including the 1997 international induction heat treating

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HeatTreating Includingthe1997International InductionHeatTreatingSymposium Proceedingsofthe17thHeatTreatingSocietyConferenceandExposition andthe1stInternationalInductionHeatTreatingSymposium 15-18September1997,Indianapolis,Indiana Editedby DavidL .Milam DaleA .Poteet,Jr . GeorgeD .Pfaffmann ValeryRudnev AlfredMuehlbauer WalterB .Albert ASt+ Heat Treating ~/society AnAffiliateSocietyofASMInternational

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Page 1: Including the 1997 International Induction Heat Treating

Heat TreatingIncluding the 1997 International

Induction Heat Treating Symposium

Proceedings of the 17th Heat Treating Society Conference and Expositionand the 1st International Induction Heat Treating Symposium

15-18 September 1997, Indianapolis, Indiana

Edited byDavid L. Milam

Dale A. Poteet, Jr.George D. Pfaffmann

Valery RudnevAlfred MuehlbauerWalter B . Albert

ASt+ Heat Treating~/ societyAn Affiliate Society of ASM International

Page 2: Including the 1997 International Induction Heat Treating

Copyright 1998 by

ASM International ® All rights reserved

No part of this book may be reproduced, stored in a retrieval system, or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording, or otherwise, without the written permission of the copyright owner.

First printing, March 1998

Great care is taken in the compilation and production of this Volume, but it should be made clear that NO WARRANTIES, EXPRESS OR IMPLIED, INCLUDING, WITHOUT LIMITATION, WARRANTIES OF MER- CHANTABILITY OR FITNESS FOR A PARTICULAR PURPOSE, ARE GIVEN IN CONNECTION WITH THIS PUBLICATION. Although this information is believed to be accurate by ASM, ASM cannot guarantee that favorable results will be obtained from the use of this publication alone. This publication is intended for use by persons having technical skill, at their sole discretion and risk. Since the conditions of product or material use are outside of ASM's control, ASM assumes no liability or obligation in connection with any use of this information. No claim of any kind, whether as to products or information in this publication, and whether or not based on negligence, shall be greater in amount than the purchase price of this product or publication in respect of which damages are claimed. THE REMEDY HEREBY PROVIDED SHALL BE THE EXCLUSIVE AND SOLE REMEDY OF BUYER, AND IN NO EVENT SHALL EITHER PARTY BE LIABLE FOR SPECIAL, INDIRECT OR CONSEQUENTIAL DAMAGES WHETHER OR NOT CAUSED BY OR RESULTING FROM THE NEGLIGENCE OF SUCH PARTY. As with any material, evaluation of the material under end-use conditions prior to specification is essential. Therefore, specific testing under actual conditions is recom- mended.

Nothing contained in this book shall be construed as a grant of any right of manufacture, sale, use, or reproduction, in connection with any method, process, apparatus, product, composition, or system, whether or not covered by letters patent, copyright, or trademark, and nothing contained in this book shall be construed as a defense against any alleged infringement of letters patent, copyright, or trademark, or as a defense against liability for such infringement.

Comments, criticisms, and suggestions are invited, and should be forwarded to ASM International.

Library of Congress Catalog-Card Number: 98-70212 ISBN: 0-87170-610-5

SAN: 204-7586

Editorial Project Manager

ASM International ® Materials Park, OH 44073-0002

Printed in the United States of America

Page 3: Including the 1997 International Induction Heat Treating

Key Individuals Involved in Organizingthe Heat Treating Conference

1997 EVENT CO-ORGANIZERS

Dale A. Poteet, Jr.Innovative Metallurgical TechnologyVerona, WisconsinCo-Chairman, HTS Programming and EventsCommittee

David L. MilamThe Timken CompanyCanton, Ohio

HEAT TREATING SOCIETY'SPROGRAMMING AND EVENTS

COMMITTEEAll committee members may not be listed here ;

please refer to the technical program list, as well .

George E.Totten, FASM-ElectUnion Carbide CorporationTarrytown, New YorkCo-Chairman

Liu DaiBeijing Research Institute of Mechanical &

Electrical EngineeringBeijing, ChinaCo-Chairman, International ProgrammingSubcommittee

Jon L. Dossett, FASMMidland Metal Treating, Inc .Franklin, WisconsinCo-Vice Chairman

Charles H. FaulknerHoughton International Inc .Valley Forge, PennsylvaniaMember at Large

Kiyoshi FunataniNihon Parkerizing Co ., Ltd .Nagoya, Aichi, JapanMember at Large

III

David GuisbertQuality Associates of BuchananBuchanan, MichiganMember at Large

Luiz Roberto HirshheimerBRASIMET Commercio a Industria S .A .Sao Paulo, BrazilMember at Large

FranzT. HoffmannStiftung Institute fur WerkstofftechnikBremen, GermanyCo-Chairman International ProgrammingSubcommittee

Joseph lovineHTG AerobrazeCincinnati, OhioChairman, Sales & Marketing Subcommittee

Larry G. JonesChaparral SteelMidlothian, TexasMember at Large

Robert E. Luetje, FASMKolene CorporationDetroit, MichiganLiaison, Detroit Chapter Programming

Lemmy MeekishoOregon Graduate InstitutePortland, OregonChairman, International On-Line ProcessModelling Subcommittee

Eric J. Mittemeijer, FASMDelft University of TechnologyDelft, The NetherlandsCo-Chairman, International ProgrammingSubcommittee

David PaddleCastrol AspacKuala Lumpur, MalaysiaMember at Large

Page 4: Including the 1997 International Induction Heat Treating

Ronald A. WallisWyman-Gordon ForgingsHouston, TexasCo-Chairman, '98 Heat Treating Conference

Alexey SverdlinBradley UniversityPeoria, IllinoisMember at Large

TECHNICAL PROGRAM

Distortion

Sponsored by: Distortion Control Subcommitteeof ASM's Heat Treating Society

Harry W. WaltonThe Torrington CompanyRutherfordton, North CarolinaChairman, Distortion Control Subcommittee, andCo-Chairman, '98 Heat Treating Conference

