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Vehicle Technology Division THE NETHERLANDS (N E D E R L A N D) COMMUNICATION Concerning (1) : - approval granted - approval extended - approval refused - approval withdrawn - production definitively discontinued of a type of CNG/LNG component pursuant to Regulation number 110. Approval number: E4-110R-010378 Extension number: 00 1. CNG/LNG component considered: - Container(s) or cylinder(s) (1) - Tank(s) or vessel(s) (1) - Pressure indicator (1) - Pressure relief valve (1) - Automatic valve(s) (1) - Excess flow valve (1) - Gas-tight housing (1) - Pressure regulator(s) (1) - Non-return valve(s) or check valve(s) (1) - Pressure relief device (PRD)(temperature triggered) (1) - Manual valve (1) - Flexible fuel lines (1) - Filling unit or receptacle (1) - Gas injector(s) (1) - Gas flow adjuster (1) - Gas/air mixer (1) - Electronic control unit (1) - Pressure and temperature sensor(s) (1) - CNG filter(s) (1) - PRD (pressure triggered) (1) - Fuel rail (1) - Heat exchanger(s)/vaporizer(s) (1) - Natural gas detector(s) (1) P.O. Box 777 Tel. + 31 (0)79 345 83 02 Vehicle Admission & Surveillance 2700 AT Zoetermeer E-mail [email protected] The Netherlands www.rdw.nl CNG-components R110-01 v5.00 Page 1 of 5

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Page 1: Vehicle Admission & Surveillance - REGO Europe GmbH€¦ · Vehicle Technology Division ... Signed by Reviewer: Name: Regina Adelmann Name: ... answers are crossed out which are not

Vehicle Technology Division

THE NETHERLANDS (N E D E R L A N D)

COMMUNICATION

Concerning (1):

- approval granted - approval extended - approval refused - approval withdrawn - production definitively discontinued

of a type of CNG/LNG component pursuant to Regulation number 110. Approval number: E4-110R-010378 Extension number: 00 1. CNG/LNG component considered:

- Container(s) or cylinder(s) (1) - Tank(s) or vessel(s) (1) - Pressure indicator (1) - Pressure relief valve (1) - Automatic valve(s) (1) - Excess flow valve (1) - Gas-tight housing (1) - Pressure regulator(s) (1) - Non-return valve(s) or check valve(s) (1) - Pressure relief device (PRD)(temperature triggered) (1) - Manual valve (1) - Flexible fuel lines (1) - Filling unit or receptacle (1) - Gas injector(s) (1) - Gas flow adjuster (1) - Gas/air mixer (1) - Electronic control unit (1) - Pressure and temperature sensor(s) (1) - CNG filter(s) (1) - PRD (pressure triggered) (1) - Fuel rail (1) - Heat exchanger(s)/vaporizer(s) (1) - Natural gas detector(s) (1)

P.O. Box 777 Tel. + 31 (0)79 345 83 02 Vehicle Admission & Surveillance 2700 AT Zoetermeer E-mail [email protected] The Netherlands www.rdw.nl CNG-components R110-01 v5.00 Page 1 of 5

haaksma
RDW
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Approval number: E4-110R-010378 Extension number: 00

- LNG filling receptacle(s) (1) - LNG pressure control regulator(s) (1) - LNG pressure and/or temperature sensor(s) (1) - LNG manual valve(s) (1) - LNG automatic valve(s) (1) - LNG non-return valve(s) (1) - LNG pressure relief valve(s) (1) - LNG excess flow valve(s) (1) - LNG fuel pump(s) (1) -

2. Trade name or mark : Macro check valve 14250-5 Engineered Controls International LLC RegO Products Macro Technologies LLC

3. Manufacturer’s name and address : Engineered Controls International LLC 100 RegO Drive NC 27244, Elon United States of America

4. If applicable, name and address ofmanufacturer’s representative :

5. Submitted for approval on : November 2014

6. Technical service responsible forconducting approval tests : Kiwa Nederland B.V.

P.O. Box 137 7300 AC Apeldoorn The Netherlands

7. Date of report issued by that service : February 3th, 2015

8. Number of report issued by that service : 141001402

9. Approval : granted/refused/extended/withdrawn (1)

10. Reason(s) of extension (if applicable) :

11. Place : Zoetermeer

12. Date :

13. Signature :

14. The documents filed with the application or extension of approval can be obtained uponrequest.

(1) Strike out what does not apply.

CNG-components R110-01 v5.00 Page 2 of 5

boekeste
Sig-name-stamp
haaksma
Getypte tekst
19-FEB-2015
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Approval number: E4-110R-010378 Extension number: 00

ADDENDUM

1. Additional information concerning the type approval of a type of CNG/LNG components pursuant to Regulation number 110.

