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r Engineering Report for the
Kaieie Mauka Well (State Well No. 4708-03)
Papaikou, South Hiio, Hawaii
Submitta{ to:
Hawaii State Department of Health Safe Drinking Water Branch
Preparei by:
Tom Nance Water Resource Engineering 680 Ala Moana BOLk3vard . Suite 406
Honolulu, Ha~"aii 96813
On '.Beliaif I)f
Department of Water Supply County Of Hawaii
December 2002
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Engineering Report for the
Kaieie Mauka Well (State Well No. 4708-03)
Papaikou, South Hilo, Hawaii
Suomittaf to:
Hawaii State Department of Health Safe Drinking Water Branch
Preparea oy:
Tom Nance Water Resource Engineering 680 Ala Moana Boulevard - Suite 406
Honolulu. Hawaii 96813
On fJ3eftaif of:
Department of Water Supply County of Hawaii
December 2002
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I Tom Nance Water I Resource Engineering
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Professional Engineer Certification
The undersigned, being a registered professional engineer, certifies that:
1. He J{e/Sfre
has prepared the attached report and the information
contained therein is true to the best of
2. The water
His information and belief; and his/tier
produced by Kaieie Mauka Well (State Well No. 4708-03) , the name of source{s) [State 'Wt{{ 9{p(s).}
potable water system identified in the attached report, will comply with the State primary potable
water regulations contained in Hawaii Administrative Rules, Title 11, Chapter 20, Rules Relating to
Potable Water Systems, and will comply with the Rules and Regulations of the
Department of Water Supply, County of Hawaii , when said 'Department of 'Water supPfiJ, County of / 'lJoart{ of 'Water supPfiJ, City atttf County of !Jionofufu
drinking water system is operated and maintained in accordance with the instructions and information
contained in this report.
This work was prepared by me or under my supervision.
Tom Nance - President Tom Nance Water Resource Engineering
680 Ala Moana Boulevard, Suite 406 • Honolulu, Hawaii 96813-5411 • Phone: (808) 537-1141 • Fax: (808) 538-7757· E-mail: office@tnwre.com
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Table of Contents
1. General Information ................................................. . A. Project Description .......................................... . B. Name of Owner and Authorized Representative ...................... .
2. Physical and Hydrologic Characteristics of the Area ......................... . A. Location .................................................. . B. Climate ................................................... . C. Topography ................................................ . D. Geology and Foundation Conditions ............................... . E. Earthquake Considerations and Design Parameters ................... . F. Groundwater Conditions ....................................... . G. Flood Problems ............................................. . H. Conformance With Local Land Use Planning and Zoning Regulations ........ . I. Water Rights and Future Use by Others ............................ .
3. Extent of the Water Works System ...................................... . A. Nature and Extent of the Area to be Served ........................ . B. Population Served, Consumption Data, and Forecast Use ............... . C. Future Service Requirements ................................... . D. Provisions for Extending the Water Works System ................... . E. Required Capacity to Meet Fire Protection and Reserve Requirements ..... . F. Alternate Solutions Considered ................................. . G. Environmental and Economic Impact .............................. .
4. Potential Sources of Contamination ...................................... . A. Description of the Well Site .................................... . B. Design Well Draft ............................................. . C. Water Quality Data on Existing Wells in the Area .................... . D. Land Use Classification of the Surrounding Area ..................... . E. Existing or Potential Sources of Contamination in the Recharge Area . . . . . . .
5. Sources of Water Supply .............................................. . A. Nature of Soil Stratum Overlying the Aquifer ....................... . B. Probability of Contaminated Surface or Groundwater Entering
the Deep Aquifer ............................................ . C. Depth to Water Table and Location and Description of Wells in the Vicinity .. . D. Slope of the Water Table ...................................... . E. Potential Flooding or Earthquake Risk ............................. . F. Expected Water Quality or Quantity During Stress Conditions ........... . G. Factors Having the Potential to Contaminate or Reduce the
Quality of the Water Source .................................... . H. Alternative Control Measures to Reduce Contamination . . . . . . . . . . . . . . . . . I. Summary ................................................. .
6. Proposed Treatment Works ............................................ . A. Summary Description ........................................ . B. Site ...................................................... . C. Plant Facilities ............................................. . D. Basis of DeSign ............................................. . E. Water Disposal ............................................. . F. Operation and Maintenance ..................................... .
98-03
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Table of Contents (continued)
7. Pumping Facilities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ... A. Purpose of Service .....•..................................... B. Pumping Layout ............................................. . C. Flow Requirements .......................................... . D. Liquid Characteristics ........................................ . E. Electric Power ............................................. . F. Pumping Arrangement ........................................ . G. Selected Pump .............................................. . H. Buildings and Other Structural Improvements ....................... . I. Water Hammer Considerations .................................. . J . Features of Construction ...................................... . K. Electrical Power ............................................ .
8. Finished Water Storage ............................................... . 9. Water Distribution System ............................................ . 1 O. Financing ......................................................... .
Appendix
A Pump Test Data and Interpretations
B
C
o
Montgomery Watson Harza Laboratories Analyses
Data Regarding USGS Monitor Well No. 4708-02
Specifications and Plan for the Well Pump
List of Figures
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1 Location Map .................................................... . 2 Site Plan ....................................................... . 3 Past and Projected Water Use in the Upper Areas of DWS' Paukaa-Papaikou
Water System ................................................... . 4 Pump Control Building ............................................. .
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This report has been prepared to comply with Hawaii Administrative Rules, Title 11 in order to certify the Kaieie Mauka Well (State Well No. 4708-03) as a new source of drinking water. The well will replace Papaikou Spring to supply upper elevation areas of the Hawaii County Department of Water
Supply (DWS) system in Papaikou, South Hilo, Hawaii. The format of this report follows the Department of Health (DOH) Guidelines dated January 2, 1996.
1 . General Information
2.
A. project Description. Construction and pump testing of the Kaieie Mauka well was completed in August 2002. Design to outfit and connect the well to the DWS system is currently in progress. This design work includes the following elements: a 100 GPM,
50-horsepower submersible pump and motor in the well itself; an adjacent 0.10 MG reinforced concrete tank; a perimeter fence and other miscellaneous site work; and
upgrades of the Supervisory Control and Data Acquisition (SCADA) system at DWS' existing Papaikou tank and well sites. Figure 1 shows the location of the well at 1130-foot elevation in upper Papaikou. Figure 2 is a layout of the site showing the well and
new tank in relation to DWS' existing 0.02 MG tank which is presently supplied by Papaikou Spring. When the new well and tank are completed, both the spring and the
0.02 MG tank will be taken out of service.
B. Name of Owner and Authorized Representative. The owner and operator of the well and
its related improvements is the Hawaii County DWS.
Physical and Hydrologic Characteristics of the Area
A.
B.
C.
D.
E.
Location. The Kaieie Mauka well is at 1130-foot elevation on the eastern slope of
Mauna Kea. It is also directly upslope from the community of Papaikou in the South Hilo District.
Climate. Based on the nearest rain gages, mean annual rainfall at the well site is on the order of 200 inches and it is reasonably well distributed throughout the year.
Topography. The site of the well and new tank is relatively level. However, the
overall mauka-to-makai slope in the general vicinity of the well is approximately 10 percent.
Geology and Foundation Conditions. The well site sits on a prehistoric lava flow from the Mauna Kea volcano. Based on the strata penetrated during drilling of the well, the
residual soil is a stiff silty clay on the order of 10 feet thick. Below the soil layer is
about 140 feet of sapprolite followed by relatively unweathered lava flows. Foundation
bearing strength for the well pad and new 0.10 MG storage tank are excellent.
EarthQuake Considerations and Design Parameters. All of the Island of Hawaii is
classified as Seismic Zone 4. This earthquake risk is reflected in the appropriate structural design parameters.
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PROPOSED 100,000 GALLON TAN~ OVERFLOW EL.= 1146.50 FINISH FLOOR EL.= 1132.00
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Tom Nance Water esource Engineering
680 ALA MOANA BLVD., SUITE 406 HONOLULU, HAWAII 96813
(808)537-1141 FAX:(808)538-7757
CLIENT:
DEPARTMENT OF WATER SUPPLY COUNTY OF HAWAII
CLIENT ADDRESS:
345 KEKUANAOA ST., SUITE 20 HILO, HAWAII 96720
JOB TITLE:
DWS JOB NO. 98-711
KAIEIE MAUKA EXPLORA TORY WELL
TMK: 2-7-02:PORTION 3
SHEET TITLE:
SITE PLAN
SCALE:
1" = 40'
JOB NUMBER:
98-03
DRAWN BY:
GS
CHECKED BY:
GF
APPROVED BY:
TN
DATE:
NOV 2002
SHEET NUMBER:
FIGURE 2
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F.
G.
H.
I.
Groundwater Conditions. The well is located in the Onomea Aquifer System as
designated by the Commission on Water Resource Management (CWRM). This triangular-shaped, 180-square mile area extends along the shoreline from Hilo to
Pepeekeo Point and its inland end is at the top of Mauna Kea. The CWRM has set the
sustainable yield of this aquifer system at 147 MGD. The only known active well in the
aquifer system is No. 4706-01, DWS' Papaikou well located nominally downslope from
the Kaieie Mauka Well (its location is shown on Figure 1). DWS' present use of Well 4706-01 is on the order of 0.10 MGD.
Groundwater tapped by the Kaieie Mauka Well stands about 27 feet above sea level, is quite cool (660 to 670 F.), and has very low chlorides (less than 3 MG/L). Pump test
data are presented in Appendix A. Based on these data, a lack of a tidal response in
water level recordings, and the well's time-dependent drawdown and recovery, the
groundwater is not basal. Its source of recharge is far upslope where the rainfall is of lower temperature than near the coast.
It should be noted that a shallow, perched aquifer exists in the sapprolite at a depth of about 100 feet. Its potential yield is quite limited. This aquifer has been sealed off by
grouting the well's annulus so that it does not contribute to the water pumped by the well.
Flood Problems. No flooding of any kind at the site is expectable. The upslope area
tributary to the site is less than 5 acres in size. The site's 1130-foot elevation is far
above possible tsunami inundation.
Conformance With Local Land Use Planning and Zoning Regulations. The well is on land
designated Agricultural by the State and County (Zone A-20a). The well and related improvements are allowable uses for both State and County designations.
Water Rights and Future Use by Others. Well Construction and Pump Installation permits have been obtained from the CWRM. Since the Onomea Aquifer System is not a
groundwater management area, a water use permit is not required. The right to use the water accrues from ownership of the land on which the well is located.
Extent of the Water Works System
A.
B.
Nature and Extent of the Area to be Served. As indicated previously, the well will replace Papaikou Spring as the source of supply for upper elevation areas in DWS'
Papaikou System. This part of the service area is comprised of residences and small farms.
Population Served, Consumption Data. and Forecast Use. Water use in the portion of the
service area to be supplied by the Kaieie Mauka Well averaged 0.012 MGD in 1990 and
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C.
D.
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reached a peak of 0.017 MGD in 1997. A modest growth to about 0.025 MGD in Year 2010 is projected by DWS. Figure 3 depicts past use and DWS' projection of future use.
Future Servjce ReQujrements. Based on the historic trend of water use, only a modest increase in future years is expected. The 100 GPM pump to be installed has more than sufficient capacity for foreseeable service requirements.
Provisions for Extending the Water Works System. There are no plans to extend the
water system at this time.
Required Capacity to Meet Fjre protection and Reserve Requirements. With the new
0.10 MG tank, reservoir storage to provide fire flow rates for required durations for agriculture and single family residences will be met (500 GPM for 0.5- and 2-hour
durations, respectively). An analysis of the hydraulic capacity of DWS' existing distribution system is not a part of this project.
Alternate Solutions Considered. There are two possible alternatives to the Kaieie Mauka well. One is to provide treatment of the Papaikou Spring water. The other is to
booster pump from DWS' lower elevation Papaikou well (No. 4706-01). Costs and dryperiod shortfalls of the spring's supply rule out the first alternative. Costs, operational flexibility, and redundancy make the Kaieie Mauka well more attractive
than the second alternative.
Envjronmental and Economic Impact. There will be only minimal environmental impact. The well, tank, and related improvements will be constructed on previously disturbed land next to DWS' existing 0.02 MG tank. Construction, outfitting, and operation of the
well are obviously far more expensive than continued use of Papaikou Spring without
treatment. However, DWS views the expense as necessary to continue to conform to
DOH's Safe Drinking Water regulations.
Potential Sources of Contamination
A. Description of the WeI! Site.
(1 ) Coordinates (Old Hawaiian Datum):
State Well No. 4708-03 TMK 2-7-02: Portion 3
t9Q 47' 42" 155 0 08' 03"
Latitude / / Longitu~
(2) The well is at elevation 1130 feet. Figure 2 depicts the topography at the well site.
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0"1
30000
25000
5' 20000 a.. CJ ........ Q) CJ)
::::> .... 2 15000
~ Q)
~ Q)
~ 10000
5000
o 1990 1995
Figure 3. Past and Projected Water Use in the Upper Areas of DWS' Papaikou Water System
2000 2005
Year
2010
• ACTUAL USE -TREND OF ACTUAL USE -PROJECTED USE I
2015
30000
25000
20000
15000
10000
5000
o 2020
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B.
C.
D.
E
(3)
(4)
(5)
The catchment area for surface runoff is less than five (5) acres. Perimeter drainage swales will be installed to intercept and direct offsite surface runoff
around the site. The "catchment area" for groundwater tapped by the well
includes the undeveloped upslope area of Mauna Kea. It is impossible to know how much of this upslope area is in the contributing watershed. The mauka-tomakai slope of the ground surface is about 10 percent.
Strata penetrated in drilling the well consisted of: residual soil to a depth of
10 feet; sapprolite (weathered volcanics) for about 140 feet; and relatively unweathered volcanics to the full depth of the well at 1300 feet.
The depth of the well is 1300 feet. The depth to groundwater from the 1130-foot pad elevation is approximately 1103 feet.
Design Well Draft. The well will be used to provide the present and projected supply
requirements shown on Figure 3. It will do this with several pump cycles each day at
100 GPM during each tank infill cycle.
Water Quality Data 00 ExjstjOg Wells jo the Area. Water quality data on the Kaieie Mauka Well, based on samples taken by DWS personnel during the 5-day constant rate test and analyzed by Montgomery Watson Harza Laboratories, can be found in Appendix
B. The only other active well in the near vicinity is State No. 4706-01, DWS' Papaikou well, which is located downslope at elevation 369 feet. Its very low salinity water
(chlorides of 4 MG/L) is similar to the Kaieie Mauka well.
Laod Use Classificatjoo of the Surroyodjng Area. All of the surrounding land is in the
State Agriculture District.
Existjng or Potential Soyrces of Cootaminatjoo jo the Recharge Area.
(1 )
(2)
(3)
(4)
Extent of Contributing Recharge Area: There is no way to determine how far up the slope of Mauna Kea the recharge area extends, although the temperature
of the water suggests it may extend far upslope. Land uses include extensive
grazing, forest reserve, and little or no ground cover at higher elevations in the alpine zone. As far as is known, no one resides in the upslope area.
Type of Contaminants: A modest amount of animal waste is the only known source of contamination.
Distance to the Well: Some grazing by a few cattle takes place within about
500 feet of the well.
Method of "Disposal": Animal wastes deposited on the ground surface.
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(5) Depth from Contaminant Sources to the Groundwater Table: It is about 1100 feet from the ground to the top of the aquifer tapped by the Kaieie Mauka well. However, the shallow, perched groundwater aquifer in the sapprolite at a depth
of about 100 feet provides excellent natural protection. Contaminants
percolating downward would be intercepted by and retained in the shallow aquifer. They are not likely to reach the deep aquifer tapped by the well.
Sources of Water Supply
A. Nature of Soil Stratum Overlying the Aquifer. As described previously in Sections 2.0. and 4.A.(4), the residual soil is about 10 feet thick, the sapprolite (weathered
volcanics) extend to about 140 feet, and relatively unweathered lava flows exist below the sapprolite. Video logging of the borehole showed no fissures or faults. In fact, with
very few exceptions, the formations looked extremely "tight" over the full depth of the borehole and the actual yield of the well was a pleasant surprise.
B.
C.
D.
Probability of Contijminated Surface or Groundwijter Entering the Deep AQuifer. The
thickness of the sapprolite, the existence of a shallow, perched groundwater body
within this sapprolite, the almost complete absence of fractures in the lava layers below, and the 1100-foot vertical travel distance make contamination of the deep
aquifer highly unlikely. The extremely low nitrate value in the well water, for
example, indicates a lack of contamination from animal waste or even natural decomposition of vegetation in the Forest Reserve upslope.
Depth to Wijter Table and Location and Description of Wells in the Vicinity. As stated previously in Sections 4.A.(5) and 4.E.(5), the depth to groundwater tapped by the well
is 1103 feet. There are only two drilled wells in the general vicinity:
(1 )
(2)
No. 4708-02 is a nearby 4-inch diameter USGS monitor well. Due to what appears to be faulty construction of the well, the water level in the well stands 145 feet above sea level and there was no water level response in it during the
pump test of the Kaieie Mauka well (refer to Appendix C for additional information).
No. 4706-01 is an active DWS well which is nominally downslope and 1.9 miles
from the Kaieie Mauka well.
Slope of the Water Table. There are insufficient data to determine a slope of the water
table. The initial static level in Well 4706-01 was 21 feet. Compared to the 27-foot
level in the Kaieie Mauka well, a slope of 3.2 feet per mile is suggested. However,
intervening and as-yet unidentified geologic structural control could make this
computed 'slope" meaningless.
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F.
G.
H.
I.
Potential Flooding or Earthquake Risk. There is absolutely no potential for flooding of the well site due to surface runoff or tsunami. With regard to earthquake risk, all of the island is classified as Seismic Zone 4. This risk is reflected in structural design
parameters.
Expected Water Quality or Quantity During Stress Conditions. Although there is no
operating history with the Kaieie Mauka well, the extensiveness of the recharge area, natural protection of the deep aquifer, and the minimal anticipated draft of the well
suggest that its quality and quantity will not change during stress conditions such as an extended drought.
Factors Having the Potential to Contaminate or Reduce the Quality of the Water Soyrce. As indicated by the previous descriptions in Sections 5.A, 5.B, and 5.F, there are
really no factors which have the potential to contaminate or otherwise reduce the quality of water pumped by the Kaieie Mauka well.
Alternative Control Measures to Reduce Contamination. No such measures are warranted.
Summary. The nature of the groundwater occurrence, the lack of development in the recharge area, and the pristine quality of the aquifer's water as shown by the data in
Appendix B all indicate that this well will continue to provide water meeting drinking water standards for the foreseeable future.
Proposed Treatment Works
A. Summary pescription. The only treatment will be the injection of chlorine into the pipeline from the well pump to the new 0.10 MG tank.
B.
C.
D.
E
F.
~. The chlorination facilities will be located inside the control building. The location of the building is shown on Figure 2. Figure 4 is a layout of the building itself.
Plant Facilities. A gas chlorinator with two 150-pound cylinders and automatic
switch over will be used.
Basis of Design. The chlorination system will be set to produce a chlorine residual of
1.0 PPM in the 100 GPM discharge rate of the pump.
Water Disposal. There is no wastewater stream associated with the chlorination process.
Operation and Maintenance. The feed rate of the chlorinator is manually adjusted.
Maintenance of the system will include regular replacement of the chlorine cylinders,
inspection of the system components, and measuring the chlorine residual.
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I~
~ CONTROL ROOM
1= CHLORINATOR
PUMP AND eX)
I STORAGE ROOM eX)
MOTOR CONTROL
I CENTER o
I~
~ = CHLORINATOR CHLORINE ':.t
ROOM STORAGE I eX)
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V V I
SIDEWALK~
11' -0" 8'-0" 6'-8"
PUMP CONTROL BUILDING SCALE: 1/4" = 1'-0"
FIGURE 4 PUMP CONTROL BUILDING
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Pumping Facilities
A.
