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AP 1001 Three Mile Island Nuclear Station SIDE 1

Figure 1001-8 Special Operating Prr,cedure SOP No. b(From SOP Log inc.s>

NOTE: in,truction. .no eviomano. in A P 1001 Aenu. o.e.....o on.n como. in. '. U Unit No.' ~

Date b ~I

1. Title^ I.

YhW^ fM ^ $* ".

2 Purpose onciuo.ou,oo e sor: J

\

3. Attach procedure to this form written according to the following format.

A. Limitations and Precautionsg ,p

1. Nuclear Safety2. Environmental Safety 6

,

3. Personnel Safety g(/ O g mg4. Equipment Protection,

fB. Prerequisites W 1

!.- -

C. Procedure

2bp4. Generated by Eb dC ("* / A.A Date'

'(45 P (t/ i #

% )5. D uration of S0 P - sn.n n. no ion.., en.n so a.,. eram in. .<t.cei o.t. ov in. som or (.> or to> o .. - .nsen. .c occur. 'ir.t.

(a) SOP will be cancelled by incorporation]-or new permanen

procedure submitted by / O-

(b) S0P is not valid af ter 0310[J.3cens in ci,eu,n.e.nc n en oni ,.. wit in soe p.ine c..c.ii.o

.

6. (a) is the procedure Nucimr Saf ety Related?

If ''yes", complete Nuclear Safety Evaluation. isio. 2 o, ini. So,m> YesO No O.. . ...

(b) Does the procedure af f ect Environmental Protection-ni. /g

.

Jrm . Yes O No OIf ''yes", complete Environmental Evaluation. < sio. 7 -. .._

(c) YesO NoC__

Does the procedure affect radiation exposure to perznnai . . . . ....

NOTE: if .si e n .r . ., . " no " en. cu. m y o. . g.ov.o ey e ri. s of t s u o.r w oor. If .ny av tion.

e. .oo,ov.o org'tn.gnit suc= rent.p.n7 ,n . . n. .o ~y ~

in. e n.ne. mv.,

7. Reviewand Aocroval / ,

k/ (Agpged - Shift Supervisor

ed#kn% eR$$jfdf "*"''"g$)::"');;f[A,,,{'|'f.',1QM.t 4Mo MR g y/ 6 ' g ' w ...

pproved Unit Superintendent / l'd < d r @ //c7//9 "''~ ~

r,.,

8. S0P is Cancelled 79091 o oogsnitt Sup.rv6.or/Snif t Foremen O.t.

~

TMl-63 R.v. S/77

-- __ - - . . _ .

~.. ..

SPECIAL OPERATING PROCEDURE

CHE!!ICAL & RADI0 CHEMICAL SAMPLING

AND ANALYSIS PROCEDURE FOR AIR

AND 'n'ATER SAMPLES

i-

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Prepared By: bD-E. D. Yochheim

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PROCEDURE FOR CHEMICAL & RADI0 CHEMICAL SAMPLING

AND ANALYSES OF AIR & WATER SAMPLES

General

1.0 All air and water samples for chemistry and radiochemistry analyses.

will be handled in accordance with this procedure.

2.0 Persons will be designated as sample coordinators, lab supervisors,

shift chemists, chem. techs, (HP foreman, HP techs), aux. operators,and drivers and will be assigned to a shift team with this as theirresponsibility. Where possible, these individuals should be consistentfrom sh'ift to shift.

Objective

1.0 This procedure is written to establish all efficient and workablemethod for sampling, analyses, data evaluation and distribution.

2.0 This procedure supercedes and replaces " Procedure for sampling air / water."Resoonsibilities

'

1.0 Sample coordinator

Determines details of analysis requesta.

b. Prepares sample tag

Establishes tentative priorityc.

d. Assess work load of labs (B & W, Unit I, Unit II) and Counting facilities(B & W, Met-Ed, SA1, RMC)

Determines f#nal priority and schedule (resolves conflicts with samplee.-

requestor).f. Directs execution of analysesg. Receives /repo ts data results

2.0 Lab Supervisor '-

- a. Schedules and directs chem. techs.b. Coordinates with HP

,

c. Reports chemistry results to sample coordinator3.0 Shift Chemist

Provides chemistry support (problem solutions) to the shif t superintendenta.,

sly Interfaces w th shift supervisor on chemistry / radiochemistry. problemsi

4.0 HP Fofeman

Schedules ar.d directs HP techs. in the collection of air samplesa.

b. Works in co3peration with Lab supervisor in the collection of watersamples cor.taining radionuclides.