1.1. Natural Gas Storage System 1.1.1. Container(s) or cylinder(s) (for CNG system) 1.1.1.1. Dimensions : 1.1.1.2. Material : 1.1.2. Tank(s) or vessel(s) (for LNG system) 1.1.1.1. Capacity : 1.1.1.2. Material :

1.2. Pressure indicator 1.2.1. Working pressure(s) (2) : ... MPa 1.2.2. Material :

1.3. Pressure relief valve (discharge valve) 1.3.1. Working pressure(s) (2) : ... MPa 1.3.2. Material :

1.4. Automatic valve(s) 1.4.1. Working pressure(s) (2) : ... MPa 1.4.2. Material :

1.5. Excess flow valve 1.5.1. Working pressure(s) (2) : ... MPa 1.5.2. Material :

1.6. Gas-tight housing 1.6.1. Working pressure(s) (2) : ... MPa 1.6.2. Material :

1.7. Pressure regulator(s) 1.7.1. Working pressure(s) (2) : ... MPa 1.7.2. Material :

1.8. Non-return valve(s) or check valve(s) 1.8.1. Working pressure(s) (2) : MPa 1.8.2. Material :

1.9. Pressure relief device (temperature triggered) 1.9.1. Working pressure(s) (2) : ... MPa 1.9.2. Material :

1.10. Manual valve 1.10.1. Working pressure(s) (2) : ... MPa 1.10.2. Material :

1.11. Flexible fuel lines 1.11.1. Working pressure(s) (2) : ... MPa 1.11.2. Material :

CNG-components R110-01 v5.00 Page 3 of 5

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Approval number: E4-110R-010378 Extension number: 00

1.12. Filling unit or receptacle 1.12.1. Working pressure(s) (2) : ... MPa 1.12.2. Material :

1.13. Gas injector(s) 1.13.1. Working pressure(s) (2) : ... MPa 1.13.2. Material :

1.14. Gas flow adjuster 1.14.1. Working pressure(s) (2) : ... MPa 1.14.2. Material :

1.15. Gas/air mixer 1.15.1. Working pressure(s) (2) : ... MPa 1.15.2. Material :

1.16. Electronic control unit 1.16.1. Basic software principles :

1.17. Pressure and temperature sensor(s) 1.17.1. Working pressure(s) (2) : ... MPa 1.17.2. Material :

1.18. CNG filter(s) 1.18.1. Working pressure(s) (2) : ... MPa 1.18.2. Material :

1.19. PRD (pressure triggered) 1.19.1. Working pressure(s) (2) : ... MPa 1.19.2. Material :

1.20. Fuel rail(s) 1.20.1. Working pressure(s) (2) : ... MPa 1.20.2. Material :

1.21. Heat Exchanger(s)/Vaporizer(s) 1.21.1. Working pressure(s) (2) : ... MPa 1.21.2. Material :

1.22. Natural gas detector(s) 1.22.1. Working pressure(s) (2) : ... MPa 1.22.2. Material : ... MPa

1.23. LNG filling receptacle(s) 1.23.1. Working pressure(s) (2) : ... MPa 1.23.2. Material : ... MPa

1.24. LNG pressure control regulator(s) 1.24.1. Working pressure(s) (2) : ... MPa 1.24.2. Material : ... MPa

1.25. LNG pressure and/or temperature sensor(s) 1.25.1. Working pressure(s) (2) : ... MPa 1.25.2. Material : ... MPa

CNG-components R110-01 v5.00 Page 4 of 5

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Approval number: E4-110R-010378 Extension number: 00

1.26. LNG manual valve(s) 1.26.1. Working pressure(s) (2) : ... MPa 1.26.2. Material : ... MPa

1.27. LNG automatic valve(s) 1.27.1. Working pressure(s) (2) : ... MPa 1.27.2. Material : ... MPa

1.28. LNG non-return valve(s) 1.28.1. Working pressure(s) (2) : Class 5 (3.8 MPa) 1.28.2. Material : See report 141001402

1.29. LNG pressure relief valve(s) 1.29.1. Working pressure(s) (2) : ... MPa 1.29.2. Material : ... MPa

1.30. LNG excess flow valve(s) 1.30.1. Working pressure(s) (2) : ... MPa 1.30.2. Material : ... MPa

1.31. LNG fuel pump(s) 1.31.1. Working pressure(s) (2) : ... MPa 1.31.2. Material : ... MPa

(2) Specify the tolerance

CNG-components R110-01 v5.00 Page 5 of 5

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Kiwa Nederland B.V. • P.O. Box 137 • 7300 AC Apeldoorn • The Netherlands Telephone: +31 555 393 393 • [email protected] • www.kiwa-automotive.com

CNG/LNG Test Report CNG/LNG components

Macro checkvalve 14250-5

Report number: 141001402 Engineered Controls International, LLC

Burlington, North Carolina

United States of America

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File Issue: 010 INDEX

Report Number: 141001402 CNG/LNG components Page: IN 1/00

Report contents:

Sheet Chapter Code # Pages

Index 1 IN 1

History sheet(s) 2 HS 1

Contact information 3 CI 1

Summary sheet(s) 4 SS 1

Identification sheet 5 IS 1

Test Sheets: Regulation 110 6 TS 1

Result Sheets: Identification of EUT 7 RID 1

Measurement equipment in use uncertainties 7 RU 1

Regulation 110 7 RS 19

Declaration sheet(s) 8 DS 3

Drawing and technical description sheet(s) 9 DR 6

Correspondence sheet(s) 10 CS -

Kiwa Nederland B.V. Files (if applicable, included in Kiwa Nederland B.V. report only)

11 KF -

Note: The revision number of each page of this report is identified in the right heading of the page by means of the last 2 digits in the page number (e.g. HS 1/00, Heading Sheet page 1, revision 00).

