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    This article was downloaded by: [Glaucia Souza]On: 08 May 2015, At: 11:17Publisher: Taylor & FrancisInforma Ltd Registered in England and Wales Registered Number: 1072954 Registered office: Mortimer House37-41 Mortimer Street, London W1T 3JH, UK

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    Drying Technology: An International JournalPublication details, including instructions for authors and subscription information:http://www.tandfonline.com/loi/ldrt20

    Soybean (Glycine max L. Merrill) Seed Drying in FixedBed: Process Heterogeneity and Seed QualityGlaucia F. M. V. Souza

    a, Ricardo F. Miranda

    b & Marcos A. S. Barrozo

    a

    a Chemical Engineering School, Federal University of Uberlândia

    b Mechanical Engineering School, Federal University of Uberlândia

    Accepted author version posted online: 08 May 2015.

    To cite this article: Glaucia F. M. V. Souza, Ricardo F. Miranda & Marcos A. S. Barrozo (2015): Soybean (Glycine max L.Merrill) Seed Drying in Fixed Bed: Process Heterogeneity and Seed Quality, Drying Technology: An International Journal, DO10.1080/07373937.2015.1039542

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    1

    Soybean (Glycine max  L. Merrill) Seed Drying in Fixed Bed: Process Heterogeneity

    and Seed Quality

    Glaucia F. M. V. Souza1, Ricardo F. Miranda2, Marcos A. S. Barrozo1

    1

    Chemical Engineering School, Federal University of Uberlândia,

    2

    MechanicalEngineering School, Federal University of Uberlândia

    Author to whom any correspondence should be addressed: Av. João Naves de Ávila,2121 – Santa Mônica, Uberlândia, MG –  38400-902, Brazil. E-mail:

    [email protected]

    Abstract 

    Soybean (Glycine max (L.) Merr.) is the most important oilseed in the world market.

    Seed quality has direct influences on the success of the crop and contributes significantly

    to productivity levels. The quality of soybean seeds can be influenced by several factors

    during drying. This study evaluated the drying of soybean seeds in a fixed bed dryer,

    considering the heterogeneity of the process and the effect of process variables on seed

    quality. Seed and air temperatures, seed moisture and seed quality were measured

    through the bed. Empirical equations were obtained relating seed quality indicators, at

    several bed axial positions, as a function of process variables.

    KEYWORDS: Glicine max L. Merril , heterogeneity of process, seed quality.

    INTRODUCTION

    High quality soybean seed production is a challenge for the agricultural sector,

    especially when tropical and subtropical regions are considered. In these regions, special

     production techniques must be used. [1] Soybean seed production also depends on

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    availability of adequate facilities at harvest and processing, such as the adequate

    conditions for seed drying. [2] 

    Seed quality is defined as a measure of characters or attributes that will determine

    the performance of seeds when sown or stored. [3]  It is a multiple concept encompassing

    genetic quality, seed health, physical aspects, viability and vigour. [4] The physical

    aspects are related to mechanical damages and fissures in the tegument. Viability refers to

    the ability of a seed to germinate and produce a normal seedling. Seed vigour is the sum

    total of those properties of the seed which determine the level of activity and performanceof the seed during germination and seedling emergence. The literature contains many

    reports about changes in soybean seed quality during drying. [5-7] These studies have

    shown that caution must be taken in any system that involves the movement of seeds,

    which can lead to mechanical damage. Due to this caution, some authors [8-9] 

    recommended the use of the fixed bed dryers. In this type of dryer, the drying air is

    forced through the interstitial space of seed mass, while the particles in the bed remain

    static.

    Artificial drying of soybean seeds involves a series of peculiarities. [10-13]  In the

    rainy season, or anticipating harvest, when seeds are harvested with about 22% moisture,

    immediate drying is mandatory. Considering such high percentage for safe storage

    without physiological quality losses, seeds should be dried down to 13%-14% (db). Seed

    viability can be considerably reduced by inadequate drying or by delayed drying. [14-15] 

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    An important problem in drying soybean seeds at high temperatures is seed coat splitting.

