international collaborative exercises (ice) · 2019-12-18 · sm-4 (lidocaine) (procaine) (cocaine)...

INTERNATIONAL COLLABORATIVE

EXERCISES (ICE)

ICE

20

19

/1

Summary Report

ICE Round 2019/1

SEIZED MATERIALS

International Collaborative Exercises (ICE)

Summary report 2019/1-Seized Materials

Copyright © 2019 UNODC

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ICE 2019/1-SM

Final summary report for ICE 2019/1 Seized Materials Test Group

Original language: English

© United Nations, December 2019. All rights reserved, worldwide.

The designations employed and the presentation of material in this publication do not imply the expression of

any opinion whatsoever on the part of the Secretariat of the United Nations concerning the legal status of any

country, territory, city or area, or of its authorities, or concerning the delimitation of its frontiers or boundaries.

This publication has not been formally edited.




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ICE 2019/1-SM

Acknowledgements

The Laboratory and Scientific Section (LSS) of the UNODC, headed by Dr. Justice Tettey, wishes to express its

appreciation and thanks to all laboratories for participating in the International Collaborative Exercises (ICE)

round 2019/1.

The valuable comments and contribution from the following members of the International Panel of Forensic

Experts are gratefully acknowledged:

Mr. Benoit Archambault, Health Canada, Canada

Mr. Elvio Dias Botelho, Brazilian Federal Police, Brazil

Prof. Heesun Chung, Chungnam National University, Republic of Korea

Prof. Niamh Nic Daéid, University of Dundee, Scotland, UK

Mr. Scott Oulton, Drug Enforcement Administration, USA

Ms. Catherine Quinn, Victoria Police, Australia

Prof. Franco Tagliaro, University of Verona, Italy

Dr. Angeline Tiong Whei Yap, Health Sciences Authority, Singapore

In addition, LSS would like to acknowledge the valuable contribution of the Chemical Metrology Laboratory of

the Health Sciences Authority, Singapore, for the provision of specific software used for the quantitative

statistical calculations in the ICE programme.

The ICE is coordinated by Ms. Yen Ling Wong, Scientific Affairs Officer, a staff member of LSS. The assistance

and the contributions of the following LSS staff members are gratefully acknowledged.

Dr. Conor Crean, Scientific Affairs Officer

Mr. Joao Rodrigues, Scientific Affairs Officer

Ms. Romana Luger, Research Assistant

Dr. Natalia Ivanova, Research Assistant

Dr. Gerd Krapf, Laboratory Technician

Mr. Michael Bell, Laboratory Technician

Ms. Mikaela Edwards, Individual Contractor

For additional information or comments, please contact:

Ms. Yen Ling Wong

ICE Coordinator

Scientific Affairs Officer

Laboratory and Scientific Section

UNODC, Vienna International Centre

Wagramer Strasse 5, P.O. Box 500

A-1400, Vienna, AUSTRIA

Email: [email protected]




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ICE 2019/1-SM

Contents

1. Codes and Abbreviations ..............................................................................................................................4

2. Test samples information .............................................................................................................................5

3. Introduction ..................................................................................................................................................6

4. Comments from the International Panel of Forensic Experts ......................................................................7

5. New Psychoactive Substances (NPS) reported .............................................................................................9

6. Response summary for Test Sample-1 ...................................................................................................... 11




10. ANNEX 1: Participants’ results for Test Sample-1 ..................................................................................... 26







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ICE 2019/1-SM

1. Codes and Abbreviations

(+) “positive” Indicates that the analyte is identified; for presumptive tests (e.g. colour reactions), indicates

that a positive reaction was obtained.

(-) “negative” Indicates that the analyte is not identified.

(ANP) Analysis not performed.

Tech Code Name

140 Colorimetric reactions

141 Marquis reagent (sulphuric acid, formaldehyde)

142 Cobalt thiocyanate

150 Thin Layer Chromatography

160 High/Ultra High Performance Liquid Chromatography

161 High Performance Liquid Chromatography with diode array detection

170 Gas Chromatography NPD

171 Gas Chromatography FID

172 Gas Chromatography ECD

180 Gas Chromatography/Mass Spectrometry

190 Fourier Transform Infrared Spectrometry

200 Spectrophotometry (visible, UV)

210 Others (specify)

211 NMR

220 Microcrystal test

230 Liquid chromatography/mass spectrometry

231 Liquid chromatography/tandem mass spectrometry

250 Raman Spectroscopy




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ICE 2019/1-SM

2. Test samples information

The following four (4) test samples for the Seized Materials test group were prepared by the Laboratory and

Scientific Section, UNODC:

Test Sample-1 (SM-1)

SM-1 was prepared from a sample of Lidocaine and Procaine. The test sample also contained lactose.


SM-2 was prepared from a seizure containing 14.2% (w/w) Morphine base. The test sample also contained

traces of codeine, which was not considered in the evaluation.


SM-3 was prepared from a seizure containing 9.4% (w/w) Metamfetamine base. The test sample also

contained caffeine.


SM-4 was prepared from a seizure containing 14.4% (w/w) Cocaine base. The test sample also contained

lactose with ecgonine, methylecgonine, benzoylecgonine and cinnamoyl cocaine as minor components.

All test samples were prepared by preliminary grounding by mortar and pestle followed by homogenisation

using a centrifugal mill and a dry powder rotator. 230 mg of each test samples were weighed into glass vials.

For each test sample, sufficient homogeneity was assured and stability studies were carried out in accordance

with methods outlined in ISO 13258:2015 “Statistical methods for use in proficiency testing by interlaboratory

comparisons” and “The international harmonized protocol for the proficiency testing of analytical chemistry

laboratories”1.

____________________________________

1 Thompson, M., Ellison, S. L. and Wood, R., The International Harmonised Protocol for the Proficiency Testing of Analytical Chemistry Laboratories,

Pure Appl. Chem., 78 (1), 145-196, 2006.




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ICE 2019/1-SM

3. Introduction

An important element of the UNODC International Quality Assurance Programme (IQAP) is the

implementation of the International Collaborative Exercises (ICE). The exercises allow laboratories, from both

developing and developed countries to continuously monitor their performance in drug testing on a truly

global scale. This report provides information on analytical results of laboratories participating in the Seized

Materials (SM) test group. In order to maintain confidentiality, the participating laboratories have been

assigned random “Round Codes”, which change every round.

The analytical results returned by laboratories participating in ICE are evaluated by UNODC and a confidential

report is provided to each laboratory on its own performance. The overall analytical results are reviewed by

the UNODC’s International Panel of Forensic Experts which oversees the implementation of these exercises,

and offers guidance and support in addressing relevant quality issues. The exercises provide an overview of

the performance and capacity of participating laboratories and enable UNODC to tailor technical support in

the laboratory sector for greatest impact.

The ICE programme is a UNODC mandated activity and is implemented through regular budget funds and

through the UNODC Global Scientific and Forensic Programme – Support Project (GLOU54), which

operationalizes the forensic aspects of the UNODC Thematic Programme on Research, Trend Analysis and

Forensics". Figure 1 shows the growth of the programme in recent years for both the Seized Materials (SM)

and the Biological Specimens (BS) test groups.

Figure 1. Growth of the ICE programme (as of 6 November 2019)

66 62

77

94100 102

116

129 132 131

151159

179173

184 185

204 204 204195

222

26 2733

42 3747

5462 58 62

72 7486 90 95 92 96 97 93

8798

0

50

100

150

200

250

No

. o

f la

bo

rato

rie

s

ICE round

SM BS




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ICE 2019/1-SM

4. Comments from the International Panel of Forensic Experts

4.1 Participation of Laboratories in ICE round 2019/1

In the 2019/1 round of the ICE programme, results were submitted within both the Seized Materials (SM)

and Biological Specimens (BS) test groups by 258 laboratories in 81 countries. Within the SM test group,

there were 222 participating laboratories from 73 countries and within the BS test group, results were

submitted by 98 laboratories from 44 countries.

4.2 Qualitative Analysis

Colour tests (53% of participants) were the most commonly used screening technique for test samples in

the SM test group, while GC-MS (95% of participants) was the most commonly used technique for

identification/confirmation of the components in the test samples followed by FTIR (40% of participants).

The results for the qualitative identification of the controlled substances in the SM test group, the number

of false positive/negative results and the analyses not performed are shown in the table 1.

Table 1. Performance of participants in the 2019/1 round of ICE.

Test sample SM-1

SM-2

(Morphine)

SM-3

(Metamfetamine)

SM-4

(Cocaine) (Lidocaine) (Procaine)

Correct identification

by participants 97.7% 98.6% 98.1% 99.0% 100.0%

Number of false

positives 5 11 6 5

Number of false

negatives 2 1 2 2 0

Number of analyses

not performed 3 2 2 0 0

With regard to false negative results reported, there were a total of 7 (3 for SM-1, 2 for SM-2 and 2 for SM-

3). As for false positive results, there were a total of 27 false positive results (5 for SM-1, 11 for SM-2, 6 for

SM-3 and 5 for SM-4), which is a slight increase in number compared to the previous round. Laboratories

reporting false positive or false negative results should investigate the reasons for this and corrective

actions should be taken as soon as possible in order to continuously improve performance. There were a

total of 7 analyses not performed, the majority of which were for SM-1. ICE participants should note that

test samples can contain any of the substances in the ICE menu and screening and identification carried

out should take this into account.




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ICE 2019/1-SM

4.3 Quantitative Analysis

The number of participants who carried out quantitative analysis, 83 (37%) for SM-2, 117 (53%) for SM-3

and 150 (68%) for SM-4 continues to be encouraging. It is also encouraging that 154 (69%) participants in

the SM test group performed quantitation and of these, 116 (75%) quantified more than one substance

and 80 (52%) quantified all three test samples. It is understood that quantitative analysis of controlled

substances is often governed by local legislation and the requirements of prosecution. With regards to the

analytical techniques used by participants performing quantitation, 56% used GC-FID, 29% used

UPLC/HPLC-DAD and 24% used mass spectrometric methods (i.e. GC-MS, GC-MS-MS, LC-MS, LC-MS-MS).

z-scores obtained by participants in quantification are shown in table 2 below.

Table 2. Quantitative performance of participants in the 2019/1 round of ICE.

According to the recommendations in ISO 13528:2015, an unacceptable z-score is considered to give an

action signal and a questionable z-score is considered to give a warning signal. A single action signal or

warning signals in two successive rounds shall be taken that an anomaly has occurred that requires

investigation. Participants with z-scores outside acceptable limits should review their quantification

procedures as soon as possible.

The following 22 laboratories obtained a single action signal or warning signal in the two successive rounds

of 2018/2 and 2019/1 and shall take this as an anomaly, which requires further investigation: 0E49T9,

2MPUPL, 2XGWKJ, 2XXLPG, 54CQ2S, 5HWYZN, 6666WM, 9YCKGZ, BIA0EZ, BMPXHL, BWSSKK, E44WTB,

FFUFOA, GZFJAG, HP2FIF, I3H5RP, KAPAAS, KII7PP, LRPCVG, OIMJHC, PIRYEY and XPYAOU.

Of the 26 laboratories that obtained a single action or warning signal in ICE rounds 2018/1 and 2018/2

reported in the previous summary report, 24 participated in 2019/1 and 11 of these improved their

performance in quantitation. The following 13 laboratories also obtained an action or warning signal in

2019/1: 2MPUPL, 2XXLPG, 5HWYZN, BIA0EZ, BMPXHL, BWSSKK, E44WTB, FFUFOA, HP2FIF, I3H5RP,

LRPCVG, OIMJHC and XPYAOU.

Laboratories that need to perform quantitation routinely are encouraged to participate regularly in

external proficiency testing or collaborative exercises such as the ICE programme. This will enable

laboratories to assess the quality of their quantitative methods through the z-score values obtained. In

addition to the use of z-scores as a measure of performance in quantitation, participants are encouraged

to compare their results with the assigned values provided in individual quantification reports, to assess

the accuracy of their quantitative performance. Laboratories reporting false positive or false negative

results should investigate the root causes and corrective actions taken promptly in order to continuously

improve performance. Participation in the ICE programme also helps in monitoring the effect of corrective

actions.

z-score

Test sample

SM-2

(14.2% Morphine)

SM-3

(9.4% Metamfetamine)

SM-4

(14.4% Cocaine)

|z| ≤ 2.00, acceptable 84.3% 76.9% 82.0%

2.00 < |z| < 3.00, questionable 8.5% 8.6% 5.3%

|z| ≥ 3.00, unacceptable 7.2% 14.5% 12.7%




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ICE 2019/1-SM

5. New Psychoactive Substances (NPS) reported

During the 2019/1 round of ICE, participating laboratories provided information on NPS that had been

identified in their laboratories. In total there were 175 reports of 109 substances. 25% of the reported

substances were from the group of structurally unrelated compounds called “other substances”. This

was largely due to an increase in reporting of benzodiazepines such as etizolam and flualprazolam. The

second most common group reported was synthetic cathinones (23%) followed by synthetic

cannabinoids (22%) as shown in Figure 2.

Figure 2. NPS reported by ICE laboratories during the 2019/1 round of ICE

In terms of the mode of action of the NPS reported by ICE participants, the predominant substances

reported were stimulants (31%) followed by synthetic cannabinoid receptor agonists (SCRA) (22%) as

shown in Figure 3.

Figure 3. Mode of action of NPS reported by ICE participants in the 2019/1 round of ICE

Synthetic

cannabinoids

22%

Synthetic

cathinones

23%Other substances

25%

Phenethylamines

19%

Phencyclidine-

type substances

5%

Tryptamines

3%

Piperazines

3%

Synthetic

cannabinoid

receptor

agonists

22%

Stimulants

31%Hallucinogens

19%

Opioids

7%

Dissociatives

5%

Sedatives/

Hypnotics

13%

Others

3%




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ICE 2019/1-SM

NPS most commonly reported by laboratories participating in ICE 2019/1

The substances most often reported by ICE participants were the synthetic cathinone N-ethylhexedrone,

the benzodiazepine etizolam and the synthetic cannabinoid 5F-MDMB-PINACA.

For further details on these substances and others reported to the UNODC Early Warning Advisory, ICE

participants can log on to the UNODC ICE portal and select the icon for the Early Warning Advisory on

New Psychoactive substances as shown below.




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ICE 2019/1-SM

6. Response summary for Test Sample-1

The response summary of all 222 participating laboratories for the identification of SM-1:

Correct identification of Test Sample-1:

False positives for Test Sample-1 (techniques(s) used):

False negatives for Test Sample-1 with respect to Lidocaine (technique(s) used):

Round Code Tech Code

1F633N 180

FEKAVF 171, 180

False negatives for Test Sample-1 with respect to Procaine (technique(s) used):


3RF39E 180

Analysis not performed for Test Sample-1 with respect to either or both Lidocaine and Procaine:

Round Code

1W4YMX ANP

QMGORR ANP

SAKRI4 ANP

Frequency of use of screening, identification and quantification techniques:

Substance Name Number of laboratories Percentage

Lactose 111 50.0%

Lidocaine (Lignocaine) 217 97.7%

Procaine 219 98.6%

Round Code Substance Reported Tech Code

1W4YMX Ketamine 140, 171

A441YE Oxybuprocaine 180

DLFBGB Caffeine 180

FEKAVF Tolycaine 171, 180

LRPCVG Phenidemitrazine 161, 180

Test Sample-1: Response Summary

No of Participants: 222 (Qualitative); 0 (Quantitative)

Technique 140 141 142 150 160 161 170 171 180 190 200 210 211 230 231 250

Screening (No.) 72 88 78 17 1 1 2 9 70 18 0 2 0 2 1 7

(%) 32.4 39.6 35.1 7.7 0.5 0.5 0.9 4.1 31.5 8.1 0.0 0.9 0.0 0.9 0.5 3.2

Identification

(No.

24 10 9 34 6 10 3 29 210 89 2 1 2 5 10 7

(%) 10.8 4.5 4.1 15.3 2.7 4.5 1.4 13.1 94.6 40.1 0.9 0.5 0.9 2.3 4.5 3.2

Quantification (No.) 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0

(%) 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0




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False positives for Test Sample-2 (technique(s) used):

False negatives for Test Sample-2 with respect to Morphine (technique(s) used):


MYD9WU 180

TUVPUU 150

Analysis not performed for Test Sample-2 with respect to Morphine:

Round Code

SAKRI4 ANP

XNJQP7 ANP



Morphine 218 98.1%


33ZZO3 Metamfetamine* 180, 190

4YFBKI Acetylcodeine 180, 190

9YCKGZ 6-monoacetylmorphine 150, 180

A441YE Hydromorphone 180

DFTIVR Lidocaine 180

EGEENO Hydromorphone 230, 231

GFWFBO Lidocaine* 180

KFULE7 Caffeine 180, 190

QZZZGT Heroin 180

R5RPYM Butabarbital 180, 190

ZAOGZZ Caffeine 180, 190

* possible transcription error



Technique 140 141 142 150 160 161 170 171 180 190 200 210 211 230 231 250

Screening (No.) 72 88 78 17 1 1 2 9 70 18 0 2 0 2 1 7

(%) 32.4 39.6 35.1 7.7 0.5 0.5 0.9 4.1 31.5 8.1 0.0 0.9 0.0 0.9 0.5 3.2

Identification

(No.

24 10 9 34 6 10 3 29 210 89 2 1 2 5 10 7

(%) 10.8 4.5 4.1 15.3 2.7 4.5 1.4 13.1 94.6 40.1 0.9 0.5 0.9 2.3 4.5 3.2


(%) 0.0 0.0 0.0 0.0 9.6 15.7 0.0 47.0 18.1 0.0 0.0 0.0 1.2 3.6 3.6 0.0




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Z-Score Report per Sample per Substance:

Round: 2019/1

Substance: SM-2; Morphine

Robust average: 13.6%

UNODC value: 14.2%

Z-scores can be interpreted by participants in line with ISO 13528:2015*, section 9.4.2 as follows:

IzI ≤ 2.00 is considered to be acceptable

2.00 < IzI < 3.00 is considered to be questionable (or warning signal)

IzI ≥ 3.00 is considered to be unacceptable (or action signal)

A single action signal or warning signal in two successive rounds shall be taken that an anomaly has occurred that requires investigation.

