certificate of analysis · 2019-12-31 · states environmental protection agency (epa). the...

[This report shall not be reproduced except in full without the written authority of the Laboratory.]

28-JUN-18

Lab Work Order #: L2121059

Date Received:GOVERNMENT OF YUKON

P.O. Box 2703 (E-1)Whitehorse YT Y1A 2C6

ATTN: Miles HumeFINAL 05-JUL-18 17:27 (MT)Report Date:

Version:

Certificate of Analysis

ALS CANADA LTD Part of the ALS Group An ALS Limited Company

____________________________________________

Heather McKenzieAccount Manager

ADDRESS: 8081 Lougheed Hwy, Suite 100, Burnaby, BC V5A 1W9 Canada | Phone: +1 604 253 4188 | Fax: +1 604 253 6700

Client Phone: 604-253-4188

Job Reference: NOT SUBMITTEDProject P.O. #:

17-653378, 17-653379, 17-653380, 17-653381, 17-653382

C of C Numbers:

Legal Site Desc:

05-JUL-18 17:27 (MT)

Sample ID Description

Client ID

Sampled Date

Grouping Analyte

Sampled Time

ALS ENVIRONMENTAL ANALYTICAL REPORT

L2121059 CONTD....

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WATER

Water Water Water Water Water28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18 28-JUN-18

DF1 INTERMEDIATE

WING

BS1 INTERMEDIATE

WING

BS2 INTERMEDIATE

WING

BS3 INTERMEDIATE

WING

DF2 INTERMEDIATE

WING

L2121059-1 L2121059-2 L2121059-3 L2121059-4 L2121059-5

10:00 10:01 10:02 10:03 10:04

Lead (Pb)-Total (mg/L) 0.000406 0.00275 0.00112 0.0179 0.00810Total Metals

05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


DF3 INTERMEDIATE

WING

*BS4 INTERMEDIATE

WING

BS5 INTERMEDIATE

WING

BS6 INTERMEDIATE

WING

CS1 INTERMEDIATE

WING

L2121059-6 L2121059-7 L2121059-8 L2121059-9 L2121059-10

10:05 10:06 10:07 10:08 10:09


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


CS2 INTERMEDIATE

WING

BS7 INTERMEDIATE

WING

BS8 INTERMEDIATE

WING (MAP)

CS3 INTERMEDIATE

WING

CF1 INTERMEDIATE

WING

L2121059-11 L2121059-12 L2121059-13 L2121059-14 L2121059-15

10:10 10:11 10:12 10:14 10:16


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


BS9 INTERMEDIATE

WING

BS10 INTERMEDIATE

WING

CS4 INTERMEDIATE

WING

CF2 INTERMEDIATE

WING

CS5 INTERMEDIATE

WING

L2121059-16 L2121059-17 L2121059-18 L2121059-19 L2121059-20

10:18 10:19 10:20 10:21 10:22


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


CF3 INTERMEDIATE

WING

LS1 MAIN HALL DENS1 MAIN HALL DENS2 MAIN HALL BS11 MAIN HALL (

L2121059-21 L2121059-22 L2121059-23 L2121059-24 L2121059-25

10:23 10:24 10:24 10:24 10:24


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


BS12 BS13 BS14 BS15 BS16

L2121059-26 L2121059-27 L2121059-28 L2121059-29 L2121059-30

10:25 10:25 10:25 10:26 10:26


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


*BS17 (SPRAY NOZZLE)

DF4 DF5 DF6 DF7

L2121059-31 L2121059-32 L2121059-33 L2121059-34 L2121059-35

10:27 10:28 10:28 10:29 10:29


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


CS6 (PRIMARY) CBS1 (PRIMARY WING)

BS18 CS7 CBS2

L2121059-36 L2121059-37 L2121059-38 L2121059-39 L2121059-40

10:29 10:30 10:32 10:32 10:33


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


CS8 CS9 OB1 CS10 CS11

L2121059-41 L2121059-42 L2121059-43 L2121059-44 L2121059-45

10:34 10:34 10:35 10:35 10:36


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER


CS12 CS13 KS1 BS19 BS20

L2121059-46 L2121059-47 L2121059-48 L2121059-49 L2121059-50

10:36 10:37 10:37 10:40 10:42


05-JUL-18 17:27 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121059 CONTD....

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WATER

Water Water Water28-JUN-18 28-JUN-18 28-JUN-18

T2-1 T2-2 T3-3

L2121059-51 L2121059-52 L2121059-53

10:44 10:45 10:46

Lead (Pb)-Total (mg/L) 0.000180 0.000176 0.000318Total Metals

Reference Information 05-JUL-18 17:27 (MT)

L2121059 CONTD....

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MET-T-CCMS-VA Total Metals in Water by CRC ICPMS

Water samples are digested with nitric and hydrochloric acids, and analyzed by CRC ICPMS.

Method Limitation (re: Sulfur): Sulfide and volatile sulfur species may not be recovered by this method.

ALS Test Code Test Description

Water EPA 200.2/6020A (mod)

Method Reference**

** ALS test methods may incorporate modifications from specified reference methods to improve performance.

Matrix

The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:

Laboratory Definition Code Laboratory Location

VA ALS ENVIRONMENTAL - VANCOUVER, BRITISH COLUMBIA, CANADA

GLOSSARY OF REPORT TERMSSurrogate - A compound that is similar in behaviour to target analyte(s), but that does not occur naturally in environmental samples. Forapplicable tests, surrogates are added to samples prior to analysis as a check on recovery.mg/kg - milligrams per kilogram based on dry weight of sample.mg/kg wwt - milligrams per kilogram based on wet weight of sample.mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight of sample.mg/L - milligrams per litre.< - Less than.D.L. - The reported Detection Limit, also known as the Limit of Reporting (LOR).N/A - Result not available. Refer to qualifier code and definition for explanation.

Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

Test Method References:

Chain of Custody Numbers:

17-653378 17-653379 17-653380 17-653381 17-653382

Version: FINAL

13

[This report shall not be reproduced except in full without the written authority of the Laboratory.]

29-JUN-18

Lab Work Order #: L2121514

Date Received:GOVERNMENT OF YUKON

113 Industrial RoadWhitehorse YT Y1A 2T8

ATTN: Trevor JustasonFINAL 06-JUL-18 09:51 (MT)Report Date:

Version:

Certificate of Analysis

ALS CANADA LTD Part of the ALS Group An ALS Limited Company

____________________________________________

Carla FuginskiAccount Manager

ADDRESS: 8081 Lougheed Hwy, Suite 100, Burnaby, BC V5A 1W9 Canada | Phone: +1 604 253 4188 | Fax: +1 604 253 6700

Client Phone: 604-253-4188

Job Reference: NOT SUBMITTEDProject P.O. #:

17-653392C of C Numbers: Legal Site Desc:

06-JUL-18 09:51 (MT)


Client ID

Sampled Date

Grouping Analyte

Sampled Time


L2121514 CONTD....

2PAGE of

* Please refer to the Reference Information section for an explanation of any qualifiers detected.

Version: FINAL

3

WATER

water29-JUN-18

MECH ROOM 1

L2121514-1

10:30

Hardness (as CaCO3) (mg/L)

Aluminum (Al)-Total (mg/L)

Antimony (Sb)-Total (mg/L)

Arsenic (As)-Total (mg/L)

Barium (Ba)-Total (mg/L)

Boron (B)-Total (mg/L)

Cadmium (Cd)-Total (mg/L)

Calcium (Ca)-Total (mg/L)

Chromium (Cr)-Total (mg/L)

Copper (Cu)-Total (mg/L)

Iron (Fe)-Total (mg/L)

Lead (Pb)-Total (mg/L)

Magnesium (Mg)-Total (mg/L)

Manganese (Mn)-Total (mg/L)

Mercury (Hg)-Total (mg/L)

Potassium (K)-Total (mg/L)

Selenium (Se)-Total (mg/L)

Sodium (Na)-Total (mg/L)

Uranium (U)-Total (mg/L)

Zinc (Zn)-Total (mg/L)

136

<0.010

<0.00050

0.00465

0.039

<0.10

<0.00020

25.3

<0.0020

0.0056

<0.030

<0.00050

17.7

0.0036

<0.00020

1.80

<0.0010

7.9

0.00219

<0.050

Physical Tests

Total Metals

HTC

Reference Information

HTC Hardness was calculated from Total Ca and/or Mg concentrations and may be biased high (dissolved Ca/Mg results unavailable).

Qualifiers for Individual Parameters Listed:

Description Qualifier

06-JUL-18 09:51 (MT)

L2121514 CONTD....

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HARDNESS-CALC-VA

HG-TOT-CVAFS-VA

MET-T-CCMS-VA

Hardness

Total Hg in Water by CVAFS LOR=50ppt

Total Metals in Water by CRC ICPMS

Hardness (also known as Total Hardness) is calculated from the sum of Calcium and Magnesium concentrations, expressed in CaCO3 equivalents. Dissolved Calcium and Magnesium concentrations are preferentially used for the hardness calculation.

This analysis is carried out using procedures adapted from "Standard Methods for the Examination of Water and Wastewater" published by the American Public Health Association, and with procedures adapted from "Test Methods for Evaluating Solid Waste" SW-846 published by the United States Environmental Protection Agency (EPA). The procedure involves a cold-oxidation of the acidified sample using bromine monochloride prior to reduction of the sample with stannous chloride. Instrumental analysis is by cold vapour atomic fluorescence spectrophotometry or atomic absorption spectrophotometry (EPA Method 245.7).

Water samples are digested with nitric and hydrochloric acids, and analyzed by CRC ICPMS.

Method Limitation (re: Sulfur): Sulfide and volatile sulfur species may not be recovered by this method.

ALS Test Code Test Description

Water

Water

Water

APHA 2340B

EPA 1631E (mod)

EPA 200.2/6020A (mod)

Method Reference**

** ALS test methods may incorporate modifications from specified reference methods to improve performance.

Matrix

The last two letters of the above test code(s) indicate the laboratory that performed analytical analysis for that test. Refer to the list below:

Laboratory Definition Code Laboratory Location

VA ALS ENVIRONMENTAL - VANCOUVER, BRITISH COLUMBIA, CANADA

GLOSSARY OF REPORT TERMSSurrogate - A compound that is similar in behaviour to target analyte(s), but that does not occur naturally in environmental samples. Forapplicable tests, surrogates are added to samples prior to analysis as a check on recovery.mg/kg - milligrams per kilogram based on dry weight of sample.mg/kg wwt - milligrams per kilogram based on wet weight of sample.mg/kg lwt - milligrams per kilogram based on lipid-adjusted weight of sample.mg/L - milligrams per litre.< - Less than.D.L. - The reported Detection Limit, also known as the Limit of Reporting (LOR).N/A - Result not available. Refer to qualifier code and definition for explanation.

Test results reported relate only to the samples as received by the laboratory.UNLESS OTHERWISE STATED, ALL SAMPLES WERE RECEIVED IN ACCEPTABLE CONDITION.Analytical results in unsigned test reports with the DRAFT watermark are subject to change, pending final QC review.

Test Method References:

Chain of Custody Numbers:

17-653392

Version: FINAL

3

certificate of analysis · 2019-12-31 · states environmental protection agency (epa). the...

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