    [16] This condition turns the beans susceptible to microbial attack in storage, and also

    reduces germination potential. Low seed moisture,

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    MATERIALS AND METHODS

    Materials

    Commercial seeds of cultivar BRS Valiosa, genetically modified, with average Sauter's

    diameter d  p=6x10-3

    m, density ρ=1.19x103 kg.m-3, and bed porosity ε = 0.37 were used

    for the experimental procedures.

    Experimental Apparatus

    Figure 1 describes the experimental apparatus used in this study. The air system

    consisted of: 1) a radial blower (Kepler-Weber); 2) a gate valve to control flow; 3) anelectric heater; 4) voltage variator to adjust temperature of incoming air (SMUN

    Ximeng Electric); 5) a flow meter (TSI Incorporated; USA) ; 6) air humidifier to adjust

    incoming air humidity; 7) conical region for air distribution; 8) drying zone, measuring

    0.25m diameter and 0.6m height.

    Operating Conditions

    Experimental conditions were chosen based on a central compost design. [27] The

    experiments were done in two repetitions. Table 1 shows temperature (T  f ), surface

    velocity (V  f ) and relative humidity (RH) levels of drying air used in the experiments.

    Equation 1 presents the non dimensional (coded) form of the independent variables:

    40 0.7 35.0; ;

    5 0.3 10

     f f  T V RH   X X X 1 2 3   (1)

    Where T  f isoC, V  f   is m s

    -1, RH is %

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    Experimental Methodology

    Before the experiments were done, samples of seeds were collected to determine initial

    moisture (by the oven method at 105 ± 3°C for 24h) and for the measurement of seed

    quality indices before drying.

    After assembling the experimental apparatus and properly calibrating the measuring

    devices, the system was adjusted to the operating conditions previously established by the

    experimental design. Soybean seeds were placed in the fixed bed through the upper

    opening until reaching a thickness of 0.4m, when the trial time was started (time zero).

    Dry and wet bulb temperatures were obtained from copper-constantan thermocouples

    calibrated in a thermostatic water bath with a mercury thermometer with a precision of

    0.05 °C. The precision of the measurements for velocity and air relative humidity were ±

    0.05m s-1 and ± 4%, respectively.

    Seed samples were collected after 0.33, 0.66, 1.16, 1.83, 2.33 and 3.0 hours for

    determination of seed moisture. Seed and air temperatures were measured at 0.42, 0.92,

    1.42, 2.0, 2.66 and 3.0 hours, and after 3.0 hours. Sampling was done along the bed in

     positions: 0.05, 0.10, 0.20, 0.30 and 0.40 m, which are equivalent to dimensionless

     positions (h/L) of the bed of 0.125, 0.25, 0.50, 0.75 and 1.0, respectively. Where h is the

    axial position and L is the fixed bed height.

    Seed moisture was determined by the oven method at 105 ± 3°C for 24h. Seed samples

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    collected for temperature measurement were immediately placed in small thermally

    isolated containers, containing copper-constantan thermocouple. The initial moisture of

    the seeds was 20.0 ± 0.2 (% db).

    Evaluation Of Seed Quality

    Before starting the drying procedure in each experiment a sample of seeds was collected

    to determine initial seed physiological (germination test, accelerated aging test,

    emergence test in sand) and physical (sodium hypochlorite test - fissures) quality. After 3

    hours of each experiment, seed samples were collected along the seed bed, at the positions 0.05, 0.10, 0.20, 0.30 and 0.40m, equivalent to dimensionless positions (h/L) of

    the bed of 0.125, 0.25, 0.50, 0.75 and 1.0, respectively. These seeds samples were also

    submitted to analyzes of physiological and physical quality.

