>

' »\ 1—'—' -* VP "^•*EcioN sire NUMBER /to &• «»<^S RPA POTENTiAL HAZARDOUS WASTE SITE . - •d H«UWDrr^ SITE INSPECTION REPORT , ° A R 1 1 6GENERAL INSTRUCTIONS: Ccmpl'.te Sections I and til through XV ol this torn as completely •* poacible. Thrift use the iafonn«-*ioo pn this form Tr develop a Tentai've OupoaittCfi ('Section 70. File this form in it* entirety in the ri ior,»l Kaz^rdoua Waste LO(File. Be awe to wciade all apptOpnale Supplemental Reports in the hie. Subaul a copy of the ^onns to; U.S. £-.:t0iim<nl»l Pro-tection Agency; Site Traclung System, Haiardoux Waste Enforcement Tack Force (EN-33S,). 401 M St.. SW. Waahir^on, DC 20460.

I. SITE IDENTIFICATIONA. SITE MAME -• &. sT«eeT«>ro*ha/f<faor<fi<^ y /1 U Mil 6s WiSSt 6^ Rt. 2

INDUSTRIAL WASTE CONTROL. INC. ^ ^les South of Fort Smith. ARC. CtTY " r" 6.'5T*Te ' E. ZIP ("006 •

Fort Smith AR 72901G. SI'T'E OPERATOR INFORMATION' . MAUE

drady Shipleyi. S¥Re£T 4. C*TY " " "'*"

2900 Wheeler Ave. Fort SmithH. REALTY 0'HHS.R lM»'dRMATION fit rif/J«f6ii( /rtfal epfiaiaf O/ *;»»J ' . . . . . ..........

t .MAME Approximately 1 /4 to 1/2 of the landfill site Is ownedGrady Shipley above. The remainder Is managed by h'arie Birdfan PL-dark ^ee-VlU-U)- — — ^ ^ - . — ^ - . ^ . ^s. S'TV •^ 'R1;. 2 Box 372 Fort Smith . .i. sue oescR'PT'oMAbandoned Industrial and Solid Waste Landfill. See Attachment A for further discussi

t. TYPE 0' awHEftSH'P

"3 I. FEC£*»AL • ] »- STA-K " 3-COUHTY Q *. MUNICIPAL £)3• f*BIVXTE

n. TCMTATIve DISPOSITION feomplflf this section last)X. QTIMATB OATg OF T Z M T A T - V K t 8. APPAflfiHT SERIOUSNXSS OF t»«08l,aM

(aSPOHTiON <^»^o*,rf<y. A t ..i -w —^v t—i i»—- 3; i. MtQH ^3». ueoiuu ^ i. i.ow ^ i. HWSC- PB£PA»£»*N|XniyAT4CK/ r -Y- ^ i i, , ,

'- —— G^ fery^^ l ————— ———y (214)742-4521

HI. INSPECTION INFORMATIONA. ISJCHNClPti. INSPtiCTOft :HFOW«ATl01- . SAME | 1. TITLI

Oave Anderson Chemist) ;«<3tMl;*'"'OM "" 'T 1 «.Tt L C^^ON in O.fSTI* COrf* & fKI*;

Ecology and Environment. Inc., 1509 Ham St.. Dallas, n 752l(l1 (214)742-4521B. 'BtSPCCTlON PABTIC'-AHTS

'. N>U« 2. OfttiANHATION

Gordon Duncan

Larry LandrySandra Kuklishpene Me Dona Id

C. r"e SSPftESRNTATlVtS IN-EflViafEO fc<MdOfa« alltCHll. wnkw, f>*td*nitJ

1 . »t«Mf

grady Shipley

Perry A. Henson

Robert Cloar

Jim Ed Newrnani

^ »

Ecology and Environment. Inc.n n «>

n 11 "n 11 n

1. Tl»h.»» TKLEPMONI MO.

Site Owner(50])782-8225AdjAcent PrO^rty Own6(501)783-7666Perry Henson's Lawyer(501)783-1186Resident North of SitePhone Number Not Avail i

1.AOOAKJ l '

.2900 Wheeler AvenueFort Smith. AR 72901t:T514•"Hend^cks """' —————yFort Smith. M 72901West Court Plaza 61dg.Fort Smith. AR 72901"r"1 ftt. 2 Box 370" •ble Fort Smith, AR 72901

•

OCCLTC13

P. c6uKfV^*UeSebastian

2. T£l.ePMOMS *4UUMER

(501)782-8225••STATE"" ^T"l'P-e'OOE~" ""'

AR | 72901)V'•/2. TlI.ePMOMC »<U"BCI»

(5011996-45904. tT.t'-e r?. zn" cooe

AR 1 72901

i. o » T c faio.. title, & /'•J4/1/81

i. rci-eBMOMt no.

(214)742-4521n

n11

n

000246

IH. INSPECTION INFORMATION (continued)0. fiEHCHATOn IHfORMATtON Source of ««»«J

1.H&UC

Various Generators

E. TaANSf*0'*TEfl/WAUl,eR INFORMATION

1.N*Mt

Industrial WasteContro1,,.«Inc., „,..„.-Whirl pool Corp.

Various Transpo»teis NAV. if »A1TE IS ?"Oce»3CO OH IIT» ANO ALSO tHt^PID TO OTMtIt SITES. tOtHTI»Y Orr-iift rACIUTtCS USCO OCR DISPOSAL.

1 - X A M X

N/A

<3. BATE or ihiPKCTlOMw"'.^*^ 3/24/81

J. KKATMCK :tf»«m«J " ' ""

Approx. 70°F-SunnyIV. SAMPLING IHPOftHAflON

A. y«rit 'X' t6i (h« <yp»* 9l it«pl«<& •k«n iad Indltiif wh<r« ih«y h««« b««n ••at «<c» n<ion*l icb, other EpA lib, coovcioc,•1C. •nd Jttlffliir wh«n (h« r««alli witt b« ivkllibl*.

i.i*u»bC ry»<

1. 4HOUHOWATCH

b.lUK^ACC MkTC«

a. ***Tl

d. AIM j

«. nuHOsf

^ »*•*».»,

1. <6<b

h. rf»»tT»TH»N

i. <»TMti*f^>"'i'fw Sopn '™SeepSed1ment

8. riCLC MtAlUHCMSMTt TAtttH f«.J., »dJadanv"r> •ipf«Jimy, PW. «n.J

*.»vi*c

N/A

i i- 1

1. rcl.tOMont no,

• • - - -

i. TIl.tPMOHS ^O.• 'uur' •of Business

(501)646-3421

1. TiLfHOHt UO.

M. +iM'B of iNSPccnoH1:30 pm

l.tJIUPUt

TAKKM^"k-.tl

X (1 )

X ( 1 )x (ul.«044?IOM Or MKAlunCMCNYl

i— .«>T»T^ «. ...,.Ji., Lii . .ii . .i.B . - i,..»i .|I[.II ..IT. ^M..iim...,l>..~.l-in --- . ,.1-1 r,rf-^T». .i.-»——«'«^-"r-r

i

I.IAM^LK

S^a^^SA Acurex Cor. v . » 405 Clyde Ave.,Inorganlcs: Versai*,SDrlftqfieTd, VA z2t5

Houston EPA lab

1.AOONCSI

See attached Us(Partial Ust Attachment H)

).koon&u'"P/O.' Box '688 1 '

Fort Smith. AR500 Jenny Lind BFort Smith. ARSee Attachment Eoartlal list

1. ACeKSJ OAINCD SY (w

C3 1. PKRMIMIOH

t of generators

Ivd.

-This is only a

i. voofteit

tf«n(J«Jl Stun k« |A«mi in *JJ 9muif

Q2.irAflMA»T(See Section VIII U)

IIMT fOt

p., Energy & Envlronmen-Mountalnvlew. CA 94042Inc. 6621 Electronics Dr..i - Houston PA Lab

i.RKSULTX

4.A*are rvac <»6»<c»«*Teo

See Attachment H

4.MAJTE TYPI T HAHJPOf* TID

Scrap WoodProducts

Solvents

Various Wastes

<.OAT»iffUl.TI

AVAH.AB^.Jr

tal

...

••

e PA i'o'at rsayM na-Mi

000247

Continued f-'roal Paife 2

IV. SAMPLING INFORMATION (continued)c.

1

D.

E.i

V. SITE INFORMATIONA.

IT

(

0

q

~Q~'

C. ARE* OF SITE r'n <£?<»}

Greater than 20

VI. CHASACTEftlZATtON OF SITE ACTIVITYIndicate the major site activltyfiasJ end details felaUng to each activity by marking 'X1 id the appropriata boxes.X

I

I

CwchPE

^

^

A. WASTE TYPE

;"?[; 1 . UOU13 (3] 2- 30L10 CS 3- SLUOC.E Q «. 6AS

9. WASTS GM*«*CTeftl5TlCS

^3 1. CORROSlVit QQ fc tONtTAOtE Q }. HAOlOACTIVe E^ 4. HIGHt.V VOLAT11.B ..... .. ,„ , ..,. ...... .

^ 5. TOSttC 'OB.REACTIV& F^ f. 1HERT g3 B. FLAMMABLE ,- 5 - — - - i

' 1 9- OTMEB/Wtt/fJ--C. WASTE CATEOOR16S

1. Ar« recuidi 6i' wff 4vjt«bl*7 Spe

No. Only records of cu

PHOTOS

TYPE O*-' PMOtOS

' X "• e"o*J>40 r^ b- *&" *i-SITE •-^PPEC'

[3 Yes- SPeClFV LOCATION OF M/

COORDINATES. t..* TI TUOE/d<(.-3H".-aec.J

35°15'27" N

SITE STATUS

'" t. ACTIVE rThaso inductiial onunicipal sites which are 6«lntf useor >tfdJ(« t/eOtBierf, Jforad^i Of <J(in « contlrtuina f>a*i«, «v«rl If infrauertfIf.J

*S G£N£PATOH OM S'TE*

L 1 - N0 ~~! 2- vesrspcetir

A. rRANSPOftTeH

f .a AIL.

