mehl quarter 2, 2016 surface water monitoring report ... · swd6* surface water run-off : 316068 ....
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02) June 2016
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Report Issue Form
IF-11B Revision: 02 (21st July 2011)
Client Name: MEHL
Client Address: Hollywood Great, Nag’s Head, Naul, Co. Dublin
Report Title: Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Project Code: MU0121
Project Manager (Name): Kerstie Flanagan
Project Manager (Sign):
Project Manager (Date): 21st June 2016
Approved by Project Director (Name): Conor Tonra
Approved by Project Director (Sign):
Approved by Project Director (Date): 21st June 2016
Issue No. Date Status
01 21/06/2016 Final version; issue to Client and EPA (EDEN)
Notes/Comments:
Patel Tonra Ltd., Environmental Solutions, 3f, Fingal Bay Business Park, Balbriggan, Co Dublin Tel: 01 8020520 Fax: 01 8020525 www.pateltonra.com
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Contents
Executive Summary ................................................................................... 1 1.0 Introduction ................................................................................... 2 2.0 Results .......................................................................................... 4 3.0 Discussion ..................................................................................... 7 4.0 Conclusion ..................................................................................... 8
Appendices Appendix 1: Calibration Records Appendix 2: Field Monitoring Records Appendix 3: Chain of Custody Form Appendix 4: Laboratory Results Figures Figure 1: Monitoring Locations
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Executive Summary
- 1 -
Executive Summary
1. Murphy Environmental Hollywood Ltd. (MEHL) holds an EPA Waste Licence (W0129-02) for the operation of an inert landfill at Hollywood Great, Nag’s Head, Naul, Co. Dublin.
2. Sampling of surface water (bi-annual and annual monitoring) was carried out by
Patel Tonra Ltd. at Hollywood inert landfill on the 27th April 2016 (Quarter 2, 2016) as required under Waste Licence W0129-02.
3. Results were compared against relevant legislative or guideline limit values, and
trigger levels specific to the site, where relevant. 4. EPA licence W0129-02 (Schedule B) specifies an Emission Limit Value (ELV) for
suspended solids emissions to surface water of 35mg/l. The ELV for suspended solids was exceeded in SW-2.
5. The level of suspended solids at SW-2 is concluded to be unrelated to the
operation of the MEHL facility. It is anticipated that elevated levels of suspended solids are associated with silt/run-off from stream bed/banks, and/or adjacent agricultural activities.
6. Suspended solids levels will be reported to the Agency as an incident, in line with
standard reporting requirements. 7. Repeat monitoring will be completed, in line with the surface water monitoring
schedule under EPA licence W0129-02.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
1
- 2 -
1.0 Introduction
1.1 Background 1.1.1 Murphy Environmental Hollywood Ltd. (MEHL) operates a landfill for inert waste at
its site at Hollywood Great, Nag’s Head, Naul, Co. Dublin. The site is a former shale and limestone quarry. Restoring the site will serve to return it in line with pre-quarrying conditions and integrate it into the surrounding landscape.
1.1.2 The landfill facility is licensed by the Environmental Protection Agency (EPA) and
operates under Waste Licence W0129-02. The licensee (Murphy Environmental Hollywood Ltd) manages and operates the facility to ensure that the activities do not cause environmental pollution.
1.1.3 MEHL is required to carry out monitoring of groundwater, surface water and
leachate in accordance with Schedule D of Waste Licence W0129-02 (or as may be amended by the EPA). This report details the surface water sampling methodology, laboratory results and a discussion of results for Quarter 2, 2016.
1.1.4 Sampling of surface water (bi-annual and annual monitoring) was carried out by
Patel Tonra Ltd. at Hollywood Landfill on the 27th April 2016 (Quarter 2, 2016) as required under Waste Licence W0129-02.