*Note: newly applied interpretation of z-scores replacing ISO 13528:2005, section 7.4.2




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Z-Scores for Test Sample-2

Code

Morphine

Code

Morphine

Concentration (mass%)

Deviation from robust

average z-score Concentration

(mass%)


average z-score

9SMHJ8 5.8 -7.8 -3.54 4YFBKI 13.7 0.1 0.06 LAWTLL 6.5 -7.1 -3.23 2TCPHH 13.8 0.2 0.07 GZFJAG 8.0 -5.6 -2.53 KII7PP 14.0 0.4 0.18 BIA0EZ 8.1 -5.5 -2.52 F3LSGY 14.0 0.4 0.18 BMPXHL 8.7 -4.9 -2.24 YHKKKB 14.0 0.4 0.18 1F633N 8.9 -4.7 -2.14 QQTH7B 14.0 0.4 0.18 FFUFOA 9.7 -3.9 -1.77 L75533 14.0 0.4 0.18 FIAC2C 9.9 -3.7 -1.70 ZFFBFT 14.0 0.4 0.18 6YZTRZ 10.4 -3.2 -1.46 C5MUOL 14.0 0.4 0.18 OHJX22 10.6 -3.0 -1.38 BWSSKK 14.3 0.7 0.32 Y7M3HZ 10.8 -2.9 -1.30 TTTILP 14.3 0.7 0.32 AZUH8X 10.8 -2.8 -1.28 KTBSBL 14.4 0.8 0.36 QPTTIT 11.3 -2.4 -1.07 7WA60O 14.4 0.8 0.36 33ZZO3 11.8 -1.8 -0.80 DUCT4E 14.4 0.8 0.36 YL2O3B 11.9 -1.7 -0.77 8FXHXS 14.4 0.8 0.36 FVP0OM 11.9 -1.7 -0.77 5Q555E 14.4 0.8 0.36 AMRMTF 12.0 -1.6 -0.73 GQQTND 14.4 0.8 0.37 MELOFZ 12.0 -1.6 -0.73 ZUZ1ZZ 14.5 0.9 0.41 S8TL74 12.0 -1.6 -0.73 AC11BX 14.6 1.0 0.45 K1NKKG 12.0 -1.6 -0.73 OHKWWZ 14.7 1.1 0.50 4J4R44 12.1 -1.5 -0.68 MJRX8A 14.8 1.2 0.54 SG5IQS 12.2 -1.4 -0.65 BZDD95 15.0 1.4 0.63 0OGHZR 12.3 -1.3 -0.59 E44WTB 15.2 1.6 0.74 CJWQGK 12.4 -1.3 -0.57 M9N99Q 15.4 1.8 0.81 QHQQUK 12.4 -1.2 -0.55 BRFRWM 15.6 2.0 0.91 TAAFSW 12.5 -1.1 -0.50 SDJTNO 15.6 2.0 0.91 PKPTJM 12.5 -1.1 -0.50 XM00GQ 15.8 2.2 0.99 6RFSER 12.6 -1.0 -0.46 KNHLNG 15.9 2.3 1.03 GI4HGG 12.7 -0.9 -0.41 CYLW4Y 15.9 2.3 1.04 ZIGGI6 12.8 -0.8 -0.36 RZDQQQ 16.1 2.5 1.13 EGEENO 12.9 -0.7 -0.32 INI2AA 17.0 3.4 1.54 5E0FMO 13.0 -0.6 -0.27 9YCKGZ 17.6 4.0 1.79 N64P66 13.0 -0.6 -0.27 N4VGXV 17.7 4.1 1.84 HHHNYB 13.0 -0.6 -0.27 252CCB 18.0 4.4 1.99 W4X1SX 13.1 -0.5 -0.24 LRPCVG 18.2 4.6 2.09 PWZDFG 13.1 -0.5 -0.23 6666WM 18.9 5.3 2.40 6JFAWA 13.1 -0.5 -0.23 8WWDBW 20.0 6.4 2.90 4CNIOX 13.1 -0.5 -0.23 5HWYZN 21.7 8.1 3.67 0E49T9 13.1 -0.5 -0.23 PIRYEY 21.9 8.3 3.78 INNQNN 13.4 -0.2 -0.09 B3FTN3 25.6 12.0 5.45 7MM6GH 13.5 -0.1 -0.05 HP2FIF 35.0 21.4 9.71 QEJKPA 13.7 0.1 0.04




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False negatives for Test Sample-3 with respect to Metamfetamine (technique(s) used):


TUVPUU 150

XNJQP7 140, 171

Analysis not performed for Test Sample-3 with respect to Metamfetamine:

All participating laboratories carried out analysis for Metamfetamine



Caffeine 207 93.2%

Metamfetamine 220 99.0%


33ZZO3 Morphine* 180, 190

A441YE Dimethylamphetamine 180

FEKAVF 4-Benzyloxy-N-methylamphetamine 171, 180


XNJQP7 Mephedrone 140, 171

YAIDDI Amfetamine 180




Technique 140 141 142 150 160 161 170 171 180 190 200 210 211 230 231 250

Screening (No.) 72 88 78 17 1 1 2 9 70 18 0 2 0 2 1 7

(%) 32.4 39.6 35.1 7.7 0.5 0.5 0.9 4.1 31.5 8.1 0.0 0.9 0.0 0.9 0.5 3.2

Identification

(No.

24 10 9 34 6 10 3 29 210 89 2 1 2 5 10 7

(%) 10.8 4.5 4.1 15.3 2.7 4.5 1.4 13.1 94.6 40.1 0.9 0.5 0.9 2.3 4.5 3.2


(%) 0.0 0.0 0.0 0.0 8.5 17.9 0.0 49.6 15.4 0.0 0.0 0.0 1.7 1.7 4.3 0.0




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Round: 2019/1

Substance: SM-3; Metamfetamine


UNODC value: 9.4%










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Code

Metamfetamine

Code

Metamfetamine




(mass%)


average z-score

1F633N 3.8 -5.3 -7.99 444444 9.0 -0.1 -0.25 LAWTLL 4.8 -4.3 -6.56 4YFBKI 9.0 -0.1 -0.20 2F51LA 4.8 -4.3 -6.50 RH08SD 9.0 -0.1 -0.19 Y7M3HZ 5.0 -4.2 -6.27 ZWM2QG 9.1 0.0 -0.15 BIA0EZ 5.5 -3.6 -5.46 QPTTIT 9.1 0.0 -0.13 OIMJHC 5.5 -3.6 -5.40 GQQTND 9.1 0.0 -0.13 GNTW2Z 7.0 -2.1 -3.25 OHKWWZ 9.1 0.0 -0.10 KII7PP 7.4 -1.7 -2.69 KC4CO7 9.1 0.0 -0.10 BZDD95 7.4 -1.7 -2.63 AC11BX 9.1 0.0 -0.10 0E49T9 7.5 -1.6 -2.48 8FXHXS 9.1 0.0 -0.10 54CQ2S 7.7 -1.4 -2.21 MYD9WU 9.1 0.0 -0.10 4J4R44 7.9 -1.2 -1.86 5Q555E 9.1 0.0 -0.10 QQ7VFQ 8.0 -1.1 -1.74 KFULE7 9.2 0.1 -0.03 MELOFZ 8.0 -1.1 -1.74 KNHLNG 9.2 0.1 0.00 OKWXFO 8.0 -1.1 -1.74 OHJX22 9.2 0.1 0.03 AMRMTF 8.1 -1.0 -1.57 0OGHZR 9.2 0.1 0.05 N4VGXV 8.1 -1.0 -1.57 QEJKPA 9.2 0.1 0.05 5HWYZN 8.2 -0.9 -1.44 PKPTJM 9.2 0.1 0.05 1999Y6 8.2 -0.9 -1.38 NGGZGG 9.2 0.1 0.11 V6ESR5 8.5 -0.6 -1.05 INNQNN 9.3 0.2 0.20 GZFJAG 8.5 -0.6 -1.01 F3LSGY 9.3 0.2 0.20 ZFFBFT 8.5 -0.6 -0.99 TTTILP 9.3 0.2 0.20 S8TL74 8.6 -0.5 -0.84 C5MUOL 9.3 0.2 0.20 R5RPYM 8.6 -0.5 -0.80 4CNIOX 9.3 0.2 0.20

8WWDBW 8.7 -0.4 -0.70 YL2O3B 9.3 0.2 0.20 AXU99T 8.7 -0.4 -0.70 X8QXDX 9.3 0.2 0.20 5E0FMO 8.7 -0.4 -0.70 M9N99Q 9.3 0.2 0.24 KTBSBL 8.8 -0.3 -0.55 EGEENO 9.4 0.3 0.33 MJRX8A 8.8 -0.3 -0.55 KHDDXD 9.4 0.3 0.35 AZUH8X 8.9 -0.2 -0.46 DUCT4E 9.4 0.3 0.35 CJWQGK 8.9 -0.2 -0.43 XM00GQ 9.4 0.3 0.39 ZIGGI6 8.9 -0.2 -0.43 QHQQUK 9.5 0.4 0.49 GI4HGG 8.9 -0.2 -0.40 SG5IQS 9.5 0.4 0.49 QQTH7B 8.9 -0.2 -0.40 6666WM 9.5 0.4 0.49 RKPGFK 8.9 -0.2 -0.40 YAIDDI 9.5 0.4 0.49 7MM6GH 8.9 -0.2 -0.38 C9BRBB 9.5 0.4 0.49 UEAZZ3 8.9 -0.2 -0.34 PWZDFG 9.6 0.5 0.64 2MPUPL 9.0 -0.1 -0.31 6RFSER 9.6 0.5 0.64 33ZZO3 9.0 -0.1 -0.28 HHHNYB 9.6 0.5 0.67 RKKTQP 9.0 -0.1 -0.25 B3FTN3 9.6 0.5 0.70 4AXZ9A 9.0 -0.1 -0.25 KMBMUQ 9.7 0.6 0.73 YHKKKB 9.0 -0.1 -0.25 W4X1SX 9.7 0.6 0.73 JNQLXX 9.0 -0.1 -0.25 PIRYEY 9.7 0.6 0.78

WCEEWA 9.0 -0.1 -0.25 JIOIBA 9.8 0.7 0.87 GNM3ON 9.0 -0.1 -0.25 ZUZ1ZZ 9.8 0.7 0.94 K1NKKG 9.0 -0.1 -0.25 7WA60O 9.8 0.7 0.94 N64P66 9.0 -0.1 -0.25 L75533 9.8 0.7 0.94




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Code

Metamfetamine



average z-score

FIAC2C 9.9 0.8 1.09 CYLW4Y 10.0 0.9 1.24 SDJTNO 10.1 1.0 1.39 RZDQQQ 10.1 1.0 1.39 6JFAWA 10.1 1.0 1.39 AFUXM7 10.2 1.1 1.54 TAAFSW 10.5 1.4 1.98 I3H5RP 10.6 1.5 2.13 9SMHJ8 10.7 1.6 2.28 BWSSKK 10.9 1.8 2.58 KAPAAS 11.0 1.9 2.73 FFUFOA 11.0 1.9 2.73 BRFRWM 11.1 2.0 2.87 YXNYHY 11.8 2.7 3.92 252CCB 12.0 2.9 4.21 BMPXHL 12.6 3.5 5.03 2Q22HI 12.6 3.5 5.11 E44WTB 13.3 4.2 6.12 HP2FIF 13.8 4.7 6.89 FVP0OM 15.0 5.9 8.68 T2S333 19.0 9.9 14.63 6YZTRZ 35.5 26.4 39.11 9YCKGZ 51.5 42.4 62.98




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False negatives for Test Sample-4 with respect to Cocaine (technique(s) used):

There were no false negative results for SM-4

Analysis not performed for Test Sample-4 with respect to Cocaine:

All participating laboratories carried out analysis for Cocaine



Cocaine 222 100.0%

Lactose 118 53.1%


1F633N Caffeine 180

1W4YMX Ketamine* 140, 171


W4X1SX Heroin 180

ZAOGZZ Caffeine 180, 190




Technique 140 141 142 150 160 161 170 171 180 190 200 210 211 230 231 250

Screening (No.) 72 88 78 17 1 1 2 9 70 18 0 2 0 2 1 7

(%) 32.4 39.6 35.1 7.7 0.5 0.5 0.9 4.1 31.5 8.1 0.0 0.9 0.0 0.9 0.5 3.2

Identification

(No.

24 10 9 34 6 10 3 29 210 89 2 1 2 5 10 7

(%) 10.8 4.5 4.1 15.3 2.7 4.5 1.4 13.1 94.6 40.1 0.9 0.5 0.9 2.3 4.5 3.2


(%) 0.0 0.0 0.0 0.0 6.7 14.7 0.7 53.3 18.7 0.0 0.0 0.7 0.7 1.3 2.0 0.0




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Round: 2019/1

Substance: SM-4; Cocaine


UNODC value: 14.4%










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Code

Cocaine

Code

Cocaine




(mass%)


average z-score

Y7M3HZ 7.6 -6.6 -5.95 CJWQGK 14.0 -0.2 -0.20 GNTW2Z 7.6 -6.6 -5.91 KHDDXD 14.0 -0.2 -0.20 54CQ2S 9.5 -4.7 -4.22 66H8C3 14.0 -0.2 -0.20 6JFAWA 9.9 -4.4 -3.91 4AXZ9A 14.0 -0.2 -0.20 LAWTLL 10.0 -4.2 -3.77 7WA60O 14.0 -0.2 -0.20 BZDD95 10.1 -4.1 -3.68 MYD9WU 14.0 -0.2 -0.20 BMPXHL 10.6 -3.6 -3.27 MELOFZ 14.0 -0.2 -0.20 JIOIBA 10.6 -3.6 -3.23 OKWXFO 14.0 -0.2 -0.20 XPYAOU 11.0 -3.2 -2.84 2Q22HI 14.0 -0.2 -0.20 2XXLPG 11.4 -2.8 -2.52 YL2O3B 14.0 -0.2 -0.20 BIA0EZ 11.5 -2.7 -2.40 UIFULT 14.0 -0.2 -0.20 2MPUPL 11.6 -2.6 -2.37 X8QXDX 14.0 -0.2 -0.20 QZZZGT 11.8 -2.4 -2.14 K1NKKG 14.0 -0.2 -0.20 MJRX8A 12.0 -2.2 -1.99 N64P66 14.0 -0.2 -0.20 GNM3ON 12.0 -2.2 -1.99 444444 14.0 -0.2 -0.20 QQ7VFQ 12.0 -2.2 -1.99 N4VGXV 14.0 -0.2 -0.19 FEKAVF 12.5 -1.7 -1.50 EGEENO 14.0 -0.2 -0.16 FIAC2C 12.6 -1.6 -1.42 33ZZO3 14.0 -0.2 -0.16

7MM6GH 12.7 -1.5 -1.36 JAXXGC 14.1 -0.1 -0.11 4J4R44 12.8 -1.5 -1.32 DFTIVR 14.1 -0.1 -0.11 AFUXM7 12.9 -1.3 -1.18 BRUEIH 14.1 -0.1 -0.11 V6ESR5 12.9 -1.3 -1.18 AC11BX 14.1 -0.1 -0.11 XNJQP7 13.0 -1.2 -1.13 KMBMUQ 14.1 -0.1 -0.11 GI4HGG 13.0 -1.2 -1.13 ZFFBFT 14.1 -0.1 -0.11 ZIGGI6 13.0 -1.2 -1.10 4CNIOX 14.1 -0.1 -0.11

DDVDDE 13.0 -1.2 -1.09 V7AWBG 14.1 -0.1 -0.11 WCEEWA 13.0 -1.2 -1.09 PWZDFG 14.2 0.0 -0.02 T2S333 13.0 -1.2 -1.09 F3LSGY 14.2 0.0 -0.02 DLFBGB 13.0 -1.2 -1.09 PKPTJM 14.2 0.0 -0.02 0E49T9 13.1 -1.1 -1.00 XM00GQ 14.2 0.0 0.01 KNHLNG 13.2 -1.0 -0.88 RH08SD 14.2 0.0 0.02 Y31S2M 13.3 -0.9 -0.82 AXU99T 14.3 0.1 0.07 C9BRBB 13.3 -0.9 -0.82 5E0FMO 14.3 0.1 0.07 QPTTIT 13.4 -0.8 -0.76 QHQQUK 14.3 0.1 0.07 TIIISI 13.5 -0.7 -0.64 INI2AA 14.3 0.1 0.07

OIMJHC 13.5 -0.7 -0.64 TAAFSW 14.3 0.1 0.07 QQTH7B 13.6 -0.6 -0.56 C5MUOL 14.3 0.1 0.07 5Q555E 13.6 -0.6 -0.56 SU4NXI 14.3 0.1 0.07 KFULE7 13.6 -0.6 -0.56 KVYOOO 14.3 0.1 0.07 S8TL74 13.6 -0.6 -0.56 SG5IQS 14.3 0.1 0.11 UEAZZ3 13.6 -0.6 -0.56 GQQTND 14.4 0.2 0.11 RRJPPR 13.6 -0.6 -0.53 OHKWWZ 14.4 0.2 0.16 HHHNYB 13.6 -0.6 -0.52 YXNYHY 14.4 0.2 0.16 9YCKGZ 13.8 -0.4 -0.38 KC4CO7 14.4 0.2 0.16 PIRYEY 13.9 -0.3 -0.31 AMRMTF 14.4 0.2 0.16 M9N99Q 13.9 -0.3 -0.29 6RVR5A 14.4 0.2 0.16 6RFSER 13.9 -0.3 -0.29 TTTILP 14.4 0.2 0.16




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Code

Cocaine

Code

Cocaine




(mass%)


average z-score

3FT9VW 14.4 0.2 0.18 SDJTNO 15.3 1.1 0.96 KTBSBL 14.5 0.3 0.25 BWSSKK 15.3 1.1 0.96 NGGZGG 14.5 0.3 0.25 DJS2XK 15.4 1.2 1.05 DUCT4E 14.5 0.3 0.25 ADW75B 15.4 1.2 1.05 L75533 14.5 0.3 0.25 1W4YMX 15.5 1.3 1.14 ZUZ1ZZ 14.6 0.4 0.34 FFUFOA 15.5 1.3 1.14 NPO333 14.6 0.4 0.34 YAIDDI 15.5 1.3 1.14 0OGHZR 14.6 0.4 0.34 INNQNN 15.7 1.5 1.32 JNQLXX 14.6 0.4 0.34 DPVGZK 15.7 1.5 1.32 6YZTRZ 14.7 0.5 0.38 I3H5RP 15.9 1.7 1.46 3TY2WR 14.7 0.5 0.43 2TCPHH 15.9 1.7 1.48 AZUH8X 14.8 0.6 0.49 GZFJAG 16.0 1.8 1.58 8FXHXS 14.8 0.6 0.52 313337 16.0 1.8 1.59 CYLW4Y 14.8 0.6 0.52 R6BICL 16.3 2.1 1.86 BRFRWM 14.9 0.7 0.61 2F51LA 16.5 2.3 2.04 ZPZ8SZ 14.9 0.7 0.61 FVP0OM 16.7 2.5 2.18

RZDQQQ 14.9 0.7 0.61 5HWYZN 16.7 2.5 2.22 QEJKPA 14.9 0.7 0.61 6666WM 17.8 3.6 3.20 4YFBKI 15.0 0.8 0.65 9SMHJ8 18.1 3.9 3.47 KAPAAS 15.0 0.8 0.70 B3FTN3 18.2 4.0 3.51 YHKKKB 15.0 0.8 0.70 2XGWKJ 18.3 4.1 3.65 1999Y6 15.0 0.8 0.70 1F633N 18.4 4.2 3.76 OHJX22 15.1 0.9 0.82 E44WTB 19.6 5.4 4.79 W4X1SX 15.2 1.0 0.87 252CCB 21.0 6.8 6.06 E4CIFO 15.2 1.0 0.87 HP2FIF 21.0 6.8 6.06 13S3E5 15.2 1.0 0.87 LRPCVG 23.4 9.2 8.20 GFWFBO 15.2 1.0 0.88 8WWDBW 32.0 17.8 15.89 9IA9GY 15.3 1.1 0.94 KII7PP 43.0 28.8 25.69




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10. ANNEX 1: Participants’ results for Test Sample-1

Identified substances for Test Sample 1

Code Identified Substances

13S3E5 Lidocaine and Procaine

1F633N -

1W4YMX ketamina

252CCB Procaine and Lidocaine

2MPUPL No

2TCPHH lidocaine, procaine

2XXLPG NONE

33ZZO3 no drugs in the sample

3FT9VW PROCAINE, LIDOCAINE AND LACTOSE

3RF39E LIDOCAINE

3TY2WR Lignocaine & Procaine

44E44K lidocaine, procaine

4XX6CI Lidocaine and procaine

4YFBKI Lidocaine(Lignocaine) and Procaine

54CQ2S lidocaine and procaine

5FFFFF Procaine, Lidocaine

5HWYZN -

5Q555E -

6666WM LIDOCAINE, PROCAINE, LACTOSE

66H8C3 NONE

6JFAWA Lidocaine,Procaine

6RFSER None

6WDJTJ Lactose, Lidocaine and Procaine

7ED7SR Lignocaine, Procaine

8FXHXS PROCAIN

9IA9GY Lidocaine and procaine

9YCKGZ Procaine, Lidocaine

A441YE lidocaïne, lidocaïne artifact, procaïne and oxybuprocaine

AC11BX lidocaine, procaine

ADW75B Procaine and Lidocaine

AMRMTF Lidocaine, Procaine, Lactose

AODFDP Lidocaine and procaine

AYTE1E Lidocaine & Procaine

AZUH8X lidocaine and procaine

B3FTN3 Lidocaine and procaine

BEPFVN none

BRUEIH Lidocaine, Procaine




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BYBCVB Only PROCAINA, LIDOCAINE and ALPHA LACTOSE were found.