2. SHIP*

3.9&RQ6.

4. T(*U=K

8, oioei.inea-oTHeBftpacf^;

ndustnal Wasteontrol d^d transportaste wood products;hem-leal wastes wereaule^ by other tranorters.

SUPPLeMENTAL ftEPORTS: 'f tfn* <tr ftllt •'tthin anyttf th< c«t*gorta« Illfd baluw, 9i«>pl«mantal R cporfJUJtt h< P"")?1*1^!,1"1'1^6"?.,whieli Suppl«manwl Reports you have filled out and attiehdd to (hi* for., 1 hererOtc 'Cnc SUpP

— ^- y-, —, siiBpA^p ,—, mental form could3 t. STORAS6 ^ 2. INCINERATION ^ 3. LAHOPll.l. 0 4. I ^MEHT Cr e^'O^'et^.

D <• P^^'f^SATMeNT C] 7- LAHOFAfly D a. OPeN DUMP Q a- TRAMSPORTSB 0 l0• BEGYCl.OR/ftECLAlU£R

VS. WASTE RELATED INFORMATION

rd

poasi

X'

,-

y

B.STOBEa

1

i.SUnFAce IMPOUNDMENT

3.0HUMS

4. T A N K . A B O V E

a. r&hiK. a6LO"

a

ps >ee Attachments

3C 2- 'NACTI\•ire* which nowm,.)

[antfftor'l /our*d

0. ARE THe?

"J i. KO

PILE

.OTHEftCtpBc^y

cify I(«(D« Jucti •

stoppers.

4, PHONOS 'N G^HTQQV Or; , . -

EPA Region VI (See Attachments)

/E '•Tfio»clonger roc«Jv«

tijit .'SIC Coda;-

E BUILDINGS ON THE SITE* '

!""} 2- YESC*p*c<fW;

fiROUNO

anouNo;

• iaami*«f, lnw<iit«n • •, «(«. b*lo«.

2. LON6lTUGe ('d»a--'"i".-«<;*J

9402^104H W

1

X'

9.0THKR(spfelly):

) 3. OTHeRf»fl»«;"yJ.-rh<i«« «J(ai (hat fncfud« Auch JneJdftnf f«e« "ni<dn»^fit Aa«pind"

Krhara 10 tesulat or condnuinrf uJa of lha •iia far •*•••(• dIspOsMiias occutr»di)

C.TBEATER

I. FILTRATION

2. INCINERATION

a. VOLUMC ReoucTiON^.ntCVCL'NK./RtCOVERY

a. GHeM./pMva./TnBATMeNT8.BIOLOGICAL TnEATMSNr

•• .WASTE CIt. F>£PROCE33'NS

••SOLVC"T RSCOVERY

X'

X

X

yc

r

D. DISPOSER

1 . LANOPILL

2-LANDFARM

3.0PEM DUMP

4.3UHPACC IMPOUNDMENT

S. ,"'ieHT OUMPfNS

«. ;r. L.NCH*TtON

7.UNOERQi'tOUNO INJECTION

i.oTMERC*p«c«.-y; surfatmpoundment supplemef-eport win not be 1 r:1uded because directiccess to the site wa•iftt-.nainf^ f^pe iM-tac

1e-nof

-EPA fwm T20?0-3 00-/91 PAGE 3 OF '0

000248

Vn. WASTE RELATED IMFOffMA^IOM /-com.nuerf,2..£»ttm*«et*'e anaount •'apoct/y urnf a/ .Measure; of wiif by c-itegory. maoc 'X' to indicia »hieh w»fa ar« or«s«rti.

». SLUCfleAMOUNT

UnknownUMIT 3^ UE&I'U'<£

-d, ————-.Vl c"<S"E*<''l

J ueT*(.aA * SL^icaea

i: BO'*

JkLnJMIKJLfU'"SLUOOC

^JuiOtHCafa^rci/J'l

C. LIST SUBSTANCES 0*' S^eATEST CONCSON BMICH ABC OM TMK SITE '(H*c< trt d«i««rtd<»« <if<^ af Aae^d)

t-suasiAMce

Lead Chromate

Lead Molydbate

PhenolUs (NOS)

Toluene

Trichloroethylene

Methyl Ethyl Ketone

Oily Wastes-

VIII. HAZARD DESCRIPTION

Pie-S EVALUATION HAZARD OesCRl^TiON. PIK» 911 •X' in (lie box lo mdtCaf th<l :he luced hjtfd <iu»l». Daacnba itrfiaxard ;n (he &o«ce pmcideii. "

A. MUMAM KeALTM MAZAffOS ' ° ' -r. f - ' - ;

i

1 , . , ....... . , - , . ....... ..^....... ... .. .. ... ........ .... - . . - - . . - .

b. O'L 1

AMOUHT

UnknownuUtT Or ufAlkJKie

I-,,. 0'^ llt'rr""'-" or»i or"e«n'<p<ei(yi-

L i.roftMf««r» -.?•;

.*0;L'O

e. SOt /ENTSAMOUNT

UnRnowniJWT 0^ >'<C*X«JAE

)(

Hi 0 nEa''tp*el;yl

,, M*L.O<i£"<*TE3>oi /e«<Ti

MON-MAt.OSMrQ.• iOL^tMTl

b.LIQ.

xxxxxxx

C.VA.BOW

1. TOXIC-TV{muls •X')

1.MUtH

X

x

d. CueMICALS*MOU**r AMOUHT ^ *MOu1* t

Unknown Unknowii I NoneWIT 0» MCkJUHe

X -

,,. *»'C<L,>MO- (.'OUORI

H*<AU3TIC»

tS 'OV tS / lUKS

—r-----—1-" ••"••"—i(t<'f*M<oe

xr•— i.i-y InOiuXTALl

^mi 0»"<it/*ptci/yJ

b.MtO.

X

l i. •C 'OS

m i»€S-'cioes

Ht re •

* BMtMOt.t

'MAI.OOEH3

e. d.LOW NOMt

X

xxx

4-CASHUMeCR

7758-97-6

10190-55-3

None

108-88-3

79-01-6

78-93-3

None

•, sores

UNIT 0^ ueAlUMC i'J^'* 0»' MEAau»te1

« ,-xl^- llPB. '**H ^——i'

»

' i lASBCl^Of

uii* >,iiu a/MiffC31 T»11.1MS1

»e«ft0ul i^Et-r^• tue wA»re» (

r -. ——- i •• l -^-.. „———t

NO**-PHI*»OU«• iMI. .'G. WA<TEI

ai OT^tH/*p»ci(y;:

Waste Wood

S.AMO

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

Unknown

/ .OTMea

———T

-, -• ao«* •roB"°-<Ai9MA£EJ*-

'21 HOSO'TA^.

(iiitAOio*cr'v<

t«>MUNIC>PAk.

isnaTMeHC*p*«/7>.

UNT i.UNIT

000249

<_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ V r n . HAZARD PESCRIPTIph[^continued)0 B. MO»-»OR<ER INJUftV/EXPOSURe

- „ ._ '~'-1^"——~ - ~ " l r-' -' ~ " - -^ ^————•—————=—'•- " -——"--— "l. BUS——-^——f.———•r - f. . . i.——..» - .-i .,«———————— - —r- -^-^,——_._^.——____^_^____- .. __._^_^_______ ___.[3] 0. COMYAMtMATlOM OF ItATKft SUPPLY

A water well currently In use just slightly updip of the landfill was sampled (seephoto ^N). Results of analyses should determine if water supply contaminationis occuring updip.

V] E. CONTAMmATIOH Of F600 CHAIN

Mr. Henson alleged that a surface impoundment overflow in 1 9 7 7 killed cattle on hisproperty when they ate contaminated grass. This was never verified by state officials

L^ f. CONTAMIMATlOM OF 5AOUNO BtATeB

See V I I I D

QC a. CONTAMINATION OP SURFACE »*T£R '7rJ^?'\ ~UJ~~l""'' ' -'-^^^ •'''^

No surface runoff diversion structures are utilized, (See pa no ran. ''photos). Runofffrom the site could be contaminated. Results of future sampling \ il determine the ,extent of contamination-

€Wf

^

V^J im-7»i —— —~ ,

SiBSSSSBSSSSSSS^

**eeT'£^" t "

K»«<»

000250

000251

VQl. HAZARD PgSCRIPTIOM (contmwd) _H. FIRS 9» EXPLOSION

"^ 0. SPtLLi L E A K I N G CONTAIN£RS/RUNOFF/STANOIN(* LIQUlO

Seep running off property (see photos 4 & 5 and attachment B)

• P. SEWER. STORM DRAIN PROBI.EMS

'J| 0. eitOSION PROBLEMS

Some evidence of erosion (drainage pattern being formed) noted during inspection,(See photos ^ 1 , f f 2 . and §3)

jf, R. iMAceouAra secuaiTvFenced only on North side of property

"~\ %. IHCOMPAnaLB »*STBS

000252

Possible due to inadequateaccess to the

J( J. OTMCCT 'ipvcHyi ~ "a~ •"- "

Or. the advice of his lawyer, Grady Shipley. (owner and operator of this inlandfill) denied permission for the FIT representatives to enter the site

{ Shipley is currently involved in litigation with Perry A. Henson, owner of[ immediately North of the landfill.) Subsequently, much of the information

tained in this report was obtained from Mr. Henson's attorney, Robert Cloa

After the FIT representatives returned to Dallas it was learned that a Mrsleased a portion of property to Grady Shipley for added capacity to his landfill.(Mrs. Clark is now incompetent to manage the property so thistransferred toto Mr. Henson and Robert Cloar, that the solid waste (mainly wood waste) portion ofthe landfill was developed.

i fill area belongs to Mrs. Clark.i"

*A.k.OCATIOM OP POPULATION

• *»< CaSlOENf 'Ak. *ai

,'».;, *-.• e n e - t -1 .31 - .^ , .1-<1A- •JICJO

•

"n ^t^i.lCLV1 ' •'•^A.tk.L.ID AHCAJ

I"' - — — " — — — — — — — — — — —' , •'•JSt.-C «-»t • 1 X A J

•fUtln. ich^ati. ute.i

X. WATER AND HYOROLOGtCAL &ATA

Approx. 2 feet1

S. fOTEMriAL y'CLO OP

Low to Moderate0. TYttg Qf? Of*lNKIN<l WATgR SUPPLY ' ' ' '"" '"——--——- - — — " • " • — — " 1 1 ' 1 — — 1 " 1 — — ' '• •"

' I yOH-CCMMUNITY

)C" i- Sl-"ACE flATKR

SPA fu« T207&.3 (lfl-7?)