1.2 Monitoring Locations 1.2.1 Surface water monitoring locations (as specified in Waste Licence W0129-02, or as
may be amended) are listed in Table 1.1 (see Figure 1). Table 1.1: Location of Surface Water Monitoring Points Ref Location Easting Northing
SW1 Clonany Bridge (North (upstream) of site, ca. 280m) 315677 258518
SW2 Joinery Bridge (East (downstream) of site, ca. 1630m) 317230 257820
SWD1 Discharge after flowing through silt trap/oil interceptor 315660 258522
SWD2* Surface water run-off 315847 258415
SWD3* Water discharge from settlement pond 315937 258366
SWD4* Surface water run-off 315999 258306
SWD5* Surface water run-off 316139 258267
SWD6* Surface water run-off 316068 257856
SWD7* Surface water run-off 315779 257719
* SWD2 to SWD7 were previously surface water discharge points from surface water pumping associated with quarrying operations. The water pumping activities have been suspended; therefore any water/flow now observed at these locations is sourced from surface water run-off from non-landfill areas. The norm is that these locations are dry; however this is verified during each surface water sampling event.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
1
- 3 -
1.3 Sampling and Analysis Sampling Personnel
1.3.1 Sampling was carried out by Niall Durham (BSc(Hons), MSc) and Luke Martin (BA(Hons), MSc) of Patel Tonra Ltd on the 27th April 2016 under the instruction of MEHL.
Sampling Methodology
1.3.2 Surface water was sampled via a ‘grab’ sample. 1.3.3 Conductivity, pH and temperature were measured in situ. Calibration records
relating to meters are included as Appendix 1. Records of odour and visual inspection of samples were also maintained. The sampling sheet for data collected in the field is included as Appendix 2.
1.3.4 Appropriate bottles/containers were used (included preservatives, as appropriate),
in accordance with laboratory requirements. All samples were appropriately stored according to standard sampling techniques before being transported to the laboratory. Chain of Custody documentation is included as Appendix 3.
Laboratory Details
1.3.5 Analysis of water samples was conducted by Jones Environmental Laboratory. Jones Environmental Laboratory is UKAS and MCERTS accredited. Certified laboratory results are included as Appendix 4.
Interpretation of Results
1.3.6 Interpretative reports have been prepared and reviewed in accordance with Patel Tonra Ltd. quality control procedures.
1.3.7 Surface water results were examined with reference to:
European Communities Environmental Objectives (Surface Water) Regulations 2009, SI 272 of 2009 – referred to as the ‘Surface Water Regulations 2009’
European Communities (Quality of Salmonid Waters) Regulations, SI 293 of 1988 – referred to as the ‘Salmonid Water Regulations’
1.3.8 EPA Parameters of Water Quality – Interpretation and Standards (2001) was referenced throughout the interpretation (however it was noted that additional/amended legislation may now be in force). Where results exceeded limits prescribed in legislation or trigger levels, this is highlighted in the report and possible causes described.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
2
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2.0 Results
2.1 Surface Water 2.1.1 The results of the surface water analysis for Quarter 2, 2016 are outlined in
following tables. Surface water results were examined with reference to:
European Communities Environmental Objectives (Surface Water) Regulations 2009, SI 272 of 2009 – referred to as the ‘Surface Water Regulations 2009’
European Communities (Quality of Salmonid Waters) Regulations, SI 293 of 1988 – referred to as the ‘Salmonid Water Regulations’
2.1.2 SWD-2, SWD-3, SWD-4, SWD-5 and SWD-7 were dry at the time of sampling. SWD-6 was very overgrown with pondweed and it was not possible to obtain sufficient sampling volume.