BZDD95 None

CJWQGK lidocaine and procaine

DDVDDE Procaine, Lidocaine, Lactose

E44WTB Procaine,Lidocaine

EAQ4S6 Procaine and Lidocaine

EEGL2R Lidocaine and procaine

EGEENO Lidocaine & Procaine

EJ4611 Lidocaine and Procaine

FIAC2C lidocaine and procaine

FLL757 Lidocaine, procaine

GDPMAM Lidocaine, procaine

GGFGG9 None drugs under control

GNM3ON Lidocaine (PDL in Canada)

GNTW2Z 1. Lidocaine 2. Procaine

HHHNYB no

HMTUQD Lidocaine and procaine

HMW24R Lidocaine and Procaine

INNQNN Lidocaine›Procaine and Lactose

IVWKXD No

J7VXH7 Lidocaine & Procaine

JHHNXN ---

JIOIBA Procaine, lidocaine

JNQLXX Procaine,Lidocaine & Lactose

K1NKKG Procaine and Lignocaine - non-controlled drugs

LE5Z5Z Lidocaine and Procaine

MLKVZO Lidocaine,Procaine

N4VGXV -

NNANPN none

OCQGSD Procaine and Lignocaine

OIKEE1 Procaine and lidocaine

OKWXFO lidocaine, procaine, lactose

P0NNSM Lidocaine and Procaine

P1JWGT Lidocaine and Procaine

QPTTIT Lidocaine ,Procaine

QQ7VFQ Lidocaine (PDL in Canada)

QZZZGT Lidocaine, Procaine

R5RPYM Procaine, Lidocaine

RKKTQP Lidocaine (lignocaine) and Procaine.

RZDQQQ LIDOCAINE AND PROCAINE

SGBOPO Lignocaine and Procaine

SU4NXI LIDOCAIN, PROCAIN




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TCVV6F lidocaine, procaine

TMWUWW Procaine and Lidocaine

TTTILP NIL

TUVPUU Procaine et lidocaine

UEAZZ3 Lidocaine and procaine

UIFULT LIDOCAINE AND PROCAINE

V6ESR5 Procaine, lidocaine

VF8TL1 Lidocaine and Procaine

W4X1SX -

WCEEWA Lidocaine (PDL in Canada)

WJRG8W No drugs, only lidocaine and procaine

X1A11B lidocaine, procaine

X6OWJR Lidocaine+Procaine

XNJQP7 LIDOCAINE AND PROCAINE (NONE OF THEM ILLEGAL SUBSTANCES)

XYXPCP Procaine and Lidocaine

Y7M3HZ no

YXNYHY Lidocaine and procaine

YYYJYT Lidocaine, Procaine and Lactose

ZE8ZAZ procaine and lidocaine

ZPZ8SZ LIDOCAINE, PROCAINE

ZWM2QG Lidocaine and procaine




Page 29 of 120

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Statement of findings for Test Sample 1

Code Lactose Lidocaine (Lignocaine)

Procaine

0E49T9 ANP + + The sample contained no controlled drugs. Lidocaine and procaine were present in the sample.

0OGHZR ANP + + Adulterant: local anaesthesic lidocaine, procaine

13S3E5 - + + The sample not contain illicit drugs

1999Y6 ANP + + procaine, lidocaine

1CNMZQ - + + lidocaine and procaine

1F633N - - + a substance identified is procaine

1IDFP1 ANP + + Procaïne+Lidocaïne

1W4YMX ANP ANP +

252CCB + + + Analysis revealed the presence of procaine, lidocaine and lactose

2F51LA ANP + + lidocaine and procaine

2MPUPL - + + White powder with lidcaine and procaine

2Q22HI + + + The sample contained Procaine and Lidocaine.

2TCPHH ANP + + Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with lidocaine and procaine.

2XGWKJ - + +

2XXLPG - + + we found procaine and lidocaine in SM 1 (as non controlled drugS).

313337 - + + Lidocaine, Procaine, no drugs found

3332NG + + + procaine, lidocaine, lactose

33ZZO3 + + + Lidokaine and procaine are not on the list of drugs.

36BDU6 - + + Sample 2019/1/SM-1 was found containing lidocaine and procaine

3FT9VW + + +

3RF39E - + -

LIDOCAINE




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Procaine

3SMK33 + + +

3TY2WR ANP + + Lignocaine and Procaine are not controlled.

444444 + + + Lidocaine, procaine and lactose.

44E44K + + + Anesthetic drug

4AXZ9A + + + A composite was formed from 1 unit for testing of 1 unit received. Procaine, lidocaine and lactose confirmed in the composite.

4CNIOX + + + The sample contains 24% lidocaine-hydrochloride, procaine-hydrochloride and lactose.

4J4R44 ANP + + lidocaine (25.6 %) and procaine (28.1%)

4XX6CI + + + The test sample 2019/1/SM-1 was found to contain the adulterants/diluents lidocaine, procaine and lactose.

4YFBKI ANP + + SM-1 sample was prepared from a sample of Lidocaine(Lignocaine) .The test sample also contained Procaine.

4Z4BDP + + + The sample contains lidocaine, procaine, lactose.

54CQ2S ANP + +

Drugs which found in SM1 were Lidocaine and Procaine.

5E0FMO + + + Presence of lidocaine, procaine and lactose was detected in the sample.

5FFFFF - + + Pracaine and lidocaine were found in the analysis.

5HWYZN + + + The sample contains lidocaine, procaine and lactose only. The identified substances are often used as adulterants of street drugs.

5Q555E + + + lidocaine,procaine, lactose

6666WM + + + WE FOUND A MIXTURE OF LIDOCAINE, PROCAINE AND LACTOSE.

66H8C3 + + +

NO DRUGS WERE FOUND. WAS FOUND PROCAINE, LIDOCAINE AND LACTOSE.

6JFAWA + + +

6RFSER + + + Mixture of lactose, lidocaine and procaine; lactose 47.6 % w/w; lidocaine 20.4 % w/w; procaine 21.0 % w/w 6RVR5A ANP + + The sample 2019/1/SM1 contain Lidocaine and Procaine.

6WDJTJ + + + Positive to Lactose, Lidocaine and Procaine.




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Procaine

6YZTRZ + + +

7ED7SR ANP + + Powder contained lignocaine and indications of procaine. Lignocaine and procaine are not controlled drugs

7MM6GH ANP + + Sample contains lidocaine and procaine.

7WA60O + + + Lidocaine and Procaine are found which are used as a local anaesthetics. Also there was a little amount of Lactose included.

8FXHXS + + + LIDOCAIN and LACTOSE

8WWDBW + + + SM-1 was found contain traces of Lactose, Procaine & lIDOCAINE

9IA9GY - + + We can´t cuantified due to we don´t have reference pattern

9OOEII ANP + + procain,lidocain

9SMHJ8 ANP + +

the white powder contains lidocaine and procaine

9YCKGZ - + + Procaine, Lidocaine were identified by GC/MS

A441YE + + + the main compounds we found in SM-1 are lidocaine and procaine after GC / MS injection. Excess compounds are in a trace state.

AC11BX + + + Lactose

ADW75B ANP + + This sample was found to contain Procaine and Lidocaine which are not controlled under the Misuse of Drugs Act 1971.

AFUXM7 + + + It is detected the presence of lidocaine and procaine in the sample

AMRMTF + + +

AO8UQ6 + + + The 2019/1 / SM-1 sample contains lidocaine, lactose and procaine.

AODFDP ANP + + It was detected the presence of lidocaine and procaine in the sample analysed

AXU99T ANP + + In the test sample 2019/1/SM-1 was detected lidocaine and procaine

AYTE1E ANP + + Lidocaine & procaine confirmed in SM-1

AZUH8X ANP + + We have found lidocaine and procaine in SM-1 sample.

B3FTN3 + + + Controlled drugs were not found in the sample 2019/01-SM1.




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Procaine

BBBLO2 ANP + + Sample contains no controlled drug however, presence of procaine and lidocaine was confirmed qualitatively

BEPFVN + + + We have not detected any controlled substance.

BIA0EZ ANP + + The sample contains lidocaine and procaine.

BMPXHL - + +

procaine and lidocaine

BRFRWM ANP + + White powder containing any controlled drug

BRUEIH + + +

BTKUST + + +

BWSSKK + + + clorhidrato de procaina 21,5%base, clorhidrato de lidocaína 17,1%base y lactosa.

BYBCVB + + + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of ALPHA LACTOSE in the sample.

BZDD95 + + + SM-1 contains no controlled substance. It was found to contain lidocaine, procaine and lactose.

C5MUOL + + +

C9BRBB + + + The analysis did not reveal any controlled drug according to french order, decree of February 22nd 1990.

CJWQGK - + +

CYLW4Y + + + lidocaïne (21,5% as base) + procaïne (14,9 % as base) + lactose

DDVDDE + + + We started with colourimetric test, then We could identify Lactose by FTIR and Procaine and lidocaine by GC-MS. We analyze the samples in different solvents and different concentrations.

DFTIVR + + +

DHDX48 - + + Procaine-lidocaine

DJS2XK ANP + +

DLFBGB ANP + + Sample was found to contain Caffeine and Lignocaine

DPVGZK + + + The sample contain Lidocaine and procaine and lactose

DUCT4E + + + Procaine, lidocaine and lactose




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Procaine

E44WTB + + + Lidocaine, Procaine and Lactose were identified in SM1

E4CIFO ANP + +

EAQ4S6 ANP + + TLC and GCMS

EEGL2R + + + White powder analysed by GC/MS was found to contain Lidocaine and Procaine. Mass spectra was similar to CRMs

EGEENO + + + The sample contains Lidocaine, Procaine and Lactose

EJ4611 + + + The sample analyzed SM1 contains lidocaine, procaine and lactose

F3LSGY + + + Lidocaine, Procaine and lactose

FEKAVF ANP - + Procaine and Tolycaine

FFUFOA + + + Lidocaine, Procaine and Lactose

FIAC2C ANP + + We have found lidocaine and procaine in SM-1 sample.

FJ7FUF + + + Sample number 1: there is not ilicit drugs (lidocaine and procaine)

FLL757 ANP + + In the seized sample was detected the presence of lidocaine and procaine, that are adulterants / diluents

FVP0OM - + + Procaine, Lidocaine

GDPMAM + + + Lidocaine, procaine and lactose were detected in sample.

GFWFBO ANP + + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample indicates the lidocaine and procaine presence.

GGFGG9 ANP + + Sample represent white powder that contains not controlled substances procaine and lidocaine.

GI4HGG + + +

GNM3ON ANP + + The following sustance(s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified: Lidocaine Should you need this (these) detected substance (s) to be certified, please contact us.

GNTW2Z ANP + + The sample 2019/1/SM-1 was found to contain Lidocaine and Procaine.




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Procaine

GQQTND + + + White powder 229 milligrams. Procaine Hydrochloride, Legal status-Not controlled Lignocaine Hydrochloride, Legal status-Not controlled Lactose, Legal Status-Not controlled Legal Status refers to the classification of the drug found under the provisions of the Misuse of Drugs Act 1971 (as amended).

GY9CXA + + +

GZFJAG ANP + + We have found %23,059 procaine and %20,152 lidocaine adulterants in sm-1 samples. We have not found drugs.

HGOHHH ANP + + The seized material contains uncontrolled substances of lidocaine and procaine

HHHNYB + + + procaine HCl, lidocaine HCl, lactose

HMTUQD ANP + + Lidocaine and procaine were detected in the SM-1 sample.

HMW24R ANP + + Sample SM-1 found to contain lidocaine and procaine

HP2FIF ANP + + procaine, lidocaine

I3H5RP ANP + +

lidocaine plus procaine

IKEYL1 ANP + + LIDOCAINE AND PROCAINE AS MINORITY

INI2AA + + + White powder odorless containing lidocaine and procaine and lactose

INNQNN + + + The samples 2019/1/SM-1 contains lidocaine, procaine and lactose detected by GC/MS and FTIR.

IQQVQB ANP + + Powder from sample 2019-1SM-1 does not contain controlled substance (contain Lidocaine & Procaine)

IVWKXD - + + Lidocaine and Procaine

J7VXH7 ANP + + Test sample 2019/1/SM-1 to contain Lidocaine which is listed in Malaysia Poison Act 1952. Procaine was also detected in this sample

JAXXGC ANP + + lidocaine, procaine

JFLFE3 + + + Material analysis using the portable Raman equipment as screening provided as a result lidocaine, procaine and lactose substances. The substances were confirmed by GCMS using a reference standards.

JHHNXN + + + Marquis reagent: negative; Cobalt thiocyanate: negative; GC-MS: lidocaine, procaine (results compared with library spectra); FTIR: lactose (result compared with library spectrum); Lactose and glucose were differentiated with Woehlk test




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Procaine

JIOIBA + + + Also lactose was found.

JNQLXX + + + Using the techniques TLC, GC-MS & FTIR , Sample SM 1 was found to contain Procaine, Lidocaine & Lactose.

K1NKKG + + + The powder in item 2019/1/SM-1 was found contain Procaine and Lignocaine, both of which are not controlled under the Misuse of Drugs Act 1971 (as amended).

KAPAAS ANP + + Analysis of a representative sample of the powder revealed the presence of lidocaine and procaine.

KC4CO7 - + +

KFULE7 + + + lactose, lidocaine, procaine

KHDDXD - + + This sample was found to contain lidocaine and procaine.

KII7PP + + +

KMBMUQ + + + This item contained 0.23 grams of white powder, found to contain Lidocaine, Procaine and Lactose, all of which are not controlled substances under the Misuse of Drugs Act 1971, as amended.

KNHLNG + + + SM-1 contains Lidocaine 20.04% (as base), Procaine HCl 14.49% (as base) and Lactose

KTBSBL + + + lidocaine and procaine were detected by GC/MS

KVYOOO + + + Mezcla de Lactosa con lidocaina y procaina

L75533 + + + SM1 contient de la Procaïne - Lidocaïne avec du lactose

LAWTLL + + + Lidocaina, Procaina, Lactosa

LE5Z5Z ANP + + Based on the above analysis, the sample was found to contain Lidocaine and Procaine

LRPCVG + + + SM1:was fond to contain lidocain,procain, lactose and phenidemitrazine

M9N99Q + + +

MELOFZ + + + Sample was a mixture of procaine HCL, Lactose and Lignocaine (lidocaine) HCL

MJRX8A + + + The test sample contained lactose, lidocaine and procaine

MLKVZO + + + Lactose

MMQ2L2 + + + lidocaine, procaine, lactose




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Procaine

MYD9WU ANP + + With the methods applied, it is not identified any controlled substances.

N4VGXV - + + lidocaína, procaína

N64P66 + + + Procaine HCl, Lignocaine HCl, Lactose

NGGZGG - + + Procaine and lidocaine

NNANPN ANP + + In the sample labeled 2019/1 / SM-1 no substances of forensic interest were found, lidocaine and procaine were found.

NPO333 + + +

Lidocaine, procaine and lactose

OCQGSD ANP + + The white powder was analysed for controlled drugs with a negative result. The powder contained Procaine and Lignocaine (Lidocaine).

OHJX22 + + + Procaine, Lignocaine & Lactose were found present in the sample SM-1

OHKWWZ + + + The sample contains Lidocaine and Procaine

OIKEE1 + + + Procaine, lidocaine and lactose were detected in SM-1 sample.

OIMJHC ANP + +

OKWXFO + + + The sample contains only cutting agents.

P0NNSM ANP + + Sample 2019/1/SM-1 found to contain Lidocaine and Procaine

P1JWGT - + + Lidocaine and Procaine are not controlled drugs under the Drug Abuse Prevention And Control Act Cap 131 of the Laws of Barbados.

PIRYEY - + + Sample 2019/1/SM-1 contains lidocaine and procaine.

PKPTJM ANP + + One glass bottle containing 0.23 grammes of a powder containing lignocaine and procaine.

PWZDFG + + + Procaine, Lidocaine and Lactose.

QEJKPA ANP + + the sample contains only lidocaine and procaine

QHQQUK ANP + + No controlled drug present Identified substance: Lidocaine, Procaine

QMGORR ANP ANP ANP

QPTTIT ANP + + We have found lidocaine and procaine in SM-1 sample.




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Procaine

QQ7VFQ ANP + + The following sustance(s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified: Lidocaine Should you need this (these) detected substance (s) to be certified, please contact us. QQTH7B + + + lactose,prokaine,lidocain

QZZZGT ANP + + The sample was found to contain uncontrolled drugs Lidocaine and Procaine.

R5RPYM + + + lactose is also present

R6BICL + + + In the 2019/1/SM-1 was proved the presence of Lactose, Lidocaine and Procaine.

RH08SD + + + This sample contains procaine and lidocaine.

RKKTQP ANP + + White powdery substance of 2019/1/SM-1 was found to contain Lidocaine (Lignocaine) and Procaine. Lignocaine is listed in The First Schedule of The Poisons Act 1952.

RKPGFK - + + Sample 2019/1/SM-1 was found containing Lidocaine and Procaine

RRJPPR - + + no substance subject to control is detected

RZDQQQ - + +

S8TL74 ANP + + LIDOCAINE, PROCAINE

SAKRI4 ANP ANP ANP

SDJTNO + + + white powder containing lidocaine and procaine. The sample contains lactose.

SG5IQS + + + SM 1 contains: Lidocaine, Procaine and Lactose

SGBOPO - + + The powder was analysed and found to contain Lignocaine and Procaine. Lignocaine and Procaine are not controlled drugs within the provisions of the Misuse of Drugs Act 1971.

SHLDPB + + + procaine, lidocaine, lactose

SU4NXI + + + LIDOCAIN 25%, PROCAIN 22%, LACTOSE

T2S333 + + +

TAAFSW + + + The sample does not contain any controlled drug.The sample contains lidocaine and procaine and lactose.

TCVV6F + + + the sample SM-1 was found lidocaine and procaine

TIIISI + + +




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Procaine

TMWUWW ANP + + 2019/1/SM-1 was confirmed for procaine and lidocaine, both of which are not controlled substances in the United States.

TTQXMT ANP + + Sample 2019/1/SM-1 consists of white powder. No prohibited substances are detected in this sample.

TTTILP + + + Sample analysed by GCMS, LCMSMS and FTIR techniques. Procaine, Lidocaine and Lactose are identified in the sample.

TUVPUU + + +

TXVZAJ ANP + + white powder containing lidocaine and procaine

UEAZZ3 + + + SM-1 was found to contain lidocaine, procaine and also lactose.

