revised: 6/20/2014 pipeline specifications yellowstone pipeline · the mercaptan sulfur...

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Product Name Pipeline Specifications Product Code(s) click on product information to go to associated specification Yellowstone Pipeline 6/20/2014 Revised: Gasoline, Conventional, 85.5 octane (no ethanol) 9.0#- D4R; >9.0#- D4Q Gasoline, Conventional, 87 octane (no ethanol) 9.0#- D7U; >9.0#- D3H Gasoline, Conventional, 91 octane (no ethanol) 9.0#- P1U; >9.0#- P64 Gasoline, Conventional, 92 octane (no ethanol) 9.0#- P2U; >9.0#- P4J Gasoline, Subgrade, 84 octane 9.0#- D69; >9.0#- D53 Gasoline, Subgrade, 81.5 octane (currently available as segregated batches only; any transmix generated is shipper's responsibility) 9.0#- D4V; >9.0#- D4U Gasoline, Premium Subgrade, 90 octane (currently for shipment from the Hillyard Manifold to Spokane and Moses Lake) 9.0#- P0C; >9.0#- P0B Gasoline, Subgrade, 87 octane after 10% ETOH addition 9.0#- D6V; >9.0#- D6U Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (for CHS Missoula Destination only, does NOT meet Jet A specifications) #1D 15 ppm Diesel- VA1 Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications) #1D 15 ppm Diesel- VA3 Distillate, #2 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets #2 Fuel Oil specifications) #2D 15 ppm Diesel- V95 Volatility Schedule, Conventional, All Grades, All product that will be delivered to WA (not MT) Various

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Page 1: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Product Name

PipelineSpecifications

Product Code(s)

click on product information to go to associated specification

Yellowstone Pipeline

6/20/2014Revised:

Gasoline, Conventional, 85.5 octane (no ethanol) 9.0#- D4R;>9.0#- D4Q

Gasoline, Conventional, 87 octane (no ethanol) 9.0#- D7U;>9.0#- D3H

Gasoline, Conventional, 91 octane (no ethanol) 9.0#- P1U;>9.0#- P64

Gasoline, Conventional, 92 octane (no ethanol) 9.0#- P2U;>9.0#- P4J

Gasoline, Subgrade, 84 octane 9.0#- D69;>9.0#- D53

Gasoline, Subgrade, 81.5 octane (currently available as segregatedbatches only; any transmix generated is shipper's responsibility)

9.0#- D4V;>9.0#- D4U

Gasoline, Premium Subgrade, 90 octane (currently for shipment fromthe Hillyard Manifold to Spokane and Moses Lake)

9.0#- P0C;>9.0#- P0B

Gasoline, Subgrade, 87 octane after 10% ETOH addition 9.0#- D6V;>9.0#- D6U

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (for CHSMissoula Destination only, does NOT meet Jet A specifications)

#1D 15 ppm Diesel- VA1

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications)

#1D 15 ppm Diesel- VA3

Distillate, #2 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets #2 Fuel Oil specifications)

#2D 15 ppm Diesel- V95

Volatility Schedule, Conventional, All Grades, All product that will be delivered to WA (not MT)

Various

Page 2: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Product Name

PipelineSpecifications

Product Code(s)

click on product information to go to associated specification

Yellowstone Pipeline

6/20/2014Revised:

Volatility Schedule, Conventional, All Sub-octane Grades, All productthat may be delivered to MT (can also go to WA), all properties (except clear RVP) must be met on 10 vol% ethanol hand blend

Various

Volatility Schedule, Conventional, All Full Octane Grades, All product that may be delivered to MT (can also go to WA)

Various

Page 3: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Yellowstone Pipeline

PipelineSpecifications

Previous Publication Date: 4/29/2014

Current Publication Date: 6/20/2014

Revision Notes:Modified volatility tables for Montana deliveries to reflect the latest requirements in ASTM D4814.

Page 4: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 85.5 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- D4R;>9.0#- D4Q

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating85.5Octane, (R+M) / 2 D2699 & 2700 OR D2885 580.5Octane, Motor D2700 OR D2885 5

ReportOctane, Research D2699 OR D2885240Oxidation Stability D525 Oxid Stab by Ind Period minutes

Oxygenates Prohibited See Note 60.003Phosphorus D3231 Phosphorus in Gasoline g/gal

Product Description See Note 7Referee Methods See Note 8

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 5: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 85.5 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- D4R;>9.0#- D4Q

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. Requirements for Octane have been adjusted for altitude per ASTM D 4814.

6. The use of alcohols and ethers as blending components at origin is prohibited.

7. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

8. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 6: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 87 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- D7U;>9.0#- D3H

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating87.0Octane, (R+M) / 2 D2699 & 2700 OR D288582.0Octane, Motor D2700 OR D2885

ReportOctane, Research D2699 OR D2885240Oxidation Stability D525 Oxid Stab by Ind Period minutes

Oxygenates Prohibited See Note 50.003Phosphorus D3231 Phosphorus in Gasoline g/gal

Product Description See Note 6Referee Methods See Note 7

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 7: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 87 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- D7U;>9.0#- D3H

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. The use of alcohols and ethers as blending components at origin is prohibited.

6. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

7. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 8: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 91 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- P1U;>9.0#- P64

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating91.0Octane, (R+M) / 2 D2699 & 2700 OR D2885

ReportOctane, Motor D2700 OR D2885ReportOctane, Research D2699 OR D2885

240Oxidation Stability D525 Oxid Stab by Ind Period minutesOxygenates Prohibited See Note 5

0.003Phosphorus D3231 Phosphorus in Gasoline g/galProduct Description See Note 6Referee Methods See Note 7

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 9: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 91 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- P1U;>9.0#- P64

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. The use of alcohols and ethers as blending components at origin is prohibited.

6. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

7. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 10: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 92 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- P2U;>9.0#- P4J

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating92.0Octane, (R+M) / 2 D2699 & 2700 OR D2885

ReportOctane, Motor D2700 OR D2885ReportOctane, Research D2699 OR D2885

240Oxidation Stability D525 Oxid Stab by Ind Period minutesOxygenates Prohibited See Note 5

0.003Phosphorus D3231 Phosphorus in Gasoline g/galProduct Description See Note 6Referee Methods See Note 7

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 11: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Conventional, 92 octane (no ethanol)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- P2U;>9.0#- P4J

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. The use of alcohols and ethers as blending components at origin is prohibited.

6. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

7. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 12: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 84 octane

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- D69;>9.0#- D53

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating84.0Octane, (R+M) / 2 D2699 & 270080.0Octane, Motor D2700 OR D2885

ReportOctane, Research D2699 OR D2885240Oxidation Stability D525 Oxid Stab by Ind Period minutes

Oxygenates Prohibited See Note 50.003Phosphorus D3231 Phosphorus in Gasoline g/gal

Product Description See Note 6Referee Methods See Note 7

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 13: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 84 octane

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- D69;>9.0#- D53

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. The use of alcohols and ethers as blending components at origin is prohibited.

6. This fuel meets or exceeds all the requirements of ASTM D4814 (Unleaded Gasoline). In addition, this fuel is a sub-octanegasoline, meant for blending with ethanol or a higher octane non-oxygenated gasoline in order to meet minimum octanerequirements. This product is base gasoline and does not meet the EPA detergent additive requirement for finished gasoline. Thisproduct does not meet the requirements for reformulated gasoline (RFG) and may not be used in any reformulated gasoline coveredarea.

7. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 14: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 81.5 octane (currently available as segregated batches only; any transmix generated is shipper's responsibility)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- D4V;>9.0#- D4U

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating85.5Octane, (R+M) / 2 w/ 10% ETOHD2699 & 2700 581.5Octane, (R+M) / 2 D2699 & 2700 OR D2885

ReportOctane, Motor D2700 OR D2885ReportOctane, Research D2699 OR D2885

240Oxidation Stability D525 Oxid Stab by Ind Period minutesOxygenates Prohibited See Note 6

0.003Phosphorus D3231 Phosphorus in Gasoline g/galProduct Description See Note 7Referee Methods See Note 8

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 15: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 81.5 octane (currently available as segregated batches only; any transmix generated is shipper's responsibility)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- D4V;>9.0#- D4U

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. Shippers must meet the 85.5 octane minimum with a hand blend containing 10 volume % denatured fuel ethanol.

6. The use of alcohols and ethers as blending components at origin is prohibited.

7. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

8. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTMD4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 16: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Premium Subgrade, 90 octane (currently for shipment from the Hillyard Manifold to Spokane and Moses Lake)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- P0C;>9.0#- P0B

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating92.0Octane, (R+M) / 2 w/ 10% ETOHD2699 & 2700 590.0Octane, (R+M) / 2 D2699 & 2700 OR D2885

ReportOctane, Motor D2700 OR D2885ReportOctane, Research D2699 OR D2885

240Oxidation Stability D525 Oxid Stab by Ind Period minutesOxygenates Prohibited See Note 6

0.003Phosphorus D3231 Phosphorus in Gasoline g/galProduct Description See Note 7Referee Methods See Note 8

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 17: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Premium Subgrade, 90 octane (currently for shipment from the Hillyard Manifold to Spokane and Moses Lake)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- P0C;>9.0#- P0B

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. Shippers must meet the 92.0 octane minimum with a hand blend containing 10 volume % denatured fuel ethanol.

6. The use of alcohols and ethers as blending components at origin is prohibited.

7. This fuel meets or exceeds all the requirements of ASTM D 4814 (Unleaded Gasoline). This product does not meet EPA additiveaddition requirements for finished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and maynot be used in any reformulated gasoline covered area.

8. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTMD4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 18: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 87 octane after 10% ETOH addition

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:9.0#- D6V;>9.0#- D6U

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 2ReportBasicity D1093 Acidity, mod. see note 3

4.0Benzene D3606 Benz & Tol by GC Vol%UndyedColor Visual

1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating0.01Lead (Pb) @ originD3237 Lead by AA gPb/gal

0.002Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 4sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

B+NACE Rust test NACE Rust TM0172-2001 Rating87.0Octane, E10, (R+M) / 2 w/ 10 vol% ETOHD2699 & 270082.0Octane, E10, Motor w/ 10 vol% ETOHD2700 OR D288583.0Octane, NEAT, (R+M) / 2 w/o ETOHD2699 & 2700

ReportOctane, NEAT, Motor w/o ETOHD2700 OR D2885ReportOctane, Research w/ and w/o ETOHD2699 OR D2885

240Oxidation Stability D525 Oxid Stab by Ind Period minutesOxygenates Prohibited See Note 5

0.003Phosphorus D3231 Phosphorus in Gasoline g/galProduct Description See Note 6Referee Methods See Note 7

1Silver Strip Corrosion D7667 or D7671 Rating5Solvent Washed Gum D381 Gum Content by Jet Evap mg/100ml

80Sulfur D2622 OR D5453 ppmsee TableVolatility & Distillation D4814 Spec for Auto SI Fuels

Page 19: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Gasoline, Subgrade, 87 octane after 10% ETOH addition

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:9.0#- D6V;>9.0#- D6U

Notes:

1. This fuel may contain antioxidants/sweeteners and corrosion inhibitors. Corrosion inhibitors may be required to meet the 1 mil/yrstandard pipeline corrosion rate. The use of other additives is prohibited. All additives and their concentrations must be previouslyapproved by the pipeline Quality Control Coordinator, and must be clearly indicated on the Certificate of Analysis. The EPAspecifically prohibits the intentional addition of additives containing lead, phosphorus, or heavy metals. No intentional addition ofMMT, phosphorus, lead, or additives containing other heavy metals is allowed.

2. The finished fuel shall be visually free of undissolved water, sediment, and suspended matter; it shall be clear and bright at theambient temperature or 21 Deg C (70 Deg F), whichever is higher. (ASTM D 4814)

3. ASTM D1093 should be performed to test for basicity according to the instructions in section 9.3 and 9.4 of the ASTM methodusing a phenolphthalein indicator solution, except as noted below. Combine 50 ml of the sample, 15 ml of water, and 3 drops ofphenolphthalein indicator solution in a clean centrifuge tube, shake vigorously for 30 seconds, let stand for 3 minutes and observeagainst a white background (the centrifugation step in the ASTM method is not required). See the method for additional details. If aslightly pink to red color is observed in the water phase, the sample shows alkalinity and fails the test. The sample tested should be alower sample as described in ASTM D4057, "...a spot sample of liquid from the middle of the lower one-third of the tank's content..."

4. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

5. The use of alcohols and ethers as blending components at origin is prohibited.

6. This fuel meets or exceeds all the requirements of ASTM D4814 (Unleaded Gasoline). In addition, this fuel is a sub-octanegasoline, meant for blending with ethanol in order to meet minimum octane requirements. All properties must be met on the neat fuel(no ethanol) unless specified otherwise. This product is base gasoline and does not meet the EPA detergent additive requirement forfinished gasoline. This product does not meet the requirements for reformulated gasoline (RFG) and may not be used in anyreformulated gasoline covered area.

7. Referee Methods for Gasoline are as follows:Vapor / Liquid Ratio, ASTM D5188. (source ASTM D4814); Oxygenates, ASTM D5599 is the EPA approved method, ASTM D4815 may be used if the method is correlated back to ASTM D5599.EPA regulated properties must be performed in accordance with EPA approved test methods published in 40 CFR Part 80.

Page 20: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (for CHS Missoula Destination only, does NOT meet Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:#1D 15 ppm Diesel- VA1

Additives General Note 1ReportAPI Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 20.01Ash D482 Ash Wt%0.15Carbon Res 10% Btms D524 Ramsbottom Carb Res Wt%

40Cetane by DSC D6890 or D7170 Cetane Number 335.0Cetane Ind-2 or Arom D1319 Hydrocarbon Typ by FIA Vol% 4

40.5Cetane Ind-2 or Arom D976 Cetane Index by 2-var 440.0Cetane Number or Ind-4 D4737 Cet Ind by 4-var calc A 540Cetane Number or Ind-4 D613 Cetane Number by Engine 5

UndyedColor Visual 6+18Color, Saybolt D156 Saybolt Color+18Color, Saybolt D6045 Color by Auto TriStim

1Copper Strip Corrosion D130 Cu Str 2 Hr @ 212 F RatingReportDist 10 Vol% Rec D2887 Sim Dist by GC Deg FReportDist 10 Vol% Rec, corr D86 Dist at Atm Press Deg FReportDist 50 Vol% Rec D2887 Sim Dist by GC Deg FReportDist 50 Vol% Rec, corr D86 Dist at Atm Press Deg F

579Dist 90 Vol% Rec D2887 Sim Dist by GC Deg F550Dist 90 Vol% Rec, corr D86 Dist at Atm Press Deg F

