petroleum crms and reference standards 2015/2016 - hpst

Petroleum CRMs and reference standards 2015/2016

Wear metal standards • Used oil analysis • Prof ciency testing • Biodiesel • Physical test standards • Sulfur, nitrogen, chlorine • Matrix oils & solvents • Metallo-organic standards

LGC Quality - ISO Guide 34 • GMP/GLP • ISO 9001 • ISO/IEC 17025 • ISO/IEC 17043

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Welcome to the LGC catalogue of petroleum Certifed Reference Materials (CRMs) The frst section of the catalogue details the extensive VHG Labs line of analytical reference standards for both new and used oil applications. Our petroleum standards may be used for analysis by ICP, ICP-MS, AA, XRF, RDE, UVF, physical testing instruments and other used oil analysis instruments. We have been manufacturing single and multi-element standards (both sulfonate-based and sulfur-free versions) for more than 30 years. We manufacture an equally extensive line of single and multi-element inorganic aqueous standards.

The second section of this catalogue gives an overview of other CRMs which LGC offers. Most norms expect to complete development of an application (calibration) by analyzing a CRM as an unknown sample to validate or verify the analytical procedure. We can offer some standards with full analysis, including C, H and N, especially for XRF and its fundamental parameter mathematics.

Our manufacturing facility is registered to ISO 9001 and accredited to ISO Guide 34. Each product must pass rigorous Quality Control in our ISO/IEC 17025 laboratory and is shipped with a comprehensive Certifcate of Analysis (COA) with actual (not nominal) concentrations. Our profciency testing program for oil analysis is ISO/IEC 17043 accredited.

Thank you to all of our customers. We look forward to supporting your continued success.

The LGC team

Our commitment to qualityVHG brand petroleum standards are subjected to rigorous Quality Assurance checks prior to shipment. Raw materials are assayed and analyzed for trace impurities. Major constituents are generally verifed both instrumentally, against the appropriate NIST SRM (when available), and through classical wet chemical methods (titrimetry or gravimetry). Our standards are blended in pre-cleaned HDPE or glass reactors. Balances and volumetric flasks are calibrated according to NIST procedures. All VHG standards are accompanied by a comprehensive Certifcate of Analysis (COA). Each COA is supported by an unbroken chain of comparisons with traceability to national or international standards of measurement.


About LGC StandardsLGC Standards is a leading global producer and distributor of reference materials and profciency testing schemes. Headquartered in Teddington, Middlesex, UK, LGC Standards has a network of dedicated sales offces extending across 20 countries in 5 continents. We have an unparalleled breadth of ISO Guide 34 accredited reference material production in facilities at 4 sites across the UK, US and Germany.

In addition to our petroleum product line, we manufacture CRMs and reference materials for the following sectors: pharmaceutical, forensic, clinical, food, beverage, environmental, pesticides and contaminants sectors. We provide profciency testing schemes in support of these sectors, as well as others, to more than 10,000 laboratories worldwide.

About our WebshopAn up-to-date listing of all products is available on the LGC website: www.lgcstandards.com. Once registered, you can use the website to order products, check delivery times and access a range of resources for a wide variety of sectors.

Prices for the products listed, as well as detailed procedures and transport charges are available from your local sales offce, where applicable. For products requiring special delivery procedures (dangerous goods, etc.), additional charges may be applied.

LGC Standards’ technical staff are available to advise on the use and suitability of a particular product. Customers requiring assistance with the use or application of a particular reference material should contact their local offce. Contact details for your local sales offce are available at the back of this catalogue and on our website.

About LGCLGC is an international life sciences measurement and testing company, building leading positions in sustainably growing markets.

We provide reference materials, genomics solutions and analytical testing products and services, based on our innovations and own intellectual property. We work with customers in the pharmaceuticals, agricultural, biotechnology, food, environment, security and sports sectors, as well as, with governments and academia to achieve excellence in investigative, diagnostic and measurement science. For more information, please visit our website: www.lgcgroup.com.


LGC Quality - ISO 9001

© LGC Limited, 2015. All rights reserved. LGC Standards is part of the LGC Group. 4436/CB/0815

www.lgcstandards.com • Science for a safer world

• #2 Diesel fuel • Crude oil • Engine oil lubricants • Simulated in service

engine oil

LGC is an accredited international provider of proficiency testing (PT) schemes. With more than 30 years of experience, we run more than 1600 PT exercises each year for more than 10,000 laboratories worldwide.

Available online www.lgcstandards.com

OIL PT Oils and fuels proficiency scheme

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Table of contentsPetroleum Standards

Standards for ICP, RDE and XRF ........................................................................................... 2 Wear Metal Standards........................................................................................................ 2 Internal Standards .............................................................................................................. 2 Metal Additives Standards.................................................................................................. 3 Matrix Oils and Solvents..................................................................................................... 3 V-SolvTM ............................................................................................................................. 4 Stabilizer for Wear Metal Standards................................................................................... 4 Single-Element Metallo-Organic Standards ....................................................................... 5 D-Series Multi-Element Wear Metal Standards.................................................................. 6Standards for Used Oil Analysis ............................................................................................ 7 Acid Number and Base Number Standards ....................................................................... 7 Soot Content Standards ..................................................................................................... 7 Fuel Dilution Standards ...................................................................................................... 8 Glycol in Oil Standards ....................................................................................................... 8 Multi-Element Coolant Standards....................................................................................... 8 Crackle Test Reference Standards .................................................................................... 9 Karl Fischer Titration Certified Reference Standards ......................................................... 9Reference Gas Oil Standards ................................................................................................. 9Distillation Standards .............................................................................................................. 9Proficiency Testing Program.................................................................................................. 10 Standards for S, N, Cl, and Metals ......................................................................................... 11 Single-Element, Sulfur-Free Metallo-Organic Standards ................................................... 11 Metallo-Organic Concentrates ................................................................................................... 12 Wear Metal Standards for XRF .......................................................................................... 13 Standards for Sulfur & Metals in Crude and Residual Oils ................................................ 13 Lube Oil Standards............................................................................................................. 14 Standards for Sulfur in Diesel Fuel Analysis ...................................................................... 15 Sulfur in Kerosene Standards ............................................................................................ 15 Sulfur in Isooctane Standards ............................................................................................ 16 Sulfur in Crude and Residual Oil Standards....................................................................... 16 Matrix Oils and Solvents..................................................................................................... 16 Polysulfide Oil Standards ................................................................................................... 17 Sulfur in Petroleum Products (Ampoules) .......................................................................... 18 Sulfur & Nitrogen Products (Ampoules) ............................................................................. 19 Chlorine in Oil Standards ................................................................................................... 19 Standards for Lead in Gasoline .......................................................................................... 20 Internal Standards for XRF Analysis .................................................................................. 20Petroleum Physical Test Standards ...................................................................................... 21

Flash Point Reference Materials ........................................................................................ 21Viscosity Reference Standards .......................................................................................... 21Pour Point, Cloud Point, and Freezing Point Reference Materials..................................... 22Cold Filter Plug Point Reference Materials ........................................................................ 22

Biodiesel................................................................................................................................... 23Metals in Biodiesel Standards ............................................................................................ 23Sulfur in Biodiesel Standards ............................................................................................. 23Biodiesel/Diesel Fuel Blends .............................................................................................. 23

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Table of contents

Reference documents

CRMs to Verify Analytical Procedures

Diesel CRMs ............................................................................................................................. 26CRMs for Bio-Diesel ................................................................................................................ 27CRMs for Gasoline / Gasoil / Kerosene ................................................................................. 28Lube Oil CRMs / Lubricants .................................................................................................... 30CRMs for Residual Oil / Bunker ............................................................................................. 32Crude Oil CRMs ...................................................................................................................... 33Waste Oil .................................................................................................................................. 34CRMs with given C-H-N-composition .................................................................................... 34Other petrochemical CRMs .................................................................................................... 35

Conversion Tables for Reference .......................................................................................... 36 Wear Metal Set (VHG-WRMTLSET-17X50G) Addendum ..................................................... 37


VHG Petroleum products



www.lgcstandards.com2

Section 1PetroleumStandards

Wear metal standardsFor ICP, RDE, XRF and other techniques

u We manufacture the highest quality metallo-organic mixes in the industry in our ISO 9001 and ISO Guide 34 facility. Customers are assured of getting the best value and consistency available.

u Each product must pass rigorous Quality Control in our ISO/IEC 17025 laboratory.u Each product is accompanied by a comprehensive Certificate of Analysis with actual

(not nominal) concentrations.

Internal Standards For Wear Metal Analysis by ICP

The use of an internal standard, such as Ce, Co or Y, can significantly improve the accuracy of your results by correcting for wide variations in the viscosity or oil composition of your samples. Internal standards are easy to use when added to the diluent prior to sample preparation.

Element Matrix Concentration Size Product No. (grams)Cerium (Ce) Hydrocarbon Oil 5000µg/g 200 VHG-OCE-5000-200G

Cobalt (Co) Mineral Spirits 6 wt. % 100 VHG-OCO-6PIS-100GCobalt (Co) Mineral Spirits 6 wt. % 200 VHG-OCO-6PIS-200GCobalt (Co) Mineral Spirits 6 wt. % 400 VHG-OCO-6PIS-400GCobalt (Co) Hydrocarbon Oil 5000µg/g 200 VHG-OCODN-5000-200GCobalt (Co) Hydrocarbon Oil 5000µg/g 800 VHG-OCODN-5000-800G

Lanthanum (La) Hydrocarbon Oil 5000µg/g 200 VHG-OLA-5000-200GYttrium (Y) Hydrocarbon Oil 5000µg/g 400 VHG-OY-5000-A-400G

Yttrium (Y) Hydrocarbon Oil 2 wt. % 100 VHG-OYDN-2P-100GYttrium (Y) Hydrocarbon Oil 2 wt. % 200 VHG-OYDN-2P-200G

V21 Wear Metal Standards V21+K Wear Meta l Standards V23 Wear Metal Standards Ag, Al, B, Ba, Ca, Cd, Cr, Cu, Fe, Mg, Mn, All of the elements included All of the elements included Mo, Na, Ni, P, Pb, Si, Sn, Ti, V, Zn in V21 plus K in V21 plus K and Sb combined in hydrocarbon oilConc.* Size Product No. Product No. Product No. (µg/g) (grams)10 100 VHG-V21-10-100G VHG-V21+K-10-100G VHG-V23-10-100G 200 VHG-V21-10-200G VHG-V21+K-10-200G VHG-V23-10-200G 30 100 VHG-V21-30-100G VHG-V21+K-30-100G VHG-V23-30-100G 200 VHG-V21-30-200G VHG-V21+K-30-200G VHG-V23-30-200G 50 100 VHG-V21-50-100G VHG-V21+K-50-100G VHG-V23-50-100G 200 VHG-V21-50-200G VHG-V21+K-50-200G VHG-V23-50-200G 100 100 VHG-V21-100-100G VHG-V21+K-100-100G VHG-V23-100-100G 200 VHG-V21-100-200G VHG-V21+K-100-200G VHG-V23-100-200G300 100 VHG-V21-300-100G VHG-V21+K-300-100G VHG-V23-300-100G 200 VHG-V21-300-200G VHG-V21+K-300-200G VHG-V23-300-200G500 100 VHG-V21-500-100G VHG-V21+K-500-100G VHG-V23-500-100G 200 VHG-V21-500-200G VHG-V21+K-500-200G VHG-V23-500-200G900 100 VHG-V21-900-100G VHG-V21+K-900-100G VHG-V23-900-100G 200 VHG-V21-900-200G VHG-V21+K-900-200G VHG-V23-900-200G

* For catalogue purposes, nominal concentrations (µg/g) are provided.

VHG TipsMetallo-organic standards should be kept away from moisture. Preferably store in a cool, dry location.