UIFULT ANP + + SCREENING BY RAMAN AND CONFIRMATION BY GC MSD

V6ESR5 ANP + +

V7AWBG + + +

VF8TL1 ANP + + Lidocaine and Procaine controlled under Malaysian Poison Act

VHYXAH + + + LIDOCAINE AND PROCAINE IN LACTOSE POWDER

W0OABU ANP + + Lidocaina-Procaína

W4X1SX ANP + + -

WCEEWA ANP + + The following sustance(s) from the Prescription Drug List of the Food and Drug Regulations has (have) been detected but not certified: Lidocaine Should you need this (these) detected substance(s) to be certified, please contact us.

WJRG8W - + + The sample does not contain drugs. Only lidocaine and procaine.

X1A11B ANP + + lidocaine, procaine

X66O46 ANP + + Sample 2019/1/SM-1 a white powder gave a negative result for substances under national legislation on drugs. Lidocaine and procaine were detected.

X6OWJR + + + Lidocaine+Procaine+Lactose

X8QXDX + + +

Lidocaïne et Procaïne Lactose XM00GQ + + + Sample with procaine, lidocaine and lactose. Identification of procaine and lidocaine by GC/MS. Identification of lactose by Raman, FTIR and by GC/MS after MSTFA derivatization.




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Procaine

XNJQP7 - + + THERE´S NO SUSTANCE FOUNDED

XPYAOU ANP + + Sample resulted negative to controlled substances. Lidocaine and Procaine detected in the sample material.

XYXPCP - + + SM1 contains Procaine and Lidocaine.

Y31S2M ANP + +

Y45Y4Y + + + It was found: procaine, lactose, lidocaine.

Y7M3HZ ANP + + procaine + lidocaine

YAIDDI + + + It does not contain any controlled drugs. It contains procaine, lidocaine and lactose.

YHKKKB + + +

YL2O3B ANP + + The sample was analysed and no common controlled drug was detected.

YXNYHY + + +

Lidocaine, procaine and lactose

YYYJYT + + + The Test sample 2019/1/SM-1 was analyzed by Thin Layer Chromatography technique and was found to contain Procaine, Lidocaine and Lactose.

ZAOGZZ + + + 2019/1/SM-1 contains lactose, procaine and lidocaine

ZE8ZAZ ANP + + Positive to procaine and lidocaine, commonly used as cocaine adulterants.

ZFFBFT - + +

ZIGGI6 + + + The sample contains lidocaine, procaine and lactose.

ZPZ8SZ ANP + +

ZUZ1ZZ + + + lidocaine, procaine and lactose

ZWM2QG ANP + + Sample 2019/1/SM-1 was found to contain lidocaine and procaine




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Identification methods for Test Sample 1

Analytical Technique Codes

Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

0E49T9 I I SI I

0OGHZR SI SI I

13S3E5 S S S I I I duquenoise-levine

1999Y6 S I I

1CNMZQ SI

1F633N SI

1IDFP1 SI I

1W4YMX SI S S I

252CCB I I SI

2F51LA I SI

2MPUPL S I I

2Q22HI S S S I I

2TCPHH S S S I

2XGWKJ I SI

2XXLPG S S S I

313337 S S I

3332NG S I SI SI

33ZZO3 S I I

36BDU6 S I

3FT9VW S S I I

3RF39E S S I

3SMK33 S S S I I I S R. Mandeline

3TY2WR S S I

444444 SI

44E44K S S S I I I

4AXZ9A I SI

4CNIOX I SI

4J4R44 S SI

4XX6CI S S S SI I

4YFBKI S I I

4Z4BDP S S S I I I

54CQ2S I SI S Strip test

5E0FMO I I I S

Legend: S ... used for Screening I ... used for Identification SI ... used for both




Page 41 of 120

ICE 2019/1-SM

Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

5FFFFF S S S SI I

5HWYZN SI I Tollens reaction

5Q555E SI SI SI SI SI I

6666WM SI SI S SI I I

66H8C3 S S I I

6JFAWA SI I

6RFSER I I I S

6RVR5A S S I S Tanred

6WDJTJ I

6YZTRZ SI I

7ED7SR I

7MM6GH SI

7WA60O S I SI SI

8FXHXS SI

8WWDB W

I

9IA9GY S S S I I

9OOEII S S S I I

9SMHJ8 I SI

9YCKGZ S S I I

A441YE I S

AC11BX I SI I

ADW75B S S I

AFUXM7 SI I

AMRMTF I SI

AO8UQ6 S S I I

AODFDP S S S I

AXU99T I

AYTE1E S SI SI I

AZUH8X SI SI SI I

B3FTN3 S S S I I

BBBLO2 S S I SI

BEPFVN I I S S Ion mobility scan

BIA0EZ SI

BMPXHL S S S I I

BRFRWM I SI

BRUEIH SI I

BTKUST SI I




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ICE 2019/1-SM

Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

BWSSKK S I I

BYBCVB S I I

BZDD95 I

C5MUOL SI I

C9BRBB I I

CJWQGK SI

CYLW4Y SI I

DDVDDE S SI I

DFTIVR SI I I

DHDX48 S I

DJS2XK S S I

DLFBGB S S I

DPVGZK S I I

DUCT4E S I I

E44WTB S S I I I I Fast Blue B test

E4CIFO S S I I

EAQ4S6 S S SI I

EEGL2R S S S I I

EGEENO I SI I

EJ4611 S I I

F3LSGY I I SI I

FEKAVF S S I I

FFUFOA S I I I

FIAC2C SI SI SI I

FJ7FUF S S I I

FLL757 SI I

FVP0OM S I I

GDPMAM S S I I

GFWFBO S S I

GGFGG9 S S I SI S Simon-s Reagent

GI4HGG SI I I spot test

GNM3ON SI I I

GNTW2Z SI SI SI I

GQQTND S S S I I

GY9CXA S I I

GZFJAG SI SI SI I

HGOHHH SI




Page 43 of 120

ICE 2019/1-SM

Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

HHHNYB SI I SI

HMTUQD SI I

HMW24R S I

HP2FIF SI

I3H5RP S S S I

IKEYL1 S S S I I

INI2AA I I

INNQNN I SI I

IQQVQB S S I I

IVWKXD SI

J7VXH7 S I

JAXXGC SI

JFLFE3 S I I

JHHNXN S S SI I

JIOIBA S I I I I

JNQLXX S S SI SI

K1NKKG S S S I I

KAPAAS SI

KC4CO7 I S

KFULE7 I SI

KHDDXD S I I

KII7PP SI

KMBMUQ S S I I

KNHLNG S S S I I

KTBSBL SI I

KVYOOO SI S I I SI RAMAN

L75533 S I I

LAWTLL S S S I I I I

LE5Z5Z S I

LRPCVG I SI

M9N99Q S S S I I

MELOFZ S S S I I

MJRX8A S I

MLKVZO S S S I I

MMQ2L2 S I SI I

MYD9WU I I I

N4VGXV SI I I SI




Page 44 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

N64P66 S S I I S Simon's & Ketamine

NGGZGG S S S I

NNANPN I I SI

NPO333 S I I

OCQGSD S I I

OHJX22 S S I SI I I Fast Blue B Salt test

OHKWWZ SI I

OIKEE1 I SI I

OIMJHC SI

OKWXFO I I

P0NNSM S I S Marquis, Simon,

Janovsky

P1JWGT S I I

PIRYEY S S S I I

PKPTJM S S I SI

PWZDFG S S I I

QEJKPA SI

QHQQUK SI

QMGORR I SI

QPTTIT SI SI SI I

QQ7VFQ I S I I Special macro

QQTH7B I SI

QZZZGT S S I S Negm's Test

R5RPYM I I S

R6BICL I SI I I I

RH08SD S I I

RKKTQP S S I

RKPGFK S I S JANOVSKY REAGENT

RRJPPR S S S I

RZDQQQ S SI SI

S8TL74 I SI

SAKRI4 I

SDJTNO I I S

SG5IQS S I I

SGBOPO S I

SHLDPB S I SI SI

SU4NXI SI

T2S333 SI I




Page 45 of 120

ICE 2019/1-SM

Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

TAAFSW S S S I I LC QTOF

TCVV6F S S I

TIIISI S S S I I

TMWUW W

S I

TTQXMT S S I

TTTILP I S S SI I I

TUVPUU I S

TXVZAJ I I SI

UEAZZ3 S S I I

UIFULT I SI

V6ESR5 I S

V7AWBG SI SI

VF8TL1 S S SI I

VHYXAH I SI I

W0OABU S I

W4X1SX SI

WCEEWA S I I

WJRG8W I I SI I

X1A11B SI

X66O46 S S I I

X6OWJR I SI I

X8QXDX SI I

XM00GQ I S I I MSTFA

derivatization and CGMS XNJQP7 SI S SI I I

XPYAOU SI

XYXPCP S S S I I

Y31S2M I I

Y45Y4Y I I SI

Y7M3HZ SI I

YAIDDI I

YHKKKB SI I

YL2O3B I SI

YXNYHY S I

YYYJYT S S SI S Fast Blue B salt Test

ZAOGZZ S S S I I

ZE8ZAZ SI




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

ZFFBFT I SI I

ZIGGI6 S I I SI I

ZPZ8SZ I SI I SI

ZUZ1ZZ S I

ZWM2QG S S SI




Page 47 of 120

ICE 2019/1-SM




0E49T9 Morphine

0OGHZR Morphine

13S3E5 Morphine

1999Y6 morphine

1CNMZQ morphine

1F633N morphine

1IDFP1 Morphine

1W4YMX morfina

252CCB Morphine

2F51LA morphine

2MPUPL Morphine

2Q22HI Morphine

2TCPHH Morphine

2XGWKJ morphine

2XXLPG morphine

313337 Morphine

3332NG morphine

33ZZO3 metamfetamine

36BDU6 Morphine and codeine

3FT9VW MORPHINE

3RF39E MORPHINE

3SMK33 morphine

3TY2WR Morphine

444444 Morphine

44E44K morphine, codeine

4AXZ9A Morphine and codeine

4CNIOX morphine

4J4R44 morphine

4XX6CI Morphine

4YFBKI Morphine

4Z4BDP morphine

54CQ2S Morphine and Codeine

5E0FMO Morphine

5FFFFF Morphine

5HWYZN Morphine

5Q555E morphine

6666WM MORPHINE AND GLUCOSE




Page 48 of 120

ICE 2019/1-SM


66H8C3 MORPHINE

6JFAWA Morphine

6RFSER morphine

6RVR5A Morphine

6WDJTJ Morphine

6YZTRZ Morphine

7ED7SR Morphine

7MM6GH Morphine

7WA60O Morphine

8FXHXS MORPHINE

8WWDBW Morphine

9IA9GY Morphine

9OOEII morphine

9SMHJ8 morphine

9YCKGZ Morphine, 6-MAM, Codeine

A441YE morphine, codeine and hydromorphone

AC11BX Morphine, Codeine

ADW75B Morphine

AFUXM7 Morphine

AMRMTF Morphine

AO8UQ6 morphine.

AODFDP Morphine

AXU99T Morphine

AYTE1E Morphine

AZUH8X Morphine

B3FTN3 Morphine

BBBLO2 Morphine

BEPFVN morphine

BIA0EZ Morphine

BMPXHL morphine

BRFRWM morphine

BRUEIH Morphin

BTKUST morphine, codeine

BWSSKK morfina y trazas de codeina

BYBCVB MORFINA

BZDD95 Morphine

C9BRBB Morphine

CJWQGK morphine

CYLW4Y morphine chlorhydrate

DDVDDE Morphine, Codeine, Glucose

DFTIVR morphine

DHDX48 Morphine




Page 49 of 120

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DJS2XK Morphine

DLFBGB Morphine

DPVGZK Morphine

DUCT4E morphine

E44WTB Morphine

E4CIFO Morphine

EAQ4S6 Morphine

EEGL2R Morphine

EGEENO Morphine

EJ4611 Morphine

F3LSGY Morphine

FEKAVF Morphine

FFUFOA Morphine

FIAC2C Morphine

FJ7FUF Morphine

FLL757 Morphine

FVP0OM Morphine, Codeine

GDPMAM Morphyne

GFWFBO Morphine

GGFGG9 Morphine

GI4HGG kodeine

GNM3ON Morphine

GNTW2Z Morphine

GQQTND Morphine Hydrochloride

GY9CXA morphine

GZFJAG Morphine

HGOHHH morphine

HHHNYB morphine HCl

HMTUQD Morphine

HMW24R Morphine

HP2FIF morphine

I3H5RP morphine

IKEYL1 MORPHINE, CODEINE

INI2AA morphine-HCl

INNQNN Morphine

IQQVQB Morphine

IVWKXD Morphine

J7VXH7 Morphine

JAXXGC morphine

JFLFE3 Morphine.

JHHNXN Morphine

JIOIBA Morphine HCl




Page 50 of 120

ICE 2019/1-SM


JNQLXX Morphine & Lactose

K1NKKG Morphine Hydrochloride

KAPAAS Morphine

KC4CO7 Morphine

KFULE7 Morphine

KHDDXD Morphine

KII7PP morphine

KMBMUQ Morphine

KNHLNG Morphine

KTBSBL morphine

KVYOOO Morfina

L75533 la Morphine

LAWTLL Morfina

LE5Z5Z Morphine

LRPCVG Morphine

M9N99Q morphine

MELOFZ Morphine HCL

MJRX8A morphine

MLKVZO Morfine

MMQ2L2 morphine

N4VGXV morfina

N64P66 Morphine HCl

NGGZGG morphine

NNANPN Morphine

NPO333 Morphine

OCQGSD Morphine

OHJX22 Morphine

OHKWWZ Morphine

OIKEE1 Morphine

OIMJHC Morphine

OKWXFO morphine

P0NNSM Morphine

P1JWGT Morphine

PIRYEY Morphine and codeine

PKPTJM Morphine

PWZDFG Morphine

QEJKPA morphine

QHQQUK Morphine

QMGORR Morphine

QPTTIT Morphine

QQ7VFQ Morphine

QQTH7B morphine




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QZZZGT Heroin, Morphine

R5RPYM Morphine

R6BICL Morphine + Lactose

RH08SD Morphine

RKKTQP Morphine

RKPGFK Morphine

RRJPPR morphine

RZDQQQ MORPHINE 16.1%

S8TL74 MORPHINE

SDJTNO morphine

SG5IQS Morphine

SGBOPO Morphine

SHLDPB morphine

SU4NXI MORPHIN, CODEIN

T2S333 morphin

TAAFSW Morphine

TCVV6F Morphine

TIIISI Morphine

TMWUWW Morphine

TTQXMT Morphine

TTTILP MORPHINE

TXVZAJ Morphine

UEAZZ3 Morphine

UIFULT MORPHINE

V6ESR5 Morphine

V7AWBG Morphine

VF8TL1 Morphine

VHYXAH MORPHINE AND TRAZE AMOUNTS OF CODEINE

W0OABU Morfina

W4X1SX Morphine

WCEEWA Morphine

WJRG8W Morphine

X1A11B morphine

X66O46 morphine

X6OWJR Morphine

X8QXDX Morphine

XM00GQ Morphine

XNJQP7 NONE

XPYAOU Morphine

XYXPCP Morphine

Y45Y4Y Morphine

Y7M3HZ yes




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YAIDDI Morphine and Codeine

YL2O3B morphine

YXNYHY Morphine

YYYJYT Morphine and Glucose

ZAOGZZ morphine

ZE8ZAZ morphine

ZFFBFT morphine

ZIGGI6 morphine

ZPZ8SZ MORPHINE

ZUZ1ZZ morphine

ZWM2QG Morphine




Page 53 of 120

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Code Morphine

0E49T9 + The sample contained 13.1% morphine. There were traces of codeine present in the sample.

0OGHZR +

13S3E5 +

1999Y6 +

1CNMZQ +

1F633N + a substance identified is morphine

1IDFP1 + Morphine

1W4YMX +

252CCB + Analysis revealed the presence of morphine

2F51LA + codeine

2MPUPL + white powder containing Morphine

2Q22HI + The sample contained Morphine.

2TCPHH + Results of screening tests were positive for opiates. Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with morphine. Morphine was detected at 13.76% by weight.

2XGWKJ +

2XXLPG + The analysis confirmed that SM 2 contains morphine (as controlled drug) but we are not able to give a quantitative result). We found also lactose as non controlled drug.

313337 + Morphine

3332NG +

33ZZO3 + Metamfetamine is on the list of drugs.

36BDU6 + Sample 2019/1/SM-2 was found containing morphine and codeine

3FT9VW +




Page 54 of 120

ICE 2019/1-SM

Code Morphine

3RF39E +

MORPHINE

3SMK33 + GD of RM nr. 1088 of 05.10.2014

3TY2WR + Morphine is a Class A drug subject to the provisions of the Misuse of Drugs Act 1971.

444444 + Morphine hydrochloride and glucose.

44E44K + Included in List of narcotic drugs whose turnover in the Republic of Uzbekistan limited (List II)

4AXZ9A + A composite was formed from 1 unit for testing of 1 unit received. Morphine, codeine and dextrose confirmed in the composite.

4CNIOX + The sample contains 13% morphine and glucose. morphine is controlled by the Royal Decree of the 6th of september 2017

4J4R44 + morphine (12.11 %), also present codeine (minor compound)

4XX6CI + The test sample 2019/1/SM-2 was found to contain the controlled drug morphine.

4YFBKI + SM-2 sample was prepared from a seizure containing 13.73%(w/w) Morphine. The test sample also contained codeine and acetylcodeine as minor components.

4Z4BDP + The sample contain morphine.

54CQ2S + Drugs which found in SM2 were Morphint and Codeine.

5E0FMO + Presence of morphine hydrochloride, glucose and codeine was detected in the sample.

5FFFFF + Morphine was analysed.

5HWYZN + The sample contains morphine and lactose as an adulterant. Apart from morphine and lactose the sample contains small amounts of codeine. Morphine is controlled substance in Poland. 5Q555E + morphine,codeine

6666WM + WE FOUND A MIXTURE OF MORPHINE AND GLUCOSE.

66H8C3 + WAS FOUND MORPHINE. DEXTROSE WAS FOUND TOO.

6JFAWA +

6RFSER + mixture of morphine and glucose (82.7 %)

6RVR5A + The sample 2019/1/SM2 contain Morphine




Page 55 of 120

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Code Morphine

6WDJTJ + Positive to Morphine.

6YZTRZ +

7ED7SR + Powder contains morphine. Morphine is a controlled drug under the Misuse of Drugs Act 1977 to 2016

7MM6GH + Sample contains 13.5 % morphine.

7WA60O + 14.4 % of Morphine is found with quantitative methods.

8FXHXS +

8WWDBW + SM-2 was found contain Morphine & traces of Glucose

9IA9GY + We can´t cuantified due to we don´t have reference pattern

9OOEII +

9SMHJ8 + the white powder contains morphine (5.8%w/w) which is controlled by national law

9YCKGZ + Morphine, 6-MAM and Codeine were identified by GC/MS

A441YE + the main compound we found in SM-2 is morphine after GC / MS injection. Excess compounds are in a trace state.

AC11BX + Codeine

ADW75B + This sample was found to contain Morphine which is a Class A controlled substance under the Misuse of Drugs Act 1971

AFUXM7 + It has been detected the presence of morphine in the sample.

AMRMTF +

AO8UQ6 + Sample 2019/1 / SM-2 contains morphine.