ReportDist End Pt D2887 Sim Dist by GC Deg FReportDist End Pt D86 Dist at Atm Press Deg FReportDist IBP D2887 Sim Dist by GC Deg FReportDist IBP, corr D86 Dist at Atm Press Deg FReportDist Loss, corr D86 Dist at Atm Press Vol%ReportDist Residue D86 Dist at Atm Press Vol%

110Flash Pt D56 Flash Pt by TCC Deg F2Haze @ 70 deg F D4176 Wtr & Part Cont, Proc 2 Rating

B+NACE Rust test NACE Rust TM0172-2001 RatingProduct Description See Note 7Referee Methods See Note 8

11Sulfur @ origin BillingsD2622, D5453, D7039 ppm 92.41.3Viscosity @ 104 F D445 Kinematic Viscosity cSt

0.05Water & Sed, total D2709 Water & Sed by Centr Vol%

Page 21: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (for CHS Missoula Destination only, does NOT meet Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:#1D 15 ppm Diesel- VA1

Notes:

1. The use of Biodiesel, including Fatty Acid Methyl Esters (FAME's), is strictly prohibited. The fuel may containantioxidants/sweeteners, corrosion inhibitors, and pour point depressants. Corrosion inhibitors may be required to meet the 1 mil/yr standard pipeline corrosion rate. All additives and their concentrations must be previously approved by the pipeline Quality ControlCoordinator, and must be clearly indicated on the Certificate of Analysis.

2. The diesel fuel shall be visually free of undissolved water, sediment, and suspended matter. (ASTM D975)

3. The derived cetane number (DSC) measured by these methods can be used for cetane measurement. D613 is the referee methodfor cetane.

4. Either the Cetane Index by 2-variables minimum or the Aromatics maximum must be met (see ASTM D975 Table 1 notes formethod version)

5. Where cetane number by Test Method D 613 is not available, Test Method D 4737 can be used as an approximation. (ASTMD975 Table 1 Notes)

6. Under United States regulations, if distillates are sold for tax exempt purposes then, at or beyond terminal storage tanks, they arerequired by 26 CFR Part 48 to contain the dye Solvent Red 164 at a concentration spectrally equivalent to 3.9 lb per thousand barrelsof the solid dye standard Solvent Red 26, or the tax must be collected. (ASTM D975 Table 1 Notes)

7. This fuel meets or exceeds all the requirements of ASTM D975 (Ultra Low Sulfur Grade No. 1-D S15 Diesel Fuel Oil), with the possible exception of the lubricity/conductivity requirements in ASTM D975. Additives or further blending may be utilized at downstream locations to meet these requirements.

8. ASTM Referee Methods for #1 Diesel Fuel, 15 ppm Sulfur, are as follows:Cloud Pt, ASTM D2500; Distillation, ASTM D86; Flash Point, ASTM D93; Sulfur, ASTM D5453. (source ASTM D975)

9. For this product, sulfur test instruments and methods used at each facility must be qualified by the current EPA approved method(see 40 CFR Part 80 for approved methods).

Page 22: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:#1D 15 ppm Diesel- VA3

0.10Acid Number D3242 Acidity in Turb Fuel mg KOH/gAdditives General Note 1

50.537.5API Gravity (60 Deg F) D287, D1298, D4052 APIClear & BrAppearance Visual 2

24.9Aromatics D1319 Hydrocarbon Typ by FIA Vol%0.01Ash D482 Ash Wt%0.15Carbon Res 10% Btms D524 Ramsbottom Carb Res Wt%

40Cetane by DSC D6890 or D7170 Cetane Number 340.0Cetane Number or Ind-4 D4737 Cet Ind by 4-var calc A 440Cetane Number or Ind-4 D613 Cetane Number by Engine 4

UndyedColor Visual 5+18Color, Saybolt D156 Saybolt Color+18Color, Saybolt D6045 Color by Auto TriStim

1Copper Strip Corrosion D130 Cu Str 2 Hr @ 212 F Rating361Dist 10 Vol% Rec D2887 Sim Dist by GC Deg F397Dist 10 Vol% Rec, corr D86 Dist at Atm Press Deg F

ReportDist 50 Vol% Rec D2887 Sim Dist by GC Deg FReportDist 50 Vol% Rec, corr D86 Dist at Atm Press Deg F

579Dist 90 Vol% Rec D2887 Sim Dist by GC Deg F550Dist 90 Vol% Rec, corr D86 Dist at Atm Press Deg F566Dist End Pt D86 Dist at Atm Press Deg F638Dist End Pt, corr D2887 Sim Dist by GC Deg F

ReportDist IBP D2887 Sim Dist by GC Deg FReportDist IBP, corr D86 Dist at Atm Press Deg F

1.5Dist Loss, corr D86 Dist at Atm Press Vol%1.5Dist Residue D86 Dist at Atm Press Vol%6Existent Gum D381 Gum Content by Jet Evap mg/100 ml 6

110Flash Pt D56 Flash Pt by TCC Deg F-41Freeze Pt D2386 Freeze Pt by manual Deg C-41Freeze Pt D5972 Freeze Pt by Ph Tech Deg C2Haze @ 70 deg F D4176 Wtr & Part Cont, Proc 2 Rating