We welcome inquiries into custom metallo-organic standards. Contact your local sales office for assistance. See back cover for list of locations.


www.lgcstandards.com


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Metal additives standardsFor ICP, RDE, XRF and other techniques

Metal Additives Standard MA3 Ca @ 5000µg/g; P, Zn @ 1600µg/g combined in hydrocarbon oil*Size (grams) Product No.100 VHG-MA3-100G200 VHG-MA3-200G

Metal Additives Standard MA5 Ba, Ca, Mg, P, Zn combined in hydrocarbon oilConc.* Size Product No. (µg/g) (grams)900 100 VHG-MA5-900-100G 200 VHG-MA5-900-200G1000 100 VHG-MA5-1000-100G 200 VHG-MA5-1000-200G3000 100 VHG-MA5-3000-100G 200 VHG-MA5-3000-200G5000 100 VHG-MA5-5000-100G 200 VHG-MA5-5000-200G* For catalogue purposes, nominal concentrations (µg/g) are provided

Solvents for the Preparation of Working Standards for Hydrocarbon/Petrochemical Analysis High-purity solvents supplied with a Certificate of Analysis that includes trace metal concentrations.Item Volume Product No. 75 cSt Hydrocarbon Oil 500mL VHG-OIL-75-500 1Gal. VHG-OIL-75-1GAL20 cSt Hydrocarbon Oil 500mL VHG-OIL-20-500 1Gal. VHG-OIL-20-1GALV-SOLV™ ICP Solvent 1 Gal. VHG-V-SOLV-1GAL 5 Gal. VHG-V-SOLV-5GALKerosene, low odor 500mL VHG-KERO-500 1 Gal. VHG-KERO-1GAL

Matrix Oils and Solvents

Metal Additives Standard MA6 B, Ba, Ca, Mg, P, Zn combined in hydrocarbon oilConc.* Size Product No. (µg/g) (grams) 900 100 VHG-MA6-900-100G 200 VHG-MA6-900-200G * For catalogue purposes, nominal concentrations (µg/g) are provided

ICP, RDE, and XRF Standards

Wear Metals Metal Additives V-Solv™

Single Elements D Series Standards for Used Oils Distillation Standards Performance Testing Program Standards for S, N, Cl and Metals Petroleum Physical Test Standards Biodiesel

Metal Additives Standard MA4 Ca @ 5000µg/g; Mg, P, Zn @ 1600µg/g combined in hydrocarbon oil*Size (grams) Product No.100 VHG-MA4-100G200 VHG-MA4-200G




V-Solv™

ICP Solvent

V-Solv™ ICP Solvent is a proprietary solvent that is used for diluting oil and other organic liquids for analysis by ICP and ICP-MS. Use V-Solv™ as a matrix blank and as a diluent for your calibration standards and samples for outstanding nebulization characteristics. V-Solv™ ICP Solvent offers the following advantages over conventional low odor/odorless kerosene, xylene and other commercial solvents:

VHG TipsThe use of stabilizer is particularly important for long-term stability when diluting these standards in solvents.

Stabilizer to Improve Stability of Mixes or Dilutions Solvent stabilizer can improve stability of mixes or dilutions of VHG’s 1000µg/g and 5000µg/g stock metallo-organic standards, as well as multi-element mixes after dilution in solvent.Product Product Use Product No. Size (grams)MO Stabilizer VHG’s wear metal VHG-STAB-50G 50 standards. Add to solutions at 0.6wt%

Stabilizer for Wear Metal Standards

ICP Solvent for the Preparation of Working Standards for Hydrocarbon/Petrochemical Analysis High-purity solvents supplied with a Certificate of Analysis that includes trace metal concentrations.Item Volume Product No.V-SOLV™ ICP Solvent 1 Gal. VHG-V-SOLV-1GAL V-SOLV™ ICP Solvent 5 Gal. VHG-V-SOLV-5GAL

u Very high purity (essentially no trace metals or sulfur) - each bottle is accompanied by a COA that states the trace impurity levels of 36 metals and sulfur.

u Makes very stable dilutions of metallo-organic standards and oil samples.u Extremely low odor (no kerosene or aromatic smell), which results in a comfortable

work environment and is also VOC-exempt for consumer products applications (EPA Title 40, Volume 5, Parts 53-59).

u Extremely low toxicity compared with kerosene or xylene.u Very competitively priced and non-hazardous to ship (flashpoint of 260°F).u One gallon bottle size for ease of use and for shipment via common carrier.




5

Single-Element Metallo-Organic StandardsFor ICP, RDE and Other Techniques

uMetallo-organic compounds* in hydrocarbon oilu Accuracy ensured by Quality Testing with NIST Standard Reference Materials when availableu Certificate of Analysis supplied with each standardu Certificate of Analysis includes trace metal concentrations confirmed with ICP-AES scansu Stocked for prompt shipment

ICP, RDE, and XRF Standards Wear Metals Metal Additives

V-Solv™ Single Elements

D SeriesStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and MetalsPetroleum Physical Test StandardsBiodiesel

Single-Element in Concentration Concentration Concentration Hydrocarbon oil (1000µg/g) (2000µg/g) (5000µg/g)Element Product No Product No. Aluminum AI VHG-OAL-1000-50G VHG-OAL-5000-50GAntimony Sb VHG-OSB-1000-50G VHG-OSB-5000-50GArsenic As VHG-OAS-1000-50G N/ABarium Ba VHG-OBA-1000-50G VHG-OBA-5000-50GBeryllium Be VHG-OBE-1000-50G InquireBismuth Bi VHG-OBI-1000-50G InquireBoron B VHG-OB-1000-50G VHG-OB-5000-50GCadmium Cd VHG-OCD-1000-50G VHG-OCD-5000-50GCalcium Ca VHG-OCA-1000-50G VHG-OCA-5000-50GCerium Ce VHG-OCE-1000-50G VHG-OCE-5000-50G Chromium Cr VHG-OCR-1000-A-50G VHG-OCR-5000-A-50GCobalt Co VHG-OCO-1000-A-50G VHG-OCODN-5000-50GCopper Cu VHG-OCU-1000-A-50G VHG-OCU-5000-A-50GIndium In Inquire InquireIron Fe VHG-OFE-1000-50G VHG-OFE-5000-50GLanthanum La VHG-OLA-1000-50G VHG-OLA-5000-50G Lead Pb VHG-OPB-1000-50G VHG-OPB-5000-50GLithium Li VHG-OLI-1000-50G VHG-OLI-5000-50GMagnesium Mg VHG-OMG-1000-50G VHG-OMG-5000-50GManganese Mn VHG-OMN-1000-50G VHG-OMN-5000-50GMercury Hg VHG-OHG-1000-50G N/AMolybdenum Mo VHG-OMO-1000-50G VHG-OMO-5000-50GNickel Ni VHG-ONI-1000-50G VHG-ONI-5000-50GPhosphorus P VHG-OP-1000-50G VHG-OP-5000-50GPotassium K VHG-OK-1000-50G VHG-OK-5000-50GScandium Sc VHG-OSC-1000-50G VHG-OSC-2000-50G N/ASelenium Se VHG-OSE-1000-50G VHG-OSE-5000-50GSilicon Si VHG-OSI-1000-50G VHG-OSI-5000-50GSilver Ag VHG-OAG-1000-50G VHG-OAG-5000-50GSodium Na VHG-ONA-1000-50G VHG-ONA-5000-50GStrontium Sr VHG-OSR-1000-50G Inquire Sulfur S VHG-OS-1000-50G VHG-OS-5000-50GThallium Tl VHG-OTL-1000-50G N/ATin Sn VHG-OSN-1000-50G VHG-OSN-5000-50GTitanium Ti VHG-OTI-1000-50G VHG-OTI-5000-50GTungsten W VHG-OW-1000-50G VHG-OW-5000-50GVanadium V VHG-OV-1000-50G VHG-OV-5000-50GYttrium Y VHG-OY-1000-A-50G VHG-OY-5000-A-50GZinc Zn VHG-OZN-1000-50G VHG-OZN-5000-50GZirconium Zr VHG-OZR-1000-50G VHG-OZR-5000-50G

* Many of these compounds are sulfonate-based, and thus, contain high levels of sulfur. If absence of sulfur is important for your application, please use VHG’s line of sulfur-free standards on .




D-Series Multi-Element Wear Metal StandardsFor Military Applications Using RDEuWe have supplied single-element concentrated standards to the Joint Oil Analysis Program -

Technical Support Center (JOAP-TSC) for making D-Series standards (D3, D12, D19) for almost a decade. Now D-Series standards are available directly from VHG.

u Our D-Series standards are made in our ISO 9001 and ISO Guide 34 facility.u Each product must pass rigorous quality control in our ISO/IEC 17025 laboratory.u Each standard is accompanied by a comprehensive Certificate of Analysis.u Each D-Series standard standard is supplied with a convenient squirt cap.

D3 Standards B, Mo, Zn in Aviation Reference OilConc. Size Product (µg/g) (mL) No.0 240 VHG-9150-00-179-5137100 240 VHG-9150-01-283-0249

D19 Standards Ag, Al, B, Ba, Cd, Cr, Cu, Fe, Mg, Mn, Mo, Na, Ni, Pb, Si, Sn, Ti, V, Zn in Aviation Reference OilConc. Size Product (µg/g) No.0 240mL VHG-9150-00-179-51375 100g VHG-D19-5-100G10 100g VHG-D19-10-100G30 100g VHG-D19-30-100G50 100g VHG-D19-50-100G80 100g VHG-D19-80-100G100 100g VHG-D19-100-100G 120 100g VHG-D19-120-100G 300 100g VHG-D19-300-100G 500 100g VHG-D19-500-100G 700 100g VHG-D19-700-100G 900 100g VHG-D19-900-100G KIT* Various VHG-9150-01-355-1178 * 9150-01-355-1178 includes 2x9150-00-179-5137, 1xD19-5-100G, 1xD19-10-100G, 1xD19-30-100G, 1xD19-50-100G, 1xD19-80-100G, 2xD19-100-100G, 1xD19-120-100G, 1xD19-300-100G, 1xD19-500-100G, 1xD19-700-100G, and 1xD19-900-100G.Special sizes, concentrations, and blends available upon request.

D12 Standards Ag, Al, Cr, Cu, Fe, Mg, Na, Ni, Pb, Si, Sn, Ti in Aviation Reference OilConc. Size Product (µg/g) (mL) No. 0 240 VHG-9150-00-179-51375 240 VHG-9150-01-307-334310 240 VHG-9150-00-179-514530 240 VHG-9150-00-179-514450 240 VHG-9150-00-179-5143100 240 VHG-9150-00-179-5142300 240 VHG-9150-00-179-5141




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ICP, RDE, and XRF Standards Wear Metals Metal Additives V-Solv™ Single Elements

D SeriesStandards for Used Oils

AN & BN Standards Fuel Dilution Coolant in Oil

Soot Crackle

Karl FischerDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and MetalsPetroleum Physical Test StandardsBiodiesel

Acid Number and Base Number Standards

Acid Number (AN) Reference MaterialsVHG Labs’ AN Reference materials are intended for use in the determination of Acid Number (AN) in petroleum products in accordance with ASTM D664/IP 177 (by potentiometric titration) or ASTM D974 (by color-indicator titration). Each standard is supplied with a full Certificate of Analysis (COA) which states the certified values and uncertainty by both ASTM D664 and D974.Matrix Nominal Value Size Product No. (mg KOH/g)* (grams)Hydrocarbon Oil 0.1 100 VHG-AN-0.1-100GHydrocarbon Oil 0.5 100 VHG-AN-0.5-100GHydrocarbon Oil 1.0 100 VHG-AN-1-100GHydrocarbon Oil 1.5 100 VHG-AN-1.5-100GHydrocarbon Oil 2.0 50 VHG-AN-2-50GHydrocarbon Oil 3.0 50 VHG-AN-3-50G*Acid number is defined as the quantity of base, expressed as milligrams (mg) of potassium hydroxide (KOH) per gram of sample, required to titrate a sample in a specific solvent to a specified end point.

Base Number (BN) Reference MaterialsVHG Labs’ BN Reference Materials are intended for use in the determination of Base Number (BN) in petroleum products in accordance with ASTM D2896/IP 276 (by potentiometric perchloric acid titration) or ASTM D4739 (by potentiometric titration). Each standard is supplied with a full Certificate of Analysis (COA) which states the certified values and uncertainty by both ASTM D2896 and D4739.Matrix Nominal Value Size Product No. (mg KOH/g)* (grams)Hydrocarbon Oil 6 50 VHG-BN-6-50GHydrocarbon Oil 10 50 VHG-BN-10-50GHydrocarbon Oil 15 50 VHG-BN-15-50GHydrocarbon Oil 30 50 VHG-BN-30-50GHydrocarbon Oil 40 50 VHG-BN-40-50GHydrocarbon Oil 70 50 VHG-BN-70-50G*Base number is defined as the quantity of acid, expressed as milligrams (mg) of potassium hydroxide (KOH) per gram of sample, required to titrate a sample in a specified solvent to a specified end point.

