Code No.: V-014 / RAPPORT D'ANALYSE DES MATIERES PREMIERES

Spec. approuvees par l'Assurance Qualite 2015-11-27

NOM DU PRODUIT: Vitamin E Acetate 500 IU/g (50%) *

NO. DE RECEPTION: R-35314@ /

DSMDISTRIBUTE UR:

;l\1.ANUF ACTURIER:DSM Nutritional Products, Inc.

LOT DU DISTRIBUTEUR:

DATE D'EXPIRATION: 2020-06-12

DATE DE RE-ANALYSE: NIA

DESCRIPTION

COULEUR:

FORME:

SPECIFICATION

Blanc a blanc beige

Poudre Iegere

ANALYSE METHODE

IDENTIFICATION:

ESSAI: (Acetate de dl-tocopheryle)

PERTE DE POIDS: (105°C)

SOP.MP.068

SOP.MP.068

Calcul

USP <891>

SOLVANTS RESIDUELS: . USP <467>

REVISE PAR: IIAJ/1111 l( J , IDATE:

COMMENTAIRE:l@Produit certifie -; /£ Analyse par Laboval t Se refere au certificat du manufacturier f Se referer a la lettre de confirmation

NO. DE LOT DU MAN.:

PAYS DU MANUFACTURIER: USA / /QUANTITE RE<;UE: 70 x 50 kg

* DL Alpha Tocophe,yl Acetate 500 U1/g

SPECIFICATION

Conforme

480.0 - 600.0 U1/g

Resultat X 1

:;6,0%

Rencontre Jes normes

OBSERVATION

Conforme£ /

Conforme£ /

RESULTAT

Conforme£ /

530 U1/g t ✓

1530 /

Entrer le resultat ci-dessus dans Visual Manufacturing

2 %t I

Conforme f ,/

J-ol::f -11-10 REJETE D Os-

/ APPROUVE [kl �{AtJ PAR:

Controle Qualite DATE: oJ.0/1-/1-l O RELACIIEPAR� Qr

Assurance Qualite RESULTATSENTRESPAR: NES DATE: 2017-11-09 DATE: J-�/.1--/ 1-10

Client:

Att:

Fax:

Produit:

Code:

Vrtamine E Acetate 500 IU/g (50%)

V-014 /

Tests

Description

Couleur

Fonne

Identification

DL-cx-tocopheryl acetate (Vilamine E)

Verifie par.

1688, 50e Avenue Lachine (Quebec} Canada H8T 2VS

Specifications

Blanc a blanc beige

Poudre legere

Conforme

Certificat d'analyses

Approuve par:

�-· .. - .

www.laboval.com

Resultats

Conforme ./

Conforme /

Conforme /

Date;

CA:

·PO:

·Req:

Lot:

Page:

2017-11-08

1/1

Methodes

Organoleptique

Organoleptique

MP.068.03

· {)ec # lt/ ?I) 3/

At--S2017 -1'1- 0 9

Tel.: 514-633-6826 1-800-561-2778

Telec.: 514-633-9679

DRY VITAMIN E ACETATE 50% TYPE SD

Certifjcate for Customer

Productcode : Lot No. : Analysis No. :

CfC Number: Articlecode : Sales Name:

0488550/

0488550395

Manufacturing Date: 13-JUN-2017 Best Use Before Date: 12-JUN-2020 ✓

Delivery Note No. Destination : Canada Customer Ref. No : Customer Article No: Customer Name:

Comment

V014

Quantity Shipped: 3500.000KG

Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at 1-800-526-0189Our webshop provides 24/7 access to the products and services of DSMNutritional Products. Visit our website at:http:/ /unlimitednutrition-na.dsm.com

DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ 07054-1298 U.S.A

Date of issue: 16-0ct-2017

DRY VITAMIN E ACETATE 50°/o TYPE SD

CERT/FICA TE OF ANALYSIS

Productcode : 0488550

Lot No.

Analysis No.

Test Result Limits/

Specifications

Dimension

/ Units

APPEARANCE

Visual

COLOR

free flowing powder free flowing powder

Visual

LOSS ON DRYING

Oven

SODIUM BENZOATE

TLC

SORBIC ACID

TLC

ASSAY: DL-ALPHA TOCOPHERYL

ACETATE

LC

MICROBIOLOGICAL PURITY (USP)

Total Aerobic Bacteria

Yeasts and Molds

Enterobacteria

Escherichia coli

Salmonella sp

Staphylococcus aureus

Pseudomonas aeruginosa

') checked at regular inteNals

white to off-white

2 /

corresponds'

corresponds*

53

<10

<10

/

less than 10

negative

negative

negative

negative

white to off-white

max. 6 %

present

present

min. 50 %

max. 1000 cfu/g

max. 100 cfu/g

less than 10 cfu/g

negative /10g

negative /259

negative /10g

negative /10g

This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above. The product meets all requirements of the following valid compendia when tested accordingly:

USP and Ph.Eur.