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 HISTORY SHEET(S)

Report Number: 141001402 CNG/LNG components Page: HS 1/00

Report history: Date: Description: Report No: Job Ref: 03-02-2015

New (initial report) Macro check valve 14250-5 E4-110R-010378L

141001402 141001402

Any modification and/or extension made to this report shall be recorded in a Report History Sheet and be inserted as a first page when opening this report. This sheet shall detail the modification and/or extension applicable to this initial report and shall clearly state where these details can be found. A copy of this sheet shall also be provided to the applicant/manufacturer, in order to keep the reports identical. Signed by Test Engineer: Signed by Reviewer: Name: Regina Adelmann Name: Eric Harmsen

Signature: Signature: Date: 03-02-2015 Date: 03-02-2015 © 2015, Kiwa Nederland B.V., Apeldoorn. - This report may only be duplicated as a complete set without any modifications and with permission of the legitimate owner. - The test results in this report are exclusively related to the samples offered and tested. - Tests marked in this report with the IRN number are part of the accreditation scope (RvA L248) unless stated differently. - With regard to measurement uncertainty information please check our website. - Conclusions for compliance with e.g. product standard requirements are not part of the lab scope (RvA L248). - In case of dispute regarding this test report please contact Kiwa Nederland BV.

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 CONTACT INFORMATION

Report Number: 141001402 CNG/LNG components Page: CI 1/00

Responsible Test House: Kiwa Nederland B.V.

Address: Wilmersdorf 50

7327 AC Apeldoorn

P.O. Box 137

7300 AC Apeldoorn

The Netherlands

Telephone: + 31 555 393 393

Facsimile: + 31 555 393 685

E-mail: [email protected]

Name of the Applicant: Engineered Controls International, LLC

Address: 100 RegO Drive

NC 27244, Elon

United States of America

Name of the Manufacturer: Engineered Controls International, LLC

Address: 100 RegO Drive

NC 27244, Elon

United States of America

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 SUMMARY SHEET(S)

Report Number: 141001402 CNG/LNG components Page: SS 1/00

Test report of the examination of the:

CNG/LNG component(s)

Macro check valve 14250-5

The CNG/LNG component(s), Macro check valve 14250-5 made by Engineered Controls International, LLC, meet(s) the requirements of:

Regulation 110 Addendum 109: Regulation No. 110

Revision 3 - Amendment 1 Incorporation all valid text up to: Supplement 2 to 01 series of amendments to the Regulation – Date of entry into force: 9 October 2014

Uniform provisions concerning the approval of: I Specific components of motor vehicles using compressed natural gas (CNG/LNG) in their propulsion system; II Vehicles with regard to the installation of specific components of an approved type for the use of compressed natural gas (CNG/LNG) in their Propulsion system.

UNITED NATIONS

See the Identification Sheet (IS) for all available types. Signed in Acceptance: Kiwa Nederland B.V.

Paul Dijkhof Unit Manager Automotive Date: 03-02-2015

Note:

The described test results are only valid for the tested materials and objects.

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 IDENTIFICATION SHEET

Report Number: 141001402 CNG/LNG components Page: IS 1/00

Type break down (including specifications) Marco check valve Make(s): Engineered Controls International LLC

RegO Products

Macro Technologies LLC

Type(s): Macro check valve 14250-5 Approval number: E4-110R-010378-L Classification(s): Class 5 Working pressure: 3.8 MPa (38 bar) Temperature range: -162 °C up to 85 °C Material(s): see drawings

Job Reference: 141001402 Initials: Adelmre

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File Issue: 001 TEST SHEET R110 CNG/LNG EQUIPMENT

Report number:

141001402 LNG Check Valve valve

Page: TS01

Partner for progress

Annex 4A: LNG check valve

Key to Test Sheet: YES = YES NA = Not Applicable NT = Not Tested NO = NO Example: YES-NA-NT-NO

Notes: When filling in Test Sheet, answers are crossed out which are not applicable for that clause.

3.1 The materials constituting the LNG check valve which are in contact with the LNG when operating, shall be compatible with the test LNG. In order to verify this compatibility the procedure described in Annex 5D shall be used.

YES-NA-NT-NO

3.2.1 The LNG check valve shall be so designed as to withstand a pressure of 1.5 times the working pressure (MPa) without leakage and deformation at cryogenic temperature.

YES-NA-NT-NO

3.2.2 The LNG check valve shall be so designed as to be leak-proof (external) at a pressure of 1.5 times the working pressure (MPa) (see Annex 5B) with the temperatures given in Annex 5O.

YES-NA-NT-NO

3.2.3 The LNG check valve, being in the normal position of use specified by the manufacturer, is submitted to 7,000 operations at cryogenic temperature (see Annex 5O); then it is deactivated. The check valve shall remain leak-proof (external) at a pressure of 1.5 times the working pressure (MPa) (see Annex 5B).

YES-NA-NT-NO

3.2.4 The LNG check valve shall be so designed to operate at temperatures as specified in Annex 5O. YES-NA-NT-NO

3.3 The LNG check valve has to comply with the test procedures for the Class 5 component. YES-NA-NT-NO

5A Overpressure or strength YES-NA-NT-NO

5B External leakage YES-NA-NT-NO

5C Internal leakage YES-NA-NT-NO

5D CNG compatibility YES-NA-NT-NO

5E Corrosion resistance

- 1 Salt spay test

- 2 Ammonia test

YES-NA-NT-NO

YES-NA-NT-NO

5F Resistance to dry heat YES-NA-NT-NO

5G Ozone ageing YES-NA-NT-NO

5H Temperature cycle YES-NA-NT-NO

5L Durability test YES-NA-NT-NO

5N Vibration resistance YES-NA-NT-NO

5O Operating temperatures YES-NA-NT-NO

N.A.: non-metallic material tests see declaration sheets part DS in this report

Job reference: 141001402 Initials: Adelmre

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File Issue: 010 RESULT SHEET(S) IDENTIFICATION OF EUT

