010 kennecott canada exploration inc. · august 22: 2gq1 2:03 kevin ki.i (sc7) 345-6666 kennecott...

31M05SE2039 2.22377 LORRAIN

KENNECOTT CANADA EXPLORATION INC.010

MICRODIAMOND ANALYSIS PRELIMINARY DATA

01MD005

R. W. Beck (Cobalt, Ont)

Prepared for:Kennecott Canada Exploration Inc

354-200 Granville St Vancouver BC V6C 1S4

Simon GriffithsLaboratory Manager

June 11, 2001

Mineral Processing Laboratory1300 West Walsh St. Thunder Bay, Ontario, Canada P7E 4X4

Telephone (807) 473-5558 Facsimile (807) 473-5660

This report refers to samples processed as-received.This report may not be reproduced except in full, without the written permission of the

Mineral Processing Laboratory

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AUGUST 22 : 2GQ1 2:03 Kevin Ki.i (SC7) 345-6666

KENNECOTT CANADA EXPLORATION INC.

Mne-al Processing Laoo'atcry 1300 Wesi Walsh Stresi Tl-jodei Bay, Or.ario CANADA P'E 4X4

Telephone: (80Vi 473-5558Facsimile. |80 7 ) 473-bteCr

-™ai kri:ca"anflaii !tey!el.ne!

Laboratory Charge Statement

Invoice to: Kennecott Canada Exploration Inc 354-200 Granville St Vancouver BC V5C1S4 ATTN: R W. Beck f Buddy Doyle

Remitance: Accounts ReceivableAddress c/o Kennecott Canada Exploration Inc.

354-2DC Granule St.Vancouver BC V6C 1S4

Project: R W. Beck (Cobalt, Ont)Project #: ^^

invoice*: T3000430Reference # : 01MDQOS

Date: 26-Jun-Ol

Quantity

3

30 3

Description

Caustic Fusion SamplesSecondary Fusions Microfusions Microdiamond Picking Microdiamond Description QC/QA and Reporting

Unit Cost

S S30.00 /sample^lOkg

S 12500 /sample<=10k^ S 10.00 /stone S 70.00 /sampie^lOkg

Total

S l. 6SC. 00

S 37500sS 21000

Total Charge to Project. S 2,475.00

Reports to follow R. W. Beck (Cobalt, Ont) 01MD005 Microciamona Processing (Causse Fusion) Microciiamond Observation St Description CERTIFICATE OF ANALYSIS

Sincerely,

Simon Griffiths Laboratory Manager

CLIENT COPY

A Eit3 Tinto

+6UB5ZUT5 T-876 P.001/001 F-894 Nov-05-Z001 11:05™ FrorfL BARNETT GEOLOGICAL

Mr. Kevin Kavi, October 23, 2001 Principal Geologist Diamonds, 309 South Court Street, Thunder Bay, Ontario, P7B 2Y1

Ph 1-807-346-1669 Fax 1-807-345-6666R. L. Barnett Geological Consulting Inc. ,9684 Longwoods Road,RR 32, London, Ontario, N6P 1P2Ph 1-519-652-1498, Fax 1-519-652-1475 Dear Kevin, INVOICE

Payment of the sum of 31872.50 is requested for services rendered in petrographic examination of four polished thin sections from sample KD4501, microprobe mineral analysis of constituent phlogopite, amphibole and chromite minerals, compilation of tables of mineral analyses, plotting of relevant graphs and preparation of a petrographic report:

-17.5 hours at J100.00 per hour - 31750.00 - plus 79 CST 3122.50

My GST number is 135072403.Please make payment as soon as possible.

Sincerely,

R. L. Barnett

KENNECOTT CANADA EXPLORATION INC,Mineral Processing Laboratory1300 West Walsh St. Thunder Bay, Ontario, Canada P7E 4X4 Telephone (807) 473-5558 Facsimile (807) 473-5660

METHOD DESCRIPTION

1 sample was submitted for caustic fusion processing and microdiamond recovery. The as-received sample w processed according to registered methods and standard operating procedures. The results are summarized in the Certificates of Analysis. Standard operating procedures are listed below, sample abnormalities and possible damage caused during shipping are noted on the Certificate.

OPERATING PROCEDURES

12J3456789

1011

Sample Receipt, Preparation, Crucible Loading and FiringCrucible Cooling, KNO3 Addition, Crucible Transfer 8*. Boil OutCrucible Unloading and Clean-out Through a 150 micron screenPrimary Acid Wash RecoverySecondary Clean-upSecurity ScreeningReburn Fusion and Clean-up (If required)Micro-fusion and Clean-up (If required)Diamond Identification and ObservationDiamond Description, Classification and MeasuringDiamond Data Reporting and Certificate of Analysis ^^^^(*) Denotes deviations from standard operating procedures.

*LOSS OCCURRED DURING PROCESSING BATCH MAY CONTAIN NON-CONFORMING SAMPLES

11-06-20019:45 AM 2 of 5

KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory1300 West Walsh St. Thunder Bay, Ontario, Canada P7E 4X4 Telephone (807) 473-5558 Facsimile (807) 473-5660

PRELIMINARY DATA METHOD 1: MICRODIAMOND PROCESSING

Date Received: 02-Apr-01Waybill: Purolator 1817 299 7902

Courier #:

Work Order #: 01MD005Project: R. W. Beck (Cobalt, Ont)

Client Billing #: Lab Billing Code:

Company: Kennecott Canada Exploration Inc 354-200 Granville St Vancouver BC V6C 1S4

Attention: R. W. Beck l Buddy Doyle Telephone: (604)669-1880

Facsimile: (604) 669-5255

1Client Sample Reference SAMPLE WT (kg.)

