5% PAN to DMFrpm radian/s 1st Run 2nd Run

10 1.04719755 Shear (s-1) RPM Viscocity [cP] Torque % RPM0.6002742455 0.3 145.8 3.8 0.3

CP-41 1.200548491 0.6 74.8 3.9 0.6angle (deg) 3 3.0013712275 1.5 62.2 7.9 1.5radius (cm) 2.4 6.0027424549 3 48 12.5 3speed (rpm) 10 12.00548491 6 51 26.5 6speed (rad/s) 1.04719755 24.01096982 12 49 50.8 12sin of angle 0.052335956 40.018283033 20 - - 20

Viscocity 51.49shear rate 20.00914152

4% PAN to DMF1st Run 2nd Run

Flow rate 1.5 mL/hr Shear (s-1) RPM Viscocity [cP] Torque % RPMDiamter 0.33 mm 1.0004570758 0.5 27.6 1 0.5Shear rate 118.0992241 s-1 2.0009141516 1 42.6 3.7 1

4.0018283033 2 48.3 8.6 25.0022853791 2.5 48.8 10.6 2.58.0036566066 4 46 16 410.004570758 5 43.5 18.9 520.009141516 10 44.1 38.2 1040.018283033 20 45.8 79.7 20100.04570758 50 - - 50Viscocity 45.7

5% PAN to DMF2nd Run 3rd Run

Viscocity [cP] Torque % RPM Viscocity [cP] Torque %140.2 3.6 0.369.8 4.2 0.664.2 8.4 1.551.8 14 347.8 25.2 648.6 50.9 12

- - 20

4% PAN to DMF2nd Run 3rd Run

Viscocity [cP] Torque % RPM Viscocity [cP] Torque %- 3.6 0.5

43.2 4.1 150.6 8.4 247.4 10.3 2.545.4 16.1 446.5 20.2 545 39.1 10

44.5 77.5 20- - 50

0 5 10 15 20 25 300

20

40

60

80

100

120

140

160

Reynolds NumberRe Flow rate Density d (g/mL)

0.00752504347065 0.3 ml/hr Ethanol 0.7898.333333E-11 m3/s TTIP 0.96

Hydraulic Diameter Acetic Acid 1.050.25 mm PVP 1.2

0.00025 m TotalDynamic viscosity Density

50 cp0.05 Pa s

Density Density d (g/mL)0.8865232975 g/ml FeEHIP 0.8886.52329749 kg/m3 Acetic Acid 1.05Kinematic viscosity PVP 1.2

5.64001E-05 m2/s TotalArea Density4.908739E-08 m2

Velocity m/s0.0016976527

Inertial force0.0003762522 Pa sViscous force

0.05 Pa s

laminar when Re < 2300transient when 2300 < Re < 4000turbulent when Re > 4000

Pump Force Shear Forcev (mL) m (g) Flow rate Flow rate

7.5 5.9175 0.3 ml/hr 0.3 ml/hr1.68 1.6128 8.333333E-11 m3/s 8.333333E-11 m3/s

3 3.15 Diameter Length0.375 0.45 0.25 mm 1.1 cm

12.555 11.1303 0.00025 m 0.011 m0.886523 g/mL Cross sectional Area Diameter

4.908739E-08 m2 0.25 mmVelocity 0.00025 m

v (mL) m (g) 0.0016976527 m/s Dynamic viscosity3 2.4 Density 44 cp

0.3 0.315 0.8342717258 g/ml 0.044 Pa s0.104167 0.125 834.27172583 kg/m3 0.044 kg/m s3.404167 2.84 Pressure Force Shear Force0.834272 g/mL 1.180253E-10 N 2.065067E-05 N

0.0001180253 uN 20.650666683 uNPressure0.0024043918 Pa