B.
C.
D.
E
F.
G.
H.
I.
Purpose of Service. The well has been developed to replace Papaikou Spring as the
source of supply for upper areas of DWS' Papaikou system.
Pumping Layout. Layout of the well and related improvements are shown on Figure 2.
The pipeline from the pump to the tank will be 4-inch.
Flow Reguirements. Present and projected supply to be provided by the Kaieie Mauka well are depicted on Figure 3. Both the 100 GPM pump capacity and the 0.10 MG reservoir storage substantially exceed design standards for present and projected use.
Liguid Characteristics. The well pumps extremely fresh and cool (670 F.) water.
Electric Power. Power for the 50 horsepower submersible motor and other
miscellaneous electrical requirements at the site will be provided by extending HELCO's
three-phase power up Kaieie Road to the well site.
Pumping Arrangement. The pump will be automatically started and stopped by a level control switch in the new 0.10 MG tank.
Selected Pump. Pump plan and section drawings, as well as data on the selected pump, can be found in Appendix D.
Buildings and Other Structural Improvements. A 17' x 25.7' control building, 15-foot high reinforced concrete tank, and well pump pad are the structural elements of this
project.
Water Hammer Considerations. Owing to the negligible above ground pressure in the pipeline from the well to the tank, water hammer is not a design consideration for this pipe. Water hammer in the well pump's column pipe is handled by column check valves
installed at locations specified by the pump manufacturer.
J. Features of Construction. All improvements will be completed in a single phase of construction.
K. Electrical power. Power will be provided by HELCO. There are no plans to provide a generator for backup power in the event that HELCO's service is interrupted.
Finished Water Storage
As indicated previously, a new 0.10 MG, reinforced concrete storage tank will be constructed.
When completed, the existing 0.02 MG tank will be taken out of service.
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Appendix A
Pump Test Data and Interpretations
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Fax#SD.182
Torn Nance Water I Resource Engineering
Original I!f will 0 will not
be mailed to you.
September 3, 2002 02/397 (98-03)
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MEMORANDUM
TO:
,FROM:
SUBJECT,:
Shari Komata - DWS
TomNance~ ..
FAXED S£P - 3 2DD2
Pump Test Results for the Kaieie Mauka Exploratory Well, DWS Job No. 98-711
This memo and its attachments present and analyze the data compi/ed during the August 22nd step-drawdown test and August 26 to 30 constant rate test of the Kaieie Mauka Well. In general, the well's hydraulic capacity and water quality exceeded expectations.
Data Collection
Water Levels. Water levels were measured in two ways, with an airline and ,with a downhole pressure transducer (Solinst LT-15 Levelogger). Water levels measured with the more accurate
pressure transducer' are used for the analyses herein. In addition to the pumped well, a pressure transducer was installed in the nearby USGS Monitor Well to record its water levels.
Flowrate. Flowrate was determined with a 4-inch, propeller-type Water Specialties meter with an accumulating, gear-driven swing arm.
Temperatyre. Temperature was periodically measured with a HACH Sens/ons 5 meter and was also recorded at 1-minute intervals downhole with the Sotinst LT-15 Levelogger.
Water Quality. Periodically collected samples were measured for conductivity with the HACH
Sensions 5 meter and analyzed for chlorides by mercuric nitrate titration. DWS collected samples for the laboratory analyses required for Department of Health certification of' the well. These results are not yet available.
Step-Drawdown Pump Test on August 22, 2002
The step test was run' at three rates for about 45 minutes at each rate. The water level recorded during, this test is shown on Figure 1. On Figure 2, drawdown at the three rates has been
fitted to a curve which can be, used to predict drawdown at flowrates other than those tested. Data for
the fitted curve are tabulated below.
680 Ala Moana Boulevard, Suite 406 • Honolulu, Hawaii 96813-5411 • Phone: (808) 537 -1141' • Fax: (808) 538-7757· E-mail: office@tnwre.com
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Memo to: Shari Komata September 3, 2002 -- 02/397 Page two
Step Test Data
Flowrate Drawdown (GPM) (Feet)
185 0.36 288 0.69 385 1.02
Fitted Curve
S = AQ2+BQ
where: S = Drawdown in Feet Q = Flowrate in GPM A = 3.526 X 10-6
8 = 1.322 X 10-3
1'2 = 0.98
The initial, step-drawdown test demonstrated the following hydraulic characteristics of the well:
• The static water level stands between 26 and 27 feet above sea level. This is about 117 feet lower than in the nearby USGS Monitor Well.
• Drawdown and recovery were very, rapid and no time-dependent component of drawdown was
evident. These characteristics are typical for a well which taps basal groundwater rather than for wells which draw fr-om a high level groundwater compartment typically have a time
dependent drawdown. • The well is capable of producing water at far greater rates than tested. Drawdown at 700 GPM
would be less than three feet, for example.
• As shown on Table 1, the water pumped is cool (an average of about 67.5° F.) and has a salinity similar to high elevation rainfall (chlorides are less than 3.0 MG/L).
Constant Rate Pump Test From August 26 to 30, 2002
After an initial electrical problem was eliminated, a 96-hour constant rate test was run/from about 2:00 p.m. on August 26th to 2:00 p.m. on August 30th at an average rate of 366 GPM. The
recorded water level prior, during, and following this test is depicted on Figure 3. The recorded downhole temperature is shown on Figure 4 and the coincident water level in the USGS Monitor Well is shown on Figure 5. These data demonstrate the following performance characteristics:
, • Other than the semi-diurnal water level change due to barometric pressure, there was no time
dependent component of drawdown or recovery. As with the step test, this response is more typical of basal rather than hig~ level groundwater.
• Drawdown averaged about 0.9 feet throughout the test.
• • •
The downhole temperature varied between 67.0° and 67.8° F. and averaged 67.5° F. The extremely low salinity of the pumped water did not change throughout the test (Table 1).
There was no water level response in the USGS Monitor Well to pumping of the Kaieie Mauka Well.
A-2
I I I I I 1 1 1 1 1 1 ·1 I I 1 1 1 1 I
(
Memo to: Shari Komata September 3, 2002 -- 02/397 Page three
USGS Monitor Well
(
Water in the USGS Monitor Well is not 1he same as in the aquifer tapped by the Kaieie Mauka
Well. The water level is 117 feet higher in the USGS well; its level did not respond to pumping in the Kaieie Mauka Well; its level response to a passing storm is not indicative of· a true groundwater response (Figure 6); and its water temperature is more than two degrees lower than in the Kaieie
Mauka Well (compare Figures 4 and 7). Based on this, the effort and cost to continue having the USGS monitor the water level in this well would be more appropriately directed elsewhere.
Sizing of the Permanent Pump for the Kaieie Mauka Well
The Septel11ber 1999 engineering report prepared by TNWRE indicates that only a small, 50 GPM pump with a new 0.05 MG tank is needed to meet forecast demands in the immediate service zone.
In view of the well's actual capacity, DWS may want. to reassess the pump capacity and tank size.
Attachments
A-3
I I I I I I I I I I I I I I I I I I I
( (
Table 1
Temperature, Conductivity, and Chlorides of Pump Test Samples From the Kaieie Mauka Exploratory Well
Step Test Samples:
Day in Sample Flowrate Temperature Conductivity August 2002 Time (GPM) (0 F.) (~S/cm)
22 14:25 185 67.9 115
22 15:10 288 67.2 113
22 15:55 385 66.8 113
Constant Rate Test Samples:
Day in Sample Flowrate Temperature Conductivity August 2002 Time (GPM) (0 F.) (~S/cm)
26 14:00 367 67.7 114
20:00 367 67.6 113
27 02:00 367 67.6 113
14:00 367 67.5 112
20:00 367 67.6 112
28 02:00 367 67.5 112
14:00 367 67.5 112
29 02:00 367 67.4 112
14:00 367 67.4 112
30 02:00 367 67.4 112
14:00 367 67.3 112
A-4
Chlorides (MG/L)
2.7
2.6
2.6
Chlorides (MG/L)
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
2.6
::J en
27.50
27.25
27.00
:2 I- 26.75 ill ill l..L. '--'
ill 26.50 > ill ....J a: ill 26.25
~ 26.00
25.75
25.50
I-
I-
I-
13
.~
FIGURE 1. WATER LEVEL RECORDED DURING THE AUG. 22, 2002 STEP TEST
~1l~
~~ l00 ~('M ~"CRM. ..... " ;. t:.f~1!'A.. --. .,.~
". ,.,-
A~ ~~ I~ "
, •
~. rJI.t. I
~ , 'WV' ~
il • ..A~ 1rJ' A
V ' I"~ Y ~
V ~
. . . 13.5 14 14.5 15 15.5 16 16.5
HOUR OF THE DAY ON AUGUST 22, 2002
» I
01
A'
I I I I I I I E m
~ :l
~
~
~ [ "
I I I I I I
3.0 0
2.7 5
2.5 0
2.2 5
2.00
~ 1.75
w !:!:.. z ~ 1.50 Cl
~ Cl 1.25
1.00
0.75'
0.50
0.25 V
•.. ~ 0.00
o 100
( (
FIGURE 2. HYDRAULIC CAPACITY OF THE KAIEIE MAUKA WELL BASED ON THE AUG. 22, 2002 STEP TEST DATA
/
/
/" V
200
y I
/ V
JI'
/ /
300 400
FLOWRATE (GPM)
500
• DATA POINTS --FITTED CURVE I
600
A-6
3.00
2.75
2.50
2.25
! /
V 2.00
1.75
1.50
1.25
1 .00
0 .75
0 .50
0 .25
O. 00
700
FIGURE 3. WATER LEVEL IN THE KAIEIE MAUKA WELL AUGUST 23 TO 30, 2002
27.50 r---T--I---i----r-----r---.,-----...,------.
27.25 r---I---t--~---l-~;-+---+---~---l--~
27.50
27.25
27.00 r---:1;~-:ii-;iA~::--t=-\--t-+---+---+---J--J---3 t 27.00
::::J C/) ~ 26.75 r---I---t----t-tH--+----+~-~+----l--l~ 0> 0>
LL
26.75
'"-"
0» 26.50 r----I---I---+-1H-+--~-+---_+---~---L-J 0> t 26.50
..J .... ~ 26.25 r---~~--T---t--HK-~--'----+---+---~--L~ > t 26.25
26.00 1---j-~--+----4---U---~ 11'--~ 26.00
25.75 r---l---t---t---+---+---+----J---~ t 25.75
25.50 .~.l..U£.WLU.LU.L~wu.u.wu.u.ww.&Jluu.wu.w.wu.w.ww.i.wJu.w.ww.u.u:...uwL.u.u.wJ.IW.U.LLLLU.IJu.w.LLLLU.I.LLW.LIwL.LLW.LI.u.u.w.u.u.wLWWLWJJ.LLuJ 23 24 25 25.50
26 27 28 . 29 30 31
Day in August 2002
» I
.....
_ _ .. r""I r""1 t~":j ..... ~ ~_.)'.MI_- - --- --
FIGURE 4. DOWNHOLE TEMPERATURE IN THE KAIEIE MAUKA WELL
68.5 f ~
68.0 ~ 1
~.5f I~
LL 67.0" I ." l' . (!) w £:) ~ 66.5 r---------~--------i-~------1---------+---------+---------~--------~--------J ::>
~ 66.0 w ~--~~~~~~~~~~-+----~------~----1-----~ a.. :::iE w I- 65.5 r---I---r-----.Jr--ff-t---:--t----+----+---~--L-i
65.0 ~ I. U "-\t4it .. ,,~ .. ·~-t_~,M ~
645 ~ I 1
29.5
29.0
28.5
28.0 @' :::iE I-w
27.5 ~
-' w >
27.0 ~ a: w I-
26.5 ~
26.0
25.5
64.0 ~ ttl t t t t t t t t t , tIt t t t , , t t t , , I , , , , , t , , , t , It,!, , t t , , , , It, , , , , t , t , t I, t"'" I,!" , , ~ 25.0
~ M ~ ~ V ~ 29 30 31
DAY IN AUGUST 2002
I~TEMPERATUR-E u_ .. WATERT-EVEC]
---,
~
,.. I
00
_-----~~~Li~--------
144.5
144.0
......... -1 (J)
~ 143.5 w w 1L --1
~ 143.0 w -1 """" ~ ex: w I-~ 142.5 -1 -1 W ~ (J) 142.0 CD (J) ::>
141.5
141.0 23 24
FIGURE 5. WATER LEVEL IN THE USGS MONITOR WELL DURING THE KAIEIE MAUKA PUMP TEST
.-. - -t~c..:
~-- -- --fO 1'i ff: t9F ~~
~~ ~""
.... , .......... ,a. JI/II\. ....... , .... r"P:".....- .. ~. J'I'III .........
25 26 27 28
DAY IN AUGUST 2002
- ... --- - ~
,..
~~ . ..... . .JJ ..'
29 30
I~USGS MONITOR WELL =-KAIEIE MAUKA WELL I
28.5
28.0
:::J Cf)
~
27.5 tu w !:S -1 W > 27.0 w -1
a: w J-«
26.5 ~
~ ::> « ~
26.0 !:!:! . w « ~
25.5
25.0
31
---."
-.,\
» I
<0
_ _ _ _ _ _ f"'""l r-1 C1 t~~oj t!!J .. .. - - - - - -
160 [
155 t ........ ....I
FIGURE 6. WATER LEVEL AND TEMPERATURE IN THE USGS MONITOR WELL JUNE 14 TO JULY 5,2002
I~
I. .. ::1 ::r-] 66.25
j 66.00
CJ) 150 :2: t 11\ . . II ] 65. 75 ~ f-ill W u.. -....I 145 w > ill ....I a: w ~ 140 s:
ill o .......
~ , , '- . I I I ~ 65.50 ~ ~ 1 ~. . , ~
ill a.. :2:
65.25 I=!
135 t T \ ] 65.00
130 t ' 1 64.75
1~ 1~ 1~ 1M 1~ 100
JULIAN DAY IN YEAR 2002
I-LEVEL -TEMP I
.--..,
-----
» , o
F1P"'1P"'1 ...... P"'I,....,,....,,....,F1,....,r"'1P"'1 ........ P"'I ........
FIGURE 7. WATER LEVEL AND TEMPERATURE IN THE USGS MONITOR WELL AUGUST 26 TO 3D, 2002
144.3 r-------------~--------------r--------------r------------~r-------------~
144.2 r------i------~t----:-----'--+-------~------J 144.1
....... 144 r---~---= ..... --I CJ)
~
ffi 143.9 r---------.:I-------t-------i-------~~~-----J ---~ 143.8 t----------.jf---I:----::----L w -I cr: W
~ 143.7 t-----I-I-UiII.
143.6 r---~~---t---------r-----------~-------~---------J 143.5
143.4 r--------~r-----------t-------+-------~-----------A
65.7
65.6
65.5
65.4 u::-(9
65.3 ~ ......-w a:
65.2 :::> ~ a: w
65.1 a. ~ w I-
65.0
64.9
64.8
64.7
30 31
I--WATER LEVEL -TEMPERATURE I
> , ......
.~
I I I I m
~
~
[
L [
[
[
t &
I I I ~
Appendix B
Montgomery Watson Harza Laboratories Analyses
I I I I I
[
[
[
[
I I I
DEPARTMENT OF WATER SUPPLY • COUNTY OF HAWAII
Mr. William Wo g, P.E., Chief Safe Drinking Water Branch Department of Health State of Hawaii P.O. Box 3378 Honolulu, HI 96801
345 KEKUANAOA STREET, SUITE 20 • HILO, HAWAII 96720
TELEPHONE (808) 961-8050 • FAX (808) 961-8657
November 25, 2002
KAIEIE MAUKA EXPLORATORY WELL LAB RESULTS
The following are the Kaieie Mauka Exploratory Well test results with the corresponding test method to the right (SM stands for Standard Method) for water quality parameters performed by our laboratory perso:QIlel. Mr. Oren Tsunezumi and Mr. Warren Sako conducted testing at the well site on September 25, 2002, at 1545 hours.
Conductivity (Field): pH (Field):
. Temperature (Field):
114.3 j.lS/cm SM2510B 7.98 SM4500-H+B
I8.8°C SM2550B
Please call Mr. Keith Okamoto or Ms. Mae Kise at the Department of Water Supply, Microbiology Laboratory, at (808) 961-8670 for more information if needed. .
Sincerely yours,
e~'E' Manager
MK:sco
copy -k. Greg Fukumitsu, Tom Nance Water Resource Engineering
." ''''', ".""~' or:," .' . ': , •. , ...... te· \ ' •• _ •. " ••.• ' ..... ' ",,·,~\·'O. ',. "'" .-~ .. , .. "-""''''~'''''''''' .,., .. ',-,". , .. -
B-1
r'l r,
DEPARTMENT OF WATER SUPPLY MICROBIOlOGICAllABORAfORY - 889lElLANI ST., HllO, HI 96720
Potable Water Sampling, Processing and Analyses Record Membrane Filtrotlon Ma/t;~ For T!1!J Do:, ;tion of Coliform Bllcteria
Audited by ...!!l.- on
Total Coliform Verification (LTBIBGLB) Total Sample
lab Point J.D. SampJin Number Number I/. Sample location f)/I
~~.2>qA1l"~ ~ 7'lSf ~CRd: .,.,..~ -"N' '7 /"'-tmu-
t:;f)vJ 'Pe'M0I\I 1
5O..,.Jl 1C"--1)N V
/(flC..
~.I""'" / .. c,.. .... 797S"
~iZ; 7'f!7r
tItIA.:;;. "/is-,,...::J .AGNII.:. '$f tI>.-7>to..
Collect {}.. ~-ed by ~ Dale If; Time/f ~
RefinqulShed by c:'~ Date S-/-rt..t.;;me IjI.;;>.s-Recefvedby t!2,~ ~ate tflH'/"LTime ljt";;{; Relinquished by ________ Date Trme __ _
Received by ~ate Time __ ._
Temp. Conlrol: Inilial ~ DC Final ___ DC
Sample Type Codes: RTE - Routine
RPT - Repeal
RPl • Replacement
S·Speciai
Membrane Filter ugend: o - No paat24houn, + - (lu at 241iours
g Residual Sampie Q -No ... at48~, (±) - Gu at 48.bours
Fecal Coliform Verif. Bacteria
Chlorine Type Sheen Non-8heen (BC) (No.lIOOmL)
1 2 3 4 5 6 7 8 9 10 ;Ufw ..s
'-,-v-n:- <9/9 4:1/6) <9/. 6>/1!$) 4>/$ ~
1'P7t:/ 4!9/<p G>/GP +7+ GPAlP $7_ , ~ D 0> 0 .c:!:) 0 c:!!) <£> to ~ cO
. ,/1;>.1,......
I /(,. / I~ I I¥" 7 It.
I~ /11> 1$'/16
-;;:1' v_ r;-/.r7;} 7.iA » 1$.$ ItS~ "~.S" :;"1ee>
f' I$';nil.S1~ 3'f7.7:$ ;~
'., ". .. ,:;;;. .. ".
7
. oale~nme I~()O -"""'F---r'-- Date I) (.. Time~ 3(,J.; 4 5~ 6~
¥l1fr~L!'l':::it S, aureus Ct lCW"M
Reported by_il __ 10.r..I.t '1 Dale .r$~;L. Time ~ ~. -
Verification:
lnocutated~-~..&..c Date -r~ Time /~ Readat24hrs.·by O. ~ . Date ~p..t4-Time "cn.~ Read al48 hrs. bY a· 7tr:Z"I: Date ;f/ • ., £-.L. Time 1~-H#::1' Conlrols: l TB (E. coli) 't l TB (S. aureus) 0
BGlB (E. coli) -I- BGlB (S. aureus) _-",0,--_
EC (E. coli) -I- EC (E. aerogenes) _0 __
No. Samples
Syslem CoUecled Reported by 1o ____ 0ale Time ___ _
Reported bY ____ 10 ____ OaI9 ____ Time __ _
Remarki: ~--------~------------
(MFCOU' 12127(01)
OJ I
I\)
.. r1
COUNTY OF_ HAWf\II DEPARTMENT OF WA"TERSUPPLY
MICROBiOlOGICAL LABORATORY- 889!LEIlANI ST .• HILO. HI 96720 Potable Water Sampling. Processing and Analyses Record
Membrane Filtration Method For The Detection of ColIform Bacteria
S8II1lIe Lab PointlD. SaJTClIIng
Number Nurriler Sample Location Time
~ K/Ttt?lf? ~w7f"'t?.u.y i/S'lFS' t.)¢<.-
2)/.r -==- IJJ./
8""f
p}( So-~ 7. 'f't! gJ
n.w- /'8',1 Cn-P<Jc,,,,,,..,,, .. 114 ~
~'PI7'Y- 0.<3/ ~-..G.s-~~S~ .....