Table 2.1: Surface Water Monitoring Results for SW-1 (upstream)
SW-1
Units Surface
Water Regs 2009
Salmonid Water
Regulations
Q2, 2016
Q4, 2015
Q2, 2015
Q4, 2014
Alkalinity, Total mg/l N/A N/A 224 N/A 212 N/A
Ammoniacal Nitrogen
mg/l NH4-N N/A 0.7 0.28 0.61 0.10 0.03
Calcium mg/l N/A N/A 110.3 N/A 96.6 N/A
Chemical Oxygen Demand mg/l N/A N/A 7 25 9 15
Chloride mg/l N/A N/A 29.9 31.5 28.5 36.4
Conductivity mS/cm N/A N/A 0.68 0.62 0.56 0.67
Dissolved Oxygen mg/l N/A >9 7 11 10 10
Magnesium mg/l N/A N/A 14.0 N/A 10.9 N/A
Manganese mg/l N/A N/A 2.274 N/A 0.161 N/A
Orthophosphate mg/l N/A N/A 0.07 N/A <0.06 N/A
pH pH 4.5-9.0 6 – 9 7.7 7.1 8.0 8.0
Phosphorus, Total mg/l N/A N/A 0.116 N/A 0.048 N/A
Sodium mg/l N/A N/A 17.2 N/A 19.6 N/A
Sulphate mg/l N/A N/A 85.31 N/A 91.24 N/A
Suspended Solids, Total mg/l N/A 351 <10 <10 <10 <10
Temperature oC N/A ≤21.5 9.1 9.1 11.3 8.2
N/A = no limit value applies; or not required to be analysed during a given quarter.
1 The Emission Limit Value (Schedule B, EPA licence W0129-02) for suspended solids is 35mg/l.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
2
- 5 -
Table 2.2: Surface Water Monitoring Results for SW-2 (downstream)
SW–2
Units Surface Water Regs
2009
Salmonid Water
Regulations
Q2, 2016
Q4, 2015
Q2, 2015
Q4, 2014
Alkalinity, Total mg/l N/A N/A 208 N/A 220 N/A
Ammoniacal Nitrogen
mg/l NH4-N N/A 0.7 0.03 0.05 0.03 0.03
Calcium mg/l N/A N/A 144.6 N/A 141.3 N/A
Chemical Oxygen Demand mg/l N/A N/A 11 19 <7 <7
Chloride mg/l N/A N/A 31.2 32.8 28.9 32.7
Conductivity mS/cm N/A N/A 0.86 0.76 0.74 0.80
Dissolved Oxygen mg/l N/A >9 11 10 10 11
Magnesium mg/l N/A N/A 11.2 N/A 12.6 N/A
Manganese mg/l N/A N/A <0.002 N/A 0.002 N/A
Orthophosphate mg/l N/A N/A 0.1 N/A <0.06 N/A
pH pH 4.5-9.0 6 – 9 8.3 7.2 8.4 8.4
Phosphorus, Total mg/l N/A N/A 0.106 N/A 0.108 N/A
Sodium mg/l N/A N/A 16.3 N/A 16.3 N/A
Sulphate mg/l N/A N/A 173.67 N/A 169.99 N/A
Suspended Solids, Total mg/l N/A 352 41 34 57 125
Temperature oC N/A ≤21.5 7.6 8.9 11.8 9.2
N/A = no limit value applies; or not required to be analysed during a given quarter.
2 The Emission Limit Value (Schedule B, EPA licence W0129-02) for suspended solids is 35mg/l.
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EPA Export 23-08-2016:01:37:46
MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
2
- 6 -
Table 2.3: Surface Water Monitoring Results for SWD-1
SWD–1
Units Surface Water Regs
2009
Salmonid Water
Regulations
Q2, 2016
Q4, 2015
Q2, 2015
Q4, 2014
Alkalinity, Total mg/l N/A N/A 200 N/A 198 N/A
Ammoniacal Nitrogen
mg/l NH4-N N/A 0.7 0.03 0.09 0.08 0.06
Calcium mg/l N/A N/A 101.6 N/A 97.7 N/A
Chemical Oxygen Demand mg/l N/A N/A 13 22 14 82
Chloride mg/l N/A N/A 33.8 31.7 28.5 36.4
Conductivity mS/cm N/A N/A 0.68 0.68 0.60 0.67
Dissolved Oxygen mg/l N/A >9 11 10 10 9
Magnesium mg/l N/A N/A 12.1 N/A 10.8 N/A
Manganese mg/l N/A N/A 0.523 N/A 0.158 N/A
Orthophosphate mg/l N/A N/A 0.1 N/A <0.06 N/A
pH pH 4.5-9.0 6 – 9 8.0 7.0 8.1 8.0
Phosphorus, Total mg/l N/A N/A 0.55 N/A 0.04 N/A
Sodium mg/l N/A N/A 21.1 N/A 19.5 N/A
Sulphate mg/l N/A N/A 91.17 N/A 92.57 N/A
Suspended Solids, Total mg/l N/A 353 <10 <10 <10 20
Temperature oC N/A ≤21.5 7.7 9.4 9.7 8.2
3 The Emission Limit Value (Schedule B, EPA licence W0129-02) for suspended solids is 35mg/l.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
3
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3.0 Discussion
3.1 Limit Values 3.1.1 Surface water results were examined with reference to:
European Communities Environmental Objectives (Surface Water) Regulations 2009, SI 272 of 2009 – referred to as the ‘Surface Water Regulations 2009’
European Communities (Quality of Salmonid Waters) Regulations, SI 293 of 1988 – referred to as the ‘Salmonid Water Regulations’
3.1.2 EPA licence W0129-02 (Schedule B) specifies an Emission Limit Value (ELV) for suspended solids emissions to surface water of 35mg/l. The ELV for suspended solids was exceeded in SW-2.
