phase ii environmental site assessment · 1 introduction . 1.1 purpose . atc was contracted by...

Phase II Environmental Site Assessment

J&B International Trucks ATC Project No. 280EM00043

Prepared for People’s United Bank, N.A. Ms. Lisa Overton 2 Burlington Square Burlington, Vermont April 20, 2016

Phase II Environmental Site Assessment

J&B International Trucks 964 Hercules Drive Colchester, Vermont ATC Project No. 280EM00043

Phase II Environmental Site Assessment J&B International Trucks

April 20, 2016 ATC ii

Document Information Prepared for People’s United Bank, N.A. Project Name J&B International Trucks File Reference Peoples United_JB International_Ph II Rpt.docx Job Reference ATC Project No. 280EM00043 Date April 20, 2016

Contact Information ATC Group Services LLC 171 Commerce Road Williston, Vermont 05495 Telephone: 802.862.1980 Facsimile: 802.862.1405 www.atcgroupservices.com

Document Control

Version Date Author Author Initials Reviewer Date Reviewer

Initials

Draft 4/19/2016 Adam Forman af Robert Montgomery 4/19/2016 rm

© ATC 2015. Copyright in the whole and every part of this document belongs to ATC and may not be used, sold, transferred, copied or reproduced in whole or in part in any manner or form or in or on any media to any person other than by agreement with ATC.

This document is produced by ATC solely for the benefit and use by the client in accordance with the terms of the engagement. ATC does not and shall not assume any responsibility or liability whatsoever to any third party arising out of any use or reliance by any third party on the content of this document.


April 20, 2016 ATC iii

Executive Summary ATC Group Services LLC (ATC) was retained by People’s United Bank, N.A.(Client) to perform a Phase II Environmental Site Assessment (ESA) at 964 Hercules Drive, Colchester, Vermont (herein referred to as “the property”). A previous Transaction Screen was completed at the property in 2016 that identified potential environmental concerns (PECs). The PECs identified at the property included potential soil and groundwater contamination associated with former waste oil underground storage tanks (USTs), significant staining throughout the truck repair shop, stained soils and petroleum odor in the vicinity of the diesel fuel dispenser, and an existing onsite 10,000-gallon diesel fuel UST.

Based on the findings of the Transaction Screen, additional investigation work was recommended at the property. ATC prepared a Proposal for Environmental Consulting Services dated February 26, 2016, which was approved by People’s United Bank, N.A. The objective of the investigation included evaluation of the following:

1. A file review with the Vermont Department of Environmental Conservation (VT DEC) to determine if any additional information was available regarding the former waste oil USTs and/or onsite contamination. In addition, ATC attempted to identify compliance documentation regarding the existing 10,000-gallon diesel UST.

2. A subsurface investigation to further define the degree and extent of potential subsurface contamination at the property.

The following summarizes conclusions from this investigation.

1. A file review for the hazardous waste site number 90-634, J&B International located at 964 Hercules Drive, did not indicate additional subsurface investigation work has been conducted since 2001. According to the VT DEC, the site is an active site with subsurface contamination and the previous investigation work no longer meets modern investigation standards.

2. ATC confirmed with the VT DEC, the existing diesel fuel UST is in compliance with the State. Appropriate testing documentation was provided by the VT DEC and the property owner. ATC did not conduct additional tank tightness testing services based on the findings of the UST compliance records search.

3. ATC utilized a private utility locator to locate buried utilities and clear proposed boring locations. Due to buried power lines approximately 17 inches below ground surface in the area of the observed surface soils staining near the fuel dispenser, the boring SB-2 was moved approximately 2.5 feet further south.

4. Eight soil borings were advanced on the property, and four of the borings were completed as temporary groundwater monitoring wells. Field screening of the soils during the boring advancement did not identify VOC impacted soils. This included screening the soils in SB-2 which was located approximately 2.5 feet south of the observed surface staining from the fuel dispenser.

5. Soil samples were collected from five of the borings and submitted for laboratory analysis of VOCs, SVOCs, RCRA 8 Metals, and TPH-DRO. The results indicated arsenic exceeded the Vermont Soil Screening Values (SSVs); however, the results were below the commonly accepted background arsenic in soil concentration in Vermont. The remaining results were below applicable screening values. PCE was identified in one soil sample (SB-2) and MEK was identified in a soil sample (SB-8); however, both results were below the appropriate screening values. The soil sampling near the former waste oil USTs did not indicate the presence of fuel or chlorinated VOCs.

6. Groundwater samples were collected from the four temporary monitoring wells and submitted for laboratory analysis of VOCs, SVOCs, RCRA 8 Metals, and TPH-DRO. The results indicated vinyl chloride exceeded the VT GWES in sample MW-3 which is located near the existing diesel fuel UST. Additionally, sample results indicated arsenic, chromium, and lead concentrations exceeded the VT GWES. The remaining analytes were below laboratory reporting limits or below applicable enforcement


April 20, 2016 ATC iv

standards. The sample collected near the former waste oil USTs (MW-7) indicated the presence of TCE at a concentration that was below the VT GWES.

7. The soil and groundwater sampling results indicate chlorinated VOCs at low concentrations are located in the vicinity of the diesel fuel UST and associated dispenser, and the former waste oil USTs. Only one chlorinated compound in the groundwater near the diesel fuel UST exceeded the applicable enforcement standard or screening value.

Based on the findings of this Phase II ESA, ATC offers the following recommendations.

> ATC recommends a copy of this report be forwarded to the VT DEC. The groundwater monitoring wells from 2001 in the vicinity of the former waste oil USTs should be located, inspected and sampled. The property owner should work with the VT DEC to perform appropriate assessment activities at the property to protect human health and the environment.


April 20, 2016 ATC v

Table of Contents Executive Summary ........................................................................................................................... iii 1 Introduction ................................................................................................................................ 1

1.1 Purpose ........................................................................................................................................... 1 1.2 Background Review ........................................................................................................................ 1

2 File Review ................................................................................................................................. 2 2.1 Historical Waste Oil USTs ............................................................................................................... 2 2.2 Existing Fuel Oil UST ...................................................................................................................... 2

3 Phase II Investigation Activities ................................................................................................ 3 3.1 Property Preparation ....................................................................................................................... 3 3.2 Private Utility Locator ...................................................................................................................... 3 3.3 Drilling Activities .............................................................................................................................. 3 3.4 Soil Sample Field Screening Results .............................................................................................. 4 3.5 Soil Sample Results ........................................................................................................................ 4 3.6 Groundwater Sample Results ......................................................................................................... 5

4 Conclusions and Recommendations ....................................................................................... 6 4.1 Conclusions ..................................................................................................................................... 6 4.2 Recommendations .......................................................................................................................... 6

5 Qualifications ............................................................................................................................. 7

Figures

Figure 1 Site Vicinity Diagram

Figure 2 Boring Location Diagram

Tables

Table 1 Soil Boring Soil Sample Results

Table 2 Groundwater Sample Results

Appendices

Appendix A File Review Documentation

Appendix B Boring Logs

Appendix C Soil and Groundwater Laboratory Report


April 20, 2016 ATC 1

1 Introduction

1.1 Purpose ATC was contracted by People’s United Bank, N.A. (People’s) (the Client) to conduct a file review and subsurface investigation activities at the J&B International Trucks facility located at 964 Hercules Drive in Colchester, Vermont (the site). A Property Plan is included as Figure 1. Based on the Request for Proposal for the JB International property, which was prepared by Lender Consulting Services, Inc. (LCS) for the People’s United Bank, N.A., ATC prepared a Proposal for Environmental Consulting Services dated February 26, 2016.

1.2 Background Review The property is a 6.97 acre parcel of land that is developed with a two-story 17,600 square foot building utilized for truck sales and services. The property is an active Vermont Hazardous Waste site identified as site number 90-634. A Subsurface Investigation and Groundwater Monitoring Report from 2001 indicated that contamination was discovered in the vicinity of waste oil USTs removed from the property. The first waste oil UST was removed in 1990 and a limited investigation was conducted at that time. A new waste oil UST was installed in the same location, which was later removed in 2000. A soil investigation in 2000 revealed soil contamination that was presumed to be from the UST that had been removed in 1990. The report identified tetrachloroethylene (PCE) in the soil and groundwater that were below the applicable regulatory guidelines at that time.

A Transaction Screen was completed at the property in 2016 that identified potential environmental concerns (PECs). The identified PECs included potential soil and groundwater contamination associated with the former waste oil USTs, significant staining throughout the truck repair shop, and stained soils and a petroleum odor in the vicinity of the diesel fuel dispenser. In addition, a 10,000-gallon diesel fuel UST is located on the property.

People’s requested proposals for additional investigations at the property. ATC provided a Proposal for Environmental Consulting Services dated February 26, 2016, and the following work was completed in accordance with the proposal except where described.



2 File Review

2.1 Historical Waste Oil USTs Based on the findings of the Transaction Screen, the property previously had two waste oil USTs that were located on the southern side of the building. Soil and groundwater contamination was reportedly identified in a 2001 Subsurface Investigation and Groundwater Monitoring report. No additional information regarding the waste oil USTs or the subsurface contamination was readily available.

ATC contacted Mr. Gerold Noyes of the VT DEC, in order to identify additional information regarding potential soil and groundwater impacts from the historical waste oil USTs (VT DEC Site Number 90-634). Based on communication with Mr. Noyes, the latest correspondence with the property owners was from 2001, and the property is an active site with subsurface contamination. The degree and extent of contamination has not been defined, and the earlier subsurface investigation no longer meets more modern standards. No additional information was available from the VT DEC.

2.2 Existing Fuel Oil UST ATC conducted a review of VT DEC and J&B International Trucks files to determine if compliance documentation for the 10,000-gallon diesel fuel UST was available. ATC spoke with Ms. Sue Thayer, of the VT DEC Underground Storage Tank Program, who confirmed the presence of a 10,000-gallon diesel UST identified as Tank identification number 1988-1, and Site identification number 1133. The UST was issued a State Permit on May 22, 2014 which will expire on June 1, 2019. The State conducts inspections of USTs at a minimum of every three years which is a federal requirement. The most recent State inspection was conducted on July 2, 2014. Ms. Thayer stated the cathodic protection on the tank was upgraded in 2009, and annual testing of the cathodic protection has been conducted including the most recent testing on September 11, 2015. Documentation of the testing is provided in Appendix A. Ms. Thayer stated the UST was in compliance with the VT DEC UST Program.

ATC spoke with Mr. Bill Cleary of J&B International Trucks, who confirmed they conduct daily inspections of the UST system. The tank contents are measured daily, the interstitial space of the UST is measured weekly, and the cathodic protection system is inspected monthly. The most recent documentation of the inspections is provided in Appendix A.

Based on the observed and reported compliance documentation, ATC determined the UST was in compliance and UST tightness testing was not required as part of this investigation.



3 Phase II Investigation Activities

3.1 Property Preparation Prior to the initiation of the investigation activities, ATC prepared a property-specific Health and Safety Plan (HASP) in accordance with the Occupational Safety and Health Administration (OSHA) Standard “Hazardous Waste Operations and Emergency Response” guidelines (29 CFR 1910.120). The HASP was reviewed and signed by ATC personnel and their subcontractors prior to performing work at the property. The HASP detailed the potential exposures and risks associated with each on-property activity and the actions necessary to minimize potential exposure.

3.2 Private Utility Locator On March 24, 2016, ATC utilized a private utility locator, Vermont Underground Locators (VUL), and contacted DigSafe (#2016-1209224) to identify buried utilities that could be impacted by drilling activities on the site. A majority of the buried utilities were identified on the northeastern side of the property. Parking lot light poles were observed throughout the property, and the buried power lines for the light poles were identified and marked.

The UST piping and associated power lines were identified. Some of the power lines were identified to be approximately 17 inches below ground surface on the southwestern corner of the dispenser island. This is the location of the identified surface soil staining from the dispenser drippings. Therefore, ATC had to move the proposed boring location (SB-2) further to the south and away from buried utilities. As will be discussed further in Section 3.3, the soil boring SB-2 is located approximately 2.5 feet south of the observed surface staining.

This investigation cleared proposed drilling locations and did not identify subsurface utilities in the areas designated for drilling activities on the site.

3.3 Drilling Activities On March 30, 2016, ATC conducted boring and temporary groundwater monitoring well installation activities at the site utilizing ENPRO Services, Inc. of Burlington, VT. Utilizing a track mounted drilling rig with direct push rods, borings were advanced in eight locations. Four of the borings (SB-1, SB-3, SB-5 and SB-7) were completed as groundwater monitoring wells. The borings were advanced utilizing direct push rods and four foot Macro-core® soil samples were collected continuously in the borings. The first five feet of each boring was hand augured in order to reduce the likelihood of damaging buried utility lines. ATC field screened the soils from the borings for the presence of VOCs using a Photoionization Detector (PID). Boring locations are presented in Figure 2. Boring logs are included in Appendix B.

Groundwater was encountered in each boring at approximately four feet below ground surface (bgs). Four soil borings were completed as temporary groundwater monitoring wells, constructed of 1-inch inside diameter (ID) Schedule 40, flush threaded polyvinyl chloride (PVC) riser pipe with an end plug. The well screen was 1-inch ID Schedule 40 flush threaded PVC with 0.010-inch slots. The temporary monitoring wells were set to a depth of 12-feet bgs. With the well screen in place, clean filter sand was installed from the bottom of the boring to a minimum of 1 foot above the top of the well screen. A one foot bentonite chip seal was placed above the sand pack.

The monitoring wells were developed through bailing techniques to remove cuttings, clean the well screens, and improve the hydraulic connection between the well screen and formation material. After groundwater samples were collected from the monitoring wells, the wells were abandoned by removing the PVC and the void was filled with bentonite chips.



3.4 Soil Sample Field Screening Results On March 30, 2016 during boring activities, soil samples were screened in the field for volatile organic compounds (VOCs) using a portable photo-ionization device (PID) MiniRAE 2000 Model PGM-7600 calibrated with Isobutylene. ATC also utilized visual and olfactory evidence for identifying potential petroleum contamination. The soil descriptions and PID results are presented in the boring logs in Appendix B.

A summary of field screening results indicated VOCs were not detected in the eight borings. This included the soil screening in boring SB-2 which was located approximately 2.5 feet south of the observed surface soil staining from the fuel dispenser. The soil screening results indicate the surface staining appears to be relatively contained to a small area near the dispenser. As will be discussed in Section 3.5, a soil sample was collected from soils between approximately 1.5-3 feet in this boring and submitted for laboratory analysis.

3.5 Soil Sample Results On March 30, 2016, ATC collected soil samples for laboratory analysis from five soil borings SB-2, SB-3, SB-6, SB-7 and SB-8. The samples were submitted for laboratory analysis of VOCs via EPA Method 8260, SVOCs via EPA Method 8270, RCRA 8 Metals, and TPH-DRO via EPA Method 8015. The soil samples were collected in properly preserved and pre-cleaned sampling containers that were provided by the laboratory. ATC also submitted a duplicate soil sample to be analyzed for VOCs for quality assurance/quality control purposes. The samples were submitted to TestAmerica of Buffalo, New York.

As discussed in Section 3.4, the field screening conducted during soil borings advancement did not identify VOCs in the soils. Therefore, ATC selected soils from varying depths in the borings to be analyzed by the laboratory. A soil sample was collected from boring SB-2 located near the fuel dispenser island, at a depth of approximately 1.5-3 feet bgs. A soil sample was collected from boring SB-3 at a depth of approximately 4-7 feet bgs. A soil sample was collected from boring SB-5 at a depth of approximately 4-5 feet bgs. A soil sample was collected from boring SB-6 at a depth of approximately 6-8 feet bgs. A soil sample was collected from boring SB-7 at a depth of approximately 8-10 feet bgs, which appeared to be the native soils beneath the former UST grave. A soil sample was collected from boring SB-8 at a depth of approximately 4-8 feet bgs.

The results of the soil sampling indicated the detectable presence of several metals and VOCs. The metals detected were relatively consistent throughout the five samples. Arsenic exceeded the Vermont Soil Screening Value (SSV) for Industrial Soils in each of the samples, and the concentrations ranged from 2.7 to 5.0 mg/kg. However, the commonly accepted background concentration of arsenic in soils in Vermont is 10 mg/kg or less. Therefore, based on the consistent concentration reported throughout the site and the concentrations below 10 mg/kg, the arsenic findings are considered to be background concentrations and do not indicate a release. The remaining metals in soil results which included chromium, lead, and mercury were well below applicable guidance values.

The soil sample results for VOCs indicated the detectable presence of several analytes that were below applicable guidance values. Soil boring SB-2 which is located near the fuel dispenser island, indicated the detectable presence of tetrachloroethene (PCE), but the concentration was J-flagged and below the Vermont Department of Health (VDH) Value which supersedes the SSV value. The J-flagged value was noted by the laboratory which indicates the concentration is an estimated value below the Reporting Limit, but greater than the Method Detection Limit. Soil boring SB-8, which is located on the western side of the property building, indicated the detectable presence of 2-Butanone (MEK), but the concentration was J-flagged and well below the VDH Value. The remaining VOCs were well below the SSV, and were common laboratory contaminants.

The laboratory did not report detectable concentrations of SVOCs or TPH-DRO in any of the soil samples.

ATC collected a duplicate sample in boring SB-7 for QA/QC purposes. The result of the duplicate sample did not indicate the detectable presence of VOCs. The results for SB-7 indicated the presence of one analyte at a concentration that was J-flagged and was a very low concentration. The relative percent difference (RPD) could not be calculated because no duplicate analytes were present in both samples. The duplicate soil sample



results did not appear to negatively affect the usability of the results. The laboratory results are provided in Appendix C.

3.6 Groundwater Sample Results On March 30, 2016, ATC collected groundwater samples from the temporary monitoring wells installed in SB-1/MW-1, SB-3/MW-3, SB-5/MW-5, and SB-7/MW-7. The groundwater samples were collected utilizing a disposable bailer, and the water samples were properly preserved in pre-cleaned glassware and kept chilled until analysed. The samples were submitted for laboratory analysis of VOCs via EPA Method 8260, SVOCs via EPA Method 8270, RCRA 8 Metals, and TPH-DRO via EPA Method 8015 at TestAmerica of Buffalo, New York. ATC also submitted a field blank and a duplicate sample to be analysed for VOCs for quality assurance/quality control purposes.

The depth to groundwater was measured in each monitoring well on March 30, 2016, using a groundwater interface probe. The measured depth to water ranged from 3.98 to 4.55 feet below ground surface. The well top of casing elevations were not measured as part of this scope of work and the groundwater flow direction was not measured. However, based on the surface topography and previous subsurface investigations, the groundwater flow direction is likely toward the southeast.

The results of the groundwater sampling indicated the detectable presence of VOCs, SVOCs, metals and TPH-DRO.

The VOC results reported chlorinated compounds in wells MW-3 and MW-7. Vinyl chloride was reported in the water sample from MW-3 at a concentration of 2.6 µg/L, which exceeds the Vermont Groundwater Enforcement Standard (VT GWES) of 2.0 µg/L. The remaining VOCs in well MW-3 were below the VT GWES or did not have a guidance value. The temporary monitoring well MW-3 was located adjacent to the existing diesel UST. Trichloroethene (TCE) was reported in well MW-7 at a concentration that was below the VT GWES. None of the remaining VOCs that were above the reporting limit were above the VT GWES. The temporary monitoring well MW-7 was located near the location of the former waste oil USTs.

The SVOC results reported several analytes that were J-flagged. The SVOCs were below applicable VT GWES, or did not have a comparison standard. TPH-DRO was reported in three of the water samples at concentrations that were J-flagged. Vermont does not have a comparison standard for TPH-DRO in groundwater; however, based on the low values that were J-flagged, and the reported VOC results, the TPH-DRO results do not indicate a significant threat to human health or the environment.

The metals results indicate the same three analytes, arsenic, chromium, and lead, exceeded the VT GWES in all four samples. The same analytes were reported in the soil samples which were determined to be background concentrations or below applicable guidance values. In addition, the groundwater sample collected from MW-1 which was the upgradient well sample indicated similar or higher concentrations than the downgradient samples collected from the remaining three water samples. Mercury was detected in two of the groundwater samples from MW-3 and MW-7; however, the concentrations were below the VT GWES.

The groundwater duplicate sample was collected from MW-5 for QA/QC purposes. The results from the groundwater sample MW-5 and the duplicate sample indicated carbon disulfide was present at concentrations that were J-flagged, and the calculated RPD is less than 20%. Additionally, the duplicate indicated the presence of acetone at a concentration that was J-flagged. Based on the very low concentrations, the RPD cannot effectively be calculated. The duplicate sample results do not appear to negatively affect the usability of the data. A field blank sample was collected and analysed for VOCs. The results indicated a low concentration of toluene. None of the other water samples indicated the presence of toluene, which indicates the field blank water source was tainted with toluene. The field blank sample does not appear to negatively affect the usability of the data.

A hardcopy of laboratory results are included as Appendix C.



4 Conclusions and Recommendations

4.1 Conclusions Based on the results of the activities conducted at the J&B International Trucks facility located at 964 Hercules Drive, in Colchester, Vermont, ATC presents the following conclusions:

• A file review for the hazardous waste site number 90-634, J&B International located at 964 Hercules Drive, did not indicate additional subsurface investigation work has been conducted since 2001. According to the VT DEC, the site is an active site with subsurface contamination and the previous investigation work no longer meets modern investigation standards.

• ATC confirmed with the VT DEC, the existing diesel fuel UST is in compliance with the State. Appropriate testing documentation was provided by the VT DEC and the property owner. ATC did not conduct additional tank tightness testing services based on the findings of the UST compliance records search.

• ATC utilized a private utility locator to located buried utilities and clear proposed boring locations. Due to buried power lines approximately 17 inches below ground surface in the area of the observed surface soils staining near the fuel dispenser, the boring (SB-2) was moved approximately 2.5 feet further south.

• Eight soil borings were advanced on the property, and four of the borings were completed as temporary groundwater monitoring wells. Field screening of the soils during the boring advancement did not identify VOC impacted soils. This included screening the soils in SB-2 which was located approximately 2.5 feet south of the observed surface staining from the fuel dispenser.

• Soil samples were collected from five of the borings and submitted for laboratory analysis of VOCs, SVOCs, RCRA 8 Metals, and TPH-DRO. The results indicated arsenic exceeded the VT SSVs; however, the results were below the commonly accepted background arsenic in soil concentration in Vermont. The remaining results were below applicable screening values. PCE was identified in one soil sample (SB-2) and MEK was identified in a soil sample (SB-8); however, both results were below the appropriate screening values. The soil sampling near the former waste oil USTs did not indicate the presence of fuel or chlorinated VOCs.

