j3099-1 stl level 2 portrait smp sort final reportjob number: 500-3099-1 job description: waukegan...

ANALYTICAL REPORT

Job Number: 500-3099-1

Job Description: Waukegan Slip 3

For:

Deigan & Associates

100 S. Genesee St.

Waukegan, IL 60085

Attention: Gary Deigan

Richard C Wright

Project Manager II

[email protected]

03/21/2007

These test results meet all the requirements of NELAC for accredited parameters.

The Lab Certification ID# is 100201.

All questions regarding this test report should be directed to the STL Project Manager whose signature appears on this report. All pages of this report are integral parts of the analytical data. Therefore, this report should be reproduced only in its entirety.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.

Project Manager: Richard C Wright

STL Chicago 2417 Bond Street, University Park, IL 60466Tel (708) 534-5200 Fax (708) 534-5211 www.stl-inc.com

Severn Trent Laboratories, Inc.

03/21/2007 of 67

Case Narrative for job: 500-J3099-1

Deigan & Associates

03/21/2007

Client:

Date:

Due to the level of target compound detected and the dilution required to get the samples within linear range of the instrument the surrogate recoveries are Diluted out.

GC Extractables_PCB

Surrogate - Diluted out

Affected Items500-3099-15 8082500-3099-17 8082500-3099-8 8082500-3099-12 8082500-3099-11 8082500-3099-16 8082500-3099-7 8082500-3099-10 8082

Surrogate (TCX) recovery for this sample was outside the upper control limit. This sample was re-analyzed with similiar results. The original was reported

GC Extractables_PCB

Other - Anomaly

Affected Items500-3099-5 8082

It was noted by the analyst that these samples exhibit the presence of a weathered Aroclor.

GC Extractables_PCB

Other - Anomaly

Affected Items500-3099-36 8082500-3099-23 8082500-3099-32 8082500-3099-12 8082500-3099-35 8082500-3099-11 8082500-3099-26 8082500-3099-24 8082500-3099-10 8082500-3099-25 8082

03/21/2007 of 67

EXECUTIVE SUMMARY - Detections

Client: Deigan & Associates Job Number: 500-3099-1

Analyte Result / QualifierReporting

Limit Units MethodLab Sample ID Client Sample ID

500-3099-1 SB-106,2.5-4.0'

34 ug/Kg 8082510PCB-124834 ug/Kg 8082510Polychlorinated biphenyls, Total0.10 % PercentMoisture3.2Percent Moisture0.10 % PercentMoisture97Percent Solids

500-3099-2 SB-106,5-7'


500-3099-3 SB-106,7-8.4'


500-3099-4 SB-106,5-7' DUPL.


500-3099-5 SB-106,10-12'


500-3099-6 SB-106,12-14'


STL Chicago

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500-3099-7 SB-105,2.2-3.7'

810 ug/Kg 80826100PCB-1248810 ug/Kg 80823700PCB-1254810 ug/Kg 80829700Polychlorinated biphenyls, Total0.10 % PercentMoisture3.3Percent Moisture0.10 % PercentMoisture97Percent Solids

500-3099-8 SB-105,5-7'


500-3099-9 SB-105 FB

0.10 % PercentMoisture0.36Percent Moisture0.10 % PercentMoisture100Percent Solids

500-3099-10 SB-105,7-8'

9200 ug/Kg 808219000PCB-12489200 ug/Kg 808219000Polychlorinated biphenyls, Total0.10 % PercentMoisture13Percent Moisture0.10 % PercentMoisture87Percent Solids

500-3099-11 SB-105,10-12'


500-3099-12 SB-105,12-13'


STL Chicago

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500-3099-13 SB-104,2.5-4.0'


500-3099-14 SB-104,2.5-4.0' DUPL.


500-3099-15 SB-104,5.7'


500-3099-16 SB-104,7-8.3'


500-3099-17 SB-104,10-11.5'


500-3099-18 SB-103,2.4-3.9'


STL Chicago

03/21/2007 of 67





500-3099-19 SB-103,5-7'


500-3099-20 SB-103,8-9.9'


500-3099-21 SB-103,10-12'


500-3099-22 SB-102,2.4-3.9'


500-3099-23 SB-102,5-7'


500-3099-24 SB-102,7-8.2'


STL Chicago

03/21/2007 of 67





500-3099-25 SB-102,7-8.2' DUPL.


500-3099-26 SB-102,10-11.3'


500-3099-27 SB-101,2.5-3.8'


500-3099-28 SB-101,5-7'


500-3099-29 SB-101,7-9'


500-3099-30 SB-101,10-12'


STL Chicago

03/21/2007 of 67





500-3099-31 SB-101,10-12' DUPL.


500-3099-32 SB-101,12-13.1'


500-3099-33 SB-102FB

0.10 % PercentMoisture0.52Percent Moisture0.10 % PercentMoisture99Percent Solids

500-3099-34 SB-107,2.5-4'


500-3099-35 SB-107,5-7'


500-3099-36 SB-107,7-9'


STL Chicago

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METHOD SUMMARY


Description Preparation MethodMethodLab Location

SolidMatrix:

PCBs SW846 8082STL CHI

SW846 3541Automated Soxhlet Extraction STL CHI

Percent Moisture EPA PercentMoistureSTL CHI

LAB REFERENCES:

STL CHI = STL Chicago

METHOD REFERENCES:

EPA - US Environmental Protection Agency

SW846 - "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

STL Chicago

03/21/2007 of 67

METHOD / ANALYST SUMMARY


Method Analyst Analyst ID

Manzano, Louis LMSW846 8082

Kolarczyk, Paul F PFKEPA PercentMoisture

STL Chicago

03/21/2007 of 67

SAMPLE SUMMARY


Client Sample IDLab Sample ID Client MatrixDate/Time Sampled

Date/Time Received

03/06/2007 0815 03/06/2007 1600SB-106,2.5-4.0'500-3099-1 Solid

03/06/2007 0830 03/06/2007 1600SB-106,5-7'500-3099-2 Solid

03/06/2007 0835 03/06/2007 1600SB-106,7-8.4'500-3099-3 Solid

03/06/2007 0845 03/06/2007 1600SB-106,5-7' Dupl.500-3099-4 Solid

03/06/2007 0850 03/06/2007 1600SB-106,10-12'500-3099-5 Solid

03/06/2007 0850 03/06/2007 1600SB-106,12-14'500-3099-6 Solid

03/06/2007 0855 03/06/2007 1600SB-105,2.2-3.7'500-3099-7 Solid

03/06/2007 0900 03/06/2007 1600SB-105,5-7'500-3099-8 Solid

03/06/2007 0905 03/06/2007 1600SB-105 FB500-3099-9 Solid

03/06/2007 0910 03/06/2007 1600SB-105,7-8'500-3099-10 Solid

03/06/2007 0915 03/06/2007 1600SB-105,10-12'500-3099-11 Solid

03/06/2007 0920 03/06/2007 1600SB-105,12-13'500-3099-12 Solid

03/06/2007 0935 03/06/2007 1600SB-104,2.5-4.0'500-3099-13 Solid

03/06/2007 0935 03/06/2007 1600SB-104,2.5-4.0' Dupl.500-3099-14 Solid

03/06/2007 0940 03/06/2007 1600SB-104,5.7'500-3099-15 Solid

03/06/2007 0945 03/06/2007 1600SB-104,7-8.3'500-3099-16 Solid

03/06/2007 0955 03/06/2007 1600SB-104,10-11.5'500-3099-17 Solid

03/06/2007 1035 03/06/2007 1600SB-103,2.4-3.9'500-3099-18 Solid

03/06/2007 1040 03/06/2007 1600SB-103,5-7'500-3099-19 Solid

03/06/2007 1045 03/06/2007 1600SB-103,8-9.9'500-3099-20 Solid

03/06/2007 1055 03/06/2007 1600SB-103,10-12'500-3099-21 Solid

03/06/2007 1105 03/06/2007 1600SB-102,2.4-3.9'500-3099-22 Solid

03/06/2007 1110 03/06/2007 1600SB-102,5-7'500-3099-23 Solid

03/06/2007 1115 03/06/2007 1600SB-102,7-8.2'500-3099-24 Solid

03/06/2007 1120 03/06/2007 1600SB-102,7-8.2' Dupl.500-3099-25 Solid

03/06/2007 1125 03/06/2007 1600SB-102,10-11.3'500-3099-26 Solid

03/06/2007 1130 03/06/2007 1600SB-101,2.5-3.8'500-3099-27 Solid

03/06/2007 1135 03/06/2007 1600SB-101,5-7'500-3099-28 Solid

03/06/2007 1140 03/06/2007 1600SB-101,7-9'500-3099-29 Solid

03/06/2007 1145 03/06/2007 1600SB-101,10-12'500-3099-30 Solid

03/06/2007 1145 03/06/2007 1600SB-101,10-12' Dupl.500-3099-31 Solid

03/06/2007 1150 03/06/2007 1600SB-101,12-13.1'500-3099-32 Solid

03/06/2007 1125 03/06/2007 1600SB-102FB500-3099-33 Solid

03/05/2007 1500 03/06/2007 1600SB-107,2.5-4'500-3099-34 Solid

03/05/2007 1505 03/06/2007 1600SB-107,5-7'500-3099-35 Solid

03/05/2007 1510 03/06/2007 1600SB-107,7-9'500-3099-36 Solid

STL Chicago

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SAMPLE RESULTS

STL Chicago

03/21/2007 of 67

Gary DeiganDeigan & Associates100 S. Genesee St.Waukegan, IL 60085


Client Sample ID:

Analyte Result/Qualifier Unit Dilution

03/06/2007 1600

03/06/2007 0815

Date Received:

Date Sampled:

500-3099-1Lab Sample ID:SB-106,2.5-4.0'

MDL RL

97Percent Solids:

Client Matrix: Solid

Method: Date Analyzed: 03/19/2007 19128082

Prep Method: 3541 Date Prepared: 03/13/2007 0759

PCB-1016 <34 ug/Kg 11 34 2.0PCB-1221 <34 ug/Kg 9.4 34 2.0PCB-1232 <34 ug/Kg 9.2 34 2.0PCB-1242 <34 ug/Kg 10 34 2.0PCB-1248 510 ug/Kg 7.4 34 2.0PCB-1254 <34 ug/Kg 7.6 34 2.0PCB-1260 <34 ug/Kg 6.7 34 2.0PCB-1268 <34 ug/Kg 34 34 2.0Polychlorinated biphenyls, Total 510 ug/Kg 6.7 34 2.0