Report Number: 141001402 CNG/LNG components Page: RID 1/00

Sample designation: Description Reference no. Date intake Macro check valve 14250-5 C141148 12-11-2014

Macro check valve 14250-5 C141149 12-11-2014

Macro check valve 14250-5 C141150 12-11-2014

Macro check valve 14250-5 C141151 12-11-2014

Macro check valve 14250-5 C141152 12-11-2014

Macro check valve 14250-5 C141153 12-11-2014

Macro check valve 14250-5 C141154 12-11-2014

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 MEASUREMENT EQUIPMENT IN USE UNCERTAINTIES

Report Number: 141001402 CNG/LNG components Page: RU 1/00

List of general measurement equipment:

Voltage ± 2 % Reading

High voltage test device (SPS) 500 – 3750 Vac ± 5 % Reading

Resistance ± 2 % Reading

Protective wire and insulation test device ± 5 % Reading

Sliding gauge ± 0.1 mm

Measuring tape ± 1 mm

Cooling and heating < -10 °C ± 5 °C

Cooling and heating –10 C / +100 °C ± 3 °C

Cooling and heating > 100 °C ± 5 % Reading

Climate chamber ± 2 °C / ± 3 %RV

Ambient temperature ± 1 °C (10-30)

Time =< 1 hour ± 0.2 s

Time > 1 hour ± 0.1 % Reading

Torque ± 5 % Reading

Bending moment ± 5 % Reading

Standard weight ± 5 % Reading

Weighing < 30 g ± 0.1 % Reading

Weighing > 30 g ± 2 % Reading

Pressure (gas + air) general ± 5 % Reading

Barometer reading ± 5 mbar

Pressure (water) ± 5 % Reading

Burst water pressure ± 1 % Reading

Gas tightness 0-100 cm3/h ± 5 cm3/h

Gas tightness > 100 cm3/h ± 5 % Reading

Actual Flow rate (general) ± 5 % Reading

More info about measurement uncertainty of testing in the context of ISO/IEC 17025 can be found on;

http://www.kiwa.nl/netherlands/publications.aspx

Job Reference: 141001402 Initials: Adelmre

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File Issue: 002

RESULT SHEETS R110 CNG/LNG EQUIPMENT

Report Number: 141001402

OVERPRESSURE TEST (STRENGHT TEST)

Page: RS 01

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 46 Pressure

Approval requirement: Annex:

Regulation 110 5A

Testing Equipment Kiwa no. Calibrated (due date)

Operation OK

Hydraulic pressure equipment 111322 September 2015 2.0 MPa, yes

Pressure gauge 111939 April 2017 2.0 MPa, yes

Stopwatch 112107 March 2017 28.03 sec., yes

Temperature

Temperature equipment (room temperature) 111256 June 2015 21°C, yes

Test Conditions Complies N.A.

- Test is to be performed before and after the durability test; Yes

- The samples are filled with water and slowly pressurised; Yes

- The samples surface shows no visible cracks as a result of this test; Yes

- Retest a new sample with a pressure gauge with accuracy +5%, if samples have failed N.A.

Test Results Requirement sample no.: C141153

sample no.: sample no.:

Moment of test Before/after Durability test

before After before after before after

Classification of component* 0 1 2 3 5 5

Test pressure (Kpa / MPa) * 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

5700

Test time > 3 min 03.25 min

Rupture None None

Permanent distortion None None

Test dated To be monitored 30-1-2015

Conclusion

Requirement Complies N.A.

Samples meet requirement Yes

Remarks: WP: 3800 kPa * Cross out which is not applicable Wp = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 002

RESULT SHEET R110 CNG/LNG EQUIPMENT

Report Number: 141001402

DURABILITY TEST (CONTINUED OPERATION)

Page: RS 02

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5P

Testing Equipment Kiwa no. Calibration (due date)

Operation OK

Robot / PLC 111379

Life test device

Pressure gauge 111655

Stopwatch 112107 March 2015 6.28 sec Yes

Room temperature equipment 111256 June 2015 21 °C Yes

Test Conditions Complies N.A.

- The test is performed with a period of not less then 10 seconds; Yes

- 96 % of the total cycles is performed at minimum temperature; Yes

- 2 % of the total cycles is performed at room temperature; Yes

- 2 % of the total cycles is performed at maximum temperature. Yes

- The counter of the duration test has been validated before the testing has started Yes

Test Results Requirement sample no.: C141153

sample no.: sample no.:

Classification of component * 0 1 2 3 5 5

Test pressure (kPa) * Wp Wp Wp Wp Wp 3800 kPa

Date & time starting the test To be monitored 10-12-2014

Date & time stopping the test To be monitored 21-01-2015

Actual cycles performed * Test cycles > 7.000 times Test cycles > 50.000 times

7000 times

Test to be performed after the endurance test are:

External leakage According to annex 5B See RS 03 See RS See RS

Seat leakage According to annex 5C See RS N.A. See RS See RS

Conclusion

Requirement Complies N.A.