• Groundwater samples were collected from the four temporary monitoring wells and submitted for laboratory analysis of VOCs, SVOCs, RCRA 8 Metals, and TPH-DRO. The results indicated vinyl chloride exceeded the VT GWES in sample MW-3 which is located near the existing diesel fuel UST. Additionally, sample results indicated arsenic, chromium, and lead concentrations exceeded the VT GWES. The remaining analytes were below laboratory reporting limits or below applicable enforcement standards. The sample collected near the former waste oil USTs (MW-7) indicated the presence of TCE at a concentration that was below the VT GWES.

• The soil and groundwater sampling results indicate chlorinated VOCs at low concentrations are located in the vicinity of the diesel fuel UST and associated dispenser, and the former waste oil USTs. Only one chlorinated compound in the groundwater near the diesel fuel UST exceeded the applicable enforcement standard or screening value.

4.2 Recommendations ATC offers the following recommendations based on the results of the subsurface investigation:

• ATC recommends a copy of this report be forwarded to the VT DEC. The groundwater monitoring wells

from 2001 in the vicinity of the former waste oil USTs should be located, inspected and sampled. The property owner should work with the VT DEC to perform appropriate assessment activities at the property to protect human health and the environment.



5 Qualifications

The work performed in conjunction with this assessment, and the data developed, are intended as a description of available information at the dates and locations given. The passage of time may result in a change in the environmental characteristics at this property and surrounding properties. This report does not warrant against future operations or conditions, nor does it warrant operations or conditions present of a type or at a location not investigated. The conclusions drawn from this investigation are considered reliable; however, localized variations in subsurface conditions may exist that have not been completely defined at this time.

Our professional services have been performed, our findings obtained, and our recommendations prepared in accordance with customary principles and practices in the fields of environmental science and engineering. This warranty is in lieu of all other warranties either expressed or implied. ATC is not responsible for the independent conclusions, opinions, or recommendations made by others based on the results and designs presented in this report.

The passage of time may result in a change in the environmental characteristics at this property and surrounding properties. This report does not warrant against future operations or conditions, nor does it warrant operations or conditions present of a type or at a location not investigated.

It must be noted that no investigation can absolutely rule out the existence of any hazardous materials at a given property. This assessment has been based upon prior property history. Existing hazardous materials and contaminants can escape detection using these methods. If a higher level of confidence is required than can be defined by this scope of work, then additional investigation would, of course, be required.

Thank you for considering ATC for your environmental management needs. If you have any questions feel free to contact us at 802 862-1980.

Respectfully Submitted,

ATC Group Services LLC

Adam Forman Robert Montgomery Project Geologist Senior Project Manager for ATC Group Services LLC for ATC Group Services Direct Line +1 802.862.1980 Direct Line +1 802.862.1980 Email: [email protected] Email:[email protected]



J&B International Trucks

FIGURES

171 Commerce Street PO Box 1486

Williston, VT 05495 Phone (802) 862-1980

Fax (802) 862-1405

ATC Project #: 280EM00043 Project Location: J&B International Trucks 964 Hercules Drive Colchester, Vermont

Drawn by: AF Field Work by: AF Checked by: TB Date: April 2016

Site Vicinity

Diagram

Property

Property Property

Boring Location DiagramJ&B International Trucks

964 Hercules DriveColchester, Vermont

280EM00043

AF

4/18/16

Figure 2171 Commerce Street, P.O Box 1486

Williston, VT 05495Ph. (802)862-1980

Proj No.

Proj. Mgr.

Date

SB-1/MW-1

SB-3/MW-3

SB-7/MW-7

SB-5/MW-5

SB-2

SB-4

SB-6

SB-8

Legend

Soil Boring Location

Soil Boring/Temporary Monitoring Well Location

Fuel Dispenser Island

Former Waste Oil USTs

Existing Diesel UST




TABLES

Table 1Soil Boring Soil Sample Results

Phase II ESAColchester, Vermont

ATC Project No. 280EM00043

Sample No. Analysis Element Result (mg/kg)VT SSV Industrial Soil

(mg/kg)

SB-2Metals

Arsenic 5 1.6*Barium 21 190,000Chromium 11 103**Lead 7.1 800Mercury 0.012 J 5.69**

VOCsMethyl acetate 0.049 J 1,000,000Methylene Chloride 0.092 B 53Tetrachloroethene 0.033 J 0.8**

SVOCsNone Detected

TPH-DRONone Detected

J -flagged value is an estimated value between the MDL and PQL. B - flagged compound was found in the blank and sample.* Commonly Accepted Background Concentrations of Arsenic in soil in Vermont is 10-12 ppm. ** Vermont Department of Health Value that supercedes the SSV ValueVT SSV - Vermont Soil Screening Values


(mg/kg)

SB-3Metals

Arsenic 4.3 1.6*Barium 16 190,000Chromium 10 103**Lead 4.1 800Mercury 0.012 J 5.69**

VOCsMethyl acetate 0.24 1,000,000Methylene Chloride 0.031 JB 53

SVOCsNone Detected


J-flagged value is an estimated value between the MDL and PQL.* Commonly Accepted Background Concentrations of Arsenic in soil in Vermont is 10-12 ppm. ** Vermont Department of Health Value that supersedes the SSVVT SSV - Vermont Soil Screening Values





(mg/kg)

SB-6Metals

Arsenic 4.9 1.6*Barium 15 190,000Chromium 10 103**Lead 3.8 800

VOCsAcetone 0.0072 JB 630,000Methylene Chloride 0.0035 JB 53

SVOCsNone Detected




(mg/kg)

SB-7Metals

Arsenic 2.7 1.6*Barium 18 190,000Chromium 7.6 103**Lead 3.7 800

VOCsMethylene Chloride 0.0033 JB 53

SVOCsNone Detected







(mg/kg)

SB-8Metals

Arsenic 3.9 1.6*Barium 31 190,000Cadmium 0.049 J 34.5**Chromium 14 103**Lead 11 800Mercury 0.032 5.69**

VOCs2-Butanone (MEK) 0.0083 J 40,400**Acetone 0.043 B 630,000Methylene Chloride 0.0028 JB 53

SVOCsNone Detected



Table 2Groundwater Sample Results

J B International Trucks964 Hercules DriveColchester, Vermont


Sample No. Analysis Detected Element Result (ug/L) VT GWES (ug/L)

MW-1VOCs

Acetone 4.7 J 700Carbon disulfide 0.24 J NA

SVOCsDi-n-butyl phthalate 0.51 J NAPhenol 0.45 J 2,100

MetalsArsenic 280 10Barium 1500 2,000Cadmium 3.3 J 5Chromium 320 100Lead 260 15

J-flagged value is an estimated value between the MDL and PQL. B - flagged compound was found in the blank and sample.NA - Not availableVT GWES - Vermont Groundwater Enforcement StandardShaded Value indicates exceedance of VT GWES


MW-3VOCs

Acetone 5.8 J 700Carbon disulfide 0.46 J NAcis-1,2-Dichloroethene 1.7 NAVinyl chloride 2.6 2

SVOCsBenzaldehyde 2.8 JB NADiethyl phthalate 1.6 J NA

MetalsArsenic 94 10Barium 590 2,000Cadmium 1.6 J 5Chromium 270 100Lead 210 15Mercury 0.36 2

TPH-DRODRO 460 J NA


Table 2Groundwater Sample Results

J B International Trucks964 Hercules DriveColchester, Vermont



MW-5VOCs

Carbon disulfide 0.43 J NA

SVOCsBenzaldehyde 2.7 JB NA

MetalsArsenic 110 10Barium 670 2,000Cadmium 1.1 J 5Chromium 320 100Lead 190 15

TPH-DRODRO 460 J NA



MW-7VOCs

Acetone 4.2 J NATrichloroethene 1.1 5

SVOCsBenzaldehyde 2.5 JB NA

MetalsArsenic 85 10Barium 520 2,000Cadmium 0.73 J 5Chromium 280 100Lead 210 15Mercury 0.24 2

TPH-DRODRO 320 J NA



April 20, 2016 ATC 10


APPENDIX A FILE REVIEW DOCUMENTATION

1

Noyes, Gerold

From: Noyes, GeroldSent: Thursday, February 18, 2016 12:24 PMTo: 'Overton, Lisa'Subject: RE: 964 Hercules Drive, Colchsester.

Good afternoon Ms. Overton, Please see the attached files regarding the 964 Hercules Drive site in Colchester. This is an active site. There is contamination on site. The degree and extent have not been determined. The last correspondence is from 2001. Please be aware that the earlier letter from 1991 references investigation that no longer meets more modern standards. No response was received from Mr. Cleary. I cannot review regulatory files for your client. The SMS advises that a Phase 1 Environmental Site Assessment according to ASTM standards be performed prior to commercial property transactions and that a Phase 2 ESA be performed if necessary. Gerold Noyes, PE

Department of Environmental Conservation Sites Management Section 1 National Life Drive ‐ Davis 1 Montpelier, VT 05620‐3704 [email protected] (the e‐mail address formerly known as [email protected]) 802‐522‐5614

From: Overton, Lisa [mailto:[email protected]] Sent: Wednesday, February 17, 2016 9:46 AM To: Noyes, Gerold <[email protected]> Subject: 964 Hercules Drive, Colchsester. Hi Gerold, We recently engaged ATC Group Services, LLC to complete an enhanced transaction screen on 964 Hercules Drive in Colchester. I see from the DEC’s website that you are the DEC contact for this site. ATC is recommending the following. In an effort to reduce the cost to my Borrower for further investigation, can you provide any addition information that would satisfy these requirements?

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Please call or email, whichever you prefer. Many thanks, Lisa C. Overton Senior Vice President Commercial Banking People's United Bank, N.A. P.O Box 820 2 Burlington Square Burlington, VT 05401 Direct (802) 660-2209 Fax (802) 862-0240 [email protected]

The security, delivery, and timeliness of delivery of electronic mail sent over the Internet is not guaranteed. Most electronic mail is not secured. Do not send us confidential information like social security numbers, account numbers, or driver's license numbers by electronic mail. The information transmitted is intended solely for the individual or entity to which it is addressed and may contain confidential, proprietary, and/or privileged material. Any review, re-transmission, dissemination, or other use of or taking action in reliance upon this information by persons or entities other than the intended recipient is prohibited. If you have received this e-mail in error, please contact the sender and delete the material from the computer.

9/15/2015

UST Corrosion Compliance Services LLC 301 Route 106

Reading, VT 05062 Tel: 802-484-5036 *Fax: 802-484-9558

Email: [email protected]

Attn: Stephanie Mangan-Office Manager J&B Leasing 964 Hercules Drive Colchester, VT 05446

SEP 1 6 2015

RE: Results of annual survey; Cathodic Protection, Underground Storage Tank; Site ID# 1133, J&B Leasing 964 Hercules Drive, Colchester VT. 1 - lOK Diesel tank.

Dear Stephanie:

On Friday September 11th, 2015 we visited the above subject site.

The purpose of the visit was to conduct the annual survey required under current regulations of the impressed current cathodic protection system for your underground storage tank.

The results were excellent and demonstrated that the protection has been restored to this tank in accordance with the NACE International Standard, SP0285-2011, "Corrosion Control of Underground Storage Tank Systems by Cathodic Protection"

Attached is a sketch and complete copy of field data which reflects the above performance.

As discussed and agreed upon, we have also sent a report marked "Copy" directly to the Vermont DEC Attn: Ms. June Reillv

If you have any questions please let us know.

Kind Regards,

Ian Lynch NACE CP Tester Certification # 00009729

Enclosures cc: FJ Lynch, P.E.

Cathodic Protection Survey

Company: J & B Leasing Plant: Garage and UST Facility ID # 1133 Location: Colchester, Vermont.

Post Upgrade Operational & Effectiveness CP Survey.

Note: All Vg readings are shown in millivolts with respect to a portable CuCuSo4 reference electrode unless a PRC is specified and the polarity reflects the structure connected to the VM "negative".

Polarization will be measured during "follow up" survey within six months.

See separate sketch for test point locations.

Survey conducted by F.J. Lynch, P.E. & LT.Lynch, CP Tester (NACE)

System commissioned at 06:00 pm 5/29/2009 9/28/09 Survey Conducted by Ian Lynch, NACE CP Tester 9/15/10 survey conducted by FJ Lynch, P .E. & IT Lynch NACE 9/15/11 Survey conducted by FJ Lynch, P .E. & I Lynch, NACE 9/6/12 survey conducted by FJ Lynch, P.E. & I Lynch, NACE 9/6/13 survey conducted by Ian Lynch, NACE

9/3/14 survey conducted by FJ Lynch, P.E. & Ian Lynch, NACE 9/11/15 survey conducted by FJ Lynch, P.E. & Ian Lynch, NACE

Survey Dates: 09/11/15 Test Point "Native" Potentials Tank Current Va.

Location No. In MV 6129/09 Milliamos I On Tank 1/01 785 56 1220

Tank 1/02 804 56 1253

Tank 1/03 803 56 1283

UST Corrosion Compliance Services LLC

Rectifier Readings 9/11/2015

Rm. Volts 3.00

Rm. Milliamps. 0.06

Settinas 8%Nariac) DMMVolts 2.64 DMMMV 5.60 DMM 56.00 Milliamps Anode# 1 0.00 Milliamos Anode#2 56.00 Milliamos Anode#3 Milliamos Anode#4 Milliamos Total of Anodes 56.00 milliamps Hour Meter 20201 .3 A/C Volts nr A/CAmps nr

A/C watts nr Effv. %

millivolt Polarization I Off oerma MV 1035 3.30 250

1053 3.57 249

1028 4.55 225 ·'

J & B Leasing Hercules Drive Colchester, VT Site ID # 1133 Cathodic Protection Annual Survey- September 2015 Drawing not to scale

Garage

TP3 TP2

10K Di set Tank

0

TP • = CP Test Point

TP 1

l·--·I

lom-1

Please see attached data sheet for readings


April 20, 2016 ATC 11


APPENDIX B BORING LOGS

Hand Auger-SAND, medium and coarse, brown, moist, no odor

Saturated around 4 feet

Bottom of boring

SAND, fine and medium, trace silt, brown, saturated, no odor

CLAY, and silt, grey, wet, no odor, 9-12'

Hand Auger-Fill SAND, medium and coarse, tan, dry, noodor


Bottom of boring

Hand Auger-SAND, coarse and medium, tan/brown,saturated, no odor, 4-7.5'

Hand Auger-SAND, fine, little silt, brown, wet, no odor, 7.5-8'

SS-2 from 1.5-3 ft

Hand Auger-SAND, medium and coarse, brown, moist, no odor


Bottom of boring

SAND, fine and medium, trace silt, brown, saturated, no odor

CLAY, and silt, brown, wet, no odor, 11-12'

SAND, fine and medium, trace silt, grey, saturated, no odor, 5.5-7'

SAND, fine, little silt, grey/brown, saturated, no odor, 7-11'

SS-3 4-7 ft

Hand Auger-Fill GRAVEL with sand, medium and coarse,brown, dry, no odor


Bottom of boring

SAND, coarse and medium, red/brown, saturated, no odor,4-8'

SAND, medium and fine, little silt, grey/brown, wet, no odor,8-12'

Hand Auger-SAND, medium and coarse, with gravel, brown,moist, no odor


Bottom of boring

SAND, fine and medium, trace silt, brown, saturated, no odorSAND, fine and medium, grey with mottling, saturated, no odor,5-9'

SAND, fine, little silt, grey/brown, saturated, no odor, 9-12'

SS-5 4-5 ft

Hand Auger-SAND, medium and coarse, with gravel, brown,moist, no odor


Bottom of boring

SAND, coarse and medium, red/brown mottled, saturated, noodor, 4-8'

SAND, medium and fine, little silt, brown, saturated, no odor,8-12'

SS-6 6-8 ft

Hand Auger-Fill SAND, medium and coarse, tan, dry, noodor


Bottom of boring

SAND, coarse and medium, tan/brown, saturated, no odor,5-10'

SAND, fine, little silt, brown, wet, no odor, 10-12'

SS-7 8-10 ft

Hand Auger-Fill GRAVEL, with sand, medium and coarse,brown, moist, no odor

Saturated around 3.5 feet

Bottom of boring

SAND, fine, brown, saturated, no odor, 4-5'

SAND, medium and fine, little silt, brown, saturated, no odor,7-12'

SAND, coarse and medium, grey/brown, saturated, no odor,5-7'

SS-8 4-8 ft


April 20, 2016 ATC 12


APPENDIX C SOIL AND GROUNDWATER LABORATORY RESULTS

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Buffalo10 Hazelwood DriveAmherst, NY 14228-2298Tel: (716)691-2600

TestAmerica Job ID: 480-97480-1Client Project/Site: JB Soil & Groundwater Project

For:ATC Associates Inc.171 Commerce StreetPO BOX 1486Williston, Vermont 05495

Attn: Mr. Adam Forman

Authorized for release by:4/15/2016 1:03:49 PMAnne Pridgeon, Project Management Assistant [email protected]

Designee for

Becky Mason, Project Manager II(413)[email protected]

The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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mailto:[email protected]

mailto:[email protected]

Table of Contents

Client: ATC Associates Inc.Project/Site: JB Soil & Groundwater Project

TestAmerica Job ID: 480-97480-1

Page 2 of 82TestAmerica Buffalo

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 41

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 68

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 78

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 79

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 80

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 81

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82

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Definitions/GlossaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.

Project/Site: JB Soil & Groundwater Project

Qualifiers

GC/MS VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

* LCS or LCSD is outside acceptance limits.

B Compound was found in the blank and sample.

GC/MS Semi VOA


* RPD of the LCS and LCSD exceeds the control limits

Qualifier


B Compound was found in the blank and sample.

GC Semi VOA



Qualifier

Metals



Qualifier

^ ICV,CCV,ICB,CCB, ISA, ISB, CRI, CRA, DLCK or MRL standard: Instrument related QC is outside acceptance limits.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

TestAmerica Buffalo

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Case NarrativeClient: ATC Associates Inc. TestAmerica Job ID: 480-97480-1Project/Site: JB Soil & Groundwater Project

Job ID: 480-97480-1

Laboratory: TestAmerica Buffalo

Narrative

Job Narrative480-97480-1

Comments

No additional comments.

Receipt

The samples were received on 4/1/2016 9:45 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperatures of the 2 coolers at receipt time were 4.3º C and 4.5º C.

GC/MS VOA Method(s) 8260C: The continuing calibration verification (CCV) associated with batch 480-293918 recovered above the upper control limit

for Trichlorofluoromethane. The samples associated with this CCV were non-detects for the affected analyte; therefore, the data have

been reported. The following samples are impacted: SB-8 (480-97480-7), SB-6 (480-97480-10) and SB-7 (480-97480-11).

Method(s) 8260C: Due to the co-elution of Ethyl Acetate with 2-Butanone in the full spike solution, 2-Butanone exceeded control limits in the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) associated with batch 480-293918 . The following samples are impacted: SB-8 (480-97480-7), SB-6 (480-97480-10) and SB-7 (480-97480-11).

Method(s) 8260C: The method blank for preparation batch 480-293913 and analytical batch 480-293918 contained Methylene Chloride above the reporting limit (RL). This compound is considered a common laboratory contaminant. The associated samples, SB-8 (480-97480-7), SB-6 (480-97480-10) and SB-7 (480-97480-11), were not re-analyzed because the concentration of the common lab contaminant in the method blank was less than 5 times the RL.

Method(s) 8260C: The continuing calibration verification (CCV) associated with batch 480-294138 recovered above the upper control limit for 1,1,2-Trichloro-1,2,2-trifluoroethane, Carbon tetrachloride, Tetrachloroethene and Trichlorofluoromethane. The sample associated with this CCV was non-detect for the affected analytes; therefore, the data has been reported. The following sample is impacted: DUP

(480-97480-12).

Method(s) 8260C: The continuing calibration verification (CCV) associated with batch 480-294734 recovered outside acceptance criteria, low biased, for Cyclohexane, Carbon disulfide, and 1,1,2-Trichloro-1,2,2-trifluoroethane. A reporting limit (RL) standard was analyzed, and the target analyte was detected. Since the associated samples were non-detect for this analyte, the data have been reported.

Method(s) 8260C: The following sample was analyzed using medium level soil analysis due to the nature of the sample matrix: SB-3

(480-97480-9). Elevated reporting limits (RLs) are provided.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA Method(s) 8270D: The following samples were diluted due to the nature of the sample matrix: MW-3 (480-97480-2), MW-5 (480-97480-3)

and MW-7 (480-97480-4). Elevated reporting limits (RLs) are provided.

Method(s) 8270D: The %RPD of the laboratory control sample (LCS) and laboratory control standard duplicate (LCSD) for preparation

batch 480-293778 recovered outside control limits for the following analytes: Caprolactam and Phenol.

Method(s) 8270D: The continuing calibration verification (CCV) analyzed in batch 480-295082 was outside the method criteria for the

following analyte: Benzaldehyde. A CCV standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. As indicated in the reference method, sample analysis may proceed; however, any detection for the affected analyte is

considered estimated.


GC Semi VOA

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Case NarrativeClient: ATC Associates Inc. TestAmerica Job ID: 480-97480-1Project/Site: JB Soil & Groundwater Project

Job ID: 480-97480-1 (Continued)

Laboratory: TestAmerica Buffalo (Continued)

Metals

Method(s) 6010, 6010C: The Low Level Continuing Calibration Verification (CCVL 480-294213/38) contained Total Chromium outside the control limits. All reported samples SB-8 (480-97480-7), SB-2 (480-97480-8), SB-3 (480-97480-9), SB-6 (480-97480-10) and SB-7

(480-97480-11) associated with this CCVL were either below the laboratory's standard reporting limit for this analyte or contained this

analyte at a concentration greater than 10X the value found in the CCVL; therefore, re-analysis of samples was not performed.

Method(s) 6010C: Due to sample matrix effect on the internal standard (Yttrium), a dilution was required for the following sample: MW-1 (480-97480-1).


Organic Prep No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.