• - - - - ^ L - H A Z A f t D OE5CRIPT.OH ^^-nusd,

landfill.)

her daughter, Marie Byrd (see I.H.I,) It

IX. POPULATION &1RECTLY APFECTEO flY SITS

1.1

J»WW<"y ffl<Ujorthern.x...,,Boundaryl^PP1

AOUtfEB

rt a. cawMuMiTv f.fl.c.fy w^, Fort Smi th

^ <• ilfELl.

PAGE 9 3F i0 Confifiuc On Page •I

8. APRROX.NO.OF P60PI.E APtEC-EO

security (See Attachment E regarding uncontrolled

It is not yet clear, however, which part of the land-

1 5

0

100

0

A. 3eo^*« TO S l l Q U H Q W A . — — " • — — — — " — — — — " - - - - . -•. OIMKGTION or/y.aw -—-»Nortn.°x.10feet %telC- OHI'AMGS TO CHINKING «A»tB SUPPLY

'•pKt/y unit •f «•««<«•> , ... ..,,1 5 Hn^s

G.Appaox. N(S. o» PEOAPfgCTEa »lTMtM

UNIT A R C A

1 5

0

100

0

was

PL2 S. APPffOX.MO.1 OF 3U11.21HG3

*Fec<:Tgs

5

C. <iiROUHD'«A-St!| JS'S"** ^

Residential». efee^iON +3 aqiKitiNQ »»rsR suP^t*1'North

responsibility has beenin this area*

1

0

0

active. (Mr.propertycon-

r.

.dark

according

e.e's-ANccTO 31-e-io<e.*y unt'i

1/4 mile

1 /4 mile

| 1^ mn^

1 / 4 mne;t£'mTY

000253

Continued From Ftont

XTV. PERMIT INFORMATIONList ill applies, ^erants held by the sitfr and provide the related iniofmaUon.

A. PERM!* TVPE^f'S..RCRA.Siaft^,vf'OES. *tc.)

Solid Waste

Note: The original permit (#n6295) was filed under the (lame of Jame{S H. mi-is,On 10/7/76 the pe

..then became Indu$regulations.

XV. PAST REGULATORY OR ENFORCEMENT ACTIONSy HONE ^J VES '••ucinKfttt irt ihn ipvef)

Several letters were sent to Mr. Shipley from the District Inspector of the ArkansasSolid Waste Control Division demanding Immediate attention be given to problemareas on the site. No enforcemert actions were ever taken.

*

MOTE- Based on the information in Sections III tnon the fitst page of this form.

8. laSU'lGAGENCY

AR Dept. OF original hermit [Pol'1 In. Control #16295 Unknown Unknown& Ecol.

•mi't was ret.rial Waste

C. PCBtillTNUMaen

Later changedto ?S-005?

ssuedContro

aiS-0052),under the n ime of GNJ, (Inc.,^ Inc. The site was]closed according

ough XV, fill out the Tentative Disposition (Section f!) infonnation

a.OAreissueo

(m»:d*y.&rr.j

10/7/76

e. ExfaATioNO*TE

iavo..d*y,^yt-)

Unknown

r. m COMPLIAKGC'amit 'X'S

' | i 1 1 usi-vea I MO 'xna*N

xx

•--r' "t"1

whichto Artansas

r-0t^00<-s

6PA Pa*". 13(174.1 (lO-Ml PAGE 1 0 QP 10

000254

^Continued Ftam. Pags S

X. W A T E R AND H Y D R O L O G I C A L DATA Ccopiinuad)n.

ti W E L L , a oePTM

; ' ipaci/f unir)

Owner iArt ie SmHh 10 FeetRt, 2 Box :Ft. Smith.72916.(^oDgss-e-

».P

aS1

XI- SOIL A N D VEGITATION DATALOCATION OF &<re is iny^] A. K H O W N F A U L T ZONE [ ] B. K A R S T ZONE 3C c- 100 ^AR FLOOD P L A I N ' J 0. W E T L A N D

""" e. A R E G U L A T E D F I O O O » A Y ^ p. CRITICAL " A B I T A T '"I G. R E C H A R G E ZONE OR SOLE souace A O U I F E "

Mark 'X' to indicate the type(s) of gecildgtcal fflatenal obaecved and specify where necessary, the component parts.•X

it-

xx

Xffi. SOIL PERMEABILITYLow to moderate permeabili t ies depending upon locatk. j A. Uh-KNOtht 0 B. V6RY H16H H9S.OOO to JOtfO cffl^Mfc~^y. 0. MOOESATE f f f l to .1 cta »ec.J •X3 E. LO'K r-J to .001 col/sue.)

-. O'SGHARGE *.REA

^ 1. VES ^J( I. MO 3. COMMENTS

i.

"j. 3TH&R OEO^OGICAL OATA.

See Attachments A and G for additional geologic In^

LIST A L L C° M K I N 3 ¥(AT£f l WELLS W*THIN Jl I/ ( MILE OfiOtUS OF SITE

RECEIVING W A T E R

^AMCralrie Creek

so'e^'ipv'TTaE rSo cLTss'^^'*'*'ui table for desirableKe. Secondary conta

»}(.A. CVeR8»'»DEN —

"

t . 3 A N O

1 C L A Y

»- Q R A V E t ,

Q &Cf LJ A ft T* * nB < ' '' ' "" - - - - T i i in l l — m - H i rir 1 1 -T-1—1-111-1 ir^ - • - -ir mW t i — M U N t t t *Kt(A

Z. 1- "E'S ^3 1. MO 3. COMMgNTS-

t. <EI'OPE '"" -"^ — - ' ' — 1 - ' " — " ' ' ' " ~ ' - ' - — " " ~ - - - - - i ^ - " - — — ~ ^ ~ ~ " - — • i »T ^ . - — —ai,u»'&e s T i M A T t n of *Loe>c i. soecipv oiAiccri«N OP suo^c. eoNoiTtOM or JLOPZ. crc.1-6 (location) Downward North (s l ight erosion on South slope. See photos.)

74AR ..

26...-iee Attachment A for addit ional

XII. T Y P E OF GEOLOGICAL MATERIAL

X

B. BEDROCK (vpucily balaw)

Shale

3. LOCA TtONfp/fiioftiv ta pofStslatlOfV duildinf*)

Across"'om road (South) troni •• l ' • • • •l a n d f i l l property (See Attach

^ 2. SELECTS (A] j. S T R C * M »

^3 <• L A K B S / H C » K B V 0 1 R a a »• O T M C R f *ON OF ReCEnr'NO iftATeST "^^ -M" -rTlJ

species of f i sh , w i l d l i f e , andct recreation. Warm water f ishe

ime

Of iSERVEO

X"

T

x

;rt.t . . -i""] G. HIGH (1000 fo tO em/^c.t - -•

Q F. VERY LO* f-OO; to .OOOOJ em/soe.)

orn

;>•• »er of thent c /

hydrologic inforin

/ n ivEAJ

pacifyJ-'

other aquat ic and semiaquaticry.

£. OTHEH (••p*et/y bJfoi?)

Covered wi th unconsondated c layand shale.(See Attachment (a)

nat ion.

4.

M U M 1 T V(•mark •X'J

X

fc ion.

9.

1T»(•n**yjt '.I")

ConfJnu« On R«va/aaEPA Fomi T2070-3 00-79)

000255

LANDFILLS SITE INSPECTION REPORT .'^^J10^(Supplemental Report) Answ<-[ clnd £xplaln

^ _ _ _ _ _ _ _ _ _ _ _ _ _ „ \ _ _ _ _ _ _ _ _ _ a s NeCt-as-.ry.'• EvTD^MCEOF&TE tH^AafLt'tyfE.aiiion.Seliline.SinliHolas. eicJ " ~ - - ' ' — — . n ^ ™ - — ^ — - , - - - —

^ l " 1=?N0 Drainage pattern (erosion) becoming established due to slope of land2. eVIOENCe OF I!M P ROPE R 01 SPOS AL OF BULK L 10 Ui05,~SE Ml -SOL t Q 5 A N D S LUOG^ES^NYo^H E~'L AN 0 Ft L L'

Q v" 0 NO Records indicate deposition of free liquids3. CHECK RECORDS OF CELL LOCATION AND CONTENTS AhO BENCHMARK

C3 ^s Cl "o

4. WASTES SURRl-^NDEO BY SOftBENT MATERIAL

C-i yes c ^o Unknown5. DIVERSION STfi^CTURES ARE EFFECTIVELY CONSTRUCTED AND PROPERLY MAINTAINED

d ves rX**0 No runoff diversion structuresfi^EViOENCeOFP^NOIHG OF WA'TeR^TsTTE^

Ct "" CX "0

7. EVIDENCE OF RMPROPER/lNAOeQUATE ORAIM1WG

C^ ves o-o' Surface runoff can traverse site8. ADEQUATE LEACKATE COLLl-CTlON SYSTEM^/

cn vEs Qn woea. SURFACE LEACHATE SPRING

03 yes m ^-o (See photo H)9. RECORDS OF LEACHATE ANALYSIS

QO vEs in ^o10. GAS MONITORING

Cn "E5 t30 ^0

1 1 . GROUNDWATER UONITORIN6 WEL.LS

0 ^-S (Xl "O12- ARTIFICIAL MEUflRANg LINER INSTALLEO

ov£s on M0

i3. SfEClPIC CONTAIhl/ENT HEASURES fC/<y floMtun. Sides,vie)

QQ v'^ 0 "o Uncon^olidated clay cover over part of fill area1 4 . FIXATION (•..•MbtliatilonJ OF WASTEa vEs (Xi -o

IS. ADEQUATE CLOSURE OF INACTIVE PORTION OF FACILITY

& YES Q NO According to state records (See Attachment F)16. COVERfrypoJ

Unconsolidated clay

16«. THICKNESSVarious-some areas have no cover

,lSb. PERMEABILITY

Low to moderate

16c. DAILY APPLICATION

C3 Y" 0 NO N/A

Closed facility

000256

POTENTIAL HAZARDOUS WASTE SITESITE INSPECTION REPORT SUPPLEMENT SHEET

Ins t ruc t ion - T h i s sheet is provided to g ive a d d i t i o n a l in fo rma t ion ''nexp lana t ion of a quest ion on the form T2070-3.