Nominal Soot Content Range (%) Volume (mL) Product No.Blank 50 VHG-SOOT-BLK-500.5-2 50 VHG-SOOT-A-502-4 50 VHG-SOOT-B-504-6 50 VHG-SOOT-C-506-9 50 VHG-SOOT-D-509-12 50 VHG-SOOT-E-50Set of all 6 6 x 50 VHG-SOOT-SET

Soot Content StandardsReference standards for use in the determination of soot content in 15W40 diesel motor oil by infrared spectroscopy or other techniques. All values certified by thermogravimetric analysis (TGA).




Fuel Dilution Standards

Fuel Dilution Standards These standards are intended for use in the determination of fuel (diesel fuel or gasoline) in used engine oils by GC, IR, fuel dilution meter (fuel sniffer), or flash point analyzer. They are prepared gravimetrically from well-characterized fuels and hydrocarbon oils, and are verified by GC-FID in accordance with ASTM Method D3524 or D3525. Volume: 100mLDescription Product No.Blank for Diesel Fuel Dilution Standards VHG-DSLFD-BLK-1002% (v/v) Devolatilized Diesel Fuel in hydrocarbon oil VHG-DSLFD-2P-1005% (v/v) Devolatilized Diesel Fuel in hydrocarbon oil VHG-DSLFD-5P-10010% (v/v) Devolatilized Diesel Fuel in hydrocarbon oil VHG-DSLFD-10P-100Blank for Gas Fuel Dilution Standards VHG-GASFD-BLK-1002% (v/v) Devolatilized Gasoline in hydrocarbon oil VHG-GASFD-2P-1005% (v/v) Devolatilized Gasoline in hydrocarbon oil VHG-GASFD-5P-10010% (v/v) Devolatilized Gasoline in hydrocarbon oil VHG-GASFD-10P-100

VHG TipsFuels for the fuel dilution standards are devolatilized by removing 10% of the lights using a rotovap.

Multi-Element Coolant StandardOur Multi-Element Coolant Standard is intended for use in the analysis of metals in ethylene glycol or other coolants. It can be diluted 1:1 with ethylene glycol (for matrix matching) or in dilute nitric acid. Matrix: 1% HNO3, tr. HF. Volume (mL) Product No.

500 VHG-GLYCOLSTD-500Element Conc. (µg/g) Element Conc. (µg/g)

Al 50 Mo 500

B 1000 Na 1000

Ca 50 P 2500

Cu 50 Pb 50

Fe 50 Si 500

K 1000 Zn 50

Mg 50

Ethylene Glycol in Engine Oil Standards These standards are intended for use in the determination of ethylene glycol in engine oil by gas chromatography (GC). They are intended for use with ASTM D7922. Matrix: Multi-grade Diesel Engine Oil

Description Volume Product No.

Ethylene Glycol Blank Standard 80mL VHG-EGOIL-BLK-80

100 µg/g Ethylene Glycol Standard 80mL VHG-EGOIL-100-80




600 µg/g Ethylene Glycol QC Check Standard 80mL VHG-EGOILCS-600-80

Set of all 6 Standards 6 x 80mL VHG-EGOIL-SET-6X80

Glycol in Oil Standards for ASTM D7922




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Crackle Test Reference Standards

Nominal Water Concentration (%) Volume (mL) Product No.Blank 100 VHG-CT-BLK-1000.1 100 VHG-CT-0.1P-1000.5 100 VHG-CT-0.5P-1001.0 100 VHG-CT-1.0P-100

“Crackle Test” reference standards for determining water in oil (all values nominal). The crackle test is a visual test performed by placing a small drop of oil onto a hot plate (usually around 300º F). The amount of water present in oil samples is estimated by comparison to these standards. All values certified by gravimetric preparation.

ICP, RDE, and XRF StandardsStandards for Used Oils AN & BN Standards

Fuel Dilution Coolant in Oil Soot Crackle Karl Fischer

Distillation StandardsPerformance Testing ProgramStandards for S, N, Cl and MetalsPetroleum Physical Test StandardsBiodiesel

Karl Fischer Titration Certified Reference Standards

Nominal Water Concentration (%) Volume (mL) Product No.Blank 100 VHG-KF-BLK-1000.05 100 VHG-KF-0.05P-1000.1 100 VHG-KF-0.1P-1000.5 100 VHG-KF-0.5P-1001.0 100 VHG-KF-1.0P-100

Karl Fischer Titration certified reference standards for determining water in motor oil (all values certified by Karl Fischer Titration). This test determines the amount of water present in the oil and is the most commonly-used test for this type of determination, with a high degree of accuracy. For use with ASTM D6304.

ASTM D86 Group 4 Distillation Standard VHG Labs’ Group 4 Distillation Standard is intended for use in accordance with ASTM Method D86 Distillation Group 4 for distillation of petroleum products at atmospheric pressure. This standard is a diesel oil whose distillation range is specified in ASTM D86 Distillation Group 4. It covers the boiling range 379º F to 700º F (193º to 371º C) and was verified by consensus analysis. Volume: 500mLDescription Product No.Distillation Standard VHG-D86-4-500

ASTM D86 Group 1 & 2 Synthetic Distillation Standard VHG Labs’ Group 1 & 2 Distillation Standard is intended for use in accordance with ASTM Method D86 Distillation Groups 1 & 2 and ASTM D850, for distillation of petroleum products at atmospheric pressure. This standard is a synthetic blend of hydrocarbons that boil in the temperature range specified in ASTM D86 Distillation Groups 1 & 2. It covers the boiling range 129°F to 368°F (54°C to 187°C), and was verified by consensus analysis. Volume: 500mL

Description Product No.

Synthetic Distillation Standard VHG-D86-500

Distillation Standards

Description Volume Product No.Reference Gas Oil No. 2 10 x 1 mL ampoules VHG-RGO-10X1Reference Gas Oil No. 2 2 oz. VHG-RGO-2OZ

Reference Gas Oil No. 2 for ASTM D2887This reference standard is intended for use in the determination of boiling range distribution of petroleum fractions by gas chromatography (GC), in accordance with ASTM Method D2887 Simulated Distilation.




Proficiency Testing ProgramISO/IEC 17043 Accredited

VHG Labs’ Proficiency Testing Program (PTP) was specially designed to give analytical laboratories instant validation while measuring metals, sulfur, viscosity, and particle count in new or used oils. The PTP provides participating labs with a superior method of monitoring their analytical performance as measured against Certified Reference Materials (CRMs) in three quick and easy steps.

Web-based, Accurate, Immediate Results:

1) Analyze the PTP Sample2) Enter results online3) Check your accuracy4) Receive immediate results

Provides an instant response to submitted values

VHG Proficiency Testing Program Each sample includes a single use log-in code with a 90-day expiration.Name Description Size Product No.Sample for Elemental Analysis of Elements: Ag, Al, B, Ba, Ca, Cd, 25g VHG-VPTPMO-25G Oils by ICP, RDE or other Cr, Cu, Fe, K, Mg, Mn, Mo, Na, techniques Ni, P, Pb, Sb, Si, Sn, Ti, V, ZnSample for Viscosity Analysis Viscosity Test Standard: 40°C 50mL VHG-VPTPVISC-50 and 100°CSample for Particle Count Analysis Particle Count Standard: 4µm, 125mL VHG-VPTPPC-125 (For ISO 11171 only) 6µm, 8µm, 14µm, 21µm, 38µm, 50µm and 70µm rangesSet: VPTPMO-25G, Elemental Analysis Test 1 each VHG-VPTPSET1 VPTPVISC-50, and Standard, Viscosity Test VPTPPC-125 Standard and Particle Count StandardSample for Elemental Analysis Elements: Ba, Ca, Cl, Mg, 25mL VHG-PTPLUBEMO-25 of Lube Oil by XRF or other Mo, P, S, Si, Zn techniquesSample for Lead in Isooctane Element: Pb 25g VHG-PTPPBISO-25G Analysis Sample for Sulfur in #2 Diesel Element: S 25mL VHG-PTPSDSL-25 Fuel AnalysisSample for Sulfur in 20 cSt Element: S 25mL VHG-PTPS20M-25 Mineral Oil AnalysisSample for Sulfur in Isooctane Element: S 25mL VHG-VHG-PTPSISO-25 AnalysisSample for Sulfur in B100 Element: S 25mL VHG-PTPSB100-25 Biodiesel Analysis




11

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals

Sulfur-Free Metallo- Organics Metallo-Organic Concentrates Sulfur & Metals for XRF Sulfur Nitrogen Chlorine Lead in GasPetroleum Physical Test StandardsBiodiesel

Single-Element, Sulfur-Free Metallo-Organic StandardsFor XRF and Other Techniques

u Sulfur-free metallo-organic compounds in hydrocarbon oilu Certificate of Analysis supplied with each standardu Accuracy ensured by Quality Testing with NIST Standard Reference Materials when availableu Certificate of Analysis includes trace metal concentrations

Sulfur-Free Single Concentration Concentration Element in Oil (1000µg/g) (5000µg/g)Element Product No. Product No.Aluminum AI VHG-OSF-AL-1000-50G VHG-OSF-AL-5000-50GAntimony Sb VHG-OSF-SB-1000-50G VHG-OSF-SB-5000-50GArsenic As VHG-OSF-AS-1000-50G N/ABarium Ba VHG-OSF-BA-1000-50G VHG-OSF-BA-5000-50GBeryllium Be VHG-OSF-BE-1000-50G VHG-OSF-BE-5000-50GBismuth Bi VHG-OSF-BI-1000-50G VHG-OSF-BI-5000-50GBoron B VHG-OSF-B-1000-50G VHG-OSF-B-5000-50GCadmium Cd VHG-OSF-CD-1000-A-50G VHG-OSF-CD-5000-A-50GCalcium Ca VHG-OSF-CA-1000-50G VHG-OSF-CA-5000-50GCerium Ce VHG-OSF-CE-1000-A-50G VHG-OSF-CE-5000-A-50GChromium Cr VHG-OSF-CR-1000-50G VHG-OSF-CR-5000-50GCobalt Co VHG-OSF-CO-1000-50G VHG-OSF-CO-5000-50GCopper Cu VHG-OSF-CU-1000-50G VHG-OSF-CU-5000-50GGallium Ga VHG-OSF-GA-1000-50G VHG-OSF-GA-5000-50GGold Au VHG-OSF-AU-1000-50G N/AIron Fe VHG-OSF-FE-1000-50G VHG-OSF-FE-5000-50GLead Pb VHG-OSF-PB-1000-50G VHG-OSF-PB-5000-50GLithium Li VHG-OSF-LI-1000-50G VHG-OSF-LI-5000-50GMagnesium Mg VHG-OSF-MG-1000-50G VHG-OSF-MG-5000-50GManganese Mn VHG-OSF-MN-1000-50G VHG-OSF-MN-5000-50GMercury Hg VHG-OSF-HG-1000-50G N/AMolybdenum Mo VHG-OSF-MO-1000-50G VHG-OSF-MO-5000-50GNickel Ni VHG-OSF-NI-1000-50G VHG-OSF-NI-5000-50GPhosphorus P VHG-OSF-P-1000-50G VHG-OSF-P-5000-50GPotassium K VHG-OSF-K-1000-50G VHG-OSF-K-5000-50GSelenium Se VHG-OSF-SE-1000-50G N/ASilicon Si VHG-OSF-SI-1000-50G VHG-OSF-SI-5000-50GSilver Ag VHG-OSF-AG-1000-50G VHG-OSF-AG-5000-50GSodium Na VHG-OSF-NA-1000-50G VHG-OSF-NA-5000-50GStrontium Sr VHG-OSF-SR-1000-50G VHG-OSF-SR-5000-50GThallium Tl VHG-OSF-TL-1000-50G N/ATin Sn VHG-OSF-SN-1000-50G VHG-OSF-SN-5000-50GTitanium Ti VHG-OSF-TI-1000-50G VHG-OSF-TI-5000-50GVanadium V VHG-OSF-V-1000-50G VHG-OSF-V-5000-50GYttrium Y VHG-OSF-Y-1000-A-50G VHG-OSF-Y-5000-A-50GZinc Zn VHG-OSF-ZN-1000-50G VHG-OSF-ZN-5000-50GZirconium Zr VHG-OSF-ZR-1000-50G VHG-OSF-ZR-5000-50G