Samples meet requirement Yes

Remarks:

* Cross out which is not applicable wp = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 004

RESULT SHEET R110 CNG/LNG EQUIPMENT

Report Number: 141001402

EXTERNAL LEAKAGE TEST including high and low temperature

Page: RS 03

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5B and 4L

Testing Equipment Kiwa no. Calibration (due date) Operation OK

Oven 111906 March 2015 85°C Yes

Cooler 111931 N.A.

Pressure gauge 111666 Sept. 2016 3.8 MPa, Yes

Leakage gauge

Stopwatch 112107 March 2017 8.0 sec., Yes

Temperature

Room temperature equipment (and temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

- The sample is slowly pressurised to the test pressure as declared by the manufacturer; Yes

- The sample has conditioned for 8 hours (at least) at the test temperature; Yes

- The test sample is submerged in the test fluid for at least 60 sec, preferred is 900 sec; Yes

- When air bubble(s) where detected after 60 sec, leakage is considered to be > 15cm3/h. N.A.

Test Results Requirement sample no.: C141153

Test temperature room temperature 85°C / 120°C* -20°C/-40°C/-157°C*

Moment of test * Corrosion / Durability / Vibration / Cycle test /

Before after Before after before After

Classification of component * 0 1 2 3 5 5 5 5 5

Test pressure (Kpa / MPa) 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

3800 kPa

5700 kPa

3800 kPa

1970 kPa

External leakage < 15cm3/h 0 cm3/h 0 cm3/h 0 cm3/h 0 cm3/h

Test date To be monitored 09-12-2014

22-01-2015

30-01-2015

29-01-2015

Conclusion

Requirement Complies N.A.

Samples meets requirement Yes

Remarks:

* Cross out which is not applicable. WP = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 002 RESULT SHEET R110 CNG EQUIPMENT

Report Number: 141001402

CORROSION RESISTANCE TEST (Salt Spray)

Page RS 04

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Part:

R110 5E 1

Task instructions*: ISO15500-2 (2012) part 10 and ISO 9227

Testing Equipment Kiwa no. Calibrated (due date)

Operation OK

Salt spray equipment 111541 June 2015 Yes

Temperature

Temperature equipment (room temperature) 111256 June 2015 21 °C, yes

Test Conditions Complies N.A.

- This test is performed on a non AISI 300 series or equivalent stainless steel component; Yes

- Before testing the sample is cleaned and dried at ambient temperatures < 40 °C; Yes

- All connections and openings are closed; Yes

- Normally installed components has been exposed to 144 hours of salt spray test; Yes

- The salt solution shall consist of 5% sodium chloride and 95% distilled water by weight; Yes

- The temperature of the test room is measured between 33 ˚C and 36 ˚C; Yes

- The adjustment of nozzle is settled at 1.5 cm3/h ±0.5cm3/h; Yes

- The received salt solution has been checked every 24 h or 48 h; Yes

- After testing the sample has been immediately cleaned; Yes

- After cleaning, leakage test and secondly a hydrostatic strength test has been performed. Yes

Test results Requirement Sample no.: C141148 Sample no.:

Date starting the test (dd-mm-yyyy) 09-12-2014

Date stopping the test (dd-mm-yyyy) 15-12-2014

Salt spray testing time 144 hours 144 hours

Ambient temperature during testing Between 33 and 36°C 35°C

Store time at room temperature 0,5 –1h 1 hour

External leakage test results See page RS 05 RS

Internal leakage test results See Page RS N.A. RS

Conclusion

Requirement Complies N.A.

Samples meet requirement Yes

Remarks:

Job Reference: 141001402 Initials: rookshe

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File Issue: 004

RESULT SHEET R110 CNG/LNG EQUIPMENT

Report Number: 141001402

EXTERNAL LEAKAGE TEST including high and low temperature

Page: RS 05

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5B and 4L

Testing Equipment Kiwa no. Calibration (due date) Operation OK

Oven 111906 March 2015 85°C Yes

Cooler 111931 N.A.

Pressure gauge 111666 Sept. 2016 3.8 MPa Yes

Leakage gauge

Stopwatch 112107 March 2017 18.0 sec Yes

Temperature

Room temperature equipment (and temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

- The sample is slowly pressurised to the test pressure as declared by the manufacturer; Yes

- The sample has conditioned for 8 hours (at least) at the test temperature; Yes

- The test sample is submerged in the test fluid for at least 60 sec, preferred is 900 sec; Yes

- When air bubble(s) where detected after 60 sec, leakage is considered to be > 15cm3/h. N.A.

Test Results Requirement sample no.: C141148

Test temperature room temperature 85°C / 120°C* -20°C/-40°C/-142°C*

Moment of test * Corrosion / Durability / Vibration / Cycle test /

Before after Before after before After

Classification of component * 0 1 2 3 5 5 5 5 5

Test pressure (Kpa / MPa) 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

3800 kPa

5700 kPa

3800 kPa

1810 kPa

External leakage < 15cm3/h 0 cm3/h 0 cm3/h 0 cm3/h 0 cm3/h

Test date To be monitored 09-12-14 17-12-14 18-12-2014 27-01-15

Conclusion

Requirement Complies N.A.

Samples meets requirement Yes

Remarks:

* Cross out which is not applicable. WP = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 002

RESULT SHEETS R110 CNG EQUIPMENT

Report Number: 141001402

OVERPRESSURE TEST (STRENGHT TEST)

Page: RS 06

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 46 Pressure

Approval requirement: Annex:

Regulation 110 5A

Testing Equipment Kiwa no. Calibrated (due date)

Operation OK

Hydraulic pressure equipment 111322 N.A. N.A.

