appendix h - der.wa.gov.au · table 2 sample sample identification date number assessment criteria...

$: APPENDIX H - der.wa.gov.au · Table 2 Sample Sample Identification Date Number Assessment Criteria Analytical Results Soil Anal_vtical Results: Acid Sulphate Soils g -c \!co$
APPENDIX H

Sample

Identification

Number

Sample

Date

f:cological Investigation Levels ElLs {mg!Kg)

Health Investigation Levels HIL·A (mg/kg)

Analytical Results

Table 1. Soil Analytical Results: Total Metals

Metals (m ikQ) Mercury Arsenic Cadmium Chromium Copper

20 3 400 100

15 100 20 210 1000

Lead Nickel

600 60

300 600

SBOI-1 00 17/2/2010 <0_1 ,, <1 <2 - _ __ , _ __c<__ ,, -"'"5-+- ,, 5801-4.00 17/2/2010 �-' <5 8 , , --- ------� -- -. --1---'' ,_, -S802-t.so --�!'3!2_�-�-� -I-- �'�O>c -�' --4--·•:os_ _ <:__________ _____ 6 -l--�7 -"'·---�---

1-----�-�9��::_�5 __ ___ 1712/2010 <0.1 <5 <1 10 16 20 SB03-1 25 _ _ _ __ ;_��!3� 0c 1'0-f _ _:'0,.::1_ _

<5 <1 11 9 16 -----�-!?_��-��__?'-�--- 171212010 <0.1 <5'--1---'0''--� - ---- -�--------- <5 7

4 3 7 5 •2

Zinc

200

7000

,, ,, <5

SBOS-1.50 1712/2010 <0.1 <5 <1 10 7 11 3 <5 . -- ------ +--""'--'----1-- - - - ��"'-1-- . -- .. ----��-!�-�--- +"1�

71 �21�2, 01�0'-1 <0_1 _____ ________ ::�--+-�-�'--+- 10 5 10 2 <5 ---��!:�� '!'-?!':�_,_g_ <0 1 <5 <1 <='---11-�-<5 -----��------ -�'''---1 ------::�----

SBOS-1 5-�---�- __ 1__?'1212010 <0_1 _______ _::�----1--_:'c' _ _ , ___ 18

----· _____ • '''----1---'8'----l-- __ ----�------j--'::''--1 SBQA 1 17/2/2010 J--�'::0c.1c__J---- <5 <1 ---l--�'2:_ __ _ ____ -------�?---� __ _ <5 <2 ____ ::_�-----��----- 171212010 <0 1 �'C''___j'___:'"-1 -------�------L_C':"5 _ _j'__ 7 ____ - - --- - ----��- <5

Table 2- Soil Analvtical R 'd s esults: Act ulohate Soils Actual Aciditv Potential Aciditv Acid Base AccountinQ

Sample Sample " ldentlfication Date il �

Number � " -% 2 • filz-.I �" rou..'l:' x"' -'2'0 2 �-" >-�"

Assessment Criteria

Analytical Results

��--"'<>Bo_01·0_5o 17/2/2010 c<u0c:>.1-!-' 8801-1.00 171212010 _____ ____ ::0_0_��1--{_:''-''

1----''"'""-o�_:_�-�qg ___ --l---'""121.�g__1_9_ _ _ ___ _ 5.1 ?_?_ __ 1---'"'""'0_1_��<?-�-- -· � -+---''"7/2�?-Q!�---- - -- ---_§_1_ 17

$801-3.50 �-+--'1'-'''"21_?_Q_1,�--- ---- 'C5-'-2 -!�" SB01-4 50 1712/2010 5.0>_j__>31 S801 5 25 171212010 4.9-11-4'>'5 $801·6.00 17/212010 4.9 --l---"'"-'--

1---�S�B,ot-7 _ 00 --1--- -'17 ,, l?l_?g_:l_q___ 4 _g }_5 ____ _ 1----"'"'""01 · 8.00 -l--''"7'?!3g_�Q_______ ·�'"· '-1--_}§____ __ _ __<_S�B,02-075 17/2/2010 5c>o.6'-J-- 4 ---"'"'"""02-1.5·�0---l--1"7"/2�2.Q!�----- - "5."_0 -1-_?_9'

$802-2.00 -�---"17'-'/2/2010 5>c·1'--+-- "' ��--'S,oB.o-02':"3.00 171212010 5 3 26 t- ____ ?_�Q3:_4__ O_{} 1713!��!?-. _ 5.3 17

----�-�9_2_�2_.92_ -- - - - - -�-�-��/20 � _Q_- - - ----l---'-5.;>0 __ 1"' __ _?_4 _____ _ ____ __ --�-�_o__?_�--I� . __ --�!:1-��9.!?_ ----· _ -!--''"'"---- _ ___ :!9 _ _

_ _ §_�2��5 __ L _ __ _ !!.!��{}!_� s.2

__ ?!3_{}?:! _ _?_5 _ __ 1_ 17/2/2010 5.1 20 21

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____ Q_._o_�---- ______ , _o. _oo�5---+-�<,,�o,_ o.o�---- ____ J�- ____ l_ _ _ _ Q&?__ _ _ ____ ,o _o _o5 __ 1--__<_<�10'--�- _Q,Q_L __ _____ i�------ ____ _i_

- _ __ Qo._Q_@_ _____ -- _•_0 _00_5 __ -l--�<�10'---i-0.10 60 - - - - �� 0 06 <0.005 <10 ______ Q_,Q_�----- . -- - __ 3_7_____ 3 o.os,_+-�<�O�.o�o�5-I-- __-<!_Q:__ o_os <0.02 <0.005 <10 <0,02 ------ ---- ----0 04 <0.005 <10 0.05 0.04 <0.005 <10 0.04

____ _Q __ Q� .. J--__<_'0�-�00�5>_+-_-<�1�0-j 0 04 o -�03'---J--�<Q�O_QL_ __ _____ __:_1�L-- -�9cQ.L __ o,,.o�''--+-�<o.oo5 _ ____ "'":'!_Q _____ ______ Q_ . .Q� _ _ 006"--+--'<Q,Q�--- -- __ <_1_Q_ - - 0.06 0.03 <Q_._9_9__2__ <10 ______ Q:_Q_L __ 0.03 <0 005 <10 0.03

38 3 ____ ":_I__Q_ - -- - -�- ''---j

29 2 28 2 27 2 19 1 24 2 40 3 20 2

-�2«'2_L__ 2

Table 2

Sample Sample Identification Date

Number

Assessment Criteria

Analytical Results

Soil Anal_vtical Results: Acid Sulphate Soils

g - c \!co Ir o3

Actual Aciditv

;;; 0 � ? -� . � �" 2 -., w rou--� -o E >-�-

� 2 "� ""'""' -f-_"Q(J) ' 0 . _\l::: -c ;g�i): Olt>;:R (!)<(�

Potential Acidltv

� '§ E "" " E .2 u • o-�in ..C�,;:;:-§;;>< o.-1::0+ E:: »GI 0 " -"' "'<!) '2-oO "� �" o • E 00 �"'-

Cont.) Acid Base Accountin!l

m m c -'"-u� �_g) -§ -� '6 c 0 X 0 X o ..,z� . " •z.- �<:r:(.) -�� z-:6� (}_ O>O '9. ·g t: u " ms u 0$ o_ c u "

<(u(l) "'u-P E2o -a>z� -zo '"' � .£' �-r:S Z<C� �·-

Table 3- Groundwater Analytical Results: Oissolved Metals

Sample

Identification

Number

Assessment Crlteria

Drinking Water

long Term \rrigahon

Freshvtaler

DoH (2006)

Sample

Date Units Metals

Arsenic Cadmium Chromium Copper Lead

0_007 ! 0.002 2.0 0_01

0.1 0_01 0.1 0.2 2.0

0.024 0.0002 1 0.0001 0_0014 0.0034

0_07 0.02 20 0 1

Nickel Zinc

0.02 3 0

0.2 2.0

0.011 0_008

0 2 30

M801 171212010 mg/L <0.001 0.0002 <0_001 0.008 0_001 0.009 0.143

MB02 171212010 mg/L

M803

QA1

Table 3- Grotmdwatcr Analytical Re.<iults: Dissolved Metals (cont.)

Sample

ldentlficati 0"

Number

Sample

Date

Assessment Criteria

Drinking Water

Long Term Irrigation

Freshwater

DoH (2006)

MB01 1712/2010

M802 171212010

Units

mgll

mgll

-�3 = ��;��r�� ------ __ ______________ _!,_ _______ __

Metals

Aluminium Manganese Iron

0.2 0 3

5.0 0 2

0.055 300

2 3

0.09 0.114

<0.05

0 71

1.44

Selenium

0 1

0_02

0.00005

<0.01

<0.01

<0.01

Mercury

0.001

0.002

0 00006

0 01

<0.0001 ·---·--

<0.0001

Table 4- Groundwater Analytical Result!i: Nitrates and Phosphorus

Sample Name

DOH Long MB01 MB02 MB03 QA1

Drinking Term Freshwater

{2006) Water Irrigation Sample Date

1712/2010 17/2/2010 1712/2010 17/212010

Ammonia asN 0.16 0.18 0.22 0.16

Nitrite as N 30 <0.01 om -<0.01 0.01 I- �------------- ----------- - - - -

Nitrate as N 500 10 31 0.07 0.06 0.03 0.05 ···- ----------------------- -·�-. "- ----· --------------

Nitrite + Nitrate as N 0.07 0.08 0.03 0.05 r- ·- -·-·�- -----r-�·-· Total Kjeldahl N as N 1.3 1 5 <1_0 1.5

·--------------- ·-···-·· ----------- - -----·· ·

T olal Nitrogen as N 1000 14 16 <1.0 1.6 c-----·-�- ------- ----------- ----------···

Reactive Phosphorus 0.05 0.89 0.17 -<0.10 0.96 ------------------ - ----------

APPENDIX I

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ALS Lal:loratono� Group ANAi..YTiCA.L CHEMISTRY & TESTING SERVICES

Environmental Division

CERTIFICATE OF ANALYSIS Work Onl�r neon\ Contact ,'\C)(�( US�

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. MS GINA PEMBERTON SHOP 1712 SOUTH WESTERN HIGHWAY ARMAOALE WA, AUSTRALIA 6112 [email protected] +61 08 9497 5000

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[email protected] +61-S-9209 7655 +61-8-9209 7600 NEPM 1999 Scheclule 8(3) anct ALS 0CS3 reqwement

18-FES-2011 28-FEB-2011

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ft11� r,;pDrt �cipBI'�(Odes <my prevl(lu�; 1<2\)0rt(s) w;th th1s rell-�rence. apply to lt\B ?S sc:bmitted. Alt pages o1 t01� 1eport haw: been (:ht:c�t:J <:�nd nppro�ed

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NATA AccreOl\e<l Lnbocmorr 825 Signatories

NATA This documer1! IS <ssued in accordarce w1th NAT/I

accreditation req�•remer>ts.

l h1s document has be>?n electro01Cally signr;>d by the au1Mnzed

C3rt red out m compliancB w,th procedur'''s speql:t:d in 21 CFR Part 11 signatories mctica\ed below_ E:ec\rorw; Slgrm\.) \<:�?> been

'>'1(0><,,\J ,1f,�<.HONL'>1() ACCI'lltDl'VATION

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ISO,'IEC 17025.

SJgn,J!onr;,�

Ciceha Bartels Lean11e Cooper

PV$;1/Cn

Metals instrument Chemist Acid Sulfa\e Seils Superv1scr

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General Comments 'it'� ""�ly(,cal pfcceduno�; �-'>Cd �'i �he E0wunmcn:ui ;),v,s:on Mvc DQ(;n d�·vclor><:J 1';crn c;swor,sned ln1Wr\1\(IOn�lil' ;·ocogmz'o'i pr\Jc.oduros �uch <;<;', \'1o�e �uCbhii.� 0 ::\<t '.iSEP/, i·f'M/'. ,1.s .C.0d C>Ef'�·1 h' r·o·��"

d<cvdt.P'o" p:oc,,ourm. "'"' on1p!oy�<; l:l HX· ah<Jt\C� ?f 0ac�mr.n\re:l �1e<ndacc)�. ;;,r !J'f client i\>qe>0SI.