Metallo-Organic ConcentratesSulfur-Free Matrix: Excellent for XRF

Metallo-Organic Concentrates - Single Element These sulfur-free, metallo-organic concentrates are ideal for X-ray fluorescence (XRF). They can be used to prepare single or multi-element standards, individually or as a set. Sulfur can be added for the simultaneous analysis of sulfur and metals. Each product is accompanied by a Certificate of Analysis that documents the assayed concentration and any trace impurities. Element Nominal Conc. Product No. Product No. Aluminum Al 3% VHG-ROSFAL3-25G VHG-ROSFAL3-100GAntimony Sb 2% VHG-ROSFSB2-25G VHG-ROSFSB2-100GBarium Ba 7% VHG-ROSFBA7-25G VHG-ROSFBA7-100GBismuth Bi 28% VHG-ROSFBI28-25G VHG-ROSFBI28-100GBoron B 3% VHG-ROSFB3-25G VHG-ROSFB3-100GCadmium Cd 7% VHG-ROSFCD7-25G VHG-ROSFCD7-100GCalcium Ca 2% VHG-ROSFCA2-25G VHG-ROSFCA2-100GCerium Ce 12% VHG-ROSFCE12-25G VHG-ROSFCE12-100GChromium Cr 9% VHG-ROSFCR9-25G VHG-ROSFCR9-100GCobalt Co 8% VHG-ROSFCO3-25G VHG-ROSFCO3-100GCopper Cu 3% VHG-ROSFCU3-25G VHG-ROSFCU3-100GIron Fe 6% VHG-ROSFFE6-25G VHG-ROSFFE6-100GLead Pb 10% VHG-ROSFPB10-25G VHG-ROSFPB10-100GLithium Li 2% VHG-ROSFLI2-25G VHG-ROSFLI2-100GMagnesium Mg 2% VHG-ROSFMG2-25G VHG-ROSFMG2-100GManganese Mn 6% VHG-ROSFMN6-25G VHG-ROSFMN6-100GMolybdenum Mo 15% VHG-ROSFMO15-25G VHG-ROSFMO15-100GNickel Ni 8% VHG-ROSFNI8-25G VHG-ROSFNI8-100GPhosphorus P 11% VHG-ROSFP11-25G VHG-ROSFP11-100GPotassium K 4% VHG-ROSFK4-25G VHG-ROSFK4-100GPraseodymium Pr 3% VHG-ROSFPR3-25G VHG-ROSFPR3-100GSilicon Si 18% VHG-ROSFSI18-25G VHG-ROSFSI18-100GSilver Ag 1% VHG-ROSFAG1-25G VHG-ROSFAG1-100GSodium Na 3% VHG-ROSFNA3-25G VHG-ROSFNA3-100GStrontium Sr 9% VHG-ROSFSR9-25G VHG-ROSFSR9-100GThallium Tl 3% VHG-ROSFTL3-25G VHG-ROSFTL3-100GTin Sn 18% VHG-ROSFSN18-25G VHG-ROSFSN18-100GTitanium Ti 7% VHG-ROSFTI7-25G VHG-ROSFTI7-100GVanadium V 4% VHG-ROSFV4-25G VHG-ROSFV4-100GYttrium Y 2% VHG-ROSFY2-25G VHG-ROSFY2-100GZinc Zn 18% VHG-ROSFZN18-25G VHG-ROSFZN18-100GZirconium Zr 24% VHG-ROSFZR24-25G VHG-ROSFZR24-100G

Stabilizer for Sulfur-Free Standard Preparation Solvent stabilizer can improve stability of mixes or dilutions of VHG’s 1000µg/g and 5000µg/g stock metallo-organic standards or concentrates, as well as multi-element mixes. Product Product Use Product No. Size (grams)MOSF Stabilizer VHG’s sulfur-free VHG-SF-STAB-100G 100 metallo-organics. Add to solutions at 15-30% v/v

VHG TipsMany commercial metallo-organic standards have matrices of sulfur-containing compounds. Use VHG’s unique sulfur-free standards if the absence of S is important for your application. Alternatively, known amounts of S can be blended intentionally.

For multi-element XRF analysis, the element concentrations should be spread randomly across the suite of standards in order to best correct for inter-element effects.




13

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals Sulfur-Free Metallo- Organics

Metallo-Organic Concentrates

Sulfur & Metals for XRF Sulfur Nitrogen Chlorine Lead in GasPetroleum Physical Test StandardsBiodiesel

Wear Metal Calibration Set Set of 17 standards with concentrations randomly arranged across the set to correct for inter-element effects. See appendix on Page 37 for exact concentrations. Suitable for ASTM D4927. Matrix: Hydrocarbon Oil Size: 50g eachElement Concentration Range (µg/g) Ag 0-500 Al 0-500 Ba 0-2000 Ca 0-5000 Cd 0-500 Cr 0-500 Cu 0-500 Fe 0-500 K 0-500 Mg 0-3000 Mn 0-500 Mo 0-500 Na 0-500 Ni 0-500 P 0-2000 Pb 0-500 Sb 0-500 Si 0-500 Sn 0-500 Ti 0-500 V 0-500 Zn 0-2000Product No. VHG-WRMTLSET-17X50G Elemental concentrations are randomly arranged across the set to correct for interelement effects. Standards in the set are not available for individual sale. See appendix on Page 37 for exact concentrations.

Wear Metal StandardsFor XRF

Standards for Sulfur & Metals in Crude and Residual OilsFor XRF

Elemental ConcentrationsSulfur (wt%) Iron (µg/g) Nickel (µg/g) Vanadium (µg/g) Product No.0.0 0 0 0 VHG-SMOIL1-1002.5 400 100 250 VHG-SMOIL2-1000.5 300 10 500 VHG-SMOIL3-1001.0 0 80 350 VHG-SMOIL4-1004.5 250 60 100 VHG-SMOIL5-1004.0 350 30 200 VHG-SMOIL6-1003.5 200 50 0 VHG-SMOIL7-1005.5 50 40 400 VHG-SMOIL8-1002.0 450 20 300 VHG-SMOIL9-1001.5 500 5 150 VHG-SMOIL10-1003.0 150 70 25 VHG-SMOIL11-1005.0 100 0 50 VHG-SMOIL12-100Product No. VHG-SMOILSET-12X100

Sulfur and Metals in Oil Suitable for ASTM D5708 For S and metals in crude and residual oils Matrix: 20 cSt Mineral Oil Volume: 100mL




Elemental ConcentrationsSulfur (wt%) Calcium (wt%) Phosphorus (wt%) Zinc (wt%) Product No.0.000 0.000 0.000 0.000 VHG-LOIL1-1000.050 0.600 0.005 0.080 VHG-LOIL2-1000.300 0.000 0.020 0.175 VHG-LOIL3-1000.150 0.500 0.030 0.070 VHG-LOIL4-1000.100 0.300 0.060 0.130 VHG-LOIL5-1000.175 0.400 0.200 0.050 VHG-LOIL6-1000.075 0.200 0.080 0.120 VHG-LOIL7-1000.125 0.250 0.050 0.000 VHG-LOIL8-1000.400 0.350 0.040 0.110 VHG-LOIL9-1000.500 0.075 0.225 0.150 VHG-LOIL10-1000.200 0.050 0.150 0.200 VHG-LOIL11-1000.550 0.005 0.000 0.140 VHG-LOIL12-1000.450 0.100 0.010 0.250 VHG-LOIL13-1000.600 0.010 0.125 0.060 VHG-LOIL14-1000.250 0.150 0.100 0.090 VHG-LOIL15-1000.350 0.025 0.175 0.100 VHG-LOIL16-100Product No. VHG-LOILSET-16X100

Lubricating Oil Standards Suitable for ASTM D4927, D6481, D6443 Matrix: Lubricating Oil Volume: 100mL

Lube Oil Standards For XRF

Lube Oil Calibration Set Suitable for ASTM D4927 Matrix: Lubricating Oil Volume: 50mLElemental Concentrations (µg/g)Ba Ca Cl Mg Mo P S Si Zn10 10 1000 400 250 2000 5000 400 50200 5000 0 350 100 1 10000 380 25030 0 400 100 0 1750 0 25 7500 4500 2000 0 200 1500 500 340 125050 0 200 300 250 20 1250 0 175030 0 1800 0 30 100 500 0 2250100 3500 0 250 150 1 12500 300 10140 20 10 800 0 1250 0 450 20300 3000 60 120 500 3 0 210 00 2000 1600 20 300 1000 15000 400 500 2500 10 50 20 1750 22500 225 0180 500 100 0 10 0 17500 220 100400 2000 600 30 150 750 0 180 0220 2 800 0 50 0 10000 140 2340 1500 100 2 0 10 1250 100 1200260 4000 4 700 0 500 0 250 1200 1000 1800 0 350 50 20000 25 2500380 500 2 400 5 250 0 10 2000300 50 1000 0 400 2250 2500 0 15000 250 1000 500 0 1250 17500 0 10000 100 1200 600 0 2500 25000 0 500340 1 1400 10 450 10 22500 0 1250 0 0 0 0 0 0 0 0 Product No. VHG-LUBESET-23X50 Elemental concentrations are randomly arranged across the set to correct for interelement effects.




15

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals Sulfur-Free Metallo- Organics Metallo-Organic Concentrates

Sulfur & Metals for XRF Sulfur

Nitrogen Chlorine Lead in GasPetroleum Physical Test StandardsBiodiesel

Sulfur Standards in Petroleum Products

u Wide range of products for ULSD analysisu Standards are manufactured in accordance with applicable ASTM methods in VHG Labs’

ISO 9001 and ISO Guide 34 facilityu Certificate of Analysis provided from our ISO/IEC 17025 laboratory showing NIST traceability

of standardu “Blank” standards include ppb-level sulfur concentration on Certificate of Analysis

Sulfur in Kerosene StandardsSulfur in Kerosene Standards suitable for use with ASTM D2622, D3120, D4045, D4294, D5453, and others. Volume: 100mL Concentration Product No. (µg/g) (wt%)Blank Blank VHG-SKERO-BLK-10010 0.0010 VHG-SKERO-10-10050 0.0050 VHG-SKERO-50-100100 0.0100 VHG-SKERO-100-100300 0.0300 VHG-SKERO-300-100500 0.0500 VHG-SKERO-500-100750 0.0750 VHG-SKERO-750-1001000 0.100 VHG-SKERO-1000-100