Equipment

Sponsored by: Process Equipment TechnologiesSubcommittee of ASM's Heat Treating Society

Daniel H . HerringC. I . Hayes, Inc .Woodridge, IllinoisCo-Chairman, Process Equipment TechnologiesSubcommittee and Liaison, Immediate NeedsCommittee

Advanced Carburizing -Materials & EquipmentConsiderations of Prepared Atmospheres

George D. PfaffmannTOCCO, Inc .Madison Heights, MichiganCo-Chairman, Process Equipment TechnologiesSubcommittee

Dick BennettJanus Technology Group, Inc .Rockford, IllinoisGas vs. Electric Heating & Recuperation

Technology

iv

Ernie BishopMetal Treating, Inc .Cincinnati, OhioSalt Bath Technology

Kevin BrennanCan Eng Furnaces Ltd .Niagara Falls, CanadaProcess, Problems and Solutions Heat TreatingFasteners In Today's Mesh Belt Furnaces

George C. CarterVacuum Furnace Systems CorporationSouderton, PennsylvaniaHigh Pressure Gas Quenching

John A. CollinsSurface Combustion, Inc .Maumee, OhioLow Temperature Vacuum Heat TreatingSolving Applications Through InnovativeEquipment Design

Upgrading Atmosphere Furnaces : Materials,Controls, Burners/Heating Elements,Automation, NFPA Updates, etc .

Robert ConnellVAC AERO International, Inc .Oakville, Ontario, CanadaControl Systems for Vacuum Furnaces

Matthew J. FischerSurface Combustion, Inc .Maumee, OhioConsiderations of Prepared Atmospheres

Marc GlasserProcedyne Corp .New Brunswick, New JerseyFluidized Bed Technology

John GuptaAtmosphere Furnace Co .Wixom, MichiganAdvances in Integral Quench Furnaces

Dick HaimbaughInduction Heat Treating Corp .Crystal Lake, IllinoisInduction Equipment Choices Important to Heat

Treaters

Page 5: Including the 1997 International Induction Heat Treating

Rick L. HoughtonC. I. Hayes, Inc .Cranston, Rhode IslandBatch vs. Continuous Furnace Designs andApplications

Craig A . KlinglerSeco/Warwick CorporationMeadville, PennsylvaniaPowder Metal Heat Treatment

Harry KurekInstitute of Gas TechnologyDes Plaines, IllinoisAdvanced Gas Fired Systems : Overview & Field

Experience

Jerry LindellTwin Disc., Inc .Racine, WisconsinGear Heat Treat for Distortion Control

Steve MausLindbergWatertown, WisconsinAdvances in Integral Quench Furnaces

Frank RagoneHolcroftLivonia, MichiganBusiness Issues & Justifying The Purchase

Melvin RenowdenAtmospheresAir Liquide Corp .Countryside, IllinoisNitrogen Based Atmospheres vs. Generated

Joseph P. SchuttertSerec CorporationProvidence, Rhode IslandCleaning and Drying of Ferrous & Non Ferrous

Parts, Before and After Heat Treating

Dick O. ThalackerPacific Industrial Furnace CompanyWixom, MichiganBusiness Issues & Justifying The Purchase

v

Doug WellingEast Ohio Gas Co .Chagrin Falls, OhioGas vs. Electric Heating & Recuperation

Technology

FerrousInternational Symposium on AcceleratedCooling/Direct Quenching of SteelsSponsored by: ASM International Primary Metals

& Processing (Ferrous) Industrial Sector &ASM Heat Treating Society

Riad AsfahaniU. S. Steel Technical CenterMonroeville, PennsylvaniaChairman, International Symposium onAccelerated Cooling/Direct Quenching of Steels

Rick L. BodnarBethlehem Steel CorporationBethlehem, Pennsylvania

Eric M. FochtNaval Surface Warfare CenterWest Bethesda, Maryland

Kiyoshi FunataniNihon Parkerizing Co., Ltd .Nagoya, Aichi, Japan

Anthony HicklNorth Star Steel Co .Minneapolis, Minnesota

Geoff TitherReference Metals Co., Inc .Bridgeville, Pennsylvania

George E.Totten, FASM-ElectUnion Carbide CorporationTarrytown, New York

Alexander D. Wilson, FASMLukens Inc .Coatesville, Pennsylvania

Page 6: Including the 1997 International Induction Heat Treating

Induction Heat Treating

1st International Induction Heat TreatingSymposiumSponsored by: Process Equipment TechnologiesSubcommittee of ASM's Heat Treating Society