25JFTOT Press Drop D3241 JFTOT@ 260 C mm Hg 7<3JFTOT Tube Rating D3241 JFTOT@ 260 C Rating 7

0.003Mercaptan Sulfur D3227 Thiol Merc S by Titra Wt% 8sweetMercaptan Sulfur D4952 Active S by Doc Tst Rating

85MSEP D3948 Water Sep by MSEP Rating20Naphthalenes or Smoke Pt D1322 Smoke Pt mm 9

2.9Naphthalenes or Smoke Pt D1840 Naphthalenes by UV Vol% 918,410Net Heat of Combustion D3338 Net Heat of Comb BTU/lb

42.9Net Heat of Combustion D3338 Net Heat of Comb MJ/kg18,410Net Heat of Combustion D4809 Heat of Comb bomb cal BTU/lb

42.9Net Heat of Combustion D4809 Heat of Comb bomb cal MJ/kgReportParticulates D2276 Parti Cont in Av Fuel mg/galReportParticulates D5452 Partic in Av Fuels mg/gal

Page 23: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:#1D 15 ppm Diesel- VA3

Product Description See Note 10Referee Methods Diesel FuelSee Note 11Referee Methods Jet FuelSee Note 12Specification Severity See Note 13

11Sulfur @ origin BillingsD2622, D5453, D7039 ppm 1413Sulfur @ origin SpokaneD2622, D5453, D7039 ppm 1413Sulfur @ origin Thom FallsD2622, D5453, D7039 ppm 14

Test Tolerances See Note 158.0Viscosity @ -4 F (-20 C) D445 Kinematic Viscosity cSt2.41.3Viscosity @ 104 F D445 Kinematic Viscosity cSt

0.05Water & Sed, total D2709 Water & Sed by Centr Vol%

Page 24: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:#1D 15 ppm Diesel- VA3

Notes:

1. The use of Biodiesel, including Fatty Acid Methyl Esters (FAME's), is strictly prohibited. Only those additives specified andwithin the concentrations noted in the current edition of ASTM D 1655 are permitted. Use of additives permitted by ASTM D 1655must be clearly indicated on the Certificate of Analysis. All additives must be previously approved by the pipeline Quality Control Coordinator. The use of any other additives is prohibited.

2. The diesel fuel shall be visually free of undissolved water, sediment, and suspended matter. (ASTM D975)

3. The derived cetane number (DSC) measured by these methods can be used for cetane measurement. D613 is the referee methodfor cetane.

4. Where cetane number by Test Method D 613 is not available, Test Method D 4737 can be used as an approximation. (ASTMD975 Table 1 Notes)

5. Under United States regulations, if distillates are sold for tax exempt purposes then, at or beyond terminal storage tanks, they arerequired by 26 CFR Part 48 to contain the dye Solvent Red 164 at a concentration spectrally equivalent to 3.9 lb per thousand barrelsof the solid dye standard Solvent Red 26, or the tax must be collected. (ASTM D975 Table 1 Notes)

6. Existent Gum is, by definition, a measurement of unwashed gum content. A washed gum content is known as "Solvent WashedGum". (ASTM D 381)

7. JFTOT Thermal stability test shall be conducted for 2.5 hours at a controlled temperature of 260 C (500 F) minimum. No peacockor abnormal color deposits are allowed. (ASTM D1655, Table 1). Tube deposit ratings shall always be reported by the VisualMethod; a rating by the Tube Deposit Rating (TDR) optical density method is desirable but not mandatory. (ASTM D1655, Table 1,Notes)

8. The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in ASTM D 4952.

9. One of the following requirements shall be met:A. Smoke Point 27 mm minimum by ASTM D 1322 ORB. Smoke Point 20 mm minimum AND Naphthalenes 2.9 Vol% maximum by ASTM D 1840.

10. This fuel meets or exceeds the requirements of ASTM D1655 (Jet A) and ASTM D975 (Ultra-Low Sulfur Grade No. 1-D S15Diesel Fuel Oil), with the possible exception of the lubricity/conductivity requirements in ASTM D975. Additives or furtherblending may be utilized at downstream locations to meet these requirements.

11. ASTM Referee Methods for #1 Diesel Fuel, 15 ppm Sulfur, are as follows:Cloud Pt, ASTM D2500; Distillation, ASTM D86; Flash Point, ASTM D93; Sulfur, ASTM D5453. (source ASTM D975)

12. ASTM Referee Methods for Jet A are as follows:Aromatics, ASTM D1319; Distillation, ASTM D86; Flash Point, ASTM D56; Existant Gum, ASTM D381; Freeze Point, ASTMD2386; Net Heat of Combustion, D 4809. (ASTM D1655) For a product satisfying both ASTM D1655 (Jet A) and ASTM D975 (#1 Diesel Fuel Oil), ASTM D56 is considered the refereemethod.

13. Because of the requirements for test tolerances in ASTM D 1655 (and detailed in footnote 749) some of the specification limits set forth

here are slightly more severe than as set forth in ASTM D 1655.