*KD4501 22.222.2

CONC. WT(gm)

0.10.1

PRIMARY FUSION

33

SECONDARY FUSION

77

MICRO FUSIONS

44

"LOSS OCCURRED DURING PROCESSINGBATCH MAY CONTAIN NON-CONFORMING SAMPLES

Printed: 11-06-2001 9:45 AM

This report refers to samples processed as-received This report may not be reproduced except in full, without written permission of the Mineral Processing Laboratory. 3 of 5


PRELIMINARY DATA METHOD 3: MICRODIAMOND OBSERVATION

Date Received: 02-Apr-01 Company: Kennecott Canada Exploration IncWaybill: Purolator 1817 299 7902

Courier #:



354-200 Granville St Vancouver BC V6C 1S4

Attention: R. W. Beck l Buddy Doyle Telephone: (604)669-1880

Facsimile: (604) 669-5255

Client Sample Reference+0.5 mm SIEVE -0.5 mm SIEVE TOTAL

DIAMOND COUNT DIAMOND COUNT DIAMOND COUNT1|| *KD4501 0 33

SYNTHETICS

0*LOSS OCCURRED DURING PROCESSINGBATCH MAY CONTAIN NON-CONFORMING SAMPLES

Printed: 11-06-2001 9:45 AM

This report refers to samles processed as-received. This report may not be reproduced except in full, without the written permission of the Mineral Processing Laboratory. 4 of 5


PRELIMINARY DATA METHOD 3: MICRODIAMOND CLASSIFICATION

Date Received: 02-Apr-01Waybill: Purolator 1817 299 7902

Couriertf:

Work Order*: 01MD005Project: R. W. Beck (Cobalt, Ont)


Company: Kennecott Canada Exploration Inc 354-200 Granville St Vancouver BC V6C 1S4

Attention, R W. Beck l Buddy Doyle Telephone: (604) 669-1880 Facsimile: (604) 669-5255

Client sample Reference

KD4501KD4501KD4501

STONE

1

23

SIEVE SIZE(mm|

0.3000.1500.150

STOCK EX SIEVE (mm)

"0.500"0.500"0.500

Xmm

0.590.420.49

Ymm

0.380.280.23

Z mm

0.230.230.15

WEIGHT IN OCTACARATS

907561647604.4829752.8

FRAGMENT/IN TACT

FragmentFragmentFragment

MORPHOLOGY

IRREGULAR WITH OCTAHEDRAL FEATURESIRREGULAR WITH OCTAHEDRAL FEATURES

IRREGULAR

COLOUR

GreyGreyGrey

CLARITY

TransparentTransparentTransparent

COLOUR INTENSITY

322

INCLUSIONS/ CLEAVAGES

333

RESORPTION

55

SURFACE FEATURES

LAMINATION LINES

COMMENTS

.i calculated using In* folowlng formula: X(mm) x Y(rtim) x Z (mm) x Sptctflc Gmtty of 3 52 / 200 mgIrrttnsrty of Colour - seal* of D - S wflh 5 bvlng Hit most Inttni*

Cliavagti and Inclusions - seal* of O - 5 wHh S having th* moil cl*avag*i and Induxlom Resorption - scat* of 1 - S vvf h 1 having mart rtxorptlon

1 carat 3 1 x 10-8 odacarati

Jun;;12-2001 10:21am From-RL BARNETT GEOLOGICAL +5196521475 T-610 P 001 F-57G

or

K

Mailing Address: 9684 I R.JR, S' 'n, ont.: :TeJ: (51?) 652-149*''. ••;^; (5^652-1^;;,

- - v.Courier Address:Suite 513 -- -..; v Mail Boxes JBtc.

ton JRoad S. Ont. ..N6E 3A9- J

S6-12-Q1 18:19 RECEIVED FROM:+5196521475 P . 81

T2S96T5+ : HOHJ U3AIH33U b T : f? T T 8 - S I - 9 N

Lamprophyre Samples KD4501 A, B, C, D Cobalt, Ontario.

For : Kevin KM, Kennecott Canada

By: R. L. Barnett, June 12, 2001

This report is a summary of detailed petrographic-electron microprobe investigation of four samples of " lamprophyre " from the Cobalt region, Ontario, KD4501 A, B, C, D. Four small hand specimens were provided and polished thin sections were made of each. These polished thin section were coated with carbon for subsequent investigation with the electron microprobe and examined in detail with a petrographic microscope. Both representative and interesting and unique mineral grains and textural relationships were photographed and circied with a diamond scribe device on the petrographic microscope. The diamond scribe makes a small circle that perturbs the conductivity of the carbon-coated polished surface of the thin section and hence induces charging when examined with electron beam. In this manner ft is possible to locate and examine in detail the photographed representative and interesting mineral grains and textures selected during petrographic investigation.

All analyses were made with a JEOL733 electron microprobe equipped with flve wavelength spectrometers and a Tracor Northern EDS system. Analyses for constituent phlogopite- biotite solid solution, ss. , amphibole and zoned zincian chrome- iron spinels are tabulated at the end of this report. Certain aspects of the chemical variation of phlogopitc-biotite ss. are portrayed in terms of AI2O3-FeO, AI2O3-TJO2 and Cr2O3-FeO on plots originally configured by Dr, R Mitchell to define the compositional variation among micas of kimberlite, orangeitic, minette and lamproite affinity. Compositional variation of amphibole is plotted In terms of aluminum in the tetrahedral site versus occupancy of Na + K in the so-called A site of the amphibole structure. This plot is commonly used to portray compositional variation of both Igneous and metamorphic amphiboles. Zincian chromlte-iron analyses are plotted in terms

200 d 019-i

' d U3AI303H GT:QT

of magnesium and chrome to allow comparison with similar minerals from the lamprophyres from the Wawa region.

The relationships, if any, among the four samples is unknown to the writer. Of the four, sample KD4501 A has a an even-grained texture while samples KD4501 B, C, D have some degree of fabric which may be indicative of some degree of moderate deformation or alternatively may derive from flow banding at the magmatic stage of Injection of the lamprophyres.

In simplest terms, sample KD4501 A consists of an Interlocking distnbution of relatively coarse-grained laths and basal sections of pale to deep brown mica, 45-55070 and relatively coarse amphibole, IQ-15% within a finer grained matrix of acicular colorless amphibole. The coarse mica and amphibole domains of the sample are interspersed with quite numerous, 35-45070, ovoid to roughly circular domains comprised by fine-grained colourless amphibole that commonly include or are associated with minute grains of zoned zinclan chrome-iron spinel included within mica. The matrix of the sample is without quartz or feldspar and consists of acicular laths and clusters of colorless amphibole included within a variable abundance of calcite, in amounts generally much less than

In simplest terms, the sample Is essentially bfmlneraffc consisting mainly of mica and amphibole. However, within this initial mineralogic simplicity, there Is a consistent com positional variation within the texturaily diverse distribution of amphiboles throughout the sample that is both interesting and enigmatic. At the very heart of the matter concerns interpretation concerning the origin of amphibole in Archean lamprophyres. Are they of primary igneous or retrogressive hydrothermal in origin?