AODFDP + It was detected the presence of morphine in the sample analysed

AXU99T + In the test sample 2019/1/SM-2 was detected morphine

AYTE1E + Morphine confirmed in SM-2

AZUH8X + We have found Morphine in SM-2 sample.




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Code Morphine

B3FTN3 + The sample 2019/01-SM-2 contains Morphine detected by GC-MS. The percentage by weight of Morphine is 25.61%.

BBBLO2 + Presence of morphine was confirmed qualitatively. Codeine is also present as minor

component BEPFVN +

The sample contains morphine. The concentration has not been determined.

BIA0EZ + The sample contains morphine.

BMPXHL + glucose

BRFRWM + White powder containing 15.6% of morphine

BRUEIH +

BTKUST + List of narcotics drugs whose circulation in the territory of the Republic of Uzbekistan is limited (Appendix to the resolution of the Cabinet of Ministers of the Republic of Uzbekistan ¼878 date 27.10.2018 y.)

BWSSKK + Morfina 14,3%base, trazas de codeína y glucosa.

BYBCVB + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of traces of codeine and LUCOSE in the sample.

BZDD95 + SM-2 contains morphine (15.0% as free base).

C5MUOL +

C9BRBB + The sample contains morphine which is listed as a controlled drug according to french order, appendix I of February 22nd 1990.

CJWQGK +

CYLW4Y + morphine (15,9% as base) + lactose

DDVDDE + We started with colourimetric test, then We could identify Glucose by FTIR and Morphine and Codeine in traces by GC-MS. We analyze the samples in different solvents and different concentrations.

DFTIVR + The sample contains morphine. Morphine is sheduled as illicit drug.

DHDX48 +

DJS2XK +

DLFBGB + Sample was found to contain Morphine. I am satisfied that the possession of powder in SN2 is not exempted from control by virtue of the Misuse of Drugs Regulations 2001 (as amended).




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Code Morphine

DPVGZK + The sample contain morphine and Lactose

DUCT4E +

%14.4 morphine

E44WTB + Morphine was identified in SM2 and percentage is 15.227%. In addition Lactose was identified.

E4CIFO +

EAQ4S6 + Color test,TLC and GCMS

EEGL2R + White powder analysed by GC/MS was found to contain Morphine. Mass spectra was similar to CRM

EGEENO + The sample contains 12.89% of Morphine and also contains hydromorphone

EJ4611 + The sample analyzed SM 2 contains morphine

F3LSGY + Codeine

FEKAVF +

FFUFOA + trace Codeine and Lactose

FIAC2C + We have found Morphine in SM-2 sample.

FJ7FUF + Sample number 2: there is ilicit drug (morphine)

FLL757 + In the seized sample was detected the presence of morphine

FVP0OM +

GDPMAM + Morphyne was detected in sample.

GFWFBO + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample indicates the lidocaine and morphine presence.

GGFGG9 + Sample represent white powder that contains controlled substance MORPHINE.

GI4HGG +

GNM3ON + controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule 1. (3) Morphine (7,8-didehydro-4,5-epoxy-17-methylmorphinan-3,6-diol) GNTW2Z + The sample 2019/1/SM-2 was found to contain Morphine.




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Code Morphine

GQQTND + Off-white powder 218 milligrams Morphine Hydrochloride (16%) Legal Status - Class A Glucose Legal Status - Not controlled

Legal Status refers to the classification of the drug found under the provisions of the Misuse of Drugs Act 1971 (as amended).

The MORPHINE content of the powder in item 2019/1/SM-2 has been accurately determined and has been found to exceed the limit of legal exception provided for by Section 4(3)(b) of the Misuse of Drugs Regulations 2001. The powder is therefore controlled as a Class A drug.

GY9CXA +

GZFJAG + We have found morphine in sm-2 samples.

HGOHHH +

HHHNYB + d-glucose

HMTUQD + Morphine was detected in the SM-2 sample.

HMW24R + Sample SM-2 found to contain morphine

HP2FIF +

I3H5RP +

IKEYL1 +

CODEINE AS MINORITY

INI2AA + White and odorless powder containing by weight 17% morphine expressed as free base and glucose. Morphine is present in form of hydrochloride.

INNQNN + The samples 2019/1/SM-2 contains morphine detected by GC/MS and FTIR. The percentage by weight of morphine is 13.4%.

IQQVQB + Powder from sample 2019-1SM-2 contain Morphine

IVWKXD + Morphine

J7VXH7 + Test sample 2019/1/SM-2 to contain Morphine

JAXXGC + morphine

JFLFE3 + Material analysis using the portable Raman equipment screening provided as a result morphine substance.The substance was confirmed by GCMS using a reference standard




Page 59 of 120

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Code Morphine

JHHNXN + Marquis reagent: positive; Cobalt thiocyanate: negative; GC-MS: morphine(result compared with library spectrum, retention time compared with certified reference material); FTIR: glucose (result compared with library spectrum); Lactose and glucose were differentiated with Woehlk test

JIOIBA + Also glucose was found.

JNQLXX + Using the techniques TLC, GC-MS & FTIR , Sample SM 2 was found to contain Morphine & Lactose.

K1NKKG + The MORPHINE content of the powder in item 2019/1/SM-2 has been accurately determined (i.e. 12% calculated as base) and has been found to exceed the limit of legal exception provided for by Section 4(3)(b) of the Misuse of Drugs Regulations 2001. The powder is therefore a Class A drug controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended).

KAPAAS + Analysis of a representative sample of the powder revealed the presence of morphine.

KC4CO7 +

KFULE7 + glucose

KHDDXD +

KII7PP +

KMBMUQ + This item contained 0.23 grams of white powder, found to contain Morphine, together with glucose. Morphine is a class A controlled substance under the Misuse of Drugs act 1971,as amended. Glucose is not a controlled substance. *Morphine is excepted from prohibition on importation, exportation and possession by Schedule 5 of the Misuse of Drugs Regulations 2001 when present in substances at concentrations less than 0.2%. As this was presented in an unmarked package and we are unable to ascertain the purity of the morphine in the powder, I am unable to comment on whether this exception would apply.

KNHLNG + SM-2 contains Morphine 15.87% (as base) and Lactose

KTBSBL + morphine was detected by GC/MS and quantified by GC/FID

KVYOOO + con Lactosa

L75533 + SM2 contient de la Morphine

LAWTLL + Dextrosa

LE5Z5Z + Based on the above analysis, the sample was found to contain Morphine




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Code Morphine

LRPCVG + SM2: was fond to contain Morphin, codeine and lactose

M9N99Q +

MELOFZ + Sample was a mixture of morphine HCL and Glucose

MJRX8A + The test sample contained morphine and glucose

MLKVZO + Glucose

MMQ2L2 +

MYD9WU - With the methods applied, it is not identified any controlled substances.

N4VGXV + -

N64P66 + Morphine HCl

NGGZGG +

impossible to quantify, standard not available

NNANPN + Morphine was found in the sample labeled 2019/1 / SM-2

NPO333 + Diluted with Glucose

OCQGSD + The white powder was analysed and found to contain Morphine.

OHJX22 + Morphine was found present in the sample SM-2

OHKWWZ + The sample contains Morphine

OIKEE1 + Morphine and dextrose were detected in SM-2 sample.

OIMJHC +

OKWXFO + Morphine is scheduled as illicit drug in France. The sample contains also glucose which is not scheduled as illicit drug in France.

P0NNSM + Sample 2019/1/SM-2 found to contain Morphine

P1JWGT + Morphine is a controlled drug under the Drug Abuse Prevention And Control Act Cap 131 of the Laws of Barbados.

PIRYEY + Sample 2019/1/SM-2 contains morphine, codeine and dextrose.

PKPTJM + One glass bottle containing 0.23 grammes of a powder containing 0.02 grammes of morphine.




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Code Morphine

PWZDFG + Morphine with Glucose.

QEJKPA + morphine was detected by GC/MS and quantified by GC/FID

QHQQUK + Controlled drug, Morphine, present in sample. Concentration approx 12%

QMGORR +

QPTTIT + We have found Morphine in SM-2 sample.

QQ7VFQ + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 1. (3) Morphine (7,8-didehydro-4,5-epoxy-17-methylmorphinan-3,6- diol).

QQTH7B +

QZZZGT + From screening test using (MR), and from confirmation test using (GC-MS) the sample was found to contain the controlled drugs Heroin and Morphine.

R5RPYM + Dextrose anhydrous, Butabarbital

R6BICL + In the 2019/1/SM-2 was proved the presence of Morphine and Lactose.

RH08SD + This sample contains morphine.

RKKTQP + White powdery substance of 2019/1/SM-2 was found to contain Morphine. Quantitative analysis was not carried-out to determine the weight of the drugs. Morphine is listed in The First Schedule of The Dangerous Drugs Act 1952.

RKPGFK +

RRJPPR + NARCOTIC. List I Unique Convention 1.961

RZDQQQ +

S8TL74 +

SAKRI4 ANP

SDJTNO + white powder containing 15.6%w/w morphine. The sample contains glucose.

SG5IQS + SM 2 contains:Morphine and Glucose, with 12.18 % Morphine base

SGBOPO + The powder was analysed and found to contain Morphine. Morphine is a class A controlled drug within the provisions of the Misuse of Drugs Act 1971.

SHLDPB +




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Code Morphine

SU4NXI + GLUCOSE

T2S333 + no quantification usually

TAAFSW + The sample contains morphine (12.5%) and glucose.

TCVV6F + the sample SM-2 was found Morphine

TIIISI +

TMWUWW + 2019/1/SM-2 was confirmed for morphine. Morphine is schedule II controlled substance in the United States.

TTQXMT + Sample 2019/1/SM-2 consists of white powder. Morphine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample.

TTTILP + Identified by GCMS & LCMSMS techniques and quantified by HPLC technique.

TUVPUU -

TXVZAJ + white powder containing morphine

UEAZZ3 +

SM-2 was found to contain morphine.

UIFULT + SCREENING BY RAMAN AND CONFIRMATION BY GC MSD THIS SAMPLE ALSO CONTAINS CODEINE

V6ESR5 +

V7AWBG +

VF8TL1 + Morphine controlled under Malaysian Dangerous Drugs Act

VHYXAH + MORPHINE AND TRAZE AMOUNTS OF CODEINE IN MANNITOL POWDER

W0OABU +

W4X1SX + -

WCEEWA + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 1. (3) Morphine (7,8-didehydro-4,5-epoxy-17-methylmorphinan-3,6- diol).

WJRG8W + the sample contains drugs, morphine. And also it contains sucrose.

X1A11B + morphine




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Code Morphine

X66O46 + Sample 2019/1/SM-2 a white powder gave a positive result for morphine, substance under national legislation on drugs.

X6OWJR + Morphine

X8QXDX + glucose

XM00GQ + Sample with morphine and glucose. Identification of morphine by GC/MS. Identification of glucose by Raman, FTIR and by GC/MS after MSTFA derivatization.

XNJQP7 ANP THERE´S NO SUSTANCE FOUNDED

XPYAOU + Sample tested positive for opiates. Negative for Heroin but positive for Morphine.

XYXPCP + SM2 contains Morphine.

Y31S2M +

Y45Y4Y + It was found glucose.

Y7M3HZ + morphine

YAIDDI + It contains morphine and codeine. It also contains glucose and lactose.

YHKKKB +

YL2O3B + The sample was found to contain 11.9% of morphine (as base).

YXNYHY + Morphine and glucose

YYYJYT + The Test sample 2019/1/SM-2 was analyzed by Thin Layer Chromatography technique and was found to contain Morphine and Glucose.

ZAOGZZ + 2019/1/SM-2 contains morphine, glucose, caffeine and codeine

ZE8ZAZ + Positive to morphine

ZFFBFT +

ZIGGI6 + The sample contains 12,81±0,70 weight% morphine-base.

ZPZ8SZ +

ZUZ1ZZ +




Page 64 of 120

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Code Morphine

ZWM2QG + Sample 2019/1/SM-2 was found to contain morphine




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

0E49T9 I I SI I

0OGHZR SI SI I


1999Y6 S I I

1CNMZQ SI

1F633N SI

1IDFP1 SI I

1W4YMX SI S S I

252CCB I I SI

2F51LA I SI

2MPUPL S I I

2Q22HI S S S I I

2TCPHH S S S I

2XGWKJ I SI

2XXLPG S S S I

313337 S S I

3332NG S I SI SI

33ZZO3 S I I

36BDU6 S I

3FT9VW S S I I

3RF39E S S I


3TY2WR S S I

444444 SI

44E44K S S S I I I

4AXZ9A I SI

4CNIOX I SI

4J4R44 S SI

4XX6CI S S S SI I

4YFBKI S I I

4Z4BDP S S S I I I


5E0FMO I I I S





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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

5FFFFF S S S SI I




66H8C3 S S I I

6JFAWA SI I

6RFSER I I I S


6WDJTJ I

6YZTRZ SI I

7ED7SR I

7MM6GH SI

7WA60O S I SI SI

8FXHXS SI

8WWDB W

I

9IA9GY S S S I I

9OOEII S S S I I

9SMHJ8 I SI

9YCKGZ S S I I

A441YE I S

AC11BX I SI I

ADW75B S S I

AFUXM7 SI I

AMRMTF I SI

AO8UQ6 S S I I

AODFDP S S S I

AXU99T I

AYTE1E S SI SI I

AZUH8X SI SI SI I

B3FTN3 S S S I I

BBBLO2 S S I SI


BIA0EZ SI

BMPXHL S S S I I

BRFRWM I SI

BRUEIH SI I

BTKUST SI I




Page 67 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

BWSSKK S I I

BYBCVB S I I

BZDD95 I

C5MUOL SI I

C9BRBB I I

CJWQGK SI

CYLW4Y SI I

DDVDDE S SI I

DFTIVR SI I I

DHDX48 S I

DJS2XK S S I

DLFBGB S S I

DPVGZK S I I

DUCT4E S I I


E4CIFO S S I I

EAQ4S6 S S SI I

EEGL2R S S S I I

EGEENO I SI I

EJ4611 S I I

F3LSGY I I SI I

FEKAVF S S I I

FFUFOA S I I I

FIAC2C SI SI SI I

FJ7FUF S S I I

FLL757 SI I

FVP0OM S I I

GDPMAM S S I I

GFWFBO S S I



GNM3ON SI I I

GNTW2Z SI SI SI I

GQQTND S S S I I

GY9CXA S I I

GZFJAG SI SI SI I

HGOHHH SI




Page 68 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

HHHNYB SI I SI

HMTUQD SI I

HMW24R S I

HP2FIF SI

I3H5RP S S S I

IKEYL1 S S S I I

INI2AA I I

INNQNN I SI I

IQQVQB S S I I

IVWKXD SI

J7VXH7 S I

JAXXGC SI

JFLFE3 S I I

JHHNXN S S SI I

JIOIBA S I I I I

JNQLXX S S SI SI

K1NKKG S S S I I

KAPAAS SI

KC4CO7 I S

KFULE7 I SI

KHDDXD S I I

KII7PP SI

KMBMUQ S S I I

KNHLNG S S S I I

KTBSBL SI I


L75533 S I I


LE5Z5Z S I

LRPCVG I SI

M9N99Q S S S I I

MELOFZ S S S I I

MJRX8A S I

MLKVZO S S S I I

MMQ2L2 S I SI I

MYD9WU I I I

N4VGXV SI I I SI




Page 69 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210


NGGZGG S S S I

NNANPN I I SI

NPO333 S I I

OCQGSD S I I


OHKWWZ SI I

OIKEE1 I SI I

OIMJHC SI

OKWXFO I I


Janovsky

P1JWGT S I I

PIRYEY S S S I I

PKPTJM S S I SI

PWZDFG S S I I

QEJKPA SI

QHQQUK SI

QMGORR I SI

QPTTIT SI SI SI I


QQTH7B I SI


R5RPYM I I S

R6BICL I SI I I I

RH08SD S I I

RKKTQP S S I


RRJPPR S S S I

RZDQQQ S SI SI

S8TL74 I SI

SAKRI4 I

SDJTNO I I S

SG5IQS S I I

SGBOPO S I

SHLDPB S I SI SI

SU4NXI SI

T2S333 SI I




Page 70 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210


TCVV6F S S I

TIIISI S S S I I

TMWUW W

S I

TTQXMT S S I

TTTILP I S S SI I I

TUVPUU I S

TXVZAJ I I SI

UEAZZ3 S S I I

UIFULT I SI

V6ESR5 I S

V7AWBG SI SI

VF8TL1 S S SI I

VHYXAH I SI I

W0OABU S I

W4X1SX SI

WCEEWA S I I

WJRG8W I I SI I

X1A11B SI

X66O46 S S I I

X6OWJR I SI I

X8QXDX SI I



XPYAOU SI

XYXPCP S S S I I

Y31S2M I I

Y45Y4Y I I SI

Y7M3HZ SI I

YAIDDI I

YHKKKB SI I

YL2O3B I SI

YXNYHY S I


ZAOGZZ S S S I I

ZE8ZAZ SI




Page 71 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

ZFFBFT I SI I

ZIGGI6 S I I SI I

ZPZ8SZ I SI I SI

ZUZ1ZZ S I

ZWM2QG S S SI




Page 72 of 120

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0E49T9 Methamphetamine

0OGHZR Metanphetamine

13S3E5 Metamfetamine

1999Y6 metamphetamine

1CNMZQ methamphetamine

1F633N metamphetamine

1IDFP1 Methamphetamine

1W4YMX metanfetamina

252CCB Methamphetamine

2F51LA methamphetamine

2MPUPL Methamphetamine hydrochoride

2Q22HI Methamphetamine

2TCPHH Metamfetamine, caffeine

2XGWKJ metamfetamine

2XXLPG metamphetamine

313337 Metamphetamine

3332NG metamphetamine

33ZZO3 morphine

36BDU6 Methamphetamine

3FT9VW METHAMPHETAMINE AND CAFFEINE

3RF39E METAMFETAMINE, CAFFEINE

3SMK33 methamphetamine

3TY2WR Metamfetamine

444444 Metamfetamine

44E44K metamfetamine

4AXZ9A Methamphetamine HCl

4CNIOX metamfetamine

4J4R44 metamfetamine

4XX6CI metamfetamine

4YFBKI Metamfetamine and Caffeine

4Z4BDP methamphetamine

54CQ2S Methamphetamine and Caffeine

5E0FMO Metamphetamine

5FFFFF Methamphetamine, Caffeine

5HWYZN Metamfetamine

5Q555E metamfetamine

6666WM METAMFETAMINE, CAFFEINE AND GLUCOSE




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66H8C3 Metamfetamine

6JFAWA Metamfetamine,Caffine

6RFSER metamfetamine

6RVR5A Metamfetamine

6WDJTJ Metamfetamine and Caffeine

6YZTRZ Metamphetamine

7ED7SR Methylamphetamine

7MM6GH Methamphetamine

7WA60O Methamphetamine

8FXHXS METAMPHETAMINE

8WWDBW Methamfetamine

9IA9GY Metamphetamine

9OOEII methamphetamin,caffeine

9SMHJ8 metamfetamine

9YCKGZ Methamphetamine

A441YE metamphetamine, caffeine anddimethylamphetamine

AC11BX Metamfetamine

ADW75B Methamphetamine and Caffeine

AFUXM7 Metamfetamine

AMRMTF Metamfetamine, Caffeine

AO8UQ6 methamphetamine

AODFDP Methamphetamine and caffeine

AXU99T Methamphetamine

AYTE1E Methylamphetamine & Caffeine

AZUH8X Methampetamine

B3FTN3 Metamfetamine and caffeine

BBBLO2 Metamfetamine

BEPFVN methamphetamine

BIA0EZ Metamfetamine

BMPXHL methamphetamine

BRFRWM metamfetamine

BRUEIH Metamfetamine

BTKUST methamphetamine

BWSSKK clorhidrato de metanfetamina

BYBCVB METANFETAMINA HCl and CAFEINE

BZDD95 Metamphetamine

C9BRBB Metamfetamine

CJWQGK methamphetamine and caffeine

CYLW4Y metamfetamine chlorhydrate

DDVDDE Metanfetamine, Caffeine and glucose

DFTIVR Méthamphétamine

DHDX48 Methamphetamine-




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DJS2XK Metamfetamine

DLFBGB Methylamphetamine

DPVGZK Metamfetamine

DUCT4E methamphetamine

E44WTB Metamfetamine

E4CIFO Metamfetamine

EAQ4S6 Methamfetamine and caffeine

EEGL2R Metamfetamine

EGEENO Methamphetamine

EJ4611 METANFETAMINE

F3LSGY Metamfetamine

FEKAVF 4-Benzyloxy-N-methylamphetamine

FFUFOA Metamfetamine

FIAC2C Methampetamine

FJ7FUF Metamfetamine

FLL757 Metanfetamine

FVP0OM Metamfetamine

GDPMAM Methamphetamine, caffeine

GFWFBO Methanphetamine

GGFGG9 Metamfetamine

GNM3ON Methamphetamine

GNTW2Z 1. Methamfetamine 2. Caffeine

GQQTND Methylamphetamine Hydrochloride

GY9CXA metamfetamine

GZFJAG Methamphetamine

HGOHHH methamphetamine

HHHNYB metamphetamine HCl

HMTUQD Metamphetamine and caffeine

HMW24R Methamphetamine and Caffeine

HP2FIF Metamfetamine

I3H5RP methamphetamine

IKEYL1 METHAMPHETAMINE

INI2AA metamfetamine

INNQNN Metamfetamine and caffeine

IQQVQB Methamphetamine

IVWKXD Methamphetamine

J7VXH7 Metamfetamine

JAXXGC metamfetamine

JFLFE3 Metamfetamine

JHHNXN Methamphetamine

JIOIBA Methamphetamine HCl

JNQLXX Caffeine & Methamphetamine




Page 75 of 120

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K1NKKG Methamphetamine Hydrochloride