CoIlectecJ by o.~CJ Date 1'/st'".. lime I~ ReI1nqu1shed by o·-,;r " Date 'Ift""- lIme..&L.CL Received by c:f'~""'-<!"'?7'= Date 9br',..... lImeiYL Relinquished by Date lIme __ _
Received by Date lime ___ .
Temp. Control: Initial IJ 6 ·C Anal ~ ·C
Sample Type Codes: RTE - Routine
RPT -Repeat
Rema'*s: pl1 '1..0::; '-/," I f'if ..,. <9 ,.. "7. '" I
,5t.,,.., ... ~2~c>
pu £.t:J.O":.. /0 •• 0
RPL - Replacement
S -Special
Audited by
• Total Colifonn VerifICation (L TBlBGLB) Total
Membrane AHer Lqpd; 0-No .11124....... • + - Goo 1124h0llll Fecal Cofrfonn Residual S,. G-NoPSII<4lhDOl'l, (J) -Goo II 48 hOllll Verif. Bacteria Chlorine Type Sheen Non-Sheen (EC) (NoJlOOmL)
1 2 3 4 5 6 7- 8 9 10 d.,iJ~ S D , I~ -.<'i:£. .:\ None Fauna
'-
!-
1
! i !
~ /
! ,
PreM!p!IYe~ ./ ~ InocuIat~ omeqfffi V" 11me /" .).:~ Inoculated by ________ Date nme __ _
Reedby~ omeo/'/¢~nme Ill;}';) Reedat2<4h1s.by Date nme __ _ Controls: 1 __ 2 __ 3 __ <4 __ 5 __ 6 __ Reed 8148 his. by Date nme __ _
E. coli S. IIU'eUS Controls: LTB (E. coli) L TB (5. aureus) ___ _
Rep(rted by ___ 10 Dale nme BGLB (E. coli) BGLB (5. aureus) __ _
EC (E. coli) EC (E. aerogenes) __ _
No. Samples
Svstem Collected Reported Reported by ___ 10 ___ Date ___ nme __ _
ReportedReportedby ___ 10 ___ Date ___ nme __ _
(MFCOU - 12117/99)
I I I I I I I·' ,.
[
[
[
I I I I
555 East Walnut Street Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Laboratory Report
for
Hawaii Department of Water Supply (Hilo) 25 Aupuni St.
DATE OF ISSUE
OCT 1 0 iOOZ
MWH LABORATORIES
Hilo , HI 96720
Attention: Mae Kise Fax: (808) 961-8759
HDS Hillary Strayer Project Manager
~ ,.... 1-~ Q<"
Q,:- ~ (.) -(.) -I
< ~
01114CA
Report#: 100134 PHASEV
L.IIJoratory certifies that the test results meet all NELAC requirements unless ~ed in the Comments section or the Case Narrative. Following the cover page ~re Comments,QC Report,QC Summary,Data Report,Hits Report, totaling 44 page[s].
8-4
1'11\ RtftWhI-h..a~rat~t·i9::"'1 r-1 ~HJ::")J <r:'1 Ct;JTt::JYf'J:ce~A[t?~'1 A '~';"14 I~ .("'00" (3r '\UII MONTGOMERYWATSONHARZA {
~:~~~~~~E:~1101 FGlNCO~~ri" __ """-"""-::-==~::INBY;-""" -~~:=.:I (800) 566-5227 SAMPLES RECEIVED DAY OF <;sALECnON? (check for yes) !
Fax: (626) 568-6324. BLUE ICE: FROZEN \.,/pARTIALLY FROZEN THAWED I ........................................................................................................................................................................................................................................ = ............................................................ = ............................. ;;::::::; ................................. : TO BE COMPLETED BY SAMPLER: (check/or yes)
~"',..c ~AMDII:~ 1"1'" ,_ ... _ •••• ___
ITAT requested: t--STD 1 week 3 day 1 day COMPLIANCE SAMPLES REGULATION: -- -- I--
- Requires state forms (SDWA, PhaseV, NPDES, FDA, ... )
I,..",,~ • ~ll , UTILITY or PROJECT: ip.o.# I PROJECf JOB #: REFER TO ATTACHED BOTTLE ORDER FOR ANALYSES 0 (check for yes)
ANALYSES REQUIRED (mark an 'X' in all tests required for each sample line) :A MPI .F.1t c.u" ..,.J) NAME AND ..,.u,,~. V~.
Warrell ~iak()~ .an Oren Tsunezumi V'1",c-. --z- SAMPLER
~~ r.;l * COMMENTS
~~ SITE NAME or IDENTIFIER or STATE ID # ~ ~ ~ <Q LOCATION U
~ ~
, ·'i· ::~:.
;,,;~ CLIENT: DEPT. OF WATER SUPPLY N(J fE: D ~E ~O I tECE IPl Of j./ l-L_ AMI ~J:R r::IA t<:~ mTTLES FOR COUNTY OF HAWAII
NEW SOURCE TESTING =-= =-= !, ~S!. ~~ I.~[ ,.~! I"'IHI .... ~O~: ,. Fe ~~} ~~ III F, ~~~ BE ADVISED PROJECT: KAI EI E MAUKA .. ,. !, ...... .. ,
SITE NAME: VI • ~ ... ~ .... .' _. rr:v / "T/ ~c.J •
EXPLORATORY WELL . .... - -~ .. .. , ..... ft. " I ..... , .. , ............. ,. .....
, /' 7' roc 801 ITlE • "'j\ ~Du ~ , PI U" ~u ,~ ~UU.L' .LUI1I\L SAMPLE DATE: p'::'; :-;..-
SAMPLE TIME: '·5~ B EXl RA T( BE US ED ~ ADDITIONAl II 1'1::' i:'UI SAMPLER: ,,/. .,c
~ SAMPLE TYPE: GRAB -- -, .-\1 ~'4 L,.
* MATRIX TYPES: Reported b~ YO!llme: sw = Storm Water RepW1~d b~ W ~ight:
RSW = Raw Surface Water FW = Other Finished Water WW = Other Waste Water ~~DNNED RGW = Raw Ground Water CFW = Chlor(am)inated Finished Water CWW = Chlorinated Waste Water
DATE TIME
C-O-C# ____ _ PAGE __ OF __
I I I I I
10-1 S - 02 A 10: 5 4 IN wJI MWH Laboratories
555 E. Walnut St., Pasadena, CA 91101 PHONE: 626-568-6400/FAX: 626-568-6324
ACKNOWLEDGMENT OF SAMPLES RECEIVED
Hawaii Department of Water Supply (Hilo) 25 Aupuni St. Customer Code: Hilo, HI 96720 PO#: Attn: Mae Kise Group#: Phone: (808) 961-8670 Project#:
Proj Mgr: Phone:
HAWAII Contract 98-2,PHASE II/V 100134 PHASEV Hillary Strayer (800) 566-5227
The following samples were received from you on 08/30/02. They have been scheduled for the tests listed beside each sample. If this information is incorrect, please contact your service representative. Thank you for using MWH Laboratories.
lamPle# Sample Id Matrix Sample Date Tests Scheduled
8·6
~~~ __________________________ T_e_s_t __ A_c __ r_O_n_ym ___ D_e_s_c_r_1_'p __ t_i_o_n ____________________________ __
Test Acronym Descriptiori
',' " .::::=::-: : :: ::: :::::::: .,' ........ :.:::
.=-= .. :~:~:.:~r~~~\:/ .;:::::::.:::~t . .... :::.: .. :::.: .. :.:.:.::
ENDOTHAL :\F(:""" GLYPHOS
NI-MS Nickel, Total, ICAP/MS
I - 1 -
~- Hawaii Department of Water Supply (Hilo) I 25 Aupuni St. Customer
Hilo, HI 96720 Attn: Mae Kise
Code: PO#:
Phone: (808) 961-8670 Group#:
Project#: Proj Mgr: I
Phone:
18-13-J2 A1J:54 l~
HAWAII Contract 98-2,PHASE II/V 100134 PHASEV Hillary Strayer (800) 566-5227
I Test Acronym Description
I I I I
Test Acronym Description
' ..
- 2 -
8-7
I I ·1 I I· I I Ii .'
I I I I I I
Report Comments #100134
555 East Walnut Street Pasadana, Galilomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 BOO 568 LABS (1 BOO 568 5227)
Group Comments
Analytical results for D1613SUB are submitted by Pace Anallytical, Minneapolis,MN HAWAII #SLD.
(QC Ref#: 180788) Test: 2-Butanone (MEK) (ML/EPA 524.2) QC Type: RPD Les
Trichlorofluoromethane recovered above QC limit in MS and MEK MSD not replicated to required precision. Defaulted to second LCS.
Test: Fluorotrichloromethane-Freon11 (ML/EPA 524.2) QC Type: MS
Trichlorofluoromethane recovered above QC limit in MS and MEK MSD not replicated to required precision. Defaulted to second LCS.
(QC Ref#: 182826) Test: Hexachlorocyclopentadiene (ML/EPA 525.2) QC Type: MS
Recovery low bias.
Comments - Page 1 of 1
8-8
I!" .... ' . Iij
I I I I ralYZed
555 East Walnut Street Pasadena, catlfornia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo)
Mae Kise 25 Aupuni St. Hilo , HI 96720
Sample# Sample ID
Laboratory Hits Report #100134
Samples Received
30-aug-2002 15:52:15
Result UNITS MRL
8-9
I 220B300156 KAIEIE MAUKA EXPLORATORY WELL
09/14/02
19/03/02 9/05/02
09/12/02
_9/04/02
'. 9/03/02 B/30/02
09/03/02
m
I I I I I I
2,3,7,B-Tcdd 1613 Drinking Wtr Alkalinity in CaC03 units Calcium, Total, ICAP Chromium, Total, ICAP/MS Fluoride Lab pH Nitrate as Nitrogen by IC Specific Conductance
I ~
SUMMARY OF POStTIVE DATA ONLY.
SUB PACE 55 9.B 1.9 0.10 B.1 0.19 11B
None mg/l mg/l ug/l mg/l Units mg/l umho/c
Hits Report - Page 1
1.000 1.000 1.000
.050
.001
.100 4.000
of 1
I 1 I 1
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 lABS (1 800 568 5227)
Hawaii Department of water Supply (Hilo)
Mae Kise 25 Aupuni St. Hilo I HI 96720
~repared Analyzed QC Ref# Method Analyte
1 J-j j -J 2 AI 0 : :5 S • )8·10
IN lJP/v
Laboratory Data Report #100134
Samples Received
08/30/02
Result Units MRL Dilution
~IEIE MAUKA EXPLORATORY WELL (2208300156) Sampled on . 09/03/02 00.00 180164 (SM2320B/E310.1) Alkalinity in CaC03 units 55
08/28/02 14:00 mg/l 1.0 1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
09/04/02
1 1 I 09/05/02
1/05/02
/05/02
09/05/02
105/02
05/0.2
I I
09/12/02 12.02 180911
09/12/02 12.02 180918
09/12/02 12.02 180915
09/05/02 13.54 180301
09/12/02 12.02 180917
09/09/02 00.00 180539
09/12/02 12.02 180928
09/12/02 12.02 180907
09/14/02 00.00
09/03/02 13.54 180178
09/11/02 00.00 181106
09/04/02 00.00 180336
09/09/02 00.00 180574
09/21/02 15.30 181453
09/12/02 12.02 180906
08/30/02 13.04 180265
08/30/02 13.04 180266
09/12/02 12.02 180921
09/03/02 00.00 180192
09/12/02 12.02 180919
09/12/02 12.02 180912
09/12/02 12:02 180920
10/03/02 00:00 182826
10/03/02 00:00 182826
10/03/02 00:00 182826
10/03/02 00:00 182826
10/03/02 00:00 182826
10/03/02 00:00 182826
EPA/ML 200.8
EPA/ML 200.8
EPA/ML 200.8
ML/EPA 200.7
EPA/ML 200.8
SM4500CN-F
EPA/ML 200.8
EPA/ML 200.8
ML/S2510B
ML/EPA 548.1
SM4500F-C
ML/EPA 547
EPA/ML 245.1
EPA/ML 200.8
ML/EPA 300.0
ML/EPA 300.0
EPA/ML 200.8
Arsenic, Total, XCAP/MS
Barium, Total, XCAP/MS
Beryllium, Total, XCAP/MS
Calcium, Total, XCAP
Cadmium, Total, XCAP/MS
Cyanide
Chromium, Total, XCAP/MS
Copper, Total, XCAP/MS
2,3,7,8-Tcdd 1613 Drinking Wtr
Specific Conductance
Endothall
Fluoride
Glyphosate
Mercury
Nickel, Total, XCAP/MS
Nitrite, Nitrogen by XC
Nitrate as Nitrogen by XC
Lead, Total, XCAP/MS
S4500HB/E150.1) Lab pH
EPA/ML 200.8 ) Antimony, Total, XCAP/MS
EPA/ML 200.8
EPA/ML 200.8
Selenium, Total, XCAP/MS
Thallium, Total, XCAP/MS
525 Semivolatiles by GC/MS ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
2,4-Dinitrotoluene
alpha-Chlordane
Diazinon
Acenaphthylene
Alachlor
Aldrin
NO
NO
NO
9.8
NO
NO
1.9
NO
SUB PACE
118
NO
0.10
NO
NO
NO
NO
0.19
NO
8.1
NO
NO
NO
NO
NO
NO
NO
NO
ND
ug/l
ug/1
ug/l
mg/l
ug/1
mg/1
ug/l
ug/l
None
umbo/cm
ug/l
mg/l
ug/l
ug/l
ug/1
mg/l
mg/l
ug/l
Units
ug/1
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
1.0
2.0
1.0
1.0
0.50
0.025
1.0
2.0
0.0000
4.0
5.0
0.050
6.0
0.20
5.0
0.10
0.10
0.50
0.0010
1.0
5.0
1.0
0.10
0.050
0.10
0.10
0.050
0.050
1
1
1
1
1
1
Data Report - Page 1 of 7
,... i...
I I I
Prepared
9/05/02
09/05/02
~9/05/02
~9/05/02 9/05/02
09/05/02
m9/05/02
W9/05/02
09/05/02
m:;::;:: 09/05/02
09/05/02
119/05/02
iW9/05/02
09/05/02
,,/05/02
~/05/02 09/05/02
~/05/02
~;::;:: 09/05/02 n/05/ 02 .
W/05/ 02
09/05/02
1/05/02
;, /05/02
/05/02
09/05/02
1/05/02
/05/02
09/05/02
1/05/02
/05/02
I I
555 East Walnut Street Pasadena, Callfomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of water Supply (Hilo) (continued)
Analyzed
10/03/02 00:00
10/03/02 00:00
10/03/02 00: 00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/.02 00: 00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
QC Ref!!
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
182826
Method
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/SPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
Analyte
Anthracene
Atrazine
Benz (a) Anthracene
Benzo(a)pyrene
Benzo (b) Fluoranthene
Benzo(g,h,i)Perylene
Benzo(k)Fluoranthene
Di(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Bromacil
Butachlor
Caffeine
Chrysene
Dibenz(a,h)Anthracene
Di-(2-Ethylhexyl)adipate
Diethylphthalate
Dieldrin
Dimethylphthalate
Dimethoate
Di-n-Butylphthalate
Endrin
Fluoranthene
Fluorene
gamma-Chlordane
Hexachlorobenzene
Hexachlorocyclopentadiene
Heptachlor
Heptachlor Epoxide
Indeno(1,2,3,c,d)Pyrene
Isophorone
Lindane
Methoxychlor
Metribuzin
Molinate
Metolachlor
1 0-1'3 - J::: A 1 0: 55 I ~1
Laboratory Data Report #100134
Result Units MRL
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
0.020
0.050
0.050
0.020
0.020
0.050
0.020
0.60
0.50
0.20
0.050
0.050
0.020
0.050
0.60
0.50
0.20
0.50
10
0.50
0.10
0.10
0.050
0.050
0.050
0.050
0.040
0.020
0.050
0.50
0.020
0.050
0.050
0.20
0.050
8-11
Dilution
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Data Report Page 2 of 7
I I I
555 East Walnut Street Pasadena. California 91101 . Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo)
10-13-02 Al0:56 IN
Laboratory Data Report #100134
8-12
(continued)
1-------------------------Prepared
109/05/02
09/05/02
~9/05/02
!~9/05/02 9/05/02
09/05/02
~9/05/02 ~9/05/02
09/05/02
[
[
[
[
E ~8/31/02 08/31/02
1/06/02
09/06/02 1/06/ 02 '
I I
Analyzed
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
10/03/02 00 :00
10/03/02 00:00
10/03/02 00:00
10/03/02 00:00
QC Ref#
182826
182826
182826
182826
182826
182826
182826
182826
182826
Method
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
ML/EPA 525.2
Surrogate
Surrogate
Surrogate
Aldicarbs
Analyte
trans-Nonachlor
Pentachlorophenol
Phenanthrene
Prometryn
Propachlor
pyrene
Simazine
Thiobencarb
Trifluralin
l,3-dimethyl-2-nitrobenze
Perylene-d12 (70-130)
Triphenylphosphate
09/13/02 00:00 181018 ML/EPA 531.1 3-Hydroxycarbofuran
09/13/02 00:00 181018 ML/EPA 531.1 Aldicarb (Temik)
09/13/02 00:00 181018 ML/EPA 531.1 Aldicarb sulfone
09/13/02 00:00 181018 ML/EPA 531.1 Aldicarb sulfoxide
09/13/02 00:00 181018
09/13/02 00:00 181018
09/13/02 00:00 181018
09/13/02 00:00 181018
09/13/02 00:00 181018
09/13/02 00:00 181018
09/05/02 00:00
09/05/02 00:00
09/06/02 00:00
09/06/02 00:00
09/06/02 00:00
180689
180689
180572
180572
180572
ML/EPA 531.1
ML/EPA 531.1
ML/EPA 531.1
ML/EPA 531.1
ML/EPA 531.1
ML/EPA 531.1
Surrogate
Baygon
Carbofuran (FUradan)
Carbaryl
Methiocarb
Methomyl
Oxamyl (Vydate)
BDMC (70-130)
Diquat and Paraquat ML/EPA 549.2
( ML/EPA 549.2
Diquat
Paraquat
EDB and DBCP by GC-ECD ML/EPA 504.1
ML/EPA 504.1
ML/EPA 504.1
Surrogate
Dibromochloropropane (DBCP)
Ethylene Dibromide (EDB)
1,2-dibromopropane (surr)
l,2-dibromopropane(60-140)
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
90
81
103
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
103
NO
NO
NO
NO
NA
NA
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
It Rec
It Rec
It Rec
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
, Rec
ug/l
ug/l
ug/l
ug/l
%R
t Rec
MRL
0.050
1.0
0.020
0.50
0.050
0.050
0.050
0.20
0.10
2.0
0.50
0.70
0.50
2.0
0.90
2.0
2.0
1.0
2.0
6.40
2.0
0.010
0.010
0.0000
Dilution
l.
l.
l.
l.
l.