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Detection SummaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Client Sample ID: MW-1 Lab Sample ID: 480-97480-1

Acetone

RL

10 ug/L

MDL

3.0

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1J4.7 8260C

Carbon disulfide 1.0 ug/L0.19 Total/NA10.24 J 8260C

Di-n-butyl phthalate 5.1 ug/L0.32 Total/NA10.51 J 8270D

Phenol 5.1 ug/L0.40 Total/NA10.45 J * 8270D

Arsenic 0.075 mg/L0.028 Total/NA50.28 6010C

Barium 0.010 mg/L0.0035 Total/NA51.5 6010C

Cadmium 0.010 mg/L0.0025 Total/NA50.0033 J 6010C

Chromium 0.020 mg/L0.0050 Total/NA50.32 6010C

Lead 0.010 mg/L0.0030 Total/NA10.26 6010C


Acetone

RL

10 ug/L

MDL

3.0


Total/NA1J5.8 8260C


cis-1,2-Dichloroethene 1.0 ug/L0.81 Total/NA11.7 8260C

Vinyl chloride 1.0 ug/L0.90 Total/NA12.6 8260C

Benzaldehyde 25 ug/L1.3 Total/NA52.8 J B 8270D

Diethyl phthalate 25 ug/L1.1 Total/NA51.6 J 8270D

Diesel Range Organics [C10-C28] 0.56 mg/L0.35 Total/NA10.46 J 8015D






Mercury 0.00020 mg/L0.00012 Total/NA10.00036 7470A


Carbon disulfide

RL

1.0 ug/L

MDL

0.19


Total/NA1J0.43 8260C









Acetone

RL

10 ug/L

MDL

3.0


Total/NA1J4.2 8260C

Trichloroethene 1.0 ug/L0.46 Total/NA11.1 8260C







TestAmerica Buffalo

This Detection Summary does not include radiochemical test results.

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Client Sample ID: MW-7 (Continued) Lab Sample ID: 480-97480-4

Lead

RL

0.010 mg/L

MDL

0.0030


Total/NA10.21 6010C

Mercury 0.00020 mg/L0.00012 Total/NA10.00024 7470A

Client Sample ID: DUP Lab Sample ID: 480-97480-5

Acetone

RL

10 ug/L

MDL

3.0


Total/NA1J5.0 8260C


Client Sample ID: FB Lab Sample ID: 480-97480-6

Acetone

RL

10 ug/L

MDL

3.0


Total/NA1J7.4 8260C

Toluene 1.0 ug/L0.51 Total/NA17.4 8260C

Client Sample ID: SB-8 Lab Sample ID: 480-97480-7

☼2-Butanone (MEK)

RL

21 ug/Kg

MDL

1.5


Total/NA1J *8.3 8260C

☼Acetone 21 ug/Kg3.5 Total/NA143 B 8260C

☼Methylene Chloride 4.2 ug/Kg1.9 Total/NA12.8 J B 8260C

☼Arsenic 2.2 mg/Kg0.44 Total/NA13.9 6010C

☼Barium 0.55 mg/Kg0.12 Total/NA131 6010C

☼Cadmium 0.22 mg/Kg0.033 Total/NA10.049 J 6010C

☼Chromium 0.55 mg/Kg0.22 Total/NA114 ^ 6010C

☼Lead 1.1 mg/Kg0.26 Total/NA111 6010C

☼Mercury 0.022 mg/Kg0.0088 Total/NA10.032 7471B


☼Methyl acetate

RL

56 ug/Kg

MDL

27


Total/NA1J49 8260C

☼Methylene Chloride 56 ug/Kg11 Total/NA192 B 8260C

☼Tetrachloroethene 56 ug/Kg7.6 Total/NA133 J 8260C




☼Lead 1.2 mg/Kg0.29 Total/NA17.1 6010C

☼Mercury 0.024 mg/Kg0.0098 Total/NA10.012 J 7471B


☼Methyl acetate

RL

61 ug/Kg

MDL

29


Total/NA1240 8260C

☼Methylene Chloride 61 ug/Kg12 Total/NA131 J B 8260C





☼Mercury 0.024 mg/Kg0.0096 Total/NA10.012 J 7471B

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☼Acetone

RL

24 ug/Kg

MDL

4.1


Total/NA1J B7.2 8260C

☼Methylene Chloride 4.8 ug/Kg2.2 Total/NA13.5 J B 8260C






☼Methylene Chloride

RL

4.4 ug/Kg

MDL

2.0


Total/NA1J B3.3 8260C



☼Chromium 0.57 mg/Kg0.23 Total/NA17.6 ^ 6010C


Client Sample ID: DUP Lab Sample ID: 480-97480-12

No Detections.

TestAmerica Buffalo


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Client Sample ResultsTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Lab Sample ID: 480-97480-1Client Sample ID: MW-1Matrix: WaterDate Collected: 03/30/16 14:20

Date Received: 04/01/16 09:45

Method: 8260C - Volatile Organic Compounds by GC/MSRL MDL

1,1,1-Trichloroethane ND 1.0 0.82 ug/L 04/09/16 14:42 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 0.21 ug/L 04/09/16 14:42 11,1,2,2-Tetrachloroethane ND

1.0 0.23 ug/L 04/09/16 14:42 11,1,2-Trichloroethane ND

1.0 0.31 ug/L 04/09/16 14:42 11,1,2-Trichloro-1,2,2-trifluoroethane ND

1.0 0.38 ug/L 04/09/16 14:42 11,1-Dichloroethane ND

1.0 0.29 ug/L 04/09/16 14:42 11,1-Dichloroethene ND

1.0 0.41 ug/L 04/09/16 14:42 11,2,4-Trichlorobenzene ND

1.0 0.39 ug/L 04/09/16 14:42 11,2-Dibromo-3-Chloropropane ND

1.0 0.73 ug/L 04/09/16 14:42 11,2-Dibromoethane ND

1.0 0.79 ug/L 04/09/16 14:42 11,2-Dichlorobenzene ND


1.0 0.72 ug/L 04/09/16 14:42 11,2-Dichloropropane ND



5.0 1.2 ug/L 04/09/16 14:42 12-Hexanone ND

10 1.3 ug/L 04/09/16 14:42 12-Butanone (MEK) ND

5.0 2.1 ug/L 04/09/16 14:42 14-Methyl-2-pentanone (MIBK) ND

10 3.0 ug/L 04/09/16 14:42 1Acetone 4.7 J

1.0 0.41 ug/L 04/09/16 14:42 1Benzene ND

1.0 0.39 ug/L 04/09/16 14:42 1Bromodichloromethane ND

1.0 0.26 ug/L 04/09/16 14:42 1Bromoform ND

1.0 0.69 ug/L 04/09/16 14:42 1Bromomethane ND

1.0 0.19 ug/L 04/09/16 14:42 1Carbon disulfide 0.24 J

1.0 0.27 ug/L 04/09/16 14:42 1Carbon tetrachloride ND

1.0 0.75 ug/L 04/09/16 14:42 1Chlorobenzene ND

1.0 0.32 ug/L 04/09/16 14:42 1Dibromochloromethane ND

1.0 0.32 ug/L 04/09/16 14:42 1Chloroethane ND

1.0 0.34 ug/L 04/09/16 14:42 1Chloroform ND

1.0 0.35 ug/L 04/09/16 14:42 1Chloromethane ND

1.0 0.81 ug/L 04/09/16 14:42 1cis-1,2-Dichloroethene ND

1.0 0.36 ug/L 04/09/16 14:42 1cis-1,3-Dichloropropene ND

1.0 0.18 ug/L 04/09/16 14:42 1Cyclohexane ND

1.0 0.68 ug/L 04/09/16 14:42 1Dichlorodifluoromethane ND

1.0 0.74 ug/L 04/09/16 14:42 1Ethylbenzene ND

1.0 0.79 ug/L 04/09/16 14:42 1Isopropylbenzene ND

2.5 1.3 ug/L 04/09/16 14:42 1Methyl acetate ND

1.0 0.16 ug/L 04/09/16 14:42 1Methyl tert-butyl ether ND

1.0 0.16 ug/L 04/09/16 14:42 1Methylcyclohexane ND

1.0 0.44 ug/L 04/09/16 14:42 1Methylene Chloride ND

1.0 0.73 ug/L 04/09/16 14:42 1Styrene ND

1.0 0.36 ug/L 04/09/16 14:42 1Tetrachloroethene ND

1.0 0.51 ug/L 04/09/16 14:42 1Toluene ND

1.0 0.90 ug/L 04/09/16 14:42 1trans-1,2-Dichloroethene ND

1.0 0.37 ug/L 04/09/16 14:42 1trans-1,3-Dichloropropene ND

1.0 0.46 ug/L 04/09/16 14:42 1Trichloroethene ND

1.0 0.88 ug/L 04/09/16 14:42 1Trichlorofluoromethane ND

1.0 0.90 ug/L 04/09/16 14:42 1Vinyl chloride ND

2.0 0.66 ug/L 04/09/16 14:42 1Xylenes, Total ND

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1,2-Dichloroethane-d4 (Surr) 108 66 - 137 04/09/16 14:42 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Toluene-d8 (Surr) 104 04/09/16 14:42 171 - 126

4-Bromofluorobenzene (Surr) 106 04/09/16 14:42 173 - 120

Dibromofluoromethane (Surr) 109 04/09/16 14:42 160 - 140

Method: 8270D - Semivolatile Organic Compounds (GC/MS)RL MDL

Biphenyl ND 5.1 0.67 ug/L 04/02/16 10:06 04/05/16 02:11 1


5.1 0.53 ug/L 04/02/16 10:06 04/05/16 02:11 1bis (2-chloroisopropyl) ether ND

5.1 0.49 ug/L 04/02/16 10:06 04/05/16 02:11 12,4,5-Trichlorophenol ND

5.1 0.63 ug/L 04/02/16 10:06 04/05/16 02:11 12,4,6-Trichlorophenol ND

5.1 0.52 ug/L 04/02/16 10:06 04/05/16 02:11 12,4-Dichlorophenol ND

5.1 0.51 ug/L 04/02/16 10:06 04/05/16 02:11 12,4-Dimethylphenol ND

10 2.3 ug/L 04/02/16 10:06 04/05/16 02:11 12,4-Dinitrophenol ND

5.1 0.46 ug/L 04/02/16 10:06 04/05/16 02:11 12,4-Dinitrotoluene ND

5.1 0.41 ug/L 04/02/16 10:06 04/05/16 02:11 12,6-Dinitrotoluene ND

5.1 0.47 ug/L 04/02/16 10:06 04/05/16 02:11 12-Chloronaphthalene ND

5.1 0.55 ug/L 04/02/16 10:06 04/05/16 02:11 12-Chlorophenol ND

5.1 0.62 ug/L 04/02/16 10:06 04/05/16 02:11 12-Methylnaphthalene ND

5.1 0.41 ug/L 04/02/16 10:06 04/05/16 02:11 12-Methylphenol ND

10 0.43 ug/L 04/02/16 10:06 04/05/16 02:11 12-Nitroaniline ND

5.1 0.49 ug/L 04/02/16 10:06 04/05/16 02:11 12-Nitrophenol ND

5.1 0.41 ug/L 04/02/16 10:06 04/05/16 02:11 13,3'-Dichlorobenzidine ND


10 2.3 ug/L 04/02/16 10:06 04/05/16 02:11 14,6-Dinitro-2-methylphenol ND

5.1 0.46 ug/L 04/02/16 10:06 04/05/16 02:11 14-Bromophenyl phenyl ether ND

5.1 0.46 ug/L 04/02/16 10:06 04/05/16 02:11 14-Chloro-3-methylphenol ND

5.1 0.61 ug/L 04/02/16 10:06 04/05/16 02:11 14-Chloroaniline ND

5.1 0.36 ug/L 04/02/16 10:06 04/05/16 02:11 14-Chlorophenyl phenyl ether ND

10 0.37 ug/L 04/02/16 10:06 04/05/16 02:11 14-Methylphenol ND


10 1.6 ug/L 04/02/16 10:06 04/05/16 02:11 14-Nitrophenol ND

5.1 0.42 ug/L 04/02/16 10:06 04/05/16 02:11 1Acenaphthene ND

5.1 0.39 ug/L 04/02/16 10:06 04/05/16 02:11 1Acenaphthylene ND

5.1 0.56 ug/L 04/02/16 10:06 04/05/16 02:11 1Acetophenone ND

5.1 0.29 ug/L 04/02/16 10:06 04/05/16 02:11 1Anthracene ND

5.1 0.47 ug/L 04/02/16 10:06 04/05/16 02:11 1Atrazine ND

5.1 0.27 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzaldehyde ND

5.1 0.37 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzo(a)anthracene ND

5.1 0.48 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzo(a)pyrene ND

5.1 0.35 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzo(b)fluoranthene ND

5.1 0.36 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzo(g,h,i)perylene ND

5.1 0.75 ug/L 04/02/16 10:06 04/05/16 02:11 1Benzo(k)fluoranthene ND

5.1 0.36 ug/L 04/02/16 10:06 04/05/16 02:11 1Bis(2-chloroethoxy)methane ND

5.1 0.41 ug/L 04/02/16 10:06 04/05/16 02:11 1Bis(2-chloroethyl)ether ND

5.1 2.3 ug/L 04/02/16 10:06 04/05/16 02:11 1Bis(2-ethylhexyl) phthalate ND

5.1 1.0 ug/L 04/02/16 10:06 04/05/16 02:11 1Butyl benzyl phthalate ND

5.1 2.3 ug/L 04/02/16 10:06 04/05/16 02:11 1Caprolactam ND *

5.1 0.31 ug/L 04/02/16 10:06 04/05/16 02:11 1Carbazole ND

5.1 0.34 ug/L 04/02/16 10:06 04/05/16 02:11 1Chrysene ND

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Di-n-butyl phthalate 0.51 J 5.1 0.32 ug/L 04/02/16 10:06 04/05/16 02:11 1


5.1 0.48 ug/L 04/02/16 10:06 04/05/16 02:11 1Di-n-octyl phthalate ND

5.1 0.43 ug/L 04/02/16 10:06 04/05/16 02:11 1Dibenz(a,h)anthracene ND

10 0.52 ug/L 04/02/16 10:06 04/05/16 02:11 1Dibenzofuran ND

5.1 0.23 ug/L 04/02/16 10:06 04/05/16 02:11 1Diethyl phthalate ND

5.1 0.37 ug/L 04/02/16 10:06 04/05/16 02:11 1Dimethyl phthalate ND

5.1 0.41 ug/L 04/02/16 10:06 04/05/16 02:11 1Fluoranthene ND

5.1 0.37 ug/L 04/02/16 10:06 04/05/16 02:11 1Fluorene ND

5.1 0.52 ug/L 04/02/16 10:06 04/05/16 02:11 1Hexachlorobenzene ND

5.1 0.70 ug/L 04/02/16 10:06 04/05/16 02:11 1Hexachlorobutadiene ND

5.1 0.61 ug/L 04/02/16 10:06 04/05/16 02:11 1Hexachlorocyclopentadiene ND

5.1 0.61 ug/L 04/02/16 10:06 04/05/16 02:11 1Hexachloroethane ND

5.1 0.48 ug/L 04/02/16 10:06 04/05/16 02:11 1Indeno(1,2,3-cd)pyrene ND

5.1 0.44 ug/L 04/02/16 10:06 04/05/16 02:11 1Isophorone ND

5.1 0.56 ug/L 04/02/16 10:06 04/05/16 02:11 1N-Nitrosodi-n-propylamine ND

5.1 0.52 ug/L 04/02/16 10:06 04/05/16 02:11 1N-Nitrosodiphenylamine ND

5.1 0.78 ug/L 04/02/16 10:06 04/05/16 02:11 1Naphthalene ND

5.1 0.30 ug/L 04/02/16 10:06 04/05/16 02:11 1Nitrobenzene ND

10 2.3 ug/L 04/02/16 10:06 04/05/16 02:11 1Pentachlorophenol ND

5.1 0.45 ug/L 04/02/16 10:06 04/05/16 02:11 1Phenanthrene ND

5.1 0.40 ug/L 04/02/16 10:06 04/05/16 02:11 1Phenol 0.45 J *

5.1 0.35 ug/L 04/02/16 10:06 04/05/16 02:11 1Pyrene ND

2,4,6-Tribromophenol 99 52 - 132 04/02/16 10:06 04/05/16 02:11 1


2-Fluorobiphenyl 86 04/02/16 10:06 04/05/16 02:11 148 - 120

2-Fluorophenol 62 04/02/16 10:06 04/05/16 02:11 120 - 120

Nitrobenzene-d5 91 04/02/16 10:06 04/05/16 02:11 146 - 120

p-Terphenyl-d14 75 04/02/16 10:06 04/05/16 02:11 167 - 150

Phenol-d5 43 04/02/16 10:06 04/05/16 02:11 116 - 120

Method: 8015D - Diesel Range Organics (DRO) (GC)RL MDL

Diesel Range Organics [C10-C28] ND 0.52 0.32 mg/L 04/04/16 15:43 04/05/16 18:46 1


o-Terphenyl 80 29 - 136 04/04/16 15:43 04/05/16 18:46 1


Method: 6010C - Metals (ICP)RL MDL

Arsenic 0.28 0.075 0.028 mg/L 04/04/16 08:30 04/05/16 11:42 5


0.010 0.0035 mg/L 04/04/16 08:30 04/05/16 11:42 5Barium 1.5

0.010 0.0025 mg/L 04/04/16 08:30 04/05/16 11:42 5Cadmium 0.0033 J

0.020 0.0050 mg/L 04/04/16 08:30 04/05/16 11:42 5Chromium 0.32

0.010 0.0030 mg/L 04/04/16 08:30 04/05/16 11:38 1Lead 0.26

0.13 0.044 mg/L 04/04/16 08:30 04/05/16 11:42 5Selenium ND

0.030 0.0085 mg/L 04/04/16 08:30 04/05/16 11:42 5Silver ND

Method: 7470A - Mercury (CVAA)RL MDL

Mercury ND 0.00020 0.00012 mg/L 04/05/16 08:35 04/05/16 12:03 1


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5.0 1.2 ug/L 04/09/16 15:09 12-Hexanone ND



10 3.0 ug/L 04/09/16 15:09 1Acetone 5.8 J

1.0 0.41 ug/L 04/09/16 15:09 1Benzene ND


1.0 0.26 ug/L 04/09/16 15:09 1Bromoform ND









1.0 0.81 ug/L 04/09/16 15:09 1cis-1,2-Dichloroethene 1.7










1.0 0.73 ug/L 04/09/16 15:09 1Styrene ND


1.0 0.51 ug/L 04/09/16 15:09 1Toluene ND





1.0 0.90 ug/L 04/09/16 15:09 1Vinyl chloride 2.6


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Toluene-d8 (Surr) 103 04/09/16 15:09 171 - 126




Biphenyl ND 25 3.3 ug/L 04/02/16 10:06 04/05/16 02:41 5


25 2.6 ug/L 04/02/16 10:06 04/05/16 02:41 5bis (2-chloroisopropyl) ether ND

25 2.4 ug/L 04/02/16 10:06 04/05/16 02:41 52,4,5-Trichlorophenol ND


25 2.6 ug/L 04/02/16 10:06 04/05/16 02:41 52,4-Dichlorophenol ND

25 2.5 ug/L 04/02/16 10:06 04/05/16 02:41 52,4-Dimethylphenol ND

50 11 ug/L 04/02/16 10:06 04/05/16 02:41 52,4-Dinitrophenol ND

25 2.2 ug/L 04/02/16 10:06 04/05/16 02:41 52,4-Dinitrotoluene ND


25 2.3 ug/L 04/02/16 10:06 04/05/16 02:41 52-Chloronaphthalene ND

25 2.7 ug/L 04/02/16 10:06 04/05/16 02:41 52-Chlorophenol ND

25 3.0 ug/L 04/02/16 10:06 04/05/16 02:41 52-Methylnaphthalene ND




25 2.0 ug/L 04/02/16 10:06 04/05/16 02:41 53,3'-Dichlorobenzidine ND


50 11 ug/L 04/02/16 10:06 04/05/16 02:41 54,6-Dinitro-2-methylphenol ND

25 2.3 ug/L 04/02/16 10:06 04/05/16 02:41 54-Bromophenyl phenyl ether ND

25 2.3 ug/L 04/02/16 10:06 04/05/16 02:41 54-Chloro-3-methylphenol ND

25 3.0 ug/L 04/02/16 10:06 04/05/16 02:41 54-Chloroaniline ND

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 54-Chlorophenyl phenyl ether ND




25 2.1 ug/L 04/02/16 10:06 04/05/16 02:41 5Acenaphthene ND

25 1.9 ug/L 04/02/16 10:06 04/05/16 02:41 5Acenaphthylene ND

25 2.7 ug/L 04/02/16 10:06 04/05/16 02:41 5Acetophenone ND

25 1.4 ug/L 04/02/16 10:06 04/05/16 02:41 5Anthracene ND

25 2.3 ug/L 04/02/16 10:06 04/05/16 02:41 5Atrazine ND

25 1.3 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzaldehyde 2.8 J B

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzo(a)anthracene ND

25 2.4 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzo(a)pyrene ND

25 1.7 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzo(b)fluoranthene ND

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzo(g,h,i)perylene ND

25 3.7 ug/L 04/02/16 10:06 04/05/16 02:41 5Benzo(k)fluoranthene ND

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Bis(2-chloroethoxy)methane ND

25 2.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Bis(2-chloroethyl)ether ND

25 11 ug/L 04/02/16 10:06 04/05/16 02:41 5Bis(2-ethylhexyl) phthalate ND

25 5.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Butyl benzyl phthalate ND

25 11 ug/L 04/02/16 10:06 04/05/16 02:41 5Caprolactam ND *

25 1.5 ug/L 04/02/16 10:06 04/05/16 02:41 5Carbazole ND

25 1.7 ug/L 04/02/16 10:06 04/05/16 02:41 5Chrysene ND

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Di-n-butyl phthalate ND 25 1.6 ug/L 04/02/16 10:06 04/05/16 02:41 5


25 2.4 ug/L 04/02/16 10:06 04/05/16 02:41 5Di-n-octyl phthalate ND

25 2.1 ug/L 04/02/16 10:06 04/05/16 02:41 5Dibenz(a,h)anthracene ND


25 1.1 ug/L 04/02/16 10:06 04/05/16 02:41 5Diethyl phthalate 1.6 J

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Dimethyl phthalate ND

25 2.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Fluoranthene ND

25 1.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Fluorene ND

25 2.6 ug/L 04/02/16 10:06 04/05/16 02:41 5Hexachlorobenzene ND

25 3.4 ug/L 04/02/16 10:06 04/05/16 02:41 5Hexachlorobutadiene ND

25 3.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Hexachlorocyclopentadiene ND