Pressure gauge, when tested pneumatically 111666 Sept. 2016 3.8 MPa, Yes

Stopwatch 112107 March 2017 18.0 sec., Yes

Temperature

Temperature equipment (room temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

- Test is to be performed before and after the durability test; N.A.

- The samples are filled with water and slowly pressurised; N.A.

- The samples surface shows no visible cracks as a result of this test; Yes

- Retest a new sample with a pressure gauge with accuracy +5%, if samples have failed N.A.

Test Results Requirement sample no.: C141148

sample no.: sample no.:

Moment of test Before/after Corrosion test

before After before after before after

Classification of component* 0 1 2 3 5 5

Test pressure (Kpa / MPa) * 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

5700

Test time > 3 min Yes

Rupture None None

Permanent distortion None None

Test dated To be monitored 17-12-2014

Conclusion

Requirement Complies N.A.

Samples meet requirement Yes

Remarks: WP: 3800 kPa * Cross out which is not applicable Wp = working pressure

Job Reference: 141001402 Initials: Adelmre

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File Issue: 002

RESULT SHEET R110 CNG EQUIPMENT

Report Number: 141001402

VIBRATION RESISTANCE TEST Page RS 07

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 46 Pressure

Approval requirement: Annex:

Regulation 110 5N

Testing Equipment Kiwa no. Calibrated (due date)

Operation OK

Resonance equipment 111515 June 2015 17 Hz, Yes

Stroboscope (check 17 Hz with stroboscope) 111162

Temperature

Temperature equipment (room temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

Component shall be vibrated for 2 hours at 17Hz with amplitude 1,5 mm; Yes

Resonance test are carried out along each of three orthogonal axes. Yes

Test results Sample no.: C141151 Sample no.:

External leakage test annex 5B (additional) see RS 08 see RS

Internal leakage test annex 5C see RS N.A. see RS

Visual inspection after test no mechanical failures None

Test date to be monitored 25-11-2014

Conclusion

Requirement Complies N.A.

Samples meets requirement Yes

Remarks:

Job Reference: 141001402 Initials: Adelmre

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File Issue: 004

RESULT SHEET R110 CNG/LNG EQUIPMENT

Report Number: 141001402

EXTERNAL LEAKAGE TEST including high and low temperature

Page: RS 08

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5B and 4L

Testing Equipment Kiwa no. Calibration (due date) Operation OK

Oven 112041 September 2015 85 °C, Yes

Cooler 111931 N.A. N.A.

Pressure gauge 111666 Sept. 2016 3.8 MPa, Yes

Leakage gauge

Stopwatch 112107 March 2017 18.0 sec., Yes

Temperature

Room temperature equipment (and temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

- The sample is slowly pressurised to the test pressure as declared by the manufacturer; Yes

- The sample has conditioned for 8 hours (at least) at the test temperature; Yes

- The test sample is submerged in the test fluid for at least 60 sec, preferred is 900 sec; Yes

- When air bubble(s) where detected after 60 sec, leakage is considered to be > 15cm3/h. N.A.

Test Results Requirement sample no.: C141151

Test temperature room temperature 85°C / 120°C* -20°C/-40°C/-142°C*

Moment of test * Corrosion / Durability / Vibration / Cycle test /

Before after Before after before After

Classification of component * 0 1 2 3 5 5 5 5 5

Test pressure (Kpa / MPa) 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

3800 kPa

5700 kPa

3800 kPa

1810 kPa

External leakage < 15cm3/h 0 cm3/h 0 cm3/h 0 cm3/h 0 cm3/h

Test date To be monitored 09-12-14 17-12-14 10-12-14 27-01-15

Conclusion

Requirement Complies N.A.

Samples meets requirement Yes

Remarks:

* Cross out which is not applicable. WP = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 002

RESULT SHEET R110 CNG EQUIPMENT

Report Number:141001402

CORROSION RESISTANCE TESTS (Ammonia) Page RS 09

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5E

Task instructions*: ISO 15500-2

Testing equipment Kiwa no. Calibrated (due date)

Operation OK

Ammonia test equipment 100195 N.A. Yes

Stopwatch 112107 March 2017 8.0 sec, Yes

Microscope

Thermometer 100717 Dec. 2015 34 °C Yes

Temperature

Temperature equipment (room temperature) 111256 June 2015 21 °C Yes

Test conditions Complies N.A.

- Three new samples shall used N.A.

- Before testing the sample is cleaned and dried at ambient temperatures < 40 °C Yes

- All connections and openings are closed Yes

- Before testing the ammonia concentration have a specific gravity of 0.94 Yes

- Position of the samples is 40mm above the ammonia Yes

- After testing the sample is cleaned and dried at ambient temperatures < 40 °C Yes

Test results Requirement Sample no.: C141149

Sample no.:

Date and time starting the test Timing aspects to be monitored 09-12-2014

Date and time stopping the test Timing aspects to be monitored 10-12-2014

Exposure time in ammonia 24 h 24 h

Ambient temperature during testing 34+2°C 34°C

Result at magnification of x25 No cracks No cracks

Test to be performed after the endurance test are:

External leakage test See page RS 10

Internal leakage test See page RS N.A.

Conclusion

Requirement Complies N.A.