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Data Report - Page 3 of 7
I 555 East Walnut Street Pasadena. CaHfornia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
I Hawaii Department of Water Supply (Hilo)
I (continued)
Prepared Analyzed QC Ref# Method Analyte
I 1It9/10/02 09/14/02 00,00 181471
1t9/10/02 09/14/02 00,00 181471
09/10/02
IU/10/02 i '9/10/02
09/10/02
E:~~:~:: 09/10/02
09/14/02 00,00 181471
09/14/02 00:00 181471
09/14/02 00,00 181471
09/14/02 00,00 181471
09/14/02 00:00 181471
09/14/02 00:00 181471
09/14/02 00:00 181471
09/10/02 09/14/02 00:00
1t99//1100//0022 09/14/02'00:00 I. 09/14/02 00:00
181471
181471
181471
181471
181471
181471
09/10/02 09/14/02 00:00
1(9/10/02' 09/14/02 00:00
~/10/02 09/14/02 00:00
[
I I I
09/10/02 00:00
09/10/02 00:00
180788
180788
09/10/02 00:00 180788
09/10/02 00,00 180788
09/10/02 00:00 180788
09/10/02 00,00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
Herbicides by 515.3 ( ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
ML/EPA 515.3
Surrogate
2.4.5-T
2.4.5-TP (Silvex)
2.4-D
2.4-DB
Dichlorprop
Acifluorfen
Bentazon
Dalapon
3.5-Dichlorobenzoic acid
Tot DCPA Mono&Diacid Degradate
Dicarnba
Dinoseb
Pentachlorophenol
Picloram
4-Nitrophenol (qualitative)
24-D(70-130)
Regulated VOCs plus Lists 1&3 (- ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
1. 1. 1. 2-Tetrachloroethane
1.1.1-Trichloroethane
1. 1. 2. 2-Tetrachloroethane
1, 1, 2-Trichloroethane
1.1-Dichloroethane
1.1-Dichloroethylene
l.l-Dichloropropene
1.2.3-Trichlorobenzene
1. 2. 3-Trichloropropane
1.2.4-Trichlorobenzene
1.2.4-Trimethylbenzene
1.2-Dichloroethane
1.2-Dichloropropane
1. 3. 5-Trimethylbenzene
'/ ()-l J - 0 2~j U: 56 I N
Laboratory Data Report #100134
Result Units MRL
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
98
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
NO
ug/1
ug/1
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
t Rec
ug/l
ug/l
ug/l
ug/1
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
0.20
0.20
0.10
2.0
0.50
0.20
0.50
1.0
0.50
0.20
0.080
0.20
0.040
0.10
1.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
8-13
Dilution
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Data Report Page 4 of 7
I I I
555 East Walnut Street Pasadena, Calilomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hila) ( continued)
Prepared Analyzed QC Ref# Method Analyte Result
[
r: ~
I I I
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00,00 180788
09/10/02 00,00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/E~A 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
ML/EPA 524.2
1.3-0ichloropropane
p-Oichlorobenzene (1.4-DCB)
2,2-0ichloropropane
2-Butanone (MEK)
o-Chlorotoluene
p-Chlorotoluene
4-Methyl-2-Pentanone (MIBK)
Benzene
Bromobenzene
Bromomethane (Methyl Bromide)
Bromoethane
cis-1,2-Dichloroethylene
Chlorobenzene
Carbon Tetrachloride
cis-1.3-Dichloropropene
Bromoform
Chloroform (Trichloromethane)
Bromochloromethane
Chloroethane
Chloromethane(Methyl Chloride)
Chlorodibromomethane
Oibromomethane
Bromodichloromethane
Oichloromethane
Di-isopropyl ether
Ethyl benzene
Oichlorodifluoromethane
Fluorotrichloromethane-Freon11
Hexachlorobutadiene
Isopropylbenzene
m-Oichlorobenzene (1,3-0CB)
m,p-Xylenes
Methyl Tert-butyl ether (MTBE)
Naphthalene
n-Butylbenzene
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
ND
ND
NO
NO
NO
NO
NO
NO
NO
NO
NO
Data Report
Laboratory Data Report #100134
Units
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
uS/1
uS/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
MRL
0.50
0.50
0.50
5.0
0.50
0.50
5.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
0.50
3.0
0.50
0.50
0.50
0.50
0.50
0.50
0.50
3.0
0.50
0.50
8-14
Dilution
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
Page 5 of 7
I I I
555 East Walnut Street Pasadena, CaliFomia 91101 Tel: 626 566 6400 Fax: 626 566 6324 1 600 566 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hila) (continued)
J- 1 3 - 0 2 Al 0 : 56 I i~
Laboratory Data Report #100134
8-15
I------------------~-----Prepared Analyzed QC Ref# Method Analyte Result Units MRL Dilution
I----------------------~-09/10/02 00:00 180788 ML/EPA 524.2 n-Propylbenzene NO ug/l 0.50 1
I'J ... ". I)
rP/ 04 / 02
~/04/02 09/04/02
1/04/02
/04/02
/04/02
09/04/02
1/04/02
/04/02
09/04/02
1/04/02
/04/02
I I
09/10/02 00:00 180788 ML/EPA 524.2 o-xylene NO ug/l 0.50 1
09/10/02 00:00 180788 ML/EPA 524.2 o-Dichlorobenzene (1,2-DCB) NO ug/l 0.50 1
09/10/02 00:00 180788 ML/EPA 524.2 Tetrachloroethylene (PCE) NO ug/l 0.50 1
09/10/02 00:00 180788 ML/EPA 524.2 p-Isopropyltoluene ND ug/l 0.50 1
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/10/02 00:00 180788
09/06/02 00:00 180522
09/06/02 OO:UO 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
09/06/02 00:00 180522
ML/EPA 524.2 sec-Butylbenzene NO ug/l 0.50 1
ML/EPA 524.2 Styrene NO ug/l 0.50 1
ML/EPA 524.2 trans-1,2-Dichloroethylene NO ug/l 0.50 1
ML/EPA 524.2 tert-amyl Methyl Ether NO ug/l 3.0 1
ML/EPA 524.2 tert-Butyl Ethyl Ether NO ug/l 3.0 1
ML/EPA 524.2 tert-Butylbenzene NO ug/l 0.50 1
ML/EPA 524.2 Trichloroethylene (TCE) NO ug/l 0.50 1
ML/EPA 524.2 Trichlorotrifluoroethane(Freon NO ug/l 0.50 1
ML/EPA 524.2 trans-1,3-Dichloropropene NO ug/l 0.50 1
ML/EPA 524.2 Toluene NO ug/l 0.501
ML/EPA 524.2 Total THM NO ug/l 0.50 1
ML/EPA 524.2 Total xylenes NO ug/l 0.50 1
ML/EPA 524.2 Vinyl chloride (VC) NO ug/l 0.30 1
Surrogate
Surrogate
Surrogate
1,2-Dichloroethane-d4(70-130) 108 , Rec
4-Bromofluorobenzene(70-130) 102 , Rec
Toluene-d8(70-130) 97' Rec
SDWA Pesticides ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
PCB 1016 Aroclor
PCB 1221 Aroc1or
PCB 1232 Aroclor
PCB 1242 Aroclor
PCB 1248 Aroclor
PCB 1254 Aroclor
PCB 1260 Aroclor
Alpha-BHC
Alachlor (Alanex)
Aldrin
Beta-BHC
Chlordane
NO
ND
ND
ND
ND
ND
NO
ND
NO
NO
ND
ND
Data Report
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
ug/l
0.070
0.10
0.10
0.10
0.10
0.10
0.10
0.010
0.050
0.010
0.010
0.10
Page 6
1
1
1
1
1
1
1
1
1
1
1
1
of 7
I I I I
555 East Walnut Street Pasadena. C8t1lomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
prepared Analyzed QC Ref# Method Analyte
9/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
19/04/02 09/06/02 00:00
9/04/02 09/06/02 00:00
9/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
19/04/02 09/06/02 00:00
9/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
m9/04/02 09/06/02 00:00
F 9/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
[9/04/02 09/06/02 00:00
9/04/02 09/06/02 00:00
09/04/02 09/06/02 00:00
[:/04/02 09/06/02 00:00
,. /04/02 09/06/02 00:00
[ III""
L
I I I I
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
180522
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 508
ML/EPA 50S
ML/EPA 50S
ML/EPA 508
ML/EPA 508
-ML/EPA 50S
ML/EPA 50S
ML/EPA 508
ML/EPA 50S
ML/EPA 50S
ML/EPA 50S
ML/EPA 508
ML/EPA 50S
Surrogate
Surrogate
Chlorthalonil (Draconil,Bravo)
Delta-BHC
P,P' DDD
p,p' DDE
p,p' DDT
Dieldrin
Endrin Aldehyde
Endrin
Endosulfan I (alpha)
Endosulfan II (beta)
Endosulfan sulfate
Heptachlor
Heptachlor Epoxide
Lindane (ganuna-BHC)
Methoxychlor
Tetrachlorometaxylene (surr)
Dibutyl chlorendate (surr)
Toxaphene
Dibutyl Chlorendate(70-130)
Tetrachlorometaxylene(70-130)
: ':, -] 3 -C) 2 Ai ') : 5 5 I N
Result
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
NO
S4
104
Laboratory Data Report #100134
Units MRL
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l 0.010
ug/l, 0.010
ug/l 0.010
ug/l 0.050
'R 0.0000
'R 0.0000
ug/l 0.50 , Rec , Rec
8-16
Dilution
l.
l.
l.
1
1
l.
1
l.
1
1
1
1
1
1
1
1
1
1
Data Report - Page 7 of 7
I I I
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo)
8-17
1:;-18-02 A10:56 IN~J Laboratory
QC Summary #100134
C Ref #180164 - Alkalinity in CaC03 units Analysis Date: 09/03/2002
I 2208300156 KAIEIE MAUKA EXPLORATORY WELL
~C Ref #180178 - Specific Conductance Analysis Date: 09/03/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
Ic Ref #180192 - Lab pH Analysis Date: 09/03/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
I " QC Ref #180265 - Nitrite, Nitrogen by IC Analysis Date: 08/30/2002
D ' ,~
2208300156 KAIEIE MAUKA EXPLORATORY WELL
DC Ref #180266 - Nitrate as Nitrogen by IC Analysis Date: 08/30/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
QC Ref #180301 - Calcium, Total, ICAP Analysis Date: 09/05/2002 !'" ~ 2208300156 KAIEIE MAUKA EXPLORATORY WELL
ic Ref #180336 - Fluoride
2208300156
I
Analysis Date: 09/04/2002
KAIEIE MAUKA EXPLORATORY WELL
QC Ref #180522 - SDWA Pesticides Analysis Date: 09/06/2002
I 2208300156 KAIEIE MAUKA EXPLORATORY WELL
I I B QC Summary - Page 1 of 4
I E
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (t 800 568 5227)
1 () -I 8 - 0 2 A I !) : 51 1;-.
Laboratory QC Summary
#100134
8-18
I 1-------------------------
Hawaii Department of Water Supply (Hilo) ( continued)
IQC Ref #180539 - Cyanide Analysis Date: 09/09/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
L ' '
QC Ref #180572 - EDB and DBCP by GC-ECD Analysis Date: 09/06/2002
C 2208300156 KAIEIE MAUKA EXPLORATORY WELL
[bC Ref #180574 - Glyphosate Analysis Date: 09/09/2002'
2208300156 KAIEIE MAUKA EXPLORATORY WELL
C QC Ref #180689 - Diquat and Paraquat Analysis Date: 09/05/2002
~ 2208300156 KAIEIE MAUKA EXPLORATORY WELL I
~
Oc Ref #180788 - Regulated VOCs plus Lists 1&3 Analysis Date: 09/10/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
r '- Ref #180906 - Nickel, QC Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
Ref #180907 - Copper, Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
Ref #180911 - Arsenic, Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
QC Summary - Page 2 of 4
E I I I
555 East Walnut Street Pasadena, Calilomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Ref #180912 - Selenium, Total, ICAP/MS
; ,)- I J - 0 2 Ai,): ~ I i i~
Laboratory QC Swmnary
#100134
Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
QC Ref #180915 - Beryllium, Total, ICAP/MS Analysis Date: 09/12/2002
E 2208300156 KAIEIE MAUKA EXPLORATORY WELL
[bC Ref #180917 - Cadmium, Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
[ QC Ref #180918 - Barium, Total, ICAP/MS Analysis Date: 09/12/2002
[ 2208300156 KAIEIE MAUKA EXPLORATORY WELL
~c " ~. Re·f #180919 - Antimony, Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
[ <i
QC Ref #180920 - Thallium, Total, ICAP/MS Analysis Date: 09/12/2002
m L 2208300156 KAIEIE MAUKA EXPLORATORY WELL
IC Ref #180921 - Lead, Total, ICAP/MS Analysis Date: 09/12/2002
2208300156 KAIEIE MAUKA EXPLORATORY WELL
We Ref #180928 - Chromium, Total, ICAP/MS Analysis Date: 09/12/2002
I 2208300156 KAIEIE MAUKA EXPLORATORY WELL
I [ QC Summary - Page 3 of 4
8-19
I 1
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Laboratory QC Swmnary
#100134
8-20
1 11
-------------------------
Hawaii Department of Water Supply (Hila) ( continued)
IQC Ref #18101~ - Aldicarbs
2208300156
E "
QC Ref #181106 - Endothall
I 2208300156
!pc Ref #181453 - Mercury
2208300156
[
Analysis Date: 09/13/2002
KAIEIE MAUKA EXPLORATORY WELL
Analysis Date: 09/11/2002
KAIEIE MAUKA EXPLORATORY WELL
Analysis Date: 09/21/2002
KAIEIE MAUKA EXPLORATORY WELL
QC Ref #181471 - Herbicides by 515.3 Analysis Date: 09/14/2002
[
Ic [
I I 1 I I
2208300156 KAIEIE MAUKA EXPLORATORY WELL
Ref #182826 - 525 Semi volatiles by GC/MS Analysis Date: 10/03/20.02
2208300156 KAIEIE MAUKA EXPLORATORY WELL
QC Summary - Page 4 of 4
I I I I
[
[
(
I I I I I
QC
HS
LCS1
LCS2
HBLX
HS
HSD
555 East Walnut Street Pasadena, California 91101 Tel: 626 566 6400 Fax: 626 566 6324 1 800 568 LABS (1 800 566 5227)
Hawaii Department of Water Supply (Hilo)
QC Ref #180164 Alkalinity in CaC03
Analyte Spiked Recovered
Spiked sample Lab # 22 08300156
Alkalinity in CaCOl units 100 99.8
Alkalinity in CaCOl units 100 99.6
Alkalinity in CaCOl units NO <1.00
Alkalinity in CaCOl units 96.2 89,9
Alkalinity in CaCOl units 96.2 90.9
units
Units
HGL
HGL
HGL
HGL
HGL
HGL
1 c)- I 3 - 0 2 A'I 0: 57 . ) 8-21
I N wt'"
Yield ('II)
99.8
99.6
9l.5
94.5
Laboratory QC Report #100134
Limits ('II) RPD ('II)
0-0
90-110
90-110 0.20
80-120
80-120 1.1
RPD_LCS Alkalini ty in CaCOl units 99.800 99.600 HGL 0.2 0-10
RPD_MS Alkalinity in CaCOl units 93.451 94.491 MGL 1.1 0-10
QC Ref #180178 Specific Conductance
QC
DUP
QC
QC
DUP
QC
QC
LCS1
LCS2
MBLK
MS
MSD
Analyte Spiked Recovered Units Yield ('II). Limits ('II) RPD ('II)
Specific Conductance 118 115 UMBO 0-20 2.6
Ref #180192 Lab pH
Analyte Spiked Recovered Units Yield ('II) Limits ('II) RPD ('II)
Lab pH 8.l 8.l UNIT ( 0-20 0.0
Ref #180265 Nitrite, Nitrogen by :IC
Analyte Spiked Recovered Units Yield ('II) Limits ('II) RPD ('II)
Nitrite, Nitrogen by IC 1.0 0.989 MGL 98.9 90-110
Nitrite, Nitrogen by IC 1.0 0.996 MGL 99.6 90-110 0.71
Nitrite, Nitrogen by IC NO <0.10 MGL
Nitrite, Nitrogen by IC 1.0 0.959 MGL 95.9 80-120
Nitrite, Nitrogen by IC 1.0 0.968 MGL 96.8 80-120 0.9l
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 1 of 31
I I I
QC
LCSl
LCS2
HBLX
MS
MSD
QC
LCSl
LCS2
HBLK
HS
MSD
[ QC
MS
LCSl
LCS2
MBLK
MS
MSD
I I I
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 826 568 6324 1 800 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
QC Ref #180266 Nitrate as Nitrogen
Analyte Spiked Recovered
Nitrate as Nitrogen by IC 2.5 2.61
Nitrate as Nitrogen by IC 2.5 2.61
Nitrate as Nitrogen by IC NO <0.10
Nitrate as Nitrogen by IC 2.5 2.56
Nitrate as Nitrogen by IC 2.5 2.79
QC Ref #180301 Calcium, Total, I CAP
Analyte Spiked Recovered
Calcium, Total, ICAP SO U.8
Calcium, Total, ICAP SO 49.3
Calcium, Total, ICAP NO <1.00
Calcium, Total, ICAP SO 49.9
Calcium, Total, ICAP SO 51.7
QC Ref #180336 Fluoride
Analyte Spiked Recovered
Spiked sample Lab II 22 08290387
Fluoride 1. 00 0.981
Fluoride 1. 00 1.00
Fluoride NO <0.05
Fluoride 1. 00 0.993
Fluoride 1. 00 1. 02
by IC
Units Yield
HaL 104.4
HaL 104.4
HGL
HaL 102.4
HaL 111.6
Units Yield
HaL 99.6
HaL 98.6
HaL
HaL 99.8
MaL 103.4
Units Yield
HGL
MGL 98.1
HGL 100.0
MGL
MGL 99.3
MGL 102.0
1 ',j-I > 02 A'I 0 : 57 1 i':
<'II)
<'II)
<'II)
Laboratory QC Report
#100134
Limits <'II) RPD <'II)
90-110
90-110 0.00
80-120
80-120 8.6
Limits <'II) RPD <'II)
85-115
85-115 1.0
70-130
70-130 3.5
Limits ('II) RPD <'II)
0-0
90-110
90-110 1.9
80-120
80-120 2.7
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 2 of 31
8-22
I I I I
r ~
[
E [
r ... [
I I I I
QC
MBLK
MBLK
MBLK
LCS1
MBLK
MS
MSD
MBLK
MBLK
MBLK
LCS1
MBLK
MS
MSD
MS
LCS1
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
LCSl
MBLIt
MS
MSD
MB'LIt
LCSl
MBLIt
555 East walnut Street Pasadena, Calilomia 91101 Tel: 626 569 6400 Fax: 626 568 6324 1 800 569 lABS (1 800 569 5227)
Hawaii Department of Water Supply (Hilo) (continued)
QC Ref #180522 SDWA Pesticides
1:)-'13-02 Al():57
Laboratory QC Report
#100134
Ii : ~
Analyte Spiked
NO
Recovered Units Yield (%) Limits (%) RPD (%)
PCB 1016 Aroc1or
PCB 1221 Aroc1or
PCB 1232 Aroclor
PCB 1242 Aroclor
PCB 1242 Aroclor
PCB 1242 Aroc1or
PCB 1242 Aroclor
PCB 1248 Aroclor
PCB 1254 Aroclor