Page 25: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #1 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets Jet A specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised: Product Codes:#1D 15 ppm Diesel- VA3

14. For this product, sulfur test instruments and methods used at each facility must be qualified by the current EPA approved method (see 40 CFR Part 80 for approved methods).

15. Test results shall not exceed the maximum or be less than the minimum values specified (herein). No allowance shall be made forthe precision of the test methods. To determine conformance to the specification requirement, a test result may be rounded to thesame number of significant figures as in this specification using Practice E 29. Where multiple determinations are made, the average result, rounded in accordance with Practice E 29, shall be used. (ASTM D1655)

Page 26: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #2 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets #2 Fuel Oil specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:#2D 15 ppm Diesel- V95

Additives General Note 130.0API Gravity (60 Deg F) D287, D1298, D4052 API

Clear & BrAppearance Visual 20.01Ash D482 Ash Wt%0.35Carbon Res 10% Btms D524 Ramsbottom Carb Res Wt%

40Cetane by DSC D6890 or D7170 Cetane Number 335.0Cetane Ind-2 or Arom D1319 Hydrocarbon Typ by FIA Vol% 4

42Cetane Ind-2 or Arom D976 Cetane Index by 2-var 440.0Cetane Number or Ind-4 D4737 Cet Ind by 4-var calc A 540Cetane Number or Ind-4 D613 Cetane Number by Engine 5

16Cloud Pt Apr - AugD2500 Cloud Pt by manual Deg F10Cloud Pt MarD2500 Cloud Pt by manual Deg F6Cloud Pt Sep - FebD2500 Cloud Pt by manual Deg F

16Cloud Pt Apr - AugD5773 Cloud Pt by Phase Tech Deg F10Cloud Pt MarD5773 Cloud Pt by Phase Tech Deg F6Cloud Pt Sep - FebD5773 Cloud Pt by Phase Tech Deg F

UndyedColor Visual 62.5Color, ASTM D1500 Color (ASTM scale)1Copper Strip Corrosion D130 Cu Str 3 Hr @ 122 F Rating

ReportDist 10 Vol% Rec D2887 Sim Dist by GC Deg FReportDist 10 Vol% Rec, corr D86 Dist at Atm Press Deg FReportDist 50 Vol% Rec D2887 Sim Dist by GC Deg FReportDist 50 Vol% Rec, corr D86 Dist at Atm Press Deg F

672572Dist 90 Vol% Rec D2887 Sim Dist by GC Deg F640540Dist 90 Vol% Rec, corr D86 Dist at Atm Press Deg F

ReportDist End Pt D2887 Sim Dist by GC Deg FReportDist End Pt, corr D86 Dist at Atm Press Deg FReportDist IBP D2887 Sim Dist by GC Deg FReportDist IBP, corr D86 Dist at Atm Press Deg F

135Flash Pt Billings orgnD93 PMCC Flash Pt Deg F130Flash Pt Spokane rcptD93 PMCC Flash Pt Deg F

2Haze @ 70 deg F D4176 Wtr & Part Cont, Proc 2 RatingB+NACE Rust test NACE Rust TM0172-2001 Rating

21Pour Pt Mar - AugD5949 Pour Pt by Phase Tech Deg F-15Pour Pt Sep - FebD5949 Pour Pt by Phase Tech Deg F

Product Description See Note 7Referee Methods See Note 8Referee Methods See Note 9

11Sulfur @ origin BillingsD2622, D5453, D7039 ppm 1013Sulfur @ origin SpokaneD2622, D5453, D7039 ppm 1013Sulfur @ origin Thom FallsD2622, D5453, D7039 ppm 10

75Thermal Stability W test unitD6468 Stab by Ref, 90 min. % Refl82Thermal Stability Y test unitD6468 Stab by Ref, 90 min. % Refl

4Thermal Stability DuPont 90 min @ 300 F Pad Rating

Page 27: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

Distillate, #2 Diesel Fuel, Ultra-Low Sulfur (15 ppm max), (also meets #2 Fuel Oil specifications)

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:

Test MethodProperty SpecificMin Max Note#Units

Product Codes:#2D 15 ppm Diesel- V95

3.41.9Viscosity @ 104 F D445 Kinematic Viscosity cSt0.05Water & Sed, total D2709 Water & Sed by Centr Vol%

Notes:

1. The use of Biodiesel, including Fatty Acid Methyl Esters (FAME's), is strictly prohibited. The fuel may containantioxidants/sweeteners, corrosion inhibitors, and pour point depressants. Corrosion inhibitors may be required to meet the 1 mil/yr standard pipeline corrosion rate. All additives and their concentrations must be previously approved by the pipeline Quality ControlCoordinator, and must be clearly indicated on the Certificate of Analysis.

2. The diesel fuel shall be visually free of undissolved water, sediment, and suspended matter. (ASTM D975)

3. The derived cetane number (DSC) measured by these methods can be used for cetane measurement. D613 is the referee methodfor cetane.