KAPAAS Methylamphetamine

KC4CO7 Methamphetamine

KFULE7 metamphetamine HCl

KHDDXD Metamphetamine

KII7PP Metamfetamine

KMBMUQ Methamphetamine

KNHLNG Methamphetamine HCl

KTBSBL metamfetamine

KVYOOO Metanfetamina

L75533 la Méthamphétamine

LAWTLL Metanfetamina

LE5Z5Z Metamfetamine

LRPCVG Metamfetamine

M9N99Q methamphetamine

MELOFZ Methylamphetamine HCL

MJRX8A METHAMFETAMINE

MLKVZO Methamfetamine-Cafeine

MMQ2L2 metamphetamine

MYD9WU Metamphetamine

N4VGXV metanfetamina

N64P66 Methylamphetamine HCl

NGGZGG metanphetamine

NNANPN Metamfetamine

NPO333 Metamfetamine

OCQGSD Methylamphetamine

OHJX22 Metamfetamine

OHKWWZ Metamfetamine

OIKEE1 Metamphetamine and cafeine

OIMJHC Metamfetamine

OKWXFO metamfetamine, caffeine

P0NNSM Methamphetamine

P1JWGT Methamphetamine

PIRYEY Methamphetamine

PKPTJM Methamphetamine

PWZDFG methamphetamine and Caffeine

QEJKPA metamphetamine

QHQQUK Metamfetamine

QMGORR Metamphetamine

QPTTIT Methampfetamine

QQ7VFQ Methamphetamine

QQTH7B metamfetamine




Page 76 of 120

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QZZZGT Methamphetamine, Caffeine

R5RPYM Metamfetamine

R6BICL Metanfetamine + Caffeine + Lactose

RH08SD Methamphetamine

RKKTQP Methamphetamine and Caffeine

RKPGFK Metamfetamine

RRJPPR methamphetamine

RZDQQQ METAMFETAMINE 10.1%

S8TL74 METAMFETAMINE

SAKRI4 metamfetamine

SDJTNO metamfetamine

SG5IQS Metamfetamine

SGBOPO Methylamphetamine and Caffeine

SHLDPB metamfetamine

SU4NXI METAMPHETAMIN, CAFEIN

T2S333 Metamfetamine hcl

TAAFSW Methamphetamine Hydrochloride

TCVV6F Methamphetamine, Caffeine

TIIISI Metanfetamine

TMWUWW Methamphetamine and Caffeine

TTQXMT Metamfetamine

TTTILP METAMFETAMINE

TXVZAJ Methamphetamine

UEAZZ3 Methamphetamine

UIFULT METHAMPHETAMINE

V6ESR5 Metamfetamine

V7AWBG METAMFETAMINE

VF8TL1 Metamfetamine and Caffeine

VHYXAH METAMFETAMINE

W0OABU Metanfetamina

W4X1SX Metamfetamine

WCEEWA Methamphetamine

WJRG8W Methamphetamine

X1A11B methamphetamine

X66O46 methamphetamine

X6OWJR Metamfetamine

X8QXDX Methamphetamine

XM00GQ Metanfetamine

XNJQP7 MEFEDRONA

XPYAOU Methamphetamine

XYXPCP Methamphetamine and caffeine

Y45Y4Y Metamfetamine




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Y7M3HZ yes

YAIDDI Metamfetamine and Amphetamine

YL2O3B methamphetamine

YXNYHY Methamphetamine

YYYJYT Metamfetamine, Caffeine and Glucose

ZAOGZZ methamphetamine

ZE8ZAZ Metamfetamine and Caffeine

ZFFBFT metamfetamine

ZIGGI6 metamfetamine

ZPZ8SZ METAMPHETAMINE, CAFFEINE

ZUZ1ZZ METAMPHETAMINE

ZWM2QG Metamfetamine and caffeine




Page 78 of 120

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Code Caffeine Metamfetamine

0E49T9 + + The sample contained 7.5% metamphetamine. There was caffeine present in the sample.

0OGHZR + + adulterant: caffeine

13S3E5 - +

1999Y6 + +

1CNMZQ + - sample found to contain methamphetamine and caffeine

1F633N + + a substance identified is metamphetamine

1IDFP1 + + Methamphetamine+Caffeine

1W4YMX + +

252CCB + + Analysis revealed the presence of methamphetamine and caffeine

2F51LA + + caffeine

2MPUPL - + White poder containing Metahamphetamine 8,96 % (base)

2Q22HI + + The sample contained 12.6% (w/w) Methamphetamine (base).

2TCPHH + + Results of screening tests were positive for amfetamines. Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with metamfetamine and caffeine.

2XGWKJ + +

2XXLPG + + The analysis confirmed that SM 3 contains metamphetamine (as controlled drug) but we are not able to give a quantitative result). We found also lactose and caffeine as non controlled drugs.

313337 + + Metamphetamine, Caffeine

3332NG + + caffeine

33ZZO3 + + Morphine is on the list of drugs.

36BDU6 + + Sample 2019/1/SM-3 was found containing methamphetamine and caffeine

3FT9VW + +




Page 79 of 120

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3RF39E + +

METAMFETAMINE, CAFFEINE

3SMK33 + + GD of RM nr. 1088 of 05.10.2014

3TY2WR + + Methylamphetamine is a Class A drug subject to the provisions of the Misuse of Drugs Act 1971.

444444 + + Metamfetamine hydrochloride (9 % base), caffeine (18 %) and glucose.

44E44K + + Included in the list of narcotic drugs whose turnover in the Republic of Uzbekistan Disallowed (List I)

4AXZ9A + + A composite was formed from 1 unit for testing of 1 unit received. Methamphetamine HCl, caffeine and dextrose confirmed in the composite.

4CNIOX + + The sample containe 9% metamfetamine, 17% caffeine and glucose. metamphetamine is controlled by the Royal Decree of the 6th of september 2017

4J4R44 + + contains also caffeine (25.7 %)

4XX6CI + + The test sample 2019/1/SM-3 was found to contain the controlled drug metamfetamine. Caffeine was also found in the sample.

4YFBKI + + SM-3 sample was prepared from a seizure containing 9.03% (w/w) Metamfetamine base. The test sample also contained Caffeine.

4Z4BDP + + The sample contains methamphetamine, caffeine.

54CQ2S + + SM3 was contained 7.68% Methamphetamine and 90% Caffeine.

5E0FMO + + Presence of metamfetamine hydrochloride, glucose and caffeine was detected in the sample.

5FFFFF + + Methamphetamine and Caffeine were identified.

5HWYZN + + The sample contains metamfetamine, caffeine and lactose as an adulterant.Metamfetamine is controlled in Poland.

5Q555E + + metamfetamine,caffeine

6666WM + + WE FOUND A MIXTURE OF METAMFETAMINE, CAFFEINE AND GLUCOSE.

66H8C3 + + WAS FOUND Metamfetamine. DEXTROSE AND CAFFEINE WERE FOUND TOO.

6JFAWA + +

6RFSER + + mixture of metamfetamine and caffeine and glucose; caffeine 18 % w/w; glucose 67.5 % w/w




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6RVR5A + + The sample 2019/1/SM3 contain Metamfetamine and caffeine .

6WDJTJ + + Positive to Metamfetamine and Caffeine.

6YZTRZ - +

7ED7SR + +

Powder contains methylamphetamine. Methylamphetamine is a controlled drug under the Misuse of Drugs Act 1977 to 2016

7MM6GH + + Sample contains 8.9 % methamphetamine and caffeine.

7WA60O + + 9.8% of Methamphetamine is found with an amount of caffeine.

8FXHXS + +

CAFFEIN

8WWDBW + + SM-3 was found contain Methamfetamine and traces of Caffiene and Glucose

9IA9GY - + We can´t cuantified due to we don´t have reference pattern

9OOEII + +

9SMHJ8 + + the pink powder contains metamfetamine (10.7%w/w) which is controlled by national law

9YCKGZ + + Methamphetamine was identified by GC/MS

A441YE + + the main compounds we founds in SM-3 are metamphetamine and caffeine after GC / MS injection. Excess compound is in a trace state.

AC11BX + + Caffeine

ADW75B + + This sample was found to contain Methamphetamine which is a Class A controlled substance under the Misuse of Drugs Act 1971. It was also found to contain Caffeine which is not controlled under the Misuse of Drugs Act 1971.

AFUXM7 + + It has been detected the presence of Metamfetamine in the sample.

AMRMTF + +

AO8UQ6 + + Sample 2019/1 / SM-3 contains caffeine and methamphetamine.

AODFDP + + It was detected the presence of methamphetamine and caffeine in the sample analysed

AXU99T + + In the test sample 2019/1/SM-3 was detected methamphetamine In the test sample 2019/1/SM-3 was also detected caffein

AYTE1E + + Methylamphetamine & caffeine confirmed in SM-3




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AZUH8X + + We have found Methampetamine and Caffeine by adulterant in SM-3 sample.

B3FTN3 + + The sample 2019/01-SM-3 contains Metamfetamine detected by GC-MS and FT-IR. The percentage by weight of Metamfetamine is 9.64%.

BBBLO2 + + Presence of metamfetamine and caffeine was confirmed qualitatively

BEPFVN + + The sample contains methamphetamine. The concentration has not been determined.

BIA0EZ + + The sample contains metamfetamine and caffeine.

BMPXHL + + caffeine

BRFRWM + + Pale pink powdercontaining 11.2% of metamfetamine

BRUEIH + +

BTKUST + + List of narcotics drugs whose circulation in the territory of the Republic of Uzbekistan is prohibited (Appendix to the resolution of the Cabinet of Ministers of the Republic of Uzbekistan ¼878 date 27.10.2018 y.)

BWSSKK + + clorhidrato de metanfetamina 10,9%base, glucosa y cafeína.

BYBCVB + + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of CAFFEIN in the sample.

BZDD95 + + SM-3 contains metamphetamine (7.4% as free base) and caffeine.

C5MUOL + +

C9BRBB + + The sample contains metamfetamine which is listed as a controlled drug according to french order, appendix III of February 22nd 1990.

CJWQGK + +

CYLW4Y + + metamfetamine (10,0% as base) + cafeine (16%) + lactose

DDVDDE + + We started with colourimetric test, then We could identify Glucose by FTIR and Metanfetamine and Caffeine by GC-MS. We analyze the samples in different solvents and different concentrations.

DFTIVR + + The sample contains Méthamphétamine Méthamphétamine is sheduled as illicit drug.

DHDX48 + + cafeine

DJS2XK + +




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DLFBGB + + Sample was found to contain Methylamphetamine and Caffeine

DPVGZK + + The sample contain metamfetamine, Caffeine and Lactose

DUCT4E + + %9.4 methamphetamine

E44WTB + + Metamfetamine was identified in SM3 and percentage is 13.28%. In addition Lactose and caffeine were identified

E4CIFO + +

EAQ4S6 + + Color test,TLC and GCMS

EEGL2R + + Slightly pink powder analysed by GC/MS was found to contain Metamfetamine. Mass spectra was similar to CRM

EGEENO + + The sample contains 9.39% of Methamphetamine and also contains Caffeine

EJ4611 + + The sample analyzed SM 3 contains caffeine and methamphetamine

F3LSGY + + Caffeine

FEKAVF + + Caffeine

FFUFOA + + Caffeine

FIAC2C + + We have found Methampetamine and Caffeine by adulterant in SM-3 sample.

FJ7FUF + + Sample number 3: there is ilicit drug (metamfetamine)

FLL757 + + In the seized sample was detected the presence of metanfetamine an caffeine, which is adulterants / diluents FVP0OM - +

GDPMAM + + Methamphetamine and caffeine were detected in the sample.

GFWFBO + + The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample indicates the lidocaine and methanphetamine presence.

GGFGG9 + +

Sample represent light rose powder that contains controlled substance METAMFETAMINE and Caffeine.

GI4HGG + +




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GNM3ON + + "controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule 1 18. Methamphetamine (N,a-dlmethylbenzeneethanamine) calculated as the hydrochloride 11 % (w/w)"

GNTW2Z + + The sample 2019/1/SM-3 was found to contain Methamfetamine and Caffeine.

GQQTND + + Pink Powder 221 milligrams

Methylamphetamine Hydrochloride (11%) Legal Status - Class A

Glucose, Legal Status - Not controlled Cafffeine, Legal Status - Not controlled


GY9CXA + +

GZFJAG + + We have found Methamphetamine in sm-3 samples. We have also found %17,289 caffeine adulterant.

HGOHHH + + The seized material contains drugs methamphetamine and uncontrolled substance caffeine

HHHNYB + + caffeine, d-glucose

HMTUQD + + Metamphetamine and caffeine were detected in the SM-3 sample.

HMW24R + + Sample SM-3 found to contain methamphetamine and caffeine

HP2FIF ANP +

I3H5RP + + methamphetamine plus caffeine

IKEYL1 + + CAFFEINE

INI2AA + + pink powder with characteristic smell containing metamfetamine and glucose

INNQNN + +

The samples 2019/1/SM-3 contains metamfetamine and caffeine detected by GC/MS and FTIR. The percentage by weight of metamfetamine is 9.3%.

IQQVQB + + Powder from sample 2019-1SM-3 contain Methamphetamine with Caffeine

IVWKXD + + Methamphetamine

J7VXH7 + + Test sample 2019/1/SM-3 to contain Methamphetamine and Caffeine

JAXXGC + + metamfetamine, caffeine




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JFLFE3 - + Material analysis using the portable Raman equipment screening provided as a result metamfetamine substance.The substance was confirmed by GCMS using a reference standard

JHHNXN + + Marquis reagent: positive; Cobalt thiocyanate: negative; GC-MS: methamphetamine, caffeine (results compared with library spectra, retention time of methamphetamine compared with reference material); FTIR: glucose (result compared with library spectrum); FTIR after extraction with ethanol: dried extract - caffeine spectrum with bands indicative of sulphate group presence, residue - glucose (spectra were compared with library); Lactose and glucose were differentiated with Woehlk test

JIOIBA + + Also caffeine and glucose was found.

JNQLXX + + (i) Using the techniques TLC, GC-MS & FTIR , Sample SM 3 was found to contain Caffeine & Methamphetamine. (ii) Using Technique GC-FID, Quantification of SM 3 was done and found to contain Methamphetamine 9.0%.

K1NKKG + +

Sample 2019/1/SM-3 contained METHAMPHETAMINE Hydrochloride, at a concentration of 9% (calculated as base). METHAMPHETAMINE Hydrochloride is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended).

KAPAAS + + Analysis of a representative sample of the powder revealed the presence of methylamphetamine with a purity of approximately 11% (calculated as base).

KC4CO7 + +

KFULE7 - + glucose, caffeine

KHDDXD + + This sample was adulterated with caffeine.

KII7PP + +

KMBMUQ + + This item contained 0.23 grams of off white powder, found to contain Methylamphetamine at a concentration of 10%, together with caffeine and glucose. Methylamphetamine is a Class A controlled substance under the Misuse of Drugs Act 1971, as amended. Caffeine and glucose are not controlled substances.

KNHLNG + + SM-3 contains Methamphetamine 9.17% (as base), Caffeine 17.42 % and Lactose

KTBSBL + + metamfetamine was detected by GC/MS and quantified by GC/FID

KVYOOO + + Lactosa y Cafeina

L75533 + + SM3 contient de la Méthamphétamine et la Caféine

LAWTLL + + Dextrosa y cafeina




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LE5Z5Z ANP + Based on the above analysis, the sample was found to contain Metamfetamine

LRPCVG + + SM3: was fond to contain Metamfetamine, Caffein and lactose

M9N99Q + +

MELOFZ + +

Sample was a mixture of methylamphetamine HCL< Glucose and Caffeine

MJRX8A + + The test sample contained methamphetamine and glucose,

MLKVZO + + Glucose

MMQ2L2 + + caffeine

MYD9WU + + The sample contains metamphetamine. The content of metamphetamine is determined to 11 % (as metamphetaminesulphate). Methamphetamine is a controlled substance in X.

N4VGXV + + cafeína

N64P66 + + Methylamphetamine HCl, Caffeine

NGGZGG + +

NNANPN + + Metamphetamine was found in the sample labeled 2019/1 / SM-3

NPO333 + + Also contains Caffeine

OCQGSD + + The beige coloured powder was analysed and found to contain Methylamphetamine.

OHJX22 + + Metamfetamine & Caffeine were found present in the sample SM-3

OHKWWZ + + The sample contains Metamfetamine and Caffeine

OIKEE1 + + Metamphetamine, cafeine and dextrose were detected in SM-3 sample.

OIMJHC + +

OKWXFO + + Metamfetamine is scheduled as illicit drug in France. The sample contains also glucose and caffeine which are not scheduled as illicit drugs in France.

P0NNSM + + Sample 2019/1/SM-3 found to contain Methamphetamine and Caffeine

P1JWGT + + Methamphetamine is a controlled drug under the Drug Abuse Prevention And Control Act Cap 131 of the Laws of Barbados.




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PIRYEY + + Sample 2019/1/SM-3 contains methamphetamine, caffeine and dextrose.

PKPTJM + + One glass bottle containing 0.22 grammes of a powder containing 0.02 grammes of methamphetamine.