The population of relatively coarse amphibole commonly displays a pronounced core to marginal color variation with deep-green central zones surrounded by pale to colorless marginal growth zones ( Plate KD4501A-1 ). Coarse brown plates of mica commonly occur within the central regions of the color-zoned amphibole ( Plate KD4501A-2 ). This intimate textural relationship fs Interpreted as evidence for simultaneous

319-d EDO d 019-i 3*^233513^ 1V

stability and growth of the brown mica and green amphibole. Further evidence for simultaneous growth of coarse mica and amphibole, Is provided by the preservation of well-developed crystal faces of amphibole against coarse mica throughout the sample ( Plates KD4501 A 3-6 and Plates KD4501 A 7-8 ) . It Is most interesting that the crystal outline of amphibole against mica as seen in Plates KD4501A 5 and 8, Is preserved and defined by the colorless marginal zones on the amphlboies. What then is the ultimate origin of this textural relationship? Review of amphibole analyses for sample KD4501 A reveals that the deep- green central regions of the color-zoned grains are significantly enriched in aluminum, titanium, and alkalis, both sodium and potassium and iron, while the colorless marginal zones that define crystal faces against mica are significantly more magnesian and are essentially without aluminum, titanium or alkalis elements. These relationships are well Illustrated in the compositional variation of the zoned amphibole grain shown In Plate KD4501A -S In analyses 1 through 6 in the Table of amphibole analyses. The deep green central regions contain 11.14 wt*7o AI2Q3, 12.25 wt0/* FeO and a maximum of 2.51 wf/o Na2O and 0.54 wf/o K2O while the colorless margin zones contain 1.90 wfft A12O3, only 6.16 wf/o FeO and sodium less than O.51 wtVo. In essence, the color zonation defined by the coarse amphlboies reflects a compositional variation in which deep-green, quite aluminum, iron and alkali-rich paragasitic amphibole is surrounded by colorless decidedly magnesian or tremolite amphibole essentially without aluminum or alkalis. The core to marginal color and concomitant systematic and predictable compositional variation of the coarse amphibole in sample KD4501 A is not one that would be considered to be indicative of equilibrium. The composition of the deep green cores Is commonly observed In rocks that contain amphlboies of igneous origin and In rocks metamorphosed to lower-middle amphibolite facies rank. The marginal zones are essentially without aluminum, alkalis and decidedly more magnesian that the cores. What then is a plausible resolution to these enigmatic textural and compositional relationships? If the deep green pargasltic cores are simply dismissed to be of metamorphic origin, what then Is the origin of the more magnesian marginal zones? In even the simplest metamorphic scenario, the

fOO d 0 1 3-1 9i?!'S35 :.3- 1V3I501033 il3NiiVa Id-^:! ^22-C( I003-6l- un r

SifTZSgGTS+iNOUJ a3AI303H 93:81 I8-ST-9S

contrasting core to marginal compositional variation demands a strong degree of magnesium metasomatism in an hydrothermal environment In a regime of decreasing metamorphic rank approaching middle greenschist facies conditions. At the very heart of the matter is interpretations concerning the ultimate origin of amphiboles of with similar contrasting compositions found in lamprophyres of Archean age from the Wawa region and Yellowknlfe, N,W.T. [f simply dismissed as a consequence of a complicated metamorphic history as yet unraveled In each of these areas, then one would hope that mafic rocks that host or are spatially related to the lamprophyres would provided abundant textural for a similar complicated hydrothermal metamorphic history. In the writer's rather limited knowledge of such matters from Yeilowknife and Wawa, this is not proven to be the case.

The relationships discussed above are best resolved if considered to be the result of a combined igneous and late- stage igneous or deuteric hydrothermal regime associated with the igneous injection of the lamprophyres. The green pargasitic cores are considerd to have formed at relatively high temperature and\or pressure conditions at depth during ascent of the lamprophyre magma and the colorless marginal zones likely formed late in the magmatic history of the rock volume from magnesian fluids of magmatic derivation.

These considerations also have a bearing on interpretations concerning the origin of the domains of fine-grained colourless amphibole that occur throughout the sample intimately associated with strongly color-zoned coarse amphibole ( Plates KD4501A 3- 4, 9-10, and 11-12). Review of the analyses, reveals that the matte of randomly-oriented amphibole grains that comprise the ovoid to roughly circular domains throughout, are decidedly magnesian or tremolitlc with near 5.50 wty0 FeO essentially without aluminum or alkali substitution. These amphiboles are similar to the colorless marginal zone on the coarse amphibole, yet contain even lower concentrations of aluminum and alkalis.

gg-d SAb I 2596 T'T t- : HOH.-I ([3AIMOHM loiNC t H - o l - g Q

In a related and unresolved matter, there is a consistent and predictable spatial association of these ovoid domains of tremolite amphibole and concentration of spinel included In mica. While there are occasional grains of zoned zincian chromite-chromian magnetite surrounded by or included within mica throughout the section ( Plate KD4501A 9-10 ), it is the writer's view that these grains are in fact situated at the margin of or within a tremolitlc domain in the third dimension perpendicular to the plane of the thin section. In fact, almost all of the zoned chromite within the section occur wfthln or at the margin of the ovoid domains of tremolitlc amphibole. Futher, these zoned chromite are not only essentially restricted to the ovoid tremolitic amphibole domains, they are also consistently enclosed within patches of mica with quite elevated contents of chrome ( Plates KD4501A 13-16,17-18 ).