Surrogate Acceptance Limits39 - 115106 %Tetrachloro-m-xylene47 - 11683 %DCB Decachlorobiphenyl

Method: Date Analyzed: 03/13/2007 1102PercentMoisture

Percent Moisture 3.2 % 0.10 0.10 1.0

03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0830

Date Received:

Date Sampled:

500-3099-2Lab Sample ID:SB-106,5-7'

MDL RL

96Percent Solids:




PCB-1016 <33 ug/Kg 11 33 2.0PCB-1221 <33 ug/Kg 9.1 33 2.0PCB-1232 <33 ug/Kg 8.9 33 2.0PCB-1242 <33 ug/Kg 9.7 33 2.0PCB-1248 470 ug/Kg 7.1 33 2.0PCB-1254 <33 ug/Kg 7.3 33 2.0PCB-1260 <33 ug/Kg 6.5 33 2.0PCB-1268 <33 ug/Kg 33 33 2.0Polychlorinated biphenyls, Total 470 ug/Kg 6.5 33 2.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0835

Date Received:

Date Sampled:

500-3099-3Lab Sample ID:SB-106,7-8.4'

MDL RL

95Percent Solids:




PCB-1016 <18 ug/Kg 5.9 18 1.0PCB-1221 <18 ug/Kg 4.8 18 1.0PCB-1232 <18 ug/Kg 4.7 18 1.0PCB-1242 <18 ug/Kg 5.1 18 1.0PCB-1248 310 ug/Kg 3.8 18 1.0PCB-1254 <18 ug/Kg 3.9 18 1.0PCB-1260 <18 ug/Kg 3.5 18 1.0PCB-1268 <18 ug/Kg 18 18 1.0Polychlorinated biphenyls, Total 310 ug/Kg 3.5 18 1.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0845

Date Received:

Date Sampled:

500-3099-4Lab Sample ID:SB-106,5-7' Dupl.

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0850

Date Received:

Date Sampled:

500-3099-5Lab Sample ID:SB-106,10-12'

MDL RL

93Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0850

Date Received:

Date Sampled:

500-3099-6Lab Sample ID:SB-106,12-14'

MDL RL

94Percent Solids:




PCB-1016 <180 ug/Kg 59 180 10PCB-1221 <180 ug/Kg 48 180 10PCB-1232 <180 ug/Kg 47 180 10PCB-1242 <180 ug/Kg 52 180 10PCB-1248 1000 ug/Kg 38 180 10PCB-1254 <180 ug/Kg 39 180 10PCB-1260 <180 ug/Kg 35 180 10PCB-1268 <180 ug/Kg 180 180 10Polychlorinated biphenyls, Total 1000 ug/Kg 35 180 10




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0855

Date Received:

Date Sampled:

500-3099-7Lab Sample ID:SB-105,2.2-3.7'

MDL RL

97Percent Solids:




PCB-1016 <810 ug/Kg 270 810 50PCB-1221 <810 ug/Kg 220 810 50PCB-1232 <810 ug/Kg 220 810 50PCB-1242 <810 ug/Kg 240 810 50PCB-1248 6100 ug/Kg 180 810 50PCB-1254 3700 ug/Kg 180 810 50PCB-1260 <810 ug/Kg 160 810 50PCB-1268 <810 ug/Kg 810 810 50Polychlorinated biphenyls, Total 9700 ug/Kg 160 810 50

Surrogate Acceptance Limits39 - 1150 D %Tetrachloro-m-xylene47 - 1160 D %DCB Decachlorobiphenyl



03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0900

Date Received:

Date Sampled:

500-3099-8Lab Sample ID:SB-105,5-7'

MDL RL

94Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0905

Date Received:

Date Sampled:

500-3099-9Lab Sample ID:SB-105 FB

MDL RL

100Percent Solids:




PCB-1016 <16 ug/Kg 5.5 16 1.0PCB-1221 <16 ug/Kg 4.5 16 1.0PCB-1232 <16 ug/Kg 4.4 16 1.0PCB-1242 <16 ug/Kg 4.8 16 1.0PCB-1248 <16 ug/Kg 3.5 16 1.0PCB-1254 <16 ug/Kg 3.6 16 1.0PCB-1260 <16 ug/Kg 3.2 16 1.0PCB-1268 <16 ug/Kg 16 16 1.0Polychlorinated biphenyls, Total <16 ug/Kg 3.2 16 1.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0910

Date Received:

Date Sampled:

500-3099-10Lab Sample ID:SB-105,7-8'

MDL RL

87Percent Solids:







Percent Moisture 13 % 0.10 0.10 1.0

03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0915

Date Received:

Date Sampled:

500-3099-11Lab Sample ID:SB-105,10-12'

MDL RL

60Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0920

Date Received:

Date Sampled:

500-3099-12Lab Sample ID:SB-105,12-13'

MDL RL

96Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0935

Date Received:

Date Sampled:

500-3099-13Lab Sample ID:SB-104,2.5-4.0'

MDL RL

96Percent Solids:





Surrogate Acceptance Limits39 - 115116 X %Tetrachloro-m-xylene47 - 116106 %DCB Decachlorobiphenyl



03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0935

Date Received:

Date Sampled:

500-3099-14Lab Sample ID:SB-104,2.5-4.0' Dupl.

MDL RL

96Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0940

Date Received:

Date Sampled:

500-3099-15Lab Sample ID:SB-104,5.7'

MDL RL

97Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0945

Date Received:

Date Sampled:

500-3099-16Lab Sample ID:SB-104,7-8.3'

MDL RL

94Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 0955

Date Received:

Date Sampled:

500-3099-17Lab Sample ID:SB-104,10-11.5'

MDL RL

93Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1035

Date Received:

Date Sampled:

500-3099-18Lab Sample ID:SB-103,2.4-3.9'

MDL RL

98Percent Solids:




PCB-1016 <83 ug/Kg 28 83 5.0PCB-1221 <83 ug/Kg 23 83 5.0PCB-1232 <83 ug/Kg 22 83 5.0PCB-1242 <83 ug/Kg 24 83 5.0PCB-1248 530 ug/Kg 18 83 5.0PCB-1254 <83 ug/Kg 18 83 5.0PCB-1260 <83 ug/Kg 16 83 5.0PCB-1268 <83 ug/Kg 83 83 5.0Polychlorinated biphenyls, Total 530 ug/Kg 16 83 5.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1040

Date Received:

Date Sampled:

500-3099-19Lab Sample ID:SB-103,5-7'

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1045

Date Received:

Date Sampled:

500-3099-20Lab Sample ID:SB-103,8-9.9'

MDL RL

94Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1055

Date Received:

Date Sampled:

500-3099-21Lab Sample ID:SB-103,10-12'

MDL RL

94Percent Solids:




PCB-1016 <88 ug/Kg 30 88 5.0PCB-1221 <88 ug/Kg 24 88 5.0PCB-1232 <88 ug/Kg 24 88 5.0PCB-1242 <88 ug/Kg 26 88 5.0PCB-1248 860 ug/Kg 19 88 5.0PCB-1254 <88 ug/Kg 20 88 5.0PCB-1260 <88 ug/Kg 17 88 5.0PCB-1268 <88 ug/Kg 88 88 5.0Polychlorinated biphenyls, Total 860 ug/Kg 17 88 5.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1105

Date Received:

Date Sampled:

500-3099-22Lab Sample ID:SB-102,2.4-3.9'

MDL RL

97Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1110

Date Received:

Date Sampled:

500-3099-23Lab Sample ID:SB-102,5-7'

MDL RL

89Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1115

Date Received:

Date Sampled:

500-3099-24Lab Sample ID:SB-102,7-8.2'

MDL RL

91Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1120

Date Received:

Date Sampled:

500-3099-25Lab Sample ID:SB-102,7-8.2' Dupl.

MDL RL

87Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1125

Date Received:

Date Sampled:

500-3099-26Lab Sample ID:SB-102,10-11.3'

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1130

Date Received:

Date Sampled:

500-3099-27Lab Sample ID:SB-101,2.5-3.8'

MDL RL

97Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1135

Date Received:

Date Sampled:

500-3099-28Lab Sample ID:SB-101,5-7'

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1140

Date Received:

Date Sampled:

500-3099-29Lab Sample ID:SB-101,7-9'

MDL RL

94Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1145

Date Received:

Date Sampled:

500-3099-30Lab Sample ID:SB-101,10-12'

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1145

Date Received:

Date Sampled:

500-3099-31Lab Sample ID:SB-101,10-12' Dupl.

MDL RL

93Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1150

Date Received:

Date Sampled:

500-3099-32Lab Sample ID:SB-101,12-13.1'

MDL RL

95Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/06/2007 1125

Date Received:

Date Sampled:

500-3099-33Lab Sample ID:SB-102FB

MDL RL

100Percent Solids:




PCB-1016 <16 ug/Kg 5.3 16 1.0PCB-1221 <16 ug/Kg 4.4 16 1.0PCB-1232 <16 ug/Kg 4.3 16 1.0PCB-1242 <16 ug/Kg 4.6 16 1.0PCB-1248 <16 ug/Kg 3.4 16 1.0PCB-1254 <16 ug/Kg 3.5 16 1.0PCB-1260 <16 ug/Kg 3.1 16 1.0PCB-1268 <16 ug/Kg 16 16 1.0Polychlorinated biphenyls, Total <16 ug/Kg 3.1 16 1.0




03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/05/2007 1500

Date Received:

Date Sampled:

500-3099-34Lab Sample ID:SB-107,2.5-4'

MDL RL

94Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/05/2007 1505

Date Received:

Date Sampled:

500-3099-35Lab Sample ID:SB-107,5-7'

MDL RL

91Percent Solids:








03/21/2007 of 67



Client Sample ID:


03/06/2007 1600

03/05/2007 1510

Date Received:

Date Sampled:

500-3099-36Lab Sample ID:SB-107,7-9'

MDL RL

84Percent Solids:








03/21/2007 of 67

DATA REPORTING QUALIFIERS


Lab Section Qualifier Description

GC Semi VOA

MS or MSD exceeds the control limitsF

RPD of the MS and MSD exceeds the control limitsF

Surrogate exceeds the control limitsX

Surrogate or matrix spike recoveries were not obtained because the extract was diluted for analysis; also compounds analyzed at a dilution may be flagged with a D.