3.2 Incidents Suspended Solids
3.2.1 Suspended Solids Emission Limit Value (ELV) specified under EPA licence W0129-02 was breached in SW-2 (41 mg/l). This exceeds the historic average of 25mg/l at this location.
3.2.2 SW-2 is located ca. 1.1km downstream of the MEHL facility, and is directly adjacent to agricultural land (horses) and an adjacent commercial/industrial unit. It is very unlikely that the MEHL facility would have an impact at this monitoring location, on the basis of the distances involved. Furthermore, the only emission to the stream from the MEHL facility on the day of sampling was SWD-1. The level of suspended solids in SWD-1 was <10mg/l.
3.2.3 The level of suspended solids at SW-2 is therefore concluded to be unrelated to
the operation of the MEHL facility. It is anticipated that elevated levels of suspended solids are associated with silt/run-off from stream bed/banks, and/or adjacent agricultural activities.
3.2.4 Suspended solids levels will be reported to the Agency as an incident, in line with
standard reporting requirements. 3.2.5 Repeat monitoring will be completed, in line with the surface water monitoring
schedule under EPA licence W0129-02.
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EPA Export 23-08-2016:01:37:46
MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Chapter
4
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4.0 Conclusion
4.1 Conclusion 4.1.1 Surface water monitoring at Hollywood Landfill (W0129-02) for Quarter 2, 2016
exhibited results which were generally in conformance with relevant legislative quality standards.
4.1.2 EPA licence W0129-02 (Schedule B) specifies an Emission Limit Value (ELV) for
suspended solids emissions to surface water of 35mg/l. The ELV for suspended solids was exceeded in SW-2.
4.1.3 The level of suspended solids at SW-2 are concluded to be unrelated to the
operation of the MEHL facility. It is anticipated that elevated levels of suspended solids are associated with silt/run-off from stream bed/banks, and/or adjacent agricultural activities.
4.1.4 Suspended solids levels will be reported to the Agency as an incident, in line with
standard reporting requirements. 4.1.5 Repeat monitoring will be completed, in line with the surface water monitoring
schedule under EPA licence W0129-02.
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Appendix
1
Appendix 1: Calibration Records
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EPA Export 23-08-2016:01:37:46
MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Appendix
2
Appendix 2: Field Monitoring Records
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Sampling Sheet for Surface Water Samples
Q2, 2016
Client: MEHL Site: Hollywood
Project No.: MU0121
Date: 27/04/2016 Time: 9.30am Consultant: ND/LM
Page 1 of 2
Monitoring
Point
Temp.
(oC)
pH Cond (µS/cm)
Odour Visual/
Other Comments
SW-1 9.1 7.7 680 None Clear
SW-2 7.7 8.0 680 None Clear
SWD-1 7.6 8.3 860 None Clear
SWD-2 Dry
SWD-3 Dry
SWD-4 Dry
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Sampling Sheet for Surface Water Samples
Q2, 2016
Client: MEHL Site: Hollywood
Project No.: MU0121
Date: 27/04/2016 Time: 9.30am Consultant: ND/LM
Page 2 of 2
Monitoring
Point
Temp.