Full-range of Sulfur Standards for XRF. ASTM Methods D2622, D4294, D5453, D7039, D7212, D7220 and others. Matrix: See Below Volume: 100mL Concentration Light Mineral Oil Heavy Mineral Oil #2 Diesel Fuel (µg/g) (wt%) Product No. Product No. Product No.Blank Blank VHG-S20MIN-BLK-100 VHG-SMIN-BLK-100 VHG-SDSL-BLK-1005 0.0005 VHG-S20MIN-5-100 VHG-SMIN-5-100 VHG-SDSL-5-10010 0.0010 VHG-S20MIN-10-100 VHG-SMIN-10-100 VHG-SDSL-10-10015 0.0015 VHG-S20MIN-15-100 VHG-SMIN-15-100 VHG-SDSL-15-10020 0.0020 VHG-S20MIN-20-100 VHG-SMIN-20-100 VHG-SDSL-20-10025 0.0025 VHG-S20MIN-25-100 VHG-SMIN-25-100 VHG-SDSL-25-10050 0.0050 VHG-S20MIN-50-100 VHG-SMIN-50-100 VHG-SDSL-50-10075 0.0075 VHG-S20MIN-75-100 VHG-SMIN-75-100 VHG-SDSL-75-100100 0.0100 VHG-S20MIN-100-100 VHG-SMIN-100-100 VHG-SDSL-100-100200 0.0200 VHG-S20MIN-200-100 VHG-SMIN-200-100 VHG-SDSL-200-100300 0.0300 VHG-S20MIN-300-100 VHG-SMIN-300-100 VHG-SDSL-300-100400 0.0400 VHG-S20MIN-400-100 VHG-SMIN-400-100 VHG-SDSL-400-100500 0.0500 VHG-S20MIN-500-100 VHG-SMIN-500-100 VHG-SDSL-500-100750 0.0750 VHG-S20MIN-750-100 VHG-SMIN-750-100 VHG-SDSL-750-1001000 0.100 VHG-S20MIN-1000-100 VHG-SMIN-1000-100 VHG-SDSL-1000-1001500 0.150 VHG-S20MIN-1500-100 VHG-SMIN-1500-100 VHG-SDSL-1500-1003000 0.300 VHG-S20MIN-3000-100 VHG-SMIN-3000-100 VHG-SDSL-3000-1005000 0.500 VHG-S20MIN-5000-100 VHG-SMIN-5000-100 VHG-SDSL-5000-1007500 0.750 VHG-S20MIN-7500-100 VHG-SMIN-7500-100 VHG-SDSL-7500-10010,000 1.00 VHG-S20MIN-1P-100 VHG-SMIN-1P-100 VHG-SDSL-1P-10020,000 2.00 VHG-S20MIN-2P-100 VHG-SMIN-2P-100 VHG-SDSL-2P-10030,000 3.00 VHG-S20MIN-3P-100 VHG-SMIN-3P-100 VHG-SDSL-3P-10040,000 4.00 VHG-S20MIN-4P-100 VHG-SMIN-4P-100 VHG-SDSL-4P-10050,000 5.00 VHG-S20MIN-5P-100 VHG-SMIN-5P-100 VHG-SDSL-5P-100

Standards for Sulfur in Diesel Fuel Analysis




Sulfur in Crude Oil and Sulfur in Residual Oil Standards that are suitable for use with ASTM D2622, D4294, and others. Matrix: See Below Volume: 100mL Concentration Crude Oil Residual Oil (µg/g) (wt%) Product No. Product No.Unspiked Matrix Blank VHG-CRUDE-1001000 0.100 VHG-SCRD-1000-1002500 0.250 VHG-SCRD-2500-100 VHG-SRES-2500-1005000 0.500 VHG-SCRD-5000-100 VHG-SRES-5000-10010,000 1.00 VHG-SCRD-1P-100 VHG-SRES-1P-10020,000 2.00 VHG-SCRD-2P-100 VHG-SRES-2P-10030,000 3.00 VHG-SCRD-3P-100 VHG-SRES-3P-10040,000 4.00 VHG-SCRD-4P-100 VHG-SRES-4P-10050,000 5.00 VHG-SCRD-5P-100 VHG-SRES-5P-100

Sulfur in Crude and Residual Oil Standards

High-purity Matrix Oils and Solvents (<1ppm Sulfur) for the preparation of working standards for petroleum analysis. Supplied with a Certificate of Analysis that includes trace sulfur and metal concentrations. Matrix Volume Product No.20 cSt Mineral Oil 500mL VHG-OIL-20MIN-50020 cSt Mineral Oil 0.5 gal. VHG-OIL-20MIN-1/2GAL75 cSt Mineral Oil 500mL VHG-OIL-MIN-50075 cSt Mineral Oil 0.5 gal. VHG-OIL-MIN-1/2GAL#2 Diesel Fuel 500mL VHG-ULSDSL-500#2 Diesel Fuel 0.5 gal. VHG-ULSDSL-1/2GALIsooctane 500mL VHG-ISO-500Isooctane 0.5 gal. VHG-ISO-1/2GALKerosene, low odor 500mL VHG-KERO-500Kerosene, low odor 0.5 gal. VHG-KERO-1/2GAL

Matrix Oils and Solvents

Concentration Product No.(µg/g) (wt%)Blank Blank VHG-SISO-BLK-1005 0.0005 VHG-SISO-5-10010 0.0010 VHG-SISO-10-10015 0.0015 VHG-SISO-15-10020 0.0020 VHG-SISO-20-10025 0.0025 VHG-SISO-25-10050 0.0050 VHG-SISO-50-10075 0.0075 VHG-SISO-75-100100 0.0100 VHG-SISO-100-100200 0.0200 VHG-SISO-200-100300 0.0300 VHG-SISO-300-100400 0.0400 VHG-SISO-400-100500 0.0500 VHG-SISO-500-100750 0.0750 VHG-SISO-750-1001000 0.100 VHG-SISO-1000-1003000 0.300 VHG-SISO-3000-100

Sulfur in Isooctane standards that are ideal for use with the following ASTM methods: D2622, D3120, D3246, D4045, D4294, D5453, D6334, D6445, D7039, D7212, D7220, and others. Volume: 100mL

Sulfur in Isooctane Standards

VHG TipsMatrix oil blanks are necessary for most analytical techniques of petroleum products. VHG Labs provides a wide range of clean, pure blanks designed to get the most from your analysis.




17

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals Sulfur-Free Metallo- Organics Metallo-Organic Concentrates Sulfur & Metals for XRF

Sulfur Nitrogen Chlorine Lead in GasPetroleum Physical Test StandardsBiodiesel

Polysulfide Oil Standards

Sulfur QC Samples, Drift Monitors and Calibration Standards Made from Polysulfide Oil

Our polysulfide oils have been formulated for long shelf life and optimal stability even when exposed to x-rays from modern high wattage XRF spectrometers. In addition, our polysulfide oil products offer high purity, low volatility, and minimal diffusion through sample films.

These standards are well suited to ultra low level sulfur analysis, quality control, drift correction, blank measurement and calibration standards for XRF and other sulfur analysis techniques. Our polysulfide oil standards are intended for use in accordance with ASTM D2622, D4294, D7039, D7212, D7220 and others.

Description Product No.QC SamplesSulfur @ 5µg/g, Polysulfide oil, 1L VHG-PS13M-5-1LSulfur @ 10µg/g, Polysulfide oil, 1L VHG-PS13M-10-1LSulfur @ 25µg/g, Polysulfide oil, 1L VHG-PS13M-25-1LDrift MonitorsSulfur @ 100µg/g, Polysulfide oil, 1L VHG-PS13M-100-1LSulfur @ 500µg/g, Polysulfide oil, 1L VHG-PS13M-500-1LSulfur @ 1000µg/g, Polysulfide oil, 1L VHG-PS13M-1000-1LBlankPolysulfide Oil Blank VHG-OIL-13-1LCalibration SetsSulfur Standard Set (low concentrations). VHG-PS13M-SET1-13X50

Set of 13 Calibration Standards with Sulfur @ 0, 1, 2.5, 5, 10, 25, 50, 75, 100, 250, 500, 750, 1000µg/g, made from high-purity polysulfide oil, 50mL each

Sulfur Standard Set (high concentrations). VHG-PS13M-SET2-12X50 Set of 12 Calibration Standards with Sulfur @ 0, 0.1, 0.5, 1, 1.5, 2,2.5, 3, 3.5, 4, 4.5 and 5wt%, made from high-purity polysulfide oil, 50mL each

Sulfur Standard Set (low concentrations). VHG-PS13M-SET3A-6X50 Set of 6 Calibration Standards with Sulfur @ 0, 10, 25, 50, 100 and 250µg/g, made from high-purity polysulfide oil, 50mL each

Ultra Low Sulfur EPA Qualification Set VHG-PS13M-SET4-40X20 Set of 40 Calibration Standards with 10 Sulfur Standards @ 5 and 15µg/g each, and 20 @ 10µg/g, made from high-purity polysulfide oil, 20mL each

High Sulfur EPA Qualification Set VHG-PS13M-SET5-40X20 Set of 40 Calibration Standards with 10 Sulfur Standards @ 100 and 500µg/g each, and 20 @ 300µg/g, made from high-purity polysulfide oil, 20mL each




Concentration (ng/µL) Matrix Size Product No.0, 1.0, 2.5, 5, 7.5, 10 Isooctane 6x2mL VHG-SUVF-SET10, 5, 25, 50, 100, 200 Isooctane 6x2mL VHG-SUVF-SET20, 100, 250, 500, 750, 1000 Isooctane 6x2mL VHG-SUVF-SET3

Total Sulfur by UV FluorescenceCalibration Set for ASTM Method D5453 - Total Sulfur in Liquid Petroleum Hydrocarbons by Ultraviolet Fluorescence. Composition: Sulfur in Isooctane. Offered only as a single set of 6 x 2mL ampoules. Sets also available in toluene upon request.

Sulfur Compounds by Selective Detection (50µg/g) Calibration Standard for ASTM D5623 - Sulfur Compounds in Light Hydrocarbon Liquids by Selective Detection. Composition: Multi-component mixture containing twenty-two (22) sulfur species in base fuel (40% LV isooc-tane/40% LV hexane/20% LV toluene). Sulfur species include: 2-methyl-1-propanethiol, 2-methylthiophene, 3-methylthiophene, 1,2-ethane dithiol, 1-pentanethiol, 2-ethylthiophene, propylsulfide, t-butyldisulfide, 1,5-pen-tanedithiol, 1-nonanethiol, 1-decanethiol, propanethiol, t-butylsulfide, 1-heptanethiol, 1,4-butanedithiol, methyl ethylsulfide, propyl disulfide, 1-octanethiol, benzothiophene, 1-hexanethiol, carbon disulfide, and methyl sulfide. Offered as a single 2mL ampoule.

Concentration of Species Matrix Size Product No.50µg/g (as component) Base Fuel 2mL VHG-MSX22-2

Sulfur Compounds by Selective Detection (100µg/g) Calibration Standard for ASTM D5623 - Sulfur compounds in Light Hydrocarbon Liquids by Selective Detection. Composition: Multi-component mixture that contains fourteen (14) sulfur species in base fuel (40% LV isooctane/40% LV hexane/20% LV toluene). Sulfur species include: methanethiol, ethanethiol, dimethylsulfide, 2-propanethiol, t-butanethiol, 1-propanethiol, thiophene, diethylsulfide, 1-butanethiol, diethyl disulfide, thiophenol, benzothiophene, bromothiophene (as internal standard), and phenyl sulfide. Offered as a single 2mL ampoule.

Concentration of Species Matrix Size Product No.100µg/g (as Sulfur) Base Fuel 2mL VHG-MSX14-2

Determination of Mercaptan SulfurCalibration Standards for UOP 163 and ASTM D3227 - Mercaptan Sulfur in Hydrocarbon Liquids by Potentiometric Titration. Composition: Sulfur (from 1-octanethiol) in isooctane/toluene. Offered only as a single set of 6 x 20mL ampoules.

Concentration (µg/g) Matrix Size Product No.30 80% Isooctane/ 6x20mL VHG-UOP163-30-6X20 20% Toluene

Sulfur by Hydrogenolysis and Rateometric ColorimetryCalibration Set for ASTM D4045 - Sulfur in Petroleum Products by Hydrogenolysis and Rateometric Colorimetry. Composition: Sulfur (from n-dibutyl sulfide) in isooctane. Offered only as a single set of 7 x 2mL ampoules.

Concentration (µg/g) Matrix Size Product No.0, 0.1, 0.5, 1.0, 2.5, 5.0, 10 Isooctane 7x2mL VHG-SRC-SET1A

Sulfur in Petroleum Products (Ampoules)For Low-Level Sulfur Analytical Techniques




19

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals Sulfur-Free Metallo- Organics Metallo-Organic Concentrates Sulfur & Metals for XRF

Sulfur Nitrogen Chlorine

Lead in GasPetroleum Physical Test StandardsBiodiesel

Sulfur and Nitrogen Products (Ampoules)For Low-Level Analytical Techniques

Chlorine in Oil Standards For XRF, ICP and Other TechniquesChlorine Standards in Oil (ASTM D4929 or D5384) Matrix: Heavy Mineral Oil Volume: 100mL Concentration (µg/g) (wt%) Oil Product NoBlank Blank VHG-CLOIL-BLK-10010 0.001 VHG-CLOIL-10-100100 0.010 VHG-CLOIL-100-100500 0.050 VHG-CLOIL-500-1001000 0.10 VHG-CLOIL-1000-10010,000 1.00 VHG-CLOIL-1P-10050,000 5.00 VHG-CLOIL-5P-100

Sulfur and Nitrogen CombinedCalibration Set for instruments designed for simultaneous determination of sulfur and nitrogen. Composition: Sulfur and Nitrogen in isooctane. Offered only as a single set of 6 x 2mL ampoules. Also available in toluene upon request.