The ultimate origin of the ovoid domains of fine-grained tremolitlc amphibole and the consistent spatial association of these domains with zoned zincian chromite-iron spinel enclosed in mica ( Plate KD4501A 19 ) remains unclear. It is logical to suggest that the formation of the tremolite in the ovoid might be time equivalent with formation of the colourless tremolitic amphibole that comprises the outer zones on the deep green relatively coarse amphibole. One Interpretation Is that a certain proportion of these ovoid to circular domains of tremolitlc amphibole are originated as vesclcles or gas cavities that formed in a late-stage deuterfc-hydrothermaf regime as the bogy of lamprophyre cooled. However, there is a certain subpopulation of these features which have quite angular outlines with decidedly linear boundary zones with regions of fine-grained mica and amphibole ( Plates KD4501A 3, 9,10,11 Z 12 ). One quite plausible interpretation that is favoured by the writer, fs that this subpopulation are indeed examples in which a pre-existing phenocryst has been replaced by fine-grained tremolitic amphibole In a late deuteric-hydrothermai environment The fact that these domains now consist of a magnesian and calcium-bearing mineral, tremolitic, allows the interpretation that the pre-existing mineral was dlopsidic clinopyroxene. Further, with some imagination, the distribution of fine-grained mica and chromite appears to define original

3/9-d 6ZO/SOO d 012-i Si?!Z225!9- l?:1301033 li-MYa Id-mo J j "^MH 1002-Zl-unr

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grain margins within some of the larger tremolltlc domains ( Plates KD4501A 13-14 ). Accordingly a certain subpopulation of these tremolite domains might have been multigranular, indeed nodules from the depths.

The oxide minerals encased in mica in sample K04501A as well as the three other samples examined in this study have a consistent core to margin zonal relationship in which a central zone of spinel with chrome greater than iron is surrounded by an outer zone of spinel In which Iron Is great than chrome ( Plate KD4501A 19 ). Both growth zones have moderate content of aluminum, manganese and remarkably zinc. Ail domains of ail grains analyzed are essentially without magnesium.

Review of chromite analyses reveals that the maximum chrome content of the central zone among the four samples approaches 61.52 wf/o Cr2O3. As such the spinels in the four samples of lamprophyre from Cobalt are quite similar to spinels from diamond-bearing lamprophyre from the Sandor occurrence north of Wawa.

Plate KD4501A-1: Random distribution and intergrowth of pale brown mica and zoned, green pargasftic amphibole in a matrix of finer-grained colourless amphibole, plane light.

Plate KD4501A-2: Blocky plates of mica, phlogopite-biotite ss. included within the deep green central regions of the coarse color-zoned amphibole. Note the birefringent pale yellow outer zones on amphibole that are colourless in plane light, same filed of view as Plate KD4501A-1 in crossed polars..

620/300'd 013-i 3^:^35:2- 1V:1001033 :i2

Jun-12-2001 10:24am From-RL BARNETT GEOLOGICAL+51SE52147ET-610 P.007/029 F-576

aia o

VZ ZZ OZ 81 91 VI Z\, 01 8 9 V Z O

31l3ONVaO

S3113NWN

OldVINOG'O'a'V31dWVS

S6-12-S1 IS:22RECEIVED FROM:+5196521475P . 07

99 ' d (33AI333H ZZ : Q T T8-6 t- !

PHLOGOPITE-BIOTITE SS. - KENNECOTTSAMPLE KD4501 A COBALT, ONTARIO

COO

2O

18

1412-

10-

86-

4-

2-

KIMBERLITEM1NETTES

ORANGEITE •^

.^LAMPROITE

ORANGEITE

n i i ii i i i i i

O 2 4 B 8 10 12 14 16 18 20 22 24

wt 'fc FeO

o RLB

3/9-d 620/800 d Ol3-i !V:iD0103D ii2

68 ' d :HOHJ (33AI33HH : 9 T 10-31-98

PHLOGOPITE-BIOTITE ss. - KENNECOTT SAMPLE KD4501 B COBALT, ONTARIO

COO

•Sk,LAMPROITE

t r i i i i i r rO 2 4 6 8 10 12 14 16 18 20 22 24

wt FeO

RLB

3/S-d 620/600 d 013-1 1V3ID0103D li3 -' O l

T ' d ',Z : 8 T TQ-Z: T -90

PHLOGOPiTE-BIOTITE SS. - KENNECOTT SAMPLE KD4S01 C COBALT, ONTARIO

MINETTES

ORANGEITE•S^

.-^.LAMPROITE

ORANGEITE

8 10 12 14 16 18 20 22 24

Wt FeO

o RLB

3/S-d 6ZO/OIO d OI9-1

T T ' d Q3AI303U : 8T T8-SI-9Q

PHLOGOPITE-BIOTITE SS. - KENNECOTT SAMPLE KD4501 D COBALT, ONTARIO

COo01

ORANGEITE

^LAMPROITE

ORANGEITE

8 1O 12 14 16 18 20 22 24

wt FeO

o RLB

319-d 620/110 d 013-1

T ' d : HOHJ C3AI303H SZ : 8 T TQ-SI-9Q

COoC

PHLOGOPITE-BIOTITE 3S. KENNECOTT SAMPLES KD4501 A,B,C,D COBALT, ONTARIO

MINETTE

LAMPROITE

XKIMBERLJTE TRENDS 1,2,3

l l l l

8 10 12 14 16 18 20 22 24

wt 96 TiO2

RLB

9iS-d 6ZO/ZIO d 019-1 9/7U93619+ iooz-zi-""r

C T ' d SifT3S96TS+:NOHJ a3AI3D3H Co:Q T T9-S T-98

PHLOGOPITE-BIOTITE 33. KENNECOTT SAMPLE KD4501 A COBALT, ONTARIO

voD•4M*

t

*

i*

5

ZV

18-

16 14-

12 10~

8-

6-

4-

2"

