inorganics data package · 2020. 12. 27. · inc. • 2425 new/holland pike • lancaster, pa...
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Data Package
Contract Lab Program Data Packagefor
DuPont Environmental Remediation Sv
INORGANICS DATA PACKAGE
Christina Tidal StudyGrab Water Samples
Collected on 12/29/92, 12/30/92 by BCLLI Sample No. 1911840-1911847, 1912267-1912280
Lancaster Laboratoriesr Where quality is a science.
Lancaster Laboratories. Inc. • 2425 New/Holland Pike • Lancaster, PA 17601-5994 717-656-2301 • Fax-717-656-2681 2262 3/1/91
SR3I955U
TABLE OF CONTENTS
A. Case Narrative...............................................1
B. Sample Data.................................................. 5
C. Quality Control Data........................................ 26
D. Verification of Instrument Parameters....................... 49
E. Preparation and Run Logs.................................... 64
F. Raw Data.................................................... 9 3
1. ICP Data............................................ 94
2. Furnace Data.......................................290
3. Mercury Data....................................... 379
4. Extraction/Distillation/Digestion Logs.............384
G. Chain-of-Custody Record....................................389
AR319555
CASE NARRATIVE
AR31955&1
Lancaster LaboratoriesWhere quality is a science.
CASE NARRATIVE FOR INORGANICS
Laboratory Name: Lancaster Laboratories
SDG Number: CRT04
Date Received: 12/31/92
Analysis;All samples were digested a second time for sodium due to
the laboratory control sample being out of the control limits.
Explanatory Notes;The inappropriate error flag, % Recovery Failed,
Repeat by Standard Additions, is due to a manufacturer's(Varian) software error. The software is designed to followthe analysis protocol for USEPA Contract Laboratory ProgramILM01.0. Following this protocol, method of standard additionsis not required for samples demonstrating sample absorbance orconcentration less than 50% of the spike absorbance orconcentration; however, the Varian software prints this flag,regardless of sample absorbance or concentration, wheneverthe percent recovery is below 85% or above 115%.
Varian has been informed of this problem and hascommunicated that the problem will be resolved in a futuresoftware revision. The software is needed to operate theinstrument and to control the automatic spiking function ofthe autosampler. Since the software will not permit thiserror to be disabled, data that demonstrates this error willbe manually corrected on the raw data by the analyst.
Calibration Standards;Instrument calibration standards are prepared monthly from stock
solutions purchased from Spex or Baker chemical.Total ICP integration time is 24 seconds.
Case Narrative reviewed and approved by:Date
Susan B./ShorterQuality Assurance Specialist I
AR3I9557Lancaster Laboratories, Inc. • 2A25 New Holland Pike, Lancaster, Fft 17601-5994 • 717-656-2301 • Fax:717-656-2681
raro
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Name: LANCASTER LABORATORIES Contract: __
Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
SOW No.: 3/90_
EPA Sample No. Lab Sample ID_BRIMT______ __1911840_____BRMTF______ __1911841_____CRMDF_______ __1912280____CRMID 1912279FBUNF________ __1912276~JASHD________ __1912270""JASHT_______ __1912269""JASHTD______ __1912272""JASHTS_______ __1912271""JSBDF________ __1912273""JSLTF________ __1912275""JSLTI________ _1912274"~MAHTF_______ __1911845""MAMTF_______ __1911843""MANHT_____ __i9ii844~"MANMT_____ _1911842"RDLOT_______ __1912267"~RDLTF_______ __1912268"~ROALT________ __1911846""ROLTF , 19 us 47"
ICP interelement corrections applied ? Yes/No YES
e ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No NO_
Comments:___THE_REPORTED_VALUE_IS_ESTIMATED_FOR_IRON_BECAUSE_OF_THE_PRESENCE_OF_
INTERFERENCE.
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.Signature; .4 • ^/,-t /•) vJ/t.C!;~t~L i Name; S/ ^ n /?.. ________
Date: TV , >.. c, : o / 5~ / 99 _______ Title ; rfu A j< 'J-u J~fS?,i/, #, ?,-s < ?Ss's ' -.rX 7~—— ^_, , ^COVER PAGE - IN IIMO2 . 1
U.S. EPA - CLP
COVER PAGE - INORGANIC ANALYSES DATA PACKAGE
Lab Name: LANCASTER__LABORATORIES__ Contract: _________
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_SOW No.: 3/90_
EPA Sample No. Lab Sample ID_SBMIT_______ __1912277____SBMTF 1912278
Were ICP interelement corrections applied ? Yes/No YES
Were ICP background corrections applied ? Yes/No YESIf yes - were raw data generated beforeapplication of background corrections ? Yes/No N0_
Comments:___THE_REPORTED_VALUE_IS_ESTIMATED_FOR_IRON_BECAUSE_OF_THE_PRESENCE_OF_
INTERFERENCE.
I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.Signature; x${ .<i3u>i\. X?. XLSLCTIA ,LJ ___ Name; ••O cTa:/? /-5, Q/,?£/-";4v-
Date: /5". //'ffj _____ Title: Jut<. t<- XV_____ _, *-' COVER PAGE - IN ILMO2 . 1
SR3I9559
SAMPLE DATA
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Lancaster LaboratoriesWhere quality is a science.
o<\Sample Reference List for SDG # CRT04
with a Package Type of CLPI
LabSample SampleNumber Code Client Sample Description
,.-1911840 BRIMT James Street Bridge Mid Tide Grab Water Sample' 1911841 BRMTF James street Bridge Mid Tide Filtered Grab Water1911842 MANMT Churchmans Road Mid Tide Grab Water Sample
r 0 1911843 MAMTF Churchmans Road Mid Tide Filtered Grab Waterj/i :/1911844 MANfTT Churchmans Road High Tide Grab Water Sample//\1911845 MAHTFJ Churchmans Road High Tide Filtered Grab Water
' 1911846 ROALT Churchmans Road Low Tide Grab Water Samplet_iai 184-7— ROLTF Churchmans Road Low Tide Filtered Grab Water1912267 RDLOT Churchmans Road Low Tide Grab Water Sample1912268 RDLTF Churchmans Road Low Tide Filtered Grab Water1912269 JASHT James Street Bridge High Tide Unspiked Grab Water1912270 JASHD James Street Bridge High Tide Unspiked Filtered1912271JASHTT" James street Bridge High Tide Matrix Spike Grab
\ 1912272 JASHT James Street Bridge High Tide Duplicate Grab*"' 1912273 JSBDF James Street Bridge High Tide Duplicate Filtered
1912274 JSLTI James Street Bridge Low Tide Grab Water Sample1912275 JSLTF James Street Bridge Low Tide Filtered Grab Water1912276 FBUNF Field Blank Grab Water Sample1912277 SBMIT James Street Bridge Mid Tide Grab Water Sample
•- 1912278 SBMTF_ James Street Bridge Mid Tide Filtered Grab Water1912279 CRMID Churchmans Road Mid Tide Grab Water Sample1912280 CRMDF Churchmans Road Mid Tide Filtered Grab Water
AR3I9565Larraster Laboratories, Inc. • 2425 New Holland Pike, Lancaster, FA 17601-5994 • 717-656-2301 • Fax:717-656-2681
iSro
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: LANCASTER LABORATORIES Contract:BRIMT
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911840Level (low/med): LOW_ Date Received: 12/30/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
GAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
26622.01.0
56.61.03.0
227005.05.05.0
10001.6887090.30.108.052801.0
11.0148002.06.0101
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
BRMTFLab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911841Level (low/med): LOW_ Date Received: 12/30/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
GAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.045.91.03.0
226005.05.05.076.61.0885077.70.108.046601.011.0161002.06.056.9
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SR3I9567
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: LANCASTER LABORATORIES Contract:MANMT
Lab Code: ______ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911842Level (low/med): LOW_ Date Received: 12/30/92
% Solids: ___0Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
38722.01.061.01.03.0
131005.05.05.015901.156601480.108.028501.011.0150002.06.074.7
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
MAMTFLab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911843__Level (low/med): LOW_ Date Received: 12/30/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
GAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration57.022.01.032.61.03.0
119005.05.05.01831.0
461027.00.108.027701.011.0515002.06.012.4
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Name: LANCASTER LABORATORIES Contract:MANHT
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911844Level (low/med): LOW_ Date Received: 12/30/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
39222.01.0
62.61.03.0
225005.05.05.011401.0884098.40.108.046601.0
11.0172002.06.0105
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Lab Name: LANCASTER LABORATORIES Contract:MAHTF
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
Matrix (soil/water): WATER Lab Sample ID: 1911845_Level (low/med): LOW_ Date Received: 12/30/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentr at ion
57.022.01.0
47.21.03.0
211005.05.05.0
59.31.0833088.30.108.044401.0
11.0163002.06.0111
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _____________
ROALTName: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1911846Level (low/med): LOW_ Date Received: 12/30/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration57.022.01.041.21.03.0
134005.05.05.03491.057101450.108.028501.011.0317002.06.044.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
ROLTFLab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1911847__
Level (low/med): LOW__ Date Received: 12/30/92
% Solids: ___0Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration107022.01.066.11.03.0
132005.05.05.029103.357902180.108.028301.011.0312002.06.071.0
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
RDLOTName: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1912267
Level (low/med): LOW_ Date Received: 12/31/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
59822.01.054.11.03.0
133005.05.05.017801.55630179
0.108.027401.011.0233002.06.043.2
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
RDLTFLab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1912268__
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.0
39.51.03.0
127005.05.05.02371.05380143
0.108.026001.0
11.0246002.06.0
30.0
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _______
JASHTName: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: ______ SDG No.: CRT04.