(oC)
pH Cond (µS/cm)
Odour Visual/
Other Comments
SWD-5 Dry
SWD-6 Dry
SWD-7 Dry
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Appendix
3
Appendix 3: Chain of Custody Form
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Appendix
4
Appendix 4: Laboratory Results
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EPA Export 23-08-2016:01:37:46
Unit 3 Deeside Point
Zone 3
Deeside Industrial Park
Deeside
Patel Tonra Ltd
Attention :
Date :
Your reference :
Our reference :
Location :
Date samples received :
Status :
Issue : 1
Jones Environmental Laboratory
CH5 2UA
Tel: +44 (0) 1244 833780
Fax: +44 (0) 1244 833781
Kerstie Flanagan
3F Fingal Bay Business Park
Balbriggan
Co Dublin
Ireland
Registered Address : Unit 3 Deeside Point, Zone 3, Deeside Industrial Park, Deeside, CH5 2UA. UK
Twelve samples were received for analysis on 28th April, 2016 of which twelve were scheduled for analysis. Please find attached our Test Report
which should be read with notes at the end of the report and should include all sections if reproduced. Interpretations and opinions are outside the
scope of any accreditation, and all results relate only to samples supplied.
All analysis is carried out on as received samples and reported on a dry weight basis unless stated otherwise. Results are not surrogate corrected.
Bruce Leslie
Project Co-ordinator
10th May, 2016
MU0121
Hollywood
28th April, 2016
Final report
Compiled By:
Test Report 16/8230 Batch 1
QF-PM 3.1.1 v16Please include all sections of this report if it is reproduced
All solid results are expressed on a dry weight basis unless stated otherwise. 1 of 6
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Client Name: Report : Liquid
Reference:
Location:
Contact: Liquids/products: V=40ml vial, G=glass bottle, P=plastic bottle
JE Job No.: 16/8230 H=H2SO4, Z=ZnAc, N=NaOH, HN=HN03
J E Sample No. 1-3 4-6 7-9 10-12 13-15 16-18 19-21 22-24 25-27 28-29
Sample ID BH-5 BH-6 BH-8A BH-9 BH-10A BH-11A BH-12 BH-13 BH-14 SW1
Depth 14.53 8.54 28.07 20.35 35.37 1.34 44.24 32.82 24.62
COC No / misc
Containers H P G H P G H P G H P G H P G H P G H P G H P G H P G H P
Sample Date 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016 27/04/2016
Sample Type Ground Water Ground Water Ground Water Ground Water Ground Water Ground Water Ground Water Ground Water Ground Water Surface Water
Batch Number 1 1 1 1 1 1 1 1 1 1
Date of Receipt 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016 28/04/2016
Dissolved Arsenic # <2.5 <2.5 <2.5 <2.5 <2.5 25.2 <2.5 <2.5 <2.5 - <2.5 ug/l TM30/PM14
Dissolved Barium # 18 57 9 3 12 17 14 7 44 - <3 ug/l TM30/PM14
Dissolved Calcium # 55.1 100.0 107.3 107.6 132.4 98.6 22.1 42.4 24.0 110.3 <0.2 mg/l TM30/PM14
Total Dissolved Iron # <20 <20 <20 <20 <20 <20 <20 <20 <20 - <20 ug/l TM30/PM14
Dissolved Magnesium # - - - - - - - - - 14.0 <0.1 mg/l TM30/PM14