PCB 1260 Aroclor
Alpha-BHC
Alpha-BHC
Alpha-SHC
Alpha-BHC
Spiked sample
Alachlor (Alanex)
Alachlor (Alanex)
Alachlor (Alanex)
Alachlor (Alanex)
Aldrin
Aldr:Ln
Aldrin
Aldrin
Beta-BHC
Beta-BHC
Beta-BHC
Beta-BHC
Chlordane
Chlorthalonil (Draconil,Bravo)
Chlorthalonil (Draconil,Bravo)
<0.07 UGL
NO
NO
0.500
NO
0.500
0.500
NO
NO
NO
0.050
NO
<0.10
<0.10
0.507
<0.10
0.557
0.608
<0.10
<0.10
<0.10
0.052
<0.01
0.050 0.053
0.050 0.054
Lab • 22 08300156
0.100
NO
0.100
0.100
0.050
ND
0.050
0.050
0.050
NO
0.050
0.050
NO
0.100
NO
0.113
<0.05
0.117
0.123
0.046
<0.01
0.049
0.050
0.053
<0.01
0.058
0.057
<0.10
0.084
<0.01
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
NONE
UGL
UGL
UGL
UGL
UGL
UGL
UGL
VGL
VGL
UGL
UGL
VGL
UGL
UGL
UGL
101.4
111.4
121.6
104.0
106.0
108.0
113.0
117.0
123.0
92.0
98.0
100.0
106.0
116.0
114.0
84.0
70-130
65-135
'65-135
62-122 )
57-127
57-127
0-0
70-130
65-135
65-135
56-116
51-121
51-121
65-125
60-130
60-130
( 61-121 )
8.8
1.9
5.0
2.0
1.7
Spikes which exceed Limits and Method Blanks with posi~ive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 3 of 31
8-23
I I E
E [
[
c
I I I I [
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
555 East Walnut Street Pasadena. california 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Chlorthalonil (Draconil,Bravo)
Chlorthalonil (Draconil,Bravo)
Delta-BHC
Delta-BHC
Delta-BHC
Delta-BHC
p,p' DOD
p,p' DOD
p,p' DOD
p,p' DOD
p,p' DOE
p,p' DOE
p,p' DOE
p,p' DOE
p,p' DDT
p,p' DDT
p,p' DDT
p,p' DDT
Dieldrin
Dieldrin
Dieldrin
Dieldrin
Endrin Aldehyde
Endrin Aldehyde
Endrin Aldehyde
Endrin Aldehyde
Endrin
Endrin
Endrin
Endrin
Endosulfan I (alpha)
Endosulfan I (alpha)
Endosulfan I (alpha)
Endosulfan I (alpha)
Endosulfan II (beta)
0.100
0.100
0.050
NO
0.050
0.050
0.100
NO
0.100
0.100
0.100
NO
0.100
0.100
0.100
NO
0.100
0.100
0.100
NO
0.100
0.100
0.100
NO
0.100
0.100
0.100
NO
0.100
0.100
0.050
NO
0.050
0.050
0.100
0.087
0.090
0.055
<0.01
0.057
0.058
0.113
<0.01
0.115
0.117
0.110
<0.01
0.111
0.116
0.106
<0.01
0.109
0.113
0.110
<0.01
0.111
0.115
0.088
<0.01
0.092
0.091
0.107
<0.01
0.110
0.113
0.054
<0.01
0.054
0.056
0.108
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
I J-I > J:2 i\ 1 0 : 58 I N
87.0
90.0
110.0
114.0
116.0
113.0
115.0
117.0
110.0
111.0
116.0
106.0
109.0
113.0
110.0
111.0
115.0
88.0
92.0
91.0
107.0
110.0
113.0
108.0
108.0
112.0
108.0
Laboratory QC Report
#100134
56-126
56-126
72-132
67-137
67-137
77-137
72-142
72-142
69-129
64-134
64-134
82-142
77-147
77-147
57-117
52-122
52-122
58-118
53-123
53-123
58-118
53-123
53-123
57-117
52-122
52-122
62-122
3.4
1.7
1.7
4.4
3.6
3.5
1.1
2.7
3.6
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on Les. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 4 of 31
8-24
I I I I I
[
c
I I I
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
KS
MSD
LCS1
MBLK
MS
MSD
MBLK
555 East Walnut Street Pasadena, GaRfomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 BOO 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Endosulfan II (beta)
Endosulfan II (beta)
Endosulfan II (beta)
Endosulfan sulfate
Endosulfan sulfate
Endosulfan sul.fate
Endosulfan sulfate
Heptachlor
Heptachlor
Heptachlor
Heptachlor
Heptachlor Epoxide
Heptachlor Epoxide
Heptachlor Epoxide
Heptachlor Epoxide
Lindane (gamma-BHC)
Lindane (gamma-BHC)
Lindane (gamma-BHC)
Lindane (gamma-BHC)
Methoxychlor
Methoxychlor
Methoxychlor
Methoxychlor
Tetrachlorometaxylene (surr)
Tetrachlorometaxylene (surr)
Tetrachlorometaxylene (surr)
Tetrachlorometaxylene (surr)
Dibutyl chlorendate (surr)
Dibutyl chlorendate (surr)
Dibutyl chlorendate (surr)
Dibutyl chlorendate (surr)
Toxaphene
NO
0.100
0.100
0.100
NO
0.100
0.100
0.050
NO
0.050
0.050
0.050
NO
0.050
0.050
0.050
NO
0.050
0.050
0.500
NO
0.500
0.500
100
100
l.00
100
100
100
100
100
NO
0.112
0.114
0.108
<0.01
0.114
0.116
0.048
<0.01
0.051
0.052
0.054
<o.oi 0.054
0.057
0.054
<0.01
0.055
0.057
0.516
<0.05
0.547
0.550
101
92
l.05
111
96
112
116
124
<0.50
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
%R
%R
tR
tR
tR
%R
tR
tR
UGL
:()-1~,-J2 A10:58
112.0
114.0
108.0
114.0
116.0
96.0
102.0
104.0
108.0
108.0
114.0
10.8.0
110.0
114.0
103.2
109.4
110.0
101.0
92.0
l.05.0
111.0
96.0
112.0
116.0
124.0
Laboratory QC Report
#100134
57-127
57-127
72-132
67-137
67-137
68-128
63-133
63-133
57-117
52-122
52-122
59-119
54-124
. ( 54-124
75-135
70-140
70-140
70-130
70-l.30
70-130
70-130
70-130
70-130
1.8
1.7
1.9
5.4
3.6
0.55
5.6
6.7
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 5
8-25
of 31
I I I I I I
Ed l' "
I I I I I
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
lJ-lS-JZ ;\'10:5G IN
Laboratory QC Report
#100134
QC Ref #180539 Cyanide
QC Analyte Spiked Recovered units Yield (Ik) Limits (Ik) RPD (Ik)
MS Spiked sample Lab It 22 09070018 MGL 0-0
LCSl Cyanide 0.10 0.103 MGL 103.0 80-120
MBLlt Cyanide HD <0.03 MGL
MS Cyanide 0.10 0.093 MGL 93.0 80-120
MSO Cyanide 0.10 0.091 MGL 91.0 80-120 2.2
QCRef #180572 EDB and DBCP by GC-ECD
QC
MS
LCSl
LCB2
MBLlt
MS
MSO
RPO_MS
LCSl
LCS2
MBLlt
MS.
MSD
RPD_MS
LCSl
LCS2
MBLK
MS
MSD
RPD_MS
Analyte spiked Recovered units Yield (Ik) Limits (Ik) RPO (Ik)
Spiked sample Lab * 22 08290312 NONE 0-0 )
Dibromochloropropane (DBCP) 0.02 0.022 UGL 110.0 70-130
Dibromochloropropane (DBCP) 0.20 0.19 UGL 95.0 70-130
Dibromochloropropane (DBCP) HD <0.01 UGL
Dibromochloropropane (DBCP) 0.20 0.22 UGL 110.0 65-135
Oibromoch1oropropane (OBCP) 0.20 0.23 UGL 115.0 65-135 4.4
Dibromochloropropane (OBCP) 110.000 115.000 UGL 4.4 0-2'0
Ethylene Dibromide (BOB) 0.02 0.025 UGL 125.0 70-130
Ethylene Dibromide (EOB) 0.20 0.17 UGL 85.0 70-130
Ethylene Dibromide (BOB) HD <0.01 UGL
Bthylene Dibromide (BOB) 0.20 0.22 UGL 110.0 65-135
Ethylene Dibramide (BOB) 0.20 0.23 UGL 115.0 65-135 4.4
Ethylene Dibramide (EDB) 110.000 115.000 UGL 4.4 0-20
1,2-dibramopropane (surr) 100 106 IIsR 106.0 60-140
1,2-dibromopropane (surr) 100 98 IIsR 98.0 60-140 7.8
1,2-dibromopropane (surr) 100 99 IIsR 99.0
1,2-dibramopropane (surr) 100 137 IkR 137.0 60-140
1,2-dibramopropane (surr) 100 123 IkR 123.0 60-140 11
1,2-dibramopropane (surr) 137.000 123.000 IkR 10.8 0-20
Spikes which exceed Limits and Method Blanks with positive results are highlighted by underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
8-26
QC Report Page 6 of 31
I I I I I I
[
I I I I I
QC
MS
LCS1
MBLIC
MS
MSD
QC
MS
MSD
LeS1
MBLIC
MS
MSD
LCS1
MBLIC
MS
MSD
QC
LCS1
MBLK
MS
MSD
555 East Walnut Street Pasadena, Calilornia 91101 Tel: 626566 6400 Fax: 626 566 6324 1 800 566 LABS (1 600 566 5227)
Hawaii Department of Water Supply (Hila) (continued)
QC Ref #180574 Glyphosate
Ana1yte Spiked Recovered
Spiked sample Lab II 22 08300105
G1yphosate 10 11.3
G1yphosate ND . <6.00
G1yphosate 10 11.0
G1yphosate 10 11.7
QC Ref #180689 Diquat and Paraquat
Ana1yte Spiked Recovered
Spiked sample Lab II 22 08300127
Spiked sample Lab II 22 08300127
Diquat 10.0 8.1
Diquat ND <0.40
Diquat '10.0 8.6
Diquat 10.0 8.3
Paraquat 10.0 9.2
Paraquat ND <2.00
Paraquat 10.0 9.6
Paraquat 10.0 9.3
units
UGL
UGL
UGL
UGL
UGL
Units
NONE
NONE
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
QC Ref #180788 Regulated VOCs plus Lists
Ana1yte Spiked Recovered Units
1,1,1,2-Tetrach1oroethane 4 4.24 UGL
1,1, 1, 2-Tetrach1oroethane ND <0.50 UGL
1,1,1,2-Tetrach1oroethane 10 11.5 UGL
1,1,1,2-Tetrach1oroethane 10 11.4 UGL
lO--lS-J2 A1Q:5'J l>J
Yield <'Is)
113.0
110.0
117.0
Yield <'Is)
81.0
86.0
83.0
92.0
96.0
93.0
1&:3
Yield (lis)
106.0
115.0
114.0
Laboratory QC Report
#100134
Limits <'Is) RPD <'Is)
0-0
70-130
70-130
70-130 6.2
Limits <'Is) RPD <'Is)
0-0 )
0-0 ) 0.00
70-130
70-130
70-130 3.6
70-130
70-130
70-130 3.2
Limits <'Is) RPD ('Is)
70-130
84-131
84-131 0.87
RPD_MS 1,1,1,2-Tetrach1oroethane 115.000 114.000 UGL 0.9 0-20
Spikes which exceed Limits and Method Blanks with positive results are highlighted by underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 7 of 31
8-27
I I I I
[
[~ . 1
[
[
E I I I I I
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
1 0-1 ~,-:;2 A 1 0 : 5 :3 I N
555 East walnut Street Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 BOO 568 LABS (1 BOO 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
1. 1. 1-Trichloroethane
1.1.1-Trichloroethane
1.1.1-Trichloroethane
1. 1, 1-Trichloroethane
l,l,l-Trichloroethane
l,l,2,2-Tetrachloroethane
l,l,2,2-Tetrachloroethane
l,l,2,2-Tetrachloroethane
l,l,2,2-Tetrachloroethane
l,l,2,2-Tetrachloroethane
l,l,2-Trichloroethane
l,l,2-Trichloroethane
l,l,2-Trichloroethane
l,l,2-Trichloroethane
l,l,2-Trichloroethane
l,l-Dichloroethane
l,l-Dichloroethane
l,l-Dichloroethane
l,l-Dichloroethane
l,l-Dichloroethane
l,l-Dichloroethylene
l,l-Dichloroethylene
l,l-Dich1oroethylene
l,l-Dichloroethylene
l,l-Dichloroethylene
l,l-Dichloropropene
l,l-Dichloropropene
l,l-Dichloropropene
l,l-Dichloropropene
l,l-Dichloropropene
l,2,3-Trichlorobenzene
l,2,3-Trich10robenzene
l,2,3-Trichlorobenzene
l,2,3-Trichlorobenzene
l,2,3-Trichlorobenzene
4
NO
10
10
126.000
4
NO
10
10
115.000
4
NO
10
10
113.000
4
NO
10
10
117.000
4
NO
10
10
104.000
4
NO
10
10
119.000
4
NO
10
10
99.100
4.79
<0.50
12.6
12.0
120.000
4.03
<0.50
11.5
11.5
115.000
4.02
<0.50
11.3
11.2
112.000
4.62
<0.50
11.7
11.5
115.000
4.29
<0.50
10.4
10.5
105.000
4.57
<0.50
11. 9
11.5
115.000
3.99
<0.50
9.91
10.5
105.000
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
119.8
126.0
120.0
4.9
100.8
115.0
115.0
0.0
100.5
113.0
112.0
0.9
115.5
117.0
115.0
1.7
107.2
104.0
105.0
1.0
114.2
119.0
115.0
3.4
99.8
99.1
105.0
5.8
Laboratory QC Report
#100134
( 70-130 )
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
81-127
81-127
0-20
70-130
70-130
70-130
0-20
4.9
0.00
0.89
1.7
0.96
3.4
5.8
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 8 of 31
8-28
I 555 East Walnut Street Pasadena, GaUfomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
iO-13-J2 A'iC):58 IN
Laboratory QC Report
#100134
8-29
[-------------------------
c c
[
[
[
I I I I
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
Lesl.
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
1,2 , 3-Trichloropropane
1,2,3-Trichloropropane
1,2,3-Trichloropropane
1,2,3-Trichloropropane
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2,4-Trimethylbenzene
1,2-Dichloroethane
1,2-Dichloroethane
1,2-Dich1oroethane
1,2-Dichloroethane
1,2-Dichloroethane
1,2-Dichloropropane
1,2-Dichloropropane
1,2-Dichloropropane
1,2-Dichloropropane
1,2-Dichloropropane
1, 3, S-Trimethylbenzene
1,3,5-Trimethy1benzene
1,3,5-Trimethy1benzene
1,3,5-Trimethylbenzene
1,3,5-Trimethylbenzene
1,3-Dichloropropane
1,3-Dichloropropane
1,3-Dichloropropane
1,3-Dichloropropane
1,3-Dichloropropane
4
ND
10
10
112.000
4
ND
10
10
99.000
4
ND
10
10
110.000
4
ND
10
10
122.000
4
ND
10
10
113.000
4
ND
10
10
111. 000
4
ND
10
10
117.000
4.16
<0.50
11.2
11.2
112.000
4.06
<0.50
9.90
10.0
100.000
4.35
<0.50
11.0
11.1
111.000
4.44
<0.50
12.2
12.0
120.000
4.32
<0.50
11.3
11.1
111. 000
4.50
<0.50
11.1
10.9
109.000
4.35
<0.50
11.7
11.4
114.000
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
104.0
112.0
112.0
0.0
101.5
99.0
100.0
1.0
108.7
110.0
111.0
0.9
111.0
122.0
120.0
1.7
108.0
113.0
111.0
1.8
112.5
111.0
109.0
1.8
108.7
117.0
114.0
2.6
( 70-130 )
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
80-140
80-140
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
0.00
1.0
0.90
1.7
1.8
1.8
2.6
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 9 of 31
I I I
555 East Walnut Sireel Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo)
1 0- 'I 3- J 2 /I. 1 0: :5 giN
Laboratory QC Report
#100134
8-30
(continued)
I----------------~~~~~
[
[
[
[
[
r Ii.
c I I I I I
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
LCS2
MBLK
MS
MSD
RPD_LCS
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
MS
LCS1
MBLK
p-Dichlorobenzene (l,4-DCB)
p-Dichlorobenzene (l,4-DCB)
p-.Dichlorobenzene (l,4-DCB)
p-Dichlorobenzene (l,4-DCB)
p-Dichlorobenzene (l,4-DCB)
2,2-Dichloropropane
2,2-Dichloropropane
2,2-Dichloropropane
2,2-Dichloropropane
2,2-Dichloropropane
2-Butanone (MEK)
2-Butanone (MEK)
2-Butanone (MEK)
2-Butanone (MEK)
2-Butanone (MEK)
2-Butanone (MEK)
4
ND
10
10
112.000
4
ND
10
10
101.000
40
40
ND
100
100
97.000
68.600
4
ND
10
10
104.000
4
ND
10
10
110.000
40
ND
100
4.11
<0.50
11.2
11.0
110.000
4.37
<0.50
10.1
9.99
99.900
38.8
30.5
<5.00
68.6
72.1
76.250
72.100
4.27
<0.50
10.4
10.1
101. 000
4.42
<0.50
11.0
11.1
111. 000
40.2
<5.00
101
102.8
112.0
110.0
1.8
109.2
101. 0
99.9
1.1
97.0
76.2
68.6
72.1
ll.:.L 5.0
106.7
104.0
101.0
2.9
110.5
110.0
111.0
0.9
100.5
70-130
70-130
70-130
0-20
70-130
84-131
84-131
0-20
70-130
70-130
56-85
56-85
0-20
0-20
70-130
70-UO
70-130
0-20
70-130
70-130
70-130
0-20
70-130
1.8
1.1
24
5.0
2.9
0.90
2-Butanone (MEK)
o-Chlorotoluene
o-Chlorotoluene
o-Chlorotoluene
o-Chlorotoluene
o-Chlorotoluene
p-Chlorotoluene
p-Chlorotoluene
p-Chlorotoluene
p-Ch1oroto1uene
p-Ch1orotoluene
4-Methyl-2-Pentanone (MIBK)
4-Methyl-2-Pentanone (MIBK)
4-Methyl-2-Pentanone (MIBK)
4-Methyl-2-Pentanone (MIBK)
4-Methyl-2-Pentanone (MIBK)
Spiked sample
100 100
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
NONE
UGL
UGL
101. 0
100.0
1.0
70-130
70-130
0-20
0-0
70-130
1.00
Benzene
Benzene
101.000 100.000
Lab # 22 09090028
4
ND
4.77
<0.50
119.2
Spikes which exceed Limits and Method Blanks with positive results are highlighted by underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 10 of 31
I
I
E c
r I.
c ,. L.
I I I [
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS'
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MB.LK
MS
MSD
RPD_MS
LCS1
MBLK
1 0-1 3 - J 2 A 1 (J: 58 I ,,;
555 East Walnut Street Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Benzene
Benzene
Benzene
Bromobenzene
Bromobenzene
Bromobenzene
Bromobenzene
Bromobenzene
Bromomethane (Methyl Bromide)
Bromomethane (Methyl Bromide)
Bromomethane (Methyl Bromide)
Bromomethane (Methyl Bromide)
Bromomethane (Methyl Bromide)
cis-1,2-Dichloroethylene
cis-1,2-Dichloroethylene
cis-1,2-Dichloroethylene
cis-1,2-Dichloroethylene
cis-1,2-Dichloroethylene
Chlorobenzene
Chlorobenzene
Chlorobenzene
Chlorobenzene
Chlorobenzene
Carbon Tetrachloride
Carbon Tetrachloride
Carbon Tetrachloride
Carbon Tetrachloride
Carbon Tetrachloride
cis-l,3-Dichloropropene
cis-1,3-Dichloropropene
cis-1,3-Dichloropropene
ciS-1,3-Dich1oropropene
cis-1,3-Dichloropropene
Bromoform
Bromoform
10
10
113.000
4
NO
10
10
113.000
4
NO
10
10
106.000
4
NO
10
10
105.000
4
NO
10
10
110.000
4
NO
~o
10
125.000
4
NO
10
10
109.000
4
NO
11.3
11.3
l13.000
4.19
<0.50
l1.3
l1.0
l10.000
5.16
<0.50
10.6
10.7
107.000
4.16
<0.50
10.5
10.7
107.000
4.34
<0.50
11.0
10.7
107.000
4.53
<0.50
12.5
12.1
121. 000
4.04
<0.50
10.9
10.8
106.000
4.13
<0.50
UGL
UGL
UGL
UGL
UGL
UGL
.UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
113.0
113.0
0.0
104.6
113.0
110.0
2.7
129.0
10B.0
107.0
0.9
.104.0
105.0
107,0
1.9
108.5
110.0
107.0
2.8
113.2
125.0
121.0
3.3
101. 0
109.0
108.0
0.9
103.2
Laboratory QC Report
#100134
70-130
70-l30
0-20
70-130
70-130
70-130
0-20.
