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Test of laminates Tests of Sandwich Construction Monitoring of Composite Construction Methods and standards for testing of composite materials Karel Doubrava Faculty of Mechanical Engineering, CTU in Prague January 11, 2016 1 / 32

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Page 1: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Methods and standards fortesting of composite materials

Karel Doubrava

Faculty of Mechanical Engineering, CTU in Prague

January 11, 2016

1 / 32

Page 2: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Contents1 Test of laminates

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

2 Tests of Sandwich ConstructionTensile propertiesCompressive propertiesshear

3 Monitoring of Composite ConstructionResistance strain gaugesOptical fiber – FBGDIC

2 / 32

Page 3: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Mechanical testing of fiber

ASTM D 3379

ASTM D 4018

Fiber properties from test of UD laminate

Property (100%) =Property× 100

Vf3 / 32

Page 4: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Mechanical properties test of matrix

Tension ASTM D 638Ftu

m, Ftym, Et

m, ν tm, εtu

m

CompressionASTM D 695Fcu

m , Fcym , Ec

m, νcm, εcu

m

Shear ASTM E 143,ASTM D 5379Fsu

m , Fsym , Gs

m

4 / 32

Page 5: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Mechanical testing of lamina andlaminate

Tension ASTM D 3039Compression ASTM D 3410, ASTM D 695Shear ASTM D 3518, ASTM D 5379, . . .Interlaminar shear ASTM D 2344

5 / 32

Page 6: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Tension properties ASTM D 3039

Tensile strengthF tu = Pmax/ATensile chord modulusof elasticityE1 =

σb1−σa

1εb

1−εa1,

a. . . 0.1%, b. . . 0.3%Poisson ratio ν = −∆ε2

∆ε1

6 / 32

Page 7: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Tensile Test Failure Code/ TypicalMode ASTM D 3039

Type Code Area Code Location Code

Angled A Inside grip I Bottom B

edge Delam. D At grip A Top T

Grip/tab G < 1W from grip W Left L

Lateral L Gage G Right R

Multi–mode M Multiple areas M Middle M

long.–Splitting S Various V Various V

eXplosive X Unknown U Unknown U

Other O

7 / 32

Page 8: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Compression in–plane tests

ASTM D 695 (SACMA SRM-1)ASTM D 3410 ( Celanese, IITRI)ASTM D 5467

8 / 32

Page 9: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Compression properties ASTM D 695

Compressive strengthF cu = Pmax/ACompressive modulusof elasticityE1 = ∆σ

∆ε

9 / 32

Page 10: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Compression ASTM D 3410

Procedure A – Celanese Procedure B – IITRI

http://www.wyomingtestfixtures.com

10 / 32

Page 11: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Failure Code ASTM D 3410Type Code Area Code Location Code

Angled A Inside grip I Bottom B

Brooming B At grip A Top T

end–Crushing C Gage G Left L

Delamination D Multiple areas M Right R

Euler bucling E Tab adhesive T Middle M

tHrough–thickness H Various V Various V

Kink bands K Unknown U Unknown U

Lateral L

Multi–mode M

long.–Splitting S

Transverse shear T

eXplosive X

Other O

11 / 32

Page 12: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Compression ASTM D 5467

4PB of sandwichbeam

F cu =Pmaxlm

(a−y+

hf2

)2w[hf (a−y)2+ Eo

Efhoy2

]E1 =

σb1−σa

1εb

1−εa1,

a. . . 0.1%, b. . . 0.3

12 / 32

Page 13: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Failure Code ASTM D 5467

Type Code Area Code Location Code

Skin to core Delamination D At load cylinder A Left L

Filament fracture F Gage G Right R

tHrough–thickness H Multiple areas M Middle M

Layer instability L Outside gage U Various V

local Wrinkling W Various V Unknown U

Multi–mode M L Unknown U

core Crushing C

long.–Splitting S

Transverse shear T

eXplosive X

Other O

13 / 32

Page 14: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear in–plane tests

±45 tensile shear testRail Shear MethodV–Notched Beam MethodTube torsion test

14 / 32

Page 15: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

±45 tensile shear test

BS EN ISO 14,129, ASTM D 3518Ply < 0.125 mm, 16 plies

σ11 = σxx2 + τxy , σ22 = σxx

2 − τxy , τ12 = ±τxy ,ε11 = ε22 =

εxx +εyy

2 , γ12 = εxx − εyy

G12 = σxx2(εxx−εyy ) =

τb12−τa

12γb

12−γa12

, S12 = Pmax2bh

15 / 32

Page 16: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Two-rail shear test ASTM D 4255

http://www.wyomingtestfixtures.com

Sxy = Pmax

Lh , G12 =∆τxy

∆γxy= ∆P

2Lh∆ε45

16 / 32

Page 17: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Three-rail shear test ASTM D 4255

http://www.wyomingtestfixtures.com

Sxy = Pmax

Lh , G12 =∆τxy

∆γxy= ∆P

4Lh∆ε45

17 / 32

Page 18: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear V-Not. Beam ASTM D 5379

