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i' l ; c.:n1t1otnet._ h oot\iKiHl(oor iflllV '1-Gravenh•Q• 1 2 JIU(. \a6.a. TllAi\'SACTlONS OF TI IE SOCIETY OF lll 1 lmLO GY U: 1, 113- 123 ( 1'.167 ) Comparison of Complex Moduli Obtained from Forced and Free Damped Oscillations H. A. HELLER, fn slilute fu r the S tudy of fi' aligue and R eli ability, Co lumbia University , New York, N ew York 10027, and C. J. NED ERVEEN, '1'. N .O ., Delft, N etherlands Synopsis While the concept of tl;i e co mplex based on a forced vib raLio n ex- per iment it is a frequent practice to perfo rm instead a much simpler free damped from which an ap prox imate value of the modulus is then evalu- ated. Th e validi ty of t hi s approach and the ensuing errors are discussed and illus- tr ated on a multielement generali zed Max we ll body. It is shown that wi th modi- fi cat ions the met hod is applicable even for highly damped mate ri als. 1. Introduction Th e de f-i11i tion of the complex modulus is based on a for ced oscilla- tion experiment in which the lag angle bet we en th e imposed sinusoidal s train a nd the resulting sinu so idal st ress as well as the shape of the st ress- st rain di agram are measured. 1 Because the measurement of a lag angle is r at her diffic ul t it is a frequent pract ice to perform, in- st ead, a free damped vib rat ion experime nt measuring the na tural freque ncy and the loga ri thmic decrement from which an approximate ra]ue of the co mplex modulus is then co mputed . 2 It is to be noted, however, that the decaying osc ill at ions are no longer sinusoidal and, conse qu ently, results obta in ed from th em are inexact, the a pproximat ions being less and less accurate with increas- ing damping. 3 4 The difference b et ween res ul ts obtained in the two ty pes of experi- ment will be analyzed wi th the assumption that a generalized Maxwell body, having a large number of spring and dashp ot element s, ca n adequ ate ly re present the behav ior of a real materi a l. Th e method has TNO 95 75 11 3 Co mmunication No. 0002 92 Cent raal La boratoriu m TN 0

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Page 1: SACTlONS OF TI IE SOCIETY OF lmLOGY U - TNOpublications.tno.nl/publication/34619922/ze6hyA/heller-1967-compar… · (2.8) and (2 .11) which are based on a forced vibration experiment

i'

l ;

c.:n1t1otnet._ h oot\iK iHl(oor iflllV

'1-Gravenh•Q• 1 2 JIU(. \a6.a.

TllAi\'SACTlONS OF TI IE SOCIETY OF lll 1 lmLOG Y U : 1, 113- 123 (1'.167 )

Comparison of Complex Moduli Obtained from

Forced and Free Damped Oscillations

H. A. HELLER, fn slilute fu r the S tudy of fi'aligue and R eliabi lity , Columbia University , N ew York , N ew York 10027,

and C. J. NEDE RVEEN, '1'. N .O., Delft , N etherlands

Synopsis

While the concept of tl;i e complex modulu~ i~ based on a fo rced vibraLion ex­periment it is a frequent pract ice to perfo rm instead a much simpler free damped o~cillat io n t e~ t from whi ch an approx imate va lue of the modulus is then evalu­ated . The va lidi ty of t his approach a nd t he ensuing errors a re discussed and illus­tr ated on a mul t ielement generalized Maxwell body. It is shown that wi th modi­fi cations t he method is appli cable even for highly damped materials.