Concentration (ng/µL) Matrix Size Product No.S @ 0, 1, 5, 10, 15, 20; Isooctane 6x2mL VHG-SN-SET1 N @ 0, 1, 5, 20, 35, 50

Trace Nitrogen by ChemiluminescenceCalibration Set for ASTM Method D4629 - Trace Nitrogen in Liquid Petroleum Hydrocarbons by Chemiluminescence Detection. Composition: N (from pyridine) in isooctane. Offered only as a single set of 9 x 2mL ampoules. Also available in toluene upon request.Concentration (ng/µL) Matrix Size Product No.0, 1, 2, 10, 20, 50, 100, Isooctane 10x2mL VHG-NCH-SET1 200, 500, 1000

Trace Nitrogen by Oxidative Combustion and Electrochemical DetectionCalibration Set for ASTM D6366 - Total Trace Nitrogen and its Derivatives in Liquid Aromatic Hydrocarbons by Oxidative Combustion and Electrochemical Detection. Composition: N (from pyridine) in p-xylene [Set 1] or isooctane [Set 2]. Offered only as single sets of 2mL ampoules. Set also available in toluene upon request (with N from carbazole).Concentration (ng/µL) Matrix Size Product No.0.1, 0.5, 1.0, 2.5, 5.0, 10 p-xylene 6x2mL VHG-NCED-SET1B10, 25, 50, 75, 100 Isooctane 5x2mL VHG-NCED-SET2




Standards for Lead in Gasoline

Bismuth Internal Standard for ASTM D5059Matrix: Mineral OilMethod Conc. Bi Size (grams) Product No.ASTM D5059 Pt. A and C 0.793g/L 100 VHG-BIIS-100G 0.793g/L 400 VHG-BIIS-400G

Lead In Isooctane Standards for XRF (ASTM D5059)Matrix: Isooctane Volume: 100 GramsMethod Conc. (g/gal)* Product No.ASTM D5059 Pt. A 0.0 VHG-PBISO-BLK-100G“ 0.1 VHG-PBISO-0.1-100G“ 1.0 VHG-PBISO-1-100G“ 2.0 VHG-PBISO-2-100G“ 3.0 VHG-PBISO-3-100G“ 4.0 VHG-PBISO-4-100G“ 5.0 VHG-PBISO-5-100GASTM D5059 Pt. A Set VHG-PBISOSETA-7X100GASTM D5059 Pt. C 0.000 VHG-PBISO-BLK-100G“ 0.001 VHG-PBISO-0.001-100G“ 0.005 VHG-PBISO-0.005-100G“ 0.010 VHG-PBISO-0.010-100G“ 0.050 VHG-PBISO-0.050-100G“ 0.100 VHG-PBISO-0.100-100G“ 0.300 VHG-PBISO-0.300-100GASTM D5059 Pt. C Set VHG-PBISOSETC-7X100G

*Note: For approximate conversion from g/gal to µg/g (ppm), multiply by 380 i.e., 0.1 g/gal=38µg/g

Internal Standards for XRF AnalysisSulfur-Free Raw Material in OilInternal Standards for XRF AnalysisElement Method Concentration Product No. Product No.Bismuth ASTM D5059 0.793g/L VHG-BIIS-100G VHG-BIIS-400G Pb AnalysisManganese ISO 14597 0.05% VHG-MNIS-100G VHG-MNIS-400G Ni and V Analysis Zirconium ISO 14596 1% VHG-ZRIS1P-100G VHG-ZRIS1P-400G Sulfur Analysis

VHG TipsTo convert lead in isooctane concentrations from g/gal to µg/g (ppm), multiply by 380 i.e., 0.1 g/gal=38µg/g.




21

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and Metals Sulfur-Free Metallo- Organics Metallo-Organic Concentrates Sulfur & Metals for XRF Sulfur Nitrogen Chlorine

Lead in GasPetroleum Physical Test Standards

Flash Point Viscosity

Pour Point Cloud Point Freezing Point Cold Filter Plug PointBiodiesel

Petroleum Physical Test Standards

Flash Point Reference Materials VHG Labs’ Flash Point Reference materials are intended for use with and certified by the appropriate ASTM Methods [ASTM D56, D92, D93]. Each standard is verified by consensus analysis, and is supplied with a full Certificate of Analysis (COA) that states the certified value. Volume: 250mL Specification Apparatus Typical Flash Product No. Point Range (°C) ASTM D93 (Flash Point) Pensky-Martens 25-35 VHG-FP27-250 Closed-Cup Tester 55-65 VHG-FPPM60-250 70-80 VHG-FP75-250 VHG-FP93-250ASTM D92 Cleveland Open Cup 190-215 VHG-FP200-250 (Flash and Fire Point) Tester 220-240 VHG-FP230-250ASTM D56 (Flash Point) Tag Closed Cup 40-50 VHG-FP40-250 Tester 50-60 VHG-FP55-250 55-65 VHG-FPTC60-250

Flash Point Certified Reference MaterialsVHG Labs’ Flash Point Certified Reference Materials are intended for use in accordance with the specified ASTM Methods [ASTM D56, D92, D93]. They consist of stable, pure hydrocarbons with a method-specific flash point de-termined by an inter-laboratory study. Each standard is supplied with a full Certificate of Analysis (COA) that states the certified value. Volume: 250mL

ASTM Method Hydrocarbon Typical Flash Product No. Point Range (°C)D93 Flash Point n-Decane 45-55 VHG-FP53-250 Pensky-Martens n-Undecane 65-75 VHG-FP70-250 Closed Cup Tester n-Tetradecane 110-120 VHG-FP114-250 n-Hexadecane 130-145 VHG-FP134-250D92 Flash & Fire Point n-Tetradecane 110-120 VHG-FP115-250 Cleveland Open Cup Tester n-Hexadecane 135-150 VHG-FP138-250D56 Flash Point n-Decane 45-55 VHG-FP51-250 Tag Closed Cup Tester n-Undecane 60-70 VHG-FP67-250

Nominal Viscosity @ 40ºC (cSt) Nominal Viscosity @ 100ºC (cSt) Product No.4.5 1.6 VHG-VISC5-50010 2.7 VHG-VISC10-50019 5 VHG-VISC20-50030 5.3 VHG-VISC30-50050 7.3 VHG-VISC50-50060 11.4 VHG-VISC60A-50073 9 VHG-VISC75-500100 16.8 VHG-VISC100A-500120 20 VHG-VISC120-500180 26 VHG-VISC180-500360 42 VHG-VISC360-500500 52 VHG-VISC500-500930 82 VHG-VISC900-500

Viscosity Reference StandardsVHG Labs provides viscosity reference standards, intended for use in accordance with standard methods [e.g. ASTM D445]. Each standard is manufactured in our ISO 9001 and ISO Guide 34 facility and certified in our ISO/IEC 17025 laboratory. Volume: 500mL




Petroleum Physical Test Standards

ASTM D2500 Cloud Point Reference MaterialsVHG Labs’ Cloud Point Reference Materials are intended for use in accordance with ASTM D2500 for the de-termination of the cloud point of petroleum products. The cloud point of a petroleum product is an index of the lowest temperature of their utility for certain applications. Each standard is verified by consensus analysis, and is supplied with a full Certificate of Analysis (COA) that states the certified value.Volume: 250mLTypical Cloud Point Range (°C) Product No.+3 to +9 VHG-C5-250-4 to 0 VHG-C2-250-12 to -8 VHG-C10-250-17 to -13 VHG-C15-250-22 to -18 VHG-C20-250

ASTM D2386 Freezing Point Reference MaterialsVHG Labs’ Freezing Point Reference Materials are intended for use in accordance with ASTM Method D2386 for determination of the freezing point of aviation fuels. Each standard is verified by consensus ayalysis, and is supplied with a full Certificate of Analysis (COA) that states the certified value.Volume: 250mLTypical Freezing Point Range (°C): Product No.-47 to -42 VHG-F45-250-52 to -48 VHG-F50-250

ASTM D97 Pour Point Reference MaterialsVHG Labs’ Pour Point Reference Materials are intended for use in accordance with ASTM D97 only, for deter-mination of the pour point of petroleum products. Each standard is verified by consensus analysis, and is sup-plied with a full Certificate of Analysis (COA) that states the certified value. Volume: 250mLTypical Pour Point Range (°C) Product No.-7 to -3 VHG-P5-250-12 to -8 VHG-P10-250-17 to -13 VHG-P15-250-22 to -18 VHG-P20-250-42 to -36 VHG-P40-250-53 to -47 VHG-P50-250

ASTM D6371 Cold Filter Plug Point Reference MaterialsVHG Labs’ Cold Filter Plug Point Standards are intended for use in accordance with ASTM Method D6371/IP309 for determination of the cold filter plug point of diesel and heating fuels. Each standard is verified by consensus analysis, and is supplied with a full Certificate of Analysis (COA) that states the certified value.Volume: 250mLTypical Plug Point Range (°C) Product No.-20 to -17 VHG-CFP1-250

u The following physical test standards are not intended for use with Phase Instruments.




23

ICP, RDE, and XRF StandardsStandards for Used OilsDistillation StandardsPerformance Testing ProgramStandards for S, N, Cl and MetalsPetroleum Physical Test Standards Flash Point Viscosity

Pour Point Cloud Point Freezing Point Cold Filter Plug Point

Biodiesel

Metals in Biodiesel Standards These standards have been formulated specifically for the analysis of metals in biodiesel fuel in accordance with ASTM D6751, EN 14107, EN 14108, EN 14109, EN 14214, or EN 14538.Description Product No.Ca, K, Mg, Na, P @ 5µg/g, B100 Biodiesel, 100g VHG-B100M5-5-100GCa, K, Mg, Na, P @10µg/g, B100 Biodiesel, 100g VHG-B100M5-10-100GCa, K, Mg, Na, P @20µg/g, B100 Biodiesel, 100g VHG-B100M5-20-100GSSulfur in Biodiesel Standards These standards have been formulated specifically for the analysis of sulfur in biodiesel fuel in accordance with ASTM D2622 , D4294, or D5453.Description Product No.Sufur @ 5µg/g, B100 Biodiesel, 100mL VHG-SB100-5-100Sufur @ 10µg/g, B100 Biodiesel, 100mL VHG-SB100-10-100Sufur @ 15µg/g, B100 Biodiesel, 100mL VHG-SB100-15-100Sufur @ 20µg/g, B100 Biodiesel, 100mL VHG-SB100-20-100Sufur @ 25µg/g, B100 Biodiesel, 100mL VHG-SB100-25-100Sufur @ 50µg/g, B100 Biodiesel, 100mL VHG-SB100-50-100Sufur @ 100µg/g, B100 Biodiesel, 100mL VHG-SB100-100-100Sufur @ 500µg/g, B100 Biodiesel, 100mL VHG-SB100-500-100Biodiesel Blanks These solutions are intended for use as calibration blanks for analysis of metals or sulfur in biodiesel. Each is supplied with a Certificate of Analysis (COA) that includes relevant trace metal and sulfur concentrations.Description Product No.B100 Biodiesel Blank, 100mL VHG-B100-BLK-100B100 Biodiesel Blank, 500mL VHG-B100-BLK-500Biodiesel/Diesel Fuel Blends These standards are intended for use as calibration or reference standards for the determination of fatty acid methyl esters (FAME) biodiesel content in diesel fuel by infrared (IR) spectroscopy. They are formulated specifically for use with ASTM Method D7371 or EN 14078..Description Product No.100% High Cetane Diesel Fuel, 20mL VHG-BDBLEND-BLK-202% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-2P-205% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-5P-2010% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-10P-2015% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-15P-2020% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-20P-2025% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-25P-2030% (v/v) Biodiesel in High Cetane Diesel Fuel, 20mL VHG-BDBLEND-30P-20 100% (v/v) Biodiesel, 20mL VHG-BDBLEND-100P-20

Biodiesel StandardsAs the demand for biofuels continues to rise, the need to reliably analyze these products has become a necessity for the petroleum industry.

