x-ray diffractometer xrd-6000
DESCRIPTION
riccat_sihotangTRANSCRIPT
X-ray Diffractometer
XRD-6000
Application Field of X-ray Diffractometer
Achievement of shimadzu XRD
NaCl Diamond
Unit Cell of NaCl
PDF2 Data of NaCl
Data list of Carbon in PDF2
DiamondC60Graphite
Crystal Structures of different Carbons
Diamond
C60
Graphite
History of Shimadzu X-ray DifractometerProducts Outline
1945 World first XRD
1996 XRD-6000 Windows95 operated XRD
1962 GX-31958 GX-21955 GX-1
Stand-alone XRD
Shimadzu first XRD}1970 VD-21965 VD-1 }Automated recording XRD with
GRS matching start function
1978 XD-3A,5A1974 XD-3,5 }Fully automated XRD with
small & safety case
1986 XD-610 Computer controlled XRD
1992 XD-D1 Fully computerized XRD
XRD-6000
Big Features of XRD-6000
1. Compact & Safety Case Design
2.High Precision & Very StableVertical Goniometer
XRD-6000
3.User Friendly Operation(Windows95/98)
1.Compact & Safety Case Design
・ Size of Main BodyW900×D700×H1600
・ Door is Locked whenthe X-ray Power is ON
・ No Switch for Cancellation of Interlock system
900 700
1600
XRD-6000
2.High Precision & Very StableVertical Goniometer
・ Angle Reproducibility±0.001 ゜ (2θ)
・ Scanning Angle Range-6 ~+ 163 ゜( 2θ )-180 ~+ 180 ゜( θ )
・ θ-Axis oscillationEquipped as Standard
XRD-6000
3.User Friendly Operation (Windows95/98 or NT)
・ Multitasking
・ Mouse Operation
・ Easy to Upgrade(H/W,S/W)
・ Ready for Network
・ Easy to Transfer the Datato the General-purposeS/W such as MS-Wordor Excel
XRD-6000
MeasurementSection
Basic Data Processing
SearchMatch
Quant.Calc Advanced Data Process
Standard Configuration Optional Software
XRD-6000 Main Window
XRD-6000
XRD-6000 STATUS DISPLAY WINDOW
X-RAY POWER CONTROL WINDOW
XRD-6000
GONIOMETER OPTICAL ADJUSTMENT
XRD-6000
MEASUREMENT CONDITION EDITING
XRD-6000
MEASUREMENT WINDOW
XRD-6000
XRD-6000
BASIC DATA PROCESSING
BASIC DATA PROCESSING
XRD-6000
BASIC DATA PROCESSING
XRD-6000
SEARCH/MATCH
XRD-6000
SEARCH/MATCH
XRD-6000
Search/Match result of some Minerals
Anorthite
Albite
Augite
Search/Match result of some Minerals
QANTITATIVE ANALYSIS
XRD-6000
CALIBRATION CURVE
XRD-6000
CALIBRATION CURVE
XRD-6000
QUANTITATIVE ANALYSIS
Thin Film Attachment
Specification・ Sample StageRotation 360°Fixation Vacuum SackingSize(max) φ102x10mm・ Adjustment for Sample Surfaceby Micrometer Head・ Rotation Speed 72rpm・ β-axis MeasurementContinuous/step scan・ Monochrometer Graphite
XRD-6000
Crystalinity Measurement
Calculation of Crystallite Size and Lattice Strain
β = β s+ βoβs: FWHM for Crystallite Size(D)
βo :FWHM for Lattice Strain(η)
β = β s+ βo =
β s= λ D ・ Cosθ
βo = 2η ・ Sinθλ
Sinθλ
λ D ・ Cosθ
+
β ・ Cosθλ
+ 2η ・ Sinθλ
1D=
Hall’s equation
Crystallite size & Lattice Strain
Counter Monochromator for XRD-6000
Rotational Sample Stage for XRD-6000
Environmental Measurement Stage for XRD-6000
Sample Heating Attachment for XRD-6000
Sample Heating Attachment for XRD-6000Low Temperature Stage TTK-450
Main Specification
Temperature Range -193 through 450degSize of ApparatusOuter Diameter 105mmThickness 60mmWindow for X-ray 12mm/200degMaterial of X-ray Window25 micron KAPTON Thin FilmDetector for TemperaturePlatinum(PT100)Consumption Rate of Liquid Nitrogen1.5 litter/hour(at -193degree)
TTK-450 Low Temperature Stage
TTK-450 Low Temperature Stage
Application Data by TTK-450
Main Specification
Sample Heating Attachment for XRD-6000High Temperature Stage HTK-1200
Temperature Range RT through 1200degSize of ApparatusOuter Diameter 150mmThickness 60mmWindow for X-ray 10mm/200degMaterial of X-ray Window25 micron KAPTON Thin FilmDetector for TemperatureThermocouple(Pt-PtRh)AtmosphereAir,Inert Gas, Vacuum, Corrosive Gas
HTK-1200 High Temperature Stage
HTK-1200 High Temperature Stage
Pole Figure Attachment for XRD-6000
Advanced Crystal Structure Analysis
• Precise Lattice Constant Calculation • Crystal System Determination• Rietveld Analysis (with NARiet
process)Refine Crystal ParametersQuantitative Analysis of Multi ComponentCrystal Solid Model Display
TiO2 Rutile structure
Ti
O
Fulleren C60 structure
Summary
1. Shimadzu XRD has long history
2. Shimadzu XRD-6000 is most compact & safety
3. Shimadzu XRD-6000 has most stable hardware
4. Shimadzu XRD-6000 has user friendly S/W
5. Shimadzu XRD-6000 has more capability