PWZDFG + + The sample contains methamphetamine and caffeine.

QEJKPA + + metamphetamine was detected by GC/MS and quantified by LC/MS-MS

QHQQUK + + Controlled drug, Metamfetamine, present in sample. Concentration approx 9,5%. Caffeine (no controlled drug) was also present in sample.

QMGORR ANP +

QPTTIT + + We have found Methampetamine and Caffeine by adulterant in SM-3 sample.

QQ7VFQ + + The sample was found to contain a controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 18. Methamphetamine (N-alpha- dimethylbenzeneethanamine)

QQTH7B + + caffeine

QZZZGT + + From screening test using (MR), and from confirmation test using (GC-MS) the sample was found to contain the controlled drug Methamphetamine, and uncontrolled drug caffeine.

R5RPYM + + Caffeine, Dextrose Anhydrous

R6BICL + + In the 2019/1/SM-3 was proved the presence of Metanfetamine, Caffeine and Lactose.

RH08SD + + This sample is methamphethamine.

RKKTQP + + Pale orange coloured powdery substance of 2019/1/SM-3 was found to contain Caffeine and 9.0% of Methamphetamine. Quantitative analysis was not carried out to determine the amount of caffeine. Methamphetamine is listed in The First Schedule of The Dangerous Drugs Act 1952 meanwhile Caffeine is listed in The First Schedule of The Poisons Act 1952.

RKPGFK + +

RRJPPR + + PSYCHOTROPY List II Vienna Convention 1971

RZDQQQ - +

S8TL74 + + CAFFEINE

SAKRI4 ANP +




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SDJTNO + + pink powder containing 10.1%w/w metamphetamine and caffeine. The sample contains glucose.

SG5IQS + + SM 3 contains:Metamfetamine, Caffeine and Glucose, with 9.50 % Metamfetamine base

SGBOPO + + The powder was analysed and found to contain Methylamphetamine and Caffeine. Methylamphetamine is a class A controlled drug within the provisions of the Misuse of Drugs Act 1971. Caffeine is not a controlled drug within the provisions of the Misuse of Drugs Act 1971.

SHLDPB + + caffeine

SU4NXI + + GLUCOSE

T2S333 + +

TAAFSW + + The sample contains methamphetamine hydrochloride (10.5% as methamphetamine free base) and glucose and caffeine.

TCVV6F + + the sample SM-3 was found Methamphetamine and Caffeine

TIIISI + +

TMWUWW + + 2019/1/SM-3 was confirmed for methamphetamine and caffeine. Methamphetamine is a schedule II controlled substance in the United States. Caffeine is not a controlled substance in the United States.

TTQXMT ANP + Sample 2019/1/SM-3 consists of light orange powder. Metamfetamine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample. TTTILP + + Identified by GCMS & LCMSMS techniques and quantified by GC-FID technique.

TUVPUU + -

TXVZAJ + + pink powder containing methamphetamine and caffeine

UEAZZ3 + + SM-3 was found to contain 8.94 % methamphetamine and also caffeine.

UIFULT + + THE SAMPLE ALSO CONTAINS CAFFEINE CONFIRMED BY GCMSD

V6ESR5 + +

V7AWBG + +

VF8TL1 + + Metamfetamine controlled under Malaysian Dangerous Drugs Act. Caffeine controlled under Malaysian Poison Act.

VHYXAH + + METAMFETAMINE IN MANNITOL POWDER




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W0OABU + + Cafeína

W4X1SX + +

-

WCEEWA + + The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 18 Methamphetamine (N,a-dimethylbenzeneethanamine) calculated as the hydrochloride 11% w/w

WJRG8W + + The sample contains drugs, methamphetamine It contains also caffeine

X1A11B + + methamphetamine and cafeine

X66O46 + + Sample 2019/1/SM-3 an off-white powder gave a positive result for methamphetamine, substance under national legislation on drugs.Caffeine was also detected.

X6OWJR + + Metamfetamine+Caffeine

X8QXDX + + caféine Glucose

XM00GQ + + Sample with metanfetamine, caffeine and glucose. Identification of metanfetamine and caffeine by GC/MS. Identification of glucose by Raman, FTIR and by GC/MS after MSTFA derivatization.

XNJQP7 + - MEFEDRONA POSITIVE

XPYAOU ANP + Sample tested positive for amphetamine type stimulants. Methamphetamine confirmed in the material.

XYXPCP + + SM3 contains Methamphetamine

Y31S2M - +

Y45Y4Y + + It was found caffeine, glucose.

Y7M3HZ + + metahamphetamine and adulterant (caffeine)

YAIDDI + + It contains metamfetamine in a purity of 9.5% and amphetamine in trace (below LLOQ). It also contains cafeine, glucose, lactose and fatty acids.

YHKKKB + +

YL2O3B + + The sample was found to contain 9.3% of methamphetamine (as base).

YXNYHY + + Methamphetamine 11,8%, cafeine and glucose

YYYJYT + + The Test sample 2019/1/SM-3 was analyzed by Thin Layer Chromatography technique and was found to contain Metamfetamine, Caffeine and Glucose.




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ZAOGZZ + + 2019/1/SM-3 contains methamphetamine, caffeine and glucose

ZE8ZAZ + +

Positive to metamfetamine (drug of abuse) and caffeine (adulterant)

ZFFBFT + +

ZIGGI6 + + The sample contains 8,88±0,55 weight% metamfetamine-base. The sample also contains caffeine.

ZPZ8SZ + +

ZUZ1ZZ + + cafeine

ZWM2QG + + Sample 2019/1/SM-3 was found to contain 9.0 % metamfetamine and caffeine




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

0E49T9 I I SI I

0OGHZR SI SI I


1999Y6 S I I

1CNMZQ SI

1F633N SI

1IDFP1 SI I

1W4YMX SI S S I

252CCB I I SI

2F51LA I SI

2MPUPL S I I

2Q22HI S S S I I

2TCPHH S S S I

2XGWKJ I SI

2XXLPG S S S I

313337 S S I

3332NG S I SI SI

33ZZO3 S I I

36BDU6 S I

3FT9VW S S I I

3RF39E S S I


3TY2WR S S I

444444 SI

44E44K S S S I I I

4AXZ9A I SI

4CNIOX I SI

4J4R44 S SI

4XX6CI S S S SI I

4YFBKI S I I

4Z4BDP S S S I I I






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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

5E0FMO I I I S

5FFFFF S S S SI I




66H8C3 S S I I

6JFAWA SI I

6RFSER I I I S


6WDJTJ I

6YZTRZ SI I

7ED7SR I

7MM6GH SI

7WA60O S I SI SI

8FXHXS SI

8WWDB W

I

9IA9GY S S S I I

9OOEII S S S I I

9SMHJ8 I SI

9YCKGZ S S I I

A441YE I S

AC11BX I SI I

ADW75B S S I

AFUXM7 SI I

AMRMTF I SI

AO8UQ6 S S I I

AODFDP S S S I

AXU99T I

AYTE1E S SI SI I

AZUH8X SI SI SI I

B3FTN3 S S S I I

BBBLO2 S S I SI


BIA0EZ SI

BMPXHL S S S I I

BRFRWM I SI

BRUEIH SI I




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

BTKUST SI I

BWSSKK S I I

BYBCVB S I I

BZDD95 I

C5MUOL SI I

C9BRBB I I

CJWQGK SI

CYLW4Y SI I

DDVDDE S SI I

DFTIVR SI I I

DHDX48 S I

DJS2XK S S I

DLFBGB S S I

DPVGZK S I I

DUCT4E S I I


E4CIFO S S I I

EAQ4S6 S S SI I

EEGL2R S S S I I

EGEENO I SI I

EJ4611 S I I

F3LSGY I I SI I

FEKAVF S S I I

FFUFOA S I I I

FIAC2C SI SI SI I

FJ7FUF S S I I

FLL757 SI I

FVP0OM S I I

GDPMAM S S I I

GFWFBO S S I



GNM3ON SI I I

GNTW2Z SI SI SI I

GQQTND S S S I I

GY9CXA S I I

GZFJAG SI SI SI I




Page 93 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

HGOHHH SI

HHHNYB SI I SI

HMTUQD SI I

HMW24R S I

HP2FIF SI

I3H5RP S S S I

IKEYL1 S S S I I

INI2AA I I

INNQNN I SI I

IQQVQB S S I I

IVWKXD SI

J7VXH7 S I

JAXXGC SI

JFLFE3 S I I

JHHNXN S S SI I

JIOIBA S I I I I

JNQLXX S S SI SI

K1NKKG S S S I I

KAPAAS SI

KC4CO7 I S

KFULE7 I SI

KHDDXD S I I

KII7PP SI

KMBMUQ S S I I

KNHLNG S S S I I

KTBSBL SI I


L75533 S I I


LE5Z5Z S I

LRPCVG I SI

M9N99Q S S S I I

MELOFZ S S S I I

MJRX8A S I

MLKVZO S S S I I

MMQ2L2 S I SI I

MYD9WU I I I




Page 94 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

N4VGXV SI I I SI


NGGZGG S S S I

NNANPN I I SI

NPO333 S I I

OCQGSD S I I


OHKWWZ SI I

OIKEE1 I SI I

OIMJHC SI

OKWXFO I I


Janovsky

P1JWGT S I I

PIRYEY S S S I I

PKPTJM S S I SI

PWZDFG S S I I

QEJKPA SI

QHQQUK SI

QMGORR I SI

QPTTIT SI SI SI I


QQTH7B I SI


R5RPYM I I S

R6BICL I SI I I I

RH08SD S I I

RKKTQP S S I


RRJPPR S S S I

RZDQQQ S SI SI

S8TL74 I SI

SAKRI4 I

SDJTNO I I S

SG5IQS S I I

SGBOPO S I

SHLDPB S I SI SI

SU4NXI SI




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

T2S333 SI I


TCVV6F S S I

TIIISI S S S I I

TMWUW W

S I

TTQXMT S S I

TTTILP I S S SI I I

TUVPUU I S

TXVZAJ I I SI

UEAZZ3 S S I I

UIFULT I SI

V6ESR5 I S

V7AWBG SI SI

VF8TL1 S S SI I

VHYXAH I SI I

W0OABU S I

W4X1SX SI

WCEEWA S I I

WJRG8W I I SI I

X1A11B SI

X66O46 S S I I

X6OWJR I SI I

X8QXDX SI I


derivatization and CGMS analysis

XNJQP7 SI S SI I I

XPYAOU SI

XYXPCP S S S I I

Y31S2M I I

Y45Y4Y I I SI

Y7M3HZ SI I

YAIDDI I

YHKKKB SI I

YL2O3B I SI

YXNYHY S I





Page 96 of 120

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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

ZAOGZZ S S S I I

ZE8ZAZ SI

ZFFBFT I SI I

ZIGGI6 S I I SI I

ZPZ8SZ I SI I SI

ZUZ1ZZ S I

ZWM2QG S S SI




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0E49T9 Cocaine

0OGHZR Cocaine

13S3E5 Cocaine

1999Y6 cocaine

1CNMZQ cocaine

1F633N cocaine

1IDFP1 Cocaine

1W4YMX ketamina

252CCB Cocaine

2F51LA cocaine

2MPUPL Cocaine hydrochloride

2Q22HI Cocaine

2TCPHH Cocaine

2XGWKJ cocaine

2XXLPG cocaine

313337 Cocaine

3332NG cocaine

33ZZO3 cocaine

36BDU6 cocaine

3FT9VW COCAINE AND LACTOSE

3RF39E COCAINE

3SMK33 cocaine

3TY2WR Cocaine

444444 Cocaine

44E44K cocaine

4AXZ9A Cocaine HCl

4CNIOX cocaine

4J4R44 cocaïne

4XX6CI Cocaine

4YFBKI Cocaine

4Z4BDP cocaine

54CQ2S Cocaine

5E0FMO Cocaine

5FFFFF Cocaine

5HWYZN Cocaine

5Q555E cocaine

6666WM COCAINE, ECGONIDINE METHYL ESTER, PSEUDOECGONINE METHYL ESTER, TRANS-CINNAMOYL COCAINE, CIS-CINNAMOYL COCAINE, LACTOSE.




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66H8C3 COCAINE

6JFAWA Cocaine

6RFSER cocaine

6RVR5A Cocaine

6WDJTJ Cocaine

6YZTRZ Cocaine

7ED7SR Cocaine

7MM6GH Cocaine

7WA60O Cocaine

8FXHXS COCAINE

8WWDBW Cocaine

9IA9GY Cocaine

9OOEII cocain

9SMHJ8 cocaine

9YCKGZ Cocaine

A441YE cocaine, cocaine artifact, ecgonine and trans cinnamoylcocainel

AC11BX Cocaine

ADW75B Cocaine

AFUXM7 Cocaine

AMRMTF Cocaine, Lactose

AO8UQ6 Cocaine

AODFDP Cocaine and anhydroecgonine methyl ester

AXU99T Cocaine

AYTE1E Cocaine

AZUH8X Cocaine

B3FTN3 Cocaine

BBBLO2 Cocaine

BEPFVN cocaine

BIA0EZ Cocaine

BMPXHL cocaine

BRFRWM cocaine

BRUEIH Cocaine

BTKUST cocaine

BWSSKK clorhidrato de cocaína

BYBCVB COCAÍNA HCl

BZDD95 Cocaine

C9BRBB Cocaine

CJWQGK cocaine

CYLW4Y cocaïne chlorhydrate

DDVDDE cocaine, cynnamoylcocaine, lactose

DFTIVR Cocaïne

DHDX48 cocaine




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DJS2XK Cocaine

DLFBGB Cocaine

DPVGZK Cocaine

DUCT4E cocaine

E44WTB Cocaine

E4CIFO Cocaine

EAQ4S6 Cocaine

EEGL2R Cocaine

EGEENO Cocaine

EJ4611 Cocaine

F3LSGY Cocaine

FEKAVF Cocaine

FFUFOA Cocaine

FIAC2C Cocaine

FJ7FUF Cocaine

FLL757 Cocaine

FVP0OM Cocaine

GDPMAM Cocaine

GFWFBO Cocaine

GGFGG9 Cocaine

GNM3ON Cocaine

GNTW2Z Cocaine

GQQTND Cocaine Hydrochloride

GY9CXA cocaine

GZFJAG Cocaine

HGOHHH cocaine

HHHNYB cocaine HCl

HMTUQD Cocaine

HMW24R Cocaine

HP2FIF cocaine

I3H5RP cocaine

IKEYL1 COCAINE

INI2AA cocaine-HCl

INNQNN Cocaine and Lactose

IQQVQB Cocaine

IVWKXD Cocaine

J7VXH7 Cocaine

JAXXGC cocaine

JFLFE3 Cocaine

JHHNXN Cocaine

JIOIBA Cocaine HCL

JNQLXX Cocaine & Lactose




Page 100 of 120

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K1NKKG Cocaine Hydrochloride

KAPAAS Cocaine

KC4CO7 Cocaine

KFULE7 Cocaine HCl

KHDDXD Cocaine

KII7PP cocaine

KMBMUQ Cocaine

KNHLNG Cocaine HCl

KTBSBL cocaine

KVYOOO Cocaina

L75533 la Cocaïne

LAWTLL Cocaina

LE5Z5Z Cocaine

LRPCVG Cocaine

MELOFZ Cocaine HCL

MJRX8A COCAINE

MLKVZO Cocaine

MMQ2L2 cocaine

MYD9WU Cocaine

N4VGXV cacaína

N64P66 Cocaine HCl

NGGZGG cocaine

NNANPN Cocaine

NPO333 Cocaine

OCQGSD Cocaine Hydrochloride

OHJX22 Cocaine

OHKWWZ Cocaine

OIKEE1 Cocaine

OIMJHC Cocaine

OKWXFO cocaine, lactose

P0NNSM Cocaine

P1JWGT Cocaine

PIRYEY Cocaine

PKPTJM Cocaine

PWZDFG Cocaine

QEJKPA cocaine

QHQQUK Cocaine

QMGORR Cocaine

QPTTIT Cocaine

QQ7VFQ Cocaine

QQTH7B cocaine

QZZZGT Cocaine




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R5RPYM Cocaine

R6BICL Cocaine + Lactose

RH08SD Cocaine

RKKTQP Cocaine.

RKPGFK Cocaine

RRJPPR cocaine

RZDQQQ COCAINE 14.9%

S8TL74 COCAINE

SAKRI4 cocaine

SDJTNO cocaine

SG5IQS Cocaine

SGBOPO Cocaine

SHLDPB cocaine

SU4NXI COCAIN

T2S333 cocaine hcl

TAAFSW Cocaine Hydrochloride

TCVV6F Cocaine

TIIISI Cocaine

TMWUWW Cocaine

TTQXMT Cocaine

TTTILP COCAINE

TUVPUU cocaine

TXVZAJ Cocaine

UEAZZ3 Cocaine

UIFULT COCAINE

V6ESR5 Cocaine

V7AWBG Cocaine

VF8TL1 Cocaine

VHYXAH COCAINE

W0OABU Cocaína

W4X1SX Cocaine

WCEEWA Cocaine

WJRG8W Cocaine

X1A11B cocaine

X66O46 cocaine

X6OWJR Cocaine

X8QXDX Cocaïne

XM00GQ Cocaine

XNJQP7 COCAINE

XPYAOU Cocaine

XYXPCP Cocaine

Y45Y4Y Cocaine




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Y7M3HZ yes

YAIDDI Cocaine

YL2O3B cocaine

YXNYHY Cocaine

YYYJYT Cocaine and Lactose

ZAOGZZ cocaine

ZE8ZAZ cocaine

ZFFBFT cocaine

ZIGGI6 cocaine

ZPZ8SZ COCAINE

ZUZ1ZZ cocaine

ZWM2QG Cocaine




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Code Cocaine Lactose

0E49T9 + + The sample contained 13.1% cocaine. The sample also contained lactose and minor components such as ecgonie, ecgonine methyl ester, beznylecgonine anhydroecgonine methyl ester and cinnamoyl cocaine.

0OGHZR + ANP

13S3E5 + -

1999Y6 + ANP

1CNMZQ + -

1F633N + - a substance identified is cocaine

1IDFP1 + ANP Cocaine

1W4YMX + ANP

252CCB + + Analysis revealed the presence of cocaine and lactose

2F51LA + ANP

2MPUPL + - White poder containg Cocaíne 11,57 % as base

2Q22HI + + The sample contained 14.0% (w/w) Cocaine (base).

2TCPHH + ANP Results of screening tests were positive for cocaine. Retention time and fragmentation pattern obtained with sample are equivalent to those obtained with cocaine. Cocaine was detected at 15.88% by weight.

2XGWKJ + +

2XXLPG + - The analysis confirmed that SM 2 contains cocaine 11.4 %w/w (as controlled drug).

313337 + - Cocaine 16% +/-1

3332NG + + lactose

33ZZO3 + + Cocaine is on the list of drugs.

36BDU6 + - Sample 2019/1/SM-4 was found containing cocaine

3FT9VW + +




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3RF39E + -

COCAINE

3SMK33 + + GD of RM nr. 1088 of 05.10.2014

3TY2WR + ANP Cocaine is a Class A drug subject to the provisions of the Misuse of Drugs Act 1971.

444444 + + Cocaine hydrochloride (14 % base) and lactose.

44E44K + + Included in the list of narcotic drugs whose turnover in the Republic of Uzbekistan limited (List II)

4AXZ9A + + A composite was formed from 1 unit for testing of 1 unit received. Cocaine HCl and lactose confirmed in the composite.