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t.OR '· L.md Oj (•JPC�:ng " l'lii$1io>idt �� \:0�\f.'CI\W� !rom ltld<V\(b.:;! onQiyH; t!et'!CiiOfl�; :1\ Of .·lbOY\1 th(Ji0VGI (Jf I'Gf.'Gc·�<"�G

Liming rata is c;alculMad an 9 uso off•M agriculturalllme (CaCOl) and e<sing a safety factor of 1.5 to anow 1or non-homogeneous mixing and

poor reactMty of lime. For conversion of Uming Rato from 'llglt d<y weight' to 'kg/m3 ln·zltu zoll', multiply •reportod results' "'wet bulk den5lty of $Oil in tlm3'.

R:etained AcidOty not required because pH KCl gro�tcr than or equal to 4.5

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MS GINA PEMBERTON SHOP H/2 SOUTH VVESTERN HIGHWAY ARMADALE WA. AUSTRALIA6112

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Accredited for compbance w,th

iSOIIEC 17025.

Sign atones Tf1;s document h% been BlG<�tronically s.igned by the i!i.i\honzed Signatories <ndicatei'J below. nectror:ic 51911;.ng 11as beer1

c:ilrne<J oc:t :n comphance with procedutes specifte<l in 21 CFF:: P:il:t 1 -;.

$JgnW'XW$ Ctceha Bartels

Leanne Cooper

PoMron

Metals Instrument Chemist

Acid Sullate Sctls Supervisor

Ern•1<oo»n"'nt"'1 Oh.>OSI<>O P<trth Pwt oi lhe Al-'5 Labor "'torq Group

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Accred,!.>!,on C�iegory Perth lnorganics

Perth ASS

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Laboratory Duplicate (DUP) Report

-:"r-� (fc<eii.l)• centro: :erm L8bo":tc>'y Dur;>lrc21·:,;, reh�;•, 10 -" ;undornly S<>iu:)M l�U�I;;boraWIY spilL L<li)<:XOlt�r)' ctuplrci.ll�·s Pro·o;C:e :niorn:�Vo0 r>'gc.n!•ng rn+Ji':M prec.s:or. �·1d Sc.H1'1Pk: helerog>!r,8>ty Tbc pern"\l'i:d "''"')t'�

(vf' :Ice Rdmrvc< P<Oie<,ni Devt;'Jl:c� (RPDi cf L.cmc<"<J1C�j C:;pl.c��ws are spec.rf:ed m .>\c.S Meth<)(l QWI<C_N.'3S «r� """' der�mkn: on (he m�gnr',"j" ct r<•::wlts i� ::ornpar•�on to th· leoe: ol 1'0ocrtrn>) R<J8dl 1J lq\leS �0? 1\;> urn.!. Ru.<;ult b�·o.v,'x-m 1 c;-<1110 2.0 <.-m�o t.Of<- OY. - so;t,: R">',�lt > Xi 1m1�·s LOR - :J % - 20'(

EPj1Qt027·012 S802 0.75

, EP1101021-033 SSOG 1 00

EAQ33' TM<;table_A_ct�al ACFd!ty__(Z3F) __

' EA033. pHKCI (23A) : EA033' sulfidic- T\lrataPle Actual Ac,cti:y (s---23F)

EA033 Tl\!atable Actual ACid>iy (23F)

EA033' Tttratable Actual Ac,d'.ty (23f)

EAo?.3' pH KCI (23A)

i--- i

-t

0.< "'

2

2 0.<

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pH Ur.1! o;; pynte-s--mcle H+ / t

mole H+it pHUM

"" <0.02

'

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_Fl -_;

___ 0,02 % py�te S 0.02 EA033- T1tratable Actual Ac1d1iy (23F) - ' 2 mole 1-1�! t 14

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.. .,, __ .;""''"o_1 -.---- "'PHunrt -. .. ..

SA , ..

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i EP1i01027-012

i EPi\01027-033 !

S8C2 0.75

5806 1_00

acidity - Chrcmium Re\l'.1C<ble Sul�ur (a-228)

EA033' Chrofl"iUn\ _Rr;duc�PI� __ Su!iu!J_2_ 28),

(a-228) EA033' Chrctnum Red:'-lC\ble Sulfur (228)

: EA033' acidity- ChrOr'l<Um Reduc•b!e Sulfur (a-226)

-i'

_ i

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moie H+/t

% S mole H+ i t

% $ mole H+ I t

<2 M

,,_,._,,.,,_,,).<•'<'';:"-'

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00 0.0 0.0 00 0.0

0.0 0.0 M

0.0 00

0.0 0.0

00 00

00 M

No L"nt NOLimr\ NoL•m<t No Lrmlt NOL;mrt

0 % - 20%

NC L•ffi>\

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0%- 20% No Limst No Umit

0%- 20%

No Limrt NoL-mrt

0 % - 20%

NOL<rn:t No L:mrt

NoLrmtt No Lim<t

'NC"um•t No Lim<\

NoLm:t No L!mJt

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Dupf,co/0 !DUPj Rl)>Ml

EA033' s.ullidic - Ac,d Neutrat.si�g C<Jpacity {s-.1.9A2) '

EA033: ac•d:ty - Ac.d Neutrnl1S1ng Capacity - ! 10 mole H + I \ 2180 , {a-19A2) . ��l'lllli�'l!l!�llll\-lj\Glllllllllllllli0lll'lll\j\10\1W'I/iJ'1j\\llclWllY'clll!c\\ ,ll ' ' ' ' -

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i EP\101027-001 SB01 0.50 EA033' ANC F1neness Factor -' O.S 1.5

{ EP1.101o:.d.::0ti'

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EA033: Net Acidity (sullur units) ,. EA033·. �et Ac.idlty. exctud•','9 ... ANC_{sullur.�!:'ls),

• EA033: Llrmng .. Rste .. EA033 Umll"lg Rate exdudm$.ANC EA033' Net Ac>dity {acidity ur)!�s)

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.. EMn Un")!�g.fZate ...

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" EA033 .Net Ac.i_dtt,: .. (act.chty �.n . .ts) .. : EA033 Net ACidl�(_e.>(CIUdlng ANC (addity.uMs)

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kg CaC031t . .

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% S :J.02 kg CaCQ3,t

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No llmrt No Lrmt\ No lim'\ No l<m't No L,mrt No L,m,\ No Lm"lft No ltmlt No L1m1\ No L,mlt NOL>mlt No l..<mrt No Lrmit NO Limll NOLil"l1it

No L:mit No um1t NO ltffill NO L!m>t No L>m<t NO \..tm� N0 L1mit NC L.rr\it No L1m'.!

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EGOOST. Arsemc

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EGOOSI_: Lead

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EGOOST: Chromum

EGOOST Nrckel

2 mgikg 5 mglkg

5 mglkg

5 mg!l<$

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<2 <2 0.0 No Ltmrt

<5 <5 o_o NO L ;mit

<5 <5 0.0 NO Ltm<t

<5 <5 0.0 No Lrmft

<5 <5 0.0 No Ltmit

q << 0.0 NoLrm<t

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Method Blank (MB) and Laboratory Control Spike (LCS) Report

"n1u qu;JI•'•Y �ontrol \()r;n ;-re:Ctcd :_,lQQr;;:tmy Blank reiors \o •'�' @n<l.lytv :r<ee :n:�l'llX to w'aO'l ull re,;,gcrH m<:o i'!doicd '' the s�rne val\.rr,es or p;cpcrt.on" ,;,s U:k"<c o! 1!11" GC

PL1nJH'd'·" <S to rnorlltUI Pc>tcntl<ll lut.omtwy wnt,\rn,nm<on Tik\ quolr1y eo;mol t�'"' Labcr:Jtory Con:rol S""'Pie tLCS) r0�0rs !:0 -� cer..r!:<:od refB<�n'::e rn<1kH1ll. or u kr:c.wn q�•:'r'"'"•n<:V :rfi:e nBtnx �prke·-1 w;th :;;:rgro\

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Ne\ At:Jd1ty {acrdJty un1ts) " % S

mole H+/t

.-..�- "'""""""� "'"'"''"'- """'"""''"""'"'"'"' ' ' ' ............ '""" ····�··-"'"''"" ....... " ···-"""" l'li<>thad SMinK (iW<>)

R�port

WO<uaW<y Comto! Sp1k� {LCS} R<•por.

R�cov�ry LJmiL> ()'.)

"'' " DO

'" 70 DO

,06 70 "'

87.4 70 DO

64.2 70 130

85,3 70 t$0

70 ' "

<'0

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EP1101027 ACE ENVIRONMENTAL PTY L TO

J010-039

MMhO<:cvery Lm"m ('/,)

·--··--sr.; ... SS-5 ' "

S<o 82.2 1 1 2

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s of 8 EP1101027

ACE ENViRONMENTAL PTY L TO

J010-039

Matrix Spike (MS) Report

'lho q:.�cJi:ty c;cnwl '·"'"' v,·;;;c;;.; S;.WJO i�tS/ mror� w <1:1 lt1\roboormory &plil �·ilmpk sprke.d w::n .� repm�'"'r<;'Jtrv.,; set o: tmgd onalyrc-o. -rvo pVCpi)S(O ot :hi� OC psrwD�r�r ;;, :o m<:>rt<roc potcontiJI m<>�m etr,cts on an>Jiyt<'

r0cc·<·>·"�''· Stut.c :·<vco�ory i.:m,:,; J� per l">lxlratcry Oat� Qu;,:lrt'/ Qb;.:-cclrv0S ;�;Q;,;,·.;-. Ideal mcov0ry ril�80$ statsd rTl3Y be W<M<l<l rn �11\\ <N·�<�t .;;! >'.'Jmple rTl:Jl�;x ;r�t()rierunc0 .

Scrt;.Ma:rr�: SO\L . -�··· ..... �- "''""·-�·�· ._,, _ ... � .. . . ..... , ..... -.. ,,_,.

M«<ox Sp1!<<1 {MS) Ropon

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"0 70 ' "

no

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ALS Lal:lloraton.-1 Group ANALYTICAL CrtEr.-11STRY & TESTiNG SERViCES

Environmental Division INTERPRETIVE QUALITY CONTROL REPORT

Work Onior

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,EP1101027 ACE ENVIRONMENTAL PTY LTD MS GiNA PEMBERTON SHOP 17/2 SOUTH WESTERN HIGHWAY ARMADALE WA, AUSTRALIA 6112

[email protected]_au +61 08 9497 5000

J010-039

GP

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1 of 8

Environmental [ljvision Perth Scott James 10 Hod Way Malaga WAAustralia 6090

[email protected] +61-8-9209 7655 +61-8-9209 7600 NEPM 1999 Schedule 8(3) and ALS OCS3 reqwrerr.ent

18-FEB-2011 28-FEB-2011

No. (!i Siln1phJS 1'0<;(iW0;j 43 :-.io. d sampi0o i.\:l>Ji'J*d 43

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Analysis Holding Time Compliance TM fdiow!n-J ;Gpor: ��m''""'""�' ox:cucl:cr1 ;ote<P:lla(rcn and G>n<Oly�rs t:m�s end cornp<:ro� w::l1 rowmrr,Gndi�d /",o:d:ng lime�-d•l\n•cn,; a0d "'"�n�- 1.n�ormclttGn :$ oh>o prav:mod "' N1e O.<Jinple ccnt,o.wc< (�n->S:·:rva\Ncl l<on-, \•,h:CI1 thO an:;,,'y�is -:\l.q,JO� w,,s

G<:L% reported \n�en. E.lapsGG

rGpr<tson: f:,-:;1 d<>le< ot G>-trnc\ion or o_na\yc;:,; 8nC pieclv:li.'-' �ub%q�·:tn\

peno<J 1o �!\;,,)·SL�< WpffO':>W\S mJmiJ·;r oC dJ)'> �rom sam:"''irrg w�u:,, n0

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d,JM "''tr. th� shortest e<l'.�iytu l�old:ng krrK\ Icc t!!e e·�uro��l�ni ,,orl rr�<:tMd 'fC1cs0 '>Oil Midrng \tn1�·>'> mG. Q;ysruc>l r14 a21ys) M<>;cc:r-y 128 dO\yS) & otlwr m<Otdo \11>0 rWy:;), A rewroe:J a/each \!<'Jf8:or<? dew� not •]Ll<lf¥rt8•o

u b,B;,dL I<X <>II rL<Jr;.,.,,·�\·0 p<ir�mete(ct,

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SSC1 • 5.25, SBO\ • 6.00, SBCt . 7.00, SB01 • S.CO,