Correspondingnumber on form

Additional Remark and/or Explanation

( 1 ) Additional geologic information be accessed regardingthe location of abandoned coal shafts at the site and par-ticulars of site geology.

(2) Further sampling be conducted to determine contami-nant pathways and the surficial extent of contamination,Samples should be analyzed for:

(a) Priority Pollutants(b) Organics(c) Oil and Grease(d) Metals(e) Phenolics

(3) A metal detector be utilized to locate buried drums.Radar can be used to locate abandoned shallow coal shaftsas well as buried drums.

(4) Determine usual f low direction of drainage ditchjunction north of property to aid in evaluating probableextent of off-site contamination.

(5) Depending upon analytical results from samplestaken, design a monitoring plan possibly utilizing monitorwells updip and lysimeters downdip.

j1^ jly^olpgyThe slope of the land and the absence of runoff diversionstructures is allowing a definite drainage pattern tobecome established which traverses the e; :ire width (southto north) of the landfill. The drainage troughs coalesceon the northern boundary of the site in a lowland area(see site sketch - Attachment Bj, leachate seeps thatappear to originate in the middle of the abandoned land"fill may also contribute to this drainage pattern.

The water table is found at shallow depths. The seasonalhigh water table is just 1 to 3 feet below the groundsurface at the northern edge of the landfill. Qroundwatermovement is through secondary permeability fractures inthe rocks and is to the north following the surf-icial dip(this has been verified by stat.c water level observa-tions).

000257

Instruction - This sheet is provided to give additional information inexplanation of a question on the form T2^70 -3 .

Correspondingnumber on form

Additional Remark and/or Explanation

I.i Gener a I j1scuss i on

A variety of free raste fluids and barrels containingwaste residues considered hazardous by RCRA regulationshave allegedly been disposed of in the Industrial HasteControl Landfill according to Robert Cloar. A partialsummary of types and estimated quantities of chemicals^isposed of in the landfill is attached (see AttachmentI). Many of the materials listed can move freely withinthe groundwater regime and are not readily attenuated bysoils characteristic of the site. This list was developedas a result of depositions obtained by Robert Cloar, Mr.Henson's lawyer. Fractured btocky shale fragments areevident throughout the fill area; the native silt loamcover having been stripped away years earlier due to coalmining. Free liquids, disposed of in surface impoundmentsat the fill site (see Attachment F) have the potential toenter the water table and migrate downdip over the bedrockto emerge north of the site as a seep or continue furtherunderground to other areas. Results of the s"ep sampletaken immediately off-site on March 24 (see photo N)should verify if contaminated fluids are leaving the sitein this manner.

Abandoned shallow angle coal shafts on-sUe could alsoart as an avenue for the migration of waste fluidsoit-sit". The precise location of these shafts is notknown but are believed to traverse the northern boundaryof the landfill on to Mr. Henson's property adjacent tothe site. High acid groundwaters, with a pH of 1 . 5 to2.5, might be expected due to acid mine drainage.

Several half bur'^ barrels were observed immediately off-site (see photos ^5 and #13) . The list of chemicalsallegedly dumped on-site describes a number of barrels ashaving been deposited in the fill.

Conclusion and Recommendations

Available geohydrologic information suggests that the po-tential for surface and groundwater contamination is highat the Industrial Waste Disposal, Inc. landfill site. Itis recommended that;

000258

ATTACHMENT A

POTENTIAL HAZARDOUS WASTE SITESITE INSPECTION REPORT SUPPLEMENT SHEET

Instruction - This sheet 1 s provided to give additional information inexplanation of a question on the form T2070-3,

Correspondingnumber on form Additional Remark and/or Explanation

Geohydrologjc SummaryWater Table:

Soils:

1 tc 3 feet below surface (north boundary)5 to 10 feet. below surface (southernboundary)

Blocky shale fragments to 35 inches.Shale, bedrock from 35 to greater than72 .ches.Slopes downward to the north.

X I I I . J

Mean Annual Precipitation: Approx. b0 inches per year.Mean Annua^ Evaporation; Approx. 50 Inches per year.Site GeologyThe Industrial Waste Control landfill site is approxi-mately 12 miles south of Fort Smith, AR. and is located onan abandoned coal strip mine (see Attachr..ent D ) . Soils atthe site are characterized by mixed, loose, blocky shalefragments with some coal fragments to depths of approxi-mately 35 inches. Below this rippabte gray shale bedrockis encountered at depths of 35 inches to greater than 72Inches (see Attachment 6 ) . The area typically has a 10 to30 Inch deep layer of silt loam, as Is evident on propertynorth of the site. This cover, however, was removed whenthe area was mined for coal.The downward slope of the site, about 3% to 6% slope is tothe north with the extreme southern most boundary of thelandfill on the toe of a small ridge (see Attachment C ) .

000259

s i &

§<3

a:

" 1

000260

000261

000262

-,< . ^^^ ••. •h<r <%<t --

Attachment E

Mr. Grady ShipleyTruck Equipment Company2900 WheelerBox 837Fort Smith, Arkansas 72901 . . .- * .Dear Mr. Shipley: ,.

':• %Quarterly Inspection reports on Industrial Sanitary Landfill have for two con" /ti?secutlve quarters now Indicated the same four unsatisfactory Items. The month- *^Tly Inspection for July shows that no significant Improvement has been made In ; ;the operation of the landfill and little or no attempt has been made to correct •-. Cthe previous noted deficiencies, .v^fa

,. . -4*•.? «^As a re^uU of uncontrolled access to the landfill, garbage Is being dumped on Y^"

gg%, •• It. The garbage Is then being left uncovered. The containment ponds still •<-YwK ' POSG a P011"^0" threat to the landfill and the adjacent areas. Liquid waste - 1^'%^ Is leaching through -the levy and onto the fill. The drainage problems described ^"

In previous correspondence still exist. \ -

Immediate attention should be given to the correction of the unsatisfactory• conditions of this lindflll. ' *."

- - _ - - _-.^,.... ...a*'District Inspector

^' -'- Solid Waste Control Division

Water Division

000263

Mr. Grady 0. ShipleyP. 0. Box 688Fort Srith. Ark . 72901

RE: C lose-Out Procedures for Your Industr ial Sani tary Landfi l l PerOur Telephone Conversa t ion July I'll 1 9 7 0

Dear :4r. Shiploy:

An Inspect ion conducted of your d i s o o s a l s i te on JulyMi 1°78,revealed severa l items that need Immediate correct ive act ion In orderto a l low you to properly c lose out the s i te In cor.iollance wi th theArkansas Solid W a s t e Management Ac t /So l id Was te Disposal Code.

You are ful ly auaro of your respons ib i l i t ies for finalbe appl ied in a compacted layer of at l eas t two (2) feet ofin addit ion to the dally cover shall he p laced ov;r the cntof all completed port ions of the fill wi th in s i x (5) nonthsthe final p lacement of refuse. Final cover shal l be gradedon the approved plan and to prevent ponding.

cover tomaterialre surfacefollowingas provided

The surface of theelevation at all t i m e s ,where necessary, Finalof two years.

final cover shall he maintained at the planby the placement of additional cover materialcover depths shall be maintained for a period

At the time of inspection one pond w a s sti l l oocn and In need ofcleaning out and f i l led in. There were still scvor' i l low spots on thesurface which wil l ca tch and hold water thus providing a leachate threato the ground water . The liquids and sluri^e which are still 1n thepond eai'lt a sl ight chemical odor and unsightly appearance.

I recommend that you remove the oil scum of f the pond. clear thedebris from the pond and the perimeter of the fill s i te . drain and fillthe pond with a su i tab le cover material . The entire s i te . includinothe fill sur face , shall be graded and provided wi th drainage fac i l i t iesto minimize run-off onto and Into the fill. and to prevent erosion orwashing of the fill. Seeding to promote stahiLlzat lon of the f inalcover shall be done as soon as weather permits.

000264

Mr, Grady 0. Shipi^uly 1 9 > 1978Page 2

An Inspection of She s i te shal l . _ _., ^.. ,,,^ci.i,ur rroii- ^ . . J W a s t e Control Division to deternlne conpl iance w i th approved

.-..-.. -. ^..^ a i n: hiidii oe made by an inspector fron theSol id W a s t e Control Division to deternlne conpUance w i th approvedplans. It wi l l be your responsibi l i ty to Inform us In wr i t ing fora final inspect ion.

be made byc1plans. It wi l l be your responsibi l i ty to Inform us In i^r-m^ ^-'"a final 1n<;nn/-n ft^

Al l cor rec t ive work wi l l be performed before final accep tanceIs made.

Arrangements shal l be made for any correct ive work on the f inalcover during the f irst two years fo l lowing complet ion of the fill.

