cumulative heat test 17 zrsio4lamcos.insa-lyon.fr/files/poster/pdf/109.pdf · pad (70 % matrix...

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Conclusions Morphology differences - correlation for the last contact phase Thermo-mechanical and tribological analysis of pad- disc contact in a braking tribometer [email protected] [email protected] [email protected] [email protected] [email protected] Mechanical features Surface evolution after contact: common aspects for both case scenarios Introduction Contacts Heat evolution: pad measurements D. Tumbajoy-Spinel 1 , Y. Desplanques 2 , A. L. Cristol 2 , A. Beaurain 2 , Y. Berthier 1 , S. Descartes 1 1. Univ Lyon, CNRS, INSA-Lyon, UMR5259 LaMCoS, F-69621 Villeurbanne, France 2. Univ Lille, CNRS, Centrale Lille, FRE 3723 LML, F-59000 Lille, France Test 1 Test 2 Short cooling period between tests Pad Disc TDo T [ºC] t [s] Test 3 Test 4 WITH CUMULATIVE HEAT Test 1 Test 2 Cooling until initial disc temperature threshold (TDo) Pad Disc TDo T [ºC] t [s] WITHOUT CUMULATIVE HEAT 50 mm The main issue of this work is to understand the material behavior in a disc-pad interaction under similar mechanical conditions but different thermal backward histories. In this project, experimental tests are performed in a braking tribometer set-up [1] using a steel disc (C45) and a metallic composite pad (70 % matrix Fe/Cu, 20 % graphite and 10 % ceramics SiC/ZrSiO4) [2]. Two different sequences are carried out using slowdown braking tests: (i) without and (ii) with cumulative heat. At the end of each cycle, a hold-braking test is done to restore the pad surface for both case scenarios. The surface tribological evolutions are correlated with the thermo-mechanical measurements. A comparison between both cases (i, ii) is carried out as well. Pad temperatures are measured by thermocouples at 2 mm from the near-surface. This data permits to point out a contour map of pad temperature gradients. Despite of the thermal fluctuations, the global mechanical conditions remain the same for both cases (mean friction coefficient of 0.4). Braking test sequences are composed by 5 main phases: Specific braking test sequences were developed in order to produce fairly recurrent mechanical states and to compare two different thermal backward histories for the same disc-pad contact. During the phase #3 (Tests), the temperature gradient reveals some contact alternation between the external regions and the central region of the pad. The IR thermography of the disc reveals that the contact starts in the outer radius and it migrates to the inner regions. For the phase #5 (hold-braking), the thermal gradient shows that the mechanical contact settle on the external radius of the pad. Effect of local temperature: The surface of the pad evolves differently according to the local temperature level at each region. Homogeneous 3 rd body plateaus appear in zones of higher temperatures (higher power dissipation) for the last mechanical phase: hold-braking. Third body morphologies: third body in the case of “cumulative heat” sequence is compacted and fully mixed, while it is powdery in the case of “without cumulative heat” sequence. Δr [mm] θ [deg] In Out Int Ext TEST 17 WITH cumulative heat Temp. Δr [mm] θ [deg] In Out Int Ext TEST 3 WITH cumulative heat Temp. 1 2 3 4 5 6 7 8 9 10 12 13 14 15 16 17 18 19 11 20 TP1 X TP4 X TP7 X Inner radius 20 tests WITHOUT cumulative heat Inner radius 20 tests WITH cumulative heat 1 2 3 4 5 6 7 8 9 10 12 13 14 15 16 17 18 19 11 20 Δr [mm] θ [deg] In Out Int Ext TEST 6 WITHOUT cumulative heat Temp. Δr [mm] θ [deg] In Out Int Ext Temp. TEST 7 WITHOUT cumulative heat TEST 6 TEST 7 TEST 3 TEST 17 TP7 = Tmax = 340 ºC TP4 = Tmax = 350 ºC TP4 = Tmax = 600 ºC TP7 = Tmax = 430 ºC Surface preparation TEST Surface Restoration 1 2 4 3 5 Scenario 1 WITHOUT cumulative heat Scenario 2 WITH Cumulative heat T9 T8 T7 T11 T6 T5 T4 T10 T3 T2 T1 V Sortie Entrée θ 40º 20º r ωdisc In PAD Out 1000 μm 1000 μm 1000 μm 1000 μm Before contact Without cumulative heat With cumulative heat Sliding direction Sliding direction Sliding direction 3 rd body (powder) SiC ZrSiO4 500 μm SEM (BSE) Graphite Metallic matrix (Cu/Sn, Fe) Sens du contact 500 μm 3 rd body - spread layer (mainly Fe, O) 3 rd body - powder (mainly Fe, O) IR Thermography of the disc References: 500 1000 1500 2000 ω [rpm] t [s] Running-in Pre-TESTS 20 TESTS HOLD Post-TESTS Scenario 1 : without C. H. Scenario 2 : with C. H. 1 2 4 3 5 TEST 3 Disc Pad ω T Ft Fn Loading Force Phase 1. Running-in 2. Pre-TESTS 3. TESTS 4. Post-TESTS 5. Hold Brakings (amount) 40 5 20 5 1 ωo [rpm] 1000 800 1700 800 500 ωf [rpm] 300 300 300 300 500 Inertia [kgm²] 5 10 10 10 --- Fn [N] 1000 1000 1000 1000 1000 Dissipated Energy [kJ] 24.9 30.2 153.5 30.2 --- Δr [mm] θ [deg] In Out Int Ext HOLD WITH cumulative heat Temp. Δr [mm] θ [deg] In Out Int Ext HOLD WITHOUT cumulative heat Temp. Tmax Tmax 500 μm TP9 = 170 ºC 500 μm TP7 = 210 ºC 500 μm TP1 = 150 ºC 500 μm TP3 = 290 ºC Patchy 3 rd body Powdery 3 rd body Compacted fully mixed 3 rd body Compacted patchy 3 rd body [1] Y. Desplanques, O. Roussette, G. Degallaix, R. Copin, Y. Berthier, Wear, Vol. 262, p. 582-591, 2007. [2] R. Mann, V. Magnier, J.F. Brunel, F. Brunel, P. Dufrénoy, M. Henrion, Wear, Vol. 386-387, p. 1-16, 2017. Acknowledgement This work is supported by the French National Research Agency (ANR-12-VPTT-0006 CoMatCo). The authors would like to thank the academic and industrial partnership with Sapienza University, Flertex Sinter and Chassis Brakes International. 500 μm 10 μm 30 μm 200 μm 5 μm 5 μm Sliding direction Thin layer of 3 rd body formed by powder agglomeration 3 rd body plateaus Internal flow of 3 rd body Fine layer of spread 3 rd body powder covering other composite elements (graphite, metallic matrix, ceramics) 3 rd body powder is spread by compacting and shearing, leading a layer of piled up thin “Stratums” 3 rd body particle size gradient SiC particles fragmentation Lamellar morphology Graphite A A B B C C D E D E Trapped 3 rd body powder filling surface valleys and hollows C O Fe Cu Si Zr Fe Fe Cu 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 0 1 2 3 4 5 6 7 8 9 10 Count keV Count EDX ZrSiO4 keV C O Fe Cu Si Mn Fe Fe Cu 0 1000 2000 3000 4000 5000 6000 7000 8000 9000 10000 0 1 2 3 4 5 6 7 8 9 10 Count Count EDX - 3 rd body keV