Most biodiesel fuels are comprised of a blend of traditional refined diesel combined with biodiesel fuel. The percentage of biodiesel in the blend is generally 5%, 10% or 15%, and is labeled B5, B10, or B15 respectively. Pure biodiesel (100%) is labeled B100. All of our diesel standards have a matrix of 100% biodiesel. This is important in the analysis of ma-terials by ICP and other methods because the analysis can often be encumbered by the variance of matrices from standards to samples.

Our biodiesel standards have been formulated specifically for the analysis of metals and sulfur in biodiesel fuel. Our B100 is made from soybean oil and is an excellent matrix match for almost all biodiesel fuel analysis.


Reference standards for residue and environmental testing

The Dr. Ehrenstorfer range of neats, solutions and mixes includes:• PAHs• Dyes• Phthalates• Toxaphene single

components• Pharmaceutical

and veterinary compounds

• PCBs• Phenols• Chlorinated paraffins

• Pesticides and pesticide metabolites

• And many more

Over 8000 pesticide and other organic reference materials

www.lgcstandards.comScience for a safer world


© LGC Limited, 2015. All rights reserved. 4436/CB/1115

4436 - Dr E.advert.indd 1 11/9/2015 1:16:00 PM

CRMs to verify analytical procedures




Section 2CRMs to verify

Analytical Procedures

CRMs to verify Analytical ProceduresDiesel

* For catalog purposes, nominal concentrations (µg/g) are provided.

Code CRM BTU C % H % N %

S % S ppm Unit

IARM-HP-14050RE

HP-14050RE (19500) (85) (13.1) 0.5 5000 each

IARM-HP-14005RD

HP-14005RD 0.0054 54 each

IARM-HP-14001C

#2 Diesel - 0.01% S 0.013 130 each

IARM-HP-14003C

#2 Diesel - 0.03% S 0.031 310 4oz bottle

IARM-HP-14003RC

#2 Diesel - 0.03% S RM 0.031 310 16oz bottle

IARM-HP-14010D

#2 Diesel - 0.10% S CRM 0.105 1050 each

IARM-HP-14300RJ

HP-14300RH 3.01 30100 each

ERM-EF673 Diesel - Sulfur 0.00524 52.4 100 mL

ERM-EF674 Diesel - Sulfur 0.0011 11 100 mL

NIST-1624d Diesel fuel oil - Sulfur 0.3882 3882 100 mL

NIST-2723B Sulfur in Diesel Fuel Oil (Nominal Mass Fraction 10mg/kg)

0.000906 9.06 100 mL

NIST-2770 Diesel fuel oil - Sulfur 0.004157 41.57 10 x 10 mL

AR-2821 #2 Diesel Oil 0.148 1480 118 mL

AR-2961 #2 Diesel Oil 0.206 2060 118 mL

AR-2822 #2 Diesel Oil 0.305 3050 118 mL

AR-2962 #2 Diesel Oil 0.4 4000 118 mL

AR-2823 #2 Diesel Oil 0.53 5300 118 mL

AR-2963 #2 Diesel Oil 0.61 6100 118 mL

AR-2824 #2 Diesel Oil 0.7 7000 118 mL

AR-2964 #2 Diesel Oil 0.808 8080 118 mL

AR-2965 #2 Diesel Oil 0.853 8530 each

AR-2825 #2 Diesel Oil 1.02 10200 118 mL

AR-2826 #2 Diesel Oil 1.50 15000 118 mL

AR-2827 #2 Diesel Oil 1.867 18670 118 mL

AR-2828 #2 Diesel Oil 2.53 25300 118 mL

AR-2829 #2 Diesel Oil 2.95 29500 118 mL

AR-2868 Ultra Low #2 Diesel Oil <0.0001 <1 118 mL

AR-2882 Sulfur #2 Diesel Oil 0.00049 4.9 118 mL

AR-2881 #2 Diesel Oil 0.0010 10 118 mL

AR-2869 #2 Diesel 0.0021 21 each

AR-2879 #2 Diesel Oil 0.0025 25 118 mL

AR-2878 #2 Diesel Oil 0.0049 49 100 mL

AR-2871 Ultra Low #2 Diesel Oil 0.0102 102 118 mL

26

LGC Petroleum Catalog-CRM-products-v10 MC 110415.indd 1 11/9/2015 11:40:27 AM


DieselCode CRM BTU C % H % N % S % S ppm UnitAR-2872 Ultra Low #2 Diesel Oil 0.0207 207 118 mL











Bio-Diesel

Code CRM FAMEAR-2971 Biodiesel Contaminant in

Synthetic Diesel0.000

AR-2972 Biodiesel Contaminant in Synthetic Diesel

0.025


0.05


0.075


0.100

AR-2980 Biodiesel Contaminant in #2 Diesel

0.000


0.025


0.050


0.075


0.100


0.500


1.00


3.00


5.00

27





Gasoline / Gasoil / Kerosene


Code CRM BTU C % H % N %

S % S ppm Unit

ERM-EF104 Gas oil - Sulfur 0.1019 1019 8 mL

ERM-EF211 Petrol - Sulfur 0.00488 48.8 19 mL

ERM-EF212 Petrol - Sulfur 0.00202 20.2 19 mL

ERM-EF213 Petrol - Sulfur 0.00091 9.1 Amp.

ERM-EF671 Gas oil - Sulfur 0.0452 452 8 mL

ERM-EF672 Gas oil - Sulfur 0.00203 20.3 8 mL

NIST-1616b Kerosene - Sulfur 0.000841 8.41 100 mL

NIST-1617B Kerosene - Sulfur (86.30) (13.90) 0.1250 1250 100 mL

NIST-2294 Reformulated gasoline - Sulfur, benzene, MTBE and toluene

0.00409 40.9 2 x 20 mL


0.0308 308 2 x 20 mL


0.0040 40 2 x 20 mL


0.03037 303.7 2 x 20 mL

NIST-2298 Gasoline (High-Octane) - Sulfur

0.00047 4.7 5 x 20 mL

NIST-2299 Gasoline (Reformulated) - Sulfur

0.00136 13.6 5 x 20 mL

BCR-105 Gas oil - Sulfur 0.363 3630 25 g



AR-6201 Ultra Low Kerosene 0.0010 10 118 mL





AR-6210 Ultra Low Kerosene 0.00635 63.5 118 mL








AR-2849 Kerosene <0.0001 <1 118 mL

AR-2841 Kerosene 0.0125 125 118 mL

AR-2951 Kerosene, 0.02% S 0.0211 211 118 mL

AR-2842 Kerosene 0.029 290 118 mL

28

VHG TipsWe stock a variety of high- quality sample cups and thin film for XRF instruments.



Gasoline / Gasoil / KeroseneCode CRM BTU C % H % Pb % N % S % S ppm UnitAR-2952 Kerosene, 0.04% S 0.0420 420 118 mL

AR-2843 Kerosene 0.049 490 118 mL

AR-2953 Kerosene, 0.06% S 0.062 620 118 mL

AR-2954 Kerosene, 0.07% S 0.071 710 118 mL

AR-2955 Kerosene, 0.08% S 0.0801 801 118 mL

AR-2956 Kerosene, 0.09% S 0.090 900 118 mL

AR-2844 Kerosene 0.1313 1313 118 mL

AR-2845 Kerosene 0.1968 1968 118 mL

AR-2846 Kerosene 0.30 3000 118 mL

AR-2847 Kerosene 0.395 3950 118 mL

AR-2848 Kerosene 0.505 5050 118 mL

AR-2921 JP Fuel 0.0051 51 118 mL

AR-2922 JP Fuel 0.0111 111 118 mL

AR-2923 JP Fuel 0.0198 198 118 mL

AR-2924 JP Fuel 0.0300 300 118 mL

AR-2925 JP Fuel 0.0433 433 118 mL

AR-2926 JP Fuel 0.050 500 118 mL

AR-2927 JP Fuel 0.062 620 118 mL

AR-2928 JP Fuel 0.093 930 118 mL

AR-3001 Sulfur in Gasoline 0.000101 1.01 118 mL

AR-3002 Sulfur in Gasoline 0.0052 52 118 mL






AR-2067 Pb in Gasoline <0.0001 118 mL

AR-2066 Pb in Gasoline 0.0101 118 mL






AR-3111 Gasoline 0.00031 0.1023 1023 118 mL

AR-3112 Gasoline 0.000090 0.0524 524 118 mL

AR-3113 Gasoline 0.0040 0.0106 106 118 mL

AR-3114 Gasoline 0.0082 0.000106 1.06 118 mL

AR-3115 Gasoline <0.0001 <0.0001 <1 118 mL

29







Lube Oil CRMs / Lubricants


Code CRM S % S ppm UnitIARM-HP-13100C

White Mineral Oil - 1.0000% S 1.01 10100 each

AR-2838 Lube Oil 0.0100 100 118 mL

AR-2931 Lube Oil 0.0207 207 118 mL

AR-2932 Lube Oil 0.0524 524 118 mL

AR-2831 Lube Oil 0.073 730 118 mL

AR-2933 Lube Oil 0.0805 805 118 mL

AR-2934 Lube Oil 0.1008 1008 118 mL

AR-2832 Lube Oil 0.230 2300 118 mL

AR-2935 Lube Oil 0.3537 3537 118 mL

AR-2833 Lube Oil 0.511 5110 118 mL

AR-2834 Lube Oil 0.753 7530 118 mL

AR-2936 Lube Oil 0.87 8700 118 mL

AR-2835 Lube Oil 1.00 10000 118 mL

AR-2937 Lube Oil 1.5113 15113 118 mL

AR-2836 Lube Oil 2.00 20000 118 mL

AR-2938 Lube Oil 2.5162 25162 118 mL

AR-2839 Lube Oil 3.020 30200 118 mL

AR-2939 Lube Oil 3.500 35000 118 mL

AR-2837 Lube Oil 4.07 40700 118 mL

AR-2857 Lube Oil 5.010 50100 118 mL

AR-2858 High Sulfur Lube Oil 6.043 60430 118 mL

Code CRM Cl % Cl ppm UnitAR-2004 Chlorine in Paraffin Oil 0.0009 9 118 mL

AR-2005 Chlorine in Paraffin Oil 0.012 120 118 mL









30



Lube Oil CRMs / LubricantsCode CRM Cl % S % UnitAR-3501 Sulfur/Chlorine in Lube Oil 4.00 7.00 118 mL

AR-3502 Sulfur/Chlorine in Lube Oil 2.00 5.00 118 mL





AR-3507 Sulfur/Chlorine in Lube Oil <0.0001 <0.0001 118 mL

Code CRM Ash %

Base No

Ca % Mg % P % S % Zn % cSt/100 cSt/40 Unit

AR-6301 Engine Oil 0.05 2.42 <0.001 <0.001 <0.001 0.29 <0.001 12.25 119.20 118 mL

AR-6302 Engine Oil 0.22 2.83 0.0005 0.0005 0.103 0.22 0.122 12.56 124.87 118 mL

AR-6303 Engine Oil 0.83 5.42 0.009 0.105 0.084 0.40 0.101 11.44 102.70 118 mL

AR-6304 Engine Oil 0.81 6.27 0.058 0.087 0.095 0.56 0.119 12.81 73.51 118 mL

AR-6305 Engine Oil 0.78 7.07 0.168 0.052 0.126 0.57 0.155 11.52 98.74 118 mL

Code CRM S % S ppm UnitAR-3521 Low Sulfur Lube Oil <0.0001 <1 118 mL

AR-3522 Low Sulfur Lube Oil 0.0036 36 118 mL







Code CRM Ni ppm S % V ppm UnitAR-2901 Lube Oil 75 4.25 407 59 mL

AR-2902 Lube Oil 50 3.11 271 59 mL

AR-2903 Lube Oil 22 2.002 168 59 mL

AR-2904 Lube Oil 18.1 1.053 104.01 59 mL

AR-2905 Lube Oil 9.9 0.5263 50.2 59 mL

31







Residual Oil / BunkerCode CRM BTU/Ib C % H % Joule/g N % S % UnitIARM-HP21-10A

3% S CHN & BTU in Residual Fuel Oil

18300 86.0 10.6 42500 0.28 3.03 each

Code CRM S % UnitIARM-HP-11050C Residual Fuel Oil CRM-

0.50% S0.50 each

IARM-HP-11200D Residual Fuel Oil - 2.00% S 2.15 each

IARM-HP-11300C Residual Fuel Oil 3.% PRELIM

3.2 each

Code CRM As ppm Co ppm

Ni ppm S ppm Se ppm

V ppm Unit

NIST-1634C

Fuel oil - Trace ele-ments

0.1426 0.151 17.54 (2.0) 0.102 28.19 100 mL

Code CRM Hg ppm S % UnitNIST-1619B Residual fuel oil - Sulfur 0.00346 0.696 100 mL