    Two hundred seeds were used for the germination test. The seeds were placed in

    germination paper and rolled, before placing them in germinators at 25ºC. Germination

     percentage was determined five days later, counting the number of normal seedlings,

    according to the International Seed Testing Association –  ISTA. [28] The accelerated

    aging test was done with 200 seeds, placed in gerboxes (0.11x0.11x0.03 m) and

    maintained for 48 hours at 41±0.5°C and 100% relative humidity. Subsequently, the

    germination test was done, according to ISTA. [28]  The emergence test in sand was done

    in sand beds using 200 seeds, sown at 0.02 m depth, and moisture was maintained by

     periodical watering. Ten days later, when no more seedling emergence was observed

    after two consecutive evaluations, the percentage of normal seedlings was determined

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    according to ISTA. [28] The sodium hypochlorite test was done with two replications of

    100 seeds, placed in containers and covered with 5% sodium hypochlorite solution. Ten

    minutes later, the number of seeds that were not imbibed was determined, and the results

    expressed as average percentage per sample. [29] 

    In order to determine the effect of drying process variables on seed quality, the values,

    obtained in each one of the tests, for each bed position, were divided by the respective

    values of initial quality (before drying), thus obtaining the indices of germination,

    accelerated aging, emergence in sand and the index of seeds without fissures.

    The individual effects and interactions of the variables T  f , V f and RH on seed quality

    indices were quantified. Prediction equations were obtained for each response studied

    (indices of germination, accelerated aging, emergence in sand, and seeds without

    fissures) at the different axial positions of the bed, by multiple regression.

    RESULTS AND DISCUSSION

    Drying Rate, Seed Moisture And Temperature, And Air Temperature Along The

    Bed

    Table 2 presents the drying rates of soybean seeds at the different axial positions

    of the bed for each experimental condition.

    A significant drop in seed drying rate is observed as it advances through the bed,

    indicating a heterogeneity of the drying potential in the different axial positions in all

    experiments. The differences between dimensionless positions 0.125 (near the bottom)

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    and 1.0 (top of bed) were about 0.30±0.05 percentage points per hour (pp h -1) for most

    experiments. The greatest differences, 0.80 and 0.49 pp h-1, were observed in low drying

    air velocity (0.27m s-1) and high air relative humidity (49.1%), respectively. The smallest

    difference between drying rates at the axial positions of the bed, 0.19 pp h -1, was obtained

    using the greatest drying air velocity (1.12 m s-1).

    Final soybean seed moisture (after drying) is shown in Table 3. As previously

    mentioned, final soybean seed moisture should be down to 13%-14% (db) to maintain

    seed quality during storage. It can be seen that, in most experiments, final seed moisturewere out of the desirable range for safe seed storage. Only three experiments (5, 7 and 13

    ) had seed with final moisture below 13 to 14% (db) at the different axial positions of the

     bed. Thus, these three experimental conditions are adequate to drying, however the seed

    quality should be also considered.

    Seed temperature and air temperature measured at the different positions of the fixed bed

     became stable in time, with a significant difference along the axial positions of the bed, in

    greater or smaller scale depending on the operating conditions. Higher heterogeneities

    were obtained with lower drying air velocities. Figure 2 makes clear the significant effect

    of air velocity on the product heterogeneity along the bed. At 0.27 m s -1, the air reached

    temperatures between 31 and 38°C and the seed between 30 and 36°C (Figure 2A); in

    contrast, at 1.12 m s-1, air temperature was between 37 and 39°C while seeds were

     between 36 and 37°C (Figure 2B).

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    High differences in seed temperature can lead to a final product with different

    levels of quality as well. Therefore, seed quality after drying should also be considered in

    order to define the best combination of the variables in the drying process

    Quality Of Soybean Seeds

    The experimental data on seed quality (indices of germination, vigor, emergence in sand,

    and seeds without fissures) obtained along the drying bed for each experiment, were

    adjusted in prediction equations for each quality indicator, as a function of drying

    variables, using the response surface technique. The fitted equations are represented inthe form.[30]

    ^

    ~~ ~ ~ ~o

     y b x b x B x  

    Where: b0: linear coefficient;~~

    'b x : first order effects;~

    b : parameter linked to isolated

    variables;~~

    '   x B x : quadratic contribution; B: parameters linked quadratic variables and

    interactions;~

     x : coded variables.

