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Chemodivergent, multicomponent-tandem facile synthesis of novel 1H- pyrazolo[1,2-b]phthalazine-5,10-dione using acetic acid functionalized imidazolium salt {[cmdmim]I} as a recyclable catalyst Parivash Jahanshahi a , Manouchehr Mamaghani a * a Department of Chemistry, Faculty of Sciences, University of Guilan, P.O. Box 41335-1914, Rasht, Iran. *Corresponding author Email: [email protected] IR and NMR data of all compounds Spectral data for [cmdmim]I (S1): Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is © The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2019

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Page 1: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

Chemodivergent, multicomponent-tandem facile synthesis of novel 1H-pyrazolo[1,2-b]phthalazine-5,10-dione using acetic acid functionalized

imidazolium salt {[cmdmim]I} as a recyclable catalyst

Parivash Jahanshahia, Manouchehr Mamaghania*

aDepartment of Chemistry, Faculty of Sciences, University of Guilan, P.O. Box 41335-1914, Rasht, Iran.

*Corresponding author Email: [email protected]

IR and NMR data of all compounds

Spectral data for [cmdmim]I

(S1):

Electronic Supplementary Material (ESI) for New Journal of Chemistry.This journal is © The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2019

Page 2: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

(S2):

Page 3: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

Spectral data for pyrrole-substituted pyrazolo[1,2-b]phthalazine

5a:

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5b:

Page 5: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
Page 6: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5c:

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5d:

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Page 9: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5e:

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5f:

Page 11: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
Page 12: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5g:

Page 13: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5h:

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Page 15: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5i:

Page 16: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5j:

Page 17: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
Page 18: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5k:

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5l:

Page 20: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
Page 21: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5m:

Page 22: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
Page 23: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957

5n:

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5o:

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5p:

Page 27: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957
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5q:

Page 29: Chemodivergent, multicomponent-tandem facile synthesis of ... · NVCI PI PLI CPDPRC2 WC 2 PCPD2 PL2 PL12 PL13 PL2K SF02 ssg PC ppm 5 3322 20171231 9.03 zqpg 30 65536 2108 0.544957