4. Either the Cetane Index by 2-variables minimum or the Aromatics maximum must be met (see ASTM D975 Table 1 notes formethod version)

5. Where cetane number by Test Method D 613 is not available, Test Method D 4737 can be used as an approximation. (ASTMD975 Table 1 Notes)

6. Under United States regulations, if distillates are sold for tax exempt purposes then, at or beyond terminal storage tanks, they arerequired by 26 CFR Part 48 to contain the dye Solvent Red 164 at a concentration spectrally equivalent to 3.9 lb per thousand barrelsof the solid dye standard Solvent Red 26, or the tax must be collected. (ASTM D975 Table 1 Notes)

7. This fuel meets or exceeds all the requirements of ASTM D975 (Ultra Low Sulfur Grade No. 2-D S15 Diesel Fuel Oil) and ASTM D396 (Grade No. 2 Low Sulfur Fuel Oil), with the possible exception of the lubricity/conductivity requirements in ASTM D975.Additives or further blending may be utilized at downstream locations to meet these requirements.

8. ASTM Referee Methods for #2 Diesel Fuel, 15 ppm Sulfur, are as follows:Cloud Pt, ASTM D2500; Flash Point, ASTM D93; Sulfur, ASTM D5453; Distillation, D 86. (source ASTM D975)

9. ASTM Referee Methods for #2 Fuel Oil, 500 ppm Sulfur, are as follows:Density, ASTM D1298; Distillation, ASTM D86; Flash Point, ASTM D93; Pour Point, ASTM D97; Sulfur, ASTM D2622. (sourceASTM D396)

10. For this product, sulfur test instruments and methods used at each facility must be qualified by the current EPA approved method(see 40 CFR Part 80 for approved methods).

Page 28: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

VolatilityClassMonth(s)

RVPmax, psi

DriveIndexmax

50%min

50%max

90%max

End Ptmax

DistResid

max, %

Distillation Requirements, oF10%max

V/L TestTemp

min, oF

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:Various

P66 Code:

Volatility Schedule, Conventional, All Grades, All product that will be delivered to WA (not MT)

Jan E-5 15.0 1200 122 170 230 365 430 2105Feb E-5 15.0 1200 122 170 230 365 430 2105Mar E-5 15.0 1200 122 170 230 365 430 2105Apr D-4 13.5 1220 131 170 235 365 430 2116May A-3 9.0 1250 158 170 250 374 430 2124Jun A-2 9.0 1250 158 170 250 374 430 2133Jul A-2 9.0 1250 158 170 250 374 430 2133Aug A-2 9.0 1250 158 170 250 374 430 2133Sep 1 - 15 A-2 9.0 1250 158 170 250 374 430 2133Sep 16 - 30 C-3 11.5 1230 140 170 240 365 430 2124Oct D-4 13.5 1220 131 170 235 365 430 2116Nov E-5 15.0 1200 122 170 230 365 430 2105Dec E-5 15.0 1200 122 170 230 365 430 2105

Volatility dates listed are those required at terminals and thus may not be equivalent to the pipeline shipping schedule provided toshippers. The above Volatility Classes are standard as set forth by the Pipeline. Other Volatility Classes may be requested as well.

Values marked with an * indicate a more restrictive requirement than that defined by the underlying ASTM Volatility Class.

Product that may be shipped to Washington State may be ultimately sold as a clear gasoline or a gasoline/ethanol blend.Washington state regulations require clear, finished gasoline to meet the current version of ASTM D4814. For gasolines orsubgrades that are intended to be blended with ethanol to produce a finished gasoline-ethanol blend, state regulations allow eithermeeting the TV/L=20 specification on a clear or blended basis. If certifying on a clear basis, the applicable standards are asfollows:

(1) Class 1 shall be 60EC (140°F)(2) Class 2 shall be 56EC (133°F)(3) Class 3 shall be 51EC (124°F)(4) Class 4 shall be 47EC (116°F)(5) Class 5 shall be 41EC (105°F)

If certifying on a blended basis, the applicable standard is the most recent version of ASTM D4814.

Test Methods: (latest version unless otherwise indicated)Distillation: ASTM D86, corrected to 760 mm Hg;Driveability Index: ASTM D4814; The DI specification limits are applicable at the refinery or import facility as defined by 40CFR Part 80.2 and are not subject to correction for precision of the test method.V/L: ASTM D5188, or the estimate method using Appendix X2 of ASTM D4814;Vapor Pressure: ASTM D5191-01. For conventional gasoline that meets a summer RVP specification of 9.0 psi or less and which is intended for sale in the summer, EPA requires the use of the EPA equation and also requires that batch reporting of RVP be to 2decimal places (example; 8.97 psi).