George D. PfaffmannTOCCO, Inc .Madison Heights, MichiganCo-Chair

Walt AlbertInductoheat, Inc .Madison Heights, MichiganCo-Chair

Alfred MuehlbauerUniversitat HanoverHanover, GermanyCo-Chair

Egbert BaakeUniversitat HanoverHanover, Germany

James BehrendsenDelphi SanduskySandusky, Ohio

F. BezmenovVNIITVChSt. Petersburg, Russia

Lui DalBeijing Research Institute of Mechanical and

Electrical EngineeringBeijing, China

Wang DewenBeijing Research Institute of Mechanical and

Electrical EngineeringBeijing, China

William Dowling, Jr.Ford Motor CompanyDearborn, Michigan

Kiyoshi FunataniNihon Parkerizing Co. Ltd .Nagoya, Aichi, Japan

vi

Dale GrechGM PowertrainYpsilanti, Michigan

Stephan HockZF Industries Inc .Friedrichshafen AG, Germany

Ronald HoppeDelphi Saginaw Steering SystemsSaginaw, Michigan

Maurice A. H. HowesIIT Research InstituteChicago, Illinois

George Krauss, FASMColorado School of MinesGolden, Colorado

J.D. LaversUniversity of TorontoToronto, Canada

Tony C. LiuFultwin Enterprise Co. Ltd .Taichung, Taiwan

Sergio LupiUniversita degli StudiPadova, Italy

Pelle OlssonBrukens ABGothenburg, Sweden

Dale A. Poteet, Jr.Innovative Metallurgical TechnologyVerona, Wisconsin

Valery RudnevInductoheat Inc .Madison Heights, Michigan

Soren SegerbergThe Swedish Institute of ProductionMolndal, Sweden

Mark ShaponaFord Motor CompanyLivonia, Michigan

Page 7: Including the 1997 International Induction Heat Treating

Satish S . UdpaIowa State UniversityAmes, Iowa

Hiyoshi WatanabeFuji Electronics Industry Co.Osaka, Japan

Michael WiezbowskiChrysler Corporation,Auburn Hills, Michigan

Non-FerrousSponsored by: Non-Ferrous Subcommittee ofASM's Heat Treating Society

Trilochan S. BainsBoeing Commercial Airplane GroupSeattle, WashingtonCo-Vice Chairman and Chairman, NonferrousSubcommittee

Murat TiryakiogluWestern Kentucky UniversityBowling Green, Kentucky

ProcessesSponsored by: Process Subcommittee of ASM's

Heat Treating SocietyModeling Carburizing, Nitriding and Related

Diffusional Surface TreatmentsSponsored by: Atomic Transport Committee of

ASM's Materials Science Critical TechnologiesSector, and the Process Subcommittee ofASM's Heat Treating Society

Dan McCurdyMarathon Monitors, Inc .Cincinnati, OhioCo-Chairman, Process Subcommittee

Sandy J. MideaAGA Gas, Inc .Cleveland, OhioCo-Chairman, Process Subcommittee

vii

Douglas H . ClingnerConsultantPerrysburg, OhioHeat Treat Processes that Reduce Distortion

Jason CrawfordAGA Gas Inc .Cleveland, OhioSteel Transformations

Matthew J. FischerSurface Combustion, Inc .Maumee, OhioDiffusion Related ProcessesModeling Carburizing, Nitriding and Related

Diffusional Surface Treatments

John E . Morral, FASMUniversity of ConnecticutStorrs, ConnecticutModeling Carburizing, Nitriding and Related

Diffusional Surface Treatments

Richard D. Sisson, Jr., FASMWorcester Polytechnic InstituteWorcester, MassachusettsModeling Carburizing, Nitriding and Related

Diffusional Surface Treatments

George E. Totten, FASM-ElectUnion Carbide CorporationTarrytown, NYQuenching and Cooling

Quality and TechnologySponsored by: Quality Subcommittee of ASM's

Heat Treating Society

Jerry O. WolfeThe Timken CompanyCanton, OhioChairman, Quality Subcommittee

Page 8: Including the 1997 International Induction Heat Treating

Resource Management

Student Research in ProgressSponsored by : Resource Management

Subcommittee of ASM's Heat Treating Society

Alexey SverdlinBradley University

William D . Stofey

Peoria, IllinoisAmerican Ultra Specialties, Inc .Hudson, OhioChairman, Resource Management Subcommittee

Page 9: Including the 1997 International Induction Heat Treating

PrefaceThe ASM Heat Treating Society Conference and Exposition is the premier information exchange eventin our industry. It is presented to provide information on heat treating subjects that will provide answersto questions, and solutions to problems experienced by heat treaters and engineers . Beginning in1998, the event will be held on an annual basis in order to serve the societal responsibilities of theASM Heat Treating Affiliate Society in providing information exchange and networking for its members .

For the first time, in 1997 a separate International Induction Symposium was held within the HeatTreating Conference . In addition, the entire Heat Treating topical offering was part of "The CompleteMetals & Materials Experience" mega-event, which also included the ASM Materials SolutionsConference, the ASM & DVS United Thermal Spray Conference and Exposition, and the ASM/TMSMaterials Week Exposition. More than 8,500 people attended the entire offering .

These proceedings are a product of the 1997 Heat Treating Conference . Submission of manuscriptswas not a requirement for speaking at the Conference; consequently, there are some speakers whochose not to prepare a manuscript . Many of the speakers at the Conference graciously agreed toexpend the time and effort necessary to prepare these manuscripts . We wish to express our thanks tothese authors .

We wish to thank the Heat Treating Society Programming and Events Committee for organizing thesessions. This committee and its subcommittees, consisting of approximately one hundred people,worked together over several months to determine the session topics and find the speakers to respondto the needs of the heat treating industry. We also appreciate the contributions made to this Conferenceby the exhibitors because they, too, are valuable sources of information for attendees .

Finally, we thank you, the attendees, for coming to this event . You are the critical element of the event .We hope that this Conference was of help to you in your work. That's what it's all about : networking,learning, and sharing to improve the heat treating process . (Feel free to send email comments tomem-serv@ po.asm-intl .org ) .

For planning purposes, please note that the 1998 Annual Heat Treating Society Conference andExposition will be held 13-15 October 1998, at the Rosemont Convention Center in Rosemont, Illinois(Chicago) .

David L. Milam

Dale A. Poteet, Jr.The Timken Company

Innovative Metallurgical TechnologyCo-Chair

Co-Chair

ix

Page 10: Including the 1997 International Induction Heat Treating

Table of ContentsDistortion

Residual Stress and Distortion

Thermal Residual Stress Relaxation and Distortion in Surface Enhanced Gas TurbineEngine Components

3

PS. Prevey, D.J. Hornbach, PW. Mason, Lambda Research, Cincinnati, Ohio

Development of Machining Procedures to Minimize Distortion During Manufacture

13

D.J. Hornbach, PS. Prevey, Lambda Research, Cincinnati, Ohio

New Quenching Technology for Distortion Control

Control of Distortion by Quenching in Fluidised Beds

19

R. W. Reynoldson, Quality Heat Treatment, Pty . Ltd., Bayswater North, Australia

Optimization of Single Part Quenching in Nozzle Fields

25

B. Gondesen, T Lubben, FT Hoffmann, P Mayr, Stiftung Institut fur Werkstofftechnik, Bremen,Germany

U. Heck, U. Fritsching, K. Baukhage, Stiftung Institut fur Verfahrenstechnik, Bremen, Germany

Hardening of Steel Parts Using Wave Technology

33

A. V Sverdlin, A.R. Ness, Bradley University, Peoria, IllinoisR.F. Ganiev, Interindustry Scientific and Engineering Wave Technology Center, Moscow, Russia