$802 -0.75, $802 . �.50,

$602 -2.00, 5602- 3.00,

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ACE ENVIRONMENTAL PTY L TO J0to.G38

QuaUty Control Parameter Frequency Comp!iance Ti�C" foibl'ilh\1 m�ort �Ml'mi'ln·c;�� tho li0•W"ncv c:l lub0ratc!y OC s�n;91<;� �n�IYS'-'d .,.,:r<c: :r:<O a<'ol·;t<CJ.I io\ls·, :n wt•·cl\ tho s,:c,.,.n\Wd ��<v:pl�\0) wos{N10!Q) ;:w.>o�··;su·Cl. Aelu�l rall',· �!10uld !;)(.• (;r0<'lt\l� th<m :x 10qual �0 '""' ¢Xf.l''C!(.)d rCLt"' A J:�"'lcl <Jf bee�"'''"' ::; ;r;w1d<ld m lh-" Su"'"'"'Y ct Outt:er.';,

,\btnx: SOIL EvJILWt:on x -' Qual:ty Control trequc�n<;y ncr w:t�:n >�P"G:Lc.;,hon ., (�<;>i.tJ Co,wol 'r>•t;L.(,nc; w:th:n so�c'.r«:c.%on

QC$3 requor\Otntmt

Schedo.�ie 6(3) and AlS QCS3 reqwrement

Schedule 6(3) and ALS QCS3 req,uement

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ACE ENVIRONMENTAL PTY l TO

J010-03S

Brief Method Summaries Tne ;l.r1alyt.csl ;xcced'"'"' c.>;Bd �y \hie f'wronmei:li>l D1Vi":o� h:wG b,;,c,-, d�'>'IOicp�d from es:eu . ._�.�<!O 1"\"'cna\:onallj rcl>·,ogr;:�e<J proc&dc�rf'� S>JCh �5 U>o�e pu;:.bi"«Cd :C.y \�\G U!.; EPC•, JWC,A AS 'wd NCYM In Mc:se

d<OvdOP<:>n the absence 0! Ce<;u:nf:nWd stand�rds. or by c.li<:t:\1 reqw<e$1. fi<<O iollcw:ng IB!X>rl P""'id<es �net <H:rM:r:pt;OilS ,jj \h•J an;-Jiy\<Cal pcor-edc;ros <;rm�loy<ed f.::•r i'%d:o r•l>'<\')1'1nd ·.n �1:1; CW1c·

'14lt0 ot A�Ji)'>·�>. SourcES �cmn wh;c.� ALS r.�,et�ods tmve :010<1n o0v<liO\K'<l 0ro pwv<cGd wnt:<n t'J(; Me�hCd De�;;r,�ttons

Moisture Content

\ Total Metals by ICP-AES

!Total Mercury by FIMS

; nv' c'"'"" Digest for metals m SOilS : sediments and sludges

EAciss-to3

EG005T

EG0;.5T

.. EN68

' ' " .. J\'i<'!.C:'\io\l',;i'J· method covers the determination of Chrom1um Reducible Sulfur (SCR): pHKCI: titratable

, actual acidity (T AA)·, acld Mutralising capacity by bacK titration (ANC): and net acid soluble sulfur (SNAS} which 1ncorporates peroxide sulfur. lt applies to soils and sediments (including sands) derived from coastal regions.

, limi!'IS Rate IS based on results for samples as submitted and incorporates a mmimum safety factor of 1 .5.

SOIL · ! A gr;,;v;ffi'etric PrOcedure baseo on �,vBi9ht lo·s·s oVer ·a 12 .. hoUf ctrYi�g Period at 1oz�'1os d.·

egrees C. This methOd is ...... ' . .;of!lpliant.<JV!Ifl .t:'t:.e':-1 .(2_01.Q .. .Dr�ft) �(;..he�ul� ... �f3L?�cti()n a.��-T<!ble ... 1 .( 1 � .. day ... hol.cJ.ing_ !ime).-.

SOIL ' (APHA 2'\st eel., 3120: USEPA SWS46- 6010) (ICPAES) Metals are determined fo!lowmg an appropriate ac1d , Oiges\lon cf the soil. The ICPAES technique 10nises samples io a plasma, emtlting a characteriStic spectrum : based on metals present Intensities at selected wavelengtl"ls are compared agamst those of matrix matched

_,.!._stanct.ar�s,.J:hio; .. �ethod .. i�.co.f!1pH!i!(I\Yiith.N_EP.� .. P.9�§l . . ?_ched�l� .. 8@....... . ... ...... ... ..... .... .. SOIL , AS 3550, APHA 21sted., 3112 Hg - B (FIOW·inject'on (SnCIZ)(Co!dVapOI.lr generation) AASj FIM-AAS tsan

awtomated flameless atom1c absorption technique. Mercul)' in solids are determmect fo\lowing an appropriate acid d1gestion. Ionic mercul)' is reduced online to atomic mercury vapour by SnCl2 which is then purged ir.to a heated

Quantlflcaflon is by cornparing absorbance against a calibration curve. This method is compliant With

SOIL " r iJsEPA'20o.2' MO'ct. HOt 8i0c1<),cid' bi9est1Qn 1'.cg Of sample 'is heated With Nitric and .. Hydrochloric acids, then

; coolecL Peroxide IS added and samples heated and cooled again before being filtered and bulKed to volume for ; analysis. Digest is appropnate for determination of selected metals in sludge. sediments, and so1ls. This method <s .... r:o.�PJ.iant NEP�t . .f.:� ��.?t'?.��€.?.�!� .... �1.�1...\.�.�!�? .. d ... ?�?L_

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earned out in co,r-,plronce w1th pro(;edl.ii'8� �peoli;,o.d m 21 CFR Part 1 1 . St!?"·''tcr:t•;· Pos;t.or:

Leanne Cooper Acid Sulfate Soils Supervisor

__________ ________ " __ _ l;;:nv!roi'i'ro"<an�"'' t:::"';�,�•on Partr> p,,, ,�jm,·. AL$ L>>bor<ltory Group

'" "\0.1 """' ,W,(qo N.\ i"->>!<�H�Js-:; T<t. .,� \.,.Ol�� 70!>< '''"· • o \ .. ;.�;-�·) :;,Q.; "'-'""'·''hU�o'>•>l.wm

$�JiliHOit00' rnG�c\led �elow. E!,:ct,·onl( �;gr:mg i)C\"' t..\i.J01';

A"r.rew!cwon CJtC•_()<l''i

Perth ASS

wo M&W@Q&Ni>ltJ!liiWUillMh ,1 Gatt,,.,,,.off Sroo��,-, (.OI''<Od C<;m,><or-y

M@fu 1i1&UMl\ID!ii$\�'', :\!!;,··-----• �

f',"l" Wo!� O•·c\•Ot

<:!,em

F'W)c'G\

2 of26 2Pt 101026 AC2 ENVIRONMENTAL PTY L TO J010-0:I8

Genera! Comments ncJ �n.�!yw;�J pte<:0du�o "sod t!\' \h" C·:�vteOP,mem:::! [),v,son i"o:!ve b-e'·""' di'>•dcp<:o fr,yn CJ%3t·hshcd mtr.·rG.U;:OI\(lily ri,•r;..lg,,led �rcc•.ldwm•; such 1:\'i· ?NJW p�bid1'Cd �y (ioe USEPf1

d·JvdJp�G p;ocud<.<i<o�. :�:.;, <w<p:<:�y0d ''" 1r11" ;m"•Jl!•>: o( (!occmwn;e<! obn<!mde. 'x :''>' d<>:i�t Nq,,•ost

\'Vh<�r<) r�Vt�(<,l'e ''i0hlrD\':'\\11.()� ha-S bO,')h P0'i�)f11",oQ, n.l�',i,ll�; �m '"P<ll'1<Cd Oh a 0:1')' w<l,§l\\ b:,Y.;<> V'i'WI'<l � r�por',CJ<.i iec,s 11\i!n (•':· ""�dr ;s h<glwr '"''.tn n·.0 LOP lh.s rnay o� dwe to prm1«•)' s6rnpk o�traclJC:iJO�lci:C, d,[,;tron ''lnd'ar rns\ifrrert sarr-p:8 jor ar1:a!y�,,

\•\hi>!ll U'"• L()C� C'l 1\ re!Jcr!cd 1\c"llt dt(%r.\ fr07l S(�rlO.:'lrd LOi': t�<S m�y b� due tQ .�<_<:;.� morst�·ce co�t"r' ,ns�ii,�\er:t 'iiV�1tlG {ie<J.::ood "'"'S'·"lt e<:�.<oy�-<:) vr .'1K<1n� 'n"''Yf<H<JnC:!

"""'"A f\S and N:O::i")..l '"' hC'-'6<·�

'h�·''"' sa:n�i·n(,l '""* ,i'fcc:r;c,t>On ,,:. i\01 p10Vtdc:d :1y tl\c' cb<e"� :;mnp!tng li8\0$ :are o�.cwr; wt\ocut lil t.rne <:C.r'i;Jon\Cr11. In thes8 :n$i'i'JnCCS, the 1>mo r..Oil1f>0!101\l h;;o-. 1Jecn J$�Ur10Q tJ·1 111e b�.·<;:(,llC>ry '!G:' pi"J0SSW;J p•.rpo�''''

K(q CAS l'umoor Cc\S mg<�.\cy :',u,;1D<''' \1\)rr\ ct<>t<lb2;<� :':'1\ll(\l;)j(l<)d b'i Chd;ucal 1\ostrac:Ts s,·,rv:c�« Th; ChQilVC�', i\b�ttil,c�s Serv.ce >Sa <liv:s,on of 'llC1 Am�'"'-"" S!'<'rDICal Soc;;,tf

i...OR �n,nt<:,f r�P''rnr.IJ � � T�.:� rroS�lll tS CCIP;>wl'>t: :·ron :�C"''d"ill an�JyK d�·tockm� .�1 '"'' ,,t•<lw tM I�·Wl <Of repmr.,�q

0 ASS Field Screening: NATA accreditation does not cover P<>rlormnncc of this S�<,..,ico.

f �o ,,.,.,;NcO,' {l.•.x.\J,'o\ �"' .. �..._, ('(NIP" "f

h18'' ·t;o·� O;J,,,r

l:!,c'r\ Pm;,Kt

Anatytic<JJ! Resufts

S,;!H,\o:r,xo SOIL

R�action Rata

3 of26 EP11C1026 ACE ENVIRONMENTAL PTY L TO J010-039

C,1.'io'O( samp�t' i0 5601 {l.25

17-FEB-2C·i1 15:00

Slight

$801 0.50

17-FE8-20 1 1 15:0Cl

Slight

SB01 0.75

17-FEB--2.011 1 5 0 0

Slight

SB01 1.00

17-FE8<20tt tSOO

EP1101026-G04

'·'

6.1 Slight

$801 1.25

17-FES-ZO: t 15 00

E?11G1026-0il5

8.8

,_, Strong

A (;,,n•�l!c•,J iJ.'�IIIC.'O L• l•,:<c.l •;y•, Yd >t

g • � " " 0

� ' ";'_ , ...,. :�:N 5; 8

, :::J-m ' .n ' m - • 0 " N N � b --g rn

g.

-' 0 • S: ' u; 0 0

0

N ... •

)> 'G 'Jj $ C. , ' � il " 0 '!! "' ' 0 • ru � -

"' m �

00 w "

F-�u" Wt·:� C<ckr Gl•a·1� PmJ�(:t

Anatytica! R.esu!ts

Sc>t>-1,\;;\nx: SO!L

pH (Fox) Reaction Rare

5 oi 26 EP11 01026 ACE ENVIRONNIENTAL PTY LTD J0\0-0'39

Cl1ent �;,>mple i.G SS01

2.75 17-FES-20 1 1 15.00

Mode raw

SB<l\

3.00 -- 17:F·Ea-.z6'i t 1so6

Modcraw

$801

3.25

17-F£8-201 1 \S.OO

Moderate

$601

3.50 17-FE8-20 1 t tsoo

EP1101026..Q14

\.7

'·'

Slight

$601

3.75

17-FES-2.01 1 15·00

EP11l!1025·015

;_;

'·'

Slight

'' CY.ortoc:, ,-1.-,{''e'" �·,miw Co-">'"';!