    In this paper we present some equations to represent the behavior of seed quality indices

    at two different axial positions (near the bottom and top of bed). The parameters with p-

    level greater than 10% (error probability of the statistical test) were disregarded, and the

    respective variables were considered irrelevant. [27]

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    The empirical equations for predicting the germination index (GI) of soybean seeds for

     bed axial positions (dimensionless) 0.125 (near the bottom) and 1.0 (top of bed) as a

    function of drying variables are the follows:

    0.125~ ~ ~

    0.043 0.026 0 0

    GI 0.981 x ' 0 x' 0 0 0 x

    0 0 0 0

      (2)

    1.0~ ~ ~

    0.038 0.025 0 0

    GI 0.987 x ' 0 x' 0 0 0 x

    0 0 0 0

      (3)

    The quadratic correlation coefficients indicate that 80 and 85% of experimental data

    variability of germination index (GI) can be explained by the equations 2 and 3,

    respectively. Temperature was the variable that most affected the germination index of

    soybean seeds. From these equations is possible to quantify the importance of this drying

    variable in reducing the germination indices of soybean seeds at these axial positions.

    Figure 3 depicts response surfaces for predicting of germination index (GI) of soybean

    seeds at dimensionless axial positions 0.125 (A) and 1.0 (B), according to the models

     previously presented, as function of non-dimensional values of temperature (X1) and

    relative humidity (X3) of drying air.

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    These surfaces (Figure 3) also demonstrate the great sensitivity of seed germination to

    drying temperature (X1) variation, which was also observed at the other axial positions.

    The best results, i.e., and the least damage to seed quality were obtained at the lowest

    drying air temperatures (X1 = − 1.41 or T f  = 32.9°C). High temperature can cause greater

    latent effect than the immediate one, which will appear in storage. [31] After a period of

    storage, the thermal damages can lead to the seed germination suffer even greater

    reductions. [20]

    Drying temperature was also the variable that most affected soybean seed vigor in theaccelerated aging index. The empirical equations for predicting soybean seed accelerated

    aging (AAI) at the dimensionless axial positions 0.125 (near the bottom) and 1.0 (top of

     bed) are:

    0.125~ ~ ~

    0.049 0, 032 0 0

    AAI 0.973 x ' 0 x' 0 0 0 x0 0 0 0, 027

      (4)

    1.0~ ~ ~

    0.046 0.034 0 0

    AAI 0.977 x ' 0 x' 0 0 0 x

    0 0 0 0

      (5)

    Figure 4 depicts the surface responses for predicting the accelerated aging index (AAI) of

    soybean seeds at bed axial positions (dimensionless) 0.125 (A) and 1.0 (B) as function of

    non-dimensional values of temperature (X1) and relative humidity (X3).

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    The best condition occurs with a lower level of drying temperature (X1 

    = − 1.05), around 35°C, and intermediate level of air relative humidity (X3 = 0), about

    35%. Germination and vigor decrease is associated with the overdrying as well as the

    underdrying. [7] Overdrying may cause invisible damage to the living cells of the seed

    and destroy its viability. [32] Underdried seeds lose viability due to mold activity.

    However, due to the drying conditions used in this study, the decreasing in germination

    and vigor are expected to be mostly due the overdrying (conditions with high air

    temperature and low air humidity values), as seen in the Figures 3 and 4.

    It also can be observed in Figure 4 results, the difference between the accelerated aging

    index at these two axial positions (h/L=0.125 and 1.0), thus indicating a heterogeneous

     profile along the bed, also for seed quality.

    All drying variables, somehow, affected soybean seed emergence in sand index at the

    first layers of the fixed bed (h/l=0.125 and 0.25). Drying temperature and air velocity

    were the variables that significantly affected this quality indicator at dimensionless

     positions 0.5 and 1.0. Such difference could be due to the greater sensitivity of the first

    layers of the fixed bed to the variables of the process, since the air is hotter and dryer at

    those positions.

    The empirical equations for predicting soybean seed emergence in sand index (ESI) at

    axial positions 0.125 and 1.0 are:

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    0.125~ ~ ~

    0.062 0.039 0 0

    ESI 0.996 x ' 0 x' 0 0.016 0 x

    0.014 0 0 0.012

      (6)

    1.0~ ~ ~

    0.064 0.042 0 0

    ESI 0.987 x ' 0 x' 0 0.013 0 x

    0 0 0 0

      (7)

    These equations, respectively, explain 94 and 96% of the variability of experimental data

    of seed emergence in sand index .