1. Introduction

The def-i11i t ion of the complex modulus is based on a forced oscilla­t ion experiment in which the lag angle between the imposed sinusoidal strain and the result ing sinusoidal stress as well as the shape of the stress- strain diagram are measured.1 Because the measurement of a lag angle is rather difficul t it is a frequent practice to perform, in­stead, a free damped vibration experiment measuring the natural frequency and the logari t hmic decrement from which an approximate ra]ue of the complex modulus is then computed. 2

It is to be noted, however, that the decaying oscillations are no longer sinusoidal and, consequently, results obtained from them are inexact, the approximations being less and less accurate with increas­ing damping. 3•

4

The difference between resul ts obta ined in the two types of experi­ment will be analyzed wi th the assumpt ion that a generalized Maxwell body, having a large number of spring and dashpot elements, can adequately represent the behavior of a real material. The method has

TNO 95 75

113 Communication No.

0002 92 Centraal Laboratorium

TN 0

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IH II . A. llELLEll AND C . .I. N l~DEllVEE'J"

been ut ilized for simple models before ;5•6 a more realistic example will be discussed here.

The complex modulus

G* = G(l + j tan 5) (1.1)

is t he constant of proportionality between an imposed sinusoida l stress

u = uo exp jwl

a nd the resul ti ng deformat ion

U Uo .

'Y = G* = IG*J exp J (wl - 8)

(1.2)

In the free vibrat ion case a mass m is attached to the model. For very soft materials a n external spring with spring constant S is also added to the model a nd one of two second-order different ial equations

m:Y + [G-(1 + j tan 5- ) + S] 'Y = 0 (1.4)

or

1n:Y + [G+(1 + j tan 5+ - (A/2) tan 5+ + Sh = 0 (1.5)

is solved with sui tab le initial conditions where a-, a+, and tan 5-or tan 5+ of eqs. (1.4) and (1.5) are not necessarily identical with G* a nd tan 8 of eq . (1.1).

The solution of eqs . (1.4) a nd (1.5)

'Y = C exp jwl (1 + j A./'2) (1.ti)

when substituted into eq. (1.4) yields7

a- = mw2 (1 - A. 2/ 4) - s (1.7)

a nd

tan 5- = 1 - A. 2/ 4 - S / mw2

(1.8)

where A. may be obtained from the measured logarithmic decrement, Ll as

(1.9)

"

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~OIHH11ee~ hoo rd, 0 11 wor t !'4\;)

'e-Gravenhao• t 2 JAr;. buci

COM PLEX MOD!JLT 115

Several a ut hors3·8 have debated the validi ty of eqs. (l.4), (1.7), a nd (l.F;) a nd use, instead, eq. (L''i) " ·hich yields

(1.10)

and

A. tano + = --------

1 + t.. 2/ -.1: - S/ inw2 (1.11)

when damping is small t he square term in eqs. (1.7), (1.8), (1.10), and (1. 11 ) is neglected. D enoti ng t he correspo nd ing mod ulw; and damping b,v G' a nd t:m 01

, respect ive ly, the fo llowing eq ll:tl'ions re­Rlll t

a nd

G' = mw2 - S

tan 01 = 1 - S/ mw2 7r (l - S/ mw2)

2. Analysis of Forced and Free Oscillations of a Generalized Maxwell Body

(1.12)

(1.1~ )

A generali zed :'ll axwe ll bod,v consist ing of rn + 1 springs a nd dnshpots as sl10\\·n in Figure 1, has the same deformat ion I' in each

G.

G.

G, r,

G, r,

O' = 0'0 SI Nwt

FORCED VIBRATION

G, T,

G, r,

G; T ;

FREE VIBRATI ON

Fig. J . Genernli i ed 1\fax well model.

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116 n . A. llELLEn Ai\D C. J . K EDl·:nn-:1·: \"

element while t he stress ui in t he ith e lement is related to t he rate of deformation t hrough t he relation

(2 .1 )

where G; is t he shear modulus (spring constant) and T ; t he relaxation time of t he ith member. The total stress on the model is

n

u = l: er ; i = 0

Performing a Laphcc transformat ion on eCJS. (2.1) a nd (2.2)

1 P"i - ,,(O) = G; (p + 1/ Ti) iT;

a nd

L: o- i i = 0

is obtained.