Equipment

Advanced Carburizing - Materials and Equipment

Continuous Vacuum Carburizing Furnace with 20 Bar High-Pressure Gas Quenching

43

F Preisser, P Heilmann, R. Seemann, ALD Vacuum Technologies GmbH, Erlensee, GermanyW.R. Zenker, ALD Vacuum Technologies, East Windsor, Connecticut

New Carburizing Techniques Using Fluidized Bed Furnaces

53

R. W Reynoldson, Quality Heat Treatment Pty. Ltd., Baywater North, Australia

Advanced Gas Fired Systems: Overview and Field Experience

The Experience at Dana Corporation, Spicer Transmission Division

61

J.E. Wright, Jr., Dana Corporation, Jonesboro, Arkansas

xi

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Advances in Integral Quench Furnaces

Progress in the Application of High Pressure Gas Quenching

65W R. Zenker, ALD Vacuum Technologies, East Windsor, ConnecticutF Preisser, ALD Vacuum Technologies GmbH, Erlensee, Germany

Atmosphere Control System to Achieve Consistent Carburizing in Batch Furnaces

69PM. Torok, Triadx Ltd., Indianapolis, IndianaM. Allen, Intool Inc., Houston, Texas

Business Issues and Justifying the Purchase

MSSR (Military Specification and Standards Reform) How Does it Affect Your Operation?

75D.E. Bell, The Boeing Company, Seattle, Washington

Advanced Radiant Tubes : Payback Calculations of Furnace Retrofits

79P Wurm, Institute of Gas Technology, Des Plaines, IllinoisS. Sikirica, Gas Research Institute, Chicago, Illinois

Cost Justification in the Selection of Heat Resistant Alloys

83J. Wilson, Rolled Alloys Inc ., Temperance, Michigan

Cleaning and Drying of Ferrous and Non Ferrous Parts,Before and After Heat Treating

Principles of AirlessTM Solvent Degreasing 91D.J. Gray, J.P. Schuttert, SEREC Corporation, Providence, Rhode Island

Considerations of Prepared Atmospheres

Principles and Use of Dissociated Ammonia

97R.G. O'Neill, D. H. Herring, C. I. Hayes, Inc., Cranston, Rhode Island

Principles and Use of Endothermic Atmosphere 107S.N. Banerjee, Aichelin-Stahl Inc., Lee's Summit, Missouri

Control Systems for Vacuum Furnaces

Supervisory Control Systems for Vacuum Furnaces 111M. F. Marshall, VAC AERO International, Inc ., Oakville, Ontario, Canada

Supervisory and Process Control to Enhance Batch Vacuum Processing

113S. G. Kowalski, Kowalski Heat Treating Co . Inc., Cleveland, Ohio

xii

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Fluidized Bed Technology

Brite HeatTreating in a Fluidized Bed

117M. Glasser, Procedyne Corp., New Brunswick, New Jersey

HeatTreating in Fluidized Bed Furnaces in CuttingTool Manufacturing

121L. Multak, Regal-Beloit Corporation, South Beloit, Illinois

Gas vs. Electric Heating and Recuperation Technology

Gas-Fired Ion Nitriding Furnace Lowers Utility Costs for Commercial Heat Treaters

125J. Greene, Ippen International, Inc ., Rockford, IllinoisG. Legge, Ispen International, Inc., Bensalem, PennsylvaniaD. Welling, East Ohio Gas, Cleveland, Ohio

Gear Heat Treat for Distortion Control

Techniques for Distortion Control During Vacuum Oil Quenching of High StrengthSteel Aircraft Components

133C. Filice, J.E. Pritchard, VAC AERO International Inc., Oakville, Ontario, Canada

Distortion Control in Gear Heat Treating 139M. Tristano, Lindberg Heat Treating Co ., Racine, Wisconsin

High Pressure Gas Quenching

Flexibility and Enhanced Performance with High Pressure Gas Quenching

143S. G. Kowalski, Kowalski Heat Treating Co ., Inc., Cleveland, Ohio

Induction Equipment Choices Important to Heat Treaters

Controls for Induction Heat Treating Systems A - Z

147FR. Specht, Ajax Magnethermic Corp ., Warren, Ohio

A Comparison of Radio Frequency Power Supplies

155R.L. Cook, Inductoheat, Inc ., Madison Heights, Michigan

Low Temperature Vacuum Heat Treating

Oxide Free Processing Below 1200°F in Atmosphere and Vacuum Tempering Furnaces

161W.J. Titus, Holcroft Inc ., Livonia, Michigan

Low Temperature Vacuum Heat Treating

173D.H. Herring, C.I. Hayes, Inc., Cranston, Rhode Island

XIra

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Nitrogen Based Atmospheres vs. Generated Atmospheres

On-Site Gas Production Service Provides Efficient Delivery of High-Purity Nitrogen

183M. Renowden, Air Liquide America Corp ., Countryside, Illinois

A Trouble -Shooting Guide for Furnace Atmospheres Used in MetalProcessing Applications

187M.S. Stanescu, J. J. Dwyer, Jr., T Philips, BOC Gases, Murray Hill, New Jersey

Powder Metal Heat Treatment

High Temperature Sintering Applications Using Vacuum Technology201D.H. Herring, C.I. Hayes, Inc ., Cranston, Rhode Island

Key Considerations in the Heat Treatment of Ferrous P/M Materials

211D.H. Herring, PT Hansen, C. I. Hayes, Inc., Cranston, Rhode Island

Process, Problems and Solutions Heat Treating Fasteners inToday's Mesh Belt Furnaces