rk

*®\ *-S

j\ ^r# \ ^--^ MINETTE0^~ P ^

1 \X.""7 \ LAMPROITE

7 \ Ni 7© \ r^J, V (t-*) KIMBERLITE TRENDS 1,2,3

S 10 12 14 16 18 20 22 24

Wt TJO2

o RLB

9/S-d 620/EIO d 019-i 1V3I30102D ilH

fr T ' d CI3AI333H CZ : 8 T TQ-2T-99

A

OCSI

PHLOGOPITE-BIOTITE 33. KENNECOTT SAMPLE KD4501 B COBALT, ONTARIO

18-

16-

14

12-1

10

8

6

4H

\ MINETTE

LAlF^OfTE

l -3 KIMBERLITE TRENDS 1,2,3( l \ l l r l i

O 2 4 6 8 10 12 14 16 18 2O 22 24

wt % TiO2

o RLB

91S-d 6ZOX?lO'd OI3-1

-d C3AI3D3H C2 : 81 19-61-98

COo

PHLOGOPITE-BIOTITE ss. KENNECOTT SAMPLE KD4501 C COBALT, ONTARIO

MINETTE

LA^R^OITE

(T-s) KIMBERLITE TRENDS 1,2,3I l l T^ l l

O 2 4 6 3 10 12 14 16 18 20 22 24

Wt 96 TJO2

RLB

6ZO/SIO d Ol9-i 1YD130103D 113NilV9 ia-

9T - d SA17TS996T9+: MOHJ (I3AI333H : 9 T T Q-oI-99

CO

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PHLOGOPITE-BIOTITE ss. KENNECOTT SAMPLE KD4501 D COBALT, ONTARIO

Q

MINETTE

LAMRftOITE

-8 KIMBERLITE TRENDS 1 f2,3

8 10 12 14 16 18 20 22 24

Wt TlO2

o RLB

9i9-d 620/310 d OL9-1

2.T ' d : 8 T T9-ZT-99

PHLOGOPITE - BIOTITE SS - KENNECOTTSAMPLES KD40S1 A.B.C.D COBALT, ONTARIO

q, 2V.o

o RLB

o.4

9o

00 3&&0

™r i

10 15

wt 9k FeO

25

6Z07ZliTd 013-1 1V3ID0103D llB

IT 'd S^Lt'ToS96TS+ : HOUJ (I3AI303H b Z : 9 T TQ-6T-9Q

PHLOGOPITE - BIOTITE SS - KENNECOTTSAMPLE KD4051 A COBALT, ONTARIO

O 2**

V~

O

1 -

o RLB

8.

10

wt

15

FeO

20 25

9ZS-d BZO/SIO d OI3-1

61 'd Sit- :^;S96T5+ : NOHJ (I3AI333H : 8 T 18-21-98

PHLOGOPITE - BIOTITE ss - KENNECOTT SAMPLE KD4051 B COBALT, ONTARIO

wq.6

RUB

opl

o ,10

wt

1S

FeO

20 25

SZO/etO'd OI9-1 9/FI3S36I9+

as - d Q3AI303H T8-2T-9Q

PHLOGOPITE - BIOTITE SS - KENNECOTT SAMPLE KD4051 C COBALT, ONTARIO

it

jf^^

otf1 1

0

1 1 ' 1 ' 1 ' l '

o-

0 oo"\

'C^y Q

^ .0 5 10 15 20 21

wt % FeOo RLB

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PHLOGOPITE - BIOTITE ss - KENNECOTTSAMPLE KD4051 D COBALT, ONTARIO

,o

10

wt

15

FeO

20 25

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9if IZ996T9+:NOtfJ (13AI3D3H : 9 T TQ-ZT-98

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ELEMENTAL SUBSTITUTION IN AMPHIBOLE SAMPLE KD4051 A COBALT, ONTARIO2.4

2.2 2.0 1.81.6 1.4

1.0 --r 0.8

0. 0. O

,6 -4 -2 -

0.0O

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0.0 0.1 O.2 0.3 0.4 0.5 O,6 0.7 0.8 O.9

A Site Occupancy - Na-A * K

o RLB

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i? Z ' d TSS96TS+: NOttJ Q3AIHO3U : 8 T 19-21-99

l

Eu cS

ELEMENTAL SUBSTITUTION IN AMPHIBOLE SAMPLE KD4051 B COBALT, ONTARIO2.4 2.2

2.0 1.8 1,6 1.4

1.2 1.0

0.8 0.6 0.4 0.20.0

O

A Site Occupancy - Na-A

RLB

.0 0.1 0.2 0.3 0.4 O.S 0.6 O.7 O.8 O.9

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- d SitTZS96TS+:HOU J (I3AI303H : 9 T T8-2T-98

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ELEMENTAL SUBSTITUTION IN AMPHIBOLE SAMPLE KD4051 D COBALT, ONTARIO2.4 2.2 2.0 1.8 1.6 1.4 1.2 1.0 0.8 0.6 0,4 0.2 O.O

O

O

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A Site Occupancy - Na-A + K

RLB

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Jun-12-2001 10:27am From-RL BARNETT GEOLOGICAL+5196521475T-610 P.027/029 F-576

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Jun-12-2001 10:27am From-RL BARNETT GEOLOGICAL +E19G521475 T-610 P.028/029 F-576

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Q6-12-S1 16:25 RECEIVED FROM:+S196521 475 P-2B*

Nov-Ol-Ol 12:O2 Kennecot.t, T Bay Lab P . O2


MICRODIAMOND ANALYSIS TESTREPORT

01MD005

R. W. Beck (Cobalt, Ont)


354-200 Granviile St Vancouver BC V6C 1S4

Simon GriffithsLaboratory Manager

August 3, 2001

Mineral Processing Laboratory13CO West Walsh St. ThunoerBay. Ontario Canada P7E 4X4

Telephone (507) 473.5553 Facsimile (507) 473 5660

This report refers to samples processed as-received.This report may not be reproduced except in full, without the written permission of the



Mineral Processing Laboratory1300 Wes! Walsh Si "^ ur. cer Bay. Oi'a'io Canada P76 4X4 Telephone ^071473-5553 Facsini le ..807) 473-i6SO

METHOD DESCRIPTION

1 sample w-as submitted for caustic fusion processing and microdiamond recovery. The as-received sample was processed

according to registered methods and standard operating procedures. The results are summarized in the Certificates of Analysis.

Standard operating procedures are listed below, sample abnormalities and possible damage caused during shipping are noted

on the Certificate.


7

1011

Sample Receipt, Preparation, Crucible Loading and FiringCrucible Cooling, KNO3 Addition, Crucible Transfer A Boil OutCrucible Unloading and Clean-out Through a 150 micron screenPrimary Acid Wash RecoverySecondary Clean-upSecurity ScreeningReburn Fusion and Clean-up (If required)Micro-fusion and Clean-up (If required)Diamond Identification and ObservationDiamond Description, Classification and MeasuringDiamond Data Reporting and Certificate of Analysis ^^^C) Denotes deviations from standard operating procedures

5.4 Kg reburn May 7/01 - possible lass due to crack along weld in bottom of pot 17. Batch may contain non-conforming samples.