P�G0 'li0(� ()�el<O!' C:.0,\ i-'rvi'';:

AnaJyticaf Results SW?Mut�'X' SOIL

R.e&ction. Rate

6 of26 EP110\026 ACE ENV!R0N'I.1ENT AL PTY L T:) J010-039

C/o&Jit $�J":,p/0 ;[; $801

4.00

17-FE6·20 1 1 15.00

Slight

5801

4.25

17-FEB-2011 1S·CO

S801

4.50

17-FEB�20 1 1 15.00

Modnrnt0

5801 $801

4.7$ 5.00

17-FEB-2011 15.00 17-FEB-201 1 1500

EP1101026-ll19 EP1101026-020

'·' '·'

'·' '·'

Moder&t\l Modwat&

h c·.,.,-,_.'"''3"''"-'> ��*''' c�·-"'".""f

i''''J'-' \'""'K Ci<dUI'

Cl1�r,! c··roy'"t

Anafyticai Resu!fs 8c<n .. r,��tr:�; S01L

''Roaction Rato

7 Ol26 EP1101026 ACE ENVIRONMENTAl PTY L TO J010-0'39

C/l&r1{ :;�mp,'�· ,'D SB01

5.25

�7-FEB-2011 15.00

Moderato

5,50

17-FEB-201115.00

Moderato

SS01

5.75

'i7-F.EB-2011 15:oo

Mod<lrato

SB01

6.00

ti-H�:B-2011 1.5 00

EP1101026.024 ---·----'

5.0 5.0

Moduate

SS01

6.25

17-Fi:B-2011 12 CO

EP1t0t02$·02S

'·' '·'

Modorato

A C.·rnipl,c•,f .�.·GC,",,,., �. ,'f,{C'V' c,x, .. ;o,ii>j

Pav� Ww�O .. ci<x C!'�'i" !0ro,�·:U

Anafytical Results ::;,,r,.�,·iitt:l�: SO!L

pH �Fox)

Reaction Rata

8 of 26 EP110tG26 ACE ENVIRONMENTAL PTY LTO J010-03S

0.1

C/•0'11 ;,;gnp!,) !!:;

pHUM

SBG1

6.50

17-f'EB-2.011 12 00

Moderato

6.75

17.FEB-201t t2:oo

"

Modwata

SB01

7.00

17-FES-2011 12.00

Moder3t\l

SB01

7.25

17-FEB-2011 12 00

€?1101026-029

'·'

.., Slight

SB01

7.50

17-FEB-20'. 1 12'00

EP1101026-030 --·-

'·'

'·'

Moderate

A(,,.,�·�·�:,· iJ.·.;;•:M;; i.•n"l''-' (',\·: r•;'""t

'<•;)'." 'A or.\ O'd�·r

(:\,Gr\

i>rc�;,,n

Ana!ytica1 Resv.fts

SCJt>-M<�tnx; SO!L

j ReactiM Rata

g of 26 EPHC1\l.?!l ACE ENIJIRONM2NTA\. PTY LTO J010-03S

Ci'"'"' sample .'D SSC1

7,75

17-FE:S-201\ <2·.oo

Moderate

SB01

8.00

17·FEB-20n 12·00

Moderate

SBG2

0.25

17'-FEB-2011 12 00

Slight

SBOZ

0.50

t?�FES-2011 1260

EP11G1021).034

'·'

'·'

S!igl'lt

SB02

0.75

r 17-FES-201 1 12 oo

Ef>1101021>·03S

'·'

'·'

Shght

A :J,�:,p�c·) [;CAlC\'� '''"'!''-' (,''-''"?Y"f

' "' ' m • � w 0 " "' w • ,:;:- 0 • � N • 0 " 0 0

" ' ';" ' m • m � w 0 0 � w • e 0 •

" it 0 m 0 0

e,,;_, '""'!'·' 0'""'"

,;:t<mt

l"•rJJ-tCl

Analytical Results

s,,p..Mmr·x: SO·IL

pH (Fox)

R<Jaction Rate-

1 1 Of213 E?\101026 ACE :ONVIRONMENTAL PTY L TO J010-039

(.'i,Mt s,;,rf'ple IC $602

2.25

17-FES-201 1 ts·oo

'·'

S!lght

SSG2

2.50

17;FE8-20 1 1 15'00

SBD2

2.75

17-FES-201 1 15:00

Slight

SS02

3.00 17-FEB-2011 1 5 00

EP1101C26-044

'·' '·'

Slight

SB02

3.25

17-FES-20 1 1 15'00

EP110102�·045

'·' u

Slight

A .:;�_,,,�Qr;,\ fcui:,o,·., ;,,/"'"" Co',' I l'<J'.'f

P<'" \''{nr�, 0<'<C: Ci,e:�t �·'IQ)'X.1

Anafyticai Resuits ·.>Q./·,ld!!lo: $0\L

1 2 cf26 EP1101026

ACE ENVIRCN!I.'ENTAL PTY LTD

J010-03'.l

C:r,;n1 �,y,p.'� iD SB02

3.50

17-FES-201� 15:00

Slight

SB02

3.75

17-FES-2011 15·00

SB02

4.00

17-FEB-2011 15.00

Slight

SB02 5602

4.25 4.50

17 -FEB-2011 1 5 00 17-FEB-2011 15'00

EP1101026-04S EPH010Z6·0W -----

'·' '·'

.., ' ' Slight Motl<lrat<>

A (>,,.-,�'-"'') !). �,-,,,., �,-, ,,,-e,.- �-"'.''"'�'•!

f>,,,_,, ..

'/\'<;cK C;.•,·i<J-r

Ci.c>n\

Prc;<>-c:

Analytical Results S"b--M;>l',�: SOIL

pH (Fo�) Reaction Rate

1 3 of26 EP1101026

ACE ENVIRONMENTAL PTY L TO J010-03S

c:.-en� $¥r:;:A:) :0 5602.

4.75

17-FES-2011 15 00

Slight

5802

s.oo 17-FES-2011 t5 00

Moderate

5602.

5.25

17-FES-2011 1 5:CO

Mod<!>rate

5602

5.50

17-FE8-201i 15·00

EP11 C1(ll:�Hl54

•••

'·'

Sligh!

5602

5.75

17-FEB-201 1 1500

EP11010Z6..US5

• ••

'·'

Moderato

A C,;·npC<· '! 3:</i''-" L"'''""' Gc-•c·pJ'>_;

Pd,i,l \-\iol). Co.\•Jr Cl,<:nl P>·q,x-!

Analytical Results Sl.C·I>.bt!.·�: SOlL

14 Of26 EP1104026

ACE ENVIRONMENTAL PTY L 10 .1010-039

C '01>1 S¥!Jp!e ID 6,00

17-�EB-2011 1 5 0 0

6.25

17-FE8·2011 15.00

6.50

n-FEe-zo·-1 'is:oo

SJlght

SB02

6.75

17-FEB-201 1 15'00

E?1101026-05S

'·' '·'

Slight

SS02

7.00

17-FES-20\1 1 5 00

E?1101!1Z6-060 ----·

'·' '·'

Slight

fl, c,,,_.,,;,�d tNI.''"'" �,,,•;:c·� �C.'·""'"I

h1Q0 V',ock C'l-1•'"' c:,ww f·'''*"l

Analytical Results

SCJt,.P,\1':"" S01L

Rea<:tior� Rare

1 5 of 26 EP�1C1026


J01 0"039

Ci,f!,;t s.'!mple !D SSOZ SB02 T'··-·

· SB02 $802 $803

7.25 7.5o 7-75 a.oo o.25

17-FEB-2011 15 00 17-FEB-201 1 15:00 17-FEB-2011 15:00 17-FEB-20i 1 15 00 17-FE8·20� 1 15.00

Slight Slight Sligl>t

E?1101026-0&4

.., '·'

Slight

EP110102$.065

" ,_,

Moderate

'

A C'•'l•;,·t>c•.J £>�·'•c•!O f.-'-'il."iC'•:I <::0>'"W'•f

)> .$ (; :;:: £ (/) I " • " � & " Cc c' " ; • ;:: ! ,, 9 "' A �-• 0 0 " o' 0

• " ru � Q -r :u * £ <4 �

� " ' '" � 0 � ' 00 � 0 • " • 0 0

i: i ' "' ! § � � � " w 0 ' 0 " 0 " : ' � b • 0< • 0 0

m � ] m !i w � � :# • " w I • 0 e • 0 " " " 0 " • � �

" • 0 0

!''�:)'·' Wo<icO•·Jc•'

Cwm� PrO)W;l

Analytical ResuJts

Sui>-Mntnx: SO!L

j Reaction Rate

17 of26 E'Pi101026 ACE ENV!RONMEN1AL P1Y L TO JCt0-039

C:'enr sormo!e IS 1.7$

F-FE8-2o11 1S.c'o

5 5

Slight

SBG3

2.00

"n-FE8-20i\ 1s-o6

5804

0.25

'17-FEi:i."2o1 1 1 5.oo

Moderllt0

SB04 SB04

o.so 0.75

17-FE8-2011 15·oo 17-FEB-2011 1 5 00

EP1101026-li74 EP1101026·075

'" '·'

'·' 5.5

MOde rat& S�gtl\

A G":nro--�,,;; & o<.'>c'"• c,·, •• tc•;l C c"''�"''r

.,.',•·?'-' ','.'�" ()1·.'-•·

C\l';'r',T

""'J"<:i

Analytical Results

i"ic;i:dhit<,x: SOJL

Reaction Rate

< 8 cl26 EP1104026

1\C€ ENVI�ONMENT AL PTY L TO

J010-039

U.t>'m s·.Jmp(e ro

(;),'':!4 .IJ.'ri/J>�·ng 1HA" I im:c

0.' prl Unit

SBCM

1.00

n-FES-201 1 ;;;-oo

M Slight

SB04

1.25 H-FES-201 1 1$·00

s.a·-

Siight

SB04

1.50

17-FEB--201 1 1 5 00

...

Slight

S804

1.75 17-."E8-2Cl 1 t5.00

EP11G102S·G79

.., Slight

S804

2.00

l7�"E6-2Ci1 1 5:00

E?110�02S·OSO --

' ' ..,

Slight

A '""'"Db¢;, 1i.-vl!'"'" c .. · ''""-: ('"";.'"'"

.�'-'·]•'' 'f<'o�:, C<d�: Ci,�·m ,c·,n ·"'�i

Analytical Res:uus :,�_,!) .. �·\Gtl\x: SOIL

pH jFoxl

Ruaetion Rate

19 of 26 EP1 1 01026 ACE EN1/iRONMENTAl "TY L TO J01C-OSS

C'li''''( $Jcr:pie !') SBOS

0.2:$ 17-FEB-2011 15:00

Mo<lerate

SBOS 0<50

17-FEB-2011 1 5 00

Moderate

$805

0.75

17-FES:.2011 15:00

$8()5

1.00

17-FE8-201 1 1 5 CO

EP110102S.·Oe4

'<' '<'

Slight

$805

1.25

17-FEB-2011 15.00

EP1101C25-0BS

,<, ,<,

Slight

A Cli.".•:-·o�;! 6r�lm�> L''""'·" C"·r•:O.n(

,'"'d0� '1\'Uril C·tdG·'

·:·:k(l\

?'C)'''("

Analytical Results

Sc.b-Mi,ifl:<: SO!L

20 of26

EP1101�2&

ACE SNVIRONMENT AL PTY LTD

J01D-039

Ci'")l� ,;.,)."'!;:>.'<! /0 saos

1.50

1!-FES-20;1 jf>·OO

'"

Slight

17-FEB-201 1 15'00 17-FEB-2011 15 oo

' ' Sn911t

saos S806

0.25 0.50

H·FES-201 1 15:00 17-FES-201 1 1 5'00

EP1101026..{)8S EP110102&-090 .. _: ., "' s.o '·'

ModtltM� Moderato

), C,;·.yrM\ (l;W''I'> L"i>J<K' c'•J',O."'l''Y

"·''�" f'Qh, (i,d,>r c.�"'

;">;-o;\0\;,'

Analyticai Results

Sc,b-\htr',�: $0\l..