Reduction of Hydrogen Embrittlement in High Strength and Precision Fasteners

221R. Rink, ALD Aichelin GmbH, Korntal, Germany

Solving Applications Through Innovative Equipment Design

Quench Tank Agitation Design for Heavy Gauge Loads

225N. Bogh, Despatch Industries, Minneapolis, Minnesota

xiv

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Non-Ferrous

Aluminum Heat Treating

Fabrication and Heat Treatment of Aluminum Automotive Components

231D. B. Rogers, Amcast Automotive, Wapakoneta, OhioB.G. Koepke, Despatch Industries, Minneapolis, Minnesota

Thermal Conductivity of a Heat Treatable Cast Aluminum Alloy

237C. Huitron, S. Valtierra, JF. Mojica, S.A. de C. V, Monterrey, MexicoE. Valdez, Instituto Tecnologico de Saltillo, Saltillo, MexicoR. Colas, Universidad Autonoma de Nuevo Leon, Monterrey, Mexico

Determination of Continuous Cooling Precipitation Diagrams by Means ofThermal Analysis 243

J.P. Vazquez, J. L. Cavazos, R. Colas, UniversidadAutonoma de Nuevo Leon, Monterrey, Mexico

Aluminum Quenching with Polymer Quenchants : An Overview

247G.E. Totten, G.M. Webster, Union Carbide Corporation, Tarrytown, New YorkC. E. Bates, University of Alabama-Birmingham, Birmingham, Alabama

Panel Discussion : Challenges in the Heat Treatment of Aluminum Castings

257D. Irani, P Olson, Hitchcock Industries, Inc., Minneapolis, MinnesotaS. Shivkumar, Worcester Polytechnic Institute, Worcester, MassachusettsM. Tiryakioglu, Western Kentucky University, Bowling Green, Kentucky

Distortion and Residual Stresses

The Interactive Effects of Sr Modification and Heat Treatment on the MechanicalProperties of Cast Aluminum Alloys

265S. Shivkumar, Worcester Polytechnic Institute, Worcester, Massachusetts

Quench Distortion in Simple Shaped Aluminum Castings

271M. Tiryakioglu, C. D. Major, R. Crowe, Western Kentucky University, Bowling Green, Kentucky

Processes

Modeling Carburizing, Nitriding and Related Diffusional SurfaceTreatments Process Control

Monitoring Carburization in Rotary Retort Furnaces

289C.A. Stickels, ERIM, Ann Arbor, Michigan

On Line Diffusion Calculation and Process Control

297T Guler, Thermovac Pty., Ltd., Queensland, Australia

A Discussion of Unique Applications Using CARB-CALC Modeling Software

303R.L. Houghton, C. I. Hayes, Inc., Cranston, Rhode Island

xv

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Modeling Carburizing, Nitriding and Related Diffusional SurfaceTreatments Microstructure and Properties

Finite Element Simulations of the Carburizing "Corner Effect"

307B. Dupen, Wix Division of Dana Corp ., Gastonia, North CarolinaJ. E. Morral, University of Connecticut, Storrs, ConnecticutC. C. Law, Pratt & Whitney, East Hartford, Connecticut

Simulation of Carburization in Secondary Hardening Steels

313C.J. Kuehmann, QuesTek Innovations, Evanston, IllinoisJ.R Wise, G.B. Olson, Northwestern University, Evanston, IllinoisC. E. Campbell, National Institute of Standards, Gaithersburg, Maryland

Modeling the Kinetics of Nitriding and Nitrocarburizing of Iron

321M.A.J. Somers, E.J. Mittemeijer, Delft University of Technology, Delft, The Netherlands

Elastic Layered-Model of Gas/Plasma Nitrided Fe-Cr System byAcoustic Spectro Microscopy

331T Aizawa, University of Tokyo, Tokyo, JapaH. Kuwabara, Institute of Applied Science, Kyoto, Japan

Quenching and CoolingNew Methods and Modeling

Heat Transfer of Turbine Disks in a Liquid Quench : Part I - Experimental Setup

341R. Bass, D. Leonard, Techxperts Inc ., Tolland, Connecticut•

Allen, J. C. Bennett Jr., M. Cross, J. Morral University of Connecticut, Storrs, Connecticut•

Brown, Computer-Aided Structural Analysis, Tolland, Connecticut

Predicting Hardness Distribution after Heat Treating Processes of Steels by FiniteElement Simulation Combined with the SAE Standard J406 347

G. S. Sanchez-Sarmiento, Universidad de Buenos Aires, ArgentinaJ. Vega, Sudosilo SA, Cordoba, Argentina•

Barragan, LEMIT, Bunos Aires, Argentia

A Numerical Validation of Lumped Capacitance Analysis for Deriving Heat TransferCoefficient Using Quenching Probe 355

Chen, L. Meekisho, M. Becker, Oregon Graduate Institute of Science and Technology,Portland, Oregon

G.E. Totten, Union Carbide Corporation, Tarrytown, New York

xvi

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Quenching and CoolingSteel Quenching Methods

Single Part Heat Treating of Rings in the Production Line

363J.G. Wuenning, WS Inc., Elyria, Ohio

Control of Quenching Systems in the Heat Treatment of Gear Products

369D.A. Guisbert, Quality Associates of Buchanan, Buchanan, Michigan

Applications of Polymer Quenchants for High Hardenability, Crack-Sensitive Steels

373S. W Han, S.H. Kang, Kum Won Industrial Co. Ltd., Chungnam, KoreaG.E. Totten, G.M. Webster, Union Carbide Corporation, Tarrytown, New York

Quenching and CoolingQuench Systems

Heat Transfer Control in Water Quenching by Fluid Vibration with Vapor Condensation

381M. Narazaki, M. Kogawara, A. Shirayori, S. Fuchizawa, Utsunomiya University, Utsunomiya,

Tochigi, Japan

Computational Simulations of Quench Tank Flow Patterns

389W W Bower, A .B. Cain, TD. Smith, McDonnell Douglas Corporation, St . Louis, Missouri