Matrix (soil/water): WATER Lab Sample ID: 1912269
Level (low/med): LOW_ Date Received: 12/31/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentrat i on28722.01.069.51.03.0
216005.05.05.0
12301.0856089.90.108.045201.011.0143002.06.595.8
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FORM I - INILMO2.1
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
JASHDLab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912270__Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration57.022.02.9
51.51.03.0
219005.05.05.091.41.0862077.70.108.045201.011.0146002.06.0
82.5
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U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
JSBDFName: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1912273
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercury-NickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.048.01.03.0
215005.05.05.01541.0854070.90.108.044101.011.0145002.06.058.1
C
UUuBUU
UUU
u
uuBUU
UU
Q
E ,W/
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
«
V
0
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I - INILM02.1
AR3I9578
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
JSLTILab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912274__
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration16922.01.0
51.51.03.0
209005.05.05.09951.0
819099.70.108.060301.0
11.0173002.06.0104
C
BUUBUU
UUU
U
UU
UU
UU
Q
E
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
rrU
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I - IN.ILM02.1
AR319579
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET __ _______
t j S L T FName: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1912275
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.0
57.51.03.0
220005.05.05.01181.0867091.60.108.046901.011.0181002.07.268.4
C
UUUBUU
UUU
U
UUBUU
UB
Q
E
W/
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I - INILM02.1
AR3I9580
U.S. EPA - CLP
1INORGANIC ANALYSES DATA SHEET
Lab Name: LANCASTER LABORATORIES Contract:
EPA SAMPLE NO.
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912276__
Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumcobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.0
r 1.0HI. 21.03.06495.05.05.07.01.01251.00.108.03111.011.07322.06.04.0
C
UUUBUUBUUUUUBUuuBUuBUuu
Q
E
W J
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
£.
J
\)
\>0
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:Clarity After: CLEAR Artifacts:
FORK I - IN .ILMO§.1
flR3i958l
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET ___
SBMITName: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER Lab Sample ID: 1912277
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
20222.01.0
54.11.03.0
211005.05.05.09471.08340107
0.108.042401.0
11.0166002.06.0100
C
UUBUU
UUU
U
UUBUU
UU
Q
E
W J
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I - INILM02.1
244R3I9582
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET _____________
Lab Name: LANCASTER LABORATORIES Contract:SBMTF
Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Lab Sample ID: 1912278__
Level (low/med): LOW_ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS NO.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.0
45.51.03.0
223005.05.05.01191.0869094.20.108.049001.0
11.0161002.06.0
54.9
C
UUUBUU
UUU
U
UUBUU
UU
Q
E
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:
Clarity After: CLEAR Artifacts:
FORM I - INILM02.1
25
flR3i9583
Kro
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
CRMIDName: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
Matrix (soil/water): WATER Lab Sample ID: 1912279
Level (low/med): LOW_ Date Received: 12/31/92
% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
38422.01.0
61.01.03.0
149006.55.05.022201.06280173
0.108.032501.0
11.0190002.06.0
43.2
C
UUBUU
BUU
U
UUBUU
UU
Q
E
W /
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
r
Color Before: COLORLESS Clarity Before: CLEAR_ Texture:Color After: COLORLESS Clarity After: CLEAR_ Artifacts:
Comments:
FORM I - IN' ILM02.1
3
U.S. EPA - CLP
1 EPA SAMPLE NO.INORGANIC ANALYSES DATA SHEET
Lab Name: LANCASTER LABORATORIES Contract:CRMDF
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
Matrix (soil/water): WATER Lab Sample ID: 1912280
Level (low/med): LOW__ Date Received: 12/31/92% Solids: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
CAS No.
7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Concentration
57.022.01.0
41.21.03.0
134005.05.05.03501.05720138
0.108.027101.011.0189002.06.0
20.3
C
UUuBU'U
UUU
U
UuBUU
UU
Q
E
M
PPFPPPPPPPPFPPCVPPFPPFPPNR
e.u
Color Before: COLORLESS
Color After: COLORLESS
Comments :
Clarity Before: CLEAR Texture:Clarity After: CLEAR Artifacts:
FORM I - INILM02.1
8
QUALITY CONTROL DATA
flR319586
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Initial Calibration Source: LLI_______Continuing Calibration Source: LLI_______
Concentration Units: ug/L
AnalyteAluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopper _____IronLeadMagnesiumManganeseMercuryNickel__ __PotassiumSeleniumSilverSodiumThalliumVanadium_ZincCyanide
Initial CalibrationTrue Found %R(1)25000.05000.050.0
5000.0500.05000.050000.05000.01000.05000.05000.020.0
25000.05000.0
2.510000.050000.0
20.0500.0
50000.040.0
2000.05000.0
24945.005156.1053.70
4983.70484.575064.6050853.005141.10994.405071.205160.3020.75
24340.005160.90
2.5410199.0051207.00
20.05507.12
50117.0042.40
2062.705142.10
99.8103.1107.499.796.9101.3101.7102.899.4101.4103.2103.897.4103.2101.6102.0102.4100.2101.4100.2106.0103,1102.8
Continuing CalibrationTrue Found %R(1) Found %R(1)
25000.05000.050.0
5000.0500.05000.050000.05000.01000.05000.05000.020.0
25000.05000.0
1.010000.050000.0
20.0500.0
50000.040.0
2000.05000.0
25222.005175.4050.67
4988.90488.665108.1050869.005199.80991.865131.905219.7020.06
24650.005209.20
0.9810289.0050953.00
20.42515.73
50659.0041.40
2057.505194.80
100.9103.5101.399.897.7102.2101.7104.099.2102.6104.4100.398.6104.298.0102.9101.9102.1103.1101.3103.5102.9103.9
24998.005104.0051.03
4997.90483.715073.4050512.005157.10989.925112.105155.9020.53
24327.005163.90
0.9810188.0050599.00
19.38509.63
49024.0042.20
2066.905140.90
100.0102.1102.1100.096.7101.5101.0103.199.0102.2103.1102.697.3103.398.0101.9101.296.9101.998.0105.5103.3102.8
M
f-PFPPP_PiFPP~CVPPFPPFPP~NR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM02.1
-•;•« £7flR3l9587
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Initial Calibration Source: LLI_______
Continuing Calibration Source: LLI_______
Concentration Units: ug/L
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalcium^ChromiumMpalt,_ppperTironLeadMagnesiumManganeseMercuryNickel.. ___PotassiumSelenium_SilverSodiumThalliumVanadiumZincCyanide _
Initial CalibrationTrue Found %R(1)
40.0 42.80
————
107.0
Continuing CalibrationTrue Found %R(1) Found %R(1)
25000.05000.0
50.05000.0500.0
—— 5000.050000.05000.01000.05000.05000.0
20.025000.05000.0
1.010000.050000.0
20.0500.0
50000.040.0
2000.05000.0
25342.005213.1049.25
5106.80490.495136.3051833.005116.801008.505175.005219.9020.20
24898.005224.50
0.9610310.0051559.00
18.70512.85
50334.0043.40
2115.005199.00
101.4104.398.5
102.198.1
102.7103.7102.3100.8103.5104.4101.099.6104.596.0
T03.1103.193.5
102.6100.7108.5105.8104.0
25843.005270.7050.37
4989.70498.53
"5206.4050588.005347.50991.175257.705325.2020.79