25 3.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Hexachloroethane ND

25 2.4 ug/L 04/02/16 10:06 04/05/16 02:41 5Indeno(1,2,3-cd)pyrene ND

25 2.2 ug/L 04/02/16 10:06 04/05/16 02:41 5Isophorone ND

25 2.7 ug/L 04/02/16 10:06 04/05/16 02:41 5N-Nitrosodi-n-propylamine ND

25 2.6 ug/L 04/02/16 10:06 04/05/16 02:41 5N-Nitrosodiphenylamine ND

25 3.8 ug/L 04/02/16 10:06 04/05/16 02:41 5Naphthalene ND

25 1.5 ug/L 04/02/16 10:06 04/05/16 02:41 5Nitrobenzene ND

50 11 ug/L 04/02/16 10:06 04/05/16 02:41 5Pentachlorophenol ND

25 2.2 ug/L 04/02/16 10:06 04/05/16 02:41 5Phenanthrene ND

25 2.0 ug/L 04/02/16 10:06 04/05/16 02:41 5Phenol ND *

25 1.7 ug/L 04/02/16 10:06 04/05/16 02:41 5Pyrene ND

2,4,6-Tribromophenol 113 52 - 132 04/02/16 10:06 04/05/16 02:41 5


2-Fluorobiphenyl 92 04/02/16 10:06 04/05/16 02:41 548 - 120

2-Fluorophenol 65 04/02/16 10:06 04/05/16 02:41 520 - 120

Nitrobenzene-d5 94 04/02/16 10:06 04/05/16 02:41 546 - 120

p-Terphenyl-d14 76 04/02/16 10:06 04/05/16 02:41 567 - 150

Phenol-d5 46 04/02/16 10:06 04/05/16 02:41 516 - 120


Diesel Range Organics [C10-C28] 0.46 J 0.56 0.35 mg/L 04/04/16 15:43 04/05/16 19:20 1


o-Terphenyl 85 29 - 136 04/04/16 15:43 04/05/16 19:20 1



Arsenic 0.094 0.015 0.0056 mg/L 04/04/16 08:30 04/05/16 11:45 1


0.0020 0.00070 mg/L 04/04/16 08:30 04/05/16 11:45 1Barium 0.59

0.0020 0.00050 mg/L 04/04/16 08:30 04/05/16 11:45 1Cadmium 0.0016 J

0.0040 0.0010 mg/L 04/04/16 08:30 04/05/16 11:45 1Chromium 0.27

0.010 0.0030 mg/L 04/04/16 08:30 04/05/16 11:45 1Lead 0.21

0.025 0.0087 mg/L 04/04/16 08:30 04/05/16 11:45 1Selenium ND

0.0060 0.0017 mg/L 04/04/16 08:30 04/05/16 11:45 1Silver ND


Mercury 0.00036 0.00020 0.00012 mg/L 04/05/16 08:35 04/05/16 12:05 1


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5.0 1.2 ug/L 04/09/16 15:36 12-Hexanone ND



10 3.0 ug/L 04/09/16 15:36 1Acetone ND

1.0 0.41 ug/L 04/09/16 15:36 1Benzene ND


1.0 0.26 ug/L 04/09/16 15:36 1Bromoform ND



















1.0 0.73 ug/L 04/09/16 15:36 1Styrene ND


1.0 0.51 ug/L 04/09/16 15:36 1Toluene ND







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Toluene-d8 (Surr) 102 04/09/16 15:36 171 - 126




Biphenyl ND 27 3.5 ug/L 04/02/16 10:06 04/05/16 03:10 5






























27 2.5 ug/L 04/02/16 10:06 04/05/16 03:10 5Atrazine ND












27 1.6 ug/L 04/02/16 10:06 04/05/16 03:10 5Carbazole ND

27 1.8 ug/L 04/02/16 10:06 04/05/16 03:10 5Chrysene ND

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27 1.2 ug/L 04/02/16 10:06 04/05/16 03:10 5Diethyl phthalate ND



27 1.9 ug/L 04/02/16 10:06 04/05/16 03:10 5Fluorene ND













27 2.1 ug/L 04/02/16 10:06 04/05/16 03:10 5Phenol ND *

27 1.8 ug/L 04/02/16 10:06 04/05/16 03:10 5Pyrene ND

2,4,6-Tribromophenol 105 52 - 132 04/02/16 10:06 04/05/16 03:10 5


2-Fluorobiphenyl 88 04/02/16 10:06 04/05/16 03:10 548 - 120

2-Fluorophenol 64 04/02/16 10:06 04/05/16 03:10 520 - 120

Nitrobenzene-d5 89 04/02/16 10:06 04/05/16 03:10 546 - 120

p-Terphenyl-d14 74 04/02/16 10:06 04/05/16 03:10 567 - 150

Phenol-d5 46 04/02/16 10:06 04/05/16 03:10 516 - 120




o-Terphenyl 87 29 - 136 04/04/16 15:43 04/05/16 19:53 1



Arsenic 0.11 0.015 0.0056 mg/L 04/04/16 08:30 04/05/16 12:01 1


0.0020 0.00070 mg/L 04/04/16 08:30 04/05/16 12:01 1Barium 0.67

0.0020 0.00050 mg/L 04/04/16 08:30 04/05/16 12:01 1Cadmium 0.0011 J

0.0040 0.0010 mg/L 04/04/16 08:30 04/05/16 12:01 1Chromium 0.32

0.010 0.0030 mg/L 04/04/16 08:30 04/05/16 12:01 1Lead 0.19

0.025 0.0087 mg/L 04/04/16 08:30 04/05/16 12:01 1Selenium ND

0.0060 0.0017 mg/L 04/04/16 08:30 04/05/16 12:01 1Silver ND


Mercury ND 0.00020 0.00012 mg/L 04/05/16 08:35 04/05/16 12:07 1


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5.0 1.2 ug/L 04/09/16 16:03 12-Hexanone ND



10 3.0 ug/L 04/09/16 16:03 1Acetone 4.2 J

1.0 0.41 ug/L 04/09/16 16:03 1Benzene ND


1.0 0.26 ug/L 04/09/16 16:03 1Bromoform ND


1.0 0.19 ug/L 04/09/16 16:03 1Carbon disulfide ND

















1.0 0.73 ug/L 04/09/16 16:03 1Styrene ND


1.0 0.51 ug/L 04/09/16 16:03 1Toluene ND



1.0 0.46 ug/L 04/09/16 16:03 1Trichloroethene 1.1




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Toluene-d8 (Surr) 104 04/09/16 16:03 171 - 126




Biphenyl ND 25 3.3 ug/L 04/02/16 10:06 04/05/16 03:40 5






























25 2.3 ug/L 04/02/16 10:06 04/05/16 03:40 5Atrazine ND












25 1.5 ug/L 04/02/16 10:06 04/05/16 03:40 5Carbazole ND

25 1.7 ug/L 04/02/16 10:06 04/05/16 03:40 5Chrysene ND

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25 1.1 ug/L 04/02/16 10:06 04/05/16 03:40 5Diethyl phthalate ND



25 1.8 ug/L 04/02/16 10:06 04/05/16 03:40 5Fluorene ND













25 2.0 ug/L 04/02/16 10:06 04/05/16 03:40 5Phenol ND *

25 1.7 ug/L 04/02/16 10:06 04/05/16 03:40 5Pyrene ND

2,4,6-Tribromophenol 80 52 - 132 04/02/16 10:06 04/05/16 03:40 5


2-Fluorobiphenyl 85 04/02/16 10:06 04/05/16 03:40 548 - 120

2-Fluorophenol 59 04/02/16 10:06 04/05/16 03:40 520 - 120

Nitrobenzene-d5 91 04/02/16 10:06 04/05/16 03:40 546 - 120

p-Terphenyl-d14 69 04/02/16 10:06 04/05/16 03:40 567 - 150

Phenol-d5 45 04/02/16 10:06 04/05/16 03:40 516 - 120




o-Terphenyl 77 29 - 136 04/04/16 15:43 04/05/16 20:27 1



Arsenic 0.085 0.015 0.0056 mg/L 04/04/16 08:30 04/05/16 12:08 1


0.0020 0.00070 mg/L 04/04/16 08:30 04/05/16 12:08 1Barium 0.52

0.0020 0.00050 mg/L 04/04/16 08:30 04/05/16 12:08 1Cadmium 0.00073 J

0.0040 0.0010 mg/L 04/04/16 08:30 04/05/16 12:08 1Chromium 0.28

0.010 0.0030 mg/L 04/04/16 08:30 04/05/16 12:08 1Lead 0.21

0.025 0.0087 mg/L 04/04/16 08:30 04/05/16 12:08 1Selenium ND

0.0060 0.0017 mg/L 04/04/16 08:30 04/05/16 12:08 1Silver ND


Mercury 0.00024 0.00020 0.00012 mg/L 04/05/16 08:35 04/05/16 12:09 1


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Lab Sample ID: 480-97480-5Client Sample ID: DUPMatrix: WaterDate Collected: 03/30/16 13:45


















5.0 1.2 ug/L 04/09/16 16:31 12-Hexanone ND



10 3.0 ug/L 04/09/16 16:31 1Acetone 5.0 J

1.0 0.41 ug/L 04/09/16 16:31 1Benzene ND


1.0 0.26 ug/L 04/09/16 16:31 1Bromoform ND



















1.0 0.73 ug/L 04/09/16 16:31 1Styrene ND


1.0 0.51 ug/L 04/09/16 16:31 1Toluene ND







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Lab Sample ID: 480-97480-5Client Sample ID: DUPMatrix: WaterDate Collected: 03/30/16 13:45




Toluene-d8 (Surr) 105 04/09/16 16:31 171 - 126



Lab Sample ID: 480-97480-6Client Sample ID: FBMatrix: WaterDate Collected: 03/30/16 14:50


















5.0 1.2 ug/L 04/09/16 16:58 12-Hexanone ND



10 3.0 ug/L 04/09/16 16:58 1Acetone 7.4 J

1.0 0.41 ug/L 04/09/16 16:58 1Benzene ND


1.0 0.26 ug/L 04/09/16 16:58 1Bromoform ND


1.0 0.19 ug/L 04/09/16 16:58 1Carbon disulfide ND

















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Lab Sample ID: 480-97480-6Client Sample ID: FBMatrix: WaterDate Collected: 03/30/16 14:50


Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)RL MDL

Styrene ND 1.0 0.73 ug/L 04/09/16 16:58 1



1.0 0.51 ug/L 04/09/16 16:58 1Toluene 7.4









Toluene-d8 (Surr) 103 04/09/16 16:58 171 - 126



Lab Sample ID: 480-97480-7Client Sample ID: SB-8Matrix: SolidDate Collected: 03/30/16 11:50

Percent Solids: 86.8Date Received: 04/01/16 09:45


1,1,1-Trichloroethane ND 4.2 0.30 ug/Kg ☼ 04/01/16 10:30 04/04/16 18:40 1


4.2 0.33 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,2-Dichlorobenzene ND

4.2 0.68 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,1,2,2-Tetrachloroethane ND

4.2 0.55 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,1,2-Trichloroethane ND

4.2 0.96 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND

4.2 0.51 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,1-Dichloroethane ND

4.2 0.51 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,1-Dichloroethene ND

4.2 0.26 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,2,4-Trichlorobenzene ND

4.2 2.1 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,2-Dibromo-3-Chloropropane ND


4.2 2.1 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,2-Dichloropropane ND



21 1.5 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼2-Butanone (MEK) 8.3 J *

21 2.1 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼2-Hexanone ND

21 1.4 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼4-Methyl-2-pentanone (MIBK) ND

21 3.5 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Acetone 43 B

4.2 0.21 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Benzene ND

4.2 0.56 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Bromodichloromethane ND

4.2 2.1 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Bromoform ND

4.2 0.38 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Bromomethane ND

4.2 2.1 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Carbon disulfide ND

4.2 0.41 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Carbon tetrachloride ND

4.2 0.55 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Chlorobenzene ND

4.2 0.54 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Dibromochloromethane ND

4.2 0.95 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Chloroethane ND

4.2 0.26 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Chloroform ND

4.2 0.25 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Chloromethane ND

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cis-1,2-Dichloroethene ND 4.2 0.54 ug/Kg ☼ 04/01/16 10:30 04/04/16 18:40 1


4.2 0.60 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼cis-1,3-Dichloropropene ND

4.2 0.59 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Cyclohexane ND

4.2 0.35 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Dichlorodifluoromethane ND

4.2 0.29 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Ethylbenzene ND

4.2 0.54 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼1,2-Dibromoethane ND

4.2 0.63 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Isopropylbenzene ND

4.2 2.5 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Methyl acetate ND

4.2 0.41 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Methyl tert-butyl ether ND

4.2 0.64 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Methylcyclohexane ND

4.2 1.9 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Methylene Chloride 2.8 J B

4.2 0.21 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Styrene ND

4.2 0.56 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Tetrachloroethene ND

4.2 0.32 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Toluene ND

4.2 0.43 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼trans-1,2-Dichloroethene ND

4.2 1.8 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼trans-1,3-Dichloropropene ND

4.2 0.92 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Trichloroethene ND

4.2 0.40 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Trichlorofluoromethane ND

4.2 0.51 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Vinyl chloride ND

8.4 0.71 ug/Kg 04/01/16 10:30 04/04/16 18:40 1☼Xylenes, Total ND

Toluene-d8 (Surr) 101 71 - 125 04/01/16 10:30 04/04/16 18:40 1


1,2-Dichloroethane-d4 (Surr) 103 04/01/16 10:30 04/04/16 18:40 164 - 126

4-Bromofluorobenzene (Surr) 104 04/01/16 10:30 04/04/16 18:40 172 - 126

Dibromofluoromethane (Surr) 103 04/01/16 10:30 04/04/16 18:40 160 - 140


Biphenyl ND 190 29 ug/Kg ☼ 04/08/16 05:53 04/11/16 15:10 1


190 39 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼bis (2-chloroisopropyl) ether ND

190 53 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2,4,5-Trichlorophenol ND


190 21 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2,4-Dichlorophenol ND

190 47 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2,4-Dimethylphenol ND

1900 900 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2,4-Dinitrophenol ND

190 40 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2,4-Dinitrotoluene ND


190 32 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Chloronaphthalene ND

190 35 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Chlorophenol ND

190 39 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Methylnaphthalene ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Methylphenol ND

380 29 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Nitroaniline ND

190 55 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼2-Nitrophenol ND

380 230 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼3,3'-Dichlorobenzidine ND


380 190 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼4,6-Dinitro-2-methylphenol ND

190 27 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼4-Bromophenyl phenyl ether ND

190 48 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼4-Chloro-3-methylphenol ND

190 48 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼4-Chloroaniline ND

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4-Chlorophenyl phenyl ether ND 190 24 ug/Kg ☼ 04/08/16 05:53 04/11/16 15:10 1





190 29 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Acenaphthene ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Acenaphthylene ND

190 26 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Acetophenone ND

190 48 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Anthracene ND

190 67 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Atrazine ND

190 150 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzaldehyde ND

190 19 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzo[a]anthracene ND

190 29 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzo[a]pyrene ND

190 31 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzo[b]fluoranthene ND

190 21 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzo[g,h,i]perylene ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Benzo[k]fluoranthene ND

190 41 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Bis(2-chloroethoxy)methane ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Bis(2-chloroethyl)ether ND

190 66 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Bis(2-ethylhexyl) phthalate ND

190 32 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Butyl benzyl phthalate ND

190 58 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Caprolactam ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Carbazole ND

190 43 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Chrysene ND

190 33 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Di-n-butyl phthalate ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Di-n-octyl phthalate ND

190 34 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Dibenz(a,h)anthracene ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Dibenzofuran ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Diethyl phthalate ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Dimethyl phthalate ND

190 21 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Fluoranthene ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Fluorene ND

190 26 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Hexachlorobenzene ND

190 29 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Hexachlorobutadiene ND

190 26 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Hexachlorocyclopentadiene ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Hexachloroethane ND

190 24 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Indeno[1,2,3-cd]pyrene ND

190 41 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Isophorone ND

190 33 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼N-Nitrosodi-n-propylamine ND

190 160 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼N-Nitrosodiphenylamine ND

190 25 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Naphthalene ND

190 22 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Nitrobenzene ND

380 190 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Pentachlorophenol ND

190 29 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Phenanthrene ND

190 30 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Phenol ND

190 23 ug/Kg 04/08/16 05:53 04/11/16 15:10 1☼Pyrene ND

2,4,6-Tribromophenol 95 39 - 146 04/08/16 05:53 04/11/16 15:10 1


2-Fluorobiphenyl 88 04/08/16 05:53 04/11/16 15:10 137 - 120

2-Fluorophenol 79 04/08/16 05:53 04/11/16 15:10 118 - 120

Nitrobenzene-d5 85 04/08/16 05:53 04/11/16 15:10 134 - 132

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Method: 8270D - Semivolatile Organic Compounds (GC/MS) (Continued)

p-Terphenyl-d14 104 65 - 153 04/08/16 05:53 04/11/16 15:10 1


Phenol-d5 82 04/08/16 05:53 04/11/16 15:10 111 - 120


Diesel Range Organics [C10-C28] ND 19 5.6 mg/Kg ☼ 04/04/16 14:00 04/05/16 14:18 1


o-Terphenyl 81 48 - 125 04/04/16 14:00 04/05/16 14:18 1



Arsenic 3.9 2.2 0.44 mg/Kg ☼ 04/04/16 14:16 04/05/16 14:18 1


0.55 0.12 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Barium 31

0.22 0.033 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Cadmium 0.049 J

0.55 0.22 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Chromium 14 ^

1.1 0.26 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Lead 11

4.4 0.44 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Selenium ND

0.66 0.22 mg/Kg 04/04/16 14:16 04/05/16 14:18 1☼Silver ND

Method: 7471B - Mercury (CVAA)RL MDL

Mercury 0.032 0.022 0.0088 mg/Kg ☼ 04/05/16 09:15 04/05/16 12:58 1





1,1,1-Trichloroethane ND 56 16 ug/Kg ☼ 04/01/16 10:30 04/08/16 19:59 1


56 9.1 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,1,2,2-Tetrachloroethane ND

56 28 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND

56 12 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,1,2-Trichloroethane ND

56 17 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,1-Dichloroethane ND

56 19 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,1-Dichloroethene ND

56 21 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,2,4-Trichlorobenzene ND

56 28 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,2-Dibromo-3-Chloropropane ND

56 14 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,2-Dichlorobenzene ND


56 9.1 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,2-Dichloropropane ND


56 7.9 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,4-Dichlorobenzene ND

280 170 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼2-Butanone (MEK) ND

280 120 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼2-Hexanone ND

280 18 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼4-Methyl-2-pentanone (MIBK) ND

280 230 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Acetone ND

56 11 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Benzene ND

56 28 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Bromoform ND

56 12 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Bromomethane ND

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Carbon disulfide ND 56 26 ug/Kg ☼ 04/01/16 10:30 04/08/16 19:59 1


56 14 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Carbon tetrachloride ND

56 7.4 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Chlorobenzene ND

56 27 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Dibromochloromethane ND

56 12 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Chloroethane ND

56 39 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Chloroform ND

56 13 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Chloromethane ND

56 16 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼cis-1,2-Dichloroethene ND

56 12 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Cyclohexane ND

56 11 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Bromodichloromethane ND

56 24 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Dichlorodifluoromethane ND

56 16 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Ethylbenzene ND

56 9.8 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼1,2-Dibromoethane ND

56 8.4 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Isopropylbenzene ND

56 27 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Methyl acetate 49 J

56 21 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Methyl tert-butyl ether ND

56 26 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Methylcyclohexane ND

56 11 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Methylene Chloride 92 B

56 7.6 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Tetrachloroethene 33 J

56 15 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Toluene ND

56 13 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼trans-1,2-Dichloroethene ND

56 5.5 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼trans-1,3-Dichloropropene ND

56 16 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Trichloroethene ND

56 26 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Trichlorofluoromethane ND

56 19 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Vinyl chloride ND

110 31 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Xylenes, Total ND

56 13 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼cis-1,3-Dichloropropene ND

56 14 ug/Kg 04/01/16 10:30 04/08/16 19:59 1☼Styrene ND

1,2-Dichloroethane-d4 (Surr) 103 53 - 146 04/01/16 10:30 04/08/16 19:59 1



Toluene-d8 (Surr) 98 04/01/16 10:30 04/08/16 19:59 150 - 149



Biphenyl ND 210 30 ug/Kg ☼ 04/08/16 05:53 04/11/16 15:37 1














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2-Nitroaniline ND 400 30 ug/Kg ☼ 04/08/16 05:53 04/11/16 15:37 1









210 25 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼4-Chlorophenyl phenyl ether ND








210 71 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼Atrazine ND













210 46 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼Chrysene ND








210 24 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼Fluorene ND












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Phenanthrene ND 210 30 ug/Kg ☼ 04/08/16 05:53 04/11/16 15:37 1


210 31 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼Phenol ND

210 24 ug/Kg 04/08/16 05:53 04/11/16 15:37 1☼Pyrene ND

2,4,6-Tribromophenol 90 39 - 146 04/08/16 05:53 04/11/16 15:37 1


2-Fluorobiphenyl 84 04/08/16 05:53 04/11/16 15:37 137 - 120

2-Fluorophenol 78 04/08/16 05:53 04/11/16 15:37 118 - 120

Nitrobenzene-d5 81 04/08/16 05:53 04/11/16 15:37 134 - 132

p-Terphenyl-d14 102 04/08/16 05:53 04/11/16 15:37 165 - 153

Phenol-d5 82 04/08/16 05:53 04/11/16 15:37 111 - 120




o-Terphenyl 82 48 - 125 04/04/16 14:00 04/05/16 13:44 1



Arsenic 5.0 2.4 0.48 mg/Kg ☼ 04/04/16 14:16 04/05/16 14:21 1


0.60 0.13 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Barium 21

0.24 0.036 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Cadmium ND

0.60 0.24 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Chromium 11 ^

1.2 0.29 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Lead 7.1

4.8 0.48 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Selenium ND

0.72 0.24 mg/Kg 04/04/16 14:16 04/05/16 14:21 1☼Silver ND


Mercury 0.012 J 0.024 0.0098 mg/Kg ☼ 04/05/16 09:15 04/05/16 13:02 1





1,1,1-Trichloroethane ND 61 17 ug/Kg ☼ 04/01/16 10:30 04/08/16 20:26 1


61 9.9 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,1,2,2-Tetrachloroethane ND

61 30 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND

61 13 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,1,2-Trichloroethane ND


61 21 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,1-Dichloroethene ND

61 23 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,2,4-Trichlorobenzene ND

61 30 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,2-Dibromo-3-Chloropropane ND



61 9.8 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,2-Dichloropropane ND


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1,4-Dichlorobenzene ND 61 8.5 ug/Kg ☼ 04/01/16 10:30 04/08/16 20:26 1


300 180 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼2-Butanone (MEK) ND

300 120 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼2-Hexanone ND

300 19 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼4-Methyl-2-pentanone (MIBK) ND

300 250 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Acetone ND

61 12 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Benzene ND

61 30 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Bromoform ND

61 13 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Bromomethane ND

61 28 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Carbon disulfide ND

61 15 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Carbon tetrachloride ND