Maintaining a Clean Quench System

395B. Paddock, Paddock Enterprises, Bloomington, Illinois

Quenching and CoolingQuenching -General Subjects

Investigation of Agitation Chamber Design for Off-Line Cooling Curve Analysis399D.A. Guisbert, Quality Associates of Buchanan, Buchanan, MichiganD.L. Moore, Instruments and Technology Inc., Naperville, Illinois

Limitations of the Use of Grossman Quench Severity Factors

411G.E. Totten, G .M. Webster, Union Carbide Corporation, Tarrytown, New YorkC. E. Bates, University of Alabama-Birmingham, Birmingham, AlabamaS. W Han, S.H. Kang, Kum Won Industrial Co. Ltd., Ahsan, Korea

Proposal to Monitor Agitation of Production Quench Tanks

423H.M. Tensi, Technical University of Munich, Munich, GermanyG.E. Totten, G .M. Webster, Union Carbide Corporation, Tarrytown, New York

Investigation of the Mechanism of Polymer Quenchant Mediation of Heat TransferDuring Quenching by ESR Spectroscopy 433

D. McLleod, Jr., Briarcliffe Manor, New YorkG.E. Totten, G .M. Webster, Union Carbide Corporation, Tarrytown, New York

xvii

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Thermal/Oxidative Stability and Polymer Dragout Behavior of Polymer Quenchants443G.E. Totten, G.M. Webster, Union Carbide Corporation, Tarrytown, New YorkL.M. Jarvis, Tenaxol Inc ., Milwaukee, WisconsinS.H. Kang, S. W. Han, Kum Won Industrial Co . Ltd., Ahsan, Korea

Performance and Computer Simulation of Large H13 Dies in Vacuum Heat Treatment

449I. ElKatatny, P Jaques, A . Blicblau, Y Morsi, D. Doyle, Swinburne University of Technology,

Hawthorn, Victoria, Australia

Four Years Experience Using an Inconel Probe to Test the Cooling Characteristicsof Production Quench Oil 457

R.A. Wallis, S. Owens, Wyman-Gordon Forgings, Houston, TexasR.I. San Pedro, Stress Engineering Services, Houston, Texas

Experimental Research of the Cooling Characteristics of Liquid-Solid Fluidized Bed

467J. Zhou, University of Hawaii, Honolulu, HawaiiR. Zhou, Jiangsu University of Science and Technology, People's Republic of China

Diffusion Related ProcessesShafts

Infrared Gas Analysis and Control Used in the Continuous Heat Treatmentof Powder Metal Parts

473M.J. Fischer, N. W. Levine, Surface Combustion, Inc., Maumee, Ohio

Diffusion Related ProcessesUnique

The Effect of Hardenability, Size and Geometry on Steel Carburizing

477A. Habib, Smith Tool, Ponca City, Oklahoma

Steel TransformationsHeat Treatment of Steels

Tempering of Case Hardened Components

489G. Fett, Dana Corporation, Fort Wayne, Indiana

Microstructure of Austempered High Silicon Alloy Steels

499Y Wang, D. Zhang, Y. Shan, Y Li,, Institute of Metal Research, Shenyang,

People's Republic of China

Page 18: Including the 1997 International Induction Heat Treating

Student Research in Progress

The Correlation Between Hardness and Strength for Cast Iron 507N. Lyssenko, A . V Sverdlin, Bradley University, Peoria, Illinois

Student Research in Progress Poster Session

Influence of Melt State on High Resistant Ferrous Powder

513B.A. Baum, G. V. Tjagunov, E.E. Barishev, T.K. Kostina, L . G. Savina, Ural State

Technical University, Ekaterinburg, RussiaA. V Sverdlin, Bradley University, Peoria, Illinois

Influence of Melt Preparing Technology on Structure and Propertiesof Superalloy Powders 517

B.A. Baum, G. V Tjagunov, E.E. Barishev, T.K. Kostina, I. V Vandisheva 0. V Savin,,Ural State Technical University, Ekaterinburg, Russia

A . V Sverdlin, Bradley University, Peoria, Illinois

1997 International Induction Heat Treating Symposium

Session 1 : Application and Technology

Induction Heat Treatment Process Under Inert Gas Atmosphere

525D. Bartknecht, Inductionserwarmung Fritz Dusselforf GmbH, Freiburg, Germany

Adjustable Single Shot Hardening Inductor

529P Nowak, K.-H. Muller, EMA Elektro Maschinen Schultz GmbH, Hirschhorn, Germany

Session 2 : Mathematical Modeling I

Simulation of Residual Stresses/Distortion and Structural Change in the Course ofStationary and Scanning Induction Hardening Processes for Steel Rings and Cylinders

541F Ikuta, Neturen Co., Ltd., Kanagawa, JapanT Inoue, Kyoto University, Kyoto, Japan

Advanced Computation Software for Everyday Use in Modern Induction Heat Treating

551V Rudnev, Inductoheat, Inc ., Madison Heights, MichiganV Demidovich, St. Petersburg El. Technical University, St. Petersburg, Russia

TORO II Simulations of Induction Heating in Ferromagnetic Materials

557D.R. Adkins, D.K. Gartling, J.B. Kelley, PM. Kahle, Sandia National Laboratories,

Albuquerque, New Mexico

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Session 3 : Innovations in Systems and Materials

Innovative Induction Heat Treating Technologies : Process/Design Features, Control,Quality Assurance and Monitoring 567

W.B. Albert, R . Cook, T Boussie, J. LaMonte, Inductoheat, Inc ., Madison Heights, Michigan

Effects of Induction Hardening and Prior Cold Work on a Microalloyed MediumCarbon Steel 575

J. L. Cunningham, American Axle and Manufacturing, Rochester Hills, MichiganD.J. Medlin, G . Krauss, Colorado School of Mines, Golden, Colorado

Session 4: Mathematical Modeling II

Numerical Simulation of Induction Heating and Quenching

587M. Swierkosz, O. Greim, J.-E Joyeux, Calcom SA, Lausanne, SwitzerlandM. Rappaz, A. Jacot, J. Rappaz, Swiss Federal Institute of Technology, Lausanne, SwitzerlandD. Mari, Amysa-Yverdon SA, Yverdon-les-Bains, Switzerland