70-130
74-137
74-137
0-20
70-130
86-129
86-129
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
85-120
85-120
0-20
70-130
0.00
2.7
0.93
1.9
2.8
3.3
0.92
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 11 of 31
8-31
r-III
I I I I
[
c [
E [
I I I I
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
MS
MSD
RPD_MS
LeS1
MBLK
555 Easl walnut Slreel Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) ( continued)
Bromoform
Bromoform'
Bromoform
Chloroform (Trichloromethane)
Chloroform (Trichloromethane)
Chloroform (Trichloromethane)
Chloroform (Trichloromethane)
Chloroform (Trichloromethane)
Bromochloromethane
Bromochloromethane
Bromochloromethane
Bromochloromethane
Bromochloromethane
Chloroethane
Chloroethane
Chloroethane
Chloroethane
Chloroethane
Chloromethane(Methyl Chloride}
Chloromethane(Methyl Chloride}
Chloromethane(Methyl Chloride}
Chloromethane(Methyl Chloride}
Chloromethane(Methyl Chloride}
Chlorodibromomethane
Chlorodibromomethane
Ch10rodibromomethane
Chlorodibromomethane
Chlorodibromomethane
Dibromomethane
Dibromomethane
Dibromomethane
Dibromomethane
Dibromomethane
Bromodichloromethane
Bromodichloromethane
10
10
108.000
4
NO
10
10
118.000
4
NO
10
10
112.000
10
NO
10
10
120.000
4
NO
10
10
108.000
4
NO
10
10
123.000
4
NO
10
10
117.000
4
NO
10.8
10.7
107.000
4.60
<0.50
11.B
11.3
113.000
4.09
<0.50
11.2
10.7
107.000
9.82
<0.50
12.0
11.B
118.000
4.52
<0.50
10.8
10.7
107.000
4.09
<0.50
12.3
12.3
123.000
4.19
<0.50
11.7
10.9
109.-000
4.25
<0.50
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
1 n '1' J" ," I 'x- j - :.:. Ale:53
108.0
107.0
0.9
115.0
11B.O
113.0
4.3
102.2
112.0
107.0
4.6
98.2
120.0
118.0
1.7
113.0
108.0
107.0
0.9
102.2
123.0
123.0
0.0
104.8
117.0
109.0
7.1
106.2
Labpratory QC R~ort
#100134
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
69-151
69-151
0-20
70-130
76-138
76-138
0-20
70-130
70-130
70-130
0-20
70-1'30
70-130
70-130
0-20
70-130
0.93
4.3
4.6
1.7
0.93
0.00
7.1
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on Les. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 12
8-32
IN
of 31
I
I
555 East Walnut Street Pasadena. CalifornIa 91101 Tat: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo)
1 C -I ::; - 0 2 ,A,) 0 : 5 3 IN
Laboratory QC Report
#100134
8-33
( continued)
I~-----------------------
c
[
[
[
[
[
I I I I
MS
MSD
RPD_MS
LCS1
~LK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
~LK
MS
MSD
RPD_MS
LCS!
LCS2
~LK
MS
MSD
RPD_LCS
RPD_MS
LeSl.
LCS2
MBLK
MS
MSD
RPD_LCS
RPD_MS
LCS1
MBLK
MS
Bromodich1oromethane
Bromodich1oromethane
Bromodichloromethane
Dichloromethane
Dichloromethane
Dichloromethane
Dichloromethane
Dichloromethane
Di-isopropyl ether
Di-isopropyl ether
Di-isopropyl ether
Di-isopropyl ether
Di-isopropyl ether
Ethyl benzene
Ethyl benzene
Ethyl benzene
Ethyl benzene
Ethyl benzene
Dichlorodifluoromethane
Dichlorodifluoromethane
Dichlorodifluoromethane
Dichlorodifluoromethane
Dichlorodifluoromethane
Dichlorodifluoromethane
Dichlorodifluoromethane
Fluorotrichloromethane-Freon11
Fluorotrichloromethane-Freonl1
Fluorotrichloromethane-Freon11
Fluorotrichloromethane-Freon11
Fluorotrichloromethane-Freon11
Fluorotrichloromethane-Freon11
Fluorotrichloromethane-Freon11
Hexachlorobutadiene
Hexachlorobutadiene
Hexachlorobutadiene
10
'10
123.000
4
NO
10
10
104.000
4
NO
10
10
104.000
4
NO
10
10
111.000
4
4
NO
10
10.
105.000
138.000
4
4
NO
10
10
111.000
131. 000
4
NO
10 .
12.3
11.9
119.000
3.95
<0.50
10.4
10.2
102.000
4.27
<3.00
10.4
10.3
103.000
4.58
<0.50
11.1
10.9
109.000
4.20
4.80
<0.50
13.8
13.5
120.000
135.000
4.44
4.99
<0.50
13.1
12.9
124.750
129.000
4.17
<0.50
9.65
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
123.0
119.0
3.3
98.8
104.0
102.0
1.9
106.7
104.0
103.0
1.0
114.5
111.0
109.0
1.8
105.0
120.0
138.0
135.0
13.3
2.2
111.0
124.8
l.ll.:..Q....
129.0
11.7
1.5
104.2
96.5
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
53-168
53-168
0-20
0-20
70-130
70-130
70-130
70-130
0-20
0-20
70-130
( 70-130 )
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
3.3
1.9
0.97
1.8
13
2.2
12
1.5
QC Report Page 13 of 31
I I I
555 East Walnut Street Pasadena. Califomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo)
Laboratory QC Report
#100134
8-34
(continued)
I~-----------------------1M ~
~ .. ,;
~
I I
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
MSD
RPD_MS
LCSI
MBLK
MS
Hexachlorobutadiene
Hexachlorobutadiene
Isopropylbenzene
Isopropylbenzene
Isopropylbenzene
Isopropylbenzene
Isopropylbenzene
m-Dichlorobenzene (l,3-DCB)
m-Dichlorobenzene (l,3-DCB)
m-Dichlorobenzene (l,3-DCB)
m-Dichlorobenzene (l,3-DCB)
m-Dichlorobenzene (l,3-DCB)
m,p-Xylenes
m,p-Xylenes
m,p-Xylenes
m,p-Xylenes
m,p-Xylenes
Methyl Tert-butyl ether (MTBE)
Methyl Tert-butyl ether (MTBE)
Methyl Tert-butyl ether (MTBE)
Methyl Tert-butyl ether (MTBE)
Methyl Tert-butyl ether (MTBE)
Naphthalene
Naphthalene
Naphthalene
Naphthalene
Naphthalene
n-Butylbenzene
n-Butylbenzene
n-Butylbenzene
n-Butylbenzene
n-Butylbenzene
'n-Propylbenzene
n-Propylbenzene
n-Propylbenzene
10
96,500
4
NO
10
10
112.000
4
NO
10
10
114.000
8
NO
20
20
111. 000
4
NO
10
10
96.200
4
NO
10
10
95.400
4
ND
10
10
101.000
4
NO
10
10.3
103.000
4.65
<0.50
11.2
11.1
111.000
4.29
<0.50
11.4
11.1
111.000
9.01
<0.50
22.2
21.9
109.500
4.67
<3.00
9.62
9.64
96.400
4.03
<0.50
9.54
10.3
103.000
4.29
<0.50
10.1
10.2
102.000
4.51
<0.50
11.2
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
103.0
6.5
116.3
112.0
111.0
0.9
107.2
114.0
111.0
2.7
112.6
111.0
109.5
1.4
116.8
96.2
96.4
0.2
100.8
95.4
103.0
7.7
107.2
101. 0
102.0
1.0
112.8
112.0
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
60-140
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
( 70-130 )
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
6.5
0.90
2.7
1.4
0.21
7.7
0.99
QC Report Page 14 of 31
I I I
555 East Walnut Street Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 566 6324 1 800 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Laboratory QC Report
#100134
8-35
1-------------------------I
c
(
c
I I I
MSD
RPD_MS
LCS1
MBLK
MS
M.SD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCS1
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LeSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
n-Propylbenzene
n-Propylbenzene
o-Xylene
o-Xylene
o-Xylene
o-Xylene
o-Xylene
o-Dichlorobenzene (l,2-DCB)
o-Dichlorobenzene (l,2-DCB)
o-Dichlorobenzene (l,2-DCB)
o-Dichlorobenzene (l,2-DCB)
o-Dichlorobenzene (l,2-DCB)
Tetrachloroethylene (PCE)
Tetrachloroethylene (PCE)
Tetrachloroethylene (PCE)
Tetrachloroethylene (PCE)
Tetrachloroethylene (PCE)
p-Isopropy1toluene
p-Isopropyltoluene
p-Isopropyltoluene
p-Isopropyltoluene
p-Isopropyltoluene
sec-Butylbenzene
sec-Butylbenzene
sec-Butylbenzene
sec-Butylbenzene
sec-Butylbenzene
Styrene
Styrene
Styrene
Styrene
Styrene
trans-l,2-Dichloroethylene
trans-l,2-Dichloroethylene
trans-l,2-Dichloroethylene
10
112.000
4
ND
10
10
111.000
4
ND
10
10
101.000
4
ND
10
10
113.000
4
ND
10
10
110.000
4
ND
10
10
113.000
4
ND
10
10
107.000
4
ND
10
10.8
108.000
4.34
<0.50
11.1
10.9
109.000
4.00
<0.50
10.1
10.3
103.000
4.45
<0.50
11.3
11.0
110.000
4.29
<0.50
11.0
10.8
108.000
4.47
<0.50
11.3
11.2
112.000
4.25
<0.50
10.7
10.7
107.000
4.32
<0.50
10.5
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
108.0
3.6
108.5
111.0
109.0
1.8
100.0
101.0
103.0
2.0
111.2
113.0
110.0
2.7
107.2
110.0
108.0
1.8
111.8
113.0
112.0
0.9
106.2
107.0
107.0
0.0
108.0
105.0
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
( 85-129 )
3.6
1.8
2.0
2.7
1.8
0.89
0.00
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 15 of 31
I I I
555 East Walnut Street Pasadena, california 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 BOO 568 LABS (1 BOO 568 5227)
Hawaii Department of Water Supply (Hila) (continued)
1 ')- I J - 0 2 1\ 1 r) : 58 I N
Laboratory QC Report
#100134
8-36
1-------------------------[
[
E c
c I I I I I
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS MSD
RPD_MS
LCSl
MBLK
MS
MSD
RPD_MS
LCSl
MBLK
MS
trans-l,2-Dichloroethylene
tra?s-l,2-Dichloroethylene
tert-amyl Methyl Ether
tert-amyl Methyl Ether
tert-amyl Methyl Ether
tert-amyl Methyl Ether
tert-amyl Methyl Ether
tert-Butyl Ethyl Ether
tert-Butyl Ethyl Ether
tert-Butyl Ethyl Ether
tert-Butyl Ethyl Ether
tert-Butyl Ethyl Ether
tert-Butylbenzene
tert-Butylbenzene
tert-Butylbenzene
tert-Butylbenzene
tert-Butylbenzene
Trichloroethylene (TCE)
Trichloroethylene (TCE)
Trichloroethylene (TCE)
Trichloroethylene (TCE)
Trichloroethylene (TCE)
Trichlorotrifluoroethane(Freon
Trichlorotrifluoroethane(Freon
Trichlorotrifluoroethane(Freon
Tr1chlorotr1fluoroethane(Freon
Trichlorotrifluoroethane(Freon
trans-1,3-Dichloropropene
trans-1,3-Dichloropropene
trans-l,3-Dichloropropene
trans-1,3-Dichloropropene
trans-1,3-Dichloropropene
Toluene
Toluene
Toluene
10
105.000
4
ND
10
10
107.000
4
ND
10
10
108.000
4
ND
10
10
115.000
4
ND
10
10
111.000
4
ND
10
10
121. 000
4
ND
10
10
109.000
4
ND
10
10.1
101.000
4.39
<3.00
10.7
10.7
107.000
4.13
<3.00
10.8
10.6
106.000
4.52
<0.50
11.5
11.1
111.000
4.52
<0.50
11.1
11.0
110.000
4.12
<0.50
12.1
11.7
117.000
4.00
<0.50
10.9
10.7
107.000
4.73
<0.50
11.5
UGL
UGL
UGL
UGL
UGL
UGL
UGI,.
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
101. 0
3.9
109.7
107.0
107.0
0.0
103.2
108.0
106.0
1.9
113.0
115.0
111.0
3.5
113.0
111.0
110.0
0.9
103.0
121.0
117.0
3.4
100.0
109.0
107.0
1.9
118.3
115.0
85-129
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
70-130
70-130
0-20
70-130
80-131
80-131
0-20
70-130
( 70-130 )
3.9
0.00
1.9
3.5
0.90
3.4
1.9
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 16 of 31
I
[
555 East Walnut Street Pasadena. Califomla 9t 101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) ( continued)
10-13-J2 Al0:58 IN
Laboratory QC Report
#100134
8-37
~--------------------------------------------------------------~-------------------------------------
[ MSD
RPD_MS
LeSl
[ MBLK
MS
MSD
RPD_MS
[ QC
[ QC
LCSl
LCS2
[ KBLK
KS
KSD
[ QC
[ QC
LCSl
LCS2
c KBLK
MS
MSD
QC
QC
LCBl
LCS2
I KBLK
I I
Toluene 10 ll.3 UGL ll3.0 '( 70-130 1.8
Toluene ll5.000 ll3.000 UGL 1.8 0-20
Vinyl chloride (ve) 4 4.74 UGL ll8.5 70-130
Vinyl chloride (ve) NO <0.30 UGL
Vinyl chloride (Ve) 10 11.3 UGL ll3.0 67-152
Vinyl chloride (Ve) 10 11.5 UGL ll5.0 67-152 1.8
Vinyl chloride (Ve) ll3.000 ll5.000 UGL 1.8 0-20
Ref #180906 Nickel, Total, ICAP/MS
Analyte Spiked Recovered Units Yield ('Is) Limits ''Is) RPD ('Is)
Nickel, Total, ICAP/KS 50 51.5 UGL 103.0 85-115
Nickel, Total, ICAP/KS 50 51.7 UGL 103.4 85-115 0.39
Nickel, Total, ICAP/KS NO <5.00 UGL
Nickel, Total, ICAP/MS 50 50.2 UGL 100.4 70-130
Nickel, Total, ICAP/KS 50 51.2 UGL 102.4 70-130 2.0
Ref #180907 Copper, Total, ICAP/MS
Ana1yte Spiked· Recovered Units Yield ('Is) Limits ('Is) RPD ('Is)
Copper, Total, ICAP/KS 100 102 UGL 102.0 85-115
Copper, Total, ICAP/KS 100 103 UGL 103.0 85-ll5 0.98
Copper, Total, ICAP/KS NO <2.00 UGL
Copper, Tota1, l:CAP/MS 100 '6.5 uaL '6.5 70-130
Copper, Total, ICAP/MS 100 98.3 uaL 98.3 70-130 1.8
Ref #180911 Arsenic, Total, ICAP/MS
Ana1yte Spiked Recovered Units Yield ('Is) Limits ('Is) RPD ('Is)
Arsenic, Total, ICAP/KS 20 19.8 UGL 99.0 85-ll5
Arsenic, Total, ICAP/KS 20 19.9 UGL 99.5 ( 85-ll5 ) 0.50
Arsenic, Total, ICAP/KS NO <1. 00 UGL
Spikes which exceed Limits and Kethod Blanks with positive results are highlighted by Underlining ..
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 17 of 31
I I I I [ MS
MSD
QC
c LeS l
LCS2
KBLJC
E KS
KSD
c QC
c LCSl
LCS2
KBLIC
KS
MSD
oC
LCSl
LCS2
KBLIC
KS
I KSD
I I I [
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 566 5227)
Hawaii Department of Water Supply (Hila) ( continued)
Arsenic, Total, ICAP/MS 20
Arsenic, Total, ICAP/MS 20
20.1
20,2
QC Ref #180912 Selenium, Total,
UGL 100.5
UGL 101.0
ICAP/MS
Laboratory QC Report
#100134
70-130
70-130 0,50
Analyte Spiked Recovered Units Yield ('II) Limits ('II) RPD ('II)
QC
QC
Selenium, Total, lCAP/KS 20 19.5 UGL 97.5 85-115
Selenium, Total, lCAP/KS 20 19.7 UGL 98.5 85-115 1.0
Selenium, Total, lCAP/KS. NO <5.00 UGL
Selenium, Total, lCAP/KS 20 18.8 UGL 94.0 70-130
Selenium, Total, lCAP/KS 20 18.8 UGL 94.0 70-130 ) 0.00
Ref #180915 Beryllium, Total, ICAP/MS
Analyte Spiked Recovered Units Yield (lis) Limits ('II) RPD ('II)
Beryllium, Total, lCAP/KS 5.00 5.02 UGL 100.4 70-130
Beryllium, Total, ICAP/KS 5.00 5.03 UGL 100.6 85-115 0.20
Beryllium, Total, lCAP/KS NO <1.00 UGL
Beryllium, Total, lCAP/KS 5.00 5.11 UGL 102.2 70-130
Beryllium, Total, lCAP/KS 5.00 5.11 UGL 102.2 70-130 0.00
Ref #180917 Cadmium, Total, ICAP/MS
Analyte Spiked Recovered Units Yield ('II) Limits (lis) RPD ('II)
Cadmium, Total, ICAP/KS 20 20 UGL 100.0 85-115
Cadmium, Total, lCAP/KS 20 20.2 UGL 101. 0 85-115 1.00
Cadmium, Total, lCAP/KS NO <0.50 UGL
Cadmium, Total, lCAP/KS 20 20 UGL 100.0 70~130
Cadmium, Total, lCAP/KS 20 20.2 UGL 101.0 70-130 1.00
Spikes which exceed Limits and Kethod Blanks with positive results are highlighted by Underlining.
Criteria for KS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 18 of 31
8-38
555 East Walnut Street Pasadena, California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 lABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) ( continued)
:0-'1"-3-;)2 Al0:53 IN
Laboratory QC Report
#100134
8-39
i~--------------~-------
[
QC
LCSl
LCS2
MBLK
MS
MSD
"..
L QC
LCSl
LCS2
( MSLK
MS
MSD
(
c QC
LeS1
LeS2
MBLK
MS
MSD
i I I I
QC Ref #180918 Barium, Total, ICAP/MS
QC
QC
Analyte Spiked Recovered Units Yield (!II) Limits ('Is) RPD (!II)
Barium, Total, lCAP/MS 100 97.4 UGL 97.4 85-115
Barium, Total, lCAP/MS 100 97.8 UGL 97.8 85-115 0.41
Barium, Total, lCAP/MS NO <2.00 UGL
Barium., Total, lCAP/MS 100 95.2 UGL 95.2 70-130
Barium, Total. lCAP/MS 100 97.7 VOL 97.7 70-130 2.6
Ref #180919 Antimony, Total, ICAP/MS
Analyte Spiked Recovered Units Yield (!II) Limits ('Is) RPD ('Is)
Antimony. Total, lCAP/MS SO 49.1 UGL 98.2 85-115
Antimony, Total, lCAP/MS SO 49.7 UGL 99.4 85-115 1.2
Antimony. Total, lCAP/MS NO <1.00 UGL
Antimony, Total, lCAP/MS SO 49.2 UGL 98.4 70-130
Antimony, Total. lCAP/MS SO 50.7 UGL 101.4 70-130 3.0
Ref #180920 Thallium, Total, ICAP/MS
.Analyte Spiked Recovered Units Yield ('Is) Limits (!II) RPD ('Is)
Tha11ium, Tota1, ICAP/MS 20.0 20.2 UGL 101.0 85-115
Thallium, Tota1, :rCAP/MS 20.0 20.1 UGL 100.5 85-115 0.50
Thallium, Total, :rCAP/MS NO <1. 00 UGL
Thallium, Total, lCAP/MS 20.0 19.6 UGL 98.0 70-130
Thallium, Total, :reAP/MS 20.0 20 UGL 100.0 70-130 2.0
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only. batch control is based on LCB. Criteria for duplicates
are adviSOry only, unless otherwise specified in the method.