(2.2)

(2 .:1)

(2.4)

In eq . (2.:3) ,, (O) is the ini t ia l strain a nd u;(O) t he ini t ial stress in th e ith element.

Subst itut.ing eCJ. (2.:1) into ef). (2.4) a nd solving for iT

iT = _ .;.., pG; .;.., u;(O) - G;'Y(O)

'Y w + w ·-1=0 P+ l / T; 1 = 0 p+l/ T;

(2Ji)

is obtained. The complex shear modulus, whi ch is t he coeffi cie nt of -y, may he

obtained in it s real a nd imagi nary form by replac ing p with jw

n pGi G(p) = L

i = 0 p + l / T; (2. fi )

G*(.jw) f_ . jwO; ·i = o}W + l / T;

(2.7)

a nd

.; (W T;)2(/; ~ (i* ,, = w

; = 0 J + (w T ;) · (2.8)

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11 7

G*1,,, = " G L WT ; •

i = 0 1 + (wT;) 2 (2 .9)

from which

IG* / = (G*,,2 + G*;,,,2 )Y:i (2. 10)

and tan o = G*;,,,/ G*,e ('.2 .11 )

Attaching a mass m a nd an elast ic spring S to the model a ppl ying a forcing fun ction f(I) a 11d assuming no11zero ini t ia l conditio11s 'Y (O) = 'Yo :ind -Y(O) -Yo t he motion will be described by the differentia.l ~riuation

m :Y + er + 'YS = f(I)

or after Laplace trn11 sformation

mp2-y - mp')'o - m-Yo + a- + -yS = F(p)

Ruhsti1uti11g a- from eq. (2 .!"i) a nd solving for -y

" 0.(Yo - er ;(0) F (p) + 11ip'Yo + m-Yo + L /

i = 0 p + 1 T ;

pG s + mp2 + .L: '1

i = 0 p + } T ;

'Y

rCSlllts .

(2. 12)

(2. 1 :))

For free vihratio11s F(p) = 0. .\fultipl~ · ing both the nl!merator " and denominator of eri. ('.2. 1.+) by fT (]J + l / T;) , -y may be ex press0d as

i = ()

t he r:ttio of t \rn pol y nomi als

(J(p) -y =

h(p)

where h(p) is a poly nomial of order n + 2. The inverse transform of eri. (2 .15) y ields t he deformation of t he

model. Considering a system with less tha n criti cal cla mping, t he motion will consist of a clamped sinusoid:tl vib r:ition superimposed on severa l creep terms. 9

Because only one mass is attached to the model the system has a single cl0g;ree of fr0cdom and will vibrate at a single freril!ency w.

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11 B n. A . llELLEn A ro c. J. YED1 ~ 1wE 1 ~ \

Consequently, eq. (2.15) when expanded into n + 2 partial fractwns will produce two terms with complex conjugate a nd n terms with real de no mi o.ators

'Y _ g(p) = aow + ai(p + k) + _ a_2 _ - h(p) (p + k) 2 + w2 p + 82

(2.16) aa

+ P + 8a + and ::tfter inversion.

where k and w are the real and imaginary parts of the single pair of complex roots and 82 .. . 8n+2 then real roots of the polynomial h(p) .

The values of k and w are independent of the ini t ial conditions and, therefore, the complex modulus can be determined directly .

Varying the appl ied mass, m , a nd spring constant, S, the logarith­mic decrement ~ = 27rk/ w can be computed as a function of the frequency w for any given set of Gi and r t. Th ese values may then be substituted into eq. (1.9) to obtain A. which in tum may be used to compute three different values of G from eqs. (1.7) , (1.10) , and (1.12) and three values of the damping, tan l'i, from eqs. (1.8), (1.11), and (1.1:3). These may then be compared with G*,. and tan l'i of eqs. (2.8) and (2 .11) which are based on a forced vibration experiment.