D

STL Chicago

03/21/2007 of 67

QUALITY CONTROL RESULTS

STL Chicago

03/21/2007 of 67

Quality Control Results


QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

ReportBasis

GC Semi VOA

Prep Batch: 500-11501Lab Control Spike Solid 3541LCS 500-11501/2-AA TMethod Blank Solid 3541MB 500-11501/1-AA T

SolidSB-106,2.5-4.0' 3541500-3099-1 TMatrix Spike Solid 3541500-3099-1MS TMatrix Spike Duplicate Solid 3541500-3099-1MSD T

SolidSB-106,5-7' 3541500-3099-2 TSolidSB-106,7-8.4' 3541500-3099-3 TSolidSB-106,5-7' Dupl. 3541500-3099-4 TSolidSB-106,10-12' 3541500-3099-5 TSolidSB-106,12-14' 3541500-3099-6 TSolidSB-105,2.2-3.7' 3541500-3099-7 TSolidSB-105,5-7' 3541500-3099-8 TSolidSB-105 FB 3541500-3099-9 TSolidSB-105,7-8' 3541500-3099-10 TSolidSB-105,10-12' 3541500-3099-11 TSolidSB-105,12-13' 3541500-3099-12 TSolidSB-104,2.5-4.0' 3541500-3099-13 TSolidSB-104,2.5-4.0' Dupl. 3541500-3099-14 TSolidSB-104,5.7' 3541500-3099-15 TSolidSB-104,7-8.3' 3541500-3099-16 TSolidSB-104,10-11.5' 3541500-3099-17 TSolidSB-103,2.4-3.9' 3541500-3099-18 TSolidSB-103,5-7' 3541500-3099-19 TSolidSB-103,8-9.9' 3541500-3099-20 T

STL Chicago

03/21/2007 of 67





ReportBasis

GC Semi VOA

Prep Batch: 500-11569Lab Control Spike Solid 3541LCS 500-11569/2-AA TMethod Blank Solid 3541MB 500-11569/1-AA T

SolidSB-103,10-12' 3541500-3099-21 TMatrix Spike Solid 3541500-3099-21MS TMatrix Spike Duplicate Solid 3541500-3099-21MSD T

SolidSB-102,2.4-3.9' 3541500-3099-22 TSolidSB-102,5-7' 3541500-3099-23 TSolidSB-102,7-8.2' 3541500-3099-24 TSolidSB-102,7-8.2' Dupl. 3541500-3099-25 TSolidSB-102,10-11.3' 3541500-3099-26 TSolidSB-101,2.5-3.8' 3541500-3099-27 TSolidSB-101,5-7' 3541500-3099-28 TSolidSB-101,7-9' 3541500-3099-29 TSolidSB-101,10-12' 3541500-3099-30 TSolidSB-101,10-12' Dupl. 3541500-3099-31 TSolidSB-101,12-13.1' 3541500-3099-32 TSolidSB-102FB 3541500-3099-33 TSolidSB-107,2.5-4' 3541500-3099-34 TSolidSB-107,5-7' 3541500-3099-35 TSolidSB-107,7-9' 3541500-3099-36 T

STL Chicago

03/21/2007 of 67





ReportBasis

GC Semi VOA

Analysis Batch:500-11805Lab Control Spike Solid 500-115018082LCS 500-11501/2-AA TMethod Blank Solid 500-115018082MB 500-11501/1-AA T

Solid 500-11501SB-106,2.5-4.0' 8082500-3099-1 TMatrix Spike Solid 500-115018082500-3099-1MS TMatrix Spike Duplicate Solid 500-115018082500-3099-1MSD T

Solid 500-11501SB-106,5-7' 8082500-3099-2 TSolid 500-11501SB-106,7-8.4' 8082500-3099-3 TSolid 500-11501SB-106,5-7' Dupl. 8082500-3099-4 TSolid 500-11501SB-106,10-12' 8082500-3099-5 TSolid 500-11501SB-106,12-14' 8082500-3099-6 TSolid 500-11501SB-105,2.2-3.7' 8082500-3099-7 TSolid 500-11501SB-105,5-7' 8082500-3099-8 TSolid 500-11501SB-105 FB 8082500-3099-9 TSolid 500-11501SB-105,7-8' 8082500-3099-10 TSolid 500-11501SB-105,10-12' 8082500-3099-11 TSolid 500-11501SB-105,12-13' 8082500-3099-12 TSolid 500-11501SB-104,2.5-4.0' 8082500-3099-13 TSolid 500-11501SB-104,2.5-4.0' Dupl. 8082500-3099-14 TSolid 500-11501SB-104,5.7' 8082500-3099-15 TSolid 500-11501SB-104,7-8.3' 8082500-3099-16 TSolid 500-11501SB-104,10-11.5' 8082500-3099-17 TSolid 500-11501SB-103,2.4-3.9' 8082500-3099-18 TSolid 500-11501SB-103,5-7' 8082500-3099-19 TSolid 500-11501SB-103,8-9.9' 8082500-3099-20 T

STL Chicago

03/21/2007 of 67





ReportBasis

GC Semi VOA

Analysis Batch:500-11845Lab Control Spike Solid 500-115698082LCS 500-11569/2-AA TMethod Blank Solid 500-115698082MB 500-11569/1-AA T

Solid 500-11569SB-103,10-12' 8082500-3099-21 TMatrix Spike Solid 500-115698082500-3099-21MS TMatrix Spike Duplicate Solid 500-115698082500-3099-21MSD T

Solid 500-11569SB-102,2.4-3.9' 8082500-3099-22 TSolid 500-11569SB-102,5-7' 8082500-3099-23 TSolid 500-11569SB-102,7-8.2' 8082500-3099-24 TSolid 500-11569SB-102,7-8.2' Dupl. 8082500-3099-25 TSolid 500-11569SB-102,10-11.3' 8082500-3099-26 TSolid 500-11569SB-101,2.5-3.8' 8082500-3099-27 TSolid 500-11569SB-101,5-7' 8082500-3099-28 TSolid 500-11569SB-101,7-9' 8082500-3099-29 TSolid 500-11569SB-101,10-12' 8082500-3099-30 TSolid 500-11569SB-101,10-12' Dupl. 8082500-3099-31 TSolid 500-11569SB-101,12-13.1' 8082500-3099-32 TSolid 500-11569SB-102FB 8082500-3099-33 TSolid 500-11569SB-107,2.5-4' 8082500-3099-34 TSolid 500-11569SB-107,5-7' 8082500-3099-35 TSolid 500-11569SB-107,7-9' 8082500-3099-36 T

Report Basis

T = Total

STL Chicago

03/21/2007 of 67





ReportBasis

General Chemistry

Analysis Batch:500-11531SolidSB-106,2.5-4.0' PercentMoisture500-3099-1 T

Duplicate Solid PercentMoisture500-3099-1DU TSolidSB-106,5-7' PercentMoisture500-3099-2 TSolidSB-106,7-8.4' PercentMoisture500-3099-3 TSolidSB-106,5-7' Dupl. PercentMoisture500-3099-4 TSolidSB-106,10-12' PercentMoisture500-3099-5 TSolidSB-106,12-14' PercentMoisture500-3099-6 TSolidSB-105,2.2-3.7' PercentMoisture500-3099-7 TSolidSB-105,5-7' PercentMoisture500-3099-8 TSolidSB-105 FB PercentMoisture500-3099-9 TSolidSB-105,7-8' PercentMoisture500-3099-10 TSolidSB-105,10-12' PercentMoisture500-3099-11 TSolidSB-105,12-13' PercentMoisture500-3099-12 TSolidSB-104,2.5-4.0' PercentMoisture500-3099-13 TSolidSB-104,2.5-4.0' Dupl. PercentMoisture500-3099-14 TSolidSB-104,5.7' PercentMoisture500-3099-15 TSolidSB-104,7-8.3' PercentMoisture500-3099-16 TSolidSB-104,10-11.5' PercentMoisture500-3099-17 TSolidSB-103,2.4-3.9' PercentMoisture500-3099-18 TSolidSB-103,5-7' PercentMoisture500-3099-19 TSolidSB-103,8-9.9' PercentMoisture500-3099-20 T

Analysis Batch:500-11533SolidSB-103,10-12' PercentMoisture500-3099-21 TSolidSB-102,2.4-3.9' PercentMoisture500-3099-22 TSolidSB-102,5-7' PercentMoisture500-3099-23 T

Duplicate Solid PercentMoisture500-3099-23DU TSolidSB-102,7-8.2' PercentMoisture500-3099-24 TSolidSB-102,7-8.2' Dupl. PercentMoisture500-3099-25 TSolidSB-102,10-11.3' PercentMoisture500-3099-26 TSolidSB-101,2.5-3.8' PercentMoisture500-3099-27 TSolidSB-101,5-7' PercentMoisture500-3099-28 TSolidSB-101,7-9' PercentMoisture500-3099-29 TSolidSB-101,10-12' PercentMoisture500-3099-30 TSolidSB-101,10-12' Dupl. PercentMoisture500-3099-31 TSolidSB-101,12-13.1' PercentMoisture500-3099-32 TSolidSB-102FB PercentMoisture500-3099-33 TSolidSB-107,2.5-4' PercentMoisture500-3099-34 TSolidSB-107,5-7' PercentMoisture500-3099-35 TSolidSB-107,7-9' PercentMoisture500-3099-36 T

Report Basis

T = Total

STL Chicago

03/21/2007 of 67



8082 PCBs

(DCB 1)(%Rec)

(TCX 1)(%Rec)

