant

Applicant

PIC of Instrument Scince Officer

TD PJI

Applicant

Applicant

Applicant

Start

Send application to dean for

approval

Approved

• Checking availability of instrument

• Email feedback & charge form

Available

Confirm by user –

Submit charge form

Send sample to PIC of

instrument

• Run analysis

• Prepare letter for charging /

applying invoice to be signed

by TD PJI

Collect sample data

End

Bring letter to UKZ8 for payment /

Process payment

Bring receipt for proof of

payment to the faculty

YES

YES

YES

NO

NO

NO

2 DIFFERENTIAL SCANNING CALORIMETER (DSC)

BRAND / MODEL : METTLER TOLEDO / DSC1

FUNCTION : MEASURES ENTHALPY CHANGES IN SAMPLES DUE TO CHANGES

IN PHYSICAL AND CHEMICAL PROPERTIES AS A FUNCTION OF TEMPERATURE

OR TIME

EQUIPMENT CHARGES : RM150 / SAMPLE

3 ATOMIC ABSORTION SPECTROMETRY (AAS)

BRAND / MODEL : HITACHI / AAS Z2000

FUNCTION : TO DETECT CONCENTRATION OF AN ELEMENT DISSOLVED IN

LIQUID SAMPLES (FLAME TECHNIQUE)

EQUIPMENT CHARGES : RM50 / ELEMENT / SAMPLE

1 T HERM OG RAVIME TRIC AN ALY ZER ( TGA )

BRAND / MODEL : METTLER TOLEDO

FUNCTION : THERMAL ANALYSIS TECHNIQUES USED TO CHARACTERIZE A

WIDE VARIETY OF MATERIALS IN WHICH MASS OF A SAMPLE IS MEASURED

OVER TIME AS THE TEMPERATURE CHANGES


4 INDUCTIVELY COUPLED PLASMA (ICP -OES)

BRAND / MODEL : THERMO SCIENTIFIC / ICAP 6000 SERIES

FUNCTION : TO DETECT CONCENTRATION OF MULTIELEMENT DISSOLVED IN

LIQUID SAMPLES (PLASMA TECHNIQUE)

EQUIPMENT CHARGES : RM50 / ELEMENT / SAMPLE

5 BOMB CALORIMETER

BRAND / MODEL : IKA WORKS / C5000 CONTROL

FUNCTION : DETERMINE GROSS CALORIFIC VALUE OF SOLID AND FUEL

SAMPLES. MEASURE THE HEAT OF COMBUSTION OF A PARTICULAR

REACTION


6 E L E M E N T A L A N A L Y Z E R ( C H N S - O )

BRAND / MODEL : THERMO FINNIGAN / FLASHEA 1112 SERIES

FUNCTION : ANALYSIS OF CARBON, HYDROGEN, NITROGEN, SULFUR AND

OXYGEN CONTENT OF SAMPLES


7 FOURIER TRANSFORM INFRA RED (FT-IR)

BRAND / MODEL : PERKIN ELMER / SPECTRUM ONE

FUNCTION : FOR ANALYSIS OF COMPOSITION OF SAMPLES. USED TO

IDENTIFY ORGANIC, POLYMERIC AND IN SOME CASES INORGANIC MATERIALS


8 X-RAY DIFFRACTOMETER (XRD)

BRAND / MODEL : RIGAKU / XRD D/MAX 2200V/PC

FUNCTION : TO ANALYZE THE STRUCTURE OF MATERIALS FROM THE

SCATTERING PATTERN PRODUCED BY A BEAM OF X-RAY INTERACTING WITH

THE PARTICLE. THIS IS THEN MATCHED TO AN EXISITING DATABASE TO

DETERMINE THE CHEMICAL COMPONENTS WITHIN THE MATERIAL.

EQUIPMENT CHARGES : RM150/300 / (QUALITATIVE/QUANTITATIVE) / SAMPLE

9 X-RAY FLUORESCENE (XRF)

BRAND / MODEL : PANALYTICAL AXIOS / HP DC7900

FUNCTION : TO ANALYZE THE PERCENTAGE COMPOSITION OF EACH

CHEMICAL COMPONENT WITHIN A PARTICULAR CHEMICAL.


10 GAS CHROMATOGRAPHY MASS SPECTROMETER

BRAND / MODEL : VARIAN / VARIAN 4000/QCMSMS

FUNCTION : TO IDENTIFY DIFFERENT SUBSTANCES WITHIN A TEST SAMPLE.

EQUIPMENT CHARGES : RM200 / INJECTION / SAMPLE

11 GAS CHROMATOGRAPHY

BRAND / MODEL : THERMO ELECTRON / FINNIGAN TRACE GC ULTRA

FUNCTION : TO IDENTIFY DIFFERENT SUBSTANCES WITHIN A TEST SAMPLE


12 HIGH PERFORMANCE LIQUID

CHROMATOGRAPHY

BRAND / MODEL : PERKIN ELMER / 200LC

FUNCTION : TO SEPARATE, IDENTIFY AND QUANTIFY EACH COMPONENT IN A

LIQUID MIXTURE.