3. Numerical Comparison

The method is illustrated for a standard solid consisting of a spring (Go = 200 psi) and a Maxwell element ( r1 = 1 sec, G1 = 800 psi) in parallel. Results are plotted as functions of the angular frequency w in Figure 2.

It is to be noted that for small damping the free and forced moduli and tan /j coincide. Appreciable differences occur for increasing damping and especially for values greater than 0.6.

The inclusion of th e A. 2/ 4 terms, with a minus sign in eqs. (1.7) and (1.8) creates large errors in both modulus and damping. 8 When it is used with a plus sign in eqs. (1.10) and (1.11) the damping, tan l'i , obtained from forced vibration computations [eq. (2.11)] is well approximated but the modulus, Q+, is considerably overestimated

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1000

800

;:;; 600 a..

.n 400 :::J _J

:::J 0 0 ::.

200 (.'.)

100

10

8

6

4

2 (.'.)

z a: ::. <l I 0

,,; 0 .8 c 0 . 6 .,,

0.4

COM l'LEX MODU Ll

°"'"'o ~'•'"°"" LJT,~ISEC

I

l-- +---- - l-------+-------1-----·--l

0 .05 0.1 0 .5 I 5 10 w , FREQUENCY, RAO/SEC

Fig. 2. :\Ludulus a m! damping of standard so lid .

11.9

:ompared with G*,,. The si mpli!ied quantiti es of eqs. (1. U) and (1.13) wit hout the sq uare term prov ide a better approximation for the modulus while the damping is too high.

As damping values greate r than O.:) are very diffi cul t to measure with some precision, the use of a 11 additional elastic element is a neces:; ity. In Figure 3 resu lts are shown for the model of Figure 2 wit h au addi t ional sp ring (S = 1200 psi) with which t he apparent tan o = t:J. / 7r of the complete system stays below 0.26. It i::; observed t hat the error i::; considerably smaller in t he transition region. Using the

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120

(/)

a. (/)

::i ...J ::i 0 0 ::;;

"' z a: ::;; <t 0

.0 c: !?

H. A. ll ELLEll A;\D C. J . NEDEBVEEN

-- G;e ---- G' - · - G+ -··- G-

1.0

0 .8

0 .6

0 .4

0 .2

0 .1 0.08

0 .06

0 .04

o .02 Lo....J.oLs- -0-'_-1 --------'o _-s __ _..1 ______ ....Js'-----'10

w, FREQUENCY, RAD /SEC

Fig. :l . M0Juh1>; nnJ damping of Lhe ~Landard ~u li d ~huw 11 i11 F ig. 2 wiLh aJJeJ elast ic member fur free vibrations.

simplif-i ed eqs. (1.12) and (1.13) it is less than 163 for the damping and less tha n 63 fo r the real part of the modulus. Because the overall damping is small t he inclusion of the square term has no appreciable effect.

The region in which an added t iffnes. can be used in practice is limi ted because a measurement uncertainty in ~ is amplified in t he same proport ion as the damping is teduced [see eq. (1. 13) ]. The practical limi t of t his method is around a material da mping of 3.

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f:OM PLEX MODT JLI 121

TABLE I Parametern Of Generafoed Maxwell :\1odel

G;, p~ i r -1 , sec

() 200 00

l 200 10 2 400 1. 0 ~ 600 10 - 1

4 800 10 - 2 ;) 2,200 io - a (i 6,200 10- • 7 2.i , GOO 10 -'' 8 141 , ()()() 10 -•

The general trend of these results conforms to t hose of :U arkovitz and Parke5•6 obtained on a standard solid.

A second example is given for a real material. A large number of free damped vibration experiments were pre­

viously conducted on a potassium chloride filled polyurethane elasto­mer to determine its complex shear modulus and da mping over a wide range of freq uencies. 10 A generalized Maxwell model, consisting of a spring and eight spring-dashpot elements in parallel, was fitted to the test results using Tobolsky 's method. 11 The obtai ned G and r

values are li sted in Table I. These parameters were then introduced into eqs. (2.8) and (2.11)

to determine the forced motion modulus and da mping and into eqs. (1.7)- (1.13) for the free damped values.