    Figure 5 depicts response surfaces for predicting soybean seed emergence in sand index

    (ESI) at the dimensionless (h/L) axial positions 0.125 and 1.0, as function of the variables

    studied. Once again, temperature was the variable that most affected seed quality in the

    sand emergence test. In general, optimum condition occurred with values near the lowest

    levels of drying air temperature, around 35°C (X1 = –  1.05)

    The quality index that was most affected by all variables simultaneously was the index of

    seeds without fissures. Empirical equations for predicting the index of seeds without

    fissures (ISWF) at the axial positions (dimensionless) 0.125 and 1.0 are:

    0.125~ ~ ~

    0.025 0 0 0.017

    ISWF 0.971 x ' 0 x' 0 0 0.013 x

    0.066 0.017 0.013 0.038

      (8)

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    1.0~ ~ ~

    0.020 0 0.012 0.016

    ISWF 0.992 x ' 0.018 x' 0.012 0 0.016 x

    0.038 0.016 0.016 0.029

      (9)

    Equations 8 to 9 explain, respectively, 85 and 83% of ISWF data variability. Figure 6

     presents surface responses for the prediction of soybean seed index of seeds without

    fissures (ISWF) at the these axial positions (h/L=0.125 and 1.0) as function of non-

    dimensional values of drying air temperature (X1), relative humidity (X3) with constant

    air velocity at the central point of the experimental design (X2= 0).

    The lower levels of ISWF (seed with low physical quality) are obtained in the first layer

    of the fixed bed, when the temperature is high and the relative humidity is low

    (conditions that lead to a high drying rate) . It is also important to highlight that the effect

    of the drying variables on this quality index, especially temperature, decreases as the

    distance of drying air intake increases, thus, showing heterogeneous behavior of the fixed

     bed in deep layer.

    As observed in Figure 6, the increase in seed coat cracking is associated with conditions

    that lead to a high drying rate, with the corresponding high shrinkage rate, [14] and high

    mechanical damages. Differential shrinkage of seed coat and cotyledons occurs during

    drying. When the drying rate is increased, the seed coat at the surface of the soybean

    tends to shrink faster than the cotyledons causing the cracks. [13] According to TeKrony

    et al. [33]  problems of seed coat cracking can occur when drying air relative humidity is

     below 35 to 40%.

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    Besides the qualitative behavior observed on the surface responses presented in this

    study, the proposed equations allow the quantification of the effects of the drying

    variables in fixed bed on the physiological and physical quality of the seeds.

    CONCLUSIONS

    The methodology developed was adequate to study the heterogeneity of the drying

     process along the bed and to analyze the grouped effect of air temperature, relative

    humidity and air velocity on the final seed quality of soybean dried in a fixed bed dryer.

    Significant differences were observed for moisture, air temperature and seeds in axialdirection of the bed.

    The used statistical technique allowed to obtain empirical correlations for the quality

    indices of soybean seeds as a function of the variables analyzed. These equations can be

    used to predict the drying conditions at which the quality indices of soybean seeds are

    commercially acceptable. The best germination and vigor indices are attained at low

    values of air temperature (lower than 35oC) coupled with a high air relative humidity

    (higher than 35%). In addition, high air relative humidity (higher than 35%) and low seed

    temperatures assure better seed physical quality, expressed by the high index of non-

    fissured seeds. In general, the decrease in seed quality is associated with conditions that

    lead to high drying rate and corresponding overdrying conditions.

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    AKNOWLEDGEMENTS

    The authors are grateful to the State of Minas Gerais Research Support

    Foundation (FAPEMIG) and National Council for Scientific and Technological

    Development (CNPq) for their financial support.