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Page Two

5.0 Chem. Techs.

a. Obtain chemistry / radiochemistry samples

NOTE: Because of sample collection & analysis frequency, aux operatorsmay collect sump samples and deliver them directly to Lab Supervisor.Should this be the case, the sample coordinator will be notified bythe Lab Supervisor in order '. hat the standard format for obtainingresults and relaying them to the appropriate individual can bemaintained.

b. Performs chemical analyses

c. Logs results of chemical analyses, in lab notebook6.0 Driver.

a. Distribute radiochemistry and air samples to appropriate countingfacility per sample tag

b. Returns counted radiochemical samples to Unit I reactor buildinghatch area for archives.

c. Obtains results from counting labs on a 45 minute schedule and delivers -

xerox copies of them.to sample coordinator

d. Returns original copies of counting data to lab performing analyses.

7.0 HP Techs .

a. Collect air samples

b. Collect reactor building gas samples

c. Distribute above samples to appropriate counting facility per samplerequest tag.

d. Returns counted radiochemical samples to Unit I reactor building hatch

area for archives.8.0 Auxiliary Operator

a. Collects sump samples as required.-

b. Delivers samples to lab supervisor.. ,

Procedure

Note: Figure 1 diagrams the flow chart for collection of air, gas, andwater samples;

Figure 2 shows ar. example of the sample request tag

1.0 Water Samoles

1.1 Any individual requesting a sample will contact the sample coordinatorwith sufficient details of analyses wanted and priority of sample.

1.2 The sample coordinator will contact the lab supervisor as to the natureof the sample, he will also prepare a sample tag detailing prioritiesand analyses requested (see figure 2) .

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1.3 The lab supervisor will instruct a chem. tech. to obtain thesample under the cognizances of HP and appropriate RWP's if necessary.

1.4 The Chem. Tech. will obtain the sample

1.4.1 Chemistry analyses will be performed and logged in the lab notebook;results will be given to the lab supervisor for communication withthe sample coordinator.

1.4.2 Radiochemistry samples will be delivered to the appropriate countingfacility as per the sample request tag by the driver.

1.4.3 In certain instances, auxiliary operators wiii collect sump samplesfor analyses. In these instances, they will deliver the samplesto the laboratory supervisor for chemical and radiochemical analysis.At such time, the aux. op. or their supervisor must notify the samplecoordinator with the appropriate information analagous to the samplerequestor.

1.5 The counting facility will analyze the sample based on the prioriT;y assigned.1.5.1 If high/ urgent priority is assigned the labs will phone results to

the sample coordinator.

1.5.2 If other priority assigned, the labs will submit the data to thedriver who will xerox the results and submit the xerox copies to thesample coordinator. The driver will return the original data to theappropriate lab.

1.6 The driver will schedule his activities sc as to contact each of the countinglabs, and the sample coordinator on a cace/45 min. basis.

1.7 The sample coordinator will distribute the results to the requestor (andother cognizant individuals as necessary) on a timely basis.

1.8 Individuals who are not sample requestors but have need of the data collectedcan obtain the results through the sample coordinator.1.8.1 Shift supervisors, shift foreman and shift superintendents may-

obtain chemistry data directly from the shift chemist if desired.~

2.0 Air and Gas Samples.

2.1 Based or sample frequencies previously established and implemented

by HP, the HP foreman shall direct the HP techs. to collect air samples.2.2 The HP foreman on his designee must notify the sample coordinator

with pertinent sample collections and analysis information.2.3 The HP techs will distribute the samples to the appropriate lab per

instruction of the sample coordinator. The HP tech must also obtain

a sample request tag from the sampie coordinator prior to deliveringthe sample to the counting facility.

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Page Four

2.4 The HP techs will collect counted samples and distribute themto the Unit I reactor building hatch for archives.

2.5 Since reactor building gas samples for H2, N , and 02 analyses are2

performed by the HP techs, the techs should report the results tothe HP foreman. The HP foreman must contact the sample coordinatewith the results as soon as possible.

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_D31330

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Sample Request Tag,,= ,

..

Sampled Priority: Date:

Sample ID & Unit # Time:.

Reques t or : Ext #

Ehone Results To : Ext #be.

mpleted Type of sample: Air flow rateSampler

ordinator Liq.uid volume

Analysis Requested:

Scan Sample Sent To: Met-Ed: B & W:

SAI: RMC:

Cther :

Name of Collector Date & Time

Chemical Results

bempleted

Chempervisor

Signature : Date & Time

-

-

Scan Completed Results Iransmitted To~ bempleted Signature Date & Time

Lab

Attach results to this form and send to sample coordination center.

be Chem results received & transmitted To:spleted

Sample Results received & transmit ced To:O rd inator

Signature Date & Time

Rev. 0 4/8/79

OO1331i i

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