united states environmental protection agelsl6v i

I 3rUNITED STATES ENVIRONMENTAL PROTECTION AGElSl6V

I ___REGION 7 >——--——

25 FUNSTON ROADKANSAS CITY. KANSAS 66115

Date: _/

MEMORANDUM

SUBJECT: Data Transmittal for Activity I: 0 \ (hSite Description: Qun

FROM: Robert D. Kleopfer, Ph.D. UUO.^^^ -f0 rActing Chief, Laboratory Branch, ENSV

TO: Robert L. MorbyChief, Superfund Branch, WSTM

ATTN:

Attached is the data transmittal for the above referenced site.

This should be considered a __ Partial __ Corrected ^xf Complete

data transmittal (completes transmittal of ____________). If you

have any questions or comments, please contact D. Simmons at 236-3881.

Attachments

cc: Data File

S00011957SUPERFUND RECORDS

EPA REGION VIIDATA QUALIFICATION CODES

U - Compound was not detected.

M - Compound was qualitatively identified; however,quantitative value is less than contract requireddetection limits (CLP data); or value is less thanlimit of quantitation (EPA data).

J - Compound was qualitatively identified; however,compound failed to meet all QA criteria andtherefore is only an estimated value.

I - Analysis attempted, but no results can be reported.

0 - Sample lost or not analyzed.

L - Value known to be higher than value reported.

f [ELD SHEET!J.b. t-:N'-'liifJMi-|[.:i-JTr--,l.. PROTECTION AGENCY, REGION VII

SLPVPJLS I'lv. '2* FUNSTQN RD. KANSAS CITY, KG

: Site Name: DUPONT LANDFILL:: Lor; at.ion: CA! lAHCHL l A

Site Number: X7Site Code: n/

: Collected: YR: Gb MO: // Day:.//__ Ti ,ne>: G3.QO Leader: J. CLEARY

: Samp 3e Number; JovX/oOl SNO #: /(/A

OTHER:le- hf::-dia (c:i. r ' c j t :

SOIL, DUST, PIM-: ,A! i - . SfciDII-IENl .

t 'c::u ;:.!.(.:• ,-, -,.•.:••: ,-r::3

-- — . . . . . . . __ „_ „._„ . _ _ _ _

: Sample Container £ Taq Cai.or : Preservative : Analysis Requested :

: 40,-nl VIAL: SOoz AMBER: 3<joz AM3ER: 1 LITER POLY: 1 LITER POLY: 1 LITER POLY

• J. i-.-f-f.- PS--Y

•

! n f .p t -h- //4u

LIME .PURPLEBLUEWHITEWHITEYELLOW

COOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4C ,

^r-J S.wt rlefr-tTt fl^W

VOASEMI-VOLPESTICIDESTOT METALS 'TOT MERCURY-NITRATE

P A n # ••fiftJpA A/4 . . Aliquot s: _. L

: 3:3.iripj orn 3 _ /v/A

MW-1script i on

cuhMENTj or riEi. .::> PILI^SDNNEL

DATE/TIME /'/^/^ -: WELL *

C?.\

FIFLD MEASUREMENTS:TEV,P.°C__ ^SAl.N

ID:-!-PL

F - E E L f ) SHEETU.S. EMVl|.;t..'MMLNI,\L. PRO TEL i ION AGENCY, REGION VII

lINVIROi-IMEI-ir.'v.. SErlR'Vir.ES 'Viv. 25 FL'NSTUN RD. KANSAS CITY, K'£ 661 lb

: S i t c- H a m c;:: D U P 0 \ I I L..;: 4 i ID FII..:_: Location: CAMANCHb In

Site Number: X7Site Code: n/a

.i.i

Collected: YR: 86 MO:...// Day:_//_ ,Time: /E^L Leader: J. CLEARY

Sample Number: J09X7CO2 SMO #: ._ yV/^._._..__

Sample Mcidia (c i i- <% '. o ono.'1: /^~~^~~*^SOIL, DUG f , RJ: IMS ATE-: . UEDn-iENT , AjATER/ OTHER:. __

S a m p l e b p i i t ( c i i c l c one) : Y E ?