500-3099-1 SB-106,2.5-4.0' 83 106

500-3099-2 SB-106,5-7' 86 105

500-3099-3 SB-106,7-8.4' 82 100

500-3099-4 SB-106,5-7' Dupl. 95 115

500-3099-5 SB-106,10-12' 89 105

500-3099-6 SB-106,12-14' 88 104

500-3099-7 SB-105,2.2-3.7' 0 D 0 D

500-3099-8 SB-105,5-7' 0 D 0 D

500-3099-9 SB-105 FB 72 74

500-3099-10 SB-105,7-8' 0 D 0 D

500-3099-11 SB-105,10-12' 0 D 0 D

500-3099-12 SB-105,12-13' 0 D 0 D

500-3099-13 SB-104,2.5-4.0' 106 116 X

500-3099-14 SB-104,2.5-4.0' Dupl. 97 107

500-3099-15 SB-104,5.7' 0 D 0 D

500-3099-16 SB-104,7-8.3' 0 D 0 D

500-3099-17 SB-104,10-11.5' 0 D 0 D

500-3099-18 SB-103,2.4-3.9' 99 112

500-3099-19 SB-103,5-7' 101 115

500-3099-20 SB-103,8-9.9' 97 107

500-3099-21 SB-103,10-12' 99 93

500-3099-22 SB-102,2.4-3.9' 113 83

500-3099-23 SB-102,5-7' 0 D 0 D

500-3099-24 SB-102,7-8.2' 0 D 0 D

500-3099-25 SB-102,7-8.2' Dupl. 0 D 0 D

Lab Sample ID Client Sample

Surrogate Recovery Report


STL Chicago 03/21/2007 of 67



(DCB 1)(%Rec)

(TCX 1)(%Rec)

500-3099-26 SB-102,10-11.3' 0 D 0 D

500-3099-27 SB-101,2.5-3.8' 0 D 0 D

500-3099-28 SB-101,5-7' 0 D 0 D

500-3099-29 SB-101,7-9' 0 D 0 D

500-3099-30 SB-101,10-12' 0 D 0 D

500-3099-31 SB-101,10-12' Dupl. 0 D 0 D

500-3099-32 SB-101,12-13.1' 0 D 0 D

500-3099-33 SB-102FB 79 57

500-3099-34 SB-107,2.5-4' 0 D 0 D

500-3099-35 SB-107,5-7' 0 D 0 D

500-3099-36 SB-107,7-9' 0 D 0 D

500-3099-1MS SB-106,2.5-4.0' 86 102

500-3099-1MSD SB-106,2.5-4.0' 81 99

500-3099-21MS SB-103,10-12' 104 93

500-3099-21MSD SB-103,10-12' 101 93

LCS 500-11501/2-AA 70 82

LCS 500-11569/2-AA 87 65

MB 500-11501/1-AA 73 87

MB 500-11569/1-AA 93 74

Surrogate Acceptance Limits

(DCB 1)(%Rec)

47 - 116DCB Decachlorobiphenyl(TCX 1)(%Rec)

39 - 115Tetrachloro-m-xylene

STL Chicago 03/21/2007 of 67


Job Number: 500-3099-1Client: Deigan & Associates

SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

03/17/2007 0216

Method Blank - Batch: 500-11501

Date Prepared:

Instrument ID:

Lab File ID:

Initial Weight/Volume:

Final Weight/Volume:

Injection Volume:

Analysis Batch: 500-11805

Prep Batch: 500-11501

03/13/2007 0759

03150723_080.d

15.000 g

5.0 mL

Units: ug/Kg

Column ID: PRIMARY

Method: 8082Preparation: 3541

HP 6890N GCMB 500-11501/1-AA

Analyte Result Qual MDL RL

<17 175.6PCB-1016<17 174.6PCB-1221<17 174.5PCB-1232<17 174.9PCB-1242<17 173.6PCB-1248<17 173.7PCB-1254<17 173.3PCB-1260<17 1717PCB-1268<17 173.3Polychlorinated biphenyls, Total

Surrogate % Rec Acceptance Limits

Tetrachloro-m-xylene 87 39 - 115DCB Decachlorobiphenyl 73 47 - 116

Solid

1.0

03/17/2007 0238Date Analyzed:

Lab Control Spike - Batch: 500-11501

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

03150723_081.d

03/13/2007 0759



15.000 g

5.0 mL

Units: ug/Kg

Column ID: PRIMARY


HP 6890N GCLCS 500-11501/2-AA

Analyte QualLimit% Rec.ResultSpike Amount

167 121 73 48 - 113PCB-1016167 117 70 62 - 117PCB-1260


Tetrachloro-m-xylene 82 39 - 115

DCB Decachlorobiphenyl 70 47 - 116

STL Chicago

Calculations are performed before rounding to avoid round-off errors in calculated results.

03/21/2007 of 67



Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

03/19/2007 1934

03/19/2007 1956

Solid

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 500-11501

2.0

2.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




03/13/2007 0759

03/13/2007 0759



03190723_024.d

15.5772 g

5.0 mL

PRIMARY

03190723_025.d

15.2895 g

5.0 mL

PRIMARY


HP 6890N GC

HP 6890N GC

500-3099-1

500-3099-1

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

271 540 48 - 113 68 30 F FPCB-1016

103 113 62 - 117 12 30PCB-1260

Surrogate MS % Rec MSD % Rec Acceptance Limits

Tetrachloro-m-xylene 102 99 39 - 115DCB Decachlorobiphenyl 86 81 47 - 116

STL Chicago


03/21/2007 of 67



SolidClient Matrix:

1.0Dilution:

Date Analyzed:

Lab Sample ID:

03/19/2007 1151

Method Blank - Batch: 500-11569

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:



03/14/2007 0753

03140731_002.d

15.000 g

5.0 mL

Units: ug/Kg

Column ID: PRIMARY


HP 6890N GCMB 500-11569/1-AA

Analyte Result Qual MDL RL

<17 175.6PCB-1016<17 174.6PCB-1221<17 174.5PCB-1232<17 174.9PCB-1242<17 173.6PCB-1248<17 173.7PCB-1254<17 173.3PCB-1260<17 1717PCB-1268<17 173.3Polychlorinated biphenyls, Total


Tetrachloro-m-xylene 74 39 - 115DCB Decachlorobiphenyl 93 47 - 116

Solid

1.0

03/19/2007 1211Date Analyzed:

Lab Control Spike - Batch: 500-11569

Client Matrix:

Lab Sample ID:

Dilution:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

03140731_003.d

03/14/2007 0753



15.000 g

5.0 mL

Units: ug/Kg

Column ID: PRIMARY


HP 6890N GCLCS 500-11569/2-AA

Analyte QualLimit% Rec.ResultSpike Amount

167 128 77 48 - 113PCB-1016167 151 90 62 - 117PCB-1260


Tetrachloro-m-xylene 65 39 - 115

DCB Decachlorobiphenyl 87 47 - 116

STL Chicago


03/21/2007 of 67



Date Analyzed:

Date Analyzed:

Dilution:

Dilution:

03/19/2007 1745

03/19/2007 1805

Solid

Matrix Spike/Matrix Spike Duplicate Recovery Report - Batch: 500-11569

5.0

5.0

MS Lab Sample ID:

MSD Lab Sample ID:

Client Matrix:

Date Prepared:

Date Prepared:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:

Instrument ID:

Lab File ID:



Injection Volume:

Column ID:




03/14/2007 0753

03/14/2007 0753



03140731_019.d

15.9088 g

5.0 mL

PRIMARY

03140731_020.d

15.3832 g

5.0 mL

PRIMARY


HP 6890N GC

HP 6890N GC

500-3099-21

500-3099-21

Analyte MSD QualMS QualRPD LimitRPDLimitMSDMS

% Rec.

321 282 48 - 113 9 30 F FPCB-1016

123 120 62 - 117 1 30 F FPCB-1260

Surrogate MS % Rec MSD % Rec Acceptance Limits

Tetrachloro-m-xylene 93 93 39 - 115DCB Decachlorobiphenyl 104 101 47 - 116

STL Chicago


03/21/2007 of 67



%Units:

Solid

Dilution: 1.0

Date Analyzed:

Duplicate - Batch: 500-11531

Lab Sample ID:

Client Matrix:

Date Prepared:

03/13/2007 1102

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Method: PercentMoisturePreparation: N/A

N/A

No Equipment Assigned500-3099-1

Analyte QualLimitRPDResultSample Result/Qual

96.697 0 20Percent Solids

STL Chicago


03/21/2007 of 67



%Units:

Solid

Dilution: 1.0

Date Analyzed:

Duplicate - Batch: 500-11533

Lab Sample ID:

Client Matrix:

Date Prepared:

03/13/2007 1107

Instrument ID:

Lab File ID:




Prep Batch: N/A

N/A

Method: PercentMoisturePreparation: N/A

N/A

No Equipment Assigned500-3099-23

Analyte QualLimitRPDResultSample Result/Qual

84.089 6 20Percent Solids

STL Chicago


03/21/2007 of 67

03/21/2007 of 67

LOGIN SAMPLE RECEIPT CHECK LIST


Question T/F/NA Comment

Login Number: 3099

Radioactivity either was not measured or, if measured, is at or below background True

The cooler's custody seal, if present, is intact. False

The cooler or samples do not appear to have been compromised or tampered with. True

Samples were received on ice. 3.7,3.5,4.1True

Cooler Temperature is acceptable. True

Cooler Temperature is recorded. True

COC is present. True

COC is filled out in ink and legible. True

COC is filled out with all pertinent information. True

There are no discrepancies between the sample IDs on the containers and the COC.