61 8.0 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Chlorobenzene ND

61 29 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Dibromochloromethane ND

61 13 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Chloroethane ND

61 42 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Chloroform ND

61 14 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Chloromethane ND

61 17 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼cis-1,2-Dichloroethene ND

61 13 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Cyclohexane ND

61 12 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Bromodichloromethane ND

61 26 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Dichlorodifluoromethane ND

61 18 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Ethylbenzene ND

61 11 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼1,2-Dibromoethane ND

61 9.1 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Isopropylbenzene ND

61 29 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Methyl acetate 240

61 23 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Methyl tert-butyl ether ND

61 28 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Methylcyclohexane ND

61 12 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Methylene Chloride 31 J B

61 8.2 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Tetrachloroethene ND

61 16 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Toluene ND

61 14 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼trans-1,2-Dichloroethene ND

61 6.0 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼trans-1,3-Dichloropropene ND

61 17 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Trichloroethene ND

61 28 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Trichlorofluoromethane ND

61 20 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Vinyl chloride ND

120 34 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Xylenes, Total ND

61 15 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼cis-1,3-Dichloropropene ND

61 15 ug/Kg 04/01/16 10:30 04/08/16 20:26 1☼Styrene ND

1,2-Dichloroethane-d4 (Surr) 102 53 - 146 04/01/16 10:30 04/08/16 20:26 1



Toluene-d8 (Surr) 99 04/01/16 10:30 04/08/16 20:26 150 - 149



Biphenyl ND 210 30 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:03 1






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2,4-Dimethylphenol ND 210 50 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:03 1

























210 71 ug/Kg 04/08/16 05:53 04/11/16 16:03 1☼Atrazine ND













210 46 ug/Kg 04/08/16 05:53 04/11/16 16:03 1☼Chrysene ND








210 24 ug/Kg 04/08/16 05:53 04/11/16 16:03 1☼Fluorene ND




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Hexachloroethane ND 210 27 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:03 1










210 31 ug/Kg 04/08/16 05:53 04/11/16 16:03 1☼Phenol ND

210 24 ug/Kg 04/08/16 05:53 04/11/16 16:03 1☼Pyrene ND

2,4,6-Tribromophenol 77 39 - 146 04/08/16 05:53 04/11/16 16:03 1


2-Fluorobiphenyl 77 04/08/16 05:53 04/11/16 16:03 137 - 120

2-Fluorophenol 68 04/08/16 05:53 04/11/16 16:03 118 - 120

Nitrobenzene-d5 76 04/08/16 05:53 04/11/16 16:03 134 - 132

p-Terphenyl-d14 93 04/08/16 05:53 04/11/16 16:03 165 - 153

Phenol-d5 72 04/08/16 05:53 04/11/16 16:03 111 - 120




o-Terphenyl 83 48 - 125 04/04/16 14:00 04/05/16 11:59 1



Arsenic 4.3 2.4 0.47 mg/Kg ☼ 04/04/16 14:16 04/05/16 14:24 1


0.59 0.13 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Barium 16

0.24 0.036 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Cadmium ND

0.59 0.24 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Chromium 10 ^

1.2 0.28 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Lead 4.1

4.7 0.47 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Selenium ND

0.71 0.24 mg/Kg 04/04/16 14:16 04/05/16 14:24 1☼Silver ND


Mercury 0.012 J 0.024 0.0096 mg/Kg ☼ 04/05/16 09:15 04/05/16 13:04 1










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1,1,2-Trichloro-1,2,2-trifluoroethane ND 4.8 1.1 ug/Kg ☼ 04/01/16 10:30 04/04/16 19:59 1










24 1.8 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼2-Butanone (MEK) ND *

24 2.4 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼2-Hexanone ND


24 4.1 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼Acetone 7.2 J B

4.8 0.24 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼Benzene ND











4.8 0.62 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼cis-1,2-Dichloroethene ND











4.8 0.24 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼Styrene ND


4.8 0.37 ug/Kg 04/01/16 10:30 04/04/16 19:59 1☼Toluene ND







Toluene-d8 (Surr) 102 71 - 125 04/01/16 10:30 04/04/16 19:59 1





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Biphenyl ND 210 31 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:30 1






























210 74 ug/Kg 04/08/16 05:53 04/11/16 16:30 1☼Atrazine ND













210 48 ug/Kg 04/08/16 05:53 04/11/16 16:30 1☼Chrysene ND








210 25 ug/Kg 04/08/16 05:53 04/11/16 16:30 1☼Fluorene ND



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Hexachlorocyclopentadiene ND 210 29 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:30 1











210 33 ug/Kg 04/08/16 05:53 04/11/16 16:30 1☼Phenol ND

210 25 ug/Kg 04/08/16 05:53 04/11/16 16:30 1☼Pyrene ND

2,4,6-Tribromophenol 84 39 - 146 04/08/16 05:53 04/11/16 16:30 1


2-Fluorobiphenyl 80 04/08/16 05:53 04/11/16 16:30 137 - 120

2-Fluorophenol 72 04/08/16 05:53 04/11/16 16:30 118 - 120

Nitrobenzene-d5 75 04/08/16 05:53 04/11/16 16:30 134 - 132

p-Terphenyl-d14 95 04/08/16 05:53 04/11/16 16:30 165 - 153

Phenol-d5 78 04/08/16 05:53 04/11/16 16:30 111 - 120




o-Terphenyl 84 48 - 125 04/04/16 14:00 04/05/16 11:25 1



Arsenic 4.9 2.3 0.46 mg/Kg ☼ 04/04/16 14:16 04/05/16 14:37 1


0.58 0.13 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Barium 15

0.23 0.035 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Cadmium ND

0.58 0.23 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Chromium 10 ^

1.2 0.28 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Lead 3.8

4.6 0.46 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Selenium ND

0.69 0.23 mg/Kg 04/04/16 14:16 04/05/16 14:37 1☼Silver ND


Mercury ND 0.023 0.0094 mg/Kg ☼ 04/05/16 09:15 04/05/16 13:12 1









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22 1.6 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼2-Butanone (MEK) ND *

22 2.2 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼2-Hexanone ND


22 3.7 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼Acetone ND

4.4 0.21 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼Benzene ND






















4.4 0.22 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼Styrene ND


4.4 0.33 ug/Kg 04/01/16 10:30 04/04/16 20:25 1☼Toluene ND







Toluene-d8 (Surr) 101 71 - 125 04/01/16 10:30 04/04/16 20:25 1




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Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)

Dibromofluoromethane (Surr) 102 60 - 140 04/01/16 10:30 04/04/16 20:25 1



Biphenyl ND 190 28 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:56 1






























190 66 ug/Kg 04/08/16 05:53 04/11/16 16:56 1☼Atrazine ND













190 42 ug/Kg 04/08/16 05:53 04/11/16 16:56 1☼Chrysene ND



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Dibenz(a,h)anthracene ND 190 33 ug/Kg ☼ 04/08/16 05:53 04/11/16 16:56 1






190 22 ug/Kg 04/08/16 05:53 04/11/16 16:56 1☼Fluorene ND













190 29 ug/Kg 04/08/16 05:53 04/11/16 16:56 1☼Phenol ND

190 22 ug/Kg 04/08/16 05:53 04/11/16 16:56 1☼Pyrene ND

2,4,6-Tribromophenol 86 39 - 146 04/08/16 05:53 04/11/16 16:56 1


2-Fluorobiphenyl 84 04/08/16 05:53 04/11/16 16:56 137 - 120

2-Fluorophenol 74 04/08/16 05:53 04/11/16 16:56 118 - 120

Nitrobenzene-d5 82 04/08/16 05:53 04/11/16 16:56 134 - 132

p-Terphenyl-d14 101 04/08/16 05:53 04/11/16 16:56 165 - 153

Phenol-d5 81 04/08/16 05:53 04/11/16 16:56 111 - 120




o-Terphenyl 83 48 - 125 04/04/16 14:00 04/05/16 09:45 1



Arsenic 2.7 2.3 0.46 mg/Kg ☼ 04/04/16 14:16 04/05/16 14:40 1


0.57 0.13 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Barium 18

0.23 0.034 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Cadmium ND

0.57 0.23 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Chromium 7.6 ^

1.1 0.28 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Lead 3.7

4.6 0.46 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Selenium ND

0.69 0.23 mg/Kg 04/04/16 14:16 04/05/16 14:40 1☼Silver ND


Mercury ND 0.021 0.0084 mg/Kg ☼ 04/05/16 09:15 04/05/16 13:14 1


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Lab Sample ID: 480-97480-12Client Sample ID: DUPMatrix: SolidDate Collected: 03/30/16 11:35

















22 1.6 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼2-Butanone (MEK) ND

22 2.2 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼2-Hexanone ND


22 3.7 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼Acetone ND

4.5 0.22 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼Benzene ND





















4.5 2.0 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼Methylene Chloride ND

4.5 0.22 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼Styrene ND


4.5 0.34 ug/Kg 04/01/16 10:30 04/05/16 20:28 1☼Toluene ND







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Lab Sample ID: 480-97480-12Client Sample ID: DUPMatrix: SolidDate Collected: 03/30/16 11:35


Toluene-d8 (Surr) 99 71 - 125 04/01/16 10:30 04/05/16 20:28 1





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Surrogate SummaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (71-125) (64-126) (72-126) (60-140)

TOL 12DCE BFB DBFM

101 103 104 103480-97480-7

Percent Surrogate Recovery (Acceptance Limits)

SB-8

102 103 106 103480-97480-10 SB-6

101 103 105 102480-97480-11 SB-7

99 102 102 103480-97480-12 DUP

101 109 105 103LCS 480-293913/22-A Lab Control Sample


101 108 107 101LCSD 480-293913/2-A Lab Control Sample Dup

102 100 105 101MB 480-293913/3-A Method Blank

77 76 79 77MB 480-294151/2-A Method Blank

Surrogate Legend

TOL = Toluene-d8 (Surr)

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

DBFM = Dibromofluoromethane (Surr)

Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid


12DCE BFB TOL DBFM

103 99 98 100480-97480-8


SB-2

102 100 99 97480-97480-9 SB-3


105 97 100 100MB 480-294617/2-A Method Blank

Surrogate Legend





Method: 8260C - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Water


12DCE TOL BFB DBFM

108 104 106 109480-97480-1


MW-1

106 103 104 110480-97480-2 MW-3

107 102 103 108480-97480-3 MW-5

109 104 104 112480-97480-4 MW-7

109 105 106 108480-97480-5 DUP

111 103 104 109480-97480-6 FB

107 105 108 111LCS 480-294920/4 Lab Control Sample

106 103 106 108MB 480-294920/6 Method Blank

Surrogate Legend


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Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (39-146) (37-120) (18-120) (34-132) (65-153) (11-120)

TBP FBP 2FP NBZ TPH PHL

95 88 79 85 104 82480-97480-7


SB-8

90 84 78 10281 82480-97480-8 SB-2

77 77 68 9376 72480-97480-9 SB-3

84 80 72 9575 78480-97480-10 SB-6

86 84 74 10182 81480-97480-11 SB-7

93 82 79 9583 84LCS 480-294686/2-A Lab Control Sample

86 87 78 9685 80MB 480-294686/1-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol

FBP = 2-Fluorobiphenyl

2FP = 2-Fluorophenol

NBZ = Nitrobenzene-d5

TPH = p-Terphenyl-d14

PHL = Phenol-d5

Method: 8270D - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (52-132) (48-120) (20-120) (46-120) (67-150) (16-120)

TBP FBP 2FP NBZ TPH PHL

99 86 62 91 75 43480-97480-1


MW-1

113 92 65 7694 46480-97480-2 MW-3

105 88 64 7489 46480-97480-3 MW-5

80 85 59 6991 45480-97480-4 MW-7

97 83 67 8888 49LCS 480-293778/2-A Lab Control Sample

104 88 86 9389 85LCSD 480-293778/5-A Lab Control Sample Dup

94 90 68 103102 46MB 480-293778/1-A Method Blank

Surrogate Legend

TBP = 2,4,6-Tribromophenol

FBP = 2-Fluorobiphenyl

2FP = 2-Fluorophenol

NBZ = Nitrobenzene-d5

TPH = p-Terphenyl-d14

PHL = Phenol-d5

Method: 8015D - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (48-125)

OTPH

81480-97480-7


SB-8

82480-97480-8 SB-2

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Method: 8015D - Diesel Range Organics (DRO) (GC) (Continued)Prep Type: Total/NAMatrix: Solid


OTPH

83480-97480-9


SB-3

84480-97480-10 SB-6

83480-97480-11 SB-7

93480-97480-11 MS SB-7

94480-97480-11 MSD SB-7

94LCS 480-293952/2-A Lab Control Sample

85MB 480-293952/1-A Method Blank

Surrogate Legend

OTPH = o-Terphenyl

Method: 8015D - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Water


OTPH

80480-97480-1


MW-1

85480-97480-2 MW-3

87480-97480-3 MW-5

77480-97480-4 MW-7

95LCS 480-293969/2-A Lab Control Sample

92MB 480-293969/1-A Method Blank

Surrogate Legend

OTPH = o-Terphenyl

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QC Sample ResultsTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Method: 8260C - Volatile Organic Compounds by GC/MS

Client Sample ID: Method BlankLab Sample ID: MB 480-293913/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 293918 Prep Batch: 293913

RL MDL

1,1,1-Trichloroethane ND 5.0 0.36 ug/Kg 04/04/16 11:22 04/04/16 15:02 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.805.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,1,2,2-Tetrachloroethane

ND 0.645.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,1,2-Trichloroethane

ND 1.15.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.605.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,1-Dichloroethane

ND 0.615.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,1-Dichloroethene

ND 0.305.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,2,4-Trichlorobenzene

ND 2.55.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,2-Dibromo-3-Chloropropane

ND 0.395.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,2-Dichlorobenzene


ND 2.55.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,2-Dichloropropane



ND 1.825 ug/Kg 04/04/16 11:22 04/04/16 15:02 12-Butanone (MEK)

ND 2.525 ug/Kg 04/04/16 11:22 04/04/16 15:02 12-Hexanone

ND 1.625 ug/Kg 04/04/16 11:22 04/04/16 15:02 14-Methyl-2-pentanone (MIBK)

6.11 J 4.225 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Acetone

ND 0.245.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Benzene

ND 2.55.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Bromoform

ND 0.455.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Bromomethane

ND 2.55.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Carbon disulfide

ND 0.485.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Carbon tetrachloride

ND 0.655.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Chlorobenzene

ND 0.635.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Dibromochloromethane

ND 1.15.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Chloroethane

ND 0.315.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Chloroform

ND 0.305.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Chloromethane

ND 0.635.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1cis-1,2-Dichloroethene

ND 0.665.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Bromodichloromethane

ND 0.695.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Cyclohexane

ND 0.415.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Dichlorodifluoromethane

ND 0.345.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Ethylbenzene

ND 0.645.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 11,2-Dibromoethane

ND 0.755.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Isopropylbenzene

ND 3.05.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Methyl acetate

ND 0.495.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Methyl tert-butyl ether

ND 0.755.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Methylcyclohexane

9.49 2.35.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Methylene Chloride

ND 0.665.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Tetrachloroethene

0.623 J 0.375.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Toluene

ND 0.515.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1trans-1,2-Dichloroethene

ND 2.25.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1trans-1,3-Dichloropropene

ND 1.15.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Trichloroethene

ND 0.475.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Trichlorofluoromethane

ND 0.605.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Vinyl chloride

ND 0.839.9 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Xylenes, Total

ND 0.715.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1cis-1,3-Dichloropropene

ND 0.255.0 ug/Kg 04/04/16 11:22 04/04/16 15:02 1Styrene

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MB MB

Surrogate

04/04/16 11:22

Dil FacPrepared AnalyzedQualifier Limits%Recovery

102 04/04/16 11:22 04/04/16 15:02 1Toluene-d8 (Surr) 71 - 125

105 04/04/16 11:22 04/04/16 15:02 14-Bromofluorobenzene (Surr) 72 - 126

101 04/04/16 11:22 04/04/16 15:02 1Dibromofluoromethane (Surr) 60 - 140

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-293913/22-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 293918 Prep Batch: 293913

1,1,1-Trichloroethane 49.5 51.7 ug/Kg 104 77 - 121

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

1,1,2,2-Tetrachloroethane 49.5 46.6 ug/Kg 94 80 - 120


1,1,2-Trichloro-1,2,2-trifluoroetha

ne

49.5 52.9 ug/Kg 107 60 - 140

1,1-Dichloroethane 49.5 49.2 ug/Kg 99 73 - 126

1,1-Dichloroethene 49.5 50.4 ug/Kg 102 59 - 125

1,2,4-Trichlorobenzene 49.5 50.8 ug/Kg 103 64 - 120

1,2-Dibromo-3-Chloropropane 49.5 47.9 ug/Kg 97 63 - 124

1,2-Dichlorobenzene 49.5 48.9 ug/Kg 99 75 - 120


1,2-Dichloropropane 49.5 45.3 ug/Kg 92 75 - 124



2-Butanone (MEK) 248 484 * ug/Kg 195 70 - 134

2-Hexanone 248 248 ug/Kg 100 59 - 130

4-Methyl-2-pentanone (MIBK) 248 236 ug/Kg 96 65 - 133

Acetone 248 313 ug/Kg 127 61 - 137

Benzene 49.5 49.4 ug/Kg 100 79 - 127

Bromoform 49.5 53.7 ug/Kg 108 68 - 126

Bromomethane 49.5 47.7 ug/Kg 96 37 - 149

Carbon disulfide 49.5 48.2 ug/Kg 97 64 - 131

Carbon tetrachloride 49.5 53.8 ug/Kg 109 75 - 135

Chlorobenzene 49.5 49.4 ug/Kg 100 76 - 124

Dibromochloromethane 49.5 51.6 ug/Kg 104 76 - 125

Chloroethane 49.5 50.1 ug/Kg 101 69 - 135

Chloroform 49.5 49.1 ug/Kg 99 80 - 118

Chloromethane 49.5 45.2 ug/Kg 91 63 - 127

cis-1,2-Dichloroethene 49.5 48.9 ug/Kg 99 81 - 117

Bromodichloromethane 49.5 49.7 ug/Kg 100 80 - 122

Cyclohexane 49.5 49.8 ug/Kg 101 65 - 106

Dichlorodifluoromethane 49.5 45.4 ug/Kg 92 57 - 142

Ethylbenzene 49.5 49.6 ug/Kg 100 80 - 120

1,2-Dibromoethane 49.5 48.7 ug/Kg 98 78 - 120

Isopropylbenzene 49.5 48.3 ug/Kg 98 72 - 120

Methyl acetate 248 248 ug/Kg 100 55 - 136

Methyl tert-butyl ether 49.5 47.7 ug/Kg 96 63 - 125

Methylcyclohexane 49.5 51.2 ug/Kg 103 60 - 140

Methylene Chloride 49.5 52.3 ug/Kg 106 61 - 127

Tetrachloroethene 49.5 56.9 ug/Kg 115 74 - 122

Toluene 49.5 49.4 ug/Kg 100 74 - 128

trans-1,2-Dichloroethene 49.5 50.3 ug/Kg 102 78 - 126

Trichloroethene 49.5 49.5 ug/Kg 100 77 - 129

Trichlorofluoromethane 49.5 55.2 ug/Kg 112 65 - 146

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Vinyl chloride 49.5 50.0 ug/Kg 101 61 - 133

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

cis-1,3-Dichloropropene 49.5 48.9 ug/Kg 99 82 - 120

Styrene 49.5 47.8 ug/Kg 97 80 - 120

1,2-Dichloroethane-d4 (Surr) 64 - 126

Surrogate

109

LCS LCS

Qualifier Limits%Recovery

101Toluene-d8 (Surr) 71 - 125

1054-Bromofluorobenzene (Surr) 72 - 126

103Dibromofluoromethane (Surr) 60 - 140

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 480-293913/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 293918 Prep Batch: 293913

1,1,1-Trichloroethane 49.2 49.3 ug/Kg 100 77 - 121 5 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

1,1,2,2-Tetrachloroethane 49.2 47.2 ug/Kg 96 80 - 120 1 20

1,1,2-Trichloroethane 49.2 47.0 ug/Kg 96 78 - 122 1 20


ne

49.2 49.2 ug/Kg 100 60 - 140 7 20

1,1-Dichloroethane 49.2 47.0 ug/Kg 96 73 - 126 5 20

1,1-Dichloroethene 49.2 47.6 ug/Kg 97 59 - 125 6 20

1,2,4-Trichlorobenzene 49.2 50.4 ug/Kg 102 64 - 120 1 20

1,2-Dibromo-3-Chloropropane 49.2 49.3 ug/Kg 100 63 - 124 3 20

1,2-Dichlorobenzene 49.2 48.8 ug/Kg 99 75 - 120 0 20

1,2-Dichloroethane 49.2 47.1 ug/Kg 96 77 - 122 1 20

1,2-Dichloropropane 49.2 44.6 ug/Kg 91 75 - 124 1 20



2-Butanone (MEK) 246 485 * ug/Kg 197 70 - 134 0 20

2-Hexanone 246 255 ug/Kg 104 59 - 130 3 20

4-Methyl-2-pentanone (MIBK) 246 242 ug/Kg 98 65 - 133 2 20

Acetone 246 317 ug/Kg 129 61 - 137 1 20

Benzene 49.2 47.1 ug/Kg 96 79 - 127 5 20

Bromoform 49.2 54.5 ug/Kg 111 68 - 126 2 20

Bromomethane 49.2 46.9 ug/Kg 95 37 - 149 2 20

Carbon disulfide 49.2 45.0 ug/Kg 91 64 - 131 7 20

Carbon tetrachloride 49.2 50.8 ug/Kg 103 75 - 135 6 20

Chlorobenzene 49.2 48.3 ug/Kg 98 76 - 124 2 20

Dibromochloromethane 49.2 52.2 ug/Kg 106 76 - 125 1 20

Chloroethane 49.2 48.1 ug/Kg 98 69 - 135 4 20

Chloroform 49.2 47.2 ug/Kg 96 80 - 118 4 20

Chloromethane 49.2 43.0 ug/Kg 87 63 - 127 5 20

cis-1,2-Dichloroethene 49.2 46.6 ug/Kg 95 81 - 117 5 20

Bromodichloromethane 49.2 49.1 ug/Kg 100 80 - 122 1 20

Cyclohexane 49.2 46.9 ug/Kg 95 65 - 106 6 20

Dichlorodifluoromethane 49.2 42.2 ug/Kg 86 57 - 142 7 20

Ethylbenzene 49.2 48.4 ug/Kg 98 80 - 120 2 20

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Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 480-293913/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 293918 Prep Batch: 293913