: Sample Container : Tag Color : Preservative : Analysis Requested

40ml VIAL80oz AMBERSOoz AMDERi LITER PULY1 LITER POLY1 LITER POLYJ. L'i(,-

LIME .PURPLEBLUEWI-IITEWHIIEYELLOW

COOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4CCGOL 4C

5. si

VOASEMI-VOLPESTICIDESTOT METALSTOT MERCURYNITRATE

Depth:

Samplers:

Pan Aliquots: A>'A

::.'.L t 1 Cr' 1. p : ! . On :

7. a.f H 3.1 o.J 7.0

0-f S?df '6?<

COMME.NT.) OF K'(ELD PERSONNEL

DATE/TIME '%/jffe ""//-To" FIELD MEASUREMENTS:WELL /«lw- 2. TEMP. ° C_ ?-O

S.\LIN

LEVEL C/4BEG;ilEND PURGE.HZO LEVEL AFTER.

.E li,'..:

FIELD SHEETU.S. ENVIRONMENTAL PROTECTION AGENCY, REGION VII

ENVIRONMENTAL SER'.'EJCS D .1V. 25 FUNSTON RD. KANG-AS CITY, KS 66115

DUPONT LANDFILLLocation: CAMANUHE IA


Collected: YR: 86 MO: ._.//_. Day: JZr Ti me: ]t$^_ Leader: J. CLEARY

Sample Numbor: J09X7003 SMO #:

S^mp1oSOIL, U1N;::M I L. . 'r'.L i.'J. Mil-l I', OTHER:

- 1 C C'P ! i f ( C j. \~ C\i. .;:; ;j; ,.;-.,. ,; yh: .:i

: Sample Container : Tag Color : Preservative : Analysis Requested

40ml VIAL80oz AMBER80o= AMBER1 LITER POLY1 LITER FOLY1 LITER POLY

LI ME .PURPLEBLUEWHITEWHITEYELLOW

COOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4C

71


Dopth:_

Samp.', er =:

Pan #: Aliquot s :._/ l _ _ . .

: G :'-.••• L'.".?scr [ o ;• •. .-jii:

roC r.-J i.e.rn: r'r .f

01- PEREUNNEL

OATE/TIMEJHWELL ••EPA

V',.CiLAl.p.

. BEGIN ^U»GEND PU

? ••"<"' ?.(;#. .

FIELD MEASUREMENTS:TEMP.« CSALIM *._ccHoucrPH__/C

//, * ,%3 %

f'R£S£^VED(VOLUME PURGED

FIELD SHEET11.'... FN"Ii:r:--!NKNT.",L PROTECTION AGENCY, RtGION VII::NTAL srRv;cc j LW, 2S i-UHSTON RD. KANSAS CITY, KG

: Sit...? N-.i;iu: DUPOIIT I..ANDFTLL: Leae.hi on: CAMAI!CHL JiA

Site Number: X7Site Code:

7"colloctcd: YR: 86 MO:.,//. L v:./!,. Time: A^Jl Leader: J. CLEARY

! Sample Number: J09x".X-^ SMO #: __/^4__.___.__.

Sample Media (circle on •::.•.•;SOIL, DUST , RIN3ATE, SED I MIEN •" ,

e Split v r i r <-. i f.-:

OTHER: ______._.._......

Sample Container : faq Color : Preservative ^Ana^ys^s^ReouRzt&d^j^

40ml VIALSOo;- AMBERGOoz AMBER1 LITER POLY1 LITER POLY1 LITER POLYJ

LIME.PURPLEBLUE

WHITEYELLOW

COOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4C

VGASEMI-VOLPESTICIDESTOT METALSTOT MERCURYNITRATE

Kepth: _./\M.._... ..