Dissolved Manganese # 79 265 <2 17 <2 396 <2 <2 19 2274 <2 ug/l TM30/PM14
Dissolved Potassium # 1.6 6.3 2.2 0.7 2.5 2.0 3.1 2.4 5.0 - <0.1 mg/l TM30/PM14
Dissolved Sodium # 51.4 19.0 11.2 16.1 26.2 16.1 3.4 19.1 9.6 17.2 <0.1 mg/l TM30/PM14
Total Phosphorus - - - - - - - - - 116 <5 ug/l TM30/PM14
Phenol # <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 - <0.01 mg/l TM26/PM0
Sulphate # 47.98 33.81 15.50 66.45 221.90 13.31 4.04 10.94 16.90 85.31 <0.05 mg/l TM38/PM0
Chloride # 15.4 20.3 33.1 28.2 50.2 22.8 2.2 42.6 27.9 29.9 <0.3 mg/l TM38/PM0
Ortho Phosphate as PO4 # - - - - - - - - - 0.07 <0.06 mg/l TM38/PM0
Total Oxidised Nitrogen as N # 0.4 <0.2 11.8 <0.2 0.3 <0.2 1.5 13.7 6.5 - <0.2 mg/l TM38/PM0
Ammoniacal Nitrogen as N # 0.03 0.30 0.03 0.12 <0.03 0.23 0.03 0.03 0.05 0.28 <0.03 mg/l TM38/PM0
Total Alkalinity as CaCO3 # - - - - - - - - - 224 <1 mg/l TM75/PM0
COD (Settled) # - - - - - - - - - 7 <7 mg/l TM57/PM0
Dissolved Oxygen 7 3 7 4 8 4 7 10 7 10 <1 mg/l TM59/PM0
Total Organic Carbon # <2 <2 <2 <2 <2 <2 5 <2 6 - <2 mg/l TM60/PM0
Total Suspended Solids # - - - - - - - - - <10 <10 mg/l TM37/PM0
Hollywood
Kerstie Flanagan
Please see attached notes for all
abbreviations and acronyms
LOD/LOR UnitsMethod
No.
Jones Environmental Laboratory
Patel Tonra Ltd
MU0121
QF-PM 3.1.2 v11Please include all sections of this report if it is reproduced
All solid results are expressed on a dry weight basis unless stated otherwise. 2 of 6
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Client Name: Report : Liquid
Reference:
Location:
Contact: Liquids/products: V=40ml vial, G=glass bottle, P=plastic bottle
JE Job No.: 16/8230 H=H2SO4, Z=ZnAc, N=NaOH, HN=HN03
J E Sample No. 30-31 32-33
Sample ID SWD1 SW2
Depth
COC No / misc
Containers H P H P
Sample Date 27/04/2016 27/04/2016
Sample Type Surface Water Surface Water
Batch Number 1 1
Date of Receipt 28/04/2016 28/04/2016
Dissolved Arsenic # - - <2.5 ug/l TM30/PM14
Dissolved Barium # - - <3 ug/l TM30/PM14
Dissolved Calcium # 101.8 144.6 <0.2 mg/l TM30/PM14
Total Dissolved Iron # - - <20 ug/l TM30/PM14
Dissolved Magnesium # 12.1 11.9 <0.1 mg/l TM30/PM14
Dissolved Manganese # 523 <2 <2 ug/l TM30/PM14
Dissolved Potassium # - - <0.1 mg/l TM30/PM14
Dissolved Sodium # 21.1 16.3 <0.1 mg/l TM30/PM14
Total Phosphorus 55 106 <5 ug/l TM30/PM14
Phenol # - - <0.01 mg/l TM26/PM0
Sulphate # 91.17 173.67 <0.05 mg/l TM38/PM0
Chloride # 33.8 31.2 <0.3 mg/l TM38/PM0
Ortho Phosphate as PO4 # 0.10 0.10 <0.06 mg/l TM38/PM0
Total Oxidised Nitrogen as N # - - <0.2 mg/l TM38/PM0
Ammoniacal Nitrogen as N # 0.12 0.03 <0.03 mg/l TM38/PM0
Total Alkalinity as CaCO3 # 200 208 <1 mg/l TM75/PM0
COD (Settled) # 13 11 <7 mg/l TM57/PM0
Dissolved Oxygen 11 11 <1 mg/l TM59/PM0
Total Organic Carbon # - - <2 mg/l TM60/PM0
Total Suspended Solids # <10 41 <10 mg/l TM37/PM0
LOD/LOR UnitsMethod
No.