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    http://lattes.cnpq.br/8216573686887098http://lattes.cnpq.br/4131011903682955http://lattes.cnpq.br/8399881058983357http://lattes.cnpq.br/1095833148260006http://lattes.cnpq.br/8352510852477951http://lattes.cnpq.br/3138002365101425http://lattes.cnpq.br/1181660568548980http://onlinelibrary.wiley.com/doi/10.1046/j.1365-2621.2001.00470.x/abstracthttp://onlinelibrary.wiley.com/doi/10.1046/j.1365-2621.2001.00470.x/abstracthttp://onlinelibrary.wiley.com/doi/10.1046/j.1365-2621.2001.00470.x/abstracthttp://onlinelibrary.wiley.com/doi/10.1046/j.1365-2621.2001.00470.x/abstracthttp://onlinelibrary.wiley.com/doi/10.1046/j.1365-2621.2001.00470.x/abstracthttp://lattes.cnpq.br/1181660568548980http://lattes.cnpq.br/3138002365101425http://lattes.cnpq.br/8352510852477951http://lattes.cnpq.br/1095833148260006http://lattes.cnpq.br/8399881058983357http://lattes.cnpq.br/4131011903682955http://lattes.cnpq.br/8216573686887098

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    11. Barrozo, M.A.S.; Sartori, D.J.M.; Freire, J.T.; Achcar, J.A. Discrimination of

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    Technology 1996, 14 (7), 1779-1794.

    12. Barrozo, M.A.S.; Henrique, H.M.; Sartori, D.J.M.; Freire, J.T. The use of the

    orthogonal collocation method on the study of the drying kinetics of soybean seeds.

     Journal of Stored Products Research 2006, 42, 348-356.

    13. Mensah, J.K.; Nelson, G.L.; Hamdy, M.Y.; Richard, T.G. A mathematical model for

     predicting soybean seedcoat cracking during drying. Transactions of the ASAE 1985, 28 

    (2), 580-591.

    14. Parde, S.R.; Kausal, R.T.; Jayas, D.S.; White, N.D.G. Mechanical damage to soybean

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    http://lattes.cnpq.br/8937961078558996http://lattes.cnpq.br/5985643393743399http://lattes.cnpq.br/2270677706718167http://lattes.cnpq.br/2270677706718167http://lattes.cnpq.br/5985643393743399http://lattes.cnpq.br/8937961078558996

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    15. Barrozo, M.A.S.; Mujundar, A.; Freire, J.T. Air-Drying of Seeds: A Review.  Drying

    Technology  2014, 32, 1127-1141.

    16. Barrozo, M.A.S.; Murata, V.V.; Assis, A.J.; Freire, J.T. Modeling of Drying in

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    17. Pfeifer, A.A.; Murata, V.V.; Barrozo, M.A.S. Modelling of soybean seed drying in

    concurrent sliding bed dryers: Effect of the number of stages on the seed quality and

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    18. Ghaly, T.F.; Sutherland, J.W. Quality aspects of heated-air drying of soybeans.

     Journal of Stored Products Research 1983, 19 (1), 31-41.19. Barrozo, M.A.S.; Murata, V.V.; Costa, S.M. The drying of soybean seeds in

    countercurrent and concurrent moving bed dryers. Drying Technology 1998, 16 , 2033-

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    20. Felipe, C.A.S.; Barrozo, M.A.S. Drying of soybean seeds in a concurrent moving bed:

    heat and mass transfer and quality analysis. Drying Technology 2003, 21 (3), 439-456.

    21. Arruda, E.B.; Lobato, F.S.; Assis, A.J.; Barrozo, M.A.S. Modeling of fertilizer drying

    in roto-aerated and conventional rotary dryers. Drying Technology 2009, 27 , 1192-1198.

    22. Vieira Neto, J.L.; Duarte, C.R.; Murata, V.V.; Barrozo, M.A.S. Effect of a draft tube

    on the fluid dynamics of a spouted bed: Experimental and CFD Studies.  Drying

    Technology 2008, 26 , 299-307

    23. Mujumdar, A.S.; Law, C.L. Drying Technology: Trends and applications in

     postharvest processing. Food and Bioprocess Technology 2010, 3, 843-852.