24644.005309.30
0.9410485.0050670.00
19.14525.05
49960.0043.80
2068.605286.00
103.4105.4100.799.899.7
104.1101.2107.099.1
105.2106.5104.098.6
106.294.0
104.8101.395.7
105.099.9
109.5103.4105.7
M
P~PFPPP~PPPP~PFPPCVPPFPPFPPNR
(l) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM02.1
SR3I9588
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Initial Calibration Source: LLI_______
Continuing Calibration Source: LLI_______
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobalt __CopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Initial CalibrationTrue Found %R(1)
Continuing CalibrationTrue Found %R(1) Found %R(1)
50.0
5000.0
___ 20.0
20.0
40.0
48.72
5291.30
___ 21.07
20.30
43.70
_ _ _ — _ — _
97.4
105.8
105.4
101.5
109.2
48.20
___ 21.28
20.72
42.00
_96.4
106.4
103.6
105.0
M
NRNRFNRNRNRNR
39FNKNRNRNRNRFNRNRFNRNRNR
»
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILMO2.1
HR3I9589
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: _______ SDG No.: CRT04_Initial Calibration Source: LLI_______
Continuing Calibration Source: LLI_______
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenic _BariumBerylliumCadmiumCalciumChromium•bait•bperxronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide _
Initial CalibrationTrue Found %R ( 1 )
20.0 20.67
————
103.4
Continuing CalibrationTrue Found %R(1) Found %R(1)
20.0
40.0
19.64
41.50
98.2
103.8
18.99
————
95.0
M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRFNRNRNR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM02 . 1
AR3I9590
U.S. EPA - CLP
2AINITIAL AND CONTINUING CALIBRATION VERIFICATION
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Initial Calibration Source: LLI_______Continuing Calibration Source: LLI_______
Concentration Units: ug/L
Analyte
AluminumAntimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Initial CalibrationTrue Found %R(1)
Continuing CalibrationTrue Found %R(1) Found %R(1)
20.0 20.26
————
101.3
————
20.44
————
102.2
M
NRNRNRNRNRNRNRNR|mNWNRNRNRNRNRNRFNRNRNRNRNRNR
(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115
FORM II (PART 1) - IN
ILM02.1
HR31959I
U.S. EPA - CLP
2BCRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
AA CRDL Standard Source: LLI________
ICP CRDL Standard Source: LLI_______
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium^ alt| K>erITonLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL £
True
10.0
3.0
0.2
5.0
10.0
Standard fc
Found
11.37
2.66
0.16
4.92
11.90
>r AA
%R
113.7
88.7
80.0
98.4
119.0
True
100.0
100.0
CRDL StarInitialFound
105.16
109.69
idard i%R
105.2
109.7
:or ICPFina]
Found
97.64
105.35
L%R
97.6
105.4
o,\vFORM II (PART 2) - IN
ILMO2.1
' "32HR3I9592
U.S. EPA - CLP
26CRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
AA CRDL Standard Source: LLI________
ICP CRDL Standard Source: LLI
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL £
True
5.0
10.0
Standard fcFound
4.87
10.40
>r AA
%R
97.4
104.0
True
120.0
10.010.0
50.0
30.0
80.0
20.0
40.0
CRDL StarInitialFound
119.13
8.889.02
50.09
30.93
70.37
18.63
40.32
idard 1%R
99.3
88.890.2
100.2
103.1
88.0
93.2
100.8
:or ICPFina]
Found
129.60
8.879.92
50.54
31.78
72.26
20.79
41.91
%R
108.0
88.799.2....
4101 .•™
105.9
90.3
104.0
104.8
FORM II (PART 2) - IN
• ILM02.1
IT' 33
SR3I9593
U.S. EPA - CLP
2BCRDL STANDARD FOR AA AND ICP
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ______ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
AA CRDL Standard Source:ICP CRDL Standard Source: LLI
Concentration Units: ug/L
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium^ •alt^ HBerronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
CRDL £
True
Standard fc
Found
ar AA
%R True
20.0
CRDL StarInitialFound
19.72
idard J
%R
98.6
for ICPFina]
Found
22.58
L%R
112.9
j \ • FORM II (PART 2) - IN
VO ILMO2.1
*•*._?•
. , . 24AR3I959I*-
U.S. EPA - CLP
3BLANKS
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Preparation Blank Matrix (soil/water): WATERPreparation Blank Concentration Units (ug/L or mg/kg): UG/L_
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_ _____PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
57.022.01.34.01.03.0
-73.5——— 5.0 ——
5.08.2
-44.41.0
-80.71.00.18.0
132.01.0
11.065.02.06.04.0
UUBUUUBUUBBUBUUUuuuuuuu
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
-77.922.01.0
24.01.03.0
239.15-.05.0
10.4-40.11.0
93.31.00.18.0
282.31.0
11.065.02.0
12.24.0
BUUBUUBUUBBUBUUuBUuuuBU
-62.122.01.0
34.31.03.0
278.15.05,05.1
-43.81.0
88.52.50.18.0
395.21.0
11.065.02~rQr=
(16.6\ J
BUUBUUBUUBBUBBUUBUUU
$U
-84.722.01.0
67.81.03.0
629.2——— • 5.0"
11.55.0
-46.31.0
241.81.00.1
-10.6734.0r.o11.0
___ 65 . 0_
28.44.0
BUUBUUBUBUBUBUUBBUUU
BU
Prepa-rationBlank C57.00022.0001.0004.0001.0003.000
-60.400——— 5.000
5.0005.000
-38.9001.000
-78.3001.0000.100
-12.500169.500
1.00011.00065.0002.0006.0004.000
UUUUUUBUUuBUBUUBBUUuuuu
M
P——PFPPP
APPFPPCVPPFPPFPPNR
FORM III - INILM02.1
,... 25
AR3I9595
U.S. EPA - CLP
3BLANKS
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Preparation Blank Matrix (soil/water): ____
Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumkcium^VomiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. _PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
-2.8 B
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
57.022.01.0
63.91.03.0
933.75.09.59.7
-35.21.0
600.43.00.18.0
621.01.0
11.065.0-2.030.04.0
UUUBUUBUBBBUBBUUBUUUBBU
-1.0
5.0
1.0
1.0
-2.8
B
U
U
U
B
1.0
-1.2
1.0
-3.3
U
B
U
B
Prepa-rationBlank C M
PPFPPPPPPPPFPPCVPPFPPFPPNR
FORM III - INILM02.1
AR3I9596
U.S. EPA - CLP
3BLANKS
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Preparation Blank Matrix (soil/water): ____
Preparation Blank Concentration Units (ug/L or mg/kg): ____
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel ______PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) C
1.0 U
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
1.0
-2.5
U
B
1.0
-4.0
U
B
1.0 U
Prepa-rationBlank C M
NRNRNRNRNRNR,,
NlPNRNRNRNRNRNRNRNRF "~NRNRFNRNRNR
FORM III - INILM02.1
AR3I9597
U.S. EPA - CLP
3BLANKS
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ______ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Preparation Blank Matrix (soil/water): ____Preparation Blank Concentration Units (ug/L or mg/kg):
Analyte
AluminumAntimonyArsenicBariumBeryllium^gdmiumBlcium^BromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. ______PotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
InitialCalib.Blank(ug/L) c
Continuing CalibrationBlank (ug/L)
1 C 2 C 3 C
1.0 U
Prepa-rationBlank C M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNR
FORM III - INILM02.1
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 4725-PE51 GF_ Method: F_
start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
ROLTFACCVCCBRDLOTRDLOTARDLTFRDLTFAJASHTJASHTAJASHDJASHDAJASHT SZZZZZZCCVCCBJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCVCCBSBMTFSBMTFACRMIDCRMIDACRMDF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
16531657170217071712171617211726173117361741174517511755180018051810181518201825183018351840184518501855185919041909191419191924
% R
(84 . 7,- — -
89.1
85.3
85.9s~* \
/81vO( /
84.6
93.7
89.6
85.5
105.5
78.2
(83. £
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FORM XIV - IN ILM02.1
~" 84
SR3I9599
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04.