F u = Pmaxwh ,

τi = Piwh ,

γ = |ε45|+|ε−45|G = ∆τ

∆γ ,

18 / 32

Page 19: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear V-Not. Beam ASTM D 5379

19 / 32

Page 20: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear V-Not. Rail ASTM D 7078

F u = Pmaxwh , τi = Pi

wh , γ = |ε45|+ |ε−45| G = ∆τ∆γ

20 / 32

Page 21: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear V-Not. Rail ASTM D 7078

21 / 32

Page 22: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Tube torsion test ASTM D 5448

τxy = 2TRoπ(R4

o−R4i)

G12 =∆τxy

∆γxy=

∆τxy

∆(ε45−ε−45)

22 / 32

Page 23: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Mechanical testing of fiberMechanical properties test of matrixMechanical testing of lamina

Shear of Short-Beam ASTM D 2344

F sbs = 0.75× Pmaxb×h

23 / 32

Page 24: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Tensile propertiesCompressive properties

shear

Sandwich Construction

Tensile properties ASTM C 297Compression ASTM C 364, ASTM C 365,ASTM D 7336Shear ASTM C 273, ASTM C 393Bending ASTM D 7249, ASTM D 6457

24 / 32

Page 25: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Tensile propertiesCompressive properties

shear

Tensile properties ASTM C 297

F ftuz = Pmax

A

Min. Cell Size Max. Cell Size Min Facing Area(mm) (mm) (mm2)

- 3 625

3 6 2500

6 9 5625

25 / 32

Page 26: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Tensile propertiesCompressive properties

shear

Compr. Edgewise ASTM C 364

Failure Type Code Area Code Location Code

Facesheet compression F At end A Top T

facesheet delam. Buckling B Gage G Bottom B

honeycomb facesheet Dimpling D Various V Middle M

core Compression C Unknown U Various V

core Shear S Unknown U

Multi mode M

overal Panel buckling P

eXplosive X

Other O 26 / 32

Page 27: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Tensile propertiesCompressive properties

shear

Flatwise Compr. ASTM C 365

Min. Cell Size Max. Cell Size Min Facing Area(mm) (mm) (mm2)

- 3 625

3 6 2500

6 9 5625

F fcuz = Pmax

A

E fcz = (P0.003−P0.001)·t

(δ0.003−δ0.001)·A

27 / 32

Page 28: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Tensile propertiesCompressive properties

shear

Shear of Core ASTM C 273

τ = PLb , γ = u

t ,G = (∆P/∆u)t

Lb

Failure Type Code Area Code Location Code

core Shear S At end A Top T

Interface failure I Gage G Bottom B

eXplosive X one Corner C Middle M

Other O Various V Entire length E

Unknown U Various V

Unknown U

28 / 32

Page 29: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Resistance strain gaugesOptical fiber – FBGDIC

Resistance strain gauges

Grid sizeSelf-heating P = U · I = U2

R R = 350Ω

Temperature compensation – half bridgeSurface preparing2 components adhesive

29 / 32

Page 30: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Resistance strain gaugesOptical fiber – FBGDIC

Fiber Bragg Grating (FBG) Sensors

∆λλ0

= (1− pe) · ε(αLamda + αn) ·∆Thttp://www.ni.com

30 / 32

Page 31: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Resistance strain gaugesOptical fiber – FBGDIC

DIC

http://www.dantecdynamics.com/

31 / 32

Page 32: Methods and standards for testing of composite materialsdrone.fsid.cvut.cz/mcmfolder/doubrava_MKM2016.pdf · Mechanical testing of lamina 45 tensile shear test BS EN ISO 14,129,ASTM

Test of laminatesTests of Sandwich Construction

Monitoring of Composite Construction

Resistance strain gaugesOptical fiber – FBGDIC

References

Mallick, P. K.: Composites Engineering Handbook, CRC Press, 1997, ISBN0824793048

Hodgkinson, J.M.:Mechanical testing of advenced fibre composites, WoodheadPublishing 2000, ISBN 1855733129

Carlsson, L.A., Adams, D.F., Pipes, R.B.:Experimental Characterization ofAdvanced Composite Materials, Third Edition, CRC Press, 2002 ,ISBN1587161001

COMPOSITE MATERIALS HANDBOOK – VOLUME 1Polymer MatrixComposites, Guidelines for Characterization of Structural MaterialsMIL-HDBK-17, US Army Research Laboratory, 2002, Fort Belvoir

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