NIST-1620C Residual fuel oil - Sulfur 4.561 100 mL

NIST-1621E Residual fuel oil - Sulfur 0.948 100 mL

NIST-1622E Residual fuel oil - Sulfur 2.1468 100 mL

NIST-2717A Residual fuel oil - Sulfur 2.9957 100 mL

Code CRM S % UnitAR-2891 Residual Fuel Oil 0.1065 118 mL

AR-2811 Residual Fuel Oil 0.1503 118 mL


















Code CRM S % UnitAR-3181 High Viscosity Residual Oil 0.292 118 mL

AR-3182 High Viscosity Residual Oil 0.9037 118 mL

32



Code CRM C % Cu ppm

Fe ppm

H % N % Na ppm

Ni ppm

S % Si ppm

gross-BTU

Unit

AR-1622 Ultimate Residual Oil

85.54 <1 16.4 12.37 0.16 (5) 4.6 2.08 (4) 18913 118 mL

Code CRM S % UnitAR-2859 High Sulfur Residual Oil 5.00 118 mL

AR-2861 High Sulfur Residual Oil 5.90 118 mL




Crude Oil Code CRM Hg ppm S % UnitNIST-2721 Crude oil (light-sour) - Sulfur

and mercury0.0417 1.5832 5 x 10

mL

NIST-2722 Crude oil (heavy-sweet) - Sulfur and mercury

0.1292 0.21037 5 x 10 mL

Code CRM S % S ppm UnitAR-2941 Stabilized Crude Oil 0.0102 102 118 mL

AR-2942 Stabilized Crude Oil 0.0205 205 118 mL


















Code CRM N ppm UnitAR-3032 Nitrogen in Crude Oil 67 118 mL

AR-3033 Nitrogen in Crude Oil 749 118 mL

AR-3034 Nitrogen in Crude Oil 1641 118 mL

33







Crude Oil Code CRM Cl

ppmCu ppm

Fe ppm

N ppm Na ppm

Ni ppm

S % Si ppm

V ppm

Unit

AR-2070 Wyoming Crude Oil

3.16 0.82 1.94 67.00 2.74 0.92 0.082 0.42 0.39 500 mL

AR-2071 North Sea Crude Oil

0.18 - 4.33 749.90 5.76 2.24 0.175 1.05 1.91 500 mL

AR-2072 Alaska Crude Oil

1.50 0.3 4.6 1780.00 2.6 16.9 1.15 1.3 43.6 500 mL

AR-2078 Vacuum Gas Oil

0.14 0.18 438.80 0.87 0.055 0.342 0.15 0.13 500 mL

Code CRM Cd ppm Cl ppm Cr ppm

Pb ppm

Unit

AR-3161 Waste Oil 2.10 506 5.07 49.8 59 mL

AR-3162 Waste Oil 5.1 1013 9.8 98.7 59 mL

AR-3163 Waste Oil 13.0 1898 20.7 210.2 59 mL

Waste Oil

Code CRM As ppm UnitAR-3171 Waste Oil 2.0 59 mL

AR-3172 Waste Oil 4.2 59 mL

AR-3173 Waste Oil 10.5 59 mL

CRMs with given C-H-N-compositionCode CRM BTU BTU/

IbC % Cu

ppmFe ppm

H % Joule/g N % Na ppm

Ni ppm

S % Si ppm

gross-BTU

Unit

IARM- HP14050RE

0.50% S in #2 Die-sel Fuel CRM

(85) 13.1 (0.1) 0.5 each

IARM-HP21-10A

3% S CHN & BTU in Residual Fuel Oil

86.0 10.6 42500 0.28 3.03 each

AR-000 Paraffin Oil

85.80 14.20 118 mL

AR-100 Residual Oil

88.8 10.1 0.19 0.93 100 mL

AR-150 Residual Oil

89.00 10.29 0.26 118 mL

AR-327 Kerosene 85.47 13.97 0.136 118 mL

AR-330 #2 Diesel Oil

87.05 13.08 0.034 118 mL

AR-1622 Ultimate Residual Oil

85.54 <1 16.4 12.37 0.16 (5) 4.6 2.08 (4) 18913 118 mL

NIST-1617B Kerosene - Sulfur

86.3 13.9 0.1250 100 mL

34



Code CRM S % UnitNIST-2720 Di-n-butyl sulfide - Sulfur (21.9) 5 x 4.5

mL

Other Petrochemical CRMs

Code CRM S % UnitAR-2851 Extreme Pressure Oil 2.00 118 mL

AR-2852 Extreme Pressure Oil 2.95 118 mL

AR-2853 Extreme Pressure Oil 4.19 118 mL

Code CRM N ppm S % UnitAR-2077 Vacuum Gas Oil 1267 0.45 118 mL

AR-3151 Nitrogen in Vacuum Gas Oil 1.05 118 mL




AR-3155 Nitrogen in Vacuum Gas Oil 49 118 mL



Code CRM %C10-C40 Ratio UnitBAM-K009 Lubricating oil (type

B) (ISO 9377-2, ISO 16703, EN 14039)

99.5 7 mL

BAM-K010F Diesel Fuel (type A)/Lubricating Oil (type B) (1:1) (ISO 9377-2, ISO 16703, EN 14039)

96.7 1.00003 1.5 mL

BAM-K011 Mineral oil calibration standard

1.471 4.5 mL

Code CRM SY124 UnitERM-EF317 Gas oil - Solvent Yellow

124 (SY124)0.141 20 mL

ERM-EF318 Gas oil - Solvent Yellow 124 (SY124)

7.0 20 mL

35




Reference Information Conversion Tables For Reference

Use these tables to find the information you need

Tubing I.D. & VolumesI.D. I.D. Vol. Vol. (in.) (mm.) (µL/in) (µL/cm)0.001 0.0254 0.0129 0.005

0.01 0.254 1.287 0.507

0.02 0.508 5.148 2.027

0.04 1.016 20.59 8.107

0.06 1.524 46.33 18.24

0.08 2.032 82.37 32.43

0.1 2.540 128.7 50.67

Weight ConversionPound Ounce Gram Kilogram (lb) (oz) (g) (kg)0.00220 0.0352 1.0 0.001

0.0625 1.0 28.38 0.0284

1.0 16 454 0.454

2.203 35.24 1000 1.0

Flow Rate ConversionL/min. L/sec. Gal./min. Gal./sec (gpm) (gps)3.785 0.0631 1.0 0.0167

227.1 3.785 60 1.0

1.0 0.0167 0.264 0.00440

60 1.0 15.85 0.264

Volume ConversionCC mL Liter Fl. Gallon (cm3) Oz. 1.0 1.0 0.001 0.0338 2.64E-04

10 10 0.01 0.338 0.00264

29.57 29.57 0.0296 1.0 0.00781

3785 3785 3.785 128 1.0

Pressure Conversionpsi bar Pa (N/m2) Torr atm1.45E-04 1.00E-05 1.0 0.00750 9.87E-06

0.0145 0.001 100 0.750 9.87E-04

0.0193 0.00133 133 1.0 0.00132

1.0 0.0689 6894 51.72 0.0680

10.0 0.689 68940 517 0.680

14.7 1.013 101,325 760 1.0

25.0 1.724 172,350 1293 1.701

50.0 3.447 344,700 2586 3.402

100 6.894 689,400 5172 6.805

Viscosity ConversionCentipoise Centistokes Examples (cp)* (cSt)1 1 water

16.5 20.635 lotion

40 43.2 veg. oil

88 110 latex paint

176 220 maple syrup

352 440 SAE 30 oil

*cp = cSt x (density in g/mL)

Dimension ConversionU.S.A. Metric U.S.A Fractional Decimal Inches Inches1/32 0.794mm 0.0313

n/a 1.00mm 0.0394

1/16 1.59mm 0.0625

1/8 3.18mm 0.125

1/4 6.35mm 0.250

5/16 7.94mm 0.313

3/8 9.53mm 0.375

n/a 10mm(1cm) 0.394

7/16 1.11cm 0.438

1/2 1.27cm 0.500

9/16 1.43cm 0.563

5/8 1.59cm 0.625

11/16 1.75cm 0.688

3/4 1.91cm 0.750

13/16 2.06cm 0.813

7/8 2.22cm 0.875

15/16 2.38cm 0.938

1 2.54cm 1.00

2 5.08cm 2.00

n/a 10.0cm 3.94

5 12.7cm 5.00

n/a 50.0cm 19.7

n/a 100cm(1m) 39.4

Aliq

uot V

olum

e

Dilution Table

Volumetric Size (mL)10 25 50 100 2501.0mL 2.5mL 5.0mL 10.0mL 25.0mL

100µL 250µL 500µL 1mL 2.5mL

(10µL) 25µL 50µL 100µL 250µL

* (2.5µL) (5µL) (10µL) 25µL

* * * * (2.5µL)

* * * * *Those shown with * or ( ) not recommended due to overly ambitious dilution factor and small aliquot.

1000 ppmstandardDesired Content:100ppm

10ppm

1ppm

100ppb

10ppb

1ppb

36


Consum

ablesReference

Information

DilutionDimensionFlow RatePressureTubing I.D. & VolumesViscosityVolumeWeight

Wea

r Met

als

Set f

or X

RF

(Par

t No:

VH

G-W

RM

TLSE

T-17

X50G

)A

gA

lB

aC

aC

dC

rC

uFe

KM

gM

nM

oN

aN

iP

PbSb

SiSn

TiV

ZnS

tand

ard

10

00

5000

00

300

200

500

040

100

200

100

400

5050

030

500

Sta

ndar

d 2

030

00

500

3050

00

00

100

010

040

1000

100

5020

400

070

0S

tand

ard

30

030

030

000

040

500

00

100

010

00

2040

030

030

200

5010

Sta

ndar

d 4

050

030

500

00

400

5050

050

300

2070

040

200

030

00

100

100

Sta

ndar

d 5

1010

050

00

200

020

00

300

00

300

1030

5050

00

400

300

Sta

ndar

d 6

2010

1500

1000

050

020

040

030

050

3050

010

00

010

040

00

012

50S

tand

ard

720

00

1000

700

5030

010

030

1250

100

040

00

1500

500

00

020

4050

Sta

ndar

d 8

300

2050

100

100

400

400

3010

2000

500

400

00

5040

200

020

00

Sta

ndar

d 9

500

1250

2000

300

200

100

015

0040

010

200

050

300

3040

00

500

0S

tand

ard

1010

050

0 1

020

200

500

030

010

00

400

030

2000

010

010

500

0S

tand

ard

1130

020

0030

1010

00

300

500

040

200

00

300

020

010

010

010

00S

tand

ard

1240

200

1030

040

00

020

070

020

500

1040

012

5010

030

00

200

3040

020

00S

tand

ard

1340

030

700

040

040

200

1010

030

0030

300

500

500

00

00

020

1500

Sta

ndar

d 14

500

00

1500

030

5040

030

00

100

200

040

050

020

00

300

1030

Sta

ndar

d15

040

010

040

0050

010

100

5020

00

030

020

050

00

030

400

00

Sta

ndar

d16

040

00

00

300

400

1000

200

2050

030

00

1050

010

030

00

Sta

ndar

d 17

00

00

00

00

00

00

00

00

00

00

00

Sta

ndar

ds n

ot a

vaila

ble

for i

ndiv

idua

l sal

e. S

ee s

et in

form

atio

n on

Pag

e 13

.

37


Notes


notes-pages.indd 1 11/9/2015 11:43:17 AM

Notes


notes-pages.indd 2 11/9/2015 11:43:17 AM


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