21 of26 EP1101026 ACE ENV!RONMENT"'-l PTY l TO J010-0:}9

Cl.1;"� �:lmpiC' IS

Chent

SSOG

0.75

" r7-FEB-2.ot't ,·s·o'o

Slight

SBOG

1.00

ti-FEs-<.Cj't tS·o6"

Slight

SS06

1.25

t7-FE6·2.0 1 1 15:00

Ef'11010:U·09l

Slight

SSOG

1,50

'i7-FE8-2ottts.6o

EP110102S-ll94

..,

.., Slight

5806

us

17-FEB-2011 15:00

EP110102S·095

5 6 5.<

Slight

..; c:"·";:t":' '""'""" "'":'.�' c'"":··�nt

hliJC'

'/.JG:k Cl(i•,;c C:.C•r.t f'rQ;CC\

Analytical Res�#ts s,,toA,l:;:m: SOIL

22 0( 26 EP1101026


;010-0::>9

(;,- SBCS

2.00

SB07

0.25 17-FEB-201 1 1 5:00

Slight

SB07 Cl.SO

17-FES-201 1 1 5:00

Slight

$807 SB07

0.75 1.00

17-FEE\-2011 15.00 17-FEB-201 1 15·00

EP11010ZS·OS9 EP11010ZS-100 �

,., '-' <.< '·'

S!�nt Slight

A (';,,,."��;>_,;! ih..\'w,-,, �""''"" 1:uo'"'''-"

r-�0'' 'o\'O'K Ct.;J,or Ci'""' !''fU,<�'"

Analytical Resuits

SuiHv\c·:m�: SO!L

R"act\on Rata

23 of 26 EP1�C1026 ACE ENVIRONMENTAL PTY L TO J010-G3e

C><J'l! S.·Jmp��· ID SB07

1.25

17-FES-20;1 15·00

SliGht

SB07

1.50 17-FE8-2011 15:0c

S!ight

S607 1.75

17-FEB-2011 i 5 00

S!igirlt

SB07 seos

2.1)0 0.25 17-FEC-2011 15 00 17-FES-2011 1 5 00

EP1101G26-104 EP110102S-10S -

'·' '·' '-0 '·'

Moderate Mod(>rate

li [\,",.';0c•\ 3t..,;'.'<;r; i..<.'l 'oiC'G C'·.· :.;'"''1

'""U" Wx� (;;,:tvr (;1;0:'•'

"''1!]\·:·(:\

Analytical Results

2·.,b·>V,Iht: SOlL

Reaction Ra�

24 of 26 EP11D1026 ACE ENVIRONMENTAL PTY LTD J01 0-0:>9

"

Cf,n,,� S$imple :!)

0.50

17-F£8-2011 15:00

Moderato

0.75 17-FES-201 1 1 5.00

..

Slight

uo 17-FEB-201 1 15.00

Slight

SB<l8

1.25

17-FES-20 1 1 1 5 00

EP110102S-1C9

'·' '"

Slight

ssos

t.so 17-FES-201 1 15·00

EP110102S-110

'·' ..

Slight

,; Cwi:,oUvo'; B:uir'"" �"'''""' C•e""""''!

P;;-;;<; 'Aor� ()l(ldt-

Ci.<>;>� \'roJ"''�;

Ana!yticaJ Results

2<Lh-Mmn�: SO!L

pH {Foxl

Rea<;tiorl Rat<>

25 of 26 EP11010;<6

ACE EN'/tRONMENTAL PTY L TO

J010-0%

Chf.'n( s,i!rnp!e .'D

Cus-n1 sarrwirf)q aM" I :rm&

·a.1

sec a 1.75

17-FEB-2011 15:00

·st·i-Eiht

$603

2.00

17-FE8-2Gt l 15'00

'·'

Slight

H-FES-201 1 1 5 00

, , ·--Siisnt

SBQA2

17-FES-201 1 15 00

EP110102S·114

'·'

"' Stlght

SSQA3

17-FEB-2011 1 5 CO EP1101026-11S

"' "'

Snght

A G.,.-,.,u.,;! "''--'1·'"''" : .. .-,;;%' (:.y:qu'-1

p-�,)0 '�""''·''' a,,;,;, ..

C":n� I'''CJC<"-t

Analytical Results

S"o·M.,.Ir•,,: SOIL

26 of 26 EP1101026 ACE ENVIRONMENTAL PTY L TO J010-02S

C!ienl 0!Jrrp!0 iD S8QA4

\7-FES-2011 1�:00

Moderato

SBQA5

Mod&rato

SBQAS

t?:FES-:<61 1 1s:ao"

Moderato

SSQA7

1?-FE8-20;1 ts·oo

E?1HHil2li-119

'·'

'" Slight

A C'�" 1''-''·'i !'•ro<�>oc; (,,, '"i'�' \:ce'''"""Y

M * w•'WWi!lii&&!!ll!'@MOOMM!lUMJlle lfJMi)t:-:···Til'Wll'''''""8''''',•---

ALS Laboraton-1 Group ANALYTICAl CHEI\1ISTRY 6. TE'ST:NG SERViCES


Work Or<:iur

Cl!<Ont

Contact ivJ;ltCJ%

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Environmental D1vis1on Pertl'\ Scott James 10 Hod Way Malaga WA Australia 6090

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Genera§ Comments

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18-FEB-2011

22-FEB-2011

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Quality Controff Parameter Frequency Compliance 'ih" follc•wtg revo:t ,,,mr�"'""�" IN: (r<Jq�sr;c\' ,_,; i'mc:o.tory O.C s:•ncp\\1� aqOif�"d 11,1\'\:n \!'"' ;1.naiyt,c�l :ot(�) ", wt,:ch \IW %�m:tted �;;rno:,;,l,s) W0S\'t.·herc) ;:>rccc.ss�d . Ac'.>.:ai r"'"' sr.q,,ic \>".l gr�3tcr •.hon cr "cual tc .h�· �xpM.�<>d :eM:>. A IISI•�g of bfe:>C�C>:i ;; povid<>d 'n 10.0 :Summmv o! Outl.er�

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Brief Method Summaries "!'tW i't�,>i;\,<:81 plOCCC\JC�S US<i<' by tt"l \"n,·II'Onm<>niul Cnv<�•on hc\Ve \)Q�rl ctevelc�N; from \CSWllt$'1ed :ntem:;t,on�liy t"�)gn1ZOC prOC�duW:> s�ch 00 lC,CS'.' p:!i:>'l"£.l>ed 'cy �M· ;,)S fp,<,, APH.•';, AS 1\�.(! Nf::Pl/ I� �0',10\; <k·•dC�(·�d prcc<o·j<lt�& �'" i:m;!io;"i:0 '"' tn<o ab�n.�v of dOc�me,;tt>C 1'·l«ndords or oy '�'enl '"�''"�1 TI\G to:tow:n\) nop011 pmv,des bMf de>n<pt,.-,,�1· of th.c :>n�lyuc:,11 procc<i1;f0$ •.Jm�loyc_•d �·x '"''idts '"'POrtee ,n :<w CW(Lic�\0 ot 1\n�;ym;, 6o.1f�'\O� -'TCII\1 wi'"<.t\ ALS �'�'hOd� hiMC b,e•,;1 <.'<-'VdOpGd ,l<'i' p;MidL'<J ,.,,;�:,,� 8\!' !>'\eF;oc Cl\,'i'CCol)bo.�s

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Summary off Outliers

Outliers : Quamy Control Samples

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Dtlp!icates, Method Blenks, L,lborato1)' Control Samples and Matrix Spikes

o For an matrices, rto Method Btanl<. value outliers occur.

0 For all matrices, no Duplicate outliers occur.

e For a!l matrices, no Laboratory Control outliers occur.

e For all rna1rice&, no Matrix Spike outners occur.

Regubr Sample Surrogiltes

e For a�\ regular sample matrici'IS, no surrogate reeovery outliers occur.

OuWers : Analysis Holding Time Comp!iance

Tnr.� rc.,oort d<spic.y� H<:lk�n\(j 1'rmw brwnch0> only. Only 1M; re,,p0d1ve Ex;r�d.tcn ! Pre��lriltVl <lnd:ar 4-.Mr.i'tt;,•, �<Jr:'.:IOM;nt 1s:nr" diSPbY'-':i

o No Analysis Holding Time Oulliers exist

Outliers : Frequency of Quality Comrot Samples

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AUSTRALIAN lABORATORY SERVICES PIL EP1101327

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MS GINA PEMBERTON SHOP 1712 SOUTH WESTERN HIGHWAY ARMADALE WA. AUSTRAUA 6112 [email protected] +61 08 9497 5000

J010-039

G P

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CERTIFICATE OF ANALYSIS P<>U"

Ldx>r�tor;

Co•\lact l"dcr,c%

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F�cs.:milo QC L.evel

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1 of 4

Environmental Division Perth Scott James 1 0 Hod Way Malaga WAAustralia 6090

perth.enviro .seTYices@aJsglobal. com +61-8-9209 7655 +61·8·9209 7600 NEPM 1999 Schedule 8(3) and ALS QCS3 reqwement

04-MAR-2011 22-MAR-2011

'"c cl so.rnples re\Xlwcd 4 :-/o_ of �;:un;::l�s <J:Vllys�d 4

Tt11s repo1� wpersed8S any prevt(IUS wpcc(s) w:tl: U1\s r"lerer.ce. Results apply to :rte sample{s) as release.

pc:ges of \h1s f(:port have oeen cnec�.ed em: 3pprovet: kr

1'11iS C0rM:caw of f\nalys1�, coflli'l:llS (M folloWII\(; m!ormation·

o General Comments e AnalytiC81 r�esults

NATA Accredited laboratory 825 Signatories

NATA Ths dccument <S issued 1n accordance w1th NATA

accreddatiOn requ1rements

ThiS document has been electronically Signed by the <lllthorize<:l signa((;ries :ndiCilled below. IC:IectrC111c scgrung has oe10n

carne(i out ,D comp!lcmce wtlh procedcires specifi'8d v-1 21 CFR Part 11.

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P�·)0

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.!010-039

Genera! Comments

-�hcc aM<ytr.:<tl wcc�:qures l;WG oy th� Enwontr�cntc;l Dr�'�"c'' hiM> lloi'�· de-,,oloped tl'0"' es:.ohi·,snco.-:t rnbrn;wcnal!y rvcog:l'.lM procedure.� �uct-. <IS �n:x;oe pcroir•;hM Cy tn0 US!;:PA A?HA AS M\d NEPM In !'ou��

(I<N0i<:po0 ;n:xwdc.n,� me- <:rq/oyc\1 "' tne ol,�<onm ol doc,:·l'�·mc•d S'i<''>dmds ot OJ ci!%t wqcr'1'\-

'·NI·"""'' niOI>Jl\l<i: ;k':er<nonu\\o� 011s ()[,·em pNforrm)•.:l no�r.Jl1S :mo rQf)(»�<'d on a d:y "'l·C>g:O� ba�''·

V'.,l:\eto � ruported 1-��'� t:L�n ('f sam pi� extrsct/0:(l�·statu �;t<Jno� and: or ;no.,, mont 2arn�:u fer �na!y�iiO.