QC Report - Page 19 of 31
I I I I
QC
LCSl
LCS2
HlILlC
KS
KSD
QC
LCS1
LCS2
c MBLlC
KS
KSD
QC
LCSl
HElLlC
KS
KSD
KS
LCS1
MBLK
KS I KSD
I LCS1
I I [
555 East Watnut Street Pasadena, California 9t 101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 600 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
QC Ref #180921 Lead, Total, ICAP/MS
Analyte Spiked Recovered
Lead, Total, ZCAP/KS 20 20.1
Lead, Total, ZCAP/KS 20 20.4
Lead, Total, ZCAP/KS NO <0.50
Lead, Total, ZCAP/KS 20 19.6
Lead, Total, ZCAP/KS 20 20
units
UGL
UGL
UGL
UGL
UGL
10-1J-J2 Al0:58 IN
Yield <'Is)
100.5
102.0
98.0
100.0
Laboratory QC Report
#100134
Limits <'Is) RPD <'Is)
85-115
85-115 1.5
70-130
70-130 2.0
QC Ref #180928 Chromium, Total, ICAP/MS
QC
Analyte Spiked Recovered units Yield ('Is) Limits <'Is) RPD
Chromium, Total, ZCAP/KS 100 100 UGL 100.0 I 85-115 )
Chromium. Total, ZCAP/KS 100 100 UGL 100.0 85-115 0.00
Chromium, Total, ZCAP/KS NO <1.00 UGL
Chromium, Total, ZCAP/KS 100 96.8 UGL 96.8 70-130
Chromium, Total, ZCAP/KS 100 98.2 UGL 98.2 70-130 1.4
Ref #181018 Aldicarbs
Analyte Spiked Recovered units Yield <'II) Limits <'Is) RPD
3-Hydroxycarbofuran 10.0 10.4 UGL 104.0 80-120
3-Hydroxycarbofuran NO <2.00 UGL
3-Hydroxycarbofuran 10.0 10.6 UGL 106.0 65-135
3-Hydroxycarbofuran 10.0 11.0 UGL 110.0 65-135 3.7
Spiked sample Lab II 22 08290062 NONE 0-0
A1dicarb ITemik) 10.0 8.56 UGL 85.6 80-120
A1dicarb ITemik) NO <0.50 UGL
A1dicarb ITemik) 10.0 10.5 UGL 105.0 65-135
A1dicarb ITemik) 10.0 10.4 UGL 104.0 65-135 0.96
A1dicarb sulfone 10.0 10.2 UGL 102.0 80-120
Spikes which exceed Limits and Kethod Blanks with positive results are highlighted by underlining.
Criteria for KS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
QC Report - Page 20
<'Is)
I'll)
of 31
8-40
I I
555 East Walnut Street Pasadena. California 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of water Supply (Hila) (continued)
Laboratory QC Report
#100134
8-41
1-------------------------
[
[
r iii
I I I
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LCS1
MBLK
MS
MSO
LeSl
MBLK
MS
MSO
LeS1
MBLK
MS
MSO
Aldicarb sulfone
Aldicarb sulfone
Aldicarb sulfone
Aldicarb sulfoxide
Aldicarb sulfoxide
Aldicarb sulfoxide
Aldicarb sulfoxide
Baygon
Baygon
Baygon
Baygon
Carbofuran (Furadan)
Carbofuran (Furadan)
Carbofuran (Furadan)
Carbofuran (Furadan)
Carbaryl
Carbaryl
Carbaryl
Carbaryl
Methiocarb
Methiocarb
Methiocarb
Methiocarb
Methomyl
Methomyl
Methomy1
Methomy1
Oxamy1 (vydate)
Oxamyl (vydate)
Oxamyl (Vydate)
Oxamyl (Vydate)
BOMC
BOMC
BOMC
BOMC
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
10.0
ND
10.0
10.0
100
100
100
100
<0.70
10.6
10.7
9.83
<0.50
10.6
10.8
9.96
<2.00
10.4
10.5
10.6
<0.90
10.9
11.6
8.98
<2.00
8.99
9.12
10.0
<2.00
9.89
10.5
10.2
<1.00
10.6
10.5
10.1
<2.00
10.3
10.4
129
101
85.9
96.5
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
%R
%R
%R
%R
106.0
107.0
98.3
106.0
108.0
99.6
104.0
105.0
106.0
109.0
116.0
89.8
89.9
91.2
100.0
98.9
105.0
102.0
106.0
105.0
101. 0
103.0
104.0
129.0
101. 0
85.9
96.5
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
80-120
65-135
65-135
70-130
70-130
70-130
0.94
1.9
0.96
6.2
1.4
6.0
0.95
0.97
12
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and OUP are advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
QC Report Page 21 of 31
~ ...
I I I
555 East Walnut Street Pasadena. caJilomla 91101 Tel: 626 568 6400 falc 626 568 6324 1 BOO 566 LABS (1 BOO 568 5227)
Hawaii Department of Water Supply (Hilo) . (continued)
Laboratory QC Report
#100134
8-42
I~-----------------------
[ QC
MS
LCSl
MBLK
MS
MSD
QC
MS
LCSl
LCS2
MBLK
MS
MSD c [ QC
LCSl
I LCS2
MBLK
MSl
MS2
I MSD
LCSl
LCS2
I MBLK
I I
QC Ref #181106 Endotha11
QC
QC
Analyte Spiked Recovered units Yield ('II) Limits (lis) RPD ('II)
Spiked sample Lab • 22 08290059 WI. 0-0
Bndothall 25 24.4 WI. 97.6 60-116
Bndothall NO <5.00 UGL
Bndothall 25 23.5 UCL 94.0 60-116
Bndothall 25 25.1 UGL 100.4 60-116 6.6
Ref #181453 Mercury
Analyte Spiked Recovered units Yield ('II) Limits (lis) RPD ('II)
Spiked sample Lab' 22 09030080 UGL 0-0
Mercury 1.50 1.36 UGL 90.7 85-115
Mercury 1.50 1.34 UGL 89.3 85-115 1.5
Mercury NO <0.20 WI.
Mercury 1.50 1.34 WL 89.3 70-130
Mercury 1.50 1.31 UGL 87.3 70-130 2.3
Ref #181471 Herbicides by 515.3
Analyte Spiked Recovered. Units Yield ('II) Limits ('II) RPD ('II)
2,4,5-T 0.75 0.86 UGL 114.7 70-130
2,4,5-T 3.0 3.00 UGL 100.0 70-130
2,4,5-T NO <0.20 UGL
2,4,5-T 3.00 3.15 UGL 105.0 70-130
2,4,5-T 0.75 0.77 UGL 102.7 70-130
2,4,S-T 3.00 3.20 UGL 106.7 70-130
2,4,5-TP (Silvex) 0.75 0.79 UGL 105.3 70-130
2,4,5-TP (Silvex) 3.0 2.63 UGL 87.7 70-130
2,4,S-TP (Silvex) NO <0.20 UCL
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report - Page 22 of 31
555 East walnut Street Pasadena, Callfomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 BOO 568 LABS (1 BOO 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
10-1'3-)2 A 10 :59 IN
Laboratory QC Report
#100134
8-43
[-------------------------
c r .. [
[
[
[
[
[
I I I I
MSl
MS2
MSO
LCSl
LCS2
MBLK
MSl
MS2
MSO
LCSl
LCS2
MBLK
MSl
MS2
MSO
LCSl
LCS2
MBLK
MSl
MS2
MSO
MSl
MS2
MSO
LCSl
LCS2
MBLK
MS1
MS2
MSO
LCSl
LCS2
MBLK
MSl
MS2
2,4,5-TP (Silvex)
2,4,5-TP (Silvex)
2,4,5-TP (Silvex)
2,4-0
2,4-0
2,4-0
2,4-0
2,4-0
2,4-0
2,4-DB
2,4-DB
2,4-DB
2,4-DB
2,4-0B
2,4-DB
Oichlorprop
Dichlorprop
Oichlorprop
Oichlorprop ,
Dichlorprop
Oichlorprop
Spiked sample
Spiked sample
Spiked sample
Acifluorfen
Acifluorfen
Acif1uorfen
Acifluorfen
Acifluorfen
Acifluorfen
Bentazon
Bentazon
Bentazon
Bentazon
Bentazon
3.00
0.75
3.00
0.375
1.5
NO
1.50
0.375
1.50
7.5
30.0
NO
30.0
7.50
30.0
1. 875
7.5
3.03
0.72
3.01
0.36
1.44
<0.10
1. 70
0.40
1. 69
7.13
26.1
<2.00
29.7
6.24
29.2
1. 90
6.69
NO <0.50
7.50 6.44
1. 875 1.66
7.50 6.44
Lab # 22 08290'087
Lab # 22 08290062
Lab # 22 08290087
0.75 0.83
3.0 2.91
NO
3.00
0.75
3.00
1. 875
7.5
NO
7.50
1.875
<0.20
3.27
0.75
3.31
2.09
7.23
<0.50
6.70
1. 93
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
NONE
NONE
NONE
UGL
lJGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
101. 0
96.0
100.3
96.0
96.0
113.3
106.7
112.7
95.1
87.0
99.0
83.2
97.3
101. 3
89.2
85.9
88.5
85.9
110.7
97.0
109.0
100.0
110.3
111.5
96.4
89.3
102.9
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
0-0
0-0
0-0
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and OUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 23 of 31
I I I I
[
[
[
I I I
MSD
LCS1
LCS2
MBLK
MS1
MS2
MSD
LCS1
LCS2
MBLK
MS1
MS2
MSD
LCS1
LCS2
MBLK
MS1
MS2
MSD
LCS1
LCS2
MBLK
MS1
MS2
MSD
LCS1
LCS2
MBLK
MS1
MS2
MSD
LCS1
LCS2
MBLK
MS1
1 0-1 3 - :J 2 AI 0 : 59 1:,1 , '\
555 East Walnut Street Pasadena. Califomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Bentazon
Dalapon
Dalapon
Dalapon
Dalapon
Dalapon
Dalapon
3.5-Dichlorobenzoic acid
3,5-Dichlorobenzoic acid
3,5-Dichlorobenzoic acid
3.5-Dichlorobenzoic acid
3.5-Dichlorobenzoic acid
3.5-Dichlorobenzoic acid
Tot DCPA Mono&Diacid Degradate
Tot DCPA Mono&Diacid Degradate
Tot DCPA Mono&Diacid Degradate
Tot DCPA Mono&Diacid Degradate
Tot DCPA Mono&Diacid Degradate
Tot DCPA Mono&Diacid Degradate
Dicamba
Dicamba
Dicamba
Dicamba
Dicamba
Dicamba
Dinoseb
Dinoseb
Dinoseb
Dinoseb
Dinoseb
Dinoseb
pentachlorophenol
Pentachlorophenol
Pentachlorophenol
Pentachlorophenol
7.50
3.75
15.0
NO
15.0
3.75
15.0
1.875
7.5
NO
7.50
1.875
7.50
0.75
3.0
NO
3.00
0.75
3.00
0.1875
0.75
NO
0.75
0.1875
0.75
0.75
3.0
NO
3.00
0.75
3.00
0.15
0.60
NO
0.60
6.57
3.88
14.4
<1.00
15.4
3.69
15.3
2.08
7.26
<0.50
7.50
1.88
7.60
0.91
3.24
<0.20
3.78
0.91
3.65
0.22
0.79
<0.08
0.97
0.19
0.97
0.8S
3.03
<0.20
3.36
0.79
3.33
0.18
0.58
<0.04
0.62
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
87.6
103.5
96.0
102.7
98.4
102.0
110.9
96.8
100.0
100.3
101.3
121.3
108.0
126.0
121.3
121. 7
117.3
105.3
129.3
101. 3
129.3
117.3
101.0
112.0
105.3
111.0
120.0
96.7
103.3
Laboratory QC Report
#100134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-13.0
70-130
70-130
70-130
70-130
70-130
70-130
70-130. )
70-130
70-130
70-130
70-130
70-130
70-130
70-130
( 70-130 )
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
QC Report Page 24 of 31
8-44
p" ...
L.
I f·
~
I E m
MS2
MSD
LCSl
LCS2
E MBLK
MSl
MS2
[ MSD
LCSl
LCS2
[ MBLK
MSl
MS2
MSD
[ LCSl
LCS2
MBLK
[ MSl
MS2
MSD
LCSl
r LCS2 ... MBLK
MSD
Ill"" LCSl
L LCS2
MBLK
MSD
I j;
I I I I [
1 () -I :3 - 0 2 A 1 0 : 5 9 I N
555 East Walnut Street Pasadena. Callfomia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
Pentachlorophenol 0.150 0.17
Pentachlorophenol 0.60 0.62
Picloram 0.375 0.43
Picloram 1.5 1-53
Picloram ND <0.10
Picloram 1. 50 1.85
Picloram 0.375 0.40
Picloram 1.50 1.87
4-Nitrophenol (qualitative) 3.75 4.16
4-Nitrophenol (qualitative) 15.0 14.1
4-Nitrophenol . (qualitati ve) ND <1.00
4-Nitrophenol (qualitative) 15.0 11. 9
4-Nitrophenol (qualitative) .3.75 3.40
4-Nitrophenol (qualitative) 15.0 11.4
2,4-Dichlorophenylacetic acid 100 110
2,4-Dichlorophenylacetic acid 100 98
2,4-Dichlorophenylacetic acid 100 101
2,4-Dichlorophenylacetic acid 100 94
2,4-Dichlorophenylacetic acid 100 109
2,4-Dichlorophenylacetic acid 100 90
Tot DCPA Mono&Diacid Degradate 0.75 0.91
Tot DCPA Mono&Diacid Degradate 3.0 3.25
Tot DCPA Mono&Diacid Degradate ND <1.00
Tot DCPA Mono&Diacid Degradate 3.00 3.65
2,4-Dichlorophenylacetic acid 100 110
2.4-Dich1orophenylacetic acid 100 98
2,4-Dichlorophenylacetic acid 100 101
2,4-Dich10ropheny1acetic acid 100 90
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
tR
tR
tR
tR
tR
tR
UGL
UGL
UGL
UGL
tR
\"R
\"R
tR
113.3
103.3
114.7
102.0
123.3
106.7
124.7
110.9
94.0
79.3
90.7
76.0
110.0
98.0
101.0
94.0
109.0
90.0
121.3
108.3
121. 7
110.0
98.0
101.0
90.0
Laboratory QC Report
#100134
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130 12
70-130
70-130
70-130 20
70-130
70-130
70-130
70-130
70-130 12
( 70-130) 20
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 25 of 31
8-45
I 555 East Walnut Street Pasadena. caJilomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) ( continued)
Laboratory QC Report
#100134
8-46
E~----~-----------------
QC
LCSl [
MBLK
MS
MSD [ MBLK
MS
MSD
LCSl [
MBLK
MS
MSD
LCSl
[ MBLK
MS
MSD
LCSl
MBLK
MS
MaD
LCSl
MBLK [ MS
MSD
LCSl
MBLK
MS
MSD
LCS1
MBLK
I KS
I I [
QC Ref #182826 525 Semivolatiles by GC/MS
Analyte Spiked Recovered Units Yield (%) Limits (%) RPD
alpha-Chlordane 2 1.76 UGL 88.0 ( 70-130 )
alpha-Chlordane NO <0.05 UGL
alpha-Chlordane 5 4.01 UGL 80.2 70-130
alpha-Chlordane 5 4.20 UGL 84.0 70-130 4.6
Diazinon NO <0.10 UGL
Spiked sample Lab " 22 08290076 NONE 0-0
Spiked sample Lab. " 22 08310027 NONE 0-0 0.24
Acenaphthylene 2 2.23 UGL 111.5 70-130
Acenaphthylene NO <0.10 UGL
Acenaphthylene 5 5.15 UGL 103.0 70-130
Acenaphthylene 5 5.45 UGL 109.0 70-130 5.7
Alachlor 2 2.26 UGL 113.0 70-130
Alachlor NO <0.05 UGL
Alachlor 5 5.10 UGL 102.0 70-130
Alachlor 5 5.37 UGL 107.4 70-130 5.2
Aldrin 2 2.09 UGL 104.5 70-130
Aldrin NO <0.05 UGL
Aldrin 5 4.41 UGL 88.2 70-130
Aldrin 5 4.85 UGL 97.0 70-130 9.5
Anthracene 2 1.84 UGL 92.0 70-130
Anthracene NO <0.02 UGL
Anthracene 5 4.37 UGL 87.4 70-130
Anthracene 5 4.68 UGL 93.6 70-130 6.9
Atrazine 2 1.84 UGL 92.0 70-130
Atrazine NO <0.05 UGL
Atrazine 5 4.32 UGL 86.4 70-130
Atrazine 5 4.56 UGL 91.2 70-130 5.4
Benz (a) Anthracene 2 1.92 UGL 96.0 70-130
Benz (a) Anthracene NO <0.05 UGL
Benz (a) Anthracene 5 4.43 UGL 88.6 ( 70-130 )
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP ar·e advisory only. batch control is based on LCS. Criteria for duplicates
are advisory only. unless otherwise specified in the method.
QC Report Page 26
(%)
of 31
555 East Walnut Street Pasadena. Galilornla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
10-'13-02 Al0:S·9 !N
Laboratory QC Report
#100134
8-47
1-------------------------
"'" L
[
c
I I I I [
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
MBLK
MBLK
LeSl
MBLK
MS
MSD
LCSl
ME!LK
MS
MSD
Benz (a) Anthracene
Benzo(a)pyrene
Benzo(a)pyrene
Benzo(a)pyrene
Benzo(a)pyrene
Benzo(b) Fluoranthene
Benzo(b) Fluoranthene
Benzo (b) Fluoranthene
Benzo(b) Fluoranthene
Benzo(g,h,i)Perylene
Benzo(g,h,i)Perylene
Benzo(g,h,i)perylene
Benzo(g,h,i)perylene
Benzo(k) Fluoranthene
Benzo (k) Fluoranthene
Benzo(k) Fluoranthene
Benzo (k) Fluoranthene
Di(2-Ethylhexyl)phthalate
Di(2-Ethylhexyl)phthalate
Di(2-Ethylhexyl)phthalate
Di(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Butylbenzylphthalate
Butylbenzylphthalate
Butylbenzylphthalate
Bromacil
Butach10r
Caffeine
Caffeine
Caffeine
Caffeine
Chrysene
Chrysene
Chrysene
Chrysene
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
NO
ND
2
ND
5
5
2
ND
5
5
4.66
2.16
cO.02
5.08
5.30
2.23
cO.02
4.95
5.37
2.25
cO.05
5.56
5.69
2.22
cO.02
5.07
5.14
2.02
cO.60
4.28
4.08
1.99
cO.50
4.47
4.91
<0420
cO.05
1. 02
cO.05
3.60
3.97
2.19
cO.02
5.14
5.34
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
93.2
108.0
101. 6
106.0
111.5
99.0
107.4
112.5
111.2
113.8
111.0
101.4
102.8
101.0
85.6
81.6
99.5
89.4
98.2
51.0
72 .0
79.4
109.5
102.8
106.8
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
50-110
50-110
50-110
70-130
70-130
70-130
5.1
4.2
8.1
2.3
1.4
4.8
9.4
9.8
3.8
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 27 of 31
555 East Walnut Street Pasadena. Califomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of water Supply (Hilo) (continued)
OJ Q-1 3 - 0 2 ft, 1 0 : 5 ~' I ~r
Laboratory QC Report
#100134
8-48
~-------------
[
[
c
I I I
LCSl
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
MBLK
LCSl
MBLK
MS
MSD
MBLK
LCSl
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
LeS1
MBLK
MS
MSD
LeSl
MBLK
MS
MSP
LeSl
Dibenz(a,h)Anthracene
Dibenz(a,h)Anthracene
Dibenz(a,h)Anthracene
Dibenz(a,h)Anthracene
Di-(2-Ethylhexyl)adipate
Di-(2-Ethylhexyl)adipate
Di-(2-Ethylhexyl)adipate
Di-(2-Ethylhexyl)adipate
Diethylphthalate
Diethylphthalate
Diethylphthalate
Diethylphthalate
Dieldrin
Dimethylphthalate
Dimethylphthalate
Dimethylphthalate
Dimethylphthalate
Dimethoate
Di-n-Butylphthalate
Di-n-Butylphthalate
Di-n-Butylphthalate
Di-n-Butylphthalate
Endrin
Endrin
Endrin
Endrin
Fluoranthene
Fluoranthene
Fluoranthene
Fluoranthene
Fluorene
Fluorene
Fluorene
Fluorene
gamma-Chlordane
2
ND
5
5
2
ND
5
5
2
ND
5
5
ND'
2
ND
5
5
ND
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
2.28
<0.05
5.39
5.44
1. 89
<0.60
4.04
4.93
1. 92
<0.50
4.77
5.01
<0.20
2.08
<0.50
4.80
5.16
<10.00
2.07
<0.50
4.74
5.19
2.11
<0.10
4.56
5.39
2.18
<0.10
5.00
5.28
1.40
<0.05
4.28
4.78
1. 95
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
114.0
107.8
108.8
94.5
80.8
98.6
96.0
95.4
100.2
104.0
96.0
103.2
103.5
94.8
103.8
105.5
91.2
107.S
109.0
100.0
105.6
70.0
85.6
95.6
97.5
( 70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
0.92
20
4.9
7.2
9.1
17
5.4
11
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlininq.