Samples meet requirement Yes

Remarks:

Job Reference:141001402 Initials: Rookshe

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File Issue: 004

RESULT SHEET R110 CNG/LNG EQUIPMENT

Report Number: 141001402

EXTERNAL LEAKAGE TEST including high and low temperature

Page: RS 10

Product: Rego: Macro Check valve 14250-5.

Tested in accordance with:

IRN 52 Leakage

Approval requirement: Annex:

Regulation 110 5B and 4L

Testing Equipment Kiwa no. Calibration (due date) Operation OK

Oven 111906 March 2015 85°C, Yes

Cooler 111931 N.A. N.A.

Pressure gauge 111666 Sept. 2016 3.8 MPa, Yes

Leakage gauge

Stopwatch 112107 March 2017 8.0 sec., Yes

Temperature

Room temperature equipment (and temperature) 111256 June 2015 21 °C, Yes

Test Conditions Complies N.A.

- The sample is slowly pressurised to the test pressure as declared by the manufacturer; Yes

- The sample has conditioned for 8 hours (at least) at the test temperature; Yes

- The test sample is submerged in the test fluid for at least 60 sec, preferred is 900 sec; Yes

- When air bubble(s) where detected after 60 sec, leakage is considered to be > 15cm3/h. N.A.

Test Results Requirement sample no.: C141149

Test temperature room temperature 85°C / 120°C* -20°C/-40°C/-157°C*

Moment of test * Corrosion / Durability / Vibration / Cycle test /

Before after Before after before After

Classification of component * 0 1 2 3 5 5 5 5 5

Test pressure (Kpa / MPa) 1,5 x wp

2 x wp

2 x wp

2 x wp

1,5 x wp

3800 kPa

5700 kPa

3800 kPa

1970 kPa

External leakage < 15cm3/h 0 cm3/h 0 cm3/h 0 cm3/h 0 cm3/h

Test date To be monitored 09-12-2014

17-12-2014

11-12-2014

29-01-2015

Conclusion

Requirement Complies N.A.

Samples meets requirement Yes

Remarks:

* Cross out which is not applicable. WP = working pressure

Job Reference: 141001402 Initials: Rookshe

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File Issue: 004

RESULT SHEET R110 CNG EQUIPMENT

Report Number: 141001402

OPERATION TEMPERATURES Page: RS 11

Product: Rego: Macro Check valve 14250-5

Tested in accordance with: IRN 52 Approval requirement Regulation 110 Annex: 5O

Test equipment used Kiwa no. Calibrated Operation OK Climate room 111417 N.A. N.A.

Stopwatch 112103 March 2017 6.18 sec, yes

Temperature Temperature equipment (room temperature) 111256 June 2015 21 °C, yes

TEST RESULTS Sample no.: C141151

Sample no.: Sample no.:

Component is tested for Moderate temperatures: (-20°C)

Component is assembled in the engine compartment (-20°C / 105°C) N.A.

Component is assembled on the engine (-20°C / 120°C) N.A.

Component is assembled on board (-20°C / 85°C) N.A.

Component is tested for Cold temperatures: (-40°C)

Component is assembled in the engine compartment (-40°C / 105°C) N.A.

Component is assembled on the engine (-40°C / 120°C) N.A.

Component is assembled on board (-40°C / 85°C) N.A.

Component is tested for LNG temperatures: (-162°C)

Component is assembled in the engine compartment (-162°C / 105°C) N.A.

Component is assembled on the engine (-162°C / 120°C) N.A.

Component is assembled on board (-162°C / 85°C) Yes

Used test pressure (kPa/ MPa) 3.8 MPa

Test monitoring date 10-12-2014

Conclusion Complies N.A.

Samples meet requirement Yes

Remarks:

* Cross out which is not applicable

Job Reference: 141001402 Initials: Adelmre

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EXAMINATION REPORT Rubber, vulcanized or thermoplastic materials used in specific equipment and parts which can be fitted and/or used on wheeled vehicles using compressed natural gas (CNG) in their propulsion system.

REPORT NUMBER

LC 11226

AUTHORISATION

H. Pauw, Co-ordinator Lab C

DEPARTMENT

Lab C

- This report may only be duplicated as a complete set. without any modifications and with permission of the legitimate owner.

- The test results in this report are exclusively related to the samples offered and tested. - With regard to measurement uncertainty information please check our website. - In case of dispute regarding this test report please contact Kiwa Nederland B.V.

Kiwa Nederland B.V. Lab C Wilmersdorf 50 NL 7327 AC Apeldoorn Netherlands Telephone +31 55 5393393 Internet www.1kiwa.com

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Report number: LC 11226 Date: 2014-12-03 2 of 4

Rubber, vulcanized or thermoplastic materials used in specific equipment and parts which can be fitted and/or used on wheeled vehicles using compressed natural gas (CNG) in their propulsion system.

Client: Rego Engineerd Controls

Reference number: 141001402

According to standard: ECE R110

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Report number: LC 11226 Date: 2014-12-03 3 of 4

1. Order

By order of Kiwa Nederland B.V. , the sample mentioned below was tested by the

Laboratory for Material Testing for determination of physical and mechanical

properties according to ECE R110.

2. General

The sample was received on 24-11-2014 and registered with number LC 11226.

The test was started on 24-11-2014 and was carried out by Mr L.M. Bloeming.