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Page 1: cumulative heat TEST 17 ZrSiO4lamcos.insa-lyon.fr/files/poster/pdf/109.pdf · pad (70 % matrix Fe/Cu, 20 % graphite and 10 % ceramics SiC/ZrSiO 4) [2]. Two different sequences are

Conclusions Morphology differences - correlation for the last contact phase

Thermo-mechanical and tribological analysis of pad-disc contact in a braking tribometer

[email protected] [email protected]

[email protected] [email protected]

[email protected]

Mechanical features

Surface evolution after contact: common aspects for both case scenarios

Introduction

Contacts

Heat evolution: pad measurements

D. Tumbajoy-Spinel1, Y. Desplanques2, A. L. Cristol2, A. Beaurain2, Y. Berthier1, S. Descartes1

1. Univ Lyon, CNRS, INSA-Lyon, UMR5259 – LaMCoS, F-69621 Villeurbanne, France 2. Univ Lille, CNRS, Centrale Lille, FRE 3723 – LML, F-59000 Lille, France

Test 1 Test 2

Short cooling period between tests

Pad

Disc

TDo

T [ºC]

t [s]Test 3 Test 4

WITH CUMULATIVE HEAT

Test 1 Test 2

Cooling until initial disc temperature threshold (TDo)

Pad

Disc

TDo

T [ºC]

t [s]

WITHOUT CUMULATIVE HEAT

50 mm

The main issue of this work is to understand the material behavior in a disc-pad interaction under similar mechanical conditions but different thermal backward histories. In this project, experimental tests are performed in a braking tribometer set-up [1] using a steel disc (C45) and a metallic composite pad (70 % matrix Fe/Cu, 20 % graphite and 10 % ceramics SiC/ZrSiO4) [2]. Two different sequences are carried out using slowdown braking tests: (i) without and (ii) with cumulative heat. At the end of each cycle, a hold-braking test is done to restore the pad surface for both case scenarios. The surface tribological evolutions are correlated with the thermo-mechanical measurements. A comparison between both cases (i, ii) is carried out as well.

Pad temperatures are measured by thermocouples at 2 mm from the near-surface. This data permits to point out a contour map of pad temperature gradients. Despite of the thermal fluctuations, the global mechanical conditions remain the same for both cases (mean friction coefficient of 0.4).

Braking test sequences are composed by 5 main phases:

Specific braking test sequences were developed in order to produce fairly recurrent mechanical states and to compare two different thermal backward histories for the same disc-pad contact.

During the phase #3 (Tests), the temperature gradient reveals some contact alternation between the external regions and the central region of the pad. The IR thermography of the disc reveals that the contact starts in the outer radius and it migrates to the inner regions.

For the phase #5 (hold-braking), the thermal gradient shows that the mechanical contact settle on the external radius of the pad.

Effect of local temperature: The surface of the pad evolves differently according to the local temperature level at each region. Homogeneous 3rd body plateaus appear in zones of higher temperatures (higher power dissipation) for the last mechanical phase: hold-braking. Third body morphologies: third body in the case of “cumulative heat” sequence is compacted and fully mixed, while it is powdery in the case of “without cumulative heat” sequence.

Δr

[m

m]

θ [deg] InOut

Int

Ext

TEST 17 – WITH cumulative heat Temp.

Δr

[m

m]

θ [deg] InOut

Int

Ext

TEST 3 – WITH cumulative heat Temp.

1 2 3 4 5 6 7 8 9 10 12 13 14 15 16 17 18 1911 20

TP1 XTP4 XTP7 X

Inner radius – 20 tests WITHOUT cumulative heat

Inner radius – 20 tests WITH cumulative heat

1 2 3 4 5 6 7 8 9 10 12 13 14 15 16 17 18 1911 20

Δr

[m

m]

θ [deg] InOut

Int

Ext

TEST 6 – WITHOUT cumulative heat Temp.