13 ULTRAVIOLET VISIBLE SPECTROPHOTOMETER

BRAND / MODEL : PERKIN ELMER / LAMBDA 750

FUNCTION : FOR QUANTITATIVE DETERMINATION OF DIFFERENT ANALYTES


14 MERCURY POROSIMETER

BRAND / MODEL : MICROMERITICS / AUTOPORE IV 9510

FUNCTION : DETERMINE VARIOUS QUANTITIABLE ASPECTS OF A MATERIALS

POROUS NATURE (PORE DIAMETER, TOTAL PORE, VOLUME, SURFACE AREA,

BULK AND ABSOLUTE DENSITIES). MERCURY INTUSION TECHNIQUE UNDER

LOW (50PSI) AND HIGH (60000PSI) PRESSURE


15 MICROPORE SURFACE AREA (BET)

BRAND / MODEL : MICROMERITIC / 3FLEX 3500

FUNCTION : FOR SURFACE AREA MEASUREMENT AND PORE SIZE ANALYSIS


16 PARTICLE SIZE ANALYZER

BRAND / MODEL : MALVERN / MASTER SIZER 2000

FUNCTION : TO DETERMINE THE SIZE OF PARTICLES.


17 CONTACT ANGLE GONIOMETER

BRAND / MODEL : AST / VCA-3000S

FUNCTION : FOR CONTACT ANGLE/SURFACE ENERGY ANALYSIS TO EVALUATE

ADHESION, CLEANLINESS AND COATINGS.

EQUIPMENT CHARGES : RM50 / ANALYSIS / SAMPLE

18 TEMPERATURE PROGRAMMED DESORPTION,

REDUCTION AND OXIDATION (TPDRO)

BRAND / MODEL : THERMO FINNIGAN / TPDRO 1100

FUNCTION : DETERMINE THE PROPERTIES OF CATALYST (SURFACE AREA,

DISPERSION, ACID/BASE SITES CONCENTRATION, ACTIVATION ENERGY)

EQUIPMENT CHARGES : RM300 / ANALYSIS / SAMPLE

19 CHEMBET PULSAR TPR/TPD/TPO & PULSE

CHEMISORBTION

BRAND / MODEL : MICROMERITIC / CHEMISORB 2750

FUNCTION : FOR CATALYST CHARACTERIZATION


20 SPRAY DRYER ( LAB SCALE )

BRAND / MODEL :

FUNCTION : TO PRODUCE A DRY POWDER FROM LIQUID SAMPLE OR SLURRY

BY RAPIDLY DRYING WITH A HOT GAS

EQUIPMENT CHARGES : RM150 / SAMPLE / 5 HOUR ( ADDITIONAL RM20 FOR

THE NEXT HOUR )

21 SPRAY DRYER ( INDUSTRIAL SCALE )

BRAND / MODEL :

FUNCTION : TO PRODUCE A DRY POWDER FROM LIQUID SAMPLE OR SLURRY

BY RAPIDLY DRYING WITH A HOT GAS

EQUIPMENT CHARGES : RM150 / SAMPLE / HOUR

22 UNIVERSAL TENSILE MACHINE

BRAND / MODEL : TINIUS OLSON / H50KT

FUNCTION : TO DETERMINE THE TENSILE STRENGTH OF MATERIALS


23 LAB SCALE INTERNAL MIXER & MINI TWIN

SCREW EXTRUDER

BRAND / MODEL : THERMO HAAKE GERMANY / POLYLAB OS SYSTEM

FUNCTION : TO MIX MULTIPLE TYPE OF POLYMERS USING ROLLS WITHIN A

CLOSED CHAMBER


24 VISCOMETER

BRAND / MODEL : FANN / 35SA 6-SPEED

FUNCTION : MEASURE THE VISCOCITY OF THAT FLUID


25 RHEOMETER

BRAND / MODEL : ANTON PAAR / MCR 301

FUNCTION : MEASURES THE RHEOLOGY OF A FLUID. USED FOR FLUIDS

WHICH CANNOT BE DEFINED BY A SINGLE VALUE OF VISCOSITY


26 COMPACT CLOUD & POUR POINT

BRAND / MODEL : STANHOPE SETA / 94100-0

FUNCTION : TO DETERMINE CLOUD AND POUR POINT OF A SUBSTANCE


27 LABORATORY OVEN

BRAND / MODEL : MEMMERT / UFP800

FUNCTION : USE FOR THERMAL APPLICATION SUCH AS CURING, DRYING

STRELIZING ect…

EQUIPMENT CHARGES : RM45 / USE

28 FURNACE

BRAND / MODEL : VT FURNACES / HT30-1400

FUNCTION : FOR HIGH-TEMPERATURE APPLICATION SUCH AS SOLDERING,

COATING ect….


29 PH METER

BRAND / MODEL : METTLER TOLEDO / F20-KIT

FUNCTION : TO MEASURE pH OF LIQUID SAMPLE


30 SOXHLET EXTRACTION

BRAND / MODEL :

FUNCTION : TO SEPARATE SOLUBLE PARTS IN THE SOLVENT

EQUIPMENT CHARGES : RM150 / SAMPLE WITH OWN SOLVENT

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