1,2-Dibromoethane 49.2 49.6 ug/Kg 101 78 - 120 2 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Isopropylbenzene 49.2 47.0 ug/Kg 96 72 - 120 3 20

Methyl acetate 246 247 ug/Kg 100 55 - 136 0 20

Methyl tert-butyl ether 49.2 47.8 ug/Kg 97 63 - 125 0 20

Methylcyclohexane 49.2 48.0 ug/Kg 98 60 - 140 6 20

Methylene Chloride 49.2 53.7 ug/Kg 109 61 - 127 3 20

Tetrachloroethene 49.2 54.4 ug/Kg 111 74 - 122 5 20

Toluene 49.2 47.5 ug/Kg 97 74 - 128 4 20

trans-1,2-Dichloroethene 49.2 47.3 ug/Kg 96 78 - 126 6 20

Trichloroethene 49.2 47.4 ug/Kg 96 77 - 129 4 20

Trichlorofluoromethane 49.2 52.6 ug/Kg 107 65 - 146 5 20

Vinyl chloride 49.2 47.2 ug/Kg 96 61 - 133 6 20

cis-1,3-Dichloropropene 49.2 48.0 ug/Kg 98 82 - 120 2 20

Styrene 49.2 47.3 ug/Kg 96 80 - 120 1 20


Surrogate

108

LCSD LCSD






RL MDL

1,1,1-Trichloroethane ND 4.9 0.36 ug/Kg 04/05/16 18:02 04/05/16 19:24 1

MB MB


ND 0.804.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,1,2,2-Tetrachloroethane

ND 0.644.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,1,2-Trichloroethane

ND 1.14.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,1,2-Trichloro-1,2,2-trifluoroethane


ND 0.604.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,1-Dichloroethene

ND 0.304.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,2,4-Trichlorobenzene

ND 2.54.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,2-Dibromo-3-Chloropropane



ND 2.54.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,2-Dichloropropane



ND 1.825 ug/Kg 04/05/16 18:02 04/05/16 19:24 12-Butanone (MEK)

ND 2.525 ug/Kg 04/05/16 18:02 04/05/16 19:24 12-Hexanone

ND 1.625 ug/Kg 04/05/16 18:02 04/05/16 19:24 14-Methyl-2-pentanone (MIBK)

5.77 J 4.225 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Acetone

ND 0.244.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Benzene

ND 2.54.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Bromoform

ND 0.444.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Bromomethane

ND 2.54.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Carbon disulfide

ND 0.484.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Carbon tetrachloride

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RL MDL

Chlorobenzene ND 4.9 0.65 ug/Kg 04/05/16 18:02 04/05/16 19:24 1

MB MB


ND 0.634.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Dibromochloromethane

ND 1.14.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Chloroethane

ND 0.304.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Chloroform

ND 0.304.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Chloromethane

ND 0.634.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1cis-1,2-Dichloroethene

ND 0.664.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Bromodichloromethane

ND 0.694.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Cyclohexane

ND 0.414.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Dichlorodifluoromethane

ND 0.344.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Ethylbenzene

ND 0.634.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 11,2-Dibromoethane

ND 0.744.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Isopropylbenzene

ND 3.04.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Methyl acetate

ND 0.484.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Methyl tert-butyl ether

ND 0.754.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Methylcyclohexane

2.92 J 2.34.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Methylene Chloride

ND 0.664.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Tetrachloroethene

0.851 J 0.374.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Toluene

ND 0.514.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1trans-1,2-Dichloroethene

ND 2.24.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1trans-1,3-Dichloropropene

ND 1.14.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Trichloroethene

ND 0.474.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Trichlorofluoromethane

ND 0.604.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Vinyl chloride

ND 0.839.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Xylenes, Total

ND 0.714.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1cis-1,3-Dichloropropene

ND 0.254.9 ug/Kg 04/05/16 18:02 04/05/16 19:24 1Styrene


MB MB

Surrogate

04/05/16 18:02


77 04/05/16 18:02 04/05/16 19:24 1Toluene-d8 (Surr) 71 - 125





Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1,2,2-Tetrachloroethane 49.8 44.9 ug/Kg 90 80 - 120



ne

49.8 55.4 ug/Kg 111 60 - 140


1,1-Dichloroethene 49.8 52.2 ug/Kg 105 59 - 125

1,2,4-Trichlorobenzene 49.8 51.2 ug/Kg 103 64 - 120

1,2-Dibromo-3-Chloropropane 49.8 44.9 ug/Kg 90 63 - 124


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Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,2-Dichloropropane 49.8 46.8 ug/Kg 94 75 - 124



2-Butanone (MEK) 249 263 ug/Kg 106 70 - 134

2-Hexanone 249 241 ug/Kg 97 59 - 130


Acetone 249 334 ug/Kg 134 61 - 137

Benzene 49.8 49.9 ug/Kg 100 79 - 127

Bromoform 49.8 52.0 ug/Kg 104 68 - 126

Bromomethane 49.8 50.8 ug/Kg 102 37 - 149

Carbon disulfide 49.8 49.5 ug/Kg 99 64 - 131

Carbon tetrachloride 49.8 54.1 ug/Kg 109 75 - 135

Chlorobenzene 49.8 49.6 ug/Kg 100 76 - 124

Dibromochloromethane 49.8 52.9 ug/Kg 106 76 - 125

Chloroethane 49.8 50.7 ug/Kg 102 69 - 135

Chloroform 49.8 50.8 ug/Kg 102 80 - 118

Chloromethane 49.8 46.5 ug/Kg 93 63 - 127

cis-1,2-Dichloroethene 49.8 49.0 ug/Kg 98 81 - 117

Bromodichloromethane 49.8 50.6 ug/Kg 102 80 - 122

Cyclohexane 49.8 49.8 ug/Kg 100 65 - 106

Dichlorodifluoromethane 49.8 55.9 ug/Kg 112 57 - 142

Ethylbenzene 49.8 50.0 ug/Kg 100 80 - 120

1,2-Dibromoethane 49.8 49.6 ug/Kg 100 78 - 120

Isopropylbenzene 49.8 47.9 ug/Kg 96 72 - 120


Methyl tert-butyl ether 49.8 48.6 ug/Kg 98 63 - 125

Methylcyclohexane 49.8 51.3 ug/Kg 103 60 - 140

Methylene Chloride 49.8 46.5 ug/Kg 93 61 - 127

Tetrachloroethene 49.8 54.1 ug/Kg 109 74 - 122

Toluene 49.8 50.4 ug/Kg 101 74 - 128

trans-1,2-Dichloroethene 49.8 49.9 ug/Kg 100 78 - 126

Trichloroethene 49.8 49.6 ug/Kg 100 77 - 129

Trichlorofluoromethane 49.8 56.8 ug/Kg 114 65 - 146

Vinyl chloride 49.8 50.3 ug/Kg 101 61 - 133

cis-1,3-Dichloropropene 49.8 48.1 ug/Kg 97 82 - 120

Styrene 49.8 48.6 ug/Kg 98 80 - 120


Surrogate

101

LCS LCS





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RL MDL

1,1,1-Trichloroethane ND 100 28 ug/Kg 04/07/16 17:02 04/08/16 12:15 1

MB MB


ND 16100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,1,2,2-Tetrachloroethane

ND 21100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,1,2-Trichloroethane

ND 50100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 31100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,1-Dichloroethane

ND 34100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,1-Dichloroethene

ND 38100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2,4-Trichlorobenzene

ND 50100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2-Dibromo-3-Chloropropane

ND 25100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2-Dichlorobenzene

ND 41100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2-Dichloroethane

ND 16100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2-Dichloropropane



ND 300500 ug/Kg 04/07/16 17:02 04/08/16 12:15 12-Butanone (MEK)

ND 200500 ug/Kg 04/07/16 17:02 04/08/16 12:15 12-Hexanone

ND 32500 ug/Kg 04/07/16 17:02 04/08/16 12:15 14-Methyl-2-pentanone (MIBK)

ND 410500 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Acetone

ND 19100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Benzene

ND 50100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Bromoform

ND 22100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Bromomethane

ND 45100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Carbon disulfide

ND 25100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Carbon tetrachloride

ND 13100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Chlorobenzene

ND 48100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Dibromochloromethane

ND 21100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Chloroethane

ND 68100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Chloroform

ND 24100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Chloromethane

ND 27100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1cis-1,2-Dichloroethene

ND 20100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Bromodichloromethane

ND 22100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Cyclohexane

ND 43100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Dichlorodifluoromethane

ND 29100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Ethylbenzene

ND 17100 ug/Kg 04/07/16 17:02 04/08/16 12:15 11,2-Dibromoethane

ND 15100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Isopropylbenzene

ND 47100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Methyl acetate

ND 38100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Methyl tert-butyl ether

ND 47100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Methylcyclohexane

29.9 J 20100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Methylene Chloride

ND 13100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Tetrachloroethene

ND 27100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Toluene

ND 24100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1trans-1,2-Dichloroethene

ND 9.8100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1trans-1,3-Dichloropropene

ND 28100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Trichloroethene

ND 47100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Trichlorofluoromethane

ND 33100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Vinyl chloride

ND 55200 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Xylenes, Total

ND 24100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1cis-1,3-Dichloropropene

ND 24100 ug/Kg 04/07/16 17:02 04/08/16 12:15 1Styrene

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MB MB

Surrogate

04/07/16 17:02


100 04/07/16 17:02 04/08/16 12:15 1Toluene-d8 (Surr) 50 - 149




1,1,1-Trichloroethane 2490 2050 ug/Kg 82 68 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1,2,2-Tetrachloroethane 2490 2100 ug/Kg 84 73 - 119

1,1,2-Trichloroethane 2490 2450 ug/Kg 98 81 - 115


ne

2490 2030 ug/Kg 82 10 - 179

1,1-Dichloroethane 2490 2340 ug/Kg 94 78 - 121

1,1-Dichloroethene 2490 2090 ug/Kg 84 48 - 133

1,2,4-Trichlorobenzene 2490 2290 ug/Kg 92 70 - 140

1,2-Dibromo-3-Chloropropane 2490 1900 ug/Kg 76 56 - 122

1,2-Dichlorobenzene 2490 2330 ug/Kg 94 78 - 125

1,2-Dichloroethane 2490 2390 ug/Kg 96 74 - 127

1,2-Dichloropropane 2490 2360 ug/Kg 95 81 - 115



2-Butanone (MEK) 12400 9680 ug/Kg 78 54 - 149

2-Hexanone 12400 11200 ug/Kg 90 59 - 127


Acetone 12400 8010 ug/Kg 64 47 - 141

Benzene 2490 2290 ug/Kg 92 77 - 125

Bromoform 2490 2100 ug/Kg 85 48 - 125

Bromomethane 2490 2220 ug/Kg 90 39 - 149

Carbon disulfide 2490 1990 ug/Kg 80 40 - 136

Carbon tetrachloride 2490 2130 ug/Kg 86 54 - 135

Chlorobenzene 2490 2380 ug/Kg 96 76 - 126

Dibromochloromethane 2490 2370 ug/Kg 95 64 - 118

Chloroethane 2490 2110 ug/Kg 85 23 - 164

Chloroform 2490 2280 ug/Kg 92 78 - 118

Chloromethane 2490 2730 ug/Kg 110 61 - 124

cis-1,2-Dichloroethene 2490 2310 ug/Kg 93 79 - 124

Bromodichloromethane 2490 2350 ug/Kg 95 71 - 121

Cyclohexane 2490 1700 ug/Kg 69 49 - 129

Dichlorodifluoromethane 2490 3570 ug/Kg 144 10 - 150

Ethylbenzene 2490 2300 ug/Kg 93 78 - 124

1,2-Dibromoethane 2490 2450 ug/Kg 99 81 - 119

Isopropylbenzene 2490 2400 ug/Kg 97 76 - 119


Methyl tert-butyl ether 2490 2210 ug/Kg 89 67 - 137

Methylcyclohexane 2490 2210 ug/Kg 89 50 - 130

Methylene Chloride 2490 2410 ug/Kg 97 75 - 118

Tetrachloroethene 2490 2560 ug/Kg 103 73 - 133

Toluene 2490 2350 ug/Kg 94 75 - 124

trans-1,2-Dichloroethene 2490 2380 ug/Kg 96 74 - 129

Trichloroethene 2490 2430 ug/Kg 98 75 - 131

Trichlorofluoromethane 2490 3160 ug/Kg 127 29 - 158

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Vinyl chloride 2490 2580 ug/Kg 104 59 - 124

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

cis-1,3-Dichloropropene 2490 2500 ug/Kg 101 75 - 121

Styrene 2490 2400 ug/Kg 96 84 - 119


Surrogate

100

LCS LCS





Client Sample ID: Method BlankLab Sample ID: MB 480-294920/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 294920

RL MDL


MB MB


ND 0.211.0 ug/L 04/09/16 09:55 11,1,2,2-Tetrachloroethane

ND 0.231.0 ug/L 04/09/16 09:55 11,1,2-Trichloroethane

ND 0.311.0 ug/L 04/09/16 09:55 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.381.0 ug/L 04/09/16 09:55 11,1-Dichloroethane

ND 0.291.0 ug/L 04/09/16 09:55 11,1-Dichloroethene

ND 0.411.0 ug/L 04/09/16 09:55 11,2,4-Trichlorobenzene

ND 0.391.0 ug/L 04/09/16 09:55 11,2-Dibromo-3-Chloropropane

ND 0.791.0 ug/L 04/09/16 09:55 11,2-Dichlorobenzene

ND 0.211.0 ug/L 04/09/16 09:55 11,2-Dichloroethane

ND 0.721.0 ug/L 04/09/16 09:55 11,2-Dichloropropane



ND 1.310 ug/L 04/09/16 09:55 12-Butanone (MEK)

ND 1.25.0 ug/L 04/09/16 09:55 12-Hexanone

ND 2.15.0 ug/L 04/09/16 09:55 14-Methyl-2-pentanone (MIBK)

ND 3.010 ug/L 04/09/16 09:55 1Acetone

ND 0.411.0 ug/L 04/09/16 09:55 1Benzene

ND 0.261.0 ug/L 04/09/16 09:55 1Bromoform

ND 0.691.0 ug/L 04/09/16 09:55 1Bromomethane

ND 0.191.0 ug/L 04/09/16 09:55 1Carbon disulfide

ND 0.271.0 ug/L 04/09/16 09:55 1Carbon tetrachloride

ND 0.751.0 ug/L 04/09/16 09:55 1Chlorobenzene

ND 0.321.0 ug/L 04/09/16 09:55 1Dibromochloromethane

ND 0.321.0 ug/L 04/09/16 09:55 1Chloroethane

ND 0.341.0 ug/L 04/09/16 09:55 1Chloroform

ND 0.351.0 ug/L 04/09/16 09:55 1Chloromethane

ND 0.811.0 ug/L 04/09/16 09:55 1cis-1,2-Dichloroethene

ND 0.391.0 ug/L 04/09/16 09:55 1Bromodichloromethane

ND 0.181.0 ug/L 04/09/16 09:55 1Cyclohexane

ND 0.681.0 ug/L 04/09/16 09:55 1Dichlorodifluoromethane

ND 0.741.0 ug/L 04/09/16 09:55 1Ethylbenzene

ND 0.731.0 ug/L 04/09/16 09:55 11,2-Dibromoethane

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Client Sample ID: Method BlankLab Sample ID: MB 480-294920/6Matrix: Water Prep Type: Total/NAAnalysis Batch: 294920

RL MDL

Isopropylbenzene ND 1.0 0.79 ug/L 04/09/16 09:55 1

MB MB


ND 1.32.5 ug/L 04/09/16 09:55 1Methyl acetate

ND 0.161.0 ug/L 04/09/16 09:55 1Methyl tert-butyl ether

ND 0.161.0 ug/L 04/09/16 09:55 1Methylcyclohexane

ND 0.441.0 ug/L 04/09/16 09:55 1Methylene Chloride

ND 0.361.0 ug/L 04/09/16 09:55 1Tetrachloroethene

ND 0.511.0 ug/L 04/09/16 09:55 1Toluene

ND 0.901.0 ug/L 04/09/16 09:55 1trans-1,2-Dichloroethene

ND 0.371.0 ug/L 04/09/16 09:55 1trans-1,3-Dichloropropene

ND 0.461.0 ug/L 04/09/16 09:55 1Trichloroethene

ND 0.881.0 ug/L 04/09/16 09:55 1Trichlorofluoromethane

ND 0.901.0 ug/L 04/09/16 09:55 1Vinyl chloride

ND 0.662.0 ug/L 04/09/16 09:55 1Xylenes, Total

ND 0.361.0 ug/L 04/09/16 09:55 1cis-1,3-Dichloropropene

ND 0.731.0 ug/L 04/09/16 09:55 1Styrene


MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

103 04/09/16 09:55 1Toluene-d8 (Surr) 71 - 126

106 04/09/16 09:55 14-Bromofluorobenzene (Surr) 73 - 120

108 04/09/16 09:55 1Dibromofluoromethane (Surr) 60 - 140

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-294920/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 294920

1,1,1-Trichloroethane 25.0 26.4 ug/L 105 73 - 126

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1,2,2-Tetrachloroethane 25.0 21.7 ug/L 87 70 - 126

1,1,2-Trichloroethane 25.0 23.5 ug/L 94 76 - 122


ne

25.0 28.2 ug/L 113 52 - 148

1,1-Dichloroethane 25.0 24.0 ug/L 96 71 - 129

1,1-Dichloroethene 25.0 25.4 ug/L 102 58 - 121

1,2,4-Trichlorobenzene 25.0 23.8 ug/L 95 70 - 122

1,2-Dibromo-3-Chloropropane 25.0 20.6 ug/L 82 56 - 134

1,2-Dichlorobenzene 25.0 23.0 ug/L 92 80 - 124

1,2-Dichloroethane 25.0 23.4 ug/L 94 75 - 127

1,2-Dichloropropane 25.0 24.0 ug/L 96 76 - 120



2-Butanone (MEK) 125 110 ug/L 88 57 - 140

2-Hexanone 125 109 ug/L 87 65 - 127

4-Methyl-2-pentanone (MIBK) 125 106 ug/L 85 71 - 125

Acetone 125 121 ug/L 97 56 - 142

Benzene 25.0 23.8 ug/L 95 71 - 124

Bromoform 25.0 25.3 ug/L 101 52 - 132

Bromomethane 25.0 29.4 ug/L 117 55 - 144

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Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-294920/4Matrix: Water Prep Type: Total/NAAnalysis Batch: 294920

Carbon disulfide 25.0 23.1 ug/L 92 59 - 134

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Carbon tetrachloride 25.0 27.5 ug/L 110 72 - 134

Chlorobenzene 25.0 23.7 ug/L 95 72 - 120

Dibromochloromethane 25.0 25.3 ug/L 101 75 - 125

Chloroethane 25.0 28.0 ug/L 112 69 - 136

Chloroform 25.0 24.3 ug/L 97 73 - 127

Chloromethane 25.0 25.9 ug/L 104 68 - 124

cis-1,2-Dichloroethene 25.0 24.4 ug/L 98 74 - 124

Bromodichloromethane 25.0 24.7 ug/L 99 80 - 122

Cyclohexane 25.0 25.7 ug/L 103 59 - 135

Dichlorodifluoromethane 25.0 32.1 ug/L 129 59 - 135

Ethylbenzene 25.0 24.0 ug/L 96 77 - 123

1,2-Dibromoethane 25.0 23.4 ug/L 93 77 - 120

Isopropylbenzene 25.0 23.5 ug/L 94 77 - 122

Methyl acetate 125 107 ug/L 85 74 - 133

Methyl tert-butyl ether 25.0 24.2 ug/L 97 64 - 127

Methylcyclohexane 25.0 26.5 ug/L 106 61 - 138

Methylene Chloride 25.0 23.1 ug/L 92 57 - 132

Tetrachloroethene 25.0 25.3 ug/L 101 74 - 122

Toluene 25.0 23.6 ug/L 95 80 - 122

trans-1,2-Dichloroethene 25.0 24.6 ug/L 98 73 - 127

Trichloroethene 25.0 25.1 ug/L 100 74 - 123

Trichlorofluoromethane 25.0 29.3 ug/L 117 62 - 152

Vinyl chloride 25.0 26.3 ug/L 105 65 - 133

cis-1,3-Dichloropropene 25.0 24.2 ug/L 97 74 - 124

Styrene 25.0 23.9 ug/L 96 70 - 130


Surrogate

107

LCS LCS





Method: 8270D - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 480-293778/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 293950 Prep Batch: 293778

RL MDL

Biphenyl ND 5.0 0.65 ug/L 04/02/16 10:06 04/04/16 22:15 1

MB MB


ND 0.525.0 ug/L 04/02/16 10:06 04/04/16 22:15 1bis (2-chloroisopropyl) ether

ND 0.485.0 ug/L 04/02/16 10:06 04/04/16 22:15 12,4,5-Trichlorophenol

ND 0.615.0 ug/L 04/02/16 10:06 04/04/16 22:15 12,4,6-Trichlorophenol

ND 0.515.0 ug/L 04/02/16 10:06 04/04/16 22:15 12,4-Dichlorophenol

ND 0.505.0 ug/L 04/02/16 10:06 04/04/16 22:15 12,4-Dimethylphenol

ND 2.210 ug/L 04/02/16 10:06 04/04/16 22:15 12,4-Dinitrophenol

ND 0.455.0 ug/L 04/02/16 10:06 04/04/16 22:15 12,4-Dinitrotoluene

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RL MDL

2,6-Dinitrotoluene ND 5.0 0.40 ug/L 04/02/16 10:06 04/04/16 22:15 1

MB MB


ND 0.465.0 ug/L 04/02/16 10:06 04/04/16 22:15 12-Chloronaphthalene

ND 0.535.0 ug/L 04/02/16 10:06 04/04/16 22:15 12-Chlorophenol

ND 0.605.0 ug/L 04/02/16 10:06 04/04/16 22:15 12-Methylnaphthalene

ND 0.405.0 ug/L 04/02/16 10:06 04/04/16 22:15 12-Methylphenol

ND 0.4210 ug/L 04/02/16 10:06 04/04/16 22:15 12-Nitroaniline

ND 0.485.0 ug/L 04/02/16 10:06 04/04/16 22:15 12-Nitrophenol

ND 0.405.0 ug/L 04/02/16 10:06 04/04/16 22:15 13,3'-Dichlorobenzidine


ND 2.210 ug/L 04/02/16 10:06 04/04/16 22:15 14,6-Dinitro-2-methylphenol

ND 0.455.0 ug/L 04/02/16 10:06 04/04/16 22:15 14-Bromophenyl phenyl ether

ND 0.455.0 ug/L 04/02/16 10:06 04/04/16 22:15 14-Chloro-3-methylphenol

ND 0.595.0 ug/L 04/02/16 10:06 04/04/16 22:15 14-Chloroaniline

ND 0.355.0 ug/L 04/02/16 10:06 04/04/16 22:15 14-Chlorophenyl phenyl ether

ND 0.3610 ug/L 04/02/16 10:06 04/04/16 22:15 14-Methylphenol


ND 1.510 ug/L 04/02/16 10:06 04/04/16 22:15 14-Nitrophenol

ND 0.415.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Acenaphthene

ND 0.385.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Acenaphthylene

ND 0.545.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Acetophenone

ND 0.285.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Anthracene

ND 0.465.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Atrazine

0.611 J 0.275.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzaldehyde

ND 0.365.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzo(a)anthracene

ND 0.475.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzo(a)pyrene

ND 0.345.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzo(b)fluoranthene

ND 0.355.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzo(g,h,i)perylene

ND 0.735.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Benzo(k)fluoranthene