True

Samples are received within Holding Time. True

Sample containers have legible labels. True

Containers are not broken or leaking. True

Sample collection date/times are provided. True

Appropriate sample containers are used. True

Sample bottles are completely filled. True

There is sufficient vol. for all requested analyses, incl. any requested MS/MSDs True

VOA sample vials do not have headspace or bubble is <6mm (1/4") in diameter. True

If necessary, staff have been informed of any short hold time or quick TAT needs True

Multiphasic samples are not present. True

Samples do not require splitting or compositing. True

STL Chicago03/21/2007 of 67

ANALYTICAL REPORT


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03/20/2007Page 1 of 44

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RTA LCats@b

03/20/2007Page 4 of 44

ANLYTIC RAAEPO


ISevrntanbo irStsrsanboCASa,bcASa,bc.s;C.bvsanbo

b<ncAsarn=>

SJl3 F&A.GeeeAWA,FILeJ68

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dS-eaejFedNMbt9Np Nu5oeSt9u 1ub9Ne-: N1w

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L.CB,nvsCb

03/20/2007Page 5 of 44

ANLYTIC CRERPOSLCCSeAARvO


Arntab Rois,cn Rois,cnC.I

S5Nl5N9Fe&9ib3 &SA.G,IeeeGWGL

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69o5t1l8yFeR5ioeh Rh6CR-eeeR t1 NuS9b3uit

SLPC;t<=i>a

03/20/2007Page 6 of 44

ANLYTICA LLNRE


POSevrCAntaOeCboTniCAntaOeCbo POSevrCLnrsS,onrec.SteCAntaOe;

onrec.SteCRe<eS=e;

WkSWnSlWWFeegngn WkSW&SlWWFeeg&WWA.agWFGgWagg,&InWWakgWWag A9obL

WkSWnSlWWFeegnlW WkSW&SlWWFeeg&WWA.agWFGgg,&agk,nInWWakgWWal A9obL

WkSWnSlWWFeegnkW WkSW&SlWWFeeg&WWA.agW6Gl,na8,kInWWakgWWak A9obL

WkSWnSlWWFeegnkn WkSW&SlWWFeeg&WWA.agW6GnaFInWWakgWWa8 A9obL

WkSWnSlWWFeegn8WWkSW&SlWWFeeg&WWA.agW6GFa6,nInWWakgWWan A9obL

WkSWnSlWWFeegn8n WkSW&SlWWFeeg&WWA.agW6GgWagl,kInWWakgWWa& A9obL

WkSW&SlWWFeegkgn WkSW&SlWWFeeg&WWy.aWlGkInWWakgWWaR A9obL

WkSW&SlWWFeegklW WkSW&SlWWFeeg&WWy.aWlG&InWWakgWWagW A9obL

WkSW&SlWWFeegkkWWkSW&SlWWFeeg&WWy.aWlGggInWWakgWWagg A9obL

WkSW&SlWWFeegk8n WkSW&SlWWFeeg&WWy.aWlGg&InWWakgWWagl A9obL

WkSW&SlWWFeegknn WkSW&SlWWFeeg&WWy.aWlGlWInWWakgWWagk A9obL

WkSW&SlWWFeeg8gn WkSW&SlWWFeeg&WWy.aWlGlkInWWakgWWag8 A9obL

WkSW&SlWWFeeg8kWWkSW&SlWWFeeg&WWy.aWgGkInWWakgWWagF A9obL

WkSW&SlWWFeeg8kn WkSW&SlWWFeeg&WWy.aWgGFInWWakgWWag6 A9obL

WkSW&SlWWFeeg88WWkSW&SlWWFeeg&WWy.aWgGggInWWakgWWagR A9obL

WkSW&SlWWFeeg88n WkSW&SlWWFeeg&WWy.aWgGgnInWWakgWWalW A9obL

WkSW&SlWWFeeg8nn WkSW&SlWWFeeg&WWy.aWgGgRInWWakgWWalg A9obL

WkSW&SlWWFeegngn WkSW&SlWWFeeg&WWy.aWgGlkInWWakgWWall A9obL

WkSW&SlWWFeeglWWWkSW&SlWWFeeg&WWA.agWkh.nWWakgWWalk A9obL

WkSW&SlWWFeeglWWWkSW&SlWWFeeg&WWA.agW8h.nWWakgWWal8 A9obL

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WkSWnSlWWFeeglWWWkSW&SlWWFeeg&WWA.agWFh.nWWakgWWal& A9obL

A.TCP>S<n?@

03/20/2007Page 7 of 44

ANLYTIC IARTEA

AETCPOSevrn

03/20/2007Page 8 of 44



Client Sample ID:


039069/002 1600

039059/002 1515

Date 7eceiRev:

Date Samdpev:

500-3900-91aL Sample ID:Sb-90B690-99,2.

4D1 R1

l/Percent Sopivs:

Cpient Matrix: Sopiv

4et'oM: Date Anapyzev: 039189/002 05B1h0hd

8rep 4et'oM: 35P9 Date Predarev: 039139/002 080l

PC<-1016 4360 ug9Kg 1/0 360 /0PC<-1//1 4360 ug9Kg 100 360 /0PC<-1/3/ 4360 ug9Kg l8 360 /0PC<-1/B/ 4360 ug9Kg 110 360 /0PC<-1/B8 3/00 ug9Kg 28 360 /0PC<-1/5B 4360 ug9Kg 80 360 /0PC<-1/60 4360 ug9Kg 2/ 360 /0PC<-1/68 4360 ug9Kg 360 360 /0Popychporinatev bidhenyps, Totap 3/00 ug9Kg 2/ 360 /0

Surrogate Accedtance Limits3l - 1150 D %Tetrachporo-m-xypeneB2 - 1160 D %DC< Decachporobidhenyp

4et'oM: Date Anapyzev: 0391B9/002 16168ercent4oisture


03/20/2007Page 9 of 44



Client Sample ID:


039069/002 1600

039059/002 15/0

Date 7eceiRev:

Date Samdpev:

500-3900-d1aL Sample ID:Sb-90B699,2-93,5.

4D1 R1

25Percent Sopivs:


4et'oM: Date Anapyzev: 039189/002 0208h0hd


PC<-1016 411000 ug9Kg 3200 11000 500PC<-1//1 411000 ug9Kg 3000 11000 500PC<-1/3/ 411000 ug9Kg 3000 11000 500PC<-1/B/ 411000 ug9Kg 3/00 11000 500PC<-1/B8 B/000 ug9Kg /B00 11000 500PC<-1/5B 411000 ug9Kg /500 11000 500PC<-1/60 411000 ug9Kg //00 11000 500PC<-1/68 411000 ug9Kg 11000 11000 500Popychporinatev bidhenyps, Totap B/000 ug9Kg //00 11000 500



Percent Moisture /5 % 0.10 0.10 1.0

03/20/2007Page 10 of 44



Client Sample ID:


039069/002 1600

039059/002 1530

Date 7eceiRev:

Date Samdpev:

500-3900-31aL Sample ID:Sb-90h6d,5-P,3.

4D1 R1

l5Percent Sopivs:




PC<-1016 48B0 ug9Kg /80 8B0 50PC<-1//1 48B0 ug9Kg /30 8B0 50PC<-1/3/ 48B0 ug9Kg /30 8B0 50PC<-1/B/ 48B0 ug9Kg /50 8B0 50PC<-1/B8 2100 ug9Kg 180 8B0 50PC<-1/5B 48B0 ug9Kg 1l0 8B0 50PC<-1/60 48B0 ug9Kg 120 8B0 50PC<-1/68 48B0 ug9Kg 8B0 8B0 50Popychporinatev bidhenyps, Totap 2100 ug9Kg 120 8B0 50



Percent Moisture 5./ % 0.10 0.10 1.0

03/20/2007Page 11 of 44



Client Sample ID:


039069/002 1600

039059/002 1535

Date 7eceiRev:

Date Samdpev:

500-3900-P1aL Sample ID:Sb-90h65-B.

4D1 R1

lBPercent Sopivs:


4et'oM: Date Anapyzev: 039/09/002 1B1lh0hd

8rep 4et'oM: 35P9 Date Predarev: 039169/002 1600

PC<-1016 488 ug9Kg /l 88 5.0PC<-1//1 488 ug9Kg /B 88 5.0PC<-1/3/ 488 ug9Kg /B 88 5.0PC<-1/B/ 488 ug9Kg /6 88 5.0PC<-1/B8 5l0 ug9Kg 1l 88 5.0PC<-1/5B 488 ug9Kg 1l 88 5.0PC<-1/60 488 ug9Kg 12 88 5.0PC<-1/68 488 ug9Kg 88 88 5.0Popychporinatev bidhenyps, Totap 5l0 ug9Kg 12 88 5.0

Surrogate Accedtance Limits3l - 115101 %Tetrachporo-m-xypeneB2 - 116l0 %DC< Decachporobidhenyp



03/20/2007Page 12 of 44



Client Sample ID:


039069/002 1600

039059/002 15B0

Date 7eceiRev:

Date Samdpev:

500-3900-51aL Sample ID:Sb-90h6B-h,5.

4D1 R1

l6Percent Sopivs:




PC<-1016 412 ug9Kg 5.6 12 1.0PC<-1//1 412 ug9Kg B.6 12 1.0PC<-1/3/ 412 ug9Kg B.5 12 1.0PC<-1/B/ 412 ug9Kg B.l 12 1.0PC<-1/B8 /l0 ug9Kg 3.6 12 1.0PC<-1/5B 412 ug9Kg 3.2 12 1.0PC<-1/60 412 ug9Kg 3.3 12 1.0PC<-1/68 412 ug9Kg 12 12 1.0Popychporinatev bidhenyps, Totap /l0 ug9Kg 3.3 12 1.0

Surrogate Accedtance Limits3l - 115l5 %Tetrachporo-m-xypeneB2 - 116l5 %DC< Decachporobidhenyp



03/20/2007Page 13 of 44



Client Sample ID:


039069/002 1600

039059/002 15B5

Date 7eceiRev:

Date Samdpev:

500-3900-21aL Sample ID:Sb-90h690-9d,3.

4D1 R1

l6Percent Sopivs:




PC<-1016 4120 ug9Kg 58 120 10PC<-1//1 4120 ug9Kg B2 120 10PC<-1/3/ 4120 ug9Kg B6 120 10PC<-1/B/ 4120 ug9Kg 50 120 10PC<-1/B8 1/00 ug9Kg 32 120 10PC<-1/5B 4120 ug9Kg 38 120 10PC<-1/60 4120 ug9Kg 3B 120 10PC<-1/68 4120 ug9Kg 120 120 10Popychporinatev bidhenyps, Totap 1/00 ug9Kg 3B 120 10

Surrogate Accedtance Limits3l - 115102 %Tetrachporo-m-xypeneB2 - 116110 %DC< Decachporobidhenyp


Percent Moisture B.3 % 0.10 0.10 1.0

03/20/2007Page 14 of 44



Client Sample ID:


039069/002 1600

039069/002 1315

Date 7eceiRev:

Date Samdpev:

500-3900-71aL Sample ID:Fb-0d63.

4D1 R1


4et'oM: Date Anapyzev: 0391B9/002 1610D-dd92


03/20/2007Page 15 of 44



Client Sample ID:


039069/002 1600

039069/002 13/0

Date 7eceiRev:

Date Samdpev:

500-3900-901aL Sample ID:Fb-0d62.