Instrument ID Number: 4725-PE51 GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
CRMDFASBMITSBMITACCVCCB
•=
D/F
1.001.001.001.001.00
Time
19291934193919441948
% R
90.2
35.5
AL
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FORM XIV - IN ILM02.1
"" 85flR319600
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04.
Instrument ID Number: 4725-PE51 GF_ Method: F_
Start Date: 01/05/93 End Date: 01/06/93
EPASampleNo.
soS5S15S25S40S50ICVICBCRACCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZ
D/F
1.001.001.001.001.001.001.001.001.001.001.0010.0010.0010.0010.005.005.005.005.0010.0010.001.001.001.001.001.001.0010.0010.0010.0010.001.00
Time
22362241224522502255230023052310231423192324232923342339234423492354235900040009001400180023002800330038004300470052005701020107
% R ALSBAS
—
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XX
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FORM XIV - IN ILM02.1
QR31960I
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 4725-PE51 GF_ Method: F_
Start Date: 01/05/93 End Date: 01/06/93
EPASampleNo.
ZZZZZZCCVCCBZZZZZZZZZZZZZZZZZZZZZZZZSBMTFSBMTFASBMITSBMITAIzzzzzz•EZZZ
WB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
011201170121012601310135014001450150015502000205021002150219
% R
^ __
/ " ~\(_103y4NX— - ~ //£3 yX.
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FORM XIV - IN ILMO2.1
87
^319602
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 3812-V40Z GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
SOsioS25S50S75S100ICVICBCRACRAACCVCCBPBWPBWALCSWLCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001,001.001.001.001.001.001.001.001.001.001.001.001.00
Time
145315001506151315201526153215391545155215581604161116171623163016361643164916561702170917151721
% R
108.5
133.1
113.9
108.3
111.0
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FORM XIV - IN ILM02.1
• ;_•;_" es6R319603
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No. :CRT04_
Instrument ID Number: 2803-V400 GF_ Method: F_Start Date: 01/04/93 End Date: 01/05/93
EPASampleNo.
SOS10S25S50S75S100ICVICBCRACRAAIccvLCCB•ezzz•ezzzMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTACCVCCBROLTFROLTFARDLOTRDLOTARDLTFRDLTFAJASHTJASHTA
D/F
1.001.001.001.001.001.001.001.001.001.001.001.005.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
20192025203220392045205220582104211021172123213021362143214921562202220922152221222822342241224722532300230623132319232523312338
•
% R
••==*•— (118.6)\ _ '112.7
112.2
107.9
106.1
104.9
110.5
106.0
ALSBASBABECDCACRCO
Arcu
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XXXXXXXXX
XX
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V zNcN
FORM XIV - IN ILMO2.1
flR3!960t4
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 2803-V400 GF_ Method: F_Start Date: 01/04/93 End Date: 01/05/93
EPASampleNo.
JASHDJASHDACCVCCBJASHT SZZZZZZJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFACCVCCBFBUNFFBUNFASBMTFSBMTFACRMIDCRMIDACRMDFCRMDFASBMITSBMITACCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
2344235123570004001000160023002900350042004800550101010801140121012701340140014701530200020602130219022602320239
% R
109.4
108.6
111.9
114.0^
(123 0\_S
— VOO A_ e107.9
113.6
111.9-
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ALSBASBABECDCACRCO
Ar
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FORM XIV - IN . ILMO2.1
SO
AR3I9605
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _______ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3998-V20 AA Method: CV
Start Date: 01/06/93 End Date: 01/06/93
EPASampleNo.
SOSO. 2SO. 5Sl.OS2.5S5.0ICVICBCRACCVICCBLfiBW^KW•|MTT?RMTFMANMTMAMTFMANHTMAHTFROALTROLTFCCVCCBRDLOTRDLTFJASHTJASHDJASHT SJASHT DJSBDFJSLTIJSLTF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
09050906090809090911091209140915091709180920092109230924092609270929093009320933093509360938093909410942094409450947094809500951
% R ALSBASBA
BECDCACRCO
Al
CU
iaJFE
LytpB
;esMGMNHG
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
NIK SEAGNATLV ZNCN
FORM XIV - IN ILMO2.1
SI
3R3I9606
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04.
Instrument ID Number: 3998-V20 AA Method: CVStart Date: 01/06/93 End Date: 01/06/93
EPASampleNo.
FBUNFCCVCCBSBMITSBMTFCRMIDCRMDFZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZCCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
095309540956095709591000100210031005100610081009101110121014
% R ALSBASBABECDCACRCO
ArcU
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XXXXXXX
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1
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FORM XIV - IN ILM02.1
SR3I9607
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS .No. : _____ SDG No.:CRT04_
Instrument ID Number: 2360-ICP1100_ Method: P_
Start Date: 01/01/93 End Date: 01/01/93
<1.
EPASampleNo.
SOSSSSSICVICBICSAICSABCRICCVUp v.•F•BCSWJASHT -JASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCV•GCB vv%>MAMTFMANHTMAHTFROALTROLTFRDLOTRDLTF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
19001904190819121915191819211925193019341939194319481952195720012006201020152020202420292033203820422047205120562101210521102114
% R ALSBASBA
XX
XXXX
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FORM XIV - IN ILM02.1
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 2360-ICP1100_ Method: P_
Start Date: 01/01/93 End Date: 01/01/93
EPASampleNo.
JASHDJSBDFJSLTICCVCCB 1-7 ."VJSLTF -(FBUNFISBMITSBMTFCRMIDCRMDFICSAICSABCRICCVICCB \,T>,4' '
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
2119212421282133213721422146215121562200220522092214221922232228
% R ALSBASBA
XXXXXXXXXXXXX
XX
BECDCA
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XX
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FORM XIV - IN ILM02.1
70
AR3I9609
oro
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 2360-ICP1100_ Method: P_
Start Date: 01/05/93 End Date: 01/06/93
EPASampleNo.
soSSSsSICVICBICSAICSABCRICVVW*TTCSWJASHTJASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCVCCBMAMTFMANHTMAHTFROALTROLTFRDLOTRDLTF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
21372145214821532156215822012205221022142219222422282233223722422246225122552300230423092313231823232327233223362341234523502354
•
% R AL
X
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71
R3I9610
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 2360-ICP1100_ Method: P_
Start Date: 01/05/93 End Date: 01/06/93
EPASampleNo.
JASHDJSBDFJSLTICCVCCBJSLTFFBUNFSBMITSBMTFCRMIDCRMDFICSAICSABCRICCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
2359000400080013001800220027003100360041004500500055005901040109
% R AL
XXXXXXXXXXXXX
XX
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FORM XIV - IN ILM02.1
HR3I96
IBs
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3144-ICP61__ Method: P_
Start Date: 01/07/93 End Date: 01/07/93
EPASampleNo.