4CNIOX + + The sample contains 14% cocaine and lactose. cocaine is controlled by the Royal Decree of the 6th of september 2017

4J4R44 + ANP also identified: ecgonine methyl ester, anhydroecgonine methyl ester, methylbenzoate

4XX6CI + + The test sample 2019/1/SM-4 was found to contain the controlled drug cocaine. Lactose was also found in the sample.

4YFBKI + + SM-4 sample was prepared from a seizure containing 14.95%(w/w) Cocaine base. The test sample also contained lactose with methylecgonine,benzoylecgonine and cinnamoyl cocaine as minor components.

4Z4BDP + + The sample contains cocaine, lactose.

54CQ2S + ANP SM4 was contained 9.5% Cocaine.

5E0FMO + + Presence of cocaine hydrochloride and lactose was detected in the sample. The sample also contaned multitude of trace level alkaloid impurities:(cis/trans)cinnamoylcocaine, benzoylecgonine, methylestarecgonine, ecgonine.

5FFFFF + - Cacaine was examined.

5HWYZN + + The sample contains cocaine and lactose as an adulterant. Apart from cocaine and lactose the sample contains small amounts of cinnamoyl cocaine and methyl ecgonidine. Cocaine as a psychoactive substance is controlled in Poland.

5Q555E + + cocaine,lactose

6666WM + + WE FOUND A MIXTURE OF COCAINE, ECGONIDINE METHYL ESTER, PSEUDOECGONINE METHYL ESTER, TRANS-CINNAMOYL COCAINE, CIS-CINNAMOYL COCAINE AND LACTOSE. 66H8C3 + + WAS FOUND COCAINE. LACTOSE WAS FOUND TOO

6JFAWA + +




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6RFSER + + mixture of cocaine and lactose 78 % w/w; and traces of natural accompanying substances - ecgognines, cinnamoylcocaine

6RVR5A + ANP The sample 2019/1/SM4 contain Cocaine.

6WDJTJ + - Positive to Cocaine.

6YZTRZ + +

7ED7SR + ANP Powder contains cocaine. Cocaine is a controlled drug under the Misuse of Drugs Act 1977 to 2016

7MM6GH + ANP Sample contains 12.7 % cocaine.

7WA60O + + 14 % of Cocaine is found with an amount of Lactose.

8FXHXS + + LACTOSE

8WWDBW + + SM-4 was found contain Cocaine traces of Lactose

9IA9GY + -

9OOEII + ANP

9SMHJ8 + ANP the white powder contains cocaine (18.1%w/w) which is controlled by national law

9YCKGZ + - Cocaine was identified by GC/MS

A441YE + + the main compound we founds in SM-4 is cocaine after GC / MS injection. Excess compounds are in a trace state.

AC11BX + + Lactose

ADW75B + ANP This sample was found to contain Cocaine, which is a Class A controlled substance under the Misuse of Drugs Act 1971

AFUXM7 + + It has been detected the presence of cocaine in the sample.

AMRMTF + +

AO8UQ6 + + Sample 2019/1 / SM-4 contains Cocaine.

AODFDP + ANP It was detected the presence of cocaine and anhydroecgonine methyl ester in the sample analysed

AXU99T + ANP In the test sample 2019/1/SM-4 was detected cocaine




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AYTE1E + ANP Cocaine confirmed in SM-4

AZUH8X + ANP We have found Cocaine in SM-4 sample.

B3FTN3 + + The sample 2019/01-SM-4 contains Cocaine detected by GC-MS and FT-IR. The percentage by weight of Cocaine is 18.15%.

BBBLO2 + ANP Presence of cocaine was confirmed qualitatively

BEPFVN + + The sample contains cocaine. The concentration has not been determined.

BIA0EZ + ANP The sample contains cocaine.

BMPXHL + + lactose

BRFRWM + ANP White powder containing 14.9% of cocaine

BRUEIH + + Cocaine HCl

BTKUST + + List of narcotics drugs whose circulation in the territory of the Republic of Uzbekistan is limited (Appendix to the resolution of the Cabinet of Ministers of the Republic of Uzbekistan ¼878 date 27.10.2018 y.)

BWSSKK + + clorhidrato de cocaína 15,3%base, acido benzoico, ecgonidina, ecgonina, norcocaína, cocaetileno, cis-cinamoilcocaína, trans-cinamoilcocaina y lactosa.

BYBCVB + + A Prelimar test and two confirmation tests, TLC and FTIR were performed. It was possible to verify the presence of Alpha LACTOSE in the sample.

BZDD95 + + SM-4 contains cocaine (10.1% as free base), lactose and cocaine derivatives as minor components.

C5MUOL + +

C9BRBB + +

The sample contains cocaine which is listed as a controlled drug according to french order, appendix I of February 22nd 1990.

CJWQGK + -

CYLW4Y + + cocaïne (14,8% as base) + lactose

DDVDDE + + We started with colourimetric test, then We could identify Lactose by FTIR and Cocaine by GC-MS. We analyze the samples in different solvents and different concentrations.

DFTIVR + + The sample contains cocaïne. Cocaïne is sheduled as illicit drug.

DHDX48 + -




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DJS2XK + ANP

DLFBGB + ANP Sample was found to contain Cocaine at the concentration of 13%.

DPVGZK + + The sample contain cocaine and Lactose

DUCT4E + + %14.5 cocaine

E44WTB + + Cocaine was identified in SM4 and percentage is 19.584%. In addition Lactose was identified

E4CIFO + +

EAQ4S6 + ANP Color test,TLC and GCMS

EEGL2R + + White powder analysed by GC/MS was found to contain Cocaine. Mass spectra was similar to CRM

EGEENO + + The sample contains 14.04% of Cocaine and also contains Benzoylecgonine, Ecgonine methyl ester and Lactose

EJ4611 + + The sample analyzed SM 4 contains cocaine and lactose

F3LSGY + + Lactose

FEKAVF + ANP

FFUFOA + + Lactose

FIAC2C + ANP We have found Cocaine in SM-4 sample.

FJ7FUF + + Sample number 4: there is ilicit drug (cocaine)

FLL757 + ANP

In the seized sample was detected the presence of cocaine

FVP0OM + -

GDPMAM + + Cocaine and lactose were detected in the sample.

GFWFBO + ANP The chemical test and the coincidence in the retention time and mass fragmentogram with the reference material in the same conditions that the analysed sample indicates the lidocaine and cocaine presence.

GGFGG9 + ANP Sample represent white powder that contains controlled substance COCAINE.

GI4HGG + +




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GNM3ON + ANP "controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 13 % (w/w)"

GNTW2Z + ANP The sample 2019/1/SM-4 was found to contain Cocaine

GQQTND + + White powder 221 milligrams Cocaine Hydrochloride (16%) Legal Status - Class A Lactose, Legal Status - Not controlled


GY9CXA + +

GZFJAG + ANP We have found Cocaine in sm-4 samples. We have also found Andhydroecgonine methyl ester.

HGOHHH + ANP

HHHNYB + + lactose

HMTUQD + ANP Cocaine was detected in the SM-4 sample.

HMW24R + ANP Sample SM-4 found to contain cocaine

HP2FIF + ANP

I3H5RP + ANP

IKEYL1 + ANP ECGONIDINE,ECGONINE, BENZOYL ECGONINE AS MINORITY

INI2AA + + White powder with characteristic smell containing by weight 14.3% cocaine expressed as free base and lactose. Cocaine is present in form of hydrochloride.

INNQNN + + The samples 2019/1/SM-4 contains cocaine and lactose detected by GC/MS and FTIR. The percentage by weight of Cocaine is 15.7%.

IQQVQB + ANP Powder from sample 2019-1SM-4 contain Cocaine

IVWKXD + - Cocaine

J7VXH7 + ANP Test sample 2019/1/SM-4 to contain Cocaine, Cinnamoylcocaine and benzoylecgonine

JAXXGC + ANP sm4 contained 14.1%w/w cocaine

JFLFE3 + - Material analysis using the portable Raman equipment screening provided as a result cocaine substance.The substance was confirmed by GCMS using a reference standard




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JHHNXN + + Marquis reagent: negative; Cobalt thiocyanate: positive; GC-MS: cocaine (result compared with library spectrum, retention time compared with reference material); FTIR: lactose (result compared with library spectrum); FTIR after extraction with ethanol: dried extract - cocaine, residue - lactose (spectra were compared with library); Lactose and glucose were differentiated with Woehlk test

JIOIBA + + Also lactose was found.

JNQLXX + + (i) Using the techniques TLC, GC-MS & FTIR , Sample SM 4 was found to contain Cocaine & Lactose. (ii) Using Technique GC-FID, Quantification of SM 4 was done and found to contain

Cocaine 14.6%.

K1NKKG + + Sample 2019/1/SM-4 contained COCAINE Hydrochloride, at a concentration of 14% (calculated as base). COCAINE Hydrochloride is a Class A controlled drug under the provisions of the Misuse of Drugs Act 1971 (as amended).

KAPAAS + ANP Analysis of a representative sample of the powder revealed the presence of cocaine with a purity of approximately 15% (calculated as base).

KC4CO7 + -

KFULE7 + + lactose

KHDDXD + -

KII7PP + +

KMBMUQ + + This item comprised of 0.23 grams of white powder, found to contain cocaine at a concentration of 14%, together with lactose. Cocaine is a Class A controlled substance under the Misuse of Drugs Act 1971, as amended. Lactose is not a controlled substance.

KNHLNG + + SM-4 contains Cocaine 13.24% (as base) and Lactose

KTBSBL + + cocaine was detected by GC/MS and quantified by GC/FID

KVYOOO + + con lactosa

L75533 + + SM4 contient de la Cocaïne avec du lactose

LAWTLL + + Lactosa

LE5Z5Z + ANP Based on the above analysis, the sample was found to contain Cocaine

LRPCVG + + SM4: was fond to contain Cocaine and Lactose

M9N99Q + + cocaine




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MELOFZ + + Sample was a mixture of Cocaine HCL and Lactose

MJRX8A + +

The test sample contained cocaine and lactose

MLKVZO + + Lactose

MMQ2L2 + + lactose

MYD9WU + + The sample contains cocaine. The content of cocaine is determined to 16 % (as cocainhydrochloride). Cocaine is a controlled substance in X.

N4VGXV + - -

N64P66 + + Cocaine HCl, Lactose

NGGZGG + -

NNANPN + ANP Cocaine was found in the sample labeled 2019/1 / SM-4

NPO333 + + Diluted with lactose

OCQGSD + ANP The white powder was analysed and found to contain Cocaine Hydrochloride.

OHJX22 + + Cocaine & Lactose were found present in the sample SM-4

OHKWWZ + + The sample contains Cocaine and Lactose

OIKEE1 + + Cocaine and lactose were detected in SM-4 sample.

OIMJHC + ANP

OKWXFO + + Cocaine is scheduled as illicit drug in France. The sample contains also lactose which is a cutting agent.

P0NNSM + ANP Sample 2019/1/SM-4 found to contain Cocaine

P1JWGT + - Cocaine is a controlled drug under the Drug Abuse Prevention And Control Act Cap 131 of the Laws of Barbados.

PIRYEY + +

Sample 2019/1/SM-4 contains cocaine, lactose and cocaine derivates as minor components.

PKPTJM + ANP One glass bottle containing 0.22 grammes of a powder containing 0.03 grammes of cocaine.

PWZDFG + + The sample contains cocaine, cis-cinnamoyl cocaine, trans cinnamoyl cocaine and lactose.

QEJKPA + ANP cocaine was detected by GC/MS and quantified by GC/MS




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QHQQUK + ANP Controlled drug, Cocaine, present in sample. Concentration approx 14%

QMGORR + ANP

QPTTIT + ANP We have found Cocaine in SM-4 sample.

QQ7VFQ + ANP The sample was found to contain a controlled substance(s) within the meaning of the Controlled Drugs and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecogonine) calculated as the hydrochloride 14% (w/w)

QQTH7B + + lactose

QZZZGT + ANP From screening test using (CT), and from confirmation test using (GC-MS) the sample was found to contain the controlled drug Cocaine.

R5RPYM + + lactose

R6BICL + + In the 2019/1/SM-4 was proved the presence of Cocaine and Lactose with a quantification as base of 16.3%

RH08SD + + This sample is cocaine.

RKKTQP + ANP White powdery substance of 2019/1/SM-4 was found to contain Cocaine. Quantitative analysis was not carried-out to determine the weight of the drugs. Cocaine is listed in The First Schedule of The Dangerous Drugs Act 1952.

RKPGFK + -

RRJPPR + - NARCOTIC. List I Unique Convention 1.961

RZDQQQ + -

S8TL74 + ANP

SAKRI4 + ANP

SDJTNO + + white powder containing 15.3%w/w cocaine. The sample contains lactose.

SG5IQS + + SM 4 contains:Cocaine and Lactose, with 14.34 % Cocaine base

SGBOPO + - The powder was analysed and found to contain Cocaine. Cocaine is a class A controlled drug within the provisions of the Misuse of Drugs Act 1971.

SHLDPB + + lactose

SU4NXI + + LACTOSE

T2S333 + +




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TAAFSW + + The sample contains cocaine hydrochloride (14.3% as cocaine free base) and lactose.

TCVV6F + + the sample SM-4 was found Cocaine

TIIISI + +

TMWUWW + ANP 2019/1/SM-4 was confirmed for cocaine. Cocaine is a schedule II controlled substance in the United States.

TTQXMT + ANP Sample 2019/1/SM-4 consists of white powder. Cocaine, a prohibited substance included in the National Law for Narcotics, is found to be present in this sample.

TTTILP + + Identified by GCMS & LCMSMS techniques and quantified by GC-FID technique.

TUVPUU + +

TXVZAJ + ANP white powder containing cocaine

UEAZZ3 + + SM-4 was found to contain 13.60 % cocaine and also lactose.

UIFULT + ANP SCREENING BY RAMAN AND CONFIRMATION BY GC MSD AND QUANTIFIED BY HPTLC DENSITOMETRIC TLC

V6ESR5 + ANP

V7AWBG + +

VF8TL1 + ANP Cocaine controlled under Malaysian Dangerous Drugs Act

VHYXAH + + COCAINE IN LACTOSE POWDER

W0OABU + ANP

W4X1SX + ANP -

WCEEWA + ANP The sample was found to contain a controlled substance within the meaning of the Controlled Drug and Substances Act: Schedule I 2. (2) Cocaine (benzoylmethylecgonine) calculated as the hydrochloride 15% w/w

WJRG8W + + The sample contains drugs, cocaine. It contains also lactose.

X1A11B + ANP cocaine

X66O46 + ANP Sample 2019/1/SM-4 a white powder gave a positive result for cocaine, substance under national legislation on drugs.

X6OWJR + + Cocaine+Lactose




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X8QXDX + + lactose

XM00GQ + + Sample with cocaine, lactose and small amounts of cis and trans cinnamoylcocaine. Identification of cocaine by GC/MS. Identification of lactose by Raman, FTIR and by GC/MS after MSTFA derivatization.

XNJQP7 + - 12.96 % COCAINE

XPYAOU + ANP Sample tested positive for cocaine. Cocaine was confirmed in the sample at 11.04% by weight.

XYXPCP + - SM4 contains Cocaine.

Y31S2M + ANP

Y45Y4Y + + It was found lactose.

Y7M3HZ + ANP cocaine

YAIDDI + + It contains cocaine in a purity of 15.5%. It also contains lactose and glucose.

YHKKKB + +

YL2O3B + ANP The sample was found to contain 14.0% of cocaine (as base).

YXNYHY + + Cocaine 14,4% and lactose

YYYJYT + + The Test sample 2019/1/SM-4 was analyzed by Thin Layer Chromatography technique and was found to contain Cocaine and Lactose.

ZAOGZZ + +

2019/1/SM-4 contains cocaine, lactose, caffeine, benzoylecgonine, ecgonine methyl ester and cinnamoylcocaine isomers

ZE8ZAZ + ANP Positive to cocaine

ZFFBFT + +

ZIGGI6 + + The sample contains 12,99±0,50 weight% cocaine-base. The sample also contains lactose.

ZPZ8SZ + ANP

ZUZ1ZZ + + lactose

ZWM2QG + ANP Sample 2019/1/SM-4 was found to contain cocaine




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

0E49T9 I I SI I

0OGHZR SI SI I


1999Y6 S I I

1CNMZQ SI

1F633N SI

1IDFP1 SI I

1W4YMX SI S S I

252CCB I I SI

2F51LA I SI

2MPUPL S I I

2Q22HI S S S I I

2TCPHH S S S I

2XGWKJ I SI

2XXLPG S S S I

313337 S S I

3332NG S I SI SI

33ZZO3 S I I

36BDU6 S I

3FT9VW S S I I

3RF39E S S I


3TY2WR S S I

444444 SI

44E44K S S S I I I

4AXZ9A I SI

4CNIOX I SI

4J4R44 S SI

4XX6CI S S S SI I

4YFBKI S I I

4Z4BDP S S S I I I






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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

5E0FMO I I I S

5FFFFF S S S SI I




66H8C3 S S I I

6JFAWA SI I

6RFSER I I I S


6WDJTJ I

6YZTRZ SI I

7ED7SR I

7MM6GH SI

7WA60O S I SI SI

8FXHXS SI

8WWDB W

I

9IA9GY S S S I I

9OOEII S S S I I

9SMHJ8 I SI

9YCKGZ S S I I

A441YE I S

AC11BX I SI I

ADW75B S S I

AFUXM7 SI I

AMRMTF I SI

AO8UQ6 S S I I

AODFDP S S S I

AXU99T I

AYTE1E S SI SI I

AZUH8X SI SI SI I

B3FTN3 S S S I I

BBBLO2 S S I SI


BIA0EZ SI

BMPXHL S S S I I

BRFRWM I SI

BRUEIH SI I




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

BTKUST SI I

BWSSKK S I I

BYBCVB S I I

BZDD95 I

C5MUOL SI I

C9BRBB I I

CJWQGK SI

CYLW4Y SI I

DDVDDE S SI I

DFTIVR SI I I

DHDX48 S I

DJS2XK S S I

DLFBGB S S I

DPVGZK S I I

DUCT4E S I I


E4CIFO S S I I

EAQ4S6 S S SI I

EEGL2R S S S I I

EGEENO I SI I

EJ4611 S I I

F3LSGY I I SI I

FEKAVF S S I I

FFUFOA S I I I

FIAC2C SI SI SI I

FJ7FUF S S I I

FLL757 SI I

FVP0OM S I I

GDPMAM S S I I

GFWFBO S S I



GNM3ON SI I I

GNTW2Z SI SI SI I

GQQTND S S S I I

GY9CXA S I I

GZFJAG SI SI SI I




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Code 140 141 142 150 160 161 170 171 180 190 200 211 230 231 250 210

HGOHHH SI

HHHNYB SI I SI

HMTUQD SI I

HMW24R S I

HP2FIF SI

I3H5RP S S S I

IKEYL1 S S S I I

INI2AA I I

INNQNN I SI I

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MJRX8A S I

MLKVZO S S S I I

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MYD9WU I I I




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OCQGSD S I I


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Janovsky

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ZAOGZZ S S S I I




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ZUZ1ZZ S I

ZWM2QG S S SI

Vienna International Centre, P.O. Box 500, 1400 Vienna, Austria

Tel. : (+43-1) 26060-0, Fax : (+43-1) 26060-5866, www.unodc.org

international collaborative exercises (ice) · 2019-12-18 · sm-4 (lidocaine) (procaine) (cocaine)...

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