Feel free to cal l on me for any needed a s s i s t a n c e In this matter.

S incere ly ,

a^ ^A. L. SparksDistr ict InspectorSolid W a s t e Contro l Div is ion

livrt 03f(iiu33 onv OJansHi "03y:usio3u 'idf333U HunuuI—•I——R——•'—'———

000265

r'-r* /..L^Sp.jrk^.'D^^rtT.^.t of Pollution Control

r-n;] ^colo^yr.C l :;J;ioncl ;J:-iv^Little Rock, ^rk^n.,35 7^20 '

De^r i-lr. Sprirk^:

Th ,- follai.iny is in reply to y^ur letter of July ]';, I1;?'-' •.;*icrcinyou noJe a report, of your in^paction of our former landfill site.

O.ir fin.-l cover is in ploco at the prc^'.-nt ti-ic. '..c c;; •,cfcc^' ;;:*!filled ?<>)020 y^rUs of .'naterial} •..hi:h i^ :;.iicli .-,nr» t.i,..n cifiJh to covrthe fill sU'- to 0 depth of t.^) fccti :"J ^Lin <;ct udc-^atc con,*<.ctionof the cover.

Oir yr-i'ili!., ....,, doiL* .'-•c-''rUin-_- to on (•,'i'Ji;T'.-r'^ pl.'n lo -cnforftiv.i th th:- surro'J'i^iny n-'tyrd tcr^oi.'., ziJ to .-issurc J^oil dr..ina<i;' ocro^sthe* site v.i th no ponJifVJ. Vi^un] in^'^^tion &ho-.-/G c.-^cllLnt (ir.iina^c.'.Native 9rJSsc& anJ t-ccJs aru gromriJ v.cll, u^athcr con^ldcn.-.:.

Th- rr'-i.-.ip.^ny Oi. .i pond has been pr^p^rcd for cont*ilnnic.;t in lin'J'.•;i fcti previous discu^siorts v-ith the Dcpr.ftr.ic-nt of I'oll'ition Control cr '^fecolofJy. '•<" corc-ditchnd and lir»cd '..ith cl^y to prevent le<:ki"J^, -inrl Tsee no cvidc'r.ce v;h<tt.,o^vcr of any l('<;k3"]c. Thcro is ^orc th^n •siJOtiiistf-*h^i'J'it of the i.olls to prevint eiccidontal ovcrflo./. Furtht.'r.-nro, thcr;-ha^ hc;;n nothing but ^<3itl..tit,'lr introdic'.'d into t-hi.- P.TI(I in o'-'--r s yi'yrvjTi a h.'.lf. In rh^rt, the p'nJ prc-- 'it^ p-3 hr.z.iri. •'•L •.'-ill Ucyin dr»iin-i:i.j, ho-.:c'vcr, in fch'- n(:<'r f-JtJrc. roll ..In; th.it) v.c do plo.. to fillthe ponj,

^our.. very fcruly,l..^.fJTi(l._L '../.JT- CO:ITn:)L, :::G.

Crtf'ly D. Snipl'J/rrc'^i't'-nt

1 1

• .'' .-<) l) ,^

.-•*!; «-»JJ.•r\—

•••< .Sl

r-i• -<.-

'•^1 •i:-.\•^• /-<*.•/

^ \^'

000266

Hr. Warren JenningsSeptember 21. 1977Page 2

Mr. Jennings, the owner has undertaken these items of improvementin the spirit of wanting to operate the facility correctly. Mr. Shipleywould appreciate your viewing the site at your next opportunity and advisingi£ you hc.ve additional suggestions* I will, of course^ be available tovisit the site with you.

Very truly yours,

ATES, INC.

CLWidjm

cc;cc;

Mr. Carl ReamesMr. Grady Shipley

000267

Attachment Q

• T, • <i-i., i1'. ,it'.1. ' ;

J^» l.iL .'ul' HAL '.;.\; I'i.. *</1 . .wiJ . Ji ,,

.cca'-ion; A..'' .;\i ^cc^t 'n 3^: r. 7 '., ^. 31 ..'*, ^-J aJt'..;i >iiii^, - . 1 '

Ciut; is cJi u zirJ-'ilJ^ ^trij) pj.t ^•^•T"•»xilli^t-^;I. '.•'C'C ''^c1 I-;.'.. i ICo "cut•riidc siitl 1 5 tc 3^ ^^^ ^yp-

Tw-1 piLJ -,Jcru c:'-sa'.'.iyt\3 ' y a 'a^l.tiuc in '.he b--'^-:' - •'' t. lu aba-J medciri^' i-ifc. T"ci" ^'c^criptiona fnllow;

* Lxcavation in oayt und or strip pib;

0-33 inc ey 'L;cclJ I-'^JL-, fhie s c.lu ^.-a u.i' ;;:'li• G'';' ' c^alj"ai;.'..yiil5

. 33-^0 inc cs '''•PI" -It-'* ^^y s^alc Icdroct;

•^caval.lo'i i" ;;uu^ nnJ o? sbrip pi".

0-20 iiicl.ua - UOIJJ 1'JOGOi fir.o s.'.ulu fra.;-y:ila •niu1. JJP.U c.-il-'^a,..'icn;.J

20-3' iiiL'iics 'i.j^l'lu bt'aJ o iilo iodr^.''

ul':l-'G^« ' l; J'.'til.'- iJ ' •'idl.i'c.tcl;' KGll di'Li;-':'-.1 h..-ll.

' <- '»

O-.-,"

'• 2^"

2ii-/-0"

''C 'i-Ott,?!-'

''•pl.ji ; ilt ly:tm

yellJwi^ . I'r'-'^ii siJ.t iQan

.btLlrfd .."ay and ^'fcU^wlJh rro'Jii silty '•lay l3;

.'.tri;' F?.1 IJ ripi'a'le u'lale 'rc'JrJck

•lU^ A. Gsm-Jr COPIED FROM -.'•i.'u*- r. vnl.'oil Sci'su'l;-1 - < , ^ „.. > . .^K Cr.'iscr-^t4.'!! ':•.:; i»i -i:.n

. r.oU ::*nL-Gr^Uoi ."(.rvieo r U ' - ' K U ' J A L I I Y ^'11 C-.^.-Vu'J-.';! ;3rvic.iv-st '. rley ( A UC9 / D iP iyAt '""^ ^''^^ ''•x 'ls00

•brfc 'it.., A"l.ci;t^J UmulnAL. -,..1 ^ =J '. rtri'?.i:a^

000268

Shwuw PJAN i

000269

^Br' I S . ® ®• 3 -» . • v ri» ^

"»,»».

J /*f

•/ >

' ?,'

' ' , - -' ' . . • • • ."- ''' "

„/'' TAtiLh; 11

. ^)/:i-^:^^^^ (.^/\,:^"(^^-7fS^

P.i-.JUJ.'! 0:-' Cii^'JUAl, /u;Al.YS;J Of-^-Lt--;^;-, T.^C/W.^^^T ^i-/c^

, • G3;.SnrUK.T U?;jT3 O.-'::i'f-.;,i^1)

Ar.->3iua Nitror,cn .is (^^ 1'1'M 79.99Total rhospitorus as P i'l;! I.C^)Oil-5; Grtiase JTM ^J.^O I

Cad.-J.a-i i-i'M 3^5 ^

<^Chl'offd-u.-'. -Total ! H: ^^.O ^ •Iron ir;' »• -. i'»3. QJ^nJ • in! ^..5 QNickel . m; ^10. ^

,^nc mi X)''o.Coi. 'r It.'l '.,0AUw.i.niini I'l'H J<'.;;C&lcian 1'I^i '/(\/JU

/.i-snic ri';; 7.^ ,Tin ^ i!-Ii ,.-. ! ,-'P^ryniuffl " - ^^ l i f l . .' < > } - ' • 'CyaniiJg —. t-: H 1 / <.i / //^ • •

\ f / '?ui rates - ini \ 1 /;;.ro^isturo ;•'. n/^.t •• ;' ;il.O ,f« (of r/a solution) JijJ "••. ^10.6 :

\ "-..,* • 10) \ /•v' 'AH values based ^•;);i ITK I/ :-;i<;ht or i.-a ^Imi^c,

'> t ,:/} DD r ^•/? w^^^s ' , s/ 1 *«-/-/ » , , —

S/^C/);^ S , \ ,'; '" / "

f .- / ^i ^r /

AllKOVU) / / . • / • • / • '•//-••— Jl*i*t /'. 1, i:;. •m ^ -.'il-.irii**^-/ T.':.Lin^ Cecvicc K'-f-rcsontaLxvo

• - i— ' /^ c

vaasasHWiasw^KW^S8SSSSSSSS8S8ltiSiSSSSS&000270

11 'L 7^30

TAB1£ II

?^:SULT£ OF CiiEmCM, ANALYSIS Oi-; DEWA'j'EP^D V.'AST^'ftTEnTR^TmiT 50LIL-3

•

(l) All pp^ values bcsydsludse.

KP

APnWED /' .' l-'U. M. Ln»50n " ^

CaiSTI7j.^Vi'5

ArrJnonIa Nitro?.en ar, 11HToLal Fhosr^rJS as P 'Oil & GreaseCadniiwa

Chromium-TotalIi'onLendNickeX

ZincCopperA l .iJiun>Cdlciur.

AraenicTinBeryl 11 vunCyanide

SuirateaMoisturepit of 1% SolutionCarbonates

Silicates as SIO-

U111TS

pp^rinpip|.'n.

ppnnwpifflpixii

PI'"FP->1.,-nr-p'n

ptrnF'lppaH^

PI1"^ by vtSi-Dpr^pl.<n

i

upon partr. piir million

tabcralory

coi.cKtTRA'na.'3/<392/.002.8

30°?,00067862

10/.0392U1^,600

3.^5:63

<,2

177.50053.6910.9513.700

5W

by we-., ht oC as

Testing Sei-vicf

<3-t\l1^ •00*^

—~5

^

' '•

. J

• J'

--^^

1

"'

™i- aEa

'."?