Z O <

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0361

r a (J

01-11-20019:48 AM 2 of 5 O 00

KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory1 300 West Walsh Si Thunder Ray, Ontano. Canada P7E 4X4 Telephone \8C7i 473-5553 Facsimile (807) 473-506-3

CERTIFICATE OF ANALYSIS METHOD 1: MICRODIAMOND PROCESSING

Date Received. 02-Apr-01Waybill: Purolator 1817 299 7902

Courier #:



Company. Kennecotl Canada Exploration Inc 354-200 Granville St Vancouver BC V6C 1S4

Attention: R. W Beck t Buddy Doyle Telephone: (604) 669-1880;

Facsimile: (604) 669-5255

1

Client Sample Reference SAMPLE WT (kg.)

KD4501 22.222.2

CONC. WT{gm)

0.10.1

PRIMARY FUSION

33

SECONDARY FUSION

11

MICRO FUSIONS

4

4

z o <lo

N

oN

103 3 IDn o c* rtH

OD Qi k

r en cr

5.4 Kg reburn May 7/01 - possible loss due to crackalong weld in bottom of pot 17. Batch may contain non-conforming samples.

Mike LiedkeProcessing Team Leader


The iXdlity ot mie ('in:!; mond futr.Kfif-n J'ld iclwrion ; 'om rack sjTplcs 'Mencid^ ' arc 3.i is -ubicc.' (ci cio'iil-:;('ny [lii;i.i,;h t

(QVQG K.h'.-fi'v. M ifoii .IOUCH' lecovety K cjVula'pd fm or.fl .^amp e in ev*rr\' balo. One bbith wi^sis oi uJ '.-i ii-r .'j'Hfj

tt-i-.'-'ilXt. Jl l('d~l i;j'i -' r lJ-llp'e.- Jl? quality L'jn'iol ?.irrplc5.

jl <1•\CX' ironiiofni^ hvolvtjj '. ::'i\parivoc ui iiic'

r\' v*Tf.trf^. or jYvrr.jv, OTi 7-''Si I'l.'i.7 ^. (^p^cdc'J

K* I'nrn cich ba'ch t^ -•.o-i?:irilly J^<:i•plJcl;! rtt-rnjl jer

irty J' Cio ^V"i cuci cciu ^ l fr''C- {if a . i o'ltoi'ityj in\ Kid

S (CfKift rf-*o.'j to sinpies p'acess cxcc'p' in Ki . wi;^ou( wfirte" per

lan Hamilton QA/QC Specialist

- niernal CLJ lv issuiaico/qua lv

n^ms; on rdA-icuji -jcfpU- .v-igh

itardiid? •''•oc vs^l-i;; .md -...|-: ., i , Jf , j;

.s* on n' Vn: Mirem; Pnoce^5,tng Labarj:c

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KENMECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory13 C O '.VosUValit! St. 'Hunder Hay. Ontario. Canada P7E-*X4 Telephone (307)^/3 5550 Facsimte {807) 473-556C

CERTIFICATE OF ANALYSIS METHOD 3: MICRODIAMOND OBSERVATION

Date Received: 02-Apr-01Waybill: Puroiator 1817 2997902

Courier^:

Work Order*: 01MD005Project. R. W. Beck (Cobalt Ont)

Client Billing #: Lab Billing Code: t

Company Kennecott Canada Exploration Inc 354-200 Granville St Vancouver BC V6C 1S4

Attention: R. W. Beck l Buddy Doyle Telephone: (604)669-1880 ;

Facsimile: (604) 669-5255

Clierrl Sanplc Reference

1 KO4501

+0.5 mm SIEVE -0.5 mm SIEVE TOTAL SYNTHETICS DIAMOND COUNT DIAMOND COUNT DIAMOND COUNT

033 Q

033 0

5.4 Kg reburn May 7/01 - possible loss due to crack along weld in bottom of pot 1 7.

Batch may contain non-conforming samples.

4-^—Cnrfs Burner Observation Team Leader

Simon Griffiths lan Hamilton Laboratory Manager QA/OC Specialist

l h; 1 rjL'jlirv -:,f (T n -iidi/iinond PN'r^' \nn ;.nd -i'1 rc'tn, i ifom rod- ^-upl' 1 -, t.v.Hli'.jfh 1 .me 'i i j i.ibji-: t *u .-"oinfof n.f '.hen qd *i ri^'/mt,^ r Kef .nl -^ jrtlitv ji-s^. f.vii'c'i.iM r-,

* vwrr:ii i ^.'.CJC ' *t lir'.n^ Mic'ixJf/mi-i.Kl i^- o.---r. -*. c. i li iJ.Tfn for an? samp ^ "n c-,Tfv botch Orv tu^ h c'.irsiH-i of c p ;o ten srnplfv. d^pendiA^ on ndnirl-. .il ^.irnplr

CC T"i j j! CÂ-'QC niv^nitd-'Ki-j ,r .'ci', t*, i Gîpafib^M o 1 1, t rtjduffu ''c f'yin -jjc'i b.uiti 'o Ûi' 'jlx.it'1 v ^\.C^pUulf nh?'n^l (^ronnjTr Ûnd^rc s. ''r.'jt.t ^vr^ J.HL! i^ t''."t!oi" ^t fh?

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Oci

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KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory

CERTIFICATE OF ANALYSIS METHOD 3: MICRODIAMOND CLASSIFICATION

("•cji—t K vV btck -;c-can o-.i

ab Riliir ^ Ccoa' ~*

™ii

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OflWTl f! (o! 17.

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COLOUR

G:-zy

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COLOUR INCLUSIONS' CLEAVAGES

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Nov-Ol-Ol 1Z-.O3 Kennecott, T Ba;y Lab P . O7


MICRODIAMOND ANALYSISTESTREPORT

01MD013

Prairie C


354^200 Granville St Vancouver BC V6C 154

Simon GriffithsLaboratory ManagerNovember 1, 2001

Mineral Processing Laboratory1300 West Walsh St. Thunder Bay Ontario Canada P7E 4X4

Telephone (807) 473-~5553 Facsimile (807) -173-5600

This report refers to samples processed as-received.This repon may not be reproduced except in full, without the written permiss on ot the


2 O

KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory1 33C West Walsh St Thunder Say, Ontarc. Canada P7t 4X4 Te.ephone iS-IR) 473-5558 Facsirtvle (807) 473-55-30

METHOD DESCRIPTION

i O

I-JI\Jo u

7.(O

1 sample was submitted for caustic fusion processing and microdiamond recovery. The as-recctved sample was processed according to registered methods and standard operating procedures. The results are summarized in (he Certificates of Analysis. Standard operating procedures are listed below, sample abnormalities and possible damage caused during shipping are noted

on the Certificate.