Page 29: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

VolatilityClassMonth(s)

ClearRVP

max, psi

DriveIndexmax

50%min

50%max

90%max

End Ptmax

DistResid

max, %

Distillation Requirements, oF10%max

V/L TestTemp

min, oF

Yellowstone Pipeline

PipelineSpecifications

6/20/2014Revised:Various

P66 Code:

RVPmax, psi

Volatility Schedule, Conventional, All Sub-octane Grades, All product that may be delivered to MT (can also go to WA), all properties (except clear RVP) must be met on 10 vol% ethanol hand blend

Jan E-5 15.0* 1200 122 150 230 365 430 210216.0Feb E-5 15.0* 1200 122 150 230 365 430 210216.0Mar E-5 15.0* 1200 122 150 230 365 430 210216.0Apr D-4 13.5* 1220 131 150 235 365 430 210714.5May A-3 9.0* 1250 158 150 250 374 430 211610.0Jun A-2 9.0* 1250 158 150 250 374 430 212210.0Jul A-2 9.0* 1250 158 150 250 374 430 212210.0Aug A-2 9.0* 1250 158 150 250 374 430 212210.0Sep 1 - 15 A-2 9.0* 1250 158 150 250 374 430 212210.0Sep 16 - 30 C-3 11.5* 1230 140 150 240 365 430 211612.5Oct D-4 13.5* 1220 131 150 235 365 430 210714.5Nov E-5 15.0* 1200 122 150 230 365 430 210216.0Dec E-5 15.0* 1200 122 150 230 365 430 210216.0

Volatility dates listed are those required at terminals and thus may not be equivalent to the pipeline shipping schedule provided toshippers. The above Volatility Classes are standard as set forth by the Pipeline. Other Volatility Classes may be requested as well.

Limits marked with an * apply to the fuel without ethanol. Unmarked limits apply to the fuel with 10 vol% ethanol.

A 1.0 psi higher vapor pressure is allowed for conventional gasoline-ethanol blends that contain greater than 1 vol % ethanol, andthis allowance is reflected in the table. During the period of May 1 through September 15 this allowance only pertains to blendsthat contain between 9 and 10 vol % ethanol.

Test Methods: (latest version unless otherwise indicated)Distillation: ASTM D86, corrected to 760 mm Hg; Driveability Index: ASTM D4814;V/L: ASTM D5188, or the estimate method using Appendix X2 of ASTM D4814; Vapor Pressure: ASTM D5191-01. For conventional gasoline that meets a summer RVP specification of 9.0 psi or less and which is intended for sale in the summer, EPA requires the use of the EPA equation and also requires that batch reporting of RVP be to 2decimal places (example; 8.97 psi).

Page 30: Revised: 6/20/2014 Pipeline Specifications Yellowstone Pipeline · The Mercaptan Sulfur determination may be waived if the fuel is considered sweet by the Doctor Test described in

VolatilityClassMonth(s)

ClearRVP

max, psi

RVPmax, psi

DriveIndexmax

Clear50%min

50%max

90%max

End Ptmax

10%max

DistResid

max, %

Distillation Requirements, oFV/L Test

Tempmin, oF

50%min

Volatility Schedule, Conventional, All Full Octane Grades, All product that may be delivered to MT (can also go to WA)

VariousP66 Code:6/20/2014Revised:

Yellowstone Pipeline

PipelineSpecifications

Jan E-5 15.0* 16.0 1200 122 170* 230 365 430 2102 150Feb E-5 15.0* 16.0 1200 122 170* 230 365 430 2102 150Mar E-5 15.0* 16.0 1200 122 170* 230 365 430 2102 150Apr D-4 13.5* 14.5 1220 131 170* 235 365 430 2107 150May A-3 9.0* 10.0 1250 158 170* 250 374 430 2116 150Jun A-2 9.0* 10.0 1250 158 170* 250 374 430 2122 150Jul A-2 9.0* 10.0 1250 158 170* 250 374 430 2122 150Aug A-2 9.0* 10.0 1250 158 170* 250 374 430 2122 150Sep 1 - 15 A-2 9.0* 10.0 1250 158 170* 250 374 430 2122 150Sep 16 - 30 C-3 11.5* 12.5 1230 140 170* 240 365 430 2116 150Oct D-4 13.5* 14.5 1220 131 170* 235 365 430 2107 150Nov E-5 15.0* 16.0 1200 122 170* 230 365 430 2102 150Dec E-5 15.0* 16.0 1200 122 170* 230 365 430 2102 150

Volatility dates listed are those required at terminals and thus may not be equivalent to the pipeline shipping schedule provided toshippers. The above Volatility Classes are standard as set forth by the Pipeline. Other Volatility Classes may be requested as well.

Limits marked with an * apply to the fuel without ethanol. Unmarked limits apply to the fuel with 10 vol% ethanol.

A 1.0 psi higher vapor pressure is allowed for conventional gasoline-ethanol blends that contain greater than 1 vol % ethanol, andthis allowance is reflected in the table. During the period of May 1 through September 15 this allowance only pertains to blendsthat contain between 9 and 10 vol % ethanol.

Test Methods: (latest version unless otherwise indicated)Distillation: ASTM D86, corrected to 760 mm Hg; Driveability Index: ASTM D4814;V/L: ASTM D5188, or the estimate method using Appendix X2 of ASTM D4814;Vapor Pressure: ASTM D5191-01. For conventional gasoline that meets a summer RVP specification of 9.0 psi or less and which is intended for sale in the summer, EPA requires the use of the EPA equation and also requires that batch reporting of RVP be to 2decimal places (example; 8.97 psi).