ND 0.355.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Bis(2-chloroethoxy)methane

ND 0.405.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Bis(2-chloroethyl)ether

ND 2.25.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Bis(2-ethylhexyl) phthalate

ND 1.05.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Butyl benzyl phthalate

ND 2.25.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Caprolactam

ND 0.305.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Carbazole

ND 0.335.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Chrysene

ND 0.315.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Di-n-butyl phthalate

0.610 J 0.475.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Di-n-octyl phthalate

ND 0.425.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Dibenz(a,h)anthracene

ND 0.5110 ug/L 04/02/16 10:06 04/04/16 22:15 1Dibenzofuran

ND 0.225.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Diethyl phthalate

ND 0.365.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Dimethyl phthalate

ND 0.405.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Fluoranthene

ND 0.365.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Fluorene

ND 0.515.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Hexachlorobenzene

ND 0.685.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Hexachlorobutadiene

ND 0.595.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Hexachlorocyclopentadiene

ND 0.595.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Hexachloroethane

ND 0.475.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Indeno(1,2,3-cd)pyrene

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RL MDL

Isophorone ND 5.0 0.43 ug/L 04/02/16 10:06 04/04/16 22:15 1

MB MB


ND 0.545.0 ug/L 04/02/16 10:06 04/04/16 22:15 1N-Nitrosodi-n-propylamine

ND 0.515.0 ug/L 04/02/16 10:06 04/04/16 22:15 1N-Nitrosodiphenylamine

ND 0.765.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Naphthalene

ND 0.295.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Nitrobenzene

ND 2.210 ug/L 04/02/16 10:06 04/04/16 22:15 1Pentachlorophenol

ND 0.445.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Phenanthrene

ND 0.395.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Phenol

ND 0.345.0 ug/L 04/02/16 10:06 04/04/16 22:15 1Pyrene

2,4,6-Tribromophenol 94 52 - 132 04/04/16 22:15 1

MB MB

Surrogate

04/02/16 10:06


90 04/02/16 10:06 04/04/16 22:15 12-Fluorobiphenyl 48 - 120

68 04/02/16 10:06 04/04/16 22:15 12-Fluorophenol 20 - 120

102 04/02/16 10:06 04/04/16 22:15 1Nitrobenzene-d5 46 - 120

103 04/02/16 10:06 04/04/16 22:15 1p-Terphenyl-d14 67 - 150

46 04/02/16 10:06 04/04/16 22:15 1Phenol-d5 16 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 480-293778/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 293950 Prep Batch: 293778

Biphenyl 16.0 14.0 ug/L 88 30 - 140

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

bis (2-chloroisopropyl) ether 16.0 13.9 ug/L 87 28 - 136

2,4,5-Trichlorophenol 16.0 14.9 ug/L 93 65 - 126

2,4,6-Trichlorophenol 16.0 12.9 ug/L 81 64 - 120

2,4-Dichlorophenol 16.0 15.4 ug/L 96 64 - 120

2,4-Dimethylphenol 16.0 14.5 ug/L 90 57 - 120

2,4-Dinitrophenol 32.0 25.8 ug/L 81 42 - 153

2,4-Dinitrotoluene 16.0 15.2 ug/L 95 65 - 154

2,6-Dinitrotoluene 16.0 15.8 ug/L 98 74 - 134

2-Chloronaphthalene 16.0 13.9 ug/L 87 41 - 124

2-Chlorophenol 16.0 14.0 ug/L 87 48 - 120

2-Methylnaphthalene 16.0 14.2 ug/L 89 34 - 122

2-Methylphenol 16.0 13.1 ug/L 82 39 - 120

2-Nitroaniline 16.0 16.5 ug/L 103 67 - 136

2-Nitrophenol 16.0 15.0 ug/L 94 59 - 120

3,3'-Dichlorobenzidine 32.0 30.2 ug/L 94 33 - 140


4,6-Dinitro-2-methylphenol 32.0 29.5 ug/L 92 64 - 159

4-Bromophenyl phenyl ether 16.0 15.2 ug/L 95 71 - 126

4-Chloro-3-methylphenol 16.0 16.1 ug/L 100 64 - 120

4-Chloroaniline 16.0 11.7 ug/L 73 10 - 130

4-Chlorophenyl phenyl ether 16.0 14.2 ug/L 89 71 - 122

4-Methylphenol 16.0 12.8 ug/L 80 39 - 120


4-Nitrophenol 32.0 22.2 ug/L 69 16 - 120

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Acenaphthene 16.0 13.8 ug/L 86 60 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthylene 16.0 14.4 ug/L 90 63 - 120

Acetophenone 16.0 14.2 ug/L 89 45 - 120

Anthracene 16.0 14.8 ug/L 93 58 - 148

Atrazine 32.0 32.7 ug/L 102 56 - 179

Benzaldehyde 32.0 25.1 ug/L 78 30 - 140

Benzo(a)anthracene 16.0 14.6 ug/L 91 55 - 151

Benzo(a)pyrene 16.0 14.1 ug/L 88 60 - 145

Benzo(b)fluoranthene 16.0 15.1 ug/L 95 54 - 140

Benzo(g,h,i)perylene 16.0 15.4 ug/L 96 66 - 152

Benzo(k)fluoranthene 16.0 14.4 ug/L 90 51 - 153

Bis(2-chloroethoxy)methane 16.0 15.1 ug/L 94 50 - 128

Bis(2-chloroethyl)ether 16.0 13.5 ug/L 85 51 - 120

Bis(2-ethylhexyl) phthalate 16.0 15.8 ug/L 99 53 - 158

Butyl benzyl phthalate 16.0 16.1 ug/L 101 58 - 163

Caprolactam 32.0 12.3 ug/L 39 14 - 130

Carbazole 16.0 15.9 ug/L 100 59 - 148

Chrysene 16.0 14.7 ug/L 92 69 - 140

Di-n-butyl phthalate 16.0 17.0 ug/L 106 58 - 149

Di-n-octyl phthalate 16.0 15.8 ug/L 99 55 - 167

Dibenz(a,h)anthracene 16.0 14.5 ug/L 91 57 - 148

Dibenzofuran 16.0 14.7 ug/L 92 49 - 137

Diethyl phthalate 16.0 16.3 ug/L 102 59 - 146

Dimethyl phthalate 16.0 16.5 ug/L 103 59 - 141

Fluoranthene 16.0 15.6 ug/L 98 55 - 147

Fluorene 16.0 14.7 ug/L 92 55 - 143

Hexachlorobenzene 16.0 13.3 ug/L 83 14 - 130

Hexachlorobutadiene 16.0 13.0 ug/L 81 14 - 130

Hexachlorocyclopentadiene 16.0 10.8 ug/L 68 13 - 130

Hexachloroethane 16.0 13.2 ug/L 82 14 - 130

Indeno(1,2,3-cd)pyrene 16.0 14.7 ug/L 92 69 - 146

Isophorone 16.0 15.8 ug/L 99 48 - 133

N-Nitrosodi-n-propylamine 16.0 14.1 ug/L 88 56 - 120

Naphthalene 16.0 13.9 ug/L 87 35 - 130

Nitrobenzene 16.0 15.0 ug/L 94 45 - 123

Pentachlorophenol 32.0 25.0 ug/L 78 39 - 136

Phenanthrene 16.0 15.0 ug/L 94 57 - 147

Phenol 16.0 8.01 ug/L 50 17 - 120

Pyrene 16.0 15.2 ug/L 95 58 - 136

2,4,6-Tribromophenol 52 - 132

Surrogate

97

LCS LCS


832-Fluorobiphenyl 48 - 120

672-Fluorophenol 20 - 120

88Nitrobenzene-d5 46 - 120

88p-Terphenyl-d14 67 - 150

49Phenol-d5 16 - 120

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Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 480-293778/5-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 293950 Prep Batch: 293778

Biphenyl 16.0 14.9 ug/L 93 30 - 140 6 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

bis (2-chloroisopropyl) ether 16.0 14.2 ug/L 89 28 - 136 2 24

2,4,5-Trichlorophenol 16.0 16.1 ug/L 101 65 - 126 8 18

2,4,6-Trichlorophenol 16.0 13.5 ug/L 85 64 - 120 5 19

2,4-Dichlorophenol 16.0 15.9 ug/L 99 64 - 120 3 19

2,4-Dimethylphenol 16.0 14.9 ug/L 93 57 - 120 3 42

2,4-Dinitrophenol 32.0 26.7 ug/L 83 42 - 153 3 22

2,4-Dinitrotoluene 16.0 16.1 ug/L 101 65 - 154 6 20

2,6-Dinitrotoluene 16.0 15.7 ug/L 98 74 - 134 1 15

2-Chloronaphthalene 16.0 14.8 ug/L 92 41 - 124 6 21

2-Chlorophenol 16.0 14.4 ug/L 90 48 - 120 3 25

2-Methylnaphthalene 16.0 14.5 ug/L 90 34 - 122 2 21

2-Methylphenol 16.0 14.9 ug/L 93 39 - 120 12 27

2-Nitroaniline 16.0 17.7 ug/L 111 67 - 136 7 15

2-Nitrophenol 16.0 15.6 ug/L 98 59 - 120 4 18

3,3'-Dichlorobenzidine 32.0 31.1 ug/L 97 33 - 140 3 25


4,6-Dinitro-2-methylphenol 32.0 29.8 ug/L 93 64 - 159 1 15

4-Bromophenyl phenyl ether 16.0 16.0 ug/L 100 71 - 126 5 15

4-Chloro-3-methylphenol 16.0 16.0 ug/L 100 64 - 120 1 27

4-Chloroaniline 16.0 11.1 ug/L 69 10 - 130 5 22

4-Chlorophenyl phenyl ether 16.0 15.7 ug/L 98 71 - 122 10 16

4-Methylphenol 16.0 14.7 ug/L 92 39 - 120 14 24


4-Nitrophenol 32.0 32.9 ug/L 103 16 - 120 39 48

Acenaphthene 16.0 14.8 ug/L 93 60 - 120 7 24

Acenaphthylene 16.0 15.0 ug/L 94 63 - 120 4 18

Acetophenone 16.0 14.6 ug/L 91 45 - 120 3 20

Anthracene 16.0 16.2 ug/L 101 58 - 148 9 15

Atrazine 32.0 33.8 ug/L 106 56 - 179 3 20

Benzaldehyde 32.0 21.9 ug/L 68 30 - 140 14 20

Benzo(a)anthracene 16.0 15.8 ug/L 99 55 - 151 8 15

Benzo(a)pyrene 16.0 14.9 ug/L 93 60 - 145 5 15

Benzo(b)fluoranthene 16.0 15.2 ug/L 95 54 - 140 1 15

Benzo(g,h,i)perylene 16.0 16.4 ug/L 102 66 - 152 6 15

Benzo(k)fluoranthene 16.0 16.0 ug/L 100 51 - 153 11 22

Bis(2-chloroethoxy)methane 16.0 15.5 ug/L 97 50 - 128 3 17

Bis(2-chloroethyl)ether 16.0 14.3 ug/L 90 51 - 120 6 21

Bis(2-ethylhexyl) phthalate 16.0 16.3 ug/L 102 53 - 158 3 15

Butyl benzyl phthalate 16.0 16.8 ug/L 105 58 - 163 4 16

Caprolactam 32.0 29.2 * ug/L 91 14 - 130 81 20

Carbazole 16.0 16.5 ug/L 103 59 - 148 3 20

Chrysene 16.0 15.5 ug/L 97 69 - 140 5 15

Di-n-butyl phthalate 16.0 17.2 ug/L 107 58 - 149 1 15

Di-n-octyl phthalate 16.0 17.2 ug/L 107 55 - 167 9 16

Dibenz(a,h)anthracene 16.0 15.7 ug/L 98 57 - 148 8 15

Dibenzofuran 16.0 15.1 ug/L 94 49 - 137 3 15

Diethyl phthalate 16.0 17.2 ug/L 108 59 - 146 5 15

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Dimethyl phthalate 16.0 17.3 ug/L 108 59 - 141 5 15

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Fluoranthene 16.0 16.9 ug/L 106 55 - 147 8 15

Fluorene 16.0 15.8 ug/L 99 55 - 143 7 15

Hexachlorobenzene 16.0 15.4 ug/L 96 14 - 130 14 15

Hexachlorobutadiene 16.0 14.5 ug/L 90 14 - 130 11 44

Hexachlorocyclopentadiene 16.0 13.5 ug/L 84 13 - 130 22 49

Hexachloroethane 16.0 14.5 ug/L 90 14 - 130 9 46

Indeno(1,2,3-cd)pyrene 16.0 15.7 ug/L 98 69 - 146 7 15

Isophorone 16.0 16.2 ug/L 101 48 - 133 2 17

N-Nitrosodi-n-propylamine 16.0 14.3 ug/L 89 56 - 120 1 31

Naphthalene 16.0 14.1 ug/L 88 35 - 130 2 29

Nitrobenzene 16.0 14.9 ug/L 93 45 - 123 1 24

Pentachlorophenol 32.0 26.7 ug/L 83 39 - 136 7 37

Phenanthrene 16.0 15.3 ug/L 96 57 - 147 2 15

Phenol 16.0 13.6 * ug/L 85 17 - 120 51 34

Pyrene 16.0 16.6 ug/L 104 58 - 136 9 19


Surrogate

104

LCSD LCSD






85Phenol-d5 16 - 120


RL MDL

Biphenyl ND 170 25 ug/Kg 04/08/16 05:53 04/11/16 11:13 1

MB MB


ND 34170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1bis (2-chloroisopropyl) ether

ND 46170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4,5-Trichlorophenol

ND 34170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4,6-Trichlorophenol

ND 18170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4-Dichlorophenol

ND 41170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4-Dimethylphenol

ND 7801600 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4-Dinitrophenol

ND 35170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,4-Dinitrotoluene

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12,6-Dinitrotoluene

ND 28170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Chloronaphthalene

ND 31170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Chlorophenol

ND 34170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Methylnaphthalene

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Methylphenol

ND 25330 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Nitroaniline

ND 48170 ug/Kg 04/08/16 05:53 04/11/16 11:13 12-Nitrophenol

ND 200330 ug/Kg 04/08/16 05:53 04/11/16 11:13 13,3'-Dichlorobenzidine


ND 170330 ug/Kg 04/08/16 05:53 04/11/16 11:13 14,6-Dinitro-2-methylphenol

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RL MDL

4-Bromophenyl phenyl ether ND 170 24 ug/Kg 04/08/16 05:53 04/11/16 11:13 1

MB MB


ND 42170 ug/Kg 04/08/16 05:53 04/11/16 11:13 14-Chloro-3-methylphenol

ND 42170 ug/Kg 04/08/16 05:53 04/11/16 11:13 14-Chloroaniline

ND 21170 ug/Kg 04/08/16 05:53 04/11/16 11:13 14-Chlorophenyl phenyl ether

ND 20330 ug/Kg 04/08/16 05:53 04/11/16 11:13 14-Methylphenol


ND 120330 ug/Kg 04/08/16 05:53 04/11/16 11:13 14-Nitrophenol

ND 25170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Acenaphthene

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Acenaphthylene

ND 23170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Acetophenone

ND 42170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Anthracene

ND 59170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Atrazine

ND 130170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzaldehyde

ND 17170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzo[a]anthracene

ND 25170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzo[a]pyrene

ND 27170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzo[b]fluoranthene

ND 18170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzo[g,h,i]perylene

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Benzo[k]fluoranthene

ND 36170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Bis(2-chloroethoxy)methane

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Bis(2-chloroethyl)ether

ND 58170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Bis(2-ethylhexyl) phthalate

ND 28170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Butyl benzyl phthalate

ND 51170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Caprolactam

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Carbazole

ND 38170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Chrysene

ND 29170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Di-n-butyl phthalate

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Di-n-octyl phthalate

ND 30170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Dibenz(a,h)anthracene

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Dibenzofuran

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Diethyl phthalate

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Dimethyl phthalate

ND 18170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Fluoranthene

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Fluorene

ND 23170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Hexachlorobenzene

ND 25170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Hexachlorobutadiene

ND 23170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Hexachlorocyclopentadiene

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Hexachloroethane

ND 21170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Indeno[1,2,3-cd]pyrene

ND 36170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Isophorone

ND 29170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1N-Nitrosodi-n-propylamine

ND 140170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1N-Nitrosodiphenylamine

ND 22170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Naphthalene

ND 19170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Nitrobenzene

ND 170330 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Pentachlorophenol

ND 25170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Phenanthrene

ND 26170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Phenol

ND 20170 ug/Kg 04/08/16 05:53 04/11/16 11:13 1Pyrene

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2,4,6-Tribromophenol 86 39 - 146 04/11/16 11:13 1

MB MB

Surrogate

04/08/16 05:53


87 04/08/16 05:53 04/11/16 11:13 12-Fluorobiphenyl 37 - 120

78 04/08/16 05:53 04/11/16 11:13 12-Fluorophenol 18 - 120

85 04/08/16 05:53 04/11/16 11:13 1Nitrobenzene-d5 34 - 132

96 04/08/16 05:53 04/11/16 11:13 1p-Terphenyl-d14 65 - 153

80 04/08/16 05:53 04/11/16 11:13 1Phenol-d5 11 - 120


Biphenyl 1660 1400 ug/Kg 84 71 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

bis (2-chloroisopropyl) ether 1660 1320 ug/Kg 80 44 - 120

2,4,5-Trichlorophenol 1660 1450 ug/Kg 87 59 - 126

2,4,6-Trichlorophenol 1660 1470 ug/Kg 89 59 - 123

2,4-Dichlorophenol 1660 1400 ug/Kg 85 52 - 120

2,4-Dimethylphenol 1660 1370 ug/Kg 83 36 - 120

2,4-Dinitrophenol 3320 2900 ug/Kg 87 35 - 146

2,4-Dinitrotoluene 1660 1470 ug/Kg 89 55 - 125

2,6-Dinitrotoluene 1660 1420 ug/Kg 86 66 - 128

2-Chloronaphthalene 1660 1370 ug/Kg 83 57 - 120

2-Chlorophenol 1660 1420 ug/Kg 85 38 - 120

2-Methylnaphthalene 1660 1400 ug/Kg 84 47 - 120

2-Methylphenol 1660 1460 ug/Kg 88 48 - 120

2-Nitroaniline 1660 1440 ug/Kg 87 61 - 130

2-Nitrophenol 1660 1400 ug/Kg 84 50 - 120

3,3'-Dichlorobenzidine 3320 2420 ug/Kg 73 48 - 126


4,6-Dinitro-2-methylphenol 3320 3010 ug/Kg 91 49 - 155

4-Bromophenyl phenyl ether 1660 1590 ug/Kg 95 58 - 131

4-Chloro-3-methylphenol 1660 1470 ug/Kg 88 49 - 125

4-Chloroaniline 1660 925 ug/Kg 56 49 - 120

4-Chlorophenyl phenyl ether 1660 1450 ug/Kg 88 63 - 124

4-Methylphenol 1660 1410 ug/Kg 85 50 - 119


4-Nitrophenol 3320 3190 ug/Kg 96 43 - 137

Acenaphthene 1660 1440 ug/Kg 87 53 - 120

Acenaphthylene 1660 1430 ug/Kg 86 58 - 121

Acetophenone 1660 1470 ug/Kg 89 66 - 120

Anthracene 1660 1520 ug/Kg 92 62 - 129

Atrazine 3320 3150 ug/Kg 95 60 - 164

Benzaldehyde 3320 2320 ug/Kg 70 21 - 120

Benzo[a]anthracene 1660 1570 ug/Kg 95 65 - 133

Benzo[a]pyrene 1660 1490 ug/Kg 90 64 - 127

Benzo[b]fluoranthene 1660 1500 ug/Kg 90 64 - 135

Benzo[g,h,i]perylene 1660 1410 ug/Kg 85 50 - 152

Benzo[k]fluoranthene 1660 1510 ug/Kg 91 58 - 138

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Bis(2-chloroethoxy)methane 1660 1400 ug/Kg 84 61 - 133

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bis(2-chloroethyl)ether 1660 1450 ug/Kg 87 45 - 120

Bis(2-ethylhexyl) phthalate 1660 1650 ug/Kg 100 61 - 133

Butyl benzyl phthalate 1660 1640 ug/Kg 99 61 - 129

Caprolactam 3320 3050 ug/Kg 92 54 - 133

Carbazole 1660 1540 ug/Kg 93 59 - 129

Chrysene 1660 1510 ug/Kg 91 64 - 131

Di-n-butyl phthalate 1660 1590 ug/Kg 96 58 - 130

Di-n-octyl phthalate 1660 1560 ug/Kg 94 62 - 133

Dibenz(a,h)anthracene 1660 1420 ug/Kg 86 54 - 148

Dibenzofuran 1660 1420 ug/Kg 86 56 - 120

Diethyl phthalate 1660 1530 ug/Kg 92 66 - 126

Dimethyl phthalate 1660 1470 ug/Kg 88 65 - 124

Fluoranthene 1660 1530 ug/Kg 92 62 - 131

Fluorene 1660 1440 ug/Kg 87 63 - 126

Hexachlorobenzene 1660 1550 ug/Kg 93 60 - 132

Hexachlorobutadiene 1660 1370 ug/Kg 82 45 - 120

Hexachlorocyclopentadiene 1660 1400 ug/Kg 84 31 - 120

Hexachloroethane 1660 1360 ug/Kg 82 41 - 120

Indeno[1,2,3-cd]pyrene 1660 1380 ug/Kg 83 56 - 149

Isophorone 1660 1450 ug/Kg 87 56 - 120

N-Nitrosodi-n-propylamine 1660 1490 ug/Kg 90 46 - 120

Naphthalene 1660 1360 ug/Kg 82 46 - 120

Nitrobenzene 1660 1330 ug/Kg 80 49 - 120

Pentachlorophenol 3320 2830 ug/Kg 85 33 - 136

Phenanthrene 1660 1490 ug/Kg 90 60 - 130

Phenol 1660 1410 ug/Kg 85 36 - 120

Pyrene 1660 1620 ug/Kg 98 51 - 133


Surrogate

93

LCS LCS






84Phenol-d5 11 - 120

Method: 8015D - Diesel Range Organics (DRO) (GC)