The solu tions of the n + 2 = lOth-order polynomial equation, h(p) , was carri ed out on an IBM 7094 computer for various values of m. The computations have in each case, as expected, produced a i;:ingle set of complex conjugate roots and therefore only one value of frequency w for each value of m.

The computed quantities are compared in Figure 4. The results indi cate a similar trend as those of t he three-element model.

4. Conclusions

An analysis of a generalized -:\Iaxwell model, representing a visco­elastic solid under conditions of fo rced and free osci llat ions shows that the complex moduli computed from t he two types of motions are not identical. For low damping t he approximation provided by a free-

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·122

(/)

a. (/)

3 ::> 0 0 :::;;

..;

c £

10° 8

6

4

2

10• 8

6

4

2

10'

10 8 6

4

2

I

0 .8

0 .6

0-4

0-2

H. A. 11 l•: LJ .E ll A 'W C. J . N 1m 1m v 1·:1•: \T

I/ /).

if/

/l/ G+ , VI .. y·

G;e . ,

1V LG-. ./ :

/ .y I /// .'

G' - IX~' \ J b IP' .

1/ L-. ~ ,... ,....

./.,....

:r\ ! ',<on8

i ton8--.. ,,,.-- ...... A1on8

1

/ < - ,_ \,

- __ / _/_.« --1 ~-~'-/:-/ . ~ l....1on8+ '>i,,: ~

__ ...,,; 'iY '\~ "':::::,::..:,- --

10 1a2 10' 10• 10° 107

w, FREQUENCY, RAD/SEC

F ig. 4. Mod ulus and damping of a generalized ~1Iaxwe ll model shown 111 Fig. with con~tan ts listed in T able I.

vibrati on experiment is good. The dev iat ions stay below 203 when the logari thmic decrement of the oscillatory system, which if needed is provided with an additi onal elastic element, is less tha n 0.6 .

D amping values are improved by the inclusion of the square of the logari t hmic decrement in eq. (1.11), while a better approximat ion of t he modulus is obta ined when thi term is neglected.

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COM l' LEX MODULI 123

Thi s research has been supported by t he U.S. Offi ce u[ Naval ll esearch under t·o11trnct Nu. NONR 266(78 ) and carried out at the Department of Civi l Engi-11 ee ri 11g, Columbia University.

References

J. D. H. Bland, The Theory of Linear Viscoelasticity, Pergamun, New York, l!J60.

2. F. R. Schwa rz! and A. J . Staverma n, J. Appl. Phys., 23, 838 (HJ:i2). 3. S. Neumark, Concept of Complex Stiffness Applied to Problems o.f O.scil­

lations with Visco1ls and H ysteretic Damping, Royal Aircraft Establi ~h men t

Heport No. Aero. 2592, 19.'i7. 4. A. J . Staverman and F. R. Schwarz!, "Linear D eformation Beha viu r of

ll igh Polymers," in Die Physik der Hochpolymeren, \ ·01. I \ ", Jl. A. f:>tuart, Ed., Springer- \"erlag, Berli n, 1956 .

. '). H . i\Iarkovitz, J. Appl. Phys., 22 , 21 (1963). 6. S. Parke, Brit. J . flppl. Phys., 17 , 27 1 (1966). 7. H. Buchda hl , "The Rheology of Organi c Glasses," in Hheology, F. E ir ich,

Ed. , Academic Press, New York, 1958, p. 148. 8. N. W. T schoegl, J. Appl. Phys., 32, 1792 (1961). 9. A. S. E lder, 'l'rans . Soc. Rheol., 9 :2, 187 (1965).

10. T. Nicholas a nd R . A. Heller, Expll. M ech., 7 :3, 110 (1967 ). 11. A. Y. Tobolsky, Properties and Strucl1lre of Polymers, Wiley, New York,

1960.