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K':y c_,>.s hwml'�'' c;;,s r<;,g,�uy number (l(lrn datab:;.s� <n'!l.rntwn<d by C:Mrv::�l Abs:ra·�bl s,,,..,,c-cs H•e cn,_nncui Abs�rocts s�rvrc�· ts :> dr·,,�,:_r� of the Amcr:c�n CMr"rJCal Socr"'�Y

LCR � Lomll ct' �-�part,l'G

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A C.t·CJp0"'! &oVWo �''''''"" CvYC;W•f

f'<1Q<" 'hcci< O<·J!o< Ci�e;nt hope:

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· cnrO-m;,;n CoppN

N;ekal

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3 of 4 EP110l327 Amendment 1 ACE 2r>;VIRONMENT AL PTY L TO J0'0·03S

M801

CIHc.''� d:Jic! t.'me "6'4:MAR'-2c1'-i' 1S'·6o

7440-4:>--9 0.0001 mgil 0.0002

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743':1-92-1 7440-66-6 0.005 mg1L 0.143

7439-96-5 0.001 mgiL 0.114

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0.0001 (1.0002

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4 of 4

EPO�G1327 Amendment 1

ACE ENVIRONMENTAl PTY l TO

.'010-039

04-MAR-2011 1 5 00

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QUALITY CONTROL REPORT

WorkOrdw Am"n<lmonr

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Contact ''"dre:ss

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MS GINA PEMBERTON

SHOP 1712 SOUTH WESTERN HIGHWAY

ARMADALE WA, AUSTRAUA 6 1 1 2

[email protected] +61 08 9497 5000

J010-039

G P

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T �l0oho0\'� Faco .. m·l0 QC l.evcl

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b�(lG Date:

1 of 7

Environmental Div'tsion Perth Scolt James 1 0 Hod Way Malaga WA Australia 6090

perth.env:ro [email protected] .,.61-8-9209 7655

+61 -8-9209 7600

NEPM 1999 Schedule 8(3} and ALS QCS3 requirement

04-MAR-2011

22-MAR-2011

No. of s&mpl�� l0Cet;0ct 4 N<;. oi �a.rnpl% anulyoc•ct 4

Tr<i� report supe1sedes any pn:.vious f(Cpott(S) with Hlis referi�rtGe Re-su:ts ar>ply to the s.:�mple-(s) as su\1r:1it\ed. ,;11 pages (Jj thiS repo1t �1:.we bec�r1 (�necked and :Jpprowd lor

rdlc'�\Sf<. Tl'o�s Quality Control Report contw:s the foilowtng 1nlormation ·

¢> l.N,cm10'y C!':p\ic&\e (OU?r i<D)-Jor":: Rel<.1wte P01C<;:(l1c>ge \J,rtsrence (?..PO; ami ACC('P1l1f1C0 L n\its

® Me:tnod bl:,1nk (Mb) :md L::�t>cr.oto:y (:(>n:roi Sp<kt· (LCSi Rq:>ort R0,:ov-�'Y .gnd Acc<lPtanco UMs

IGI :;1iltr�x Spt<e i.\1S) Ro0oart: Recov''IY ;v-,c Acceop\i.lnce Lmt,ts '"'"'''"'''"'�'•'� '"'�'''"�"-''�--�---•�• """-�--·-•"•-ww�··•-••n*--""'-'--�·-'•,>M_M_ """"""""-"'""'-'"'"'-"''--'"""""--��""-�-•·---" •••·--'-•"""""'-�"'"" """""'�""'"'""'-""-""""' ___ "_"_"""'"'" '"' "-"""""""""��-"""" •

NATA NO'<·•' �!'�O�NI�•f'? ACCR!l:C�TATlON

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Th's document 's issued tn

accor<Jance with NATA

accredTtallon req\h·renwnt;;,

Acefed:ted fer compliance Mth

ISO/IEC 17025.

Signatories Ttits (J<)Cument ras been 10kcttcnicaliy signed by t�e authonx.ed $1\)natones mdLCaled bdovv. Eiedron:c St(Jn1ng has been

carried out in compliarv;;e with procedures spec1fled in 21 CFR Part 1 L

fN;f!l"��·ni•S Chas Tucker Cicelia Bartels

Po�'�'OI" Inorganic CMmist Metals Instrument Chem1st

;:.ccwd,win;m Ca1eqcx; Perth lnorganics Penh 1norgan1c.s

I'';Jq"'

'A<xK O<J.;r c:,cn:

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2 of 7 EP11C1'0-27 Amendmen1 1

ACE ENVIRONMENTAL. PTY LT:J J010·039

Genera! Comments T�f! :l11il';1<·;,$) ,?.·oa;;dwe� c<S0() o·1 the! E�Y-<<>n;n<:rl;>i Cw'�'o" �:<.1-Jt' b�en devdq,,ed !'I<Jm e�t;Jbld>ed <r<te!Mtlonol!y recogn,zcd ::Orcctodur.c�, guch «s :t,oc·,e p"f.lid1ed :;;y 1he L.'SEPt•. F·i"HA 1\S ;,r\'Cl !':O'Y)� h r·,o��\\

<JI!VdopcJd f!I'Oe<o•dcrr�s �'� �rnr.•luyc-<1 11'1 \lve Oli�Vnct> o( dOCUI'I<irnl�d t<l��d�r<JS Oi' by <::i,�·nl f'il(J�O-�t

\\'w1r� rno<�l�c<0 d,,�,11'1ln>;>t.o0 n<>:< b<'"n (l�·icrmed re�·ulb ue reprt0d on Cl ;:,·1· W'i"Jhl )')n''"'

\•';:'"'" o '�porWNly t;..o dC'io' to-"""'�� I'Opln ,;O<!ruc:/di�:JeO'W\<c �ll..tt!On :ond;or tnsufh·�-� ·o:.nn.clo hr ;.>'Only,,,,�

W�<OW \M LOR or <l reporkC:: r"su:t dl�h;n; \rcrn 'i:\andNd lOR. th<S :nay be (']''"' 1.0 'WJ�\ '1\Ciiltufb CGnkr:t. :ns"t:':G:"'nt S;Jm;-,!<J (roo:uoed w<:"i)h\ employ cO! or m<:l'nx ,n,ecf.,.�n:r>C'-'

K·,1y Ar,<l"'l'nO'.!O ·" Ruf,;,;� '<l S<ttn�>ic-� wh:Gh '""'-' not s:;,,c,h:a;ly p�!1 of tlw; WJI'k orctor l>ul (<:,:r�,1d pG<'t oi �11� QC prcceos 1'-11 c,:,s IJ""m"r '·' Ci\S 'O(Ttt\ti'Y �umbe1· fro"l �:>tBbil.><O n'-'l1nt�:l1ed o; GMm,�<>l Ah��m.ct& Serv<Gf�!l. TM Ctwn'''""l (\ilstwGt� Sc:r�IG� � � a d;vo'i,<0<1 ct tn� ,-".m<�>lC�n Ch"'rnc�l So,-,,,.�1 \.OR " L1�1,; of re;:>CI�W.g

RPD Rd.!!(<'<<; P"''o.'nwge Di:br1l!1f��

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Laboratory Duplicate (DUP) Report . ,.,_,. qc�e;i,ty COil\r-:>1 \8:'!!'1 lmX!r'ltory Ou�lrcc.:\l<e '•Jk\S �? s run�r;mJy 11<'k><;1("J u1t<illab::.raTo<y o·.;;hL L-aborale>:y ;;t\ld,Gal�'' ;;ro<'tde> :ntomvrMn 1C'SJUC\11rtQ <nd:":Od ,I)!C:<:.is<on <.tnd oa-�p!v h.:>ir�r·cgo�'"1'i ""I'"' pe:·m,,:�c,.;J r:

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for �11(· !'��l.atrw.> P,"rC•"�( Dc>:·<rC>�:cn (Rf>Di :of L.ai:orntcry 0\:picJ:os ,,,.,, s�r;,::t'IG·d u1 '"LS Methed OV·il--Et\:38w:cl 8fel depcnden\ on In<.> nugn:lc,dCl ot c.c·:.u::·o :n c:C"fop,;r:v:�n �o �!-,e it':vCI ot ro[Xlrnrq :��zc.l1 'iQ l:mc•; l.CR �,;o "'"a:. ?;cv.::, b0tW<>'-ln ',() "/� 20 �""'"·' l.OR.- G-,.�. · �O-% f�C%1t ,, <:O t>rh"t' �OR.- G%- 2(h'< ..

EP1101324-0C2 Anortymcus

, EGOZOA·F· Arser11C ' EG020A-F: Chrom;um

EG020A-F Copper EG020A-F lo�d EG020A-F _Manl!an:Sl:l

, EG020A-F· N<C>;el . EG020A-F· Zmc

EG020A-F· Alummium EG020A-F. Selen1um

:·EGOzoA·F· !ron 'EGozoA:·f. Cadm1um

EG020A-F. Arnemc EG020A-F: Chrcmrum

77$2-49-2: ,, ____ 7439-69-6 i

7440-43-9! ; ..

7440-38-2 i ..

7440-47-$''"'

0.001 mg/L 0.001 mgiL 0.001 mgiL 0.001 mg;L

06' mg!L 0.005 mgA. O.G1 mg/L 0.01 mg/L

0.05 mgiL

0.0001 mgll 0.001 mgiL

0.001 mg/L

L,,l<ot�l�ry D�plicMe (I./UP) R�pon.

6.54 '·" 0% " 20% 4.14 07 0%" 2.0%

0%- 20% 13�0 17.:; 0%" 20%

,, 0.0 No L'm't

" 00 No L1m1l

,, 0.0 No Lrm1t ,, 0.0 No Limn

" 0.0 0 % " 50% eo; ' 0 0%- 20%

" SA 0 % - 20% <1 00 No Lim•t

" 0%- ZO% "' o.s 0%- 20%

<0. 0001 0 0 No L<m'� <0,001 <0.001 o.o No Lim<l

<0,001 "<o.'O'oi" o.o No Lim't �o oo1 <O_Q01 o.o NoL,m;t <0.001 <0.001 00 No Ll1'l1Jl 0.007 0.007 00 No Llmrt

<0.001 <0.001 0_() No Lnut

<0.005 <0.005 00 Nolimft

0 02 0.02 00 No Llmlt

<0.01 <0.01 o o No Um1t

<O.OS <0.05 00 No b-mt

<O.OW1 <(!.COOt M NOL<mrl

<0.001 <0.001 0.0 No L<mrt

<0.001 <0.001 00 No Limrt

A c."· 'P'-"''-' 6ui,\cc; u"''""' C•. n�""Y

;�:.·y" 1Nor� OldcJ

C!·cm """'"''" 4 of 7 EP1101327 Amendment 1 ACE': ENVIRONMENTAL PTY L TO .lOt0-039

EG020A-F .

EG020A-F: Manganese EG020A·F: N<ckel EG020A-F Z1�C EG020A-F. Al<.!mrnrum

Ar�en<c EG020A-f· Chromium

EGC20f\.F: Copper ' EG02�A-F· �ead

EG020A-F _Manganese EG020A-F. Nlckel EG020A-F Zrnc

EG020A-F' Al<.!mrn<um

EG020A-F- Seler-1um

7�39-96-5 :· 0.001

7440-{)2-0 0.001 ' 7440-€6·6 0.005

7429-90-5 ' 0.01

C.001

0.001

7439-96-s !· c.oai

7440--02-C i 0 001

7440-6&-6 0.005

7429-90·51

7762-49-2 ' I

0,01

0.01

mgil mgiL

m•c

mgiL

mgrL

mg1L mg/L mg/L mgiL mgiL

<0.001 <0.001 0.013 0.02

<0,01

<0.05

<0.001

0.00&

<'0,00�

0.061

0.005

0,076

<Q.Q1

<Q_Q1

' EG020A-F' !ron 7439-89-B i 0.05 mgJL <O.OS

-l&r&lll\�llilRI.W'i'Vill-lll�llfll!lill!��l�lll' llllli''''IIW\IlWIIi'.WI/1TI'ill"'il!:C\1\II' '' ' '' •··· Wii&liiii:&'RI.�, liilllllllll)l\itl\llll1ltJill.B.\\'l&\1!Jiii'lif,,W\ . ik\iil '.1!kit1k$,QIQ-$fiL\io1�l)l(�>:-.¥:s-WN;\_;:_!)\i' ._., . . · '·'··

74�9--97-6} 0.0001 , mg/L -<0.000\ ... ' ''"'"\"li"�'II'�111W!i!IW�W'&''"!I''"'""'I'��'!'''''""' ·w , · � Willilli@lJl; Wif]KU11 •lf1ll)fiHil0 . \\;!· \ l\-)fft' �!�). '-''\'&'k! FiY1U>'·y, ,..,,_ ,.-.. __. ... • d4 ,. , ,K * . . �0 Hi) ·";:J},).ii M!it (,,,,�\1,,,,,,, '"''"""'"'"� ........ ,-c.· .. -EP110t324-00i Artcnymous EK05SG. Ammor1a as N 7064--41-7! o.ot mg1L 0.05

7664-41-7!