SOsSSSslevICBICSAICSABCRI«£CVKVzzzzTcvCCBPBWLCSWJASHTJASHT AJASHT DJASHT SJASHT LBRIMTBRMTFMANMTCCVCCBMAMTFMANHTMAHTFROALT
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.0025.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.00
Time
10011006101010141017102010231027103210371041104610511056110011051110111411191124112911331138114311471152115712021206121112161221
% R ALSBASBABECDCACR
XX
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FORM XIV - IN ILM02.1
73
flR3196(2
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 3144-ICP61__ Method: P_
Start Date: 01/07/93 End Date: 01/07/93
EPASampleNo.
ROLTFRDLOTRDLTFJASHDJSBDFJSLTICCVCCBJSLTFFBUNFSBMITSBMTFCRMIDCRMDFICSAICSABCRICCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
1225123012351240124412491254125913031308131313181322132713321337134113461351
% R ALSBASBABECDCACR
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c0
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FORM XIV - IN ILM02.1
' 74
SR3I9613
KHD
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3144-ICP61__ Method: P_Start Date: 01/08/93 End Date: 01/08/93
EPASampleNo.
SOSSSSSICVICBICSAICSABCRI.CCV•PV*TcswJASHDZZZZZZJASHT DJASHT SJASHD LRDLOTRDLTFJASHTCCVCCBJSBDFJSLTIJSLTFFBUNFSBMITSBMTFCRMID
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
01120118012201260129013201350140014401490154015802030208021302170222022702310236024102460250025503000305030903140319032403280333
% R ALSBASBABECDCACRC0
AT
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FORM XIV - IN ILMO2.1
75
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3144-ICP61__ Method: P_
Start Date: 01/08/93 End Date: 01/08/93
EPASampleNo.
CRMDFBRIMTBRMTFCCVCCBMANMTMAMTFMANHTMAHTFROALTROLTFICSAICSABCRICCVCCB
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
0338034303470352035704020406041104160421042504300435044004440449
% R ALSBASBABECDCACRC0
Ar
CU
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FE
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5
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XXXXXXXXXXXXX
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FORM XIV - IN ILM02.1
SR3I96I5
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 4724-PE51 GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
SOS10S20S40S60S80ICV-,ICCRACCVCCB wj-jLEBW•HA•BWTCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCB V>\;MAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTAROLTF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
15071511151615201524152915341538154215471551155616001605160916141618162316271632163616411645164916541658170317071712171617201725
% R
102.8
96.1
107.1
__ 105.1
100.9
101.1
94.6.-
-f71*,8'85.8
Analytes
ALSBAS
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
BABECDCACRCOCUFEPBMGMNHGNIK SEAGNATLV ZNCN
FORM XIV - IN ILM02.1
,.. ' 77
3R3I9616
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04_Instrument ID Number: 4724-PE51 GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
ROLTFACCV _CCB *>\)RDLOTRDLOTARDLTFRDLTFAJASHTJASHTAJASHDJASHDAJASHT SZZZZZZCCVCCB UOJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCV ,CCB -\SBMTFSBMTFACRMIDCRMIDACRMDF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
17291734173817421747175117551800180418081813181718221826183118351839184418481853185719021907191119161920192419291933193819431947
% R
93.1
108.8
91.0
101.3— "*>
f 76. )6\ _ /
92.8
94.0
88.7
94.2
87.4
93.6
89.4
ALSBAS
XXXXXXXXXXXX
XXXXXXXXXXXXXXXXXXX
BABECDCACRCO
Ar
CU
laJ
FE
•ytpB
:es
MGMNHGNIK SEAGNATLV
•
ZN
*
CN
FORM XIV - IN ILM02.1
ftR3196i7
U.S. EPA - CLP
14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04.
Instrument ID Number: 4724-PE51 GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
CRMDFASBMITSBMITAZZZZZZZZZZZZCCVCCB vl J
r=
D/F
1.001.001.001.001.001.001.00
Time
1952195620002005200920142018
% R
93.9
93.7
ALSBAS
XXX
XX
BA
BECDCACRCO
Ar
CU
ia]
FE
iy1
PB
:es
MG
;
MNHGNIK SEAGNATLV ZNCN
FORM XIV - IN ILM02.1
„... 78
AR3I96I8
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3812-V40Z GF_ Method: F_Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
SOS5S10S25S40S50ICVICBCRACRAACCVCCBPBWPBWALCSWLCSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCBMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTA
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
10131019102610331040104610521059110511121118112411311138114411511157120412101217122312301236124312491256130213091315132213281335
% R
101.2
103.8
89.2__ _ ,_
'82.9,. _ •"92.8
>8"l7)DCL--89.5
85.3
,-81.7v x
AL
/'
SBASBABECDCACRC0
Ar
CU
laJ
FE
-ytpB
XXXXXXXXX
XXXXXXXXXXXXXXXXXXXXXX
:e£
MGMNHGNIK SEAGNATLV ZN
t
CN
»
FORM XIV - IN ILM02.1
-' 80
SR3196I9
U.S. EPA - CLP
, 14ANALYSIS RUN LOG
Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 3812-V40Z GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
ROLTFROLTFACCVCCBRDLOTRDLOTARDLTFRDLTFAJASHTJASHTA
I JASHDtASHDAKHT S•zzzzIccvCCBJASHT DJASHT DAJSBDFJSBDFAJSLTIJSLTIAJSLTFJSLTFAFBUNFFBUNFACCVCCBSBMTFSBMTFACRMIDCRMIDA
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
13411348135414001407141314201427143314401446145314591506151215191525153215381545155115581605161216181625163116381644165116571704
% R
88.2
91.6
86.1
88.6-r>
x84 ;'jw( — -'"
86.3-———— T-s
,84.9^ — ---••"'90.2
85.7
102.8
85.9
97.4
AL
t
SBASBABECDCACRCO
ArcU
laJ
FE
Lyi
PB
XXXXXXXXXXXXX
XXXXXXXXXXXXXXXXXX
:es
MG
3
MNHGNIK SEAGNATLV ZNCN
FORM XIV - IN ILM02.1
81
HR3I9620
U.S. EPA - CLP
14ANALYSIS RUN LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.:CRT04_
Instrument ID Number: 3812-V40Z GF_ Method: F_Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
CRMDFCRMDFASBMITSBMITAZZZZZZZZZZZZCCVCCB
D/F
1.001.001.001.001.001.001.001.00
Time
17111718172417311737174417501757
% R
93.9
93.0
ALSBASBABECDCACRC0
Ar
CU
ial
FE
-ytpB
XXXX
XX
;es
MG
i
MNHGNIK SEAGNATLV ZN
-<
1
cN
FORM XIV - IN ILM02.1
'82
&R319621
U.S. EPA - CLP
14ANALYSIS RUN LOG
ame: LANCASTER LABORATORIES__ Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.:CRT04.Instrument ID Number: 4725-PE51 GF_ Method: F_
Start Date: 01/04/93 End Date: 01/04/93
EPASampleNo.
soS5S15S25S40S50ICVICBCRACCVCCBIPBW•LAV"WSWABRIMTBRIMTABRMTFBRMTFAMANMTMANMTACCVCCBMAMTFMAMTFAMANHTMANHTAMAHTFMAHTFAROALTROALTAROLTF
D/F
1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00
Time
14171422142614311436144014461450145515001505150915151519152515291535153915441549155415591604160916141618162316281633163816431648
•
% R
105.4
113.5-x—— ' -•
/ ''84.8'^ ^86.2
91.1
. y*2.TJ—/89.7
85.6x- 82/2
V^'-
ALSBASBA
BECDCACRCO
Arcu
laJFE
LylpB
:es
MG
5
MNHGNIK SE
XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX
AGNATLV ZNCN
FORM XIV - IN ILMO2.1
83
flR3J9622
U.S. EPA - CLP
4ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No: _____ SDG No.: CRT04_
ICP ID Number: 2360-ICP1100 ICS Source: LLI _____
Concentration Units: ug/L
TrueSol. Sol.