10n ort-i03


123456789

1011

Sample Receipt, Preparation, Crucible Loading and FiringCrucible Cooling, KNO3 Addition, Crucible Transfer 8. Boil OutCrucible Unloading and Clean-out Through a 150 micron screenPrimary Acid Wash RecoverySecondary Clean-upSecurity ScreeningReburn Fusion and Clean-up (If required)Micro-fusion and Clean-up (If required)Diamond Identification and ObservationDiamond Description, Classification and MeasuringDiamond Data Reporting and Certificate of Analysis

r0)d

(") Denotes deviations from standard operating procedures.

(T-11-20017.45 AM 2 of 4 O03

KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory1300 West Walsh St. Thunder Bay. Ontario, Canada P7E 4X4 Telephone W?;. 473-5558 Facsimile \B07. 473-65-30

CERTIFICATE OF ANALYSIS METHOD 1: MICRODIAMOND PROCESSING

z o

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IM

O W

Date Received 18-Jun-01Waybill Klvi Drop-off #2

Courier #:

Work Order #: 01M0013 Project: Prairie C

Client Billing #: Lab Billing Code: D073

Company: Kennecort Canada Exploration Inc 354-200 Granville St Vancouver BC V6C 1S4

Attention. Kevin Kivi l Telephone: (604)669-1880

Facsimile: (604) 669-5255

1

Ghent Sample Re'er*nce SAMPLE WT (kg.}

VR43624A 26.026.0

CONC. WT(gm)

0.10.1

PRIMARY FUSION

33

SECONDARY FUSION

33

MICRO FUSIONS

55

IDn or*- rt

OD O

r -ucr

Mike LiedkeProcessing Team Leader

l 'tt.' q J j! it v o' ri \jr-jd jrro''d vvifî.t on j 'i J i

:Q\-QC ^cheTit. .Microdiarrond .•f.-'.-vKy i?

Ti('*e r ore. ii( li?j^ 10'- oi ^jnp f.^ JT îj^lit\-


for -unt i-ampl^ :r uvtn,'

id .1.'' i 1. i.jn t^^t tij ir od i loci 1 1^ fhr::u^h 3 r

Ore aatch vOfM-^'i o' up tu (ci â.-nnlorttfrj q

ndinj; <:-l

IK mi: md i j duic d fn,m nj( h n.'.T' 1^ (o -r di i M 1 * j l v WM ( epljtili: irr.i'f :ijl ^letiu'i

a.'i:1-.-c uruiM,in:v .it (''i1 r*V:. tiuvidHrKV linnii ;i- .jll -. untoif.rJ (MI, (cdu'U'.^CJ:Hl.lKl:.

[an Hamilton QA/QC Specialist

i.uiiK'i'-'vjcd ty \ r.ntd.1

:-drr pie vxci^ht;

-.frt CI l l ;301 AM

This '^prio( tC rr.-|"^Ju:iJJ exc

i refers :c sarp^s C'' l^^pt in full *rhcu' *r t'^n ( e' O' Tfie f/1 nerdl Proressing Lat 3oM

oIfl

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KENNECOTT CANADA EXPLORATION INC.Mineral Processing Laboratory'330 V.'*5lWa:sh S: Tim not- tidy, O-uaria. Cana-Ja P7t 4X4 Tel-phone 1807; ^73-5558 Facsimile (807;-4 73-5650

CERTIFICATE OF ANALYSIS METHOD 3: MiCRODIAMOND OBSERVATION

Date Received: 18-Jun-01Waybill: Kivi Drop-off #2

Courier*:

Work Order #; 01M0013 Project: Prairie C

Client Billing #: ' Lab Billing Code: D073

Company: Kennecott Canada Exploration Iric 354-200 Granville St Vancouver BC V6C 1S4

Attention: Kevin Kivi Telephone: (604) 669-1880

Facsimile: (604) 669-5255

1

Client Sarrple Reference+O.S mm SIEVE

DIAMOND COUNTVR43624A 0

0

-0.5 mm SIEVE DIAMOND COUNT

00

TOTAL DIAMOND COUNT

0Q

SYNTHETICS

00

Cmis Berne' ^x~- Observation Tearr leader


lanQA/QC Specialist

The cuiJ 'TV of ma roHi.'ifi'Cio -ri.Tj'- en an:! ^r 'vTon f'OTi rt ( rk ; J(T-(ro^ :\V"l'(x1 ; l ^rt] i- i^ -vjbj-''" lu fn-^n'df if'g thfiiji;^ .1 rij;i

f (.'j'Kri'jl CÂ. QC. ^^ '.t^ f ^. V, ; /'..-Jijrnji- J 'r-; ;- \r- , i- v.j'i.uld'.tfd "of O'ly ^ ~.plr i', c. r'.- Life "i Od-r SaUh C015 'A: :J .ip Ui f-^n -:.if(

I .vt(.?.'i(^. Tlie/îo'C. ,)( i'-î-: 1Q ::-- ot i.i'nplf^ J'*- (]...i|itv conrcl i.'(npl?:

i Ccr'tnu J l Q.-V^-L niorii:(jnr^ ir.ôl\-(:- ( r.\-n[j,K iv;:i '?t ff afOiliilfnitf d 'f'jiu c.uh "Jjt.ft to i' Jd - he J K j*.*-i.(H Jblo trli-tc^l (x-iu.ific;iH

rjOf;ifn-v F\:rjrf ; . m .itpr.i^''. H 6. /9 '. i' i. l."N, o\pardfd ^nrp-tjirtv ^( t- o 9b^- c^nfid^nco : : rn t: of jil ^.<JrlJlf•cd .'~k''od'.ifi'o' d

n:^ci.;l vîijhr\' J^.if j'lc

J- pen.: j MX "jf r. d i, id.

j jnd M- tH to 'i .'t 't 1

lO

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T^ s fopnn '.^crs to sa-nio? fi-c-rnsi?*1 as-feceiêd y ic:( be repf(xjjco3 exoepl m fuii. '^(tnout ffie w"t;*.- r pernissio^ oflhc V

•o

MO

Oct-31-Ol 16:OO Kennecott T Bay Lab

Jun-26-Ol 1G:51 Kcnnocot-t. T Bay Lab

P . OZ

P . O6


1300 Wi:sl Wnl*N .Mrn.il ThulK'Jui Giiy. O(il;iii". CANAOA P7h 4X4

(fl07) 473

Igjppratory Charge StatementInvoice to: Kennecotl Canada Exploration Ire

354-200 Granville St Vancouver BC V6C 1S4 ATTN: Kevin Kivi

Rwmitancs: Account* ReceivableAddress c/o Kennecott Canada exploration Inc.