Optimization of Process Parameters for Induction Heat Treating by Means ofNumerical Simulation

595A. Schopfel, K. Storzel, Fraunhofer-Institut fur Betriebsfestigkeit LBF, Darmstadt, Germany

Modeling Induction Heating Processes for Numerical Simulation 601M. Enokizono, T Todaka, Oita University, Oita, Japan

Session 5 : Innovations In Power Supply Design I

Design of a High Power, Very High Bifrequency Inverter for Contour InductionHardening Applications

611E. J. Dede, J. V. Gonzalez, V Esteve, J. Jordan, G.H. -EL/N International S.A ., Valencia, Spain

Solid State Power Supplies for Modern Induction Metal Heat Treating

615D.L. Loveless, Inductoheat, Inc ., Madison Heights, Michigan

Session 6: Application and Processes I

Induction Hard-Facing for Restoration and Hardening Details of Machinesand Mechanisms

623V V Vologdin, FREAL -Ltd ., St. Petersburg, RussiaV.M. Ganiuchenko, Electrotechnical University, St . Petersburg, Russia

Residual Internal Stresses After Induction Hardening and Grinding

629J. Grum, D. Ferlan, University of Ljubjana, Ljubljana, Slovenia

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Session 7: Quenching, Processing and Materials

Induction Carburizing

643S.M. Gugel, Sanova-PolyTech Inc ., Brooklyn, New York

Advanced Steels for Modern Induction Through and Surface Hardening

651K.Z. Shepelyakovskii, "TECHMASH," Moscow, RussiaF Bezmenov, VNIITVCh, St. Petersburg, Russia

Session 8: Innovations In Power Supply Design li

Latest Developments of Voltage-Fed Resonant High-Frequency Inverter with Load ResonantFrequency Tracking Scheme for Induction Heating 657

M. Kurokawa, M. Nakaoka, B. Guo, Yamaguchi National University, Yamaguchi, JapanA. Okuno, Shinko Electric Co., Ltd., Mie, Japan

Power Supplies for Induction Heat Treating with Special Method of Energy Control

665TS. Todorov, N. D. Madgarov, E. P. Tsonkov, D. T. Alexiev, P T Ivanov Technical University,

Gabrovo, Bulgaria

Session 9: Process and Equipment Innovations

Determination of Austenitic Transformation During Fast Heat Treatment

671C. Durban, D. Durand, P Chevre, ENSAM, Talence, France

Innovations in Induction Heat Treating Techniques for Control of Distortion andImproving Dimensional Results

677G.D. Pfaffmann, TOCCO, Inc., Madison Heights, Michigan

Advanced Design of Induction Heat Treating Coils

687R. S. Ruffini, R. T Ruffini, Fluxtrol Manufacturing, Inc ., Auburn Hills, MichiganVS. Nemkov, Centre for Induction Technology, Auburn Hills, Michigan

Session 10: Innovations In Power Supply Design III

Past, Present, and Future in Transistorised Inverters for Induction Heating Applications

699E.J. Dede, V Esteve, J. V Gonzalez, J. Jordan, GH-ELIN International S.A ., Valencia, Spain

Future Trends in Solid State Induction Heating Power Supplies On-Board Diagnostics

705T Gupta, TOCCO, Inc., Boaz, Alabama

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Session 11 : Equipment Design Developments

Latest Technology in Flux Field Concentrators

711J. Stambaugh, Alpha 1 Induction Service Center, Columbus, OhioT Learman, LearTech, Ferrysberg, Michigan

Optimization Techniques Applied to the Design of Continuous Induction Hardeningand Tempering Lines 719

M. Battistetti, F Dughiero, S . Lupi, University of Padova, Padova, Italy

Session 12: Process Control Developments

Novel Process of Quality Control During Inductive Hardening Process

727H. Matthes, AEG Elotherm GmbH, Remscheid, Germany

Fundamentals of Specifying Induction Power Supplies for Wire and Rod Heating735D.J. Williams, G .J. Traverse, Welduction Corporation, Farmington Hills, Michigan

Session 13: Innovations In Power Supply Design IV

Electromagnetic Induction-Based Fluid Heating Appliance Using New Phase-ShiftedPWM Load Resonant Inverter 747

M. Yamamoto, M. Nakaoka, B. Guo, T Iseki, A . Chibani, L . Gamage, YamaguchiNational University, Yamaguchi, Japan

Session 14: Materials and Processes Considerations

Input and Output Control of Steel Intended for Surface Hardening

763J. Grum, University of Ljubljana, Ljubljana, Slovenia

Reduction of Electromagnetic Stray-Fields in the Surrounding of Industrial InductionHeating Installations by Optimized Design

769E. Baake, G. Nauvertat, University of Hanover, Hanover, Germany

Intrinsic Material Properties After Short Time Austenitization

777J. Rollmann, B . Kaiser, K.H. Kloos, C. Berger, University of Darmstadt, Darmstadt, Germany

Session 15 : Mathematical Modeling III

Computer Simulation-an Effective Creative Tool for Development of InductionHeat Treating Processes

785VS. Nemkov, Centre for Induction Technology, Auburn Hills, MichiganV Bukanin, A. Zenkov, D. Koutchmassov, Electrotechnical University, St. Petersburg, Russia

Math Modeling Techniques Applied to Induction Heat Treating

793R.A. Akers, R.H. McKelvey, L. Wang, TOCCO, Inc., Boaz, Alabama

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Seaaion 16: Innovaaiona in Inducaion Heaa Taeaaing

Deaigning Poweaaaain Comaonenaa ao Oaaimize Inducaion Heaa Taeaamena Pefoamance801E. Peaaaon, GM Poweaaaain, Uaailanai, Michigan

Technology and Eauiamena foa Haadening of Geaaa 811F V Bezmenov, VNIITVCh, Sa. Peaeaabuag, RuaaiaKZ. Sheaelyakovaky, NPO "Tekhmaah", Moacow, Ruaaia