Analyte A AB
AluminumAntimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSelenium_SilverSodiumThalliumVanadiumZinc
0
500000
0
500000
0
500
_500000
500
_500000
500
Initial FoundSol. Sol.A AB %R
11
_484640
-2
_500700
11
478.9
_484840.0
443.6
_501250.0
478.7
95.8
_97.0
88.7
100.2
95.7
Final FoundSol. Sol.A AB %R
6
_486500
0
_503570
9
491.6
_503680.0
452.4
_520080.0
493.8
98.3
100.7
90.5
104.0
98.8
FORM IV - IN
ILMO2.1
AR3I9623
U.S. EPA - CLP
4ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No: _____ SDG No.: CRT04_
ICP ID Number: 2360-ICP1100 ICS Source: LLI
Concentration Units: ug/L
TrueSol. Sol.
Analyte A AB
AluminumAntimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltpopper•ronPeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadium_Zinc
500000
00
0200000
0
0
0
0
_500000
5001000
500200000
500
1000
1000
1000
Initial FoundSol. Sol.A AB %R
_490050
028
8186430
-13
-40
-38
-8
_491950.0
454.6918.8
480.2187170.0
453.9
857.8
961.1
933.8
_98.4
90.991.9
96.093.6
90.8
85.8
96.1
93.4
Final FoundSol. Sol.A AB %R
_497770
030
7188780
-14
-39
-41
-9
_509010.0
470.5953.8
502.5193190.0
468.8
888.6
993.9
959.9
101.8
94.195.4
100.596.6
93.8
88.9
99.4
96.0
FORM IV - IN
ILMO2.1
U.S. EPA - CLP
4ICP INTERFERENCE CHECK SAMPLE
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No. : _____ SAS No: _____ SDG No. : CRT04_
ICP ID Number: 3144-ICP61 ICS Source: LLI
Concentration Units: ug/L
TrueSol. Sol.
Analyte A AB
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel.. __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc
0 500
Initial FoundSol. Sol.A AB %R
73 525.0 105.0
Final FoundSol. Sol.A AB %R
73 532.0 106.4
FORM IV - IN
ILMO2.1
AR319625
U.S. EPA - CLP
5A EPA SAMPLE NO.SPIKE SAMPLE RECOVERY
JASHT SName: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water): WATER_ Level (low/med): LOW_
% Solids for Sample: _0.0Concentration Units (ug/L or mg/kg dry weight): UG/L_
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperJLron»d _____•gnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit%R
75-12575-12575-12575-12575-12575-125
75-12575-12575-12575-12575-125
75-12575-12575-125
75-12575-125
75-12575-12575-125
Spiked SampleResult (SSR)
2390.0000464.100040.1500
1893.200046.720046.9300
189.5900463.5700240.66002053.000016.1400
560.37000.9500
474.5600
9.000045.2100
59.7000477.8300573.1600
CSample
Result (SR)
286.520022.00001.000069.52001.00003.0000
5.00005.00005.0000
1234.60001.0000
89.91000.10008.0000
1.000011.0000
2.00006.480095.8200
C
UUBUU
UUU
U
UU
UU
UB
SpikeAdded (SA)
2000.00500.0040.00
2000.0050.0050.00
200.00500.00250.001000.0020.00
500.001.00
500.00
10.0050.00
50.00500.00500.00
%R
105.292.8100.491.293.493.9
94.892.796.381.880.7
94.195.094.9
90.090.4
119.494.395.5
Q M
PPFPPPNRPPPPFNRPCVPNRFPNRFPPNR
Comments:
FORM V (Part 1) - IN ILM02.1
42
U.S. EPA - CLP
6 EPA SAMPLE NO.DUPLICATES
JASHT DLab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Matrix (soil/water) : WATER . Level (low/med) : _LOW____
% Solids for Sample: ___0 % Solids for Duplicate: ___0
Concentration Units (ug/L or mg/kg dry weight): UG/L_
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
ControlLimit200.0
5000.0
5000.0
5000.0
20.0
Sample (S)
286.520022.00001.000069.52001.00003.0000
21555.00005.00005.00005.0000
1234.60001.0000
8562.700089.91000.10008.0000
4520.60001.000011.0000
14311.00002.00006.480095.8200
C
UUBUU
UUU
U
UuBUU
UB
Duplicate (D)
323.140022.00001.000068.66001.00003.0000
21360.00005.00005.00005.0000
1209.90001.1000
8451.300089.07000.10008.0000
4435.80001.000011.0000
15610.00002.00007.560084.2800
C
UUBUU
UUU
B
UUBUU
UB
RPD
12.0
1.2
0.9
2.0200.01.30.9
1.9
8.7
15.412.8
Q M
PPFPPPPPPPPFPPCVPPFPPFPPNR
FORM VI - INILM02.1
AR3I9627
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Solid LCS Source: __________
Aqueous LCS Source: LLI________
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltfcpoer_____PbnjBeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide
Aqueous (ug/L)True Found %R
2000.0500.040.0
2000.050.050.0
4000.0200.0500.0250.01000.020.0
2000.0500.01.0
500.04000.010.050.0
50.0500.0500.0
1979.60527.7641.68
2103.8052.4053.98
4663.60208.63524.37274.241061.4018.80
2074.30542.040.93
537.574671.60
9.3854.32
50.60540.39552.03
99.0105.6104.2105.2104.8108.0116.6104.3104.9109.7106.194.0103.7108.493.0107.5116.893.8108. 6_
101.2108.1110.4
Solid (mg/kg)True Found C Limits %R
—
—
FORM VII - INILM02.1
U.S. EPA - CLP
7LABORATORY CONTROL SAMPLE
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
Solid LCS Source: __________
Aqueous LCS Source: LLI_______
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_i ______PotassiumSeleniumSilver ______SodiumThalliumVanadiumZincCyanide
Aqueous (ug/L)True Found %R
4000.0 4202.90 105.1
Solid (mg/kg)True Found C Limits %R
—
31
FORM VII - INILM02.1
„ 45AR3I9629
Kfo
U.S. EPA - CLP
8STANDARD ADDITION RESULTS
Cab Name:
Lab Code:
LANCASTER LABORATORIES
Case No. :
Contract :
SAS No. : SDG No. :CRT04
Concentration Units: ug/L
EPASampleNo.