"'0.001

<Q.OD\ 0 ,01 3 0.02

<0.01

�0.05

0.0001

-<0.001

<0 001

0 009

<O.V01

OJ)$0

o_oos

0,075

<:0.01

�0.01

<0.05

<0.0001

0.04

0.12

9.07

a.os

0 9

1.5

"'"Q.'i.i' ' ·a,x: "2o%

0.0 N0 L1mt 0.0 No;_:mLI 00 �u L<m•t

0.0 Noum't 0 0 No L•mt

0 0 r--;o L,mt

0.0 NCl>mrt

00 No L:mt\ 0.0 No Lrm1r 0.0 NoL:mr\ 0 0 NOL1m1t 0.0 No L;mn

1.9 0%- 20% 0.0 No Lim<!

00 0%- SO%

0 0 NO Lim1t

0 0 NO L1m1t 00 No L;m:t

0.0 No Lim•\

0.0 No LLm<1

30.0 0 % . 50%

0.0 No L•mrt

0 0 No l>m>t

1A 0%- 20% o o No L<m,t

0.0 No L1m·t

0.0 0%- 50%

0.0 No Llmd

1()_6 0% - 50%

A (;".copiN.'l ih\'w;; L '>"!t'-J (;c,'''P�>''>'

PJ·)� 'XC<"� OrJ•Jt Ckc»� �''ra:,,�,

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J010-039

Method Biank {MB) and Laboratory Controi Spike [LC$) Report

! '"·'' qcwli\V c<;n'.rOI 1c;""' �,\,·;t;od L,JIJO'Gtmy 81;mk rd.:::•� to Jtr\ C<:HIVIc !:ee m.Jtrox 10 w�1,GI'\ all r<la')or·,O, ��·Q 3ddc;ct m \he g�rne •mivm<l� or ;;coprt:ons �$ UG�il ,n %'<M.J: CC p.,lr8n'"''": ;(, (V "nGrno: p(>ior:,-�1 !c1b<:nW,'t) C<lnWrnln:>\IOI'L 1't1� q;J.o!,ty GVt'ctrul t<?rm L,J.bO;<>tny C</\(rol Somplu n.CS; wrer� to a Cd1dl'io:l <U:Bc''"'c"' rnmen!.1!. 01 o. known ;nt.c,c,,,er,o.' tro<.'" rna�rv. o.p:�iJd '''"' '·'-''�;s•\ :.cn�l)';os. ·;·ne P'•<'PV''" o: \111� GC p!.lriln1e'k;' �� lo mon;tO( n'i>�Md ,-,,.;;c,s<or and nc,;,>raot t'ld.:Op�n,�ent o( sa:n9k mMnx. Dyn.'H'fl<C R'OGO·owy '-"POt:< are Mo.e·ct en swm;trc;JI ilVUiiJ<liton cf Pro-.c:.�>():l LCS. 3ur-�r,LW·x; WATER

C:aclm,um 7446.-13�'9 ' O.COC1 Chrom1um 7440-47-3 0.001

Co.oper 7440-50-8 0.001 0.001 0.001 o·:cm

Sclen<Um 7?82-49-2 :· 0.01

!EG020A-F' CadffiHJm 7440-43-$ 0.0001

:'2G02CA·F. Chromtum 7440-47-3 0.001 ;EG020A-f Coppfrf 7443-50-8 o:Oo1

"""""'"""'" '"'"'""''""""-"' '''"""'""'-"'" ''""" '"" "'" L,1�<>mmry Cor,r;ol SpiJ,·o (LCS) R�por: Sp�h R�C<>v<'fY (%j Raov'"Y �'"'"" (%!

" ;30

79.8 ij6

88.1 " "'

'70"" DO

e5 13.0

il:l."S" 7S ;so

" " "' . .

88.2 73 ; ; ; mgJL <0.0001 0.1000 mgiL " ' n 109

mgiL <O.OCi 0.100 rngiL "' " ; ; ; """ <0.001 0.100 mgll 97.8 73 \ 1 j

mgiL <0.001 0.100 mg/L 88.9 " '" mgiL <0.001 o.�OO mg/L "' 7? 107

mgJL <0 001 0.100 mg/L " ' 7S no mg'C ;,:c·:o; 0.10 mg/L 96.8 76 "'

" ' n 115 99.7 " "'

88.1 " "' 87.7 " ; ; ;

mgll �0.0001 0.1000 mg/L S6.5 n '" """ <O.GC1 0.100 m;;/L 006 75 ; ; ; ""

0.\00'fngll."

- <0.001 S8.6 " 1 1 1

-·--·-··--�-----�··---· ··------·-----· A C.1'n;>l'-�' i�·d."!�iO '-"''.!<'" C•Y"'P""I

P;y;<e Wct'r, ;)"okr Ci.cnt ."'m,vc.'

01"\:l•M:::t,.x,: WATER

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J010-%'9

98,1

'" '" ' "

"'

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"

B7.$

"

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123

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124

1.24

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J.\ Cs.'>ofJC'-':' ih-:'<lcCO �"'"'",� (.',y,-,H''f

p;,.y, 'f·,0rk C,J..,r (;l,•gq

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7 ol7 EP1-t01327 Amendment 1 ACE ENVIRONMENTAL PTY l TO

J0�0-03$

Matrix. Spike (MS) Reporl

'i're 'l'-'dld)' ccM'OI \\.<rrr; �\:;r�� S).>\k\� (rc1S) nd.,rs :o e<n n1ir->bborutory !,p\:l ''"''">Pk ;;p:ke<O w:1r, " <epno<>ent.:lt<VC. o�t (�1 t:J")N 8l1iJiyt�·�. Th� pu;po<;o ol tnr,; Z)C pnmmetor c$ \iJ mc�oW< potQn'.:i.\1 ,-:,?.tr�x utf·2c:� Or> OJ!\CJiyt,i• ru�'""'"-'''"�' Stat:c R•lO.WC.'"' l •• m:t� �' per iCJbor�:0;y ;')ilta Qual•:Y OD;'lc:w,,s .;:;cOs) lcWJI rc,cov�·ry r;mgu·.', ;;\3Hct m�y br.• war;·erJ >n e1o e�0N of NJ.�1pk m�tr<.� ;nt0rl¢k�C"

S�o-Matr;x: WATER

EG02CA-F Cadmn.rm

:EG020A-F: ChN,mium EG020A-F. Cop?e,r .. ,

....... 7446-so-s EG020A·F· Lead 7439-92-1 EG020A-F: Manganese -i4iS:S6·�s.

• " """"""" """"'' " '"'" " " '"""···· Mcc,c,C"C'.,"··,·,

,.,,.

{MIC

'II if

i C,·,"··,··,

"·""" '

o_zo'O' mg.il 0.2:i0 mgll 0.200m�IL

"' "' 9'5 ' " "' 95.1

EGOZC.".·f. N>CI;el 7440-02-0 0.200 mg/L 113 EG020A·F. Zmc 7440-66-6 , O . .:Wo mgiL j22 "1!1�1' ��g •. , 'il'l"w'll. �"1!1""''1"�·��,��1'&'''·1""''"'''"'''' ,. •····" >;� ' !m�lii! j • ' {{)\! !M(! � 'i'UI 11 '�M)'i' il<!• -��< '"'l '-·\h':J<; ,:,·.·:. .. ·,· 1' '®liiMl ' : · . . &1/ If\", l•iJi\rit&JL,11fi•l\tc\,·\\SH\i1fiLi·,,\iX:\\ <>L< · . . EP1101327-003 M803 :EG020A·F. Arsenic 7440.38-2 ' 0.2?0mg/.L 104

, EG020A-F: Ca\lm<L>m 7440-43-S 0.0500 mg/L 103 •EGC20A-f· O.romrurn

.. ..... i<i4i:i-47�3----· o:206 n1�C 86':$ EG020A·F: Copper

lead Man£lar>es_e

7440-50-8 7438-9:?.-1

"74s9:9e-s"

0.200 mg/L O.zoomgiL 0.266 mg1L

1Ci9 "' 75.9 1 \ 3 9!3.5

' "

80'3

·ns

'02

"'

f!�C<>v�ry LJmJW (%}

" no

" m

70 130 " 130 70 ' " 70 no " no 70 130 70 '" 70 no

70 130 " no " 130 70 '" 70 '" " '" " '" 70 130

70 "'

70 130

70 '"

70 1 30

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ALS Lalborator4 Group /\NALYTICAL CHEMISTRY & TESTiNG SERVICES


INTERPRETIVE QUALITY CONTROL REPORT

Wor� Ordor Ame,Himent

Ci<<'n\ Contac\ Addr()S'i

S-rn;:hi

1d€p1G0'>

F�<;•;rn111n

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gina@aceenvironmen\al.Com.au ,.61 08 9497 5001}

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Environmental Division Perth Scott James 10 Hod Way Malaga WA Australia 6090

[email protected] ,.61-8-9209 7655 +61-8-9209 7600

!iJ!Il\\''Yi'!N"pm ____ _

PrO;�GI J010-039 oc �"''d NEPM 1999 Schedule B(3) and ALS QCS3 requirement S<�<o C-0·C mi·:TI0"'

�)iJmpll'r

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o�o:;,:, nurn�d

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EP-163,10 BQ

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I%Uii tlJI<l 04-MAR-2011 22-MAR-2011

No. <;J! .SDr:1;1)('"$ 10C01Vild 4

No. of sarnples unal�s;,:,d 4 Tn<e; '"'port s�p�'<c<('d0� uny provrou� I'<JP(lrl($) w;ti; r.n<� r.o(erenc<!. l�e>ol�� WIY to tiK s'>mp!o(sj <>S �ubnwi1·�J. All p<>�<c5 "' �h,s !'€Pot: "'"'"' biJ0G cM,ck,;oo ill\d @pprovcd !or rdei.\�''

Thro1 lnt<'rpr;,;rwr Ocral,ty Control Report con�,ogns th'� 1oi!o-.,;ng ,nfo�cnatron

e Ar<lly"� Hoidsng Trnoe Comptr;,nce

e ·:hlt�dy Cop:n:li »11r:m1�'l'Y Freqw<cc.cy Complton<.:c

41 3nd M?:,ryod Sim·:manl':s

111 S\lmrllary of Ootii?<S

<Snut�o"'""'nt.J>I O>v•slon P.,rtn P:."1 d llk' AI.S L.:>bo�a:ton-< Group

: ') hO') ft�)' j.j,>[,�J 'NA AC')'iJkL 1/#J ;�\ <•t1.o,1CWYIM> FA< •0'·9· \;•O<, /';00 """"'·�'"'"'"""""'

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3 of8 EP1101327 Amendment 1 ACE ENViRONMENTAl PTY LTD

J01C-03S

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SWlll.l.>'(l<hO � - No,'tmg t,, ne ll-'""'"� ' '�''"''-'! �c,,','!i<:(! '''"'"

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01-APR-2011 OS..MAR-201 1

06-MAR-2011 \ 0:4·MAR·201 1

0:6-MAR-201 1

1 1 ·MAR-20:11

01-APR-201 l ./ 1 1 -MAR-2011

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Quality Controf Parameter Frequency CompJiance bt< :cl\cw;ng report <-ut'nr�:otno·.e� lC•& '""'�''�-�.C/ -:>\ 'abo: &toy CC �v;mpi<;s erwi;��eo ntt111n t�e aPolyt,cal lot(�,} "' wl\:ch the $�tbrnt:�·d s:>rrpi0\5) w:·J�I,wlwr�:) ptOC0%�d Act•Jal mle st:o"IC oe \VeDtcc �lwn or '"'<"ill to :hu

c<pL<;1�d '"1()_ A h>�-ng al oru;c>•o'.< t•1 prov1d�d rn \M Seit'nfn�r"f o( Oeiti>ers �:<>t<cx: WATER

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f.v�l�atr-cn � ·' Quc:�Uy Conl.rcl ;cequsncy not wrlhrq specrtrCil\IOn - Ct:<li•�Y Ccr:<r-�i fr,!<qur,ncy w.tf,,n sp,,(·(;c;...>�,,�,

�$.2 11.1 U3

12.5 12.5

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6 oi 8 EP1101327 Amendment 1

ACE ENVIRONMENTAL PTY LTO JOi0-039

Brief Method Summaries 'I" no Ofl.,liy\;·�:.1 p;cced\JCcs c·5cd 'c:i tt'->J En,rcnrn<JnDI Dtwo.or; r.ave bt<';ll <hOW-ioped from e•;,wbk.hn<l \f",bn13hcn<�Hv '"cogn,zed prcccc:ut,;os �'uch �� tho>'J P'J\:>L�l,cd �y \C\C US f:ro;, .c,PHc\, AS unci Ni:'.'' :Jl. in '>OCIS" 'k"''"lop<Jd ti'0(.�\1�180. ;,w <OmpicJy"d ''1 lho �b;x,ncc of ctc<;.uno(-m\<c·J �l:lnd;;,r¢s ex l)y Gi''''"' '�"i\H%1. "lhe !i)lioW;ni) 1epor! pr,:,vi<J,';S bn\;! d%cnptwns '!I \�c an<>IJ(IC'�I pmC,l(il.,rc:; o·l<"rp!CVed ''Y :o·,,),L; ''�;:.::rwd ,n \!1(; t;,•rt;t<cnl� ot An-;,ly��. Sc'"".::e\ I rom \Nh,cn /oLS fMthOds haw Oe&n d\lV8Ioped ilr<:l pmv1:.>ed w•tllm trw Mot0Cd 00SC:<9-:;Ms

, Total D1ssolved Sol:ds (High Level) '

'i AlKalinity by PC Titrator

i AC1d1ty as CalCIUm Carbonate

: Sulfate (Turbidimetric) as $04 2- by · Discrete Analyser

: ChiOncte· n;;· Dis.Crete AKiar/S

.er

..