Δr

[m

m]

θ [deg] InOut

Int

Ext

Temp.TEST 7 – WITHOUT cumulative heat

TEST 6 TEST 7

TEST 3

TEST 17

TP7 = Tmax = 340 ºC TP4 = Tmax = 350 ºC

TP4 = Tmax = 600 ºCTP7 = Tmax = 430 ºC

Surf

ace

p

rep

arat

ion

TEST

Surf

ace

Res

tora

tio

n

1 2 43

5

Scenario 1WITHOUT

cumulativeheat

Scenario 2WITH

Cumulativeheat

T9

T8

T7

T11

T6

T5

T4

T10 T3

T2

T1

V

Sortie Entrée

θ40º

0º20º

r

ωdisc

In

PAD

Out

1000 µm

1000 µm

1000 μm

1000 μm

1000 μm

Before contact

Without cumulative heat

With cumulative heat

Sliding direction

Sliding direction

Sliding direction

3rd body(powder)

SiC

ZrSiO4

500 μm

SEM (BSE)

Graphite

Metallic matrix(Cu/Sn, Fe)

Sens du contact500 μm

3rd body -spread layer (mainly Fe, O)

3rd body - powder(mainly Fe, O)

IR Thermography of the disc

References:

……

500

1000

1500

2000

ω [rpm]

t [s]

Running-in Pre-TESTS

20 TESTS

HOLDPost-TESTS

Scenario 1 : without C. H.Scenario 2 : with C. H.1 2 4

3

5

TEST

3

Disc

Pad

ω

T

Ft

Fn

Loading Force

Phase 1. Running-in 2. Pre-TESTS 3. TESTS 4. Post-TESTS 5. Hold

Brakings (amount) 40 5 20 5 1

ωo [rpm] 1000 800 1700 800 500

ωf [rpm] 300 300 300 300 500

Inertia [kgm²] 5 10 10 10 ---

Fn [N] 1000 1000 1000 1000 1000

Dissipated Energy [kJ] 24.9 30.2 153.5 30.2 ---

Δr

[m

m]

θ [deg] InOut

Int

Ext

HOLD – WITH cumulative heat Temp.

Δr

[m

m]

θ [deg] InOut

Int

Ext

HOLD – WITHOUT cumulative heat Temp.

Tmax

Tmax

500 μm

TP9 = 170 ºC

500 μm

TP7 = 210 ºC

500 μm

TP1 = 150 ºC

500 μm

TP3 = 290 ºC

Patchy 3rd body

Powdery 3rd body

Compacted fully mixed 3rd body

Compacted patchy 3rd body

[1] Y. Desplanques, O. Roussette, G. Degallaix, R. Copin, Y. Berthier, Wear, Vol. 262, p. 582-591, 2007. [2] R. Mann, V. Magnier, J.F. Brunel, F. Brunel, P. Dufrénoy, M. Henrion, Wear, Vol. 386-387, p. 1-16, 2017.

Acknowledgement This work is supported by the French National Research Agency (ANR-12-VPTT-0006 CoMatCo). The authors would like to thank the

academic and industrial partnership with Sapienza University, Flertex Sinter and Chassis Brakes International.

500 μm10 μm 30 μm

200 μm 5 μm 5 μm

Sliding direction

Thin layer of 3rd body formed by powder agglomeration

3rd bodyplateaus

Internal flow of 3rd body

Fine layer of spread 3rd body powdercovering other

composite elements (graphite,

metallic matrix, ceramics)

3rd body powder is spread by

compacting and shearing, leading a

layer of piled up thin “Stratums”

3rd body particle size

gradient

SiC particles fragmentation

Lamellar morphology

Graphite

A

A B

B

C

C D E

D

E

Trapped 3rd body powder filling

surface valleys and hollows

C

O

Fe

Cu

Si Zr

Fe

Fe Cu0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

0 1 2 3 4 5 6 7 8 9 10

Co

un

t

keV

Co

un

t

EDX – ZrSiO4

keV C

O

Fe

Cu Si Mn

Fe

Fe Cu0

1000

2000

3000

4000

5000

6000

7000

8000

9000

10000

0 1 2 3 4 5 6 7 8 9 10

Co

un

t

keV

Co

un

t

EDX - 3rd body

keV