'= ——•=
An
—
—
0 ADDABS
1 ADDCON ABS
2 ADDCON ABS
3 ADDCON ABS
FinalCone. r Q
—
—
—
—
_
FORM VIII - IN ILMO2.1
II ' 46
flR3i9630
U.S. EPA - CLP
9 EPA SAMPLE NO.ICP SERIAL DILUTION
JASHD LLab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_Matrix (soil/water): WATER Level (low/med): LOW_
Concentration Units: ug/L
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Initial SampleResult (I)
14642.00
C
SerialDilutionResult (S)
14806.50
C
B
%Differ-ence
l.i
Q M
P
FORM IX - INILM02.1
„...: 47SR3I963
U.S. EPA - CLP
9 EPA SAMPLE NO.ICP SERIAL DILUTION
JASHT LName: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
Matrix (soil/water): WATER Level (low/med): LOW_
Concentration Units: ug/L
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Initial SampleResult (I)
286.5222.00
69.521.003.00
21555.005.005.005.00
1234.60
8562.7089.91
8.004520.60
11.00
6.4895.82
C
U
BUU
UUU
UB
U
B
SerialDilutionResult (S)
285.00110.00
128.705.00
15.0022371.00
25.0025.0025.00
1052.50
8545.5090.75
40.005509.00
55.00
30.00256.55
C
UU
BUUBUUU
B
UB
U
U
%Differ-ence
100.0
85.1
3.8
14.7
0.20.9
21.9
100.0167.7
Q
E
M
PP
PPPPPPPP
PP
PP
P
PP
FORM IX - INILM02.1
. C8
HR3I9632
VERIFICATION OF INSTRUMENT PARAMETERS
43f • •*
SR3I9633
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: 2360-ICP1100 Date: 10/15/92
Flame AA ID Number : __________
Furnace AA ID Number :
Comments:
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
308.22206.84
493.41313.04226.50317.93
228.62324.75259.94
279.08257.61
231.60766.49
328.07
292.40213.86
Back-ground
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
5000105020
IDL(ug/L)
57.022.0
4.01.03.0
23.0
5.05.07.0
45.01.0
8.0132.0
11.0
6.04.0
M
PPNRPPP .PNRPPPNRPPNRPPNRPNRNRPP
FORM X - IN ILMO2.1
HR3I963U
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
Lab Name: LANCASTER LABORATORIES__ Contract: _________
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
ICP ID Number: 3144-ICP61_ Date: 10/15/92
Flame AA ID Number : 3998-V20_AA_
Furnace AA ID Number :
Comments:
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
267.72
253.65
589.59
Back-ground
CRDL(ug/L)
200601020055
5000105025100
35000
150.240
5000510
5000105020
IDL(ug/L)
5.0
0.1
65.0
M
NRNRNRNRNRNRNRPNRNRNRNRNRNRCVNRNRNRNRPNRNRNR
FORM X - IN ILM02.1
51
SR319635
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: __________ Date: 10/15/92
Flame AA ID Number : _____________Furnace AA ID Number : 2803-V400 GF
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
276.80
Back-ground
BD
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
5000105020
IDL(ug/L)
2.0
M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNR
Comments:
FORM X - IN ILMO2.1
&R319636
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: __________ Date: 10/15/92
Flame AA ID Number : __________
Furnace AA ID Number : 3812-V40Z GF
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganesfeMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
283.30
276.80
Back-ground
BZ
BZ
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
5000105020
IDL(ug/L)
1.0
1.0
M
NRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNRNRNRNRFNRNR
Comments:
FORM X - IN ILMO2.1
8R319637
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
ame: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: __________ Date: 10/15/92
Flame AA ID Number : _________
Furnace AA ID Number : 4724-PE51 GF
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
193.70
Back-ground
BZ
CRDL(ug/L)
200601020055
5000105025100
35000150.240
5000510
5000105020
IDL(ug/L)
1.0
M
NRNRFNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNR
Comments:
FORM X - IN ILMO2.1
54
flR3i9638
U.S. EPA - CLP
10Instrument Detection Limits (Quarterly)
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: __________ Date: 10/15/92
Flame AA ID Number : __________
Furnace AA ID Number : 4725-PE51 GF
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length(nm)
196.00
Back-ground
BZ
CRDL(ug/L)
200601020055
50001050251003
5000150.240
5000510
5000105020
IDL(ug/L)
1.0
M
NRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRNRFNRNRNRNRNR
Comments:
FORM X - IN ILM02.1
...... 55
&R319639
ram
U.S. EPA - CLP
11AICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04.ICP ID Number: 2360-ICP1100 Date: 01/15/92
AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalcium ______ChromiumCobaltCopperIroniead•gnesiumHnganeseMercuryNickel.. _____PotassiumSeleniumSilverSodiumThallium_Vanadium_Zinc
Wave-length(nm)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __
231.60766.49196.03328.07589.59377.57292.40213.86
Ir
Al
0.0000000-0.0000120-0.00711200.00000000.0000000-0.00003900.00000000.00000000.00000000.00000000.0000000-0.00098300.0000000
_0. 0005890
0.00001000.00000000.00021300.00000000.00000000.00067900.00000000.0000350
iterelement C
Ca
0.0001640"0. 00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000320-0.00001100.0000890
_0.0000000_
0.00000000.00021400.00001700.00001700.0000000-0.00024200.00000000.0000000
Correction I
Fe
0.00000000.0001220-0.0071120-0.00003200.00000000.0000710-0.00001700.0000050-0.00000400.00001100.00000000.00000000.0002080
_0. 0000460
0.00008100.00000000.00004200.00006300.00000000.0000460-0.00003000.0001160
?actors for
Mg
0.00023400.00000000.00000000.00000000.00000000.00000900.00039600.0000080-0.00000200.00000000.0000600-0.00001900.0000000
_0. 0000280
0.0000000-0.0000270-0.00008100.00000000.00000000.00001100.00000000.0000380
••
BE_
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000-0.0031410_0. 0000000
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000
Comments:
FORM XI (Part 1) - IN ILM02.1
U.S. EPA - CLP
11AICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: 3144-ICP61_ Date: 01/15/92
AnalyteAluminum_Antimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobalt _____Copper _____IronLeadMagnesiumManganeseMercuryNickel _____PotassiumSelenium__SilverSodium _____ThalliumVanadium_Zinc
Wave-length(nra)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08
_257.61 __
231.60766.49196.03328.07589.59377.57292.40213.86
Interelement Correction Factors for :
Al Ca Fe Mg C0_0.00000000.00000000.00023100.00000000.00000000.00000000.0000150-0.00002400.00000000.00000000.0000000-0.00059000.0000000
_0. 0000000
0.00000000.00000000.00007700.00000000.00000000.00001300.00000000.0000000
0.00002000.0000000-0.00001200.00000000.00000000.00000000.0000000-0.00002400.00000000.00000000.00000000.00000000.0000000_0.0000000_
0.0000000-0.0000150-0.00002900.00000000.0000000-0.00010400.00000000.0000000
0.0000270-0.0022600-0.00258000.00000000.00000000.0002430-0.0003870-0.00034500.0000000-0.00015000.00000000.00011000.0001330-0.0000150
-0.00003900.00000000.0002430-0.00019500.0000000-0.0000320-0.00002800.0001050
0.00004800.00000000.00000000.00000000.00000000.00000000.00000000.00004200.00000000.00000000.00004900.00000000.0000000
_0. 0000320
0.00000000.0000000-0.00005700.00000000.0000000-0.00011400.00000000.0000290
-0.0167000-0.0000510-0.00211000.00000000.00000000.00006000.0000110-0.00048200.0000000-0.00114000.0000430-0.0008890-0.000366_f_0.000000
0.00049700.00000000.00109000.00000000.00000000.00016100.00001300.0000000
I
Comments:
FORM XI (Part 1) - IN . ILM02.1
, ..' 57
AR3I96M
Ml N,
U.S. EPA - CLP
11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
ame: LANCASTER LABORATORIES Contract:
Lab Code: ______ Case No.: ______ SAS No.: .______ SDG No.: CRT04_
ICP ID Number: 2360-ICP1100 Date: 01/15/92
Analyte
Aluminum_AntimonyArsenic _BariumBerylliumCadmium _____CalciumChromiumCobalt __CopperIronLeadknesium^ pganeseSrcuryNickelPotassiumSelenium_SilverSodium ______ThalliumVanadium_Zinc
Wave-length(ran)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __
231.60766.49196.03328.07589.59377.57292.40213.86
Ir
CO_
0.0001860-0.0038310-0.00308000.00000000.00000000.00003200.0000000-0.00007600.00000000.00005700.00008100.0002700-0.0018810_0. 0000000