4D1 R1



Percent Moisture B.2 % 0.10 0.10 1.0

03/20/2007Page 16 of 44



Client Sample ID:


039069/002 1600

039069/002 1330

Date 7eceiRev:

Date Samdpev:

500-3900-991aL Sample ID:Fb-0d699.

4D1 R1



Percent Moisture 2./ % 0.10 0.10 1.0

03/20/2007Page 17 of 44



Client Sample ID:


039069/002 1600

039069/002 13B5

Date 7eceiRev:

Date Samdpev:

500-3900-9d1aL Sample ID:Fb-0d692.

4D1 R1



Percent Moisture /l % 0.10 0.10 1.0

03/20/2007Page 18 of 44



Client Sample ID:


039069/002 1600

039069/002 1355

Date 7eceiRev:

Date Samdpev:

500-3900-931aL Sample ID:Fb-0d6d0.

4D1 R1



Percent Moisture B5 % 0.10 0.10 1.0

03/20/2007Page 19 of 44



Client Sample ID:


039069/002 1600

039069/002 1B15

Date 7eceiRev:

Date Samdpev:

500-3900-9P1aL Sample ID:Fb-0d6d3.

4D1 R1



Percent Moisture 1l % 0.10 0.10 1.0

03/20/2007Page 20 of 44



Client Sample ID:


039069/002 1600

039069/002 1B30

Date 7eceiRev:

Date Samdpev:

500-3900-9B1aL Sample ID:Fb-0963.

4D1 R1




03/20/2007Page 21 of 44



Client Sample ID:


039069/002 1600

039069/002 1B35

Date 7eceiRev:

Date Samdpev:

500-3900-9h1aL Sample ID:Fb-096B.

4D1 R1



Percent Moisture B1 % 0.10 0.10 1.0

03/20/2007Page 22 of 44



Client Sample ID:


039069/002 1600

039069/002 1BB0

Date 7eceiRev:

Date Samdpev:

500-3900-971aL Sample ID:Fb-09699.

4D1 R1




03/20/2007Page 23 of 44



Client Sample ID:


039069/002 1600

039069/002 1BB5

Date 7eceiRev:

Date Samdpev:

500-3900-d01aL Sample ID:Fb-09695.

4D1 R1



Percent Moisture BB % 0.10 0.10 1.0

03/20/2007Page 24 of 44



Client Sample ID:


039069/002 1600

039069/002 1B55

Date 7eceiRev:

Date Samdpev:

500-3900-d91aL Sample ID:Fb-09697.

4D1 R1




03/20/2007Page 25 of 44



Client Sample ID:


039069/002 1600

039069/002 1515

Date 7eceiRev:

Date Samdpev:

500-3900-dd1aL Sample ID:Fb-096d3.

4D1 R1




03/20/2007Page 26 of 44



Client Sample ID:


039069/002 1600

039069/002 1/00

Date 7eceiRev:

Date Samdpev:

500-3900-d31aL Sample ID:Sb-903Qb

4D1 R1

100Percent Sopivs:




PC<-1016 416 ug9Kg 5.3 16 1.0PC<-1//1 416 ug9Kg B.B 16 1.0PC<-1/3/ 416 ug9Kg B.3 16 1.0PC<-1/B/ 416 ug9Kg B.2 16 1.0PC<-1/B8 416 ug9Kg 3.B 16 1.0PC<-1/5B 416 ug9Kg 3.5 16 1.0PC<-1/60 416 ug9Kg 3.1 16 1.0PC<-1/68 416 ug9Kg 16 16 1.0Popychporinatev bidhenyps, Totap 416 ug9Kg 3.1 16 1.0

Surrogate Accedtance Limits3l - 11522 %Tetrachporo-m-xypeneB2 - 116l/ %DC< Decachporobidhenyp


Percent Moisture 0.B2 % 0.10 0.10 1.0

03/20/2007Page 27 of 44



Client Sample ID:


039069/002 1600

039069/002 1/00

Date 7eceiRev:

Date Samdpev:

500-3900-dP1aL Sample ID:Sb-90PQb

4D1 R1

100Percent Sopivs:




PC<-1016 416 ug9Kg 5.B 16 1.0PC<-1//1 416 ug9Kg B.B 16 1.0PC<-1/3/ 416 ug9Kg B.3 16 1.0PC<-1/B/ 416 ug9Kg B.2 16 1.0PC<-1/B8 11 J ug9Kg 3.B 16 1.0PC<-1/5B 416 ug9Kg 3.5 16 1.0PC<-1/60 416 ug9Kg 3./ 16 1.0PC<-1/68 416 ug9Kg 16 16 1.0Popychporinatev bidhenyps, Totap 11 J ug9Kg 3./ 16 1.0

Surrogate Accedtance Limits3l - 115l2 %Tetrachporo-m-xypeneB2 - 116103 %DC< Decachporobidhenyp


Percent Moisture 0.3/ % 0.10 0.10 1.0

03/20/2007Page 28 of 44



Client Sample ID:


039069/002 1600

039069/002 1/00

Date 7eceiRev:

Date Samdpev:

500-3900-d51aL Sample ID:Sb-902Qb

4D1 R1

l8Percent Sopivs:


4et'oM: Date Anapyzev: 039129/002 161lh0hd


PC<-1016 416 ug9Kg 5.B 16 1.0PC<-1//1 416 ug9Kg B.5 16 1.0PC<-1/3/ 416 ug9Kg B.B 16 1.0PC<-1/B/ 416 ug9Kg B.8 16 1.0PC<-1/B8 416 ug9Kg 3.5 16 1.0PC<-1/5B 416 ug9Kg 3.6 16 1.0PC<-1/60 416 ug9Kg 3./ 16 1.0PC<-1/68 416 ug9Kg 16 16 1.0Popychporinatev bidhenyps, Totap 416 ug9Kg 3./ 16 1.0

Surrogate Accedtance Limits3l - 11585 %Tetrachporo-m-xypeneB2 - 11610B %DC< Decachporobidhenyp


Percent Moisture /.0 % 0.10 0.10 1.0

03/20/2007Page 29 of 44



Client Sample ID:


039069/002 1600

039059/002 1/00

Date 7eceiRev:

Date Samdpev:

500-3900-d21aL Sample ID:Sb-90BQb

4D1 R1

100Percent Sopivs:




PC<-1016 412 ug9Kg 5.6 12 1.0PC<-1//1 412 ug9Kg B.6 12 1.0PC<-1/3/ 412 ug9Kg B.5 12 1.0PC<-1/B/ 412 ug9Kg B.l 12 1.0PC<-1/B8 412 ug9Kg 3.6 12 1.0PC<-1/5B 412 ug9Kg 3.2 12 1.0PC<-1/60 412 ug9Kg 3.3 12 1.0PC<-1/68 412 ug9Kg 12 12 1.0Popychporinatev bidhenyps, Totap 412 ug9Kg 3.3 12 1.0

Surrogate Accedtance Limits3l - 11586 %Tetrachporo-m-xypeneB2 - 116l8 %DC< Decachporobidhenyp



03/20/2007Page 30 of 44

ANLNYTIC TLREPYOSNeRvRITr


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03/20/2007Page 31 of 44

ANLYTIC REPIOEY OSeNYIe

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03/20/2007Page 32 of 44

ANLYTIC REPIOEY SevNYIv


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l9obA nWWaggnWGlyagWRhggdGagkdnC jWjInWWakgWWaI Ll9obA nWWaggnWGlyagWjhIdna.dkC jWjInWWakgWWak Ll9obA nWWaggRWIlyagWjhnaRC jWjInWWakgWWa. Ll9obA nWWaggnWGlyagWjhRajdnC jWjInWWakgWWan Ll9obA nWWaggnWGlyagWjhgWagIdkC jWjInWWakgWWaG Ll9obA nWWaggnWGlyagWkMy jWjInWWakgWWaIk Ll9obA nWWaggnWGlyagW.My jWjInWWakgWWaI. Ll9obA nWWaggnWGlyagWGMy jWjInWWakgWWaIn Ll9obA nWWaggnWGlyagWRMy jWjInWWakgWWaIG L

SeiEOI >LvTv

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03/20/2007Page 33 of 44





SeiEOI>LvTv

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rPLYCvTv >LIn;BCDDEFFGIFl9obA@yaWIhkC raIIgGnWWakgWWa/ Ll9obA@yaWIhGC raIIgGnWWakgWWagW Ll9obA@yaWIhggC raIIgGnWWakgWWagg Ll9obA@yaWIhgGC raIIgGnWWakgWWagI Ll9obA@yaWIhIWC raIIgGnWWakgWWagk Ll9obA@yaWIhIkC raIIgGnWWakgWWag. Ll9obA@yaWghkC raIIgGnWWakgWWagR Ll9obA@yaWghRC raIIgGnWWakgWWagj Ll9obA@yaWghggC raIIgGnWWakgWWag/ Ll9obA@yaWghgnC raIIgGnWWakgWWaIW Ll9obA@yaWghg/C raIIgGnWWakgWWaIg Ll9obA@yaWghIkC raIIgGnWWakgWWaII L

rPLYCvTv >LIn;BCDDEFFGIIl9obAlyagWRhgWaggdGC 2 t1 Nu69b3uit nWWakgWWag L

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03/20/2007Page 34 of 44

Gary Deiiigyrn& iAisooctr&Dyo 1c0iS.W0yueiiik,,IL6,,I6

Client SamptImeSD:AletA

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Qfa/SrUQoD:5U

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k,,IL6,,IL 85I6,3b-NkI9NL: ,iiig ,iiig

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k,,IL6,,I-k 85I6,m25 6,9iii 3kiii

k,,IL6,,I-m 85I6,J25 /3iii 3miii

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k,,IL6,,I678g 85I6,Jb6,I66Nm: ,iiig ,iiig

RG8ik,,I66k,mv-Iss 6,kiii Jmiii

RG8ik,,I66J,-v-Iss m/iii JJiii

RG8gik,,I66J,-vLIss

J/iii 3kiii

75ik,,I66k,mv6Iss /kiii JLiii

75ik,,I66J,-v6Iss Jkiii J3iii

3i9S1iLbe:SBfSSSSSSSSSSSSSSSSSSSSSSSSaen:ptS1iLbe:S

1lIIm6it:SD:5m,:I SD:bmIt

aen:ptS2itIn.4SSS1men'

1lIIm6it: M55:btip5:S3nLntA

dgG5i6pdlPytp

9JiIi66mgG5igyt&tCacuc0rMCy xadzGBi6pdlPytp

L/iIi66kzyDu&tCacucIWI<xay y

103Sahn5i6m 03/20/2007Page 35 of 44


Job Number: 500-3900-91Dseci: pestnc W akkogsniek

SoDsl1Dseci Fnirs&:

9A0psDuisoc:

pnie acnD.Gel:

,nb SnmIDe Lp:

036986y008 900R

reInEt aYLPb o aLIins ,cco..,c;

pnie hreInrel:

Lckirumeci Lp:

,nb dsDe Lp:

LcsisnD CestPi6joDume:

dscnD CestPi6joDume:

LcMegisoc joDume:

acnD.ksk wnigP: 500-99R0@

hreI wnigP: 500-9950/

036936y008 0R0@

039508y32909Al

95A000 t

5A0 m,

7csik: ut6Tt

1oDumc Lp: hqLFaqf

reInEts <c<=>Oe?LOLITEPs @,A.