Jones Environmental Laboratory
Patel Tonra Ltd
MU0121
Hollywood
Kerstie Flanagan
Please see attached notes for all
abbreviations and acronyms
QF-PM 3.1.2 v11Please include all sections of this report if it is reproduced
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JE Job No.:
SOILS
DEVIATING SAMPLES
SURROGATES
DILUTIONS
NOTE
% Asbestos in Asbestos Containing Materials (ACMs) is determined by reference to HSG 264 The Survey Guide - Appendix 2 : ACMs in buildings
listed in order of ease of fibre release.
All analysis is reported on a dry weight basis unless stated otherwise. Results are not surrogate corrected. Samples are dried at 35°C ±5°C unless
otherwise stated. Moisture content for CEN Leachate tests are dried at 105°C ±5°C.
Where Mineral Oil or Fats, Oils and Grease is quoted, this refers to Total Aliphatics C10-C40.
Please note we are not a UK Drinking Water Inspectorate (DWI) Approved Laboratory .
Samples must be received in a condition appropriate to the requested analyses. All samples should be submitted to the laboratory in suitable
containers with sufficient ice packs to sustain an appropriate temperature for the requested analysis. If this is not the case you will be informed and
any test results that may be compromised highlighted on your deviating samples report.
NOTES TO ACCOMPANY ALL SCHEDULES AND REPORTS
Please note we are only MCERTS accredited (UK soils only) for sand, loam and clay and any other matrix is outside our scope of accreditation.
Where Mineral Oil or Fats, Oils and Grease is quoted, this refers to Total Aliphatics C10-C40.
16/8230
WATERS
Data is only reported if the laboratory is confident that the data is a true reflection of the samples analysed. Data is only reported as accredited when
all the requirements of our Quality System have been met. In certain circumstances where all the requirements of the Quality System have not been
met, for instance if the associated AQC has failed, the reason is fully investigated and documented. The sample data is then evaluated alongside
the other quality control checks performed during analysis to determine its suitability. Following this evaluation, provided the sample results have not
been effected, the data is reported but accreditation is removed. It is a UKAS requirement for data not reported as accredited to be considered
indicative only, but this does not mean the data is not valid.
Where possible, and if requested, samples will be re-extracted and a revised report issued with accredited results. Please do not hesitate to contact
the laboratory if further details are required of the circumstances which have led to the removal of accreditation.
Where an MCERTS report has been requested, you will be notified within 48 hours of any samples that have been identified as being outside our
MCERTS scope. As validation has been performed on clay, sand and loam, only samples that are predominantly these matrices, or combinations
of them will be within our MCERTS scope. If samples are not one of a combination of the above matrices they will not be marked as MCERTS
accredited.
Negative Neutralization Potential (NP) values are obtained when the volume of NaOH (0.1N) titrated (pH 8.3) is greater than the volume of HCl (1N)
to reduce the pH of the sample to 2.0 - 2.5. Any negative NP values are corrected to 0.
Where a CEN 10:1 ZERO Headspace VOC test has been carried out, a 10:1 ratio of water to wet (as received) soil has been used.
All samples will be discarded one month after the date of reporting, unless we are instructed to the contrary.
It is assumed that you have taken representative samples on site and require analysis on a representative subsample. Stones will generally be
included unless we are requested to remove them.
ISO17025 (UKAS) accreditation applies to surface water and groundwater and one other matrix which is analysis specific, any other liquids are
outside our scope of accreditation.
As surface waters require different sample preparation to groundwaters the laboratory must be informed of the water type when submitting samples.
Where appropriate please make sure that our detection limits are suitable for your needs, if they are not, please notify us immediately.
Surrogate compounds are added during the preparation process to monitor recovery of analytes. However low recovery in soils is often due to peat,
clay or other organic rich matrices. For waters this can be due to oxidants, surfactants, organic rich sediments or remediation fluids. Acceptable
limits for most organic methods are 70 - 130% and for VOCs are 50 - 150%. When surrogate recoveries are outside the performance criteria but
the associated AQC passes this is assumed to be due to matrix effect. Results are not surrogate corrected.