The Quality Assurance Manager

Joan Ji

DSM Nutritional Products 253 Macks Island Drive Belvidere New Jersey 07823 U.S.A

1 I 1 Date of Issue: 05-Jul-2017

Document Control Unique ID

· 1 11111111111111�11111 11111111111111111111111RAPPORT D'ANALYSE DES MATIERES PREMIERES Code No.: V-014

0108449

Spec. approuvees par l'Assurance Qualite 2015-11-27

NOM DU PRODUIT: Vitamin E Acetate 500 IU/g (50%) *

NO. DE MCEPTION:

DISTRIBUTE UR: ..;MANlJFACTURIER:

DSM Nutritional Products, Inc. DSM

NO. DE LOT DU MAN.:

PAYS DU MANUFACTURIER: USA LOT DU DISTRIBUTEUR:

DATE D'EXPIRATION: 2020-06-14

DATE DEM-ANALYSE: NIA QUANTITE RE<;UE: 35 x 50 kg .1

DESCRIPTION

COULEUR:

FORME:

ANALYSE

SPECIFICATION

Blanc a blanc beige

Poudre legere

METHODE

* DL Alpha Tocophetyl Acetate 500 UI/g

SPECIFICATION

OBSERVATION

Blanc beige ,,

Poudre legere /

MSULTAT

IDENTIFICATION: SOP.MP.068

SOP.MP.068

Conforme Conforme£ /

ESSAI: 480.0 - 600.0 UI/g 530 UI/g t "'(Acetate de dl-tocopheryle)

PERTE DE POIDS: (105°C)

SOLVANTS MSIDUELS:

Calcul

USP <891>

USP <467>

Resultat X 1

:,;; 6.0%

Rencontre !es normes

1530 /

Entrer le resultat ci-dessus dans Visual Manufacturing

2%t /

Conforme f .✓

I-R _E_V _IS_E _P _AR_:

-J.:.J...:..t!:U:w...,_-=.:.��--____,J...;_D _A _TE_:___;_2...;_0_17_-_·1_'1.----=-1 ...;_5_--IREJETE D

COMMENT AI @ Produit certifie ,, APPROUVE [LI . {j , ;

II J'n ,, l't •I /J '({,/a/J: VW'I £ Analyse par Laboval / PAR

J t Se refere au certificat du manufacturier / U-MtU4't:' �,r f Se referer a la lettre de confirmation _,, Controle Qualite

RESUL TAT S ENTRES PAR: NES

I

DATE: 2017-12-14

DATE: 2017 -12- i J

RE LA CHE P j�;ta,_;,, c},,NJ9f!

Assurance QualiteDATE: ,,.. '""'""- ,, �.. ,, ....

LUii -•c I J

DRY VITAMIN E ACETATE 50% TYPE SD

Certificate for Customer

Productcode : Lot No. : Analysis No. :

L..'

CfC Number : Articlecode :

0488550 ,IJ

Sales Name : Manufacturing Date : 15-JUN-2017 Best Use Before Date : 14-JUN-2020 -:,,Delivery Note No. Destination : Canada Customer Ref. No : 102799 Customer Article No: V014 ,1

Customer Name:

Comment Quantity Shipped: 1750.000KG

Thank you for your order and continued business. DSM Nutritional Products is committed to delivering superior quality products and excellent services for our valued customers. If you have any questions, please contact our Account Service Center at 1-800-526-0189 Our webshop provides 24/7 access to the products and services of DSM Nutritional Products. Visit our website at: http:/ /unlimitednutrition-na.dsm.com

DSM Nutritional Products, Inc. 45 Waterview Boulevard Parsippany, NJ 07054-1298 U.S.A

Date of issue: 07-Nov-2017

DRY VITAMIN E ACETATE 50% TYPE SD

CERTIFICATE OF ANALYSIS

Productcode : 0488550

Lot No.

Analysis No.

Test Result Limits/

Specifications

Dimension . / Units

APPEARANCE

Visual free flowing powder free flowing powder

COLOR

Visual

LOSS ON DRYING

Oven

SODIUM BENZOATE

TLC

SORBIC ACID

TLC

ASSAY: DL-ALPHA TOCOPHERYL

ACETATE

LC

MICROBIOLOGICAL PURITY (USP)

Total Aerobic Bacteria

Yeasts and Molds

Enterobacteria

Escherichia coli

Salmonella sp

Staphylococcus aureus

Pseudomonas aeruginosa

*) checked at regular intervals

white to off-white

2 /

corresponds*

corresponds*

53

<10

<10

✓

less than 10

negative

negative

negative

negative

white to off-white

max.6 %

present

present

min. 50 %

max. 1000 cfu/g

max. 100 cfu/g

less than 10 cfu/g

negative /1 0g

negative /25g

negative /10g

negative /10g

This lot was analysed and released by our authorized Quality Control Department and was found to meet the specifications as given above.

The product meets all requirements of the following valid compendia when tested accordingly:

USP and Ph.Eur.

The Quality Assurance Manager

Joan Ji

DSM Nutritional Products

253 Macks Island Drive Belvidere New Jersey 07823 U.S.A

1 / 1 Date of issue: 10-Jul-2017