    http://lattes.cnpq.br/1095833148260006http://lattes.cnpq.br/1526946408801828http://lattes.cnpq.br/2270677706718167http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://lattes.cnpq.br/5969496186215144http://lattes.cnpq.br/7640108116459444http://lattes.cnpq.br/1526946408801828http://lattes.cnpq.br/4074369473895050http://lattes.cnpq.br/8399881058983357http://lattes.cnpq.br/1095833148260006http://lattes.cnpq.br/1095833148260006http://lattes.cnpq.br/8399881058983357http://lattes.cnpq.br/4074369473895050http://lattes.cnpq.br/1526946408801828http://lattes.cnpq.br/7640108116459444http://lattes.cnpq.br/5969496186215144http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://www.scopus.com/record/display.url?eid=2-s2.0-78249263204&origin=reflist&sort=plf-f&refeid=2-s2.0-78249263204&src=s&imp=t&sid=351FFACBD5EAB6C89EBC277E1F8156D7.f594dyPDCy4K3aQHRor6A%3a150&sot=ctocbw&sdt=a&sl=37&s=PUBYEAR+AFT+2010+AND+PUBYEAR+BEF+2014http://lattes.cnpq.br/2270677706718167http://lattes.cnpq.br/1526946408801828http://lattes.cnpq.br/1095833148260006

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    24. Santos, K.G.; Santos, D.A.; Duarte, C. R.; Murata, V.V.; Barrozo, M.A.S. Spouting

    of Bidisperse Mixture of Particles: A CFD and Experimental Study. Drying Technology 

    2012, 30, 1354-1367

    25. Arruda, E.B.; Façanha, J.M.F.; Pires, L.N.; Assis, A.J.; Barrozo, M.A.S.

    Conventional and modified rotary dryer: Comparison of performance in fertilizer drying.

    Chemical Engineering and Processing 2009, 48, 1414-1418.

    26. Ratti, C., Crapiste, G.H. Modeling of batch dryers for shrinkable biological materials.

     Food and Bioprocess Technology 2009, 2, 248-256.

    27. Box, M.J.; Hunter, W.G.; Hunter, J.S. Statistics for experimenters: an introduction todesign, data analysis and model building. New York: John Wiley and Sons, 1978.

    28. International Seed Testing Association (ISTA). International Rules For Seed Testing.

    Seed Science and Technology 1985, 13, 299-355.

    29. Vaughan, C.E. The chlorox test (soybean). Quality assurance technique. In: Short

    Course for Seedsmen, Proccedings [S.l.] (pp.117-118). Mississippi State University: Seed

    Technology Laboratory, 1982.

    30. Myers, R.H.; Montgomery, D.C. Response Surface Methodology: Process and

     Product Optimization Using Designed Experiments. New York: John Wiley and Sons,

    Inc, 2002.

    31. Pollock, B.M.; Ross, E.E. Seed and seedling vigour in seed biology. New York:

    Academic Press, 1972.

    32. Nellist, M. E.; Hughes, M. Physical and biological processes in the drying of seeds.

    Seed Science and Technology 1973, 1, 613-643.

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    33. TeKrony, D.M.; Egli, D.B.; White, G.M. Seed production and technology. In:

    Wilcox, J.R. (2.ed), Soybeans: improvement, production and uses. Madison:

    ASA/CSSA/SSSA, 1987.

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    Table 1. Levels of operating conditions

    Levels Variables

     x T f  (°C) V f (m/s) RH  (%)

     –  α = – 1.41 32.9 0.27 20.8

     –  1 35.0 0.4 25.0

    0 40.0 0.7 35.0

    + 1 45.0 1.0 45.0

    + α = 1.41  47.0 1.12 49.1

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    Table 2.  –  Drying rates in percentage points per hour at the different axial positions (at

    the end of drying).

    Experiments (T f  -V f  -RH)

    Drying rate (pp h-

    ) Bed axial position, h/L (-)