.i iiSsotveii Metals bY 1CP-MS :s·u-ii·e A ...

t·o'issOiVed .. MerCury bY 'F1Ms

Arnmon1a as N by DIScrete analyser

Nitrite as N by Discrete Analyser

i'Nitiate as N by· Discrete Analyser

J Nitn\e and N;traie as N (i-!Ox) by Discrete (.Analy.ser i Total KJeldahl Nitrogen as N By Discrete :', At1.a1yser

--·EAot$1-l E0037-P

E003$

ED04lG

... Ec'64sG ...

EG020A-F

EGO:iSF

EKOS5G

E"Ko57G EKOS8G

EKOS9G 'EKos�G ..

WATER

WATER

WATER

WATER

WATER

4500 H+ B. Th1s procedure de!erm:nes oH oi water samo!es bv automated ISE . . • . coffipli,al1t INJtt: .. !:IE.P.M .. (1.9�.9) .':'.ch��ul!":.f3@. (�pp��: .. 2l.... · APHA 21st ed .. 2540C A gravimetric procedure that determines the amount of "filterable' residue in an aqueous . sample. A well-mixed sample is filtered through a glass fibre filter (12um). Ttle filtrate :s evaporated to dryness : .and dried to col)stant weight at 1 8.0""/:SC. This m<)lhod IS compl1ant with NEP¥ (1999) Schedule B(3) (Appdx. 2)

APHA 21st ed .. 2320 B This procedure determines alkalinity by automated measurement (e.g. PC Titrate) using ' pH 4.5 for indicating the total alkalinity end-point. This metnoct ts compliant with NEPM (1999) Schedule B(3) .. _\Appdx .. 2) .. . ... . . .. .. . . ... . . .. . , APHA 21st ed., 2310 B ACidl\Y is determ:ned by titra\lon with a standardiSed alkali to an end-potnt ph of $.3. ThiS , [llet);?_d)�-C�fnplia0t.�t�_N.J::f>".'! {19.�9)..Sch�dl;llf0. i?.\.3) .\1\PP.?:<·_ 2). i APHA21st ed., 4500-S04 Sulfate l(lns are C<lnvertecl to a barium sulfate suspens1on in an ace\!c acid med1um

w1\h barium chloride. light absorbance of the Ba$04 suspension is measured by a photometer and the $04-2 concentration is determined by comparison of the reading With a standard curve_ This method is compliant Wllh

.. L,_N �1;'10 ... \1.�?9L�<:�ed.�Je.f?;£3)_{jl,pp�:<.:.2) ..... -_...... ....... . ........ . ..... .... - .............. - ..... .... ... - .. . .. � APHA 21st ed., 4500 C!- G. The thtocyanate tOn is liberated from mercunc th10cyanate through sequestration ol i mercury by the chloride ion to iorm non·ionisect nwrcuric chloride.in the presence of ferne 1ons the libra ted ' thiocynate forms highly-coloured ferric thiocynate which is measured at 480 nm APHA 21st edition seal method 2

.... _·: CI.17:.1.:L.�p�1.20,{}3 """"""""'""'"'""""'""'" _,_ .. ....... - "·-·--....... ----................ - ......... ""' ......... ' ""' ....... '"'"'" '"'" """ """ "' '" "

WATER , (APHA 21st ed., 3125', USEPA SW846 - 6020, ALS QWI-ENJEG020): Sa:T.ples are 0.45 um filtered pr10r to ana!yS.1s. The ICPMS technique utilizes a highly eff1cient argon plasma to ionize selected elements. lo11s are then passed into a high vacuum mass spectrometer, Which separates tne analytes based on their distinct mass to

WATER

WATER

WATER

WAT.ER

WATER

WATER

�h<l[S.e,rati(l.S P.r.l?rYU��i.r_f!l_e<lsu.r_�.m.,,nt ,'Dy_ <�-�-i�.<;�et�.?Yr\,O_de_,ior� .. �etecto.�. .. ..... ..... ..... ... ... ·- .. , AS 3550. APHA21st ed. 3112 Hg - B (Flow-inJection (SnC\2)(Cold Vapour geflera\lon) AAS) Samples are 0.45 um filtered prior to analysis. FIM-AAS is an automated flameless atom1c absorption tecflnique. A bromate/bromide

' reagent is used to oxidise any organic mercury compounds in the filtered sample. The ion1c mercury IS reduced : online to atomic mercury vapour by SnCI2 which is then purged into a heated quartz celL Quantification is by ' compar'1ng absorbance against a calibration curve. Th1s method IS compliant with NEPM (199g) Sciledute 6(3) , {Appdx. 2) .... .... ..... .... .... .. .... ... .. . .. .. .. ... .. ... .. ·- . · APHA 21st ed., 450Q.-NH3 G Ammonia IS determined 'r:rj direct colorimetry by Discrete Analyser. This method is

...... co.rnpti�!lt..'J>i_�h.�N!�O_f'?.¥ .. �1-�?9L�S::t:�OlJJ�.§Q.l_ .. (Appdx.:..f) .............. � - ...... ....... .. .. .... .. .. .... ... . , APHA 21st ed .. 4500-NOZ- B. Nitrite is determined by direct co\ounmetry by Dtscrete Analyser. This method is

.compliant wrth. NEP.M (199.9) .S:chectule. B{_3) .(Appdx . . �l APHA 21st ed .. 4500-NO:.O- F. Nitrate IS reduced to nitrite by way of a cadmium reduCtiOn column followed by

' quantification by Discrete Analyser. Nitrite is determined seperately by direct colounmetry and result for Nitrate 1 calculated as the difference between the two results. This method is compliant w\th NEPM {1999) Schedule 8(3) : (Appdx. 2). ·- .... ... . .. . . . .. .. .. ... . . .. . ... .. .. .. .. . . ... .. .... ... .. : APHA 21st eel., 45DO-N03- F. Comtmed oxidised Nitrogen (N02+N03) is determined by Cadmium Reduction and

. _!, .dir.ec:t,c.ol�uri.l!lelrY..bY..Pis_cre.t<;J.h!1al�.e�._ .. T�.i_:> .. rll�\.h?� .. is. -�crr;pli,aD�V{i.th .t'/.EP.":l. _\ 1.?9?) ... �.c.he.�.ul.e ... B.@ \App�.x._.2) . APHA 21st ed., 4500-Norg D. 25ml water samples are d1gested using a traditional Kjeldaht digestion followed by ·. determination by .Discrete. Ana!ysl'!r, .. This me.thod is .compliant with NEPM .(1�99).Schedule 6(3). (Appdx. 2)

·''· Cu·"�""';; B!<CM'> !.ii0,1c'.l (;,:m;>"<'l

Pi10'-'

Aarf, O'd':"· Ckn '"'"JOC)

7 ol8 EP1101327 Ame'tdmen\ 1


J01C.039

Phosphorus as P By Discrete --Analyser

EKC67G WATER APHA 21st ed., 4500-P B&F ·n.;;s--prOcedure involves sulphuric acid digestion of a 100ml sample to break

; phosphorus down to orthophosphate. The orthophosphate reacts with ammoruum molybdate and ant1mony ' potassium tartrate to form a complex which is then reduced and its concentrat10n measured at 880nm usmg ... SJ.i��!�.t�_fy:�!y_��-: · .. I��-m�i�2�.!-� .... �?!0e!i_S:0� ... ��h��!:�J].�?91..?.�-�-�9.�.1� __ !3_\0l. (�Pp_t!x ••. . '.!..�········· ......... .

'1.(/'<):".T"·'"''" ' ' "'"""''""""

2)

Schedule

A C.!:''·"�'"!i i'ifuln&.'> L""''�'' ()"'""'"'>'

?clg,:

'•/or� Ord O:e·': �'m;x:

8 of8

EP1 1 C1327 Amendment 1

ACE ENVIRONMENTAL PTY lTD

JCi0-039

Summary of Out!iers

Outiiers : Quality Control Samples

1'1··u lol:ow,n<) 1�po11 l'lgtll'911ts -�utl:ers ti'19JO..:< !1 \i'k a�u!:ty Contcoi :OCj Rl.'po�'- Surro�n:e r<!Co""''l i1mns "'"' �,t;t,-� 2>1'\d ;:>a sod on USfPA S'fi8413 or ·"'L.S-Q'iVI!ECJ/3S (rn :n� c:t!s"'''�"' ct s��;;;,(lc USEPA � rc-.t�r T•,,s

Fti!)01\ (li>'J)ia�� OC C\l�h"s (biC::ilC��s.', or,Jy

D(iplfcates, Method Blanks, Labomto1y Control Samples and Matrix Spikes

Oe<ermmed MS recovery not detcrminm;J, background lov!ll greatllr than or <X;ual to 4:<: spike

"-•- ,_,,,,,,,..,,,,,,.,_,,_ ..... �.-· '""'' , , ,�, .. ..__,_, .. ,,.,, ,., -· '"""""'"'" ,, ,,, .. ... ......... ,_,.,.,,,, __ .. ................. "''"'"'"'-�'""""' �-.. -� .. --- " , . .................... ,,,� ................. '" , """' .......... "" '"""' , , ... __ .... _l?�.0��-, "''�·-- ,

0 For a!J matrices, no Method Blank vaJue- outliers occur,

s Fer aU matrices, no Duplicate o-utliers occur,

G For all matrices, no Laboratory Control outHers occur.

Regular Sample Surrogates

o For all regular sample matrices, no surrogate recovery ouWers occur.

OuWers : Anafysis HoJding Time CompJiance

Tr:;$ rqJ():1 1iWb·n Ho:dng T"'"' Ql'ec'>CG�·s <;dy Cnl·; 1hu n,sp()Ct•V\1 e.xU&ctron I PrupC<IG.(IO:.r· il:1r;J:or •O,r\�lys.s car:-·-�cMm i:<tu.nJ i:li�piC>ye�.

Mi\ti'Ot: WATER

Outliers : Frequency of Quality Control Samples

Tn,,• tolk:.-w1ng <'.Opon h>;f:i.gnts �omad:eC' :n (h" Fwqu�ncy of OuGil\; Contn;t S�mpl;;l'.

o No Quallty Control Sample Frequancy Outliers c;:o;lst.

.,,,-., "'' ;J,p, ·l>' .. li,'<c'(/ :;"•- '<-n :,,•p.-! Day.<

08-MAR.-;<011 04·MAR-20i 1 '

A C.;:r•!--'-"·' tbi!>t•,; (,,'""'"' C'c"C'P.ii\y

APPENDIX J

appendix h - der.wa.gov.au · table 2 sample sample identification date number assessment criteria...

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