-; S3-1^

•—aa

received ^-""Sf"'•'

•--'aj

£ Rcpresenlat.iYt '--i-fci.'.•?iE,

ai?

000271

HENSEH V. INDUSTRIAL WASTE CO.SUMMARY OF TYPES A»D ESTIMATED y0 ANTI-TIES

OP CHEMICALS IH DUMP SITE:

i'aritfr ' •-••"i;.^ •r .36ly Bhct.-ier A^-.-nn*'Pore Sfflltn 78*)-^33l

Whirlpool Corp.500 Jenny Llwl BlvdFort Saien

General SlectricSouth ZeroPore Saltn

3aldor Ueccrtc Co. Inc*Poet Sritft

Dpaoso Inc.

irs-77, iffy •Jii .-ii, ):-. ;.,.•• if-'-.^ir Ho. ioti;

23; aecnyl ett\yl ketone1 1 1 aceconelli ootnanol3S bueyl cellasolv«

13i tolUene

copy or 2 LaHson teacs (attactied)luantltles not divulged inIntarcoa. (^1-59 drua»/wic inlatter 10 AK Pol. Gonb. Dcpt.)aludg« now bo K«nsa« Ind. ^nv. Sorv.W i c n t t n , Kansa*,paint tnlnaara to Solvents SecoveryCorp., Tul««, OlcU.

Ho analyst* avaUaoLo."faatis psinea and aolvan^a"(now ualntf Solvent! RacovapjfCorp. or Tulaa and U.S. PollutionControl Ctp., 0*cla. CUy)Quantity: vaa/75/33

8/3/76/85</25/76/2»3/10/77/*?

an<l «o oa —

1 of 55 lial. druaaTyp«a NOK: a/ao. danatupatf paint a

(acpyUc)8/10. uflcurcd acrylic

paint and xylol -dnd coluol »rnt itfau

? d«gF«aaar riultf*f/crlchlopo»lhyro»,5P«ft«« and oil a

</»o iftauUfclon adfleslva/aya. rubMr/rsainand pat. diatillaf

2/yr KlF® color 4y/iMdcaroaau* raoli^ta.auTftttfand *olv^n6s

2 6la/yp polyafpeoaclfts ;soX?«n£)polyp)

quant Itl»« avg./wK:unlenoirn

!to aoaiJaia a« or ?/21/79 -in p»w»» or ooflniAg.Quantity: 186 Oru«i» $/76-*/77new uaJLA« Solvnc* RecovapJ Corp.of Tula*. Waata cutting oiluftiiwane say "L^uSinT^aMAA.ssby CaPtirrd Laoo-»corl«»,Pt. Wort ft

UnkftOHn «uMnCltl«« irici contant -(—terlal aaf«ty dRts «n««tA?)Jod. Mut« ttefc«f? -Co. plant not In o^«r«tlon now -Letter froa Ind. Waate fte (4'naxardoua" material* 3/17/77

000272

Grain Industries, Inc. Urethane roam and paper -Liquid wastes stored on site 55 galdrums and sniped to Tulsa for disp.- objected to disclosure of analysisInd. Waste said mefchylene chloride

Other C o . * s : Solid waste only —except Pfc. Smith Barrel and Drum: solvent baseand waste hydrolicbil

R^eem? left ore Infcerrog. by mistakeAffit. and types unknown

000273

Photogidpher / Witness

CW^ AiJ^yn/Wf;/ ^AJ^

Date / Time / Direction

3"^"^ /^^/ ^^

Conmen ts :^lyib5 (> 7rf-i

rjyft^romfc, (//e,*^ tfF cta'Kp

5^'i <3.r^^ <sk<3^ <sc.f^e^

Photographer / Witness

Date / Time / Direction

Comments:

Photographer / Witness

Date / Time / Direction

Cowients:

000274

Photographer / Witness

Ch^Ai^w/^ l ^Date / Tiee / Direction

^'Zl/W/Sw.^

telMntsioKjhu ?Afft A3

PIS iff to mi. t/.-t^ af- y^c^

Itete / T(«e / fill-action

WitfEograpttar / Mitnais

Dale / Tfee / 51race*w

000275

., -c^., < '" • iM<5cii---t L ""STC 1^- ( ^' r-^^^^^^--^ iO. ^ / ,. ^

^otWdpher / Witness

liMv^d /fn^pf^ft/l^rn/ 1-^A^ty

3ate / Tinie / Direction

3^-^/^^/ 5^^

^omnients: /)^b ^-^______

g&M^le. l^^h^ ^/

^ t^a^_r <^^y/^________

• Photographer / Witness

^^SfcOate / TiRie / Directioni , ••^^^^/m8-/^JK

Conwents :_p}yd<? ^ £

^a^pl^ I^CciTiQf^ ^Z

&0tl QO^pl^. ft^F Jtf/o^^^ft.

g' ^^1

Photographer / Witness

(/^ /flJpr^fi/6p^ /Af^^^^

/ Time / Oi reckon

^^/s-ar/^u/AConwen ts: _/>Wa_^ /^

Ig- ^^ ^J

000276

Photogrdphar / Witness

QJ, 'J f\n\wai,/^cf,^kl

Oate / Tffas / Direction

3-3tj-^l /i-Hf/J^^

Coaaents: Pho^ fr 1.- " ^

Photogr»ph<r / Witness

Qi^AvJQaotAo^ ^o*Jry

Oate / Tit / Otrectiofl

CanMntt: .Btaba,

Qs&lS^S^^U^-MS^i.

Phoio^raphcr / Witness

Date / Tine / airect'ofl

000277

•KB

UNITECC^ATES ENVIRONMENTAL PROTlcTlON AGENCYt1 5 Jurt 198(

Potential Hazardous Waste Site

Charles A. Gazda» Chief ^Compliance Sect-ion (6ASASC)

Sruce Elliot. ChiefGeneral Enforcement Branch (6AEG)

\ \W

Site NameLocationHazlt No.TO No.

^n.d.i -fa7i ..(...Z lg5^a C^^Tm./ „„„„,„.f^^ <?^. -(-k, Af-^___________^K? f^.-g— < - g/^^- ?" '

A. Field Report:

1. T2070-2 attachedT2070-3 recon sampling attached

2. $311 potential

Priority —^Lyes (

forwarded on ______forwarded on _4~.fS~-Jr/

} nofXL

analytical results attached . . . ..- » /

Proposed ^11 action^ (Emergency Response Branch) . ^ ^e^^L/^ t i g^ .^^<-fZ-^f^ ^<^^L< AiK^J^^ — ^ ^I_^y':l-f7I ^^e^

3. ISS Inspection conductedISS Compliance Report attachedISS Non-notlfter Report attached'

4. Suggested further action

^s ( ) no ( V )

yes ( ) no (y)Yes ( ) no (V)/• i

B, Analytical Results:

1. Contract lab resultsHouston Lab results attached ( / ) est. completion date

attached p^ ) est., completion date2. Drinking water wells, samples yes (^_ ) no ( )3. Suggested further action

cc: Adele Mitchell (6AWS)

000278

SUBJECT: Transmittal of Laboratory Report:Industrial Waste Control Landfill, AR-W16

FROM; William D. Langley. ChiefLaboratory Services Section, 6SA-HL

TO; William J. Librizzi. DirectorSurveillance and Analysis Division, 6SA

Thru: Malcolm F. Kallus. CMeHouston Branch. 6SA-H

TransmUted herewith are the laboratory report sheets for analyses per-formed on one aqueous and one soil asmple collected by F-IT personnel atthe subject site on March 24, 1981 and received at CRL-Houston on March25. Parameters requested were metals. pH. and phenolics. The cyanideanalysis was performed additionally at our discretion.

^^ y-^William D. Langley

Attachment; Laboratory Report

WDL/mal

6FA Fora 1520-6 Wav.3-76)

000279

•HokJSton Branch Lal 3fery~Nuinber ~ ^3'7y^Field Sample Number wTaq No. ,6- 73^71_____Source ^s/^;^L^t^<; (W^/ Lo^^fiH^&oo^ . s^-^ 01 u/.^^^^

e^.c.^^e, .^<sJQ ... .._________________^__________Date/Tin»e Conected^6^/^/^-»to Collected By

Paranieter

Antimony »SbArsenici AsBeryl Hua, BeCadmium, CdChromium, CrCopper» CuLead, PbMercury, HgNickel, NiSelemum, Se

I'ype Sample ^jyaei^w" 6 ' "

ConcentrattonParameterConcentration

Silver, AgTh£t1iu.?i, T12ir.c> 2n

^S^sM^pb),*&^—z?_<..30 •// ft

,/< SLO if2/ //

Phenol ?, Total by 4AAP <2. (^j>JCyanide, Total as CN <^i / / _ * /

//

//

' . ' \^\. . .——————————————-————————————————:——————— Chlorinated Pesticides/PCB's by Gas Chromatosraphy/Electron Capture Detector ^Name _______ Concen tratj on_ tiaine Concentra'tion 0

0

Priority Pollutants Detected by Gas Chromato$ra?hy/Mass SpectrometryName_______ jConcenfcratjjon liar.e ___ Cpjicentratlon

Other Orgamcs Tentatively Identified by GC/;-iSName Est. Cone. - Har e Est. Cone.'

REMARKS :J^A.^^^erf^t<2£^^^_g^^^^^z^^ -m^Z^ , H, ^A^fifL^^AA^I^ '*-1^ <K^.^U.^^ .^r &^JL^ ^A-^^A^"^_. _ _ ' f

000280

Parameter 'Concentration Concentration. < &?, 6 •^fy/^ (pa^.} Silvsr» AgJ.^/''-^7' 'Thallii;.n. Tl

Antimony»SbArsenic, AsBeryllium, BeCadmium, CdChromium, CrCopper> CuLead, PbMercury, HgNickel. NiSelenium, Se

2inc» Zn-<^ ^ .sr v n

////

^i2^7 . ^

.t'heno]s,.TotaTby 4AAP,<^ ^yj^6^^)Cyanide. Total as CN ^A^^ '.