    0.125 0.25 0.50 0.75 1.0

    1 35°C –  0.4m s-  - 25% 2.06 1.97 1.92 1.86 1.75

    2 35°C - 0.4m s-  - 45% 1.55 1.44 1.33 1.32 1.17

    3 35°C - 1.0m s-  - 25% 2.16 2.12 1.98 1.96 1.84

    4 35°C - 1.0m s-  - 45% 1.73 1.65 1.50 1.48 1.37

    5 45°C - 0.4m s-

     - 25% 2.30 2.25 2.17 2.07 2.00

    6 45°C - 0.4m s-  - 45% 1.93 1.90 1.77 1.72 1.68

    7 45°C - 1.0m s-  - 25% 2.39 2.31 2.22 2.14 2.06

    8 45°C - 1.0m s-  - 40% 2.10 2.07 2.00 1.92 1.86

    9 32.9°C - 0.7m s-  - 35% 1.83 1.76 1.68 1.59 1.50

    10 47°C - 0.7m s-  - 35% 2.31 2.28 2.13 2.11 2.01

    11 40°C - 0.27m s-  - 35% 2.10 2.02 1.73 1.66 1.30

    12 40°C - 1.12m s-  - 35% 2.13 2.09 2.07 2.02 1.94

    13 40°C - 0.7m s-  - 20.8% 2.35 2.23 2.19 2.16 2.06

    14 40°C - 0.7m s-  - 49.1% 1.64 1.52 1.41 1.35 1.15

    15 40°C - 0.7m s-  - 35% 1.84 1.77 1.70 1.63 1.57

    16 40°C - 0.7m s-  - 35% 1.85 1.79 1.73 1.66 1.59

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    Table 3.  –  Final moisture of soybean seed at the axial positions of fixed bed (at the end

    of drying).

    Experiments (T f  -V f  -RH) Final moisture (% db) at bed axial position, h/L

    (-)

    0.125 0.25 0.50 0.75 1.0

    1 35°C - 0.4m s-  - 25% 14.2 14.5 14.6 14.8 15.2

    2 35°C - 0.4m s-  - 45% 15.1 15.5 15.8 15.8 16.3

    3 35°C - 1.0m s-  - 25% 13.9 14.0 14.4 14.5 14.9

    4 35°C - 1.0m s-

     - 45% 15.3 15.5 16.0 16.1 16.4

    5 45°C - 0.4m s-  - 25% 13.1 13.3 13.5 13.8 14.0

    6 45°C - 0.4m s-  - 45% 14.1 14.2 14.6 14.7 14.9

    7 45°C - 1.0m s-  - 25% 12.6 12.9 13.1 13.4 13.6

    8 45°C - 1.0m s-  - 40% 13.7 13.8 14.0 14.3 14.4

    9 32.9°C - 0.7m s-  - 35% 14.4 14.6 14.8 15.1 15.3

    10 47°C - 0.7m s-  - 35% 13.7 13.8 14.2 14.3 14.6

    11 40°C - 0.27m s-  - 35% 14.8 15.0 15.9 16.1 17.2

    12 40°C - 1.12m s-  - 35% 14.5 14.6 14.7 14.8 15.1

    13 40°C - 0.7m s-  - 20.8% 13.0 13.4 13.5 13.6 13.9

    14 40°C - 0.7m s-  - 49.1% 15.3 15.6 16.0 16.1 16.7

    15 40°C - 0.7m s-  - 35% 13.7 13.9 14.1 14.3 14.5

    16 40°C - 0.7m s-  - 35% 13.7 13.8 13.9 13.9 14.2

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    Figure 1. Experimental apparatus.

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    Figure 2. Profiles of drying air and seeds temperatures over time at different axial

     positions (h/L) with air velocity of 0.27 m/s (A) and 1.12 m/s (B); with inlet air

    temperature of 40 ° C and relative humidity of 35%.

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    Figure 3. Response surfaces for predicting soybean seed germination index (GI) at the

     bed axial positions (h/L) of 0.125 (A) and 1.0 (B) as a function of T  f  and RH.

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    Figure 4. Response surfaces for predicting soybean accelerated aging index (AAI) at the

    axial positions (h/L) of 0.125 (A) and 1.0 m (B) as a function of T  f  and RH.

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    Figure 5. Response surfaces for predicting soybean emergence in sand index (ESI) at the

    dimensionless axial position of 0.125 (A) as a function of RH   and V  f , and 1.0 (B) as a

    function of T  f   and V  f .

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    Figure 6. Response surfaces for predicting soybean index seeds with no fissures (ISWF)

    at the dimensionless axial position of 0.125 (A) and 1.0 (B) as function of T  f   and RH.