LAB DATA MANAGEMENT SYSTEM - REGION IICOMPLETED PROJECT APPROVAL REPORT DATE 95/04/11

PROJECT NUMBER PROJECT DATE PROJECT NAME

023 95/03/09 TUTU 0'HENRY CLEANER /\ '/ APPROVED

PROJECT NO: 023

REMARK CODE

BJKLN0TU

CODE

QDQEQFQJQGQSORQPQHQTQMQBQQ

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

EXPLANATIONS OF REMARK CODES

EXPLANATION

RESULTS BASED UPON COLONY COUNTS OUTSIDE ACCEPTABLE RANGEESTIMATED VALUEACTUAL VALUE KNOWN TO BE LESS THAN VALUE GIVENACTUAL VALUE KNOWN TO BE GREATER THAN VALUE GIVENNO OBSERVABLE EFFECT CONCENTRATION < 0.3%SAMPLED BUT NOT ANALYZED DUE TO LAB ACCIDENTREPORTED VALUE LESS THAN CRITERIA OF DETECTIONREPORTING LIMIT

PAGE 1

REPORT DATE: 95/04/11

QA/QC REMARK CODES

EXPLANATION

ACCURACY CHECK SAMPLE ABOVE UPPER ACCEPTANCE LIMITACCURACY CHECK SAMPLE BELOW LOWER ACCEPTANCE LIMITPRECISION OF CALIBRATION CURVE LESS THAN ACCEPTANCE CRITERIAESTIMATED DETECTION LIMIT DUE TO INTERFERENCECONTINUING CALIBRATION CHECK DOES NOT MEET ACCEPTANCE CRITERIASPIKE RECOVERIES ABOVE UPPER ACCEPTANCE LIMITSPIKE RECOVERIES BELOW LOWER ACCEPTANCE LIMITSAMPLE REPLICATE PRECISION DOES NOT MEET ACCEPTANCE CRITERIARECOMMENDED HOLDING TIMES EXCEEDEDTENTATIVELY IDENTIFIED COMPOUNDPRESENCE OF MATERIAL VERIFIED BUT NOT QUANTIFIEDBLANK CONTAMINATED BY ANALYTE IN EXCESS OF ACCEPTANCE CRITERIASAMPLE IMPROPERLY PRESERVED

LOCATION CODES FOR IDENTIFICATION OF SAMPLING POINTS AT INDUSTRIAL /SANITARY FACILITIES, LANDFILLS, HAZARDOUS WASTE SITES.

CODE NUMBERS

1001 - 10501051 - 1099

1100143515XX200030003100320033003400350036003700

12491454

30993199329933993499359936993799

SAMPLING POINTS

EFFLUENT PIPE NUMBER 001 TO 050OTHER EFFLUENTS SUCH AS COOLING TOWER DISCHARGE,DISCHARGE FROM HOLDING PONDS, ETC...IN PLANT SAMPLESSEPARATE INFLUENT POINTS/WATER SOURCESINFLUENT ASSOCIATED WITH EFFLUENT 10XXBLANK FOR VOLATILE ORGAN ICSGROUND WATER FROM WELL 01 TO 99SEDIMENT SAMPLE (WATER BOTTOM)SOIL SAMPLESTREAM WATER SAMPLELAGOON SAMPLESTORAGE TANK SAMPLELEACHATE SAMPLEOTHER TYPE SAMPLE

PROJECT NO: 023

STATION NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU O'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 2

REPORT DATE: 95/04/11

VALUE & QA/QCUNITS CHEMISTRY REMARK REMARK

XS023 95/03/09 1153COMPOSITE 95/03/09 1155'EPTH: 0004 SUBSTRATE: SEDIMENTESCRIPTION: EXS023

KS025 95/03/09 1250:OHPOSITE 95/03/09 1255^PTH: 0004 SUBSTRATE: SEDIMENTESCRIPTION: EXS025

109401 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1.3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1.3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLORODIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2.2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

11 U11 U11 U11 U11 U21 J11 U11 U11 U11 U11 U11 U2 J11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U36 J43 J2 J

100 J11 U11 U11 U11 U11 U2 J

0000000000OQQQ0000000000QM0000000000OQ000000000000ON000000000000QM

109403 34421 METHYL CHLORIDE UG/KG 11 U 00

PROJECT NO: 023

TAT I ON NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 3

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/QCREMARK

(S024 95/03/09 1218:OMPOSITE 95/03/09 1220fPTH: 7.66 SUBSTRATE: SEDIMENTASCRIPTION: EXS024

109403 34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DlCHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1,3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLORODIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109404 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG

11 U11 U11 U11 U4 J11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U

210 J11 U11 U11 U11 U11 U11 U

QQQQ00QQOM00QQQQ0000QQ0000QQ00000000000000QQ00QQ00QQ00QQ000000QQ

11 U QQ11 U QQ11 U 00

PROJECT NO: 023

• TATION NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE l>

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/QCREMARK

(S031 95/03/09 1558:OMPOSITE 95/03/09 1600;PTH: 3.75 SUBSTRATE: SEDIMENT£SCRIPT10N: EXS031

109404 34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1,3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLORODIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109405 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG

11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U2 J

11 U11 U11 U11 U11 U11 U

12 U12 U12 U12 U12 U

QQQQQQ0000QQ000000QQ00QQQQ00QQ00000000000000QQQMQQQQQQ00QQ00

QQ00QQQQ00

PROJECT NO: 023

STATION NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 5

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/OCREMARK

EXS034 95/03/09 1638COMPOSITE 95/03/09 16403EPTH: 08.3 SUBSTRATE: SEDIMENTDESCRIPTION: EXS034

109405 75059 ACETONE UG/KG78544 CARBON BISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1,3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLOR001BROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109406 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG

51 J12 U12 U12 U12 U12 U12 U12 U12 U12 U12 U12 U12 U4 J12 U12 U12 U12 U12 U12 U12 U

630 J— 19~ rIT J12 U12 U12 U12 U12 U

11 U11 U11 U11 U11 U10 J11 U

00QQ0000QQ00QQQQ00QQQQ00OQQMQQQQQQ00QQQQ00QQ

00000000QQ

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PROJECT NO: 023

TATION NODATEFROMTO

TIMEOF

DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 7

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/QCREMARK

5032 95/03/09 1623JMPOSITE 95/03/09 16253TH: 02.5 SUBSTRATE: SEDIMENTSCRIPT I ON: EXS032

109407 99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1,3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLOROOIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109408 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG

11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U30 J11 U11 U11 U11 U11 U11 U

11 U11 U11 U11 U11 U15 J11 U11 U11 U11 U11 U

QQ00QQOQQQQQ000000QQQOQQ00QQOQ000000QQ00000000QQ

0000000000OQ0000OQ0000

PROJECT NO: 023

STATION NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 8

REPORT DATE: 95/04/11

VALUE & QA/QCUNITS CHEMISTRY REMARK REMARK

EXS030 95/03/09 1532COMPOSITE 95/03/09 1535

DEPTH: 5.33 SUBSTRATE: SEDIMENTDESCRIPTION: EXS030

109408 75078 2-BUTANONE . UG/KG34534 1,2-DICHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1,3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLOROOIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109409 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-DICHLOROETHANE UG/KG

11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U9 J7 J

11 U34 J11 U11 U11 U11 U11 U11 U

11 U11 U11 U11 U2 J

45 J11 U11 U11 U11 U11 U11 U11 U

000000000000QQ0000QQ00QQQMQM00QQQQ00QQ0000QQ

QQ000000OM0000QQQQQQ00QQQQ

PROJECT NO: 023

STATION NODATE TIMEFROM OFTO DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 9

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/QCREMARK

EXS028 95/03/09 1408COMPOSITE 95/03/09 1410

DEPTH: A.25 SUBSTRATE: SEDIMENTDESCRIPTION: EXS028

109409 34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1.3-DICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1.3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLORODIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

109410 34421 METHYL CHLORIDE UG/KG34416 METHYL BROMIDE UG/KG34495 VINYL CHLORIDE UG/KG34314 CHLOROETHANE UG/KG34426 METHYLENE CHLORIDE UG/KG75059 ACETONE UG/KG78544 CARBON DISULFIDE UG/KG34504 1,1-DICHLOROETHYLENE UG/KG34499 1,1-DICHLOROETHANE UG/KG99999 TOTAL 1,2-DICHLOROETHYLENE UG/KG34318 CHLOROFORM UG/KG75078 2-BUTANONE UG/KG34534 1,2-01CHLOROETHANE UG/KG34509 1,1,1-TRICHLOROETHANE UG/KG34299 CARBON TETRACHLORIDE UG/KG

11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U3 J

11 U11 U

480 J11 U11 U11 U11 U11 U11 U

11 U11 U11 U11 U11 U9 J

11 U11 U11 U11 U11 U11 U11 U11 U11 U

000000000000000000QQOM000000000000QQ0000

QQQQQQ00QQQMQQ00QQ

00OQ0000OQQQ

if V

o

PROJECT NO: 023

STATION NODATEFROMTO

TIMEOF

DAY

COMPLETED ANALYSIS REPORT

PROJECT NAME: TUTU 0'HENRY CLEANER

LABNO PARNO PARAMETER NAME

PAGE 10

REPORT DATE: 95/04/11

UNITS CHEMISTRYVALUE &REMARK

QA/QCREMARK

109410 34330 DICHLOROBROMOMETHANE UG/KG34544 1,2-DICHLOROPROPANE UG/KG34702 CIS-1,3-D ICHLOROPROPENE UG/KG34487 TRICHLOROETHYLENE UG/KG34237 BENZENE UG/KG34697 TRANS-1.3-DICHLOROPROPENE UG/KG34514 1,1,2-TRICHLOROETHANE UG/KG34309 CHLORODIBROMOMETHANE UG/KG75166 2-HEXANONE UG/KG75169 4-METHYL-2-PENTANONE UG/KG34290 BROMOFORM UG/KG34478 TETRACHLOROETHYLENE UG/KG34519 1,1,2,2-TETRACHLOROETHANE UG/KG34483 TOLUENE UG/KG34304 CHLOROBENZENE UG/KG34374 ETHYLBENZENE UG/KG99904 STYRENE UG/KG73382 XYLENES (TOTAL) UG/KG

11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U11 U

220 J11 U11 U11 U11 U11 U11 U

00QQQQ000000000000000000QQ

0000000000

***** END OF PROJECT *****

APR 13 iv'Si DATA NARRATIVE

Project #023

Tutu O1Henry Cleaner

All samples were received at 16°C. Therefore, all data have beenflagged as improperly preserved ("QQ").

Tij'T OO 4