/^yi^^^/-,c\i. J^4*^ ' <^^ ^a^'Z^^ft^e/^^Je?/tfA^ ^CM^_, ._________

Chlorinated Pesticides/PCB's by Gas Chromatosraphy/Electron Capture DetectorName- -______ Concentration Kaina ' ' Concentration

Priority Pollutants Detected by Gas Chromatography/Nass SpectromefcryName_______ Concentration Kafna______ Concentration

Other Organics Tentatively Identified by GCflSName Est. Cone. flaae Est* Cone,

REMARKS : gfr y i £^»S^^ fti^l^ zo^u^_^fceZt2^ i<?/ . rfi ^A^^^ ^Gfiq^tM ff^^^^y^f i^tff^^ ^Li^^A, /^ ,——^——————————————.

^^^y^c^^ ^.4 /<^^/ ^^/^/

000281

000282

/, n'»x Kf^i Alrx.mdri.i,•

1 AH/MS AT/tn v n »•• • •« • — —

V A ' • - 703/^3-Om

ORGANtCS ANALYStS DATA

v.i«.fii • ti»icieSHEET

SarnpIc"Nurn&cr

P0314S

LABORATORY NAME ACUREX

LAB 5AMPLB ID NO,. A8^

QC REPORT NO. _____LV 6• ,„——.. -... ir ,„ .-T. - . . ——. . - . — — . „ ^ --r-r—^-r.m-r^u- -—n

ff '

ACID COMPOUNDS Ug/1 BASE/NEUTRAL COMPOUNDS

21A 2,^i6-Irichlorophcno! ^f) 41B t-bromo&henvl hh-^oi **i.—22A p-chloro-m-crft&ol2<iA 2- chiorophcnol31 A Zift-dichlorophcnol3^ A 2»<»- dirricthylphcnol57A 2-niuophc-nol58A ft- nitrophcnol59A 2,<t- diniifop»icnolCOA ^6- (iinliro-o-crcsol&*»A ^pc-tmrhlo'^hcnol

6^A J^hcnol i

DA5E/NEUTKAL COMPOUNDS

1B iicenarhili&ne 1^5B benzidmeKB Ii2i<(* trichlorobenzene9B hexachlorobenxene!2B hexachloroethaneISB bh(2-chloro lhyl)elher70B 2-chlofonAphlhalcne25B 1,2-dichlorobenzene26B I.S-dichlorobfrnzene27B 1 -dichlorobcrucne2SB 3,3'"dichlorol>en2idine35B 2,^- dinilrotoluene36B 2»6- tiiniuoioluene37& 1,2- diphrnylhydraiirtft

(as azobcnzene)3$B fluoranthene

ftOB <" chIorophenylJ^henyl etter ^ f

*2B '• bl» (2-chloroisopropyl) ether<i3B bis (2-chloroethoxy) methane^?B hexadiforobutadienc53B hexachlorocydopentadiene^B iwphorone55B naphlhatene56B nilrobenzene61B N-nllrosodimethylamine62B N-nitrosodiphenylamine63B N-nifosodi.n-propylaminfe66B bis (2-ethy Ihexy!) phthalate67B butyl benzyl phihalate6&B di-n-bulyl phthalatft

D 69B di-rt-oclyl phihalate70D diethyl phthalate7IB dimethy! phthalate72B benzo(a)anthracene73B bcnzo(a)pyrene7<i B 3,<i -benzoflcoraJithene75B ben2o(k)fluoranihcne76B chrysene77B •cenaphlhyknc7(6 anthracene79 B benzotehOpcryleneSOB fluoreneXIB phenanthrene12B d*ben2o(ath)an; hracene

j—— 13B tndeno(l,2,3"c3)pyrene[7— 14 B pyrene <

ug/1

^0

— —'

—"•-"

—

000283

000284

000285

*.'

LABC

LAB

QCR

21A22A2^ A3 1 A3<iA?7A5»A

^L

60 A^A

SiA.

1 B5B16yBi2B1X62062>B266276WiS^-m16637b

5&406

•ORG/

5RATORYNAMB ACUREX

SAMPLE ID NO, A81 "03-030

EPORT NO. LV 6

,ACID COMPOUNDS

2i<Si&- irichlofophcnolp-chloro-m-crcwl2- chloropheno!2i<i-dichlorophcno!2ttt- dimeihylphcnol2" nil/opht.'nolEt- nitiophcnol2t<i- dinllroplwnol^,6- din'lfO-o-crcsolpfiftlftrhlo'o^hcriol

J>hcnol

&\5E/N£UTKAL COMPOUNDS

tcena^hlhenebenzidinel,2i^- lr!chlorobenzenehe&achlorobenzcneheiiachloroethanebii(2-chloroeihyl)ether2-chlofonaphthalcne1,2-dichlorobenzeneliS-tfichlorobenxenel,*-dich!orobcn2eneS '-dichtorflbenzldine2,4- dinilrololoane2.6- diniirotoluenej,2" dipht nylhydratiw(ai azobcnzene)fluorxnthene»- ehlorophenidpSsnyl elhet-

**t^-uaB>

^N»CS ANAL1

ug/l

^pS-6t±-AJP

—^^, »

uJ*ifc *••»••'

-.A...a-."'

-.„.(.?.„„UD..,ir, Jyp,-

-/.„ ..4r.

i/P ?9B

1

-, ..

DE*•——J-^

ySIS DA

BASE/

«IB»26'-43B52B53B5<1&^B^B61B6?B

SiB«66B67B

.6SB69B70B .71B72B75B7«B75B76B77B71&

{OB»!&t2BS)&l B

6TA SHEET

NEUTRAL COMPOU

**bromophcnyl phenybis (2-chloroisopropyl) etherbit (2-chlorocthoxy) methanehexachlorobutadienehcxachlorocyclopcniadienehophoronenaphthalenenitrobcnzene-N-nitrosodimethYlarnIneN-nilrosodiphenylarninc ^ ^N-nifosodj-n-propylamine ^'/'bis (2-cih^lhexyl) phlhalatebulyf benzyl phthaladi-n-butyl phihalaledi-n-octyJ phihalalediethy! phlhalatedimethyl phthalalebenzo(a)anthrace*'«benzo(a)pyrene5i^-benzofJuoranthenebenzo(k)nuoranthenechrysene•cenaphlhyleneanihraceneberuot hifeen^neUuorenephenanthrenedtb^nio(»,h^aft:hracelndeno( B »2»5"cd)pyrepyrene

ifom|>lc"

„ F0314

ND5

f\ ether

ie }

^0

nene

•furntcr

SS

ug/J

NO

K/D

^,

1

- , 4 S

J^t^

"^—o»,,JO

/-^

/

000286

J3^ S-TnpIc N'itnt<-r

ORGANICS ANALYSIS DATA SHEET - Page 2 »JP.C3^ 5>

LABORATORY NAME _ AGO r ^ ?c

LAB SAMPLE ID N0. Al,L-o3- 030

QC REPORT NO.

U i?i?_-tetrachlofoethaneJtlofoe thane_____

2-chlofoelhylvinyl eU>erchlpfQfofm________i 1 1 ••dJchJQfocthyiene___l.g-trans-dichlorogthylene

^V^J.^-'dichIoropfopane33V !»3-JLchJoy_QP!ropylene3&V ethylbefizene

dichlofobfomomethaneIfichlorofluofomfcthafte

30y_ __dicbtQCQJiOuo<'ornc»h&nc51V , gjll<yotf|bf0fnognc thanet?V tetfacbLofoethylcne>6V toluene_____

1 . ^Ig^y^^y^e8>V yiilyi dilofjde

J9P aidrin9QP. dieldrin

9LP chlordane92P__^^DT7£f

93P9^P95P96P97P98 P99P

f.^f'-DDTt.^'-DDE<l,<l'-DDD

"endosuKan-cndosulfan

endosulfan sullateeftdrinendrin atdehyde

•

\

——0.J-,h——^<T^

00<^

/

101 P heptachlor epoxide102P -BHC

JQAP 'BHClg6P PCB-I2»2J07P PCB-lSJft

10&P PCBdl211109P^ PC6^2J2110P PCB-12UmP ^CBdl?£0mP _PCB-|OJ61 1 3 P loxaphene

2f),7gS-UtrachJorodibcnzo-P-rfjoxin

«Lesi than IOug/1(pcslicirics Ic&s ttian 0.1 ug/l)

Nil • Not <fct.-cird

000287

000288

r^^^c^n^ y: yo^s^ c Mir 'g^ f1"

ORGANtCS ANALYSIS DATA SHEET^ "humKr "F0314 OS

LABORATORY NAME

LAB SAMPLE ID N0.

QC REPORT NO.