0.00155900.00000000.00059900.00001200.00000000.00013300.00000000.0000000
iterelement C
CR_
0.00024500.00701100.00095000.00000000.0000180-0.00001200.00091400.00000000.00007500.00000000.0001150-0.0010390-0.0007860_0.0000000_
0.00000000.0000000-0.00029800.00004200.0000000-0.0007970-0.00222400.0000620
Correction I
CU_
0.0000420-0.00001500.00001800.00000000.00000000.00001200.0000000-0.00001500.00000000.00000000.0000000-0.00001100.0000000-0.0000770
0.00000000.00013300.00043800.00007400.00000000.0000000-0.00006400.0043410
"•actors for
K _
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0001870
_0. 0000000
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000
••
MN_
0.0013450-0.0001910-0.00041300.00000000.00000000.00000000.0003530-0.00112400.00000000.00003900.00089800.0000920-0.0080910_0. 0000000
0.00000000.00000000.00027500.00013400.0000000-0.0002470-0.00017600.0000000
Comments:
FORM XI (Part 2) - IN / ILMO2.1
U.S. EPA - CLP
11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: 2360-ICP1100 Date: 01/15/92
AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryn J.W.NCSXPotassiumSeleniumSilverSodiumThalliumVanadium_Zinc
Wave-length(nm)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08_257.61 __
231.60766.49196.03328.07589.59377.57292.40213.86
Ir
M0_
0.00895500.00488900.00107200.00001200.00001900.00013700.0007860-0.0012330-0.00173200.00068900.0003620-0.0019300-0.0215500-0.0001860
-0.00266000.00189500.00010700.00064000.00048830.00000000.00000000.0000000
iterelement C
s*_0.01054400.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000_0.0000000_
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000
Correction I
SR_
0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0001940
_0. 0000000
0.00000000.00000000.00000000.00000000.00000000.00237400.00000000.0000000
actors forTI_
0.00248100.0011430-0.00001200.0000000-0.00003500.00029200.00071400.00017100.00170600.00031400.00024200.0003340-0.0036750_0. 0000430
0.00000000.0002270-0.00032700.0002520-0.0049410-0.05503000.00031400.0000360
"••
V _
0.0228200-0.00177100.00551000.00000000.0029800-0.00001500.0008280-0.08807000.00003000.00006200.0002960-0.0003050-0.000324*-0.000150
-0.00045600.00026700.00020300.00029100.0007290-0.00423800.00000000.0002510
I
Comments:
FORM XI (Part 2) - IN ILMO2.1
U.S. EPA - CLP
11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Name: LANCASTER LABORATORIES__ Contract:
Lab Code: ____ Case No.: ____ SAS No.: ____ SDG No.: CRT04_ICP ID Number: 3144-ICP61_ Date: 01/15/92
AnalyteAluminum_Antimony_Arsenic _BariumBerylliumCadmium _Calcium _ChromiumCobalt _____Copper _____IronLead•jnesiumHganeseMercuryNickel_> _____PotassiumSelenium_Silver ____SodiumThallium_Vanadium_Zinc
Wave-length(nm)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08
_257.61 __
231.60766.49196.03328.07589.59377.57292.40213.86
Ir
CR_
-0.00007800.00824000.00098200.00000000.00000000.00000000.00065200.0000000-0.00011000.00014400.0000490-0.0011200-0.0004700_0. 0000130
-0.00003800.0000150-0.00022900.00000000.0000000-0.0006260-0.00305000.0000000
vterelement C
CU_
-0.00001600.00000000.00001400.00000000.00000000.00000000.00003400.0000300-0.00001900.00000000.0000000-0.00004600.0000000-0.0001000_
0.00000000.00000000.00019800.00000000.0000000-0.0002620-0.00006000.0027800
Correction I
MN_
0.0006990-0.0000670-0.00014000.00000000.00000000.00000000.00018400.00097100.00000000.0000530-0.00014200.0000640-0.0081200_0. 0000000
-0.00031200.00005800.00024500.00011700.0000520-0.0002250-0.00016100.0000200
?actors for
MO_
0.01280000.00286000.00130000.0000000-0.00007800.00012300.0004250-0.00205000.00002300.00053700.0001470-0.00282200.0002440-0.0002920
-0.00224000.00156000.00022700.00000000.00324000.0006520-0.0026200-0.0000730
••
NI_
0.0000950-0.00060000.00004200.00000000.00000000.00027200.00000000.00005400.00038800.00004600.00000000.0002870-0.0008810_0. 0000000
0.00000000.0000290-0.00001600.00000000.00000000.05404000.00002000.0032600
Comments:
FORM XI (Part 2) - IN ILM02.1
60
U.S. EPA - CLP
11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: 3144-ICP61_ Date: 01/15/92
AnalyteAluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Wave-length
(nm)
308.22206.84193.70493.41313.04226.50317.93267.72228.62324.75259.94220.35279.08257.61
231.60766.49196.03328.07589.59377.57292.40213.86
Ir
V
-0.0153400-0.00360000.00669200.00000000.0022540-0.00001400.00041800.00559000.0000140-0.00003300.0002220-0.00024100.0005090-0.0001510
-0.00031000.00010100.0003280-0.00016400.0000000-0.00053700.0000000-0.0064500
it er element CCorrection I actors for •*
— I.Comments:
FORM XI (Part 2) - IN ILM02.1
61
AR3196I*5
U.S. EPA - CLP
12ICP LINEAR RANGES (QUARTERLY)
Lab Name: LANCASTER LABORATORIES__ Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04.
ICP ID Number: 2360-ICP1100 Date: 10/15/92
Comments:
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Integ.Time(sec. )
6.006.006.006.006.006.006.006.006.006.006.006.006.006.00
6.006.006.006.006.006.006.006.00
Concentration(ug/L)
600000.0200000.0200000.0100000.010000.0100000.0600000.0100000.0100000.0100000.0250000.0100000.0800000.0100000.0
100000.0900000.0200000.050000.0900000.0200000.0100000.0100000.0
M
ppppppppppppppNRPPPPPPPP
FORM XII - IN ILM02.1
62
U.S. EPA - CLP
12ICP LINEAR RANGES (QUARTERLY)
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.: _____ SAS No.: _____ SDG No.: CRT04_
ICP ID Number: 3144-ICP61 Date: 10/15/92
Analyte
AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc
Integ .Time(sec. )
6.006.006.006.006.006.006.006.006.006.006.006.006.006.00
6.006.006.006.006.006.006.006.00
Concentration(ug/L)
600000.0200000.0200000.0100000.010000.0100000.0600000.0100000.0100000.0100000.0250000.0100000.0800000.0100000.0
100000.0900000.0200000.050000.0900000.0200000.0100000.0100000.0
M
ppppppppppppppNRPPPPPPPP
Comments:
FORM XII - IN ILM02.1
SR3I96U7
PREPARATION AND RUN LOGS
64
U.S. EPA - CLP
13PREPARATION LOG
Lab Name: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04.
Method: P
EPASampleNo.
BRIMTBRMTFCRMDFCRMIDFBUNFJASHDJASHTJASHT DJASHT SJSBDFJSLTFJSLTILCSWMAHTFMAMTFMANHTMANMTPBWRDLOTRDLTFROALTROLTFSBMITSBMTF
PreparationDate
12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92
Weight(gram)
Volume(mL)
100100100100100100100100100100100100100100100100100100100100100100100100
FORM XIII - IN ILM02.1
65
oro
U.S. EPA - CLP
13PREPARATION LOG
Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_
Method: P
EPASampleNo.
BRIMTBRMTFCRMDFCRMIDFBUNFJASHDJASHTJASHT DJASHT SJSBDFJSLTFJSLTILCSWMAHTFMAMTFMANHTMANMTPBWRDLOTRDLTFROALTROLTFSBMITSBMTF
PreparationDate
01/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/9301/07/93
Weight(gram)
Volume(mL)
100100100100100100100100100100100100100100100100100100100100100100100100
FORM XIII - IN ILMO2.1
66
U.S. EPA - CLP
13PREPARATION LOG
Lab Name: LANCASTER LABORATORIES Contract:Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_
Method: F
EPASampleNo.
BRIMTBRMTFCRMDFCRMIDFBUNFJASHDJASHTJASHT DJASHT SJSBDFJSLTFJSLTILCSWMAHTFMAMTFMANHTMANMTPBWRDLOTRDLTFROALTROLTFSBMITSBMTF
PreparationDate
12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92
Weight(gram)
Volume(mL)
100100100100100100100100100100100100100100100100100100100100100100100100
FORM XIII - IN ILM02.1
raro N
U.S. EPA - CLP
13PREPARATION LOG
ame: LANCASTER LABORATORIES Contract:
Lab Code: _____ Case No.:______ SAS No.: _____ SDG No.:CRT04_
Method: CV
EPASampleNo.
BRIMTBRMTFCRMDFCRMIDFBUNFJASHDJASHTJASHT DJASHT SJSBDFJSLTFJSLTILCSWMAHTFMAMTFMANHTMANMTPBWRDLOTRDLTFROALTROLTFSBMITSBMTF
PreparationDate
12/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/9212/31/92
Weight(gram)
Volume(mL)100100100100100100100100100100100100100100100100100100100100100100100100
FORM XIII - IN ILMO2.1
C8
SR3I9652
RAW DATA
""• 93
AR319653
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