Criteria for MS and DUP are advisory only, batch control is based on LeS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC Report Page 28 of 31
I 555 East Walnut Street Pasadena. california 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 800 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
10-13-J:2 Al0:59 p~
Laboratory QC Report
#100134
8-49
E~--------------~-------[
[
[
[
[ ,... L
(
I I I I
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
LCS1
MBLK
MS
MSD
MBLK
LCS1
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
MBLK
LCS1
MBLK
gamma-Chlordane
gamma-Chlordane
gamma-Chlordane
Hexachlorobenzene
Hexachlorobenzene
Hexachlorobenzene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachlorocyclopentadiene
Hexachlorocyclopentadiene
Hexachlorocyclopentadiene
Heptachlor
Heptachlor
Heptachlor
Heptachlor
Heptachlor Epoxide
Heptachlor Epoxide
Heptachlor Epoxide
Heptachlor Epoxide
Indeno(l,2,3,c,d)Pyrene
Indeno(l,2,3,c,d)Pyrene
Indeno(l,2,3,c,d)Pyrene
Indeno(1,2,3,c,d)Pyrene
Isophorone
Lindane
Lindane
Lindane
Lindane
Methoxychlor
Methoxychlor
Methoxychlor
Methoxychlor
Metribuzin
Molinate
Molinate
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
2
ND
5
5
ND
2
ND
5
5
2
ND
5
5
ND
2
ND
<0.05
4.17
4.39
1.91
<0.05
4.26
4.46
1. 85
<0.05
2.46
4.57
1.94.
<0.04
4.54
4.66
1.94
<0.02
4.38
4.55
2.47
<0.05
5.70
5.84
<0.50
2.12
<0.02
4.88
5.18
2.06
<0.05
4.86
5.38
<0.05
2.10
<0.20
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
83.4
87.8
95.5
85.2
89.2
92.5
~ 91.4
97.0
90.8
93.2
97.0
87.6
91.0
123.5
114.0
116.8
106.0
97.6
103.6
103.0
97.2
107.6
105.0
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
( 70-130
70-130
70-130
70-130
70-130
70-130
( 70-130 )
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
5.1
4.6
60
2.6
3.8
2.4
6.0
10
QC Report Page 29 of 31
I 555 East Walnut Street . Pasadena, Califomla 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 1100 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) ( continued)
10-13-J2 A10:59 Ii'l
Laboratory QC Report
#100134
8-50
~-------------------------
[
c r .. £ I I I
MS
MSD
LeSl
MBLK
MS
MSD
LeSl
MBLK
MS
MSD
LeSl
MBLK
MS
MSD
LeSl
MBLK
MS
MSD
MBLK
MBLK
LeSl
MBLK
MS
MSD
LeSl
MBLK
MS
MSD
LCSl
MBLK
MS
MSD
LCSl
MBLK
MS.
Molinate
Molinate
Metolachlor
Metolachlor
Metolachlor
Metolachlor
trans-Nonachlor
trans-Nonachlor
trans-Nonachlor
trans-Nonachlor
Pentachlorophenol
Pentachlorophenol
Pentachlorophenol
Pentachlorophenol
Phenanthrene
Phenanthrene
Phenanthrene
Phenanthrene
Prometryn
Propachlor
pyrene
Pyrene
Pyrene
Pyrene
Simazine
Simazine
Simazine
Simazine
Perylene-d12
Perylene-d12
Perylene-d12
Perylene-d12
1,3-dimethyl-2-nitrobenzene
1,3-dimethyl-2-nitrobenzene
1,3-dimethyl-2-nitrobenzene
5
5
2
NO
5
5
2
NO
5
5
8
NO
20
20
2
NO
5
5
NO
NO
2
NO
5
5
2
Nt>
5
5
100
100
100
100
100
100
100
5.19
5.25
2.33
<0.05
5.27
5.55
1.87
<0.05
4.16
4.35
9.22
<1.00
21.0
23.2
2.07
<0.02
4.77
5.15
<0.50
<0.05
2.46
<0.05
5.62
5.95
2.08
<0.05
4.72
5.06
107
92
102
102
92
95
90
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
UGL
'UGL
UGL
UGL
UGL
UGL
UGL
tR
tR
tR
%R
%R
%R
tR
103.8
105.0
116.5
105.4
111.0
93.5
83.2
87.0
115.3
105.0
116.0
103.5
95.4
103.0
123.0
112.4
119.0
104.0
94.4
101.2
107.0
92.0
102.0
102.0
92.0
95.0
90.0
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
70-130
( 70-130 )
1.1
5.2
4.5
10.0
7.7
5.7
7.0
0.00
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on Les. Criteria for duplicates
are advisory only, unless otherwise specified in the method.
QC 'Report Page 30 of 31
-. .. ... L.
I ,A~
I I !
MSD
LCSl
MBLK
MS
[ MSD
LCSl
MBLK
L MS
MSD
MBLK
[
[
L [
[
I I I I I [
8-51 lC)-iJ-;2 F\1'):59 !\)
555 East Walnut Street Pasadena, Calilornia 91101 Tel: 626 568 6400 Fax: 626 568 6324 1 600 568 LABS (1 800 568 5227)
Hawaii Department of Water Supply (Hilo) (continued)
1,3-dimethyl-2-nitrobenzene 100
Triphenylphosphate 100
Triphenylphosphate 100
Triphenylphosphate 100
Triphenylphosphate 100
Thiobencarb 2
Thiobencarb NO
Thiobencarb 5
Thiobencarb 5
Trifluralin NO
90
112
115
108
108
2.00
<0.20
4.57
5.29
<0·.10
tR 90.0
tR 112.0
tR 115.0
%R 108.0
%R 108.0
UGL 100.0
UGL
UGL 91.4
UGL 105.8
UGL
Laboratory QC Report
#100134
70-130 0.00
70-130
70-130
70-130 0.00
70-130
70-130
70-130 15
Spikes which exceed Limits and Method Blanks with positive results are highlighted by Underlining.
Criteria for MS and DUP are advisory only, batch control is based on LCS. Criteria for duplicates
are advisory only, unless otherwise specified in t·he method.
QC Report Page 31 of 31
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1J-13-::12 Al0:59 IN~-52
._,/ ace Analyticar~ Pace AnalytIcal Services, Inc. tI J"jtJ{f( / 1100 Elm Street, Suite 200
I 0 I J if.. Minneapolis, MN 55414
.. ' 7I'(f' ~ www.paceJabs.com () / . Phone: 612.601.1100
Fax: 612.601.6444
This report contains..!. pages.
The results reported herein conform to the most current NELAC standards, where applicable, unless otherwise narrated in the body ofthe report.
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced. except in full.
without the written consent of Pace Analytical Services. Inc.
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ace Analytica/® www.pacelabs.com
September 17, 2002
Attn: Martha Frost MWH 555 East Walnut Street Pasadena, CA 91101
Dear Ms. Frost:
'I C- 'I J -:) 2 A 1 ~) : 59 I:~ 8-53
Pace Analytical Services, Inc. 1700 Elm Street, Suite 200
Minneapolis, MN 55414 Phone: 612,601.1700
Fax: 612,607.6444
MWL Project # 100134 MWL Sub PO # 99-8651 Pace Project # 1062106 m State Cert. #: 2155 Expiration Date: 6/30/03
Enclosed are analytical results of one water sample analY.led for 2,3,7,8-TeDD content. This sample was analyzed according to Method 1613B by High Resolution Gas ChromatographylHigh Resolution Mass Spectrometry.
MWL Sample ID Pace Sample ID Date Collected Date Received
2208300156 3824942 08/28/02 09/04/02
The results reported for this sample and the associated quality control samples were all within the criteria described in Method 1613B. If you have any questions or concerns regarding these results, please contact me at (612) 607-6331, by facsimile at (612) 607-6444 or bye-mail atDan.Hoseck@pacelabs.com.
Sincerely,
Dan Hoscck, Project Manager High Resolution Mass Spectrometry
Enclosure
REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
In:r··era:·· '~:~tC~1~~'i "": , ... .0:: .;¥
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8·54
10-13-J2 A10:59 I~;
P"oICC AnaIyticaIServiCC$. Inc. 1100 Eltn Sl{eCl- Suite 200
Minneapolis. MN 55414-
Tel: 612·607-1100 Drinking Water Analysis Results Pax: 612.607-6444
2,3,7,8-TCDD - USEPA Method 1613B MWH Laboratories
Sample ID ••••••••••• 2208300156 Source ID ............. Kaieie Mauka Exploratory Well Project # ............... 100134 Sub PO # .............. 99-8651 Lab Sample 10 ..... 103824942
[2,3,7,8-1rCDD]
RL
2,3,7,8-TCDD Recovery
Spike Recovery Limit
RPD
IS Recovery
IS Recovery Limits
CS Recovery
CS Recovery Limits
Filename Analysis Date Analysis Time Analyst Volume Dilution ICALDate CCAL Filename
Sample 2208300156
ND
5 pgIL
86%
31-137%
115%
42-164%
A20913B_13 09/14/2002
00:34 CMP
1.032L NA
08/28/2002 A20913A_2
ND = Outside the Control Limits = Not Detected
RL = Reporting Limit
Date CoIIected .... . 08/28/2002 Spike .................... 200 pg Date Received ...... 09/04/2002 IS Spike ................ 2000 pg Date Extracted .... . 0911212002 CS Spike .............. 200 pg
Method Blank
ND
5 pgIL
76%
31-137%
120%
42-164%
A20913B_3 0911312002
18:42 CMP
1.036L NA
08/28/2002 A209.13A_2
Lab Spike
93%
73-146%
70%
25·141%
112%
37-158%
A20913B_l 09113/2002
17:31 CMP
1.034L NA
08/28/2002 A20913A_2
10.2%
Lab SpikeDup
84%
73-146%
83%
25-141%
118%
37-158%
A20913B_2 0911312002
18:06 CMP
1.035L NA
08/28/2002 A20913A_2
Analyst: ~~ilI=M,-,--__
Limits RPD
= Control Limits from Method 1613 (10/94 Revision), Tables 6A and 7 A = Relative Percent Difference of Lab Spike Recoveries
IS = Internal Standard [2,3,7,8-TCDD· 13CI2] CS = Cleanup Standard [2.3.7,8-TCDD-37CI4]
Project No .............. 1062106
r ..
Appendix C
Data Regarding USGS Monitor Well No. 4708-02
Tom Nance Water ~ Resource Engineering
September 4, 2002 02/403 (98-03)
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Mr. Gordon Tribble District Chief Water Resources Division U.S. Geological Survey an Ala Moana Boulevard - Suite 415 Honolulu, Hawaii 96813
Dear Mr. Tribble:
Monitoring in USGS Well 4708-02 During 'Pump Testing of DWS' Kaieie Mauka Well, State No. 4708-03
Kalele, Soyth Hilo, Hawaii
Pump testing of DWS' Kaleie Mauka Well was completed on August 30th arid my equipment has now been removed from the USGS' nearby monitoring well. In order to produce useable yield, it was necessary to drill DWS' well to 170 feet below sea level, substantially deeper than the USGS well. There are a number of other differences between the two wells:
•
•
•
Groundwater in the DWS well stands about 27 feet above sea level, some 117 feet lower than the 144-foot level In the USGS well. No water level response to pumping in the USGS well was measured when pumping of the DWS well was conducted (refer to enclosed Figure 1; pumping In the DWS well was at. about 370 GPM). Water in the USGS well is more than 2° F.cooler than in the DWS well (Figure 2).
Also, in response to a rainstorm in June, a water level rise in excess of 10 feet was 'recorded In . the USGS well (Figure 3). This response, along with the other differences noted above, suggest that there may not be much value in continuing to monitor the water level in the USGS well.
Thank you for providing access to your well to enable it to be used for our monitoring purposes. The key to the well is being returned to Dale Nishimoto in your Hilo office along with a copy of this letter.
Sincerely.
Tom Nance
cc: Shari Komata - DWS Dale Nishimoto - USGS Hilo
Attachments
680 Ala Moana Boulevard, Suite 406 • Honolulu, Hawaii 96813-5411 • Phone: (808) 537-1141 • Fax: (808) 538-7757· E-mail: office@tnwre.com
C-1
1""""1 ~ .. _ .. r::I 1-', rI r'1 r'l r1 F1 r1 rl r1 ~ r1 r1 11·
144.5
144.0
........
...I Cf)
~ 143.5 LU LU LL. -...I ~ 143.0 LU
. """-...I
0:: LU J-~ 142.5 ...I ...I LU ~ ~ 142.0 Cf) :::>
141.5
141.0 23
FIGURE 1. WATER LEVEL IN THE USGS MONITOR WELL DURING THE KAIEIE MAUKA PUMP TEST
f:~ ~~ '"('t(C'~ ~~t'2 .' - ... --- .... --- - - ~'-
~al-L- _ - -
- ~6-Utua CO t-!SQAI tz ~~ -. ~ ~~ ~ ...
..... ~ ..... .... , ..... ~ .,.. "'"'..".... ,..... ...... ,.
24 25 26 27 28 29
DAY IN AUGUST 2002
I~USGS MONITOR WELL -KAIEIE MAUKA WELL I
28.5
- ~ - 28.0 "] - .J
...I Cf)
::2: 27.5 tu
LU -.- LL. -...I LU
27.0 Gj ,.. ...I 0:: LU
~ 26.5 ~
';2 :::> ~
~ • .J.I. -.. ' ::2:
26.0 LU ~ w · · ~ \
-J ·
25.5
25.0 30 31
(') I I\)
1"'"1 iJ .. 11ft III!I .. F'1 r1 r1 r1 r1 r-t r1 f""'I ftl .... Ibl I!!I r1
FIGURE 2. COMPARISON OF TEMPERATURES IN THE DWS AND USGS KAIEIE WELLS AUGUST 26 TO 30, 2002
69.0 rl ----r-----,--------,-----,-----.,.....,....-----. I- ~
69.0
68.5 ~ 1 68.0 ~ • . \ j l 1 67.5 I ....
~ .. . .., r ,~ .... "' ...... ' ... ,. .. , ~ ~ 67.0
i 66.5 ~ ~
~ 66.0 ! ~ ~ W I-
65.5 ~ 1 65.0 ~ '0/1 "wry- ..... II ,otII't_ \ 11Op:1 , •• :1 /: "'"" .. ni" ~., I.,,,, •• f" .. ,_..... ~
6~5 l \ . 1 64.0 ~ I I I I I . I I II I I I ~
68.5
68.0
67.5
67.0
66.5
66.0
65.5
65.0
64.5
64.0 26 27 28 29 30 31
DAY IN AUGUST 2002
I~DWS WELC'=-USG8WELL I
.J
"
,~
o I
eN
~~---~~~~~~~~~~~~~~
160
155
::::J (J) 150 :2: IW W LL -m 145 > w ...J a: w ~ 140
135
130 14
~
FIGURE 3. WATER LEVEL AND TEMPERATURE IN THE USGS MONITOR WELL JUNE 14 TO 28, 2002
-W~
~ ~t fl3~ 1;i ~,.n ~
V"'-m ?1:;rdJ ~
J ~~~ ~ -- ~
\ \ ~
fJ~ ~ . 'I( r~ ~ ~ ~ ~ V rw. ~ ~ LII ..... \I~
~ "
--'- ... . .. . . -
15 16 17
~
.
18 19 20 21 22 23
DAY IN JUNE 2002 24 25 26 27 28
I-LEVEL -TEMP I
66.25
66.00
65.75 LL (!J w o -w a:
65.50 ~
a: w a.. :2:
65.25 ~
65.00
64.75
~
,~
(') . .j>.
Appendix 0
Specifications and Plan for the Well Pump
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TNWRE Goulds Turbine Pump Selection ver: 6.00a 11/18/02
Curve: 1012-5
PUMP DATA SHEET
Goulds Turbine 60 Hz
Design Point: Flow: 100 US gpm Head: 1190 ft
Pump: TURBINE - 3600 Speed: 3450 rpm
Limits: Temperature: -- of Pressure: 430 psig
Specific Speed: Ns: 1290
Size: 7RAHC; (15 stages) Dia: 4.625 in
Sphere size: 0.18 in Power: --- bhp
Nss: ---
Dimensions: Suction: --- in Discharge: -- in
Vertical Turbine: Bowl Dia: 7.5 in Max Lateral: 0.25 in Thrust K Factor: 1.61
Motor: 50 hp Speed: 3600 Frame: 326TS NEMA Standard TEFC Enclosure sized for Max Power on Design Curve
Fluid: Water
NPSHa: --- ft
Piping:
Discharge Sizes-3",4"
--- Data Point --
Flow: 100 US gpm
Head: 1212 ft
Eff: 73.2%
Power: 41.8 bhp
NPSHr: 9.98 ft
ft 2000
1600
1200
800
400
0
~.Il :') .,."
~ [1 17
~'
N 'l
P
Selection file: (untitled)
Catalog: TURB60.MPC v 1.6.1
Temperature: 60 of SG: 1 Viscosity: 1 .122 cP Vapor pressure: 0.2568 psia Atm pressure: 14.7 pSia
System: -Suction: -'-- in Discharge: -- in
.,
I--"'" l---
--
-- Design Curve -
Shutoff Head: 1499 ft
Pressure: 649 psig
Min Flow: - US gpm
BEP: 73.5% eff S 1h e-i--@ 103 US gpm
NOL Pwr: 49.7 bhp @ 151 US gpm
- Max Curve -
Max Pwr: 54.5 bhp @ 156 US gpm
Flow Speed USgpm rpm
120 3450 100 3450 80 3450 60 3450 40 3450
H r n
r- I--
US gpm 20 40 60 80 100 120 140 160 180
-- PERFORMANCE EVALUATION --
Head Pump Power NPSHr Motor Motor Hrslyr Cost ft %eff bhp ft %eff hp IkW
1075 71.7 45.4 12.1 1212 73.2 41.8 9.98 1319 70.2 37.9 9 1397 63.5 33.3 8.98 1442 48.6 30 8
50 b h
25 p
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