Eh /R@0N #1Fw 500-9950/69-aa

acnD.ie qekuDi zunD Fp, q,

498 985A/h1w-909/498 98BA/h1w-9yy9498 98BA5h1w-9y3y498 98BA@h1w-9yBy498 983A/h1w-9yBR498 983A8h1w-9y5B498 983A3h1w-9y/0498 9898h1w-9y/R498 983A3hoD.gPDorscniel bsIPec.DkU voinD

Surrotnie ( qeg aggeIincge ,smsik

veirngPDoro-m-&.Dece 83 3@ - 995p1w pegngPDorobsIPec.D @5 B8 - 99/

SoDsl

9A0

036986y008 9030pnie acnD.Gel:

BLC REPIOEY D?Tbe o aLIins ,cco..,c;

1Dseci Fnirs&:

,nb SnmIDe Lp:

psDuisoc:

pnie hreInrel:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:

039508y3290yAl

036936y008 0R0@



95A000 t

5A0 m,

7csik: ut6Tt

1oDumc Lp: hqLFaqf


Eh /R@0N #1,1S 500-9950/6y-aa

acnD.ie zunD,smsi( qegAqekuDiSIs)e amouci

9/8 9/@ 909 BR - 993h1w-909/9/8 989 90y /y - 998h1w-9y/0


veirngPDoro-m-&.Dece 8/ 3@ - 995

p1w pegngPDorobsIPec.D 905 B8 - 99/

DEB RnTiLFE

1nDguDnisock nre Ierxormel bexore rouclsct io nbosl roucl-oxx errork sc gnDguDniel rekuDikA

03/20/2007Page 36 of 44



pnie acnD.Gel:

pnie acnD.Gel:

psDuisoc:

psDuisoc:

0369R6y008 0/03

0369R6y008 0/y5

SoDsl

rLIOTG D?TbeHrLIOTG D?Tbe IN?YTiLIe SeiEJeOC Se?EOI o aLIins ,cco..,c;

y0

y0

FS ,nb SnmIDe Lp:

FSp ,nb SnmIDe Lp:

1Dseci Fnirs&:

pnie hreInrel:

pnie hreInrel:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:

1oDumc Lp:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:

1oDumc Lp:

1Dseci Fnirs&: SoDsl



036936y008 0R0@

036936y008 0R0@



039508y329y/Al

95AB@3y t

5A0 m,

hqLFaqf

039508y329y8Al

95A9y5@ t

5A0 m,

hqLFaqf


Eh /R@0N #1

Eh /R@0N #1

500-3900-9

500-3900-9

acnD.ie FSp zunDFS zunDqhp ,smsiqhp,smsiFSpFS

( qegA

0 0 BR - 993 N1 30 p p dh1w-909/

0 0 /y - 998 N1 30 p ph1w-9y/0

Surrotnie FS ( qeg FSp ( qeg aggeIincge ,smsik

veirngPDoro-m-&.Dece 0 0 3@ - 995p pp1w pegngPDorobsIPec.D 0 0 B8 - 99/p p

DEB RnTiLFE


03/20/2007Page 37 of 44



SoDsl1Dseci Fnirs&:

9A0psDuisoc:

pnie acnD.Gel:

,nb SnmIDe Lp:

0369@6y008 9809

reInEt aYLPb o aLIins ,cco..Kc=

pnie hreInrel:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:


hreI wnigP: 500-9980y

0369/6y008 9/00

039@08y32098Al

95A000 t

5A0 m,

7csik: ut6Tt

1oDumc Lp: hqLFaqf


Eh /R@0N #1Fw 500-9980y69-aa

acnD.ie qekuDi zunD Fp, q,

498 985A/h1w-909/498 98BA/h1w-9yy9498 98BA5h1w-9y3y498 98BA@h1w-9yBy498 983A/h1w-9yBR498 983A8h1w-9y5B498 983A3h1w-9y/0498 9898h1w-9y/R498 983A3hoD.gPDorscniel bsIPec.DkU voinD


veirngPDoro-m-&.Dece 8R 3@ - 995p1w pegngPDorobsIPec.D 85 B8 - 99/

DEB RnTiLFE


03/20/2007Page 38 of 44



pnie acnD.Gel:

pnie acnD.Gel:

psDuisoc:

psDuisoc:

0369@6y008 98y3

0369@6y008 98B5

BLC REPIOEY D?TbeHBLC REPIOEY D?Tbe IN?YTiLIe SeiEJeOC Se?EOI o aLIins ,cco..Kc=

9A0

9A0

SoDsl

,1S ,nb SnmIDe Lp:

,1Sp ,nb SnmIDe Lp:

1Dseci Fnirs&:

pnie hreInrel:

7csik:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:

1oDumc Lp:

1Dseci Fnirs&: SoDsl

pnie hreInrel:

7csik:

Lckirumeci Lp:

,nb dsDe Lp:



LcMegisoc joDume:

1oDumc Lp:

ut6Tt

0369/6y008 9/00



039@08y3209RAl

95A000 t

5A0 m,

hqLFaqf

039@08y3209@Al

95A000 t

5A0 m,

hqLFaqf

ut6Tt

0369/6y008 9/00




Eh /R@0N #1

Eh /R@0N #1

,1S 500-9980y6y-aa

,1Sp 500-9980y63-aa

acnD.ie ,1Sp zunD,1S zunDqhp ,smsiqhp,smsi,1Sp,1S

( qegA

8/// BR - 993 95 30h1w-909/

8@/R /y - 998 9B 30h1w-9y/0

Surrotnie ,1S ( qeg ,1Sp ( qeg aggeIincge ,smsik

veirngPDoro-m-&.Dece 88 R5 3@ - 995p1w pegngPDorobsIPec.D /@ 8@ B8 - 99/

DEB RnTiLFE


03/20/2007Page 39 of 44



(7csik:

SoDsl

psDuisoc: 9A0

pnie acnD.Gel:

IN?YTiLIe o aLIins ,cco..;==

,nb SnmIDe Lp:

1Dseci Fnirs&:

pnie hreInrel:

0369B6y008 9/9/

Lckirumeci Lp:

,nb dsDe Lp:



acnD.ksk wnigP: 500-99/yy

hreI wnigP: N6a

N6a

reInEts >eOiePIrETvINOe>Oe?LOLITEPs LHM

N6a

No cdusImeci akkstcel500-3900-9

acnD.ie zunD,smsiqhpqekuDiSnmIDe qekuDi6zunD

@yAy@y 0 y0hergeci SoDslk

DEB RnTiLFE


03/20/2007Page 40 of 44

03/20/2007Page 41 of 44

03/20/2007Page 42 of 44

03/20/2007Page 43 of 44

ANLYTIC REAPIOPSPYEeISvPSrIAYCe


ntabois, ec.cT Ss;;a,o

As<i,ITt;=a>? I@ABBI

S5lb951ubFbu&e buA te.53eN9uep 53it le9tGeb,ep 53it lGeb3e5ue9tes o9.es51I:t9iNlLti

LA e199o t63e1i3u9l&e3 5oGeb,e8t 3 NuGeb3ebNu51uy R5o3

LA e199o te9te35p8o 3el9eN9ue588 5teu9eA5F es Ne19p8t9pb3 le9teu5p8 t le.buAyLti

h5p8o 3e. t et 1 bF le9Neb1 y kynGkydGCygLti

J99o teL p8 t5uit eb3e511 8u5so y Lti

J99o teL p8 t5uit eb3et 19tl ly Lti

JPJeb3e8t 3 Nuy Lti

JPJeb3e,boo le9iuebNebNIe5Nleo :bso y Lti

JPJeb3e,boo le9iue.buAe5ooe8 tubN NuebN,9tp5ub9Ny Lti

LA t e5t eN9elb31t 85N1b 3es u. NeuA e35p8o ejr3e9NeuA e19Nu5bN t3e5NleuA eJPJy

Lti

h5p8o 3e5t et 1 bF le.buAbNeM9olbN:eLbp y Lti

h5p8o e19Nu5bN t3eA5F eo :bso eo5s o3y Lti

J9Nu5bN t3e5t eN9uest9I Ne9teo 5IbN:y Lti

h5p8o e19oo 1ub9Nel5u wubp 3e5t e8t9Fbl ly Lti

-88t98tb5u e35p8o e19Nu5bN t3e5t ei3 ly Lti

h5p8o es9uuo 3e5t e19p8o u o&e,boo ly Lti

LA t eb3e3i,,b1b NueF9oye,9te5ooet @i 3u le5N5o&3 3GebN1oye5N&et @i 3u le/hw/hr3Lti

2P-e35p8o eFb5o3el9eN9ueA5F eA 5l3851 e9tesisso eb3e7TppeqgwCfEebNelb5p u tyLti

j,eN 1 335t&Ge3u5,,eA5F es NebN,9tp le9,e5N&e3A9tueA9oleubp e9te@ib1IeL-LeN l3Lti

/ioub8A53b1e35p8o 3e5t eN9ue8t 3 Nuy Lti

h5p8o 3el9eN9uet @ibt e38obuubN:e9te19p893bubN:y Lti

CeAISCiDE<s03/20/2007Page 44 of 44

ANALYTICAL REPORT


Job Description: Waukegan Slip 3

For:

Deigan & Associates

900 S. Genesee St.

Waukegan, IL 60085

Attention: Gary Deigan

Rric A. Lang

hrodect Canager II

elangPstl-inc.com

03j11j100M

w@ese test results meet all t@e re/uirements o2 NRLA7 2or accreTiteT parameters.

w@e Lab 7erti2ication IDq is 900109.

