xe vessel pumpout

3
The scheme below distributes Xenon to and from the vessel through a set of 72 flow tubes. Thes are PTFE tubes located in the interstitial space behind the quartz tubesThe flow path from the Xenon vessel interior out to vacuum pumps is through a series of graded orifi in each tube ( to equalize flow both top to bottom and transversely), through the tube, through an inlet tube, then to one of two large diameter manifolds (one inlet, one outlet), and finally out through several large diameter tubes which lead out of the water tank. A cross section detail is shown below: Q m 80 torr L s = Q m v a d tube 3 l tube ΔP tube := then: v a 124 m s := ΔP tube 1torr := l tube 1in := d tube 1in := Since Mathcad does real units , let: Q mol 80 d tube 3 l tube ΔP tube := Q m π d tube 3 12l tube v a P e P i - ( ) := for dry air@20C, d, L in inches Q in (torr *L) /s equation is: Tube gas conductance, molecular flow, from Practical Vacuum Techniques , Brunner & Batzer, 1974 Xenon Vessel Pumping Speed D. Shuman 3/5/11 DRAFT

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Page 1: Xe Vessel Pumpout

The scheme below distributes Xenon to and from the vessel through a set of 72 flow tubes. Thes are

PTFE tubes located in the interstitial space behind the quartz tubesThe flow path from the Xenon vessel

interior out to vacuum pumps is through a series of graded orifi in each tube ( to equalize flow both top to

bottom and transversely), through the tube, through an inlet tube, then to one of two large diameter

manifolds (one inlet, one outlet), and finally out through several large diameter tubes which lead out of the

water tank. A cross section detail is shown below:

Qm 80torr L⋅

s=Qm

va dtube3

ltube

∆Ptube⋅:=

then:

va 124m

s:=∆Ptube 1torr:=ltube 1in:=dtube 1in:=

Since Mathcad does real units , let:

Qmol

80 dtube3

ltube

∆Ptube⋅:=

Qm

πdtube3

12ltube

va⋅ Pe Pi−( )⋅:=

for dry air@20C, d, L in inches Q in (torr *L) /s equation is:

Tube gas conductance, molecular flow, from Practical Vacuum Techniques , Brunner & Batzer, 1974

Xenon Vessel Pumping SpeedD. Shuman 3/5/11DRAFT

Page 2: Xe Vessel Pumpout

Cm_ft

va dft3

0.5lft

:= Cm_tm

va dtm3

ltm

:= Cm_man

va dman3

lman

:= Cm_mp

va dmp3

lmp

:=

Cm_ft 0.1L

s= Cm_tm 0.1

L

s= Cm_man 41.3

L

s= Cm_mp 45.9

L

s=

Assume bends are negligible compared to length of tube, then total conductance is:

Cm_tot nft Cm_ft⋅( )1−

nfm Cm_tm⋅( )1−

+ nman Cm_man⋅( )1−

+ nmp Cm_mp⋅( )1−

+

1−

:=

Cm_tot 2.968L

s=

Most pumps have pumping speeds much higher than this, so this conductance will dominate and set

the pumping speed. To find pressure in Xe vessel, we need to estimate outgassing rate for Xe vessel.

Plexiglass outgassing rate, from chart: http://www.ece.ualberta.ca/~schmaus/vacf/outgas.html

qPMMA 106− torr L⋅

s cm2

:= after full degassing

Area of Xenon vessel

AXe_v 2πrXe2

2πrXe lXe⋅+:= AXe_v 5.932 m2

=

Total outgass rate:

QXe_v qPMMA AXe_v⋅:= QXe_v 0.059torr L⋅

s=

Equilibrium pressure in Xe vessel

Conductance path, from Xe interior to vacu pumps (assume 4, one one for each support leg):

number in parallel

nft 72:=dft .78cm:= lft 1.6m:=

Xe flow tube

dtm 0.7cm:= ltm 40cm:= nfm 72:=Xe inlet/outlet tube

dman 10cm:= lman 3m:= nman 2:=manifold

dmp 10cm:= lmp 2.7m:= nmp 4:=manifold to pump(s)

The flow holes are graded in size, in order to match flow rates through them from top to bottom. the

lower holes must have a smaller diameter to match the conductance of the tube plus the largest hole at

the top, further assume tube is open at top. Before we can go further with this design, we need to know

the desired flow rate of Xe through the vessel. We will simplify here by assuming the tube "disappears"

at the top and its effective conductance will be the conductance of a half height tube (effective tube

height will likely be less). Conductances, for molecular flow are:

Flow tube inlet/outlet tube manifold manifold to pump line

Page 3: Xe Vessel Pumpout

This is an inconsequential amount of Xe in the buffer region, regarding dielectric strength and cost, so it

does not appear that N2 gas circulation is needed to reduce this to a lower concentration. N2 buffer gas

circulation might be desirable for other reasons, however.

CostXe 10euro

gm=CostXe

106euro

100kg:=MXe_buf 2.715 gm=MXe_buf

1m3

PXe_buf⋅ Ma_Xe⋅

R 293⋅ K:=

PXe_buf 0.365 torr=PXe_buf 108−torr

2QXe R 293⋅ K( )⋅

0.1Cm_tot

+:=

This does not include leaks, which will likely double the flux into N2. There will need to be cryopumping

of the N2 to reclaim Xe, it is not clear whether circulation will also be needed; Xe will likely find its way

to cryopanels outside. Assuming a Xe partial pressure of 10^-8 torr at a cryopanel surface combined

with a pumping speed 10% of that for the Xe vessel, we find an Xe partial pressure and mass in the N2

buffer region:

Ma_Xe QXe⋅ 12.71kg

yr=Ma_Xe QXe⋅ 0.403

mg

s=In mass terms:

QXe 2.962 106−

×mol

s=QXe

Ci

0.5cmDXe_PP⋅ AXe_v⋅:=

Flux through walls, from Fick's Law (assume vessel walls and ends = 0.5 cm thick)

Ci 624.094mol

m3

=Ci

PMOPa

R 293⋅ K:=v

RT

P:=Ci

1

v:=

Xe concentration in Xe vessel

DXe_PP 4 1012−

⋅m

2

s:=

(assume at room temp, not stated in ref)

From Xenon Self-Diffusion in organic polymers by Pulsed Field Gradient NMR Spectroscopy, Junker &

Veeman 1998, self-diffusion coefficient for polypropylene (assume similar to acrylic) is:

Xenon diffusion through Acrylic Xenon vessel

this may actually be in viscous flow mode PXe_v 0.02 torr=PXe_v 106−torr

QXe_v

Cm_tot

+:=