A dilution suffix indicates a dilution has been performed and the reported result takes this into account. No further calculation is required.
If you have not already done so, please send us a purchase order if this is required by your company.
QF-PM 3.1.9 v32Please include all sections of this report if it is reproduced
All solid results are expressed on a dry weight basis unless stated otherwise. 4 of 6
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JE Job No.:
#
B
DR
M
NA
NAD
ND
NDP
SS
SV
W
+
++
*
AD
CO
LOD/LOR
ME
NFD
BS
LB
N
TB
OC
Analysis subcontracted to a Jones Environmental approved laboratory.
Matrix Effect
Blank Sample
Client Sample
Trip Blank Sample
AQC Sample
Suspected carry over
Limit of Detection (Limit of Reporting) in line with ISO 17025 and MCERTS
MCERTS accredited.
ISO17025 (UKAS) accredited - UK.
16/8230
AQC failure, accreditation has been removed from this result, if appropriate, see 'Note' on previous page.
Calibrated against a single substance
Not applicable
No Asbestos Detected.
No Determination Possible
Indicates analyte found in associated method blank.
None Detected (usually refers to VOC and/SVOC TICs).
Outside Calibration Range
No Fibres Detected
Result outside calibration range, results should be considered as indicative only and are not accredited.
Results expressed on as received basis.
Surrogate recovery outside performance criteria. This may be due to a matrix effect.
Samples are dried at 35°C ±5°C
Dilution required.
ABBREVIATIONS and ACRONYMS USED
QF-PM 3.1.9 v32Please include all sections of this report if it is reproduced
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JE Job No: 16/8230
Test Method No. Description
Prep Method
No. (if
appropriate)
Description
ISO
17025
(UKAS)
MCERTS
(UK soils
only)
Analysis done
on As Received
(AR) or Dried
(AD)
Reported on
dry weight
basis
TM26Determination of phenols by Reversed Phased High Performance Liquid
Chromatography and Electro-Chemical Detection.PM0 No preparation is required. Yes
TM30Determination of Trace Metal elements by ICP-OES (Inductively Coupled Plasma -
Optical Emission Spectrometry). Modified US EPA Method 200.7PM14
Analysis of waters and leachates for metals by ICP OES. Samples are filtered for
dissolved metals and acidified if required.
TM30Determination of Trace Metal elements by ICP-OES (Inductively Coupled Plasma -
Optical Emission Spectrometry). Modified US EPA Method 200.7PM14
Analysis of waters and leachates for metals by ICP OES. Samples are filtered for
dissolved metals and acidified if required.Yes
TM37Modified USEPA 160.2 .Gravimetric determination of Total Suspended Solids. Sample is
filtered and the resulting residue is dried and weighed.PM0 No preparation is required. Yes
TM38Soluble Ion analysis using the Thermo Aquakem Photometric Automatic Analyser.
Modified US EPA methods 325.2, 375.4, 365.2, 353.1, 354.1PM0 No preparation is required. Yes
TM57Modified US EPA Method 410.4. Chemical Oxygen Demand is determined by hot
digestion with Potassium Dichromate and measured spectrophotometerically.PM0 No preparation is required. Yes
TM59 Determination of Dissolved Oxygen using the Hach HQ30D Oxygen Meter PM0 No preparation is required.
TM60
Modified USEPA 9060. Determination of TOC by calculation from Total Carbon and
Inorganic Carbon using a TOC analyser, the carbon in the sample is converted to CO2
and then passed through a non-dispersive infrared gas analyser (NDIR).
PM0 No preparation is required. Yes
TM75Modified US EPA method 310.1. Determination of Alkalinity by Metrohm automated
titration analyser.PM0 No preparation is required. Yes
Jones Environmental Laboratory Method Code Appendix
QF-PM 3.1.10 v14 Please include all sections of this report if it is reproduced 6 of 6
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MEHL Quarter 2, 2016 Surface Water Monitoring Report, Hollywood Inert Landfill (EPA Licence W0129-02)
Figure
1
Figure 1: Monitoring Locations
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