All /uestions regarTing t@is test report s@oulT be TirecteT to t@e SwL hrodect Canager f@ose signature appears on t@is report. All pages o2 t@is report are integral parts o2 t@e analytical Tata. w@ere2ore, t@is report s@oulT be reproTuceT only in its entirety.

Eeporting limits are aTdusteT 2or sample si#e useT, Tilutions anT moisture content i2 applicable.

hrodect Canager: Eic@arT 7 Wrig@t

SwL 7@icago 1z9M 4onT Street, BniUersity hark, IL 60z66wel vM08( 53z-5100 Fa) vM08( 53z-5199 fff.stl-inc.com


Page 1 of 20

Case Narrative 1.....................................................................................................

Chain of Custody 2................................................................................................

Sample Data Summary Package - Geotechnical 6..............................................

Sample Handling 11.................................................................................................

Last Page of this Document 16...............................................................................

Page 3 of 20

Case Narrative

1Page 4 of 20

Chain of Custody

2Page 6 of 20

3Page 7 of 20

4Page 8 of 20

5Page 9 of 20

Sample Data Summary Package - Geotechnical

6Page 10 of 20

7Page 11 of 20

8Page 12 of 20

9Page 13 of 20

10Page 14 of 20

Sample Handling

11Page 15 of 20

12Page 16 of 20

13Page 17 of 20

14Page 18 of 20

15Page 19 of 20

Last Page of this Document

16Page 20 of 20

ANALYTICAL REPORT

Job Number: 500-391D-1

Job secirptnpoW: akugeSkW lFpt 3

&or:

sepSkW A .ccoipknec

900 lG ,eWecee lnG

akugeSkWI L6 D0085

.nneWnpoW: ,kry sepSkW

Rrpi .G 6kWS

hrodein CkWkSer LL

eFkWSPcnF-pWiGiom

03j11j100M

w@ece necn recuFnc meen kFF n@e re/upremeWnc o2 NR6.7 2or kiireTpneT tkrkmenercG

w@e 6kb 7ernp2piknpoW Lsq pc 900109G

.FF /uecnpoWc reSkrTpWS n@pc necn retorn c@ouFT be TpreineT no n@e lw6 hrodein CkWkSer f@oce cpSWknure kttekrc oW n@pc retornG .FF tkSec o2 n@pc retorn kre pWneSrkF tkrnc o2 n@e kWkFynpikF TknkG w@ere2oreI n@pc retorn c@ouFT be retroTuieT oWFy pW pnc eWnprenyG

EetornpWS Fpmpnc kre kTducneT 2or ckmtFe cp#e uceTI TpFunpoWc kWT mopcnure ioWneWn p2 kttFpikbFeG

hrodein CkWkSer: Epi@krT 7 arpS@n

lw6 7@pikSo 1z9M 4oWT lnreenI BWpUercpny hkrgI L6 D0zDDweF vM08( 53z-5100 &k) vM08( 53z-5199 fffGcnF-pWiGiom


Page 1 of 14

Case Narrative 1.....................................................................................................

Chain of Custody 2................................................................................................

Sample Data Summary Package - Geotechnical 4..............................................

Sample Handling 7.................................................................................................

Last Page of this Document 10...............................................................................

Page 3 of 14

Case Narrative

1Page 4 of 14

Chain of Custody

2Page 6 of 14

3Page 7 of 14

Sample Data Summary Package - Geotechnical

4Page 8 of 14

5Page 9 of 14

6Page 10 of 14

Sample Handling

7Page 11 of 14

8Page 12 of 14

9Page 13 of 14

Last Page of this Document

10Page 14 of 14

ANALYTICAL REPORT

Job Number: 500-391D-9

Job secirptnpoW: akugeSkW lFpt 3

&or:

sepSkW A .ccoipknec

900 lG ,eWecee lnG

akugeSkWI L6 D0085

.nneWnpoW: ,kry sepSkW

Rpihkrd C arpShn

Projein MkWkSer LL

rwrpShn@cnF-pWiGiom

03/92/1007

Thece necn recuFnc meen kFF nhe requpremeWnc of NE6.C for kiiredpned tkrkmenercG

The 6kb CernpfpiknpoW Ls# pc 900109G

.FF quecnpoWc reSkrdpWS nhpc necn retorn chouFd be dpreined no nhe lT6 Projein MkWkSer whoce cpSWknure kttekrc oW nhpc retornG .FF tkSec of nhpc retorn kre pWneSrkF tkrnc of nhe kWkFynpikF dknkG ThereforeI nhpc retorn chouFd be retroduied oWFy pW pnc eWnprenyG

RetornpWS Fpmpnc kre kdjucned for ckmtFe cpze ucedI dpFunpoWc kWd mopcnure ioWneWn pf kttFpikbFeG

Projein MkWkSer: Rpihkrd C arpShn

lT6 ChpikSo 1497 BoWd lnreenI UWpvercpny PkrgI L6 D04DDTeF (708) 534-5100 &kx (708) 534-5199 wwwGcnF-pWiGiom


03/19/2007Page 1 of 10

ANLYTICA LLNRE

Job Numeeer b:5Ne0e-3391b5u 3 D9secips tmeeenWWakgSlag

POSevrCAntaOeCboTniCAntaOeCbo POSevrCLnrsS,onrec.SteCAntaOe;

onrec.SteCRe<eS=e;

WkFWlFSWW&eeglWWWkFWAFSWW&eegWWW.GaWk,kInWWakgSlaS L9ob6

WkFWlFSWW&eeglSn WkFWAFSWW&eegWWW.GaWk,SWInWWakgSla8 L9ob6

A.TCP>S<n?@

03/19/2007Page 2 of 10

ANLYTIC IARTEA

AETCPOSevrn

03/19/2007Page 3 of 10



Client Sample ID:


03/08/9002 1000

03/06/9002 1600

Date 7eceiRev:

Date Samdpev:

500-391L-1baB Sample ID:6,-0323.

4Db Rb

lpient PatriC: Sopiv

4et'oM: Date AnapyMev: 03/1x/9002 1610D-119L

zercent Poisture 3.5 B 0.10 0.10 1.0

03/19/2007Page 4 of 10



Client Sample ID:


03/08/9002 1000

03/06/9002 1695

Date 7eceiRev:

Date Samdpev:

500-391L-hbaB Sample ID:6,-03210.

4Db Rb

lpient PatriC: Sopiv

4et'oM: Date AnapyMev: 03/1x/9002 1610D-119L

zercent Poisture 1x B 0.10 0.10 1.0

03/19/2007Page 5 of 10

ANLYTIC REPIOEY OSeNYIe

eIY Rvrntab

03/19/2007Page 6 of 10





SeiEOI>LvTv

?ePeOLY R;eaTvIOC

rPLYCvTv >LIn;@ABBCDDEFDF9ob&A.aWkGk, raSSglnWWakgSlaS IF9ob&A.aWkGSW, raSSglnWWakgSlaL I

SeiEOI >LvTv

Ie6eI9u5o

tGb R;TnLHE

03/19/2007Page 7 of 10


Job Nboumer:5o0-53-09e01-D5s-9e0-50eNrDmrc5ue5oiemD50eNrDpe995-00e0:5mr5 ob Nbou-D50-:Nbu:t

03/19/2007Page 8 of 10

03/19/2007Page 9 of 10

ANLYTIC REAPIOPSPYEeISvPSrIAYCe


ntabois, ec.cT Ss;;a,o

As<i,ITt;=a>? I@ABCI

F5&b951ubAbu.e buG te,53eN9uep 53it &e9tIebLep 53it &Ieb3e5ue9tes o9,es516:t9iN&8ti

8G e199o ty3e1i3u9&.e3 5oIebLeRt 3 NuIeb3ebNu51uh d5o3

8G e199o te9te35pRo 3e&9eN9ue5RR 5teu9eG5A es Ne19pRt9pb3 &e9teu5pR t &e,buGh8ti

C5pRo 3e, t et 1 bA &e9Neb1 h khk8ti

J99o te8 pR t5uit eb3e511 Ru5so h 8ti

J99o te8 pR t5uit eb3et 19t& &h 8ti

JPJeb3eRt 3 Nuh 8ti

JPJeb3eLboo &e9iuebNebN6e5N&eo :bso h 8ti

JPJeb3eLboo &e9iue,buGe5ooeR tubN NuebNL9tp5ub9Nh 8ti

8G t e5t eN9e&b31t R5N1b 3es u, NeuG e35pRo ejr3e9NeuG e19Nu5bN t3e5N&euG eJPJh

8ti

C5pRo 3e5t et 1 bA &e,buGbNeM9o&bN:e8bp h 8ti

C5pRo e19Nu5bN t3eG5A eo :bso eo5s o3h 8ti

J9Nu5bN t3e5t eN9uest96 Ne9teo 56bN:h 8ti

C5pRo e19oo 1ub9Ne&5u wubp 3e5t eRt9Ab& &h 8ti

-RRt9Rtb5u e35pRo e19Nu5bN t3e5t ei3 &h 8ti

C5pRo es9uuo 3e5t e19pRo u o.eLboo &h 8ti

8G t eb3e3iLLb1b NueA9oheL9te5ooet @i 3u &e5N5o.3 3IebN1ohe5N.et @i 3u &e/Cw/Cr38ti

2P-e35pRo eAb5o3e&9eN9ueG5A eG 5&3R51 e9tesisso eb3e7lppeTgwqfEebNe&b5p u th8ti

jLeN 1 335t.Ie3u5LLeG5A es NebNL9tp &e9Le5N.e3G9tueG9o&eubp e9te@ib16e8-8eN &38ti

/ioubRG53b1e35pRo 3e5t eN9ueRt 3 Nuh 8ti

C5pRo 3e&9eN9uet @ibt e3RobuubN:e9te19pR93bubN:h 8ti

CeAISDiEF<s03/19/2007Page 10 of 10

j3099-1 stl level 2 portrait smp sort final reportjob number: 500-3099-1 job description: waukegan...

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