Seaaion 17: Paoceaa Conaaol Technology Imaaovemenaa

Auaomaaic Veaificaaion of Inducaion Haadening Uaing Eddy Cuaaena and PaevenaiveMulai-FaeauencyTeaaing 817

B. Buachua, ibg NDT Syaaema Coaa., Faamingaon Hilla, Michigan

Exaeaience faom Teaaing wiah Senaoaa and IR -Techniaue foa Moniaoaing aheInducaion Heaaing Paoceaa 827

H. Kaiaaoffeaaen, The Swediah Inaaiauae of Paoducaion Engineeaing Reaeaach, Molndal, Sweden

Inaeaacaive Moniaoaing and Conaaol of Inducaion Heaa Taeaa Paoceaaea835G.M. Gaaiglio, Inaea-Powea Coaa ., Imlay Ciay, Michigan

Seaaion 18: Maahemaaical Modeling IV

Inducaea-B : A Finiae Elemena Heaa Taanafea- Phaae Taanafoamaaion Model of InducaionHeaa Taeaaing of Saeela Senaiaive ao Chemical Comaoaiaion 841

G.S. Sanchez-Saamienao, Univeaaidad de Buenoa Aiaea, Buenoa Aiaea, AagenainaJ. Vega, SUDOSILO SA, Coadoba, AagenainaA. Gaaaon, Univeaaidad Nacional de Roaaaio, Roaaaio, Aagenaina

Numeaical and Exaeaimenaal Saudy of an Inducaion Heaaea foa Haadening ofTaaveling Caane Wheela 849

PA. Kaaamanaki, A. Kauaaeva, A . Dimiaaova, Technical Univeaaiay, Sofia, BulgaaiaM. Dimiaaov, Inaaiauae of Meaal Science, Sofia, Bulgaaia

Seaaion 19 : Maahemaaical Modeling V

Coualed Phenomena and Modeling of Maaeaial Paoaeaaiea in Quench HaadeningFollowing Inducaive Heaaing of ahe Suaface 855

Duaand, C. Duaban, F Giaoa, ENSAM, Talence, Faance

Meahoda and Toola foa All -Round Oaaimizaaion of Taanaveaae-Flux Inducaion Heaaeaa865A. Muehlbauea, A. Ruhnke, Univeaaiay of Hanovea, Hanovea, GeamanyV Demidoviach, A . Nikanoaov, Elecaaoaechnical Univeaaiay of Sa . Peaeaabuag, Sa. Peaeaabuag, RuaaiaS. Luai, F Dughieao, Univeaaiay of Padova, Padova, Iaaly

Numeaical Simulaaion of Conainuoua Inducaion Baa End Heaaing foa Foaging oa Haadening871•

Ludake, D. Schulze, Technical Univeaaiay of llmenau, llmenau, Geamany•

Wohlfahaa, Inducal Gollingen GmbH, Gollingen, Geamany

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Session 20: Process Technology Advancements

The Influence of Tempering and Sprface Conditions on the Fatigue Behavior ofSurface Induction Hardened Parts

879PK. Braisch, Institut fur Werkstoffkunde, Darmstadt, GermanyG.D. Pfaffmann, TOCCO Inc ., Madison Heights, Michigan

Multi Frequency Induction Hardening of Gears to Replace Carburizing -Methodology of Development

887B. Criqui, Renault DR, Rueil-Malmaison, FranceS. Plano, Centro Ricerche FIAT, Orbassano, ItalyF Ruckstuhl, PSA MXT, Montbelliard, FranceB. Ottosson, Volvo, Goteborg, SwedenO. Longeot, C. Delaleau, ENSAM, Talence, FranceG. Bonzano, SAET, Leini-Torino, ItalyC. Pichard, Ascometal-CREAS, Amneville, France

Prediction of the Hardness Decrease Occurring During Non-Isothermal Tempering

895T Reti, L. Horvath, Bank Donat Polytechnic, Budapest, HungaryG.D. Pfaffmann, TOCCO Inc., Madison Heights, Michigan

Poster Session

Improvement of Scale Reduction in Induction Heaters for Forging

907A. Muehlbauer, R. Boergerding, R. Drewek, K.-U. Joern, University of Hanover,

Hanover, Germany

Technology and Equipment for Induction Annealing of Rolling Surface ofRailroad Wheels

915VV Vologdin, S. S. Nemkov, FREAL-Ltd., St. Petersburg, Russia

The Electrical and Magnetic Field (EMF) Surrounding Induction Heaters and Workcoilsand Ways of Reducing Operator Exposure

917T Learman, LearTech, Inc., Ferrysburg, Michigan

How Induction Tempering Works

923G.D. Pfaffmann, TOCCO, Inc., Madison Heights, Michigan

Systems for Automatic Control of Induction Heating Devices with ContinuousSeries Action

927PA. Karamanski, A . Krusteva, S. Denchev, A . Dimitrova, Technical University, Sofia, Bulgaria

CELINE: Compact Electromagnetic Induction Equipment - High Flux InductionHeating for Metallurgical Semi-Products

933J. Uring, Celes, Lautenbach, France

Induction Skull Melting of Glasses, Oxides, Salts and Similar Materials

939J. Uring, Celes, Lautenbach, France

Induction Heating Applications in Railway Transport

943V.N. Ivanov, VG. Shevchenko, VI. Chervinsky, VV Vologdin, VNIITVCh, St. Petersburg, Russia

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Computer Simulaton and Optimization of Local Induction Heating of Flat Metal

947N. Kandev, Hydro-Quebec (LTEE), Shawinigan, Quebec, CanadaVS. Nemkov, Center for Induction Technology, Auburn Hills, Michigan

Bath Maintenance and Troubleshooting of Polymer Quenchant-Related Problemsfor Induction Heat Treating 951

G.E. Totten, G .M. Webster, Union Carbide Corporation, Tarrytown, New YorkR.R. Blackwood, L.M. Jarvis, Tenaxol, Inc ., Milwaukee, Wisconsin

xxv