354-200 Granvrle StVancouver BC V6C 1S4

Project: Prairie C Project tt: DO/3

Invoice*: TB000421WorK Order: 01MD013

Dal* 26-Jun-01

Quanti(y

3

0 0 0

Description

Caustic Fusion Samples ~~ Secondary Fusions Microfusiong Microdiamond Picking Micrcxjiamond Description QC^QA and Reporting

Unit Cost

S 630.00 /jample^lOkg

5 125,00 /sample^ 10kg S 10.00 /stone S 70.00 /sample^ 10kg

Total

? 1,390.00

5 55

Total Charye lo Project S 1,890, CO

Reports to follow Prairie CMlcrodlamond Processing (Caustic Fusion) Microdiamond Observation t, Description CERTIFICATE QF ANALYSIS

Sincerely,

SimonLaboratory Manager

ACCOUNTING COPY

Oct-31-Ol 16:OO Kennecott. T Ba.y Lab

Aug-o2-Ol 13:13 Kennecott T Bay Lmb

P, . 03

P.O3

49 KENNECOTT CANADA EXPLORATION INC.

MiiVi.il P'';cpv,ing 1^03 Wes ( Walsh SuT.IUflfMi Bxy. O'Hs'i

p/F 4X4

Chargeto: Kennecott Canada Exploration Inc

354-200 Granville St Vancouver BC V6C 1S4 ATTN: Kevin Kivi

ono: 'SO/) n.li- (8D7) nl'jjyO hlgil

Remitanc*: Accounts ReceivableQ'O Kennecott Canada Exploration lie 354-200 Granville St. Vancouver BC V6C 1 S*

Project: Prairie C Project ff; 0073 9? 7

Invoice* TBQ00432 Work Order: 01MD013

Date: 02-Aug-Ol

Quantity

3

30 3

Description

Caustic Fusion Samples Secondary Fusions MicrofusionsMicrodiamond Picking Microdiamond Description QC/QA and Reporting

Unit Cost

S 630 CO /sample^ 10kg

S 125.00 teample^lOkg S 10.00 /stone S 70,00 /sample** 10kg

Total

5 1.890.00

S 375.00^ SS 210. CO

Total Charge to Project: S 2.475.00

-Oc 14

Reports to foilow; Prairie CMicrodiamond Processing (Caustic Fusion) Microdiamond Observation S Description CERTIFICATE OF ANALYSIS

Sincerely,

Laboratory Manager

ACCOUNTING COPY

A ffi.-) 7/nrrj ^rrm.i

- Qisnmio MINISTRY OF NORTHERN DEVELOPMENT AND MINES

Work Report Summary

Transaction No:

Recording Date:Approval Date:

Client(s):302234302646

Survey Type(s):

W0 180. 3 1048

2001-NOV-06

2002-FEB-18

SIMPSON, MURRAY DWAREING, SIMON KEITH

BENEF

Status: APPROVED

Work Done from: 2000-NOV-12to: 2001-JUN-26

Work Report Details:Perform

Claim* Perform Approve Applied

L 1225262

L 1225263

L 1225265

External Credits:

Reserve:

SO SO S3.600SO SO 54,000

S8.712 S6.237 SO

S8.712 S6.237 57,600

SO

S2,237 Reserve of Work

S2.237 Total Remaining

Applied Assign Approve Assign Approve Reserve

SO SO 0 SO54,000 SO 0 SO

SO S7.600 4,000 S1.112

S4.000 57,600 54,000 51,112

Report*: W0 180. 3 1048

Reserve Approve Due Date

SO 2001-NOV-06SO 2002-NOV-06

S2.237 2002-AUG-19

52,237

Status of claim is based on information currently on record.

31M05SE2039 2.22377 LORRAIN 900

2002-Mar-08 13:25 Armstrong-d Page 1 of 1

Ministry ofNorthern Developmentand Mines

Date: 2002-FEB-20

Ministere duDeveioppement du Nord etdes Mines Ontario

GEOSCIENCE ASSESSMENT OFFICE 933 RAMSEY LAKE ROAD, 6th FLOOR SUDBURY, ONTARIO P3E 6B5

SIMON KEITH WAREING UNIT 1 3RD STREET P.O. BOX 270NORTH COBALT, ONTARIO POJ1RO CANADA

Tel: (888)415-9845 Fax:(877)670-1555

Dear Sir or Madam

Submission Number: 2.22377 Transaction Number(s): W0180.31048

Subject: Approval of Assessment Work

We have approved your Assessment Work Submission with the above noted Transaction Number(s). The attached Work Report Summary indicates the results of the approval.

At the discretion of the Ministry, the assessment work performed on the mining lands noted in this work report may be subject to inspection and/or investigation at any time.

The revisions outlined in the Notice dated February 18, 2002 have been only partly corrected. The expected results associated with Invoice TB000432 have not been supplied (there is only one set of results for 2 separate analyses). The 32,475.00 associated with this invoice has been removed.

The assessment credit is being reduced by 32,475.00. The TOTAL VALUE of assessment credit that will be allowed, based on the information provided in this submission, is S6,237.00.

Allowable changes to your credit distribution can be made by contacting the Geoscience Assessment Office by March 6, 2002 otherwise assessment credit will be cut-back and distributed as outlined in Section #6 of the Declaration of Assessment Work form.

If you have any question regarding this correspondence, please contact [email protected] or by phone at (705) 670-5856.

Yours Sincerely,

BRUCE GATES by email at

Ron GashinskiSenior Manager, Mining Lands Section

Gc: Resident Geologist

Murray D Simpson (Claim Holder)Simon Keith Wareing (Assessment Office)

Assessment File Library

Simon Keith Wareing (Claim Holder)

Visit our website at http://www.gov.on.ca/MNDM/LANDS/mlsmnpge.htm Page: 1 Correspondence 10:16895

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010 kennecott canada exploration inc. · august 22: 2gq1 2:03 kevin ki.i (sc7) 345-6666 kennecott...

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