3. Sample description

Number/type of samples : 14 O-rings Macro Technologies 14250-5

Check Valve

Material : Part 14538, Filled PTFE(Teflon) 25% Glass

Dimensions : 33 x 28,5 x 4,56 mm

Colour : white

Marking : no marking on the O-rings

Date of production : not specified

4. Test conditions

The tests were carried out at a temperature of 23 ± 2°C.

5. Apparatus

Tensile-pressure machine, cooling-heating equipment, ozone equipment and

measuring equipment.

6. Preservation of the sample

In case of failure the basic sample material will be kept for 3 months.

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Report number: LC 11226 Date: 2014-12-03 4 of 4

7. Test results

Physical and mechanical properties:

Type of sample:

Properties Test method Units Require-

ments

Test

results

Tensile strength

Elongation at break

ISO 37 complete ring

ISO 37 complete ring

MPa

%

-

-

17,1

245

Changes after heat ageing

7x 24 h. at 85°°°°C

Tensile strength

Elongation at break

NEN-ISO 188

ECE R110 annex 5F

ECE R67 annex 15

part 13

%

%

≤ 25

+ 10/-30

4

5

Resistance to ozone

Concentration 50 pphm

Time 72 h.

ISO 1431-1 - no cracks no cracks

8. Conclusion The test pieces meet the requirements for the investigated aspect in accordance with ECE R110.

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EXAMINATION REPORT Rubber, vulcanized or thermoplastic materials used in specific equipment and parts which can be fitted and/or used on wheeled vehicles using compressed natural gas (CNG) in their propulsion system.

REPORT NUMBER

LC 11227

AUTHORISATION

H. Pauw, Co-ordinator Lab C

DEPARTMENT

Lab C

- This report may only be duplicated as a complete set. without any modifications and with permission of the legitimate owner.

- The test results in this report are exclusively related to the samples offered and tested. - With regard to measurement uncertainty information please check our website. - In case of dispute regarding this test report please contact Kiwa Nederland B.V.

Kiwa Nederland B.V. Lab C Wilmersdorf 50 NL 7327 AC Apeldoorn Netherlands Telephone +31 55 5393393 Internet www.1kiwa.com

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Report number: LC 11227 Date: 2014-12-03 2 of 4

Rubber, vulcanized or thermoplastic materials used in specific equipment and parts which can be fitted and/or used on wheeled vehicles using compressed natural gas (CNG) in their propulsion system.

Client: Rego Engineerd Controls

Reference number: 141001402

According to standard: ECE R110

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Report number: LC 11227 Date: 2014-12-03 3 of 4

1. Order

By order of Kiwa Nederland B.V. , the sample mentioned below was tested by the

Laboratory for Material Testing for determination of physical and mechanical

properties according to ECE R110.

2. General

The sample was received on 24-11-2014 and registered with number LC 11227.

The test was started on 24-11-2014 and was carried out by Mr L.M. Bloeming.

3. Sample description

Number/type of samples : 14 O-rings Macro Technologies 14250-5

Check Valve

Material : Part 14532, Delrin 150sa

Dimensions : 17 x 9,5 x 2,95 mm

Colour : black

Marking : no marking on the O-rings

Date of production : not specified

4. Test conditions

The tests were carried out at a temperature of 23 ± 2°C.

5. Apparatus

Tensile-pressure machine, cooling-heating equipment, ozone equipment and

measuring equipment.

6. Preservation of the sample

In case of failure the basic sample material will be kept for 3 months.

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Report number: LC 11227 Date: 2014-12-03 4 of 4

7. Test results

Physical and mechanical properties:

Type of sample:

Properties Test method Units Require-

ments

Test

results

Tensile strength

Elongation at break

ISO 37 complete ring

ISO 37 complete ring

MPa

%

-

-

67,0

60

Changes after heat ageing

7x 24 h. at 85°°°°C

Tensile strength

Elongation at break

NEN-ISO 188

ECE R110 annex 5F

ECE R67 annex 15

part 13

%

%

≤ 25

+ 10/-30

1

9

Resistance to ozone

Concentration 50 pphm

Time 72 h.

ISO 1431-1 - no cracks no cracks

8. Conclusion The test pieces meet the requirements for the investigated aspect in accordance with ECE R110.

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File Issue: 010 DECLARATION SHEET(S)

Report Number: 141001402 CNG/LNG components Page: DS 1/00

Manufacturer’s declaration(s): Declaration title Date Declaration sheet rubber material 24-11-2015 Declaration sheet product classification N.A. Declaration sheet compliance with general design rules N.A.

Job Reference: 141001402 Initials: Adelmre

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Project no. 141001402

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Project no. 141001402

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File Issue: 010 DRAWING AND TECHNICAL DESCRIPTION SHEET(S)

Report Number: 141001402 CNG/LNG components Page: DR 1/00

Drawings and Technical Descriptions: Description # Pages Date Photo Sheets 1 12-11-2014 Drawing 11395-ECE, rev. D 1 17-12-2014 Drawing 62529, rev. B 2 17-12-2014 Component list 14250-5 Check valve 1 10-06-2014

Job Reference: 141001402 Initials: Adelmre

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File Issue: 010 DRAWING AND TECHNICAL DESCRIPTION SHEET(S)

Report Number: 141001402 CNG/LNG components Page: DR 2/00

Photo sheet of Macro check valve 14250-5

Job Reference: 141001402 Initials: Adelmre

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Project no. 141001402

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Project no. 141001402

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Project no. 141001402

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Project no. 141001402