ACUREXA81-03-030

LV 6

000289

OKCANICS AF

LABORATORY NAME ACUREX

LAB SAMPLE ID NO.. A81-03-030

OC REPORT NO. , , J-V 6

VOLATILE5

2V acroiein ^3V ' acrylonilrHeftV benzene€V carboo leirachlon'de7V chlorobenzcne10 V 1,7-dichloroethaneHV lil,Mricliloroelhane13V l,I-dichlorocl*.anei<)V l,i,2-1rirhlorocl»idnci5V 1,1,7,2-lflrdChIoroelhdncJ6V chloroeUiarte19V 2.ctiloroclhj-jvinyl ciher23V chloroform29V U-dichlort.clhylene30V 1.2-U&n&-dichJorocthylene3?V Ii?-d*ch!oropropane33V !,3-dichloropropy!ene^BV ethylbenzene<f<(V rnethylcne chloride*5V methyl chloride46V fnelhy! bromide»7V bromofoffn<iSV dichlorobromomelhanet9V Irichloronuo'oinclhane

50V dithlorodi/fuoroniclhaneSJV clilorod»bromo*nelhi»ne85V iRlrachlc/oclhyk-ne(6V toluene87V trtchlorocthylcne»aV ^nyl divide ,

&W inipic Ni*r

^ALYSIS DATA SHEET-P^e 2 F0314 Ds

U&/1 PESTICIDES

ft t9P Aldrin ^SOP. dieldrin5 IP chlordane92P fi^'-DDT93P M'-DDEW t.<i*-DDD95P -endosulfan96P -endosulfan97P endosulfan sulfale

. 9 & P c n d f i n„ 99Pend ' i n aldehyde—^ lOOP hc^tachlor

,101 P hepiachlor epoxideJ02P .BUCJ03P ^HC10<tP. -BHC105P -BHC106P PCB-im107P PCB-125^10&P PCB-1221JO^P PCB-1232HOP PCB-12t»J 1 1 P PCB-1260HTP PCB-10161 1 3 P toxaphene ^

DIOXIN^

:—— 129B 2,3.y,8-leir»chlofodibcn2o-^&-<fioKin

< •Lei& than 10 ue/1

in*cr '*

"&/!^^

^——^

ii/<., .. i'n00

———^

-

i^^'

^fr^

000290

000291

: • ' . - • • . wORGANIC

tABORATORV NAME A^W

LAB SAMPLE ID NO. 4-t /- ^3- ^Jo

QC REPORT NO. Z^l/ 6

ACID COMPOUNDS l

2IA 2,<ti&- trichlorophcnol ^22A p-chloro-m-crciol24A 2- chIoropScnol31 A 2,6-dicMorophcnol3^A ?i<i- dimclhylphcno!57A 2- nilropht-nol5tA 'i. nilrop*wnol59A 2J,<i- dinH/ophcno!60A <46- dinliro-0-crcsol ^fctiA penurhlo'oi henol J 62B N-nltroio iDhenylamine0 A J^hcnol ' A,

ii

DASE/NEUTRAL COMPOUNDSl

1B iicena^Stliene ff5^ benzidineSB Ii2i<'- Irlchlorobenien®9B hek»chlorobenaienej2& hexachloro&thafte]£& bis{2-chloro<thyl)eth8r206 2-ehloronaphlhalene25B 1.2*diehJofoberi2ene26B 1.3-dichlorobenzene2 7B 11* -dichlofobenaefte2SB 3J'-dichfofob&ftz!diw3^B ?it- dinivoioluene36B 2.&" dinivotoluefte37& 1»2- dipht-nylhydfazins

fas azobcmefte) ^39a fluwa^tbeneftOB ft- chloropSen l phenyl clher ^

M5 9 ^^Fc^nKr"< A^^I V<.K r^ATA !WPFT ————^ ' '•

, f •Jfi/1 BASE/NEUTRAL COMPOUNDS

D *IB ^-bromophenylphcnyl ether ^<2B'- bl»(2-chloro]sopropyl) ether<i3B bi» (2-chloroethoxy) methaneW hexachlorobuladiene53B hexachlorocyclopcnt^dicne

.5<iB isophorone55B naphthalene565 nitrobenzene

f 61B N-nltroiodimttthylaminc

^D ^6 N-nifoiodi-n-prooylamlne i66B bis (2-Mh» Ihotyl) phthalate /67B butyl benzyl phlhalate ^^

.68B di-n-buly! phthalateD 69B di-n-octyj phihalate

70B . diethylphthalate7JB dimethyl phlhalate72B benxo(a)anthracenft73B ben£o(a)pyrene7*& 3^-benzoffuor6nth«ne7JB benzo(k){luoranthert976p chrysene77p •eenaphlhyl«ne7BB •Alhracene?$B benio( hi}pcry!eneSOB (Juorene '1{B phenanthrene /12B dibenzota.hUh'.hracew NO

—— Jt3B lndeno(l,2,3-cd)pyrene?—— J^B pyrene i

ug/J

R

"in—^r

v\a0

———/-Tt

|

^

/

{

000292

• " " " — — 6 •OKCANiCS ANALYSIS DATA SHEET - P^c 2

LABORATORY NAME /^^V

LAB SAMPLE ID NO, Ai-l--0>-o30

OC REPORT NO. ^</C

VOLATILES ufi/J PESTICIDES

7V acrotein Ut) W aldrin3V ' acrylonitrileftV benzene6V carbon Icl/achfori'de7V chlwobenitcne10 V J,?-dichloro£thanc^IIV LliMrrcliloroelhane1 3 V I.l-riichlwocl'tdni-^V l.l,7.U*fhlo?oeth*ncJ|^V J^?,?-lpl/dC»»lo*oelhar»c16V chloroetl^ne19V 2-chlo/Otlh/h-iml cit<ryV chJorofOfni^V Ll-tt*ch!ou-cl*iylente30V l,?-lf|>/u.dichlof0clh»lene^?V j,?-dich)of0t>rftpa^e^V ^.3-dichlorooyopylene31 V elhy?ben2cnc „ „ , , „ ,tdV melhylene chloride0V melhylchloflde*6V melhyl bfomldet7V bfomofofm4fV dichlCtfObromofficihAnet5V iflchlerofluyoinelhane

50V jjicMorodinuwomciSane^IV cy*l«otf'^omiMnei»dn^l^V lcl/acMoro<thy(cne16V lolucne , ,... .„ .pV UlcMoroclliyIme . .( i iedo ^HV^ vinyl dilwidc ^ •L»u lhan 10 us/I

90P. rfieldrin91P chlordaneHP ^.^-ODT93P ^ -M£^P t^'-DDDW oL -c"dosuJ(An96P P »efido»ul/an97? endOAuKan »ulf«le^&P cndrin99P cnd'ln aldeliydeIOOP hcpiachlofIOIP heptachfor epoxi^J02P^.BHC103P <S -PHCJO*(P. ^BHC105P ^ -BMCJ^P PCB.W2{07P ffiB-l?^10»P PCB.)??!\W PC8-1?MHOP PCB.12t»1 1 IP PCB.12tO;1?P PCB-ISKI OP toxiphene

l?'o,W— l*tfin 9 t V • .•«tr«J>l«lM.rJHu

Saniph^hunihcr''"

. M^'

' a&flOiPl

^ „..„,. ff I.T/UD

O.O?"••""'""'" 1 ' " ' • no—————^.JA gt

0 .1^ t^0 .13 0

^^ S&.&/0.<(.A /&O.o^&,?',2- ,•Offt

00^£.0^

^&,A/Q==t=

>•'

dibciKO- •v'>

Nn«f—' i L ^ - r-Ti ,,,,,,,i, i. M^M-Bnit iiiii amfyili

000293

L»b M»rnci

QC Rtywt NO(

COMPOUND(((•Phenoldi-2-NUrophenol

. dj-Nltrobenitnt

-J

tit-Benzened.-1 ,2-D<ch1orotlh*r»tdg-To1utn»

-L2.L.AJLJL2»AA10,LL\2-VLLL!1-l«.111:'»-2£-

g-H*phthtl<ne*••

CASf COMPOUND NAME

•

•

,,i.i., „„„„ „....„., .n,,

•

Fftrtlon

Af^-,,..Add

I/A.,..B/H

W"V&A

VOA

Pnictlcel

Cooc. y^"6 "

, , i ,r,(^ i<^•^/'» ..-..„/, a...

. •1-/ .

% MAXllTK.Mua Mfttchi

.

•

———1

—»^.,.. '••—" 1 ^•r r-" ^Sunox^iftr^

SpikeAd3ed(ujg^.. /Co

/PP.,,,,,

/OO/ o o

Jo^0

^e

•mi Scorfc AnaJm^ntRo<fllnfti

^r—Recovery

^S^IJ -•-'

———————^^

^1 .„

^2.

9r?r

./<rr

000294

,.... . .^s^.W^^T^^^^3^.to^.^.n£y*7^INORGftNIdS TOIFETC fiEpigRgi

^@.s^^<(?^On4^^^ShtpTo?^ ..;J;^^-.....^•T——.'RunOl^ifc'ff.Ir^.r.' i ' -g»w Jiswg»B£ i»i ^ - a; yL;;.

a'LjilL^^-aK.-t •i**'*'^»*'»-*"*"-••••• -i-^"*-^ •' KrtmaVBV^V it- —— - . - -. ^y>F. w^^ •' ' F r-J^nr ^^ jr" <^:^^^WT^—— -^"1-^

^ Ri gwinlOfe - >/?/^. ^fiJ Q Shipping Inbrmatioii:

'-^'f^^. i^"-,^.,.(Nama) S^^-^ i ^ M ———c^w, , ,^.,,,-f..,—(Phono» Lii±L2^3^^2LSffiupling Dal» ,

ffl«g«)^^-SZ<Endl.,^-M

^)Doa?^bcxio(San^Lanfian[(^NtoAVdumoLwrfOoSMi

I^^TXfA^ &^rS Cw^n^J Tcafel62 .- - • t • • - ' -AA- /»»,l i r^(, , ^ ^•

^r€ J^*n(^ A:&j^&^:c'^ 5 e: ;*p, y •• /i » TI ££_ "

fcUTCHES 6ftGW5<3»Ate HO L-21H

RBQlONAL TKEFnJEOOPY .:^: -

000295

^ ^U.S. ELSVlRO^^U.NiAL-PROTECnON AGENCY - HWI Sample Mana^moil OHicsP.O. 5ox 3 1 S - Alexandria, Virginia 22313 - 793/ 557-2a90/rrS-3-537-2<!°0

INORCAN1C5 ANALYSIS DATA SHEET585-1/3

LAS

LAS

i.2-3.^.

^6,7.8.9.

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SAMPL5 ID

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000297

000298

000299

000300

000301

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(2) Sample Type: (Check One)

Sample Site Name /Code:Xn^LU&Ls

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MAfi 3 0 1981

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