RL MDL

Diesel Range Organics [C10-C28] ND 16 4.9 mg/Kg 04/04/16 14:00 04/05/16 08:38 1

MB MB


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Method: 8015D - Diesel Range Organics (DRO) (GC) (Continued)


o-Terphenyl 85 48 - 125 04/05/16 08:38 1

MB MB

Surrogate

04/04/16 14:00



Diesel Range Organics

[C10-C28]

49.8 48.7 mg/Kg 98 63 - 127

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

o-Terphenyl 48 - 125

Surrogate

94

LCS LCS


Client Sample ID: SB-7Lab Sample ID: 480-97480-11 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294004 Prep Batch: 293952


[C10-C28]

ND 55.4 51.5 mg/Kg 93 43 - 153☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

93

MS MS


Client Sample ID: SB-7Lab Sample ID: 480-97480-11 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294004 Prep Batch: 293952


[C10-C28]

ND 55.8 51.5 mg/Kg 92 43 - 153 0 35☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

94

MSD MSD



RL MDL

Diesel Range Organics [C10-C28] ND 0.50 0.31 mg/L 04/04/16 15:43 04/05/16 15:25 1

MB MB


o-Terphenyl 92 29 - 136 04/05/16 15:25 1

MB MB

Surrogate

04/04/16 15:43


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Method: 8015D - Diesel Range Organics (DRO) (GC) (Continued)



[C10-C28]

6.00 5.88 mg/L 98 54 - 128

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

95

LCS LCS


Method: 6010C - Metals (ICP)


RL MDL

Arsenic ND 0.015 0.0056 mg/L 04/04/16 08:30 04/05/16 11:09 1

MB MB


ND 0.000700.0020 mg/L 04/04/16 08:30 04/05/16 11:09 1Barium

ND 0.000500.0020 mg/L 04/04/16 08:30 04/05/16 11:09 1Cadmium

ND 0.00100.0040 mg/L 04/04/16 08:30 04/05/16 11:09 1Chromium

ND 0.00300.010 mg/L 04/04/16 08:30 04/05/16 11:09 1Lead

ND 0.00870.025 mg/L 04/04/16 08:30 04/05/16 11:09 1Selenium

ND 0.00170.0060 mg/L 04/04/16 08:30 04/05/16 11:09 1Silver


Arsenic 0.200 0.213 mg/L 107 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 0.200 0.208 mg/L 104 80 - 120

Cadmium 0.200 0.204 mg/L 102 80 - 120

Chromium 0.200 0.201 mg/L 101 80 - 120

Lead 0.200 0.207 mg/L 103 80 - 120

Selenium 0.200 0.193 mg/L 97 80 - 120

Silver 0.0500 0.0486 mg/L 97 80 - 120


Arsenic 0.200 0.211 mg/L 106 80 - 120 1 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Barium 0.200 0.208 mg/L 104 80 - 120 0 20

Cadmium 0.200 0.203 mg/L 102 80 - 120 1 20

Chromium 0.200 0.200 mg/L 100 80 - 120 1 20

Lead 0.200 0.205 mg/L 103 80 - 120 1 20

Selenium 0.200 0.197 mg/L 98 80 - 120 2 20

Silver 0.0500 0.0491 mg/L 98 80 - 120 1 20

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Method: 6010C - Metals (ICP) (Continued)


RL MDL

Arsenic ND 2.0 0.40 mg/Kg 04/04/16 14:16 04/05/16 13:26 1

MB MB


ND 0.110.50 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Barium

ND 0.0300.20 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Cadmium

ND 0.200.50 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Chromium

ND 0.240.99 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Lead

ND 0.404.0 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Selenium

ND 0.200.60 mg/Kg 04/04/16 14:16 04/05/16 13:26 1Silver

Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 480-293904/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294213 Prep Batch: 293904

Arsenic 98.5 89.0 mg/Kg 90.4 69.3 - 145.

2

1 20

Analyte

LCDSRM LCDSRM


Spike

Added

%Rec.

Limits LimitRPD

RPD

Barium 308 270 mg/Kg 87.7 74.0 - 126.

0

1 20

Cadmium 146 125 mg/Kg 85.3 73.3 - 126.

7

2 20

Chromium 182 154 mg/Kg 84.6 70.9 - 129.

7

1 20

Lead 130 130 mg/Kg 100.3 72.5 - 126.

9

4 20

Selenium 154 136 mg/Kg 88.6 67.5 - 132.

5

2 20

Silver 40.9 35.6 mg/Kg 87.1 66.0 - 133.

7

4 20


Arsenic 40.3 42.6 mg/Kg 106 69 - 131

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 40.3 41.9 mg/Kg 104 72 - 127

Cadmium 40.3 40.8 mg/Kg 101 73 - 127

Lead 40.3 41.5 mg/Kg 103 70 - 130

Selenium 40.3 39.7 mg/Kg 99 64 - 137

Silver 10.1 9.64 mg/Kg 96 66 - 135

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 480-293904/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294213 Prep Batch: 293904

Arsenic 98.5 88.4 mg/Kg 89.7 69.3 - 145.

2

Analyte

LCSSRM LCSSRM


Spike

Added

%Rec.

Limits

Barium 308 268 mg/Kg 86.9 74.0 - 126.

0Cadmium 146 127 mg/Kg 87.1 73.3 - 126.

7

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Method: 6010C - Metals (ICP) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 480-293904/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294213 Prep Batch: 293904

Chromium 182 152 mg/Kg 83.5 70.9 - 129.

7

Analyte

LCSSRM LCSSRM


Spike

Added

%Rec.

Limits

Lead 130 136 mg/Kg 104.7 72.5 - 126.

9Selenium 154 134 mg/Kg 87.2 67.5 - 132.

5Silver 40.9 34.2 mg/Kg 83.7 66.0 - 133.

7

Method: 7470A - Mercury (CVAA)


RL MDL

Mercury ND 0.00020 0.00012 mg/L 04/05/16 08:35 04/05/16 11:53 1

MB MB



Mercury 0.00667 0.00672 mg/L 101 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: 7471B - Mercury (CVAA)


RL MDL

Mercury ND 0.020 0.0079 mg/Kg 04/05/16 09:15 04/05/16 12:42 1

MB MB


Client Sample ID: Lab Control Sample DupLab Sample ID: LCDSRM 480-293905/3-A ^5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 294098 Prep Batch: 293905

Mercury 7.10 8.16 mg/Kg 114.9 51.3 - 149.

3

6 20

Analyte

LCDSRM LCDSRM


Spike

Added

%Rec.

Limits LimitRPD

RPD

Client Sample ID: Lab Control SampleLab Sample ID: LCSSRM 480-293905/2-A ^5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 294098 Prep Batch: 293905

Mercury 7.10 7.66 mg/Kg 107.9 51.3 - 149.

3

Analyte

LCSSRM LCSSRM


Spike

Added

%Rec.

Limits

TestAmerica Buffalo

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Method: 7471B - Mercury (CVAA) (Continued)

Client Sample ID: SB-3Lab Sample ID: 480-97480-9 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294098 Prep Batch: 293905

Mercury 0.012 J 0.409 0.437 mg/Kg 104 80 - 120☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: SB-3Lab Sample ID: 480-97480-9 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 294098 Prep Batch: 293905

Mercury 0.012 J 0.408 0.433 mg/Kg 103 80 - 120 1 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

TestAmerica Buffalo

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QC Association SummaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


GC/MS VOA

Prep Batch: 293913

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 5035480-97480-7 SB-8 Total/NA

Solid 5035480-97480-10 SB-6 Total/NA

Solid 5035480-97480-11 SB-7 Total/NA

Solid 5035LCS 480-293913/22-A Lab Control Sample Total/NA

Solid 5035LCSD 480-293913/2-A Lab Control Sample Dup Total/NA

Solid 5035MB 480-293913/3-A Method Blank Total/NA

Analysis Batch: 293918


Solid 8260C 293913480-97480-7 SB-8 Total/NA



Solid 8260C 293913LCS 480-293913/22-A Lab Control Sample Total/NA

Solid 8260C 293913LCSD 480-293913/2-A Lab Control Sample Dup Total/NA

Solid 8260C 293913MB 480-293913/3-A Method Blank Total/NA



Solid 8260C 294151480-97480-12 DUP Total/NA



Prep Batch: 294151


Solid 5035480-97480-12 DUP Total/NA

Solid 5035LCS 480-294151/1-A Lab Control Sample Total/NA

Solid 5035MB 480-294151/2-A Method Blank Total/NA

Prep Batch: 294617


Solid 5035A480-97480-8 SB-2 Total/NA

Solid 5035A480-97480-9 SB-3 Total/NA

Solid 5035ALCS 480-294617/1-A Lab Control Sample Total/NA

Solid 5035AMB 480-294617/2-A Method Blank Total/NA









Water 8260C480-97480-1 MW-1 Total/NA




Water 8260C480-97480-5 DUP Total/NA

Water 8260C480-97480-6 FB Total/NA

Water 8260CLCS 480-294920/4 Lab Control Sample Total/NA

TestAmerica Buffalo

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GC/MS VOA (Continued)

Analysis Batch: 294920 (Continued)


Water 8260CMB 480-294920/6 Method Blank Total/NA

GC/MS Semi VOA

Prep Batch: 293778






Water 3510CLCS 480-293778/2-A Lab Control Sample Total/NA

Water 3510CLCSD 480-293778/5-A Lab Control Sample Dup Total/NA

Water 3510CMB 480-293778/1-A Method Blank Total/NA



Water 8270D 293778480-97480-1 MW-1 Total/NA




Water 8270D 293778LCS 480-293778/2-A Lab Control Sample Total/NA

Water 8270D 293778LCSD 480-293778/5-A Lab Control Sample Dup Total/NA

Water 8270D 293778MB 480-293778/1-A Method Blank Total/NA

Prep Batch: 294686


Solid 3550C480-97480-7 SB-8 Total/NA





Solid 3550CLCS 480-294686/2-A Lab Control Sample Total/NA

Solid 3550CMB 480-294686/1-A Method Blank Total/NA



Solid 8270D 294686480-97480-7 SB-8 Total/NA





Solid 8270D 294686LCS 480-294686/2-A Lab Control Sample Total/NA

Solid 8270D 294686MB 480-294686/1-A Method Blank Total/NA

GC Semi VOA

Prep Batch: 293952




TestAmerica Buffalo

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GC Semi VOA (Continued)

Prep Batch: 293952 (Continued)





Solid 3550C480-97480-11 MS SB-7 Total/NA

Solid 3550C480-97480-11 MSD SB-7 Total/NA

Solid 3550CLCS 480-293952/2-A Lab Control Sample Total/NA

Solid 3550CMB 480-293952/1-A Method Blank Total/NA

Prep Batch: 293969






Water 3510CLCS 480-293969/2-A Lab Control Sample Total/NA

Water 3510CMB 480-293969/1-A Method Blank Total/NA












Solid 8015D 293952480-97480-11 MS SB-7 Total/NA

Solid 8015D 293952480-97480-11 MSD SB-7 Total/NA

Solid 8015D 293952LCS 480-293952/2-A Lab Control Sample Total/NA

Water 8015D 293969LCS 480-293969/2-A Lab Control Sample Total/NA

Solid 8015D 293952MB 480-293952/1-A Method Blank Total/NA

Water 8015D 293969MB 480-293969/1-A Method Blank Total/NA

Metals

Prep Batch: 293844


Water 3005A480-97480-1 MW-1 Total/NA




Water 3005ALCS 480-293844/2-A Lab Control Sample Total/NA

Water 3005ALCSD 480-293844/3-A Lab Control Sample Dup Total/NA

Water 3005AMB 480-293844/1-A Method Blank Total/NA

Prep Batch: 293904


Solid 3050B480-97480-7 SB-8 Total/NA

TestAmerica Buffalo

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Metals (Continued)

Prep Batch: 293904 (Continued)






Solid 3050BLCDSRM 480-293904/3-A Lab Control Sample Dup Total/NA

Solid 3050BLCS 480-293904/22-A Lab Control Sample Total/NA

Solid 3050BLCSSRM 480-293904/2-A Lab Control Sample Total/NA

Solid 3050BMB 480-293904/1-A Method Blank Total/NA

Prep Batch: 293905





Solid 7471B480-97480-9 MS SB-3 Total/NA

Solid 7471B480-97480-9 MSD SB-3 Total/NA



Solid 7471BLCDSRM 480-293905/3-A ^5 Lab Control Sample Dup Total/NA

Solid 7471BLCSSRM 480-293905/2-A ^5 Lab Control Sample Total/NA

Solid 7471BMB 480-293905/1-A Method Blank Total/NA

Prep Batch: 294014






Water 7470ALCS 480-294014/2-A Lab Control Sample Total/NA

Water 7470AMB 480-294014/1-A Method Blank Total/NA



Water 7470A 294014480-97480-1 MW-1 Total/NA




Water 7470A 294014LCS 480-294014/2-A Lab Control Sample Total/NA

Water 7470A 294014MB 480-294014/1-A Method Blank Total/NA



Solid 7471B 293905480-97480-7 SB-8 Total/NA



Solid 7471B 293905480-97480-9 MS SB-3 Total/NA

Solid 7471B 293905480-97480-9 MSD SB-3 Total/NA



Solid 7471B 293905LCDSRM 480-293905/3-A ^5 Lab Control Sample Dup Total/NA

Solid 7471B 293905LCSSRM 480-293905/2-A ^5 Lab Control Sample Total/NA

TestAmerica Buffalo

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Metals (Continued)

Analysis Batch: 294098 (Continued)


Solid 7471B 293905MB 480-293905/1-A Method Blank Total/NA



Water 6010C 293844480-97480-1 MW-1 Total/NA





Water 6010C 293844LCS 480-293844/2-A Lab Control Sample Total/NA

Water 6010C 293844LCSD 480-293844/3-A Lab Control Sample Dup Total/NA

Water 6010C 293844MB 480-293844/1-A Method Blank Total/NA








Solid 6010C 293904LCDSRM 480-293904/3-A Lab Control Sample Dup Total/NA


Solid 6010C 293904LCSSRM 480-293904/2-A Lab Control Sample Total/NA


General Chemistry



Solid Moisture480-97480-7 SB-8 Total/NA







Solid Moisture480-97480-12 DUP Total/NA

TestAmerica Buffalo

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Lab ChronicleClient: ATC Associates Inc. TestAmerica Job ID: 480-97480-1Project/Site: JB Soil & Groundwater Project

Client Sample ID: MW-1 Lab Sample ID: 480-97480-1Matrix: WaterDate Collected: 03/30/16 14:20


Analysis 8260C 04/09/16 14:42 NMD11 294920 TAL BUF

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3510C 293778 04/02/16 10:06 RJS TAL BUFTotal/NA

Analysis 8270D 1 293950 04/05/16 02:11 LMW TAL BUFTotal/NA

Prep 3510C 293969 04/04/16 15:43 JIL TAL BUFTotal/NA

Analysis 8015D 1 294004 04/05/16 18:46 JMO TAL BUFTotal/NA

Prep 3005A 293844 04/04/16 08:30 KJ1 TAL BUFTotal/NA

Analysis 6010C 1 294207 04/05/16 11:38 LMH TAL BUFTotal/NA



Prep 7470A 294014 04/05/16 08:35 TAS TAL BUFTotal/NA

Analysis 7470A 1 294090 04/05/16 12:03 TAS TAL BUFTotal/NA




Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA












Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









TestAmerica Buffalo

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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Client Sample ID: DUP Lab Sample ID: 480-97480-5Matrix: WaterDate Collected: 03/30/16 13:45



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: FB Lab Sample ID: 480-97480-6Matrix: WaterDate Collected: 03/30/16 14:50



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: SB-8 Lab Sample ID: 480-97480-7Matrix: SolidDate Collected: 03/30/16 11:50


Analysis Moisture 04/04/16 10:54 MJH1 293907 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035 04/01/16 10:30 CDC293913 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 293918 04/04/16 18:40 CDC TAL BUFTotal/NA

Prep 3550C 294686 04/08/16 05:53 CAM TAL BUFTotal/NA


Prep 3550C 293952 04/04/16 14:00 AVW TAL BUFTotal/NA


TestAmerica Buffalo

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Prep 3050B 04/04/16 14:16 KJ1293904 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Prep 7471B 293905 04/05/16 09:15 TAS TAL BUFTotal/NA

Analysis 7471B 1 294098 04/05/16 12:58 TAS TAL BUFTotal/NA




Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035A 04/01/16 10:30 SWO294617 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 294734 04/08/16 19:59 RRS TAL BUFTotal/NA





Prep 3050B 293904 04/04/16 14:16 KJ1 TAL BUFTotal/NA







Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035A 04/01/16 10:30 SWO294617 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260C 1 294734 04/08/16 20:26 RRS TAL BUFTotal/NA


TestAmerica Buffalo

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Analysis 8270D 04/11/16 16:03 LMW1 295082 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



Prep 5035 04/01/16 10:30 CDC293913 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

TestAmerica Buffalo

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Prep 5035 04/01/16 10:30 CDC293913 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










Client Sample ID: DUP Lab Sample ID: 480-97480-12Matrix: SolidDate Collected: 03/30/16 11:35


Analysis Moisture 04/04/16 13:42 CDC1 293944 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Client Sample ID: DUP Lab Sample ID: 480-97480-12Matrix: SolidDate Collected: 03/30/16 11:35


Prep 5035 04/01/16 10:30 CDC294151 TAL BUF

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Laboratory References:

TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL (716)691-2600

TestAmerica Buffalo

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Certification SummaryClient: ATC Associates Inc. TestAmerica Job ID: 480-97480-1Project/Site: JB Soil & Groundwater Project

Laboratory: TestAmerica BuffaloAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Arkansas DEQ 88-06866State Program 07-06-16

California State Program 9 1169CA 09-30-17

Connecticut State Program 1 PH-0568 09-30-16

Florida NELAP 4 E87672 06-30-16

Georgia State Program 4 N/A 03-31-17

Illinois NELAP 5 200003 09-30-16

Iowa State Program 7 374 03-01-17

Kansas NELAP 7 E-10187 05-31-16 *

Kentucky (DW) State Program 4 90029 12-31-16

Kentucky (UST) State Program 4 30 03-31-16 *

Kentucky (WW) State Program 4 90029 12-31-16

Louisiana NELAP 6 02031 06-30-16

Maine State Program 1 NY00044 12-04-16

Maryland State Program 3 294 03-31-17

Massachusetts State Program 1 M-NY044 06-30-16

Michigan State Program 5 9937 03-31-16 *

Minnesota NELAP 5 036-999-337 12-31-16

New Hampshire NELAP Secondary AB 1 2337 11-17-16

New Jersey NELAP 2 NY455 06-30-16

New York NELAP 2 10026 03-31-17

North Dakota State Program 8 R-176 03-31-16 *

Oklahoma State Program 6 9421 08-31-16

Oregon NELAP 10 NY200003 06-09-16

Pennsylvania NELAP 3 68-00281 07-31-16

Rhode Island State Program 1 LAO00328 12-30-16

Tennessee State Program 4 TN02970 03-31-17

Texas NELAP 6 T104704412-15-6 07-31-16

USDA Federal P330-11-00386 11-26-17

Virginia NELAP 3 460185 09-14-16

Washington State Program 10 C784 02-10-17

West Virginia DEP State Program 3 252 09-30-16

Wisconsin State Program 5 998310390 08-31-16

TestAmerica Buffalo

* Certification renewal pending - certification considered valid.

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Method SummaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Method Method Description LaboratoryProtocol

SW8468260C Volatile Organic Compounds by GC/MS TAL BUF

SW8468270D Semivolatile Organic Compounds (GC/MS) TAL BUF

SW8468015D Diesel Range Organics (DRO) (GC) TAL BUF

SW8466010C Metals (ICP) TAL BUF

SW8467470A Mercury (CVAA) TAL BUF

SW8467471B Mercury (CVAA) TAL BUF

EPAMoisture Percent Moisture TAL BUF

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL BUF = TestAmerica Buffalo, 10 Hazelwood Drive, Amherst, NY 14228-2298, TEL (716)691-2600

TestAmerica Buffalo

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Sample SummaryTestAmerica Job ID: 480-97480-1Client: ATC Associates Inc.


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

480-97480-1 MW-1 Water 03/30/16 14:20 04/01/16 09:45

480-97480-2 MW-3 Water 03/30/16 12:15 04/01/16 09:45

480-97480-3 MW-5 Water 03/30/16 13:40 04/01/16 09:45

480-97480-4 MW-7 Water 03/30/16 13:10 04/01/16 09:45

480-97480-5 DUP Water 03/30/16 13:45 04/01/16 09:45

480-97480-6 FB Water 03/30/16 14:50 04/01/16 09:45

480-97480-7 SB-8 Solid 03/30/16 11:50 04/01/16 09:45

480-97480-8 SB-2 Solid 03/30/16 09:00 04/01/16 09:45

480-97480-9 SB-3 Solid 03/30/16 09:20 04/01/16 09:45

480-97480-10 SB-6 Solid 03/30/16 10:45 04/01/16 09:45

480-97480-11 SB-7 Solid 03/30/16 11:30 04/01/16 09:45

480-97480-12 DUP Solid 03/30/16 11:35 04/01/16 09:45

TestAmerica Buffalo

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Login Sample Receipt Checklist

Client: ATC Associates Inc. Job Number: 480-97480-1

Login Number: 97480

Question Answer Comment

Creator: Williams, Christopher S

List Source: TestAmerica Buffalo

List Number: 1

TrueRadioactivity either was not measured or, if measured, is at or below background

TrueThe cooler's custody seal, if present, is intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the sample IDs on the containers and the COC.

TrueSamples are received within Holding Time (Excluding tests with immediate HTs)..

FREEZE 4/1/16 1030

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

TrueSample Preservation Verified

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueVOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter.

TrueIf necessary, staff have been informed of any short hold time or quick TAT needs

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

TrueSampling Company provided. ATC

TrueSamples received within 48 hours of sampling.

N/ASamples requiring field filtration have been filtered in the field.

N/AChlorine Residual checked.


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phase ii environmental site assessment · 1 introduction . 1.1 purpose . atc was contracted by...

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