Sampltz/'s: __../\/&

Par, 11: ..... A'V.. ._ .

r*. - e

Al iqnots: .

LCS-1I-IENT;.: OF FIEI..L- PERSONNEL

; 2;;. I:, a Oescr i p r :. on .:

DATE.TIME."'''t-'te ~ fg/iT FIELD MEASUREMENTS:WELL ;• /Hu'-V_____ TEMP. ° C /C,£

SALIM >. i.c **,.

A/o

TOt/.e 7.0

H20 IE.'ELBEGIiJENU r:J-1ii£_K7J LEV-1 A,T

PH 7* 3RLTcREO YES^O:'

VOL'Jr/C PURGED ^X-'.^0

FIELD SHELFU.S. FliWIRUNMI/IMl-rtl r-RUT tl'JI I C'N ni^N'JY, REG I UN V! I

LNVjRUNMENTAL :-t:vv [LJtiS 01V. :.-., M. INST UN KD. KANSAS C I T Y , KG

: Si 'it.- No. .no: DUl-'unT I ,'VIDr [!. L: Location: L; MlMLMti. 1A

Si <-.£_> Number; X'.'bi I..- Code: n/,,

YP: f;6 i-l(j: // .

ri-.i.:,b."-,- ;

: o>.iMplti Medi :> • --1 ,•-L :. •_• ...ii -• .> :: SulL, DUST, R L ML.., : I t . . , • ,tu 1 f'.L. : I .

Split ' c i r c l e

: Sample Lent r-.i r:;/r :

: - !0mj VIAL

Lol;:! : f,\i:~''. /T: i/l '•/tiV.

: L1HL -; . ; ; ( • ! 4;

:L-E\ - ';OOL-4l-

aV..!. v:.- v - io ; Rc-f ,•-.'. ' . • - • t ..-d

i LITER POLYi LITER POLY1 LITER POLY

WM! TEWH I TE\XL.L!3W

~ .->•,- : J I..O-

'-'D.'iSE.Mt -VOL.

OUL 4C :COOL 4C :CUOL 4C :C'JOL 4C :

AvC

TOT METALSTOT MERCURYNITRATE

Depth:

Gampl fj: -•_:

Par; i qi'.ot. = : _ A'n.

IV- t . r - V- • i. t

CF: /^ c

DATE/TIMEWELL *__ERA # -I

Tr HNU/OVAfi H2° LEVEL B/J

PURGE xvp!jr;CE- ^^

H2° LEV£L AFTER

SAMPLE -

FIELD"MEASW£MENTS:' TEMP. ° C .*/••*SALin %._____A^CONDUCT U-HOS___/;PH

YES/NO.FILTEREDPRESERVED YES/NOVOLUME PURGED "

SIGNATURES

FIQ.D SHEETU.S. ElMVIKCl i l iE i l i r i i . PI^OTEU'I ION AGENCY, REGION VII

LNVi:i'.'.j|\!MENT'f,L SER'-J'[. !• '"•; D I v. 2';:i Fi INSTON RO. KANSAS CITY, KS 66115

: Lii t.c N.-jme: DURO: II L.iitiDI- .1.1..i..: Locution: CAMANCHE IA

Site Number: X7 :Site Code: n/a :

Collected: YR: 86 ML]:.//.. Da : /%r Time: /A C Leader: J. CLEARY

Sample Numb.2,-: JOVX7OO5 SMU #:

'-OIL. i)l..:'• !' , R !.l I;.-;'. :t. SL'DUILI I! , fWAT ER ,1 OTHER:

L J.ivi- I. D \~r I , ••• < ;;: i ! ' • .:•. •:.;,: ,...• • ; '. r. '-.

'.">;••.iT;p 1 (-• Con h -:.; i n --r : f: to L.. 1 or r. •vat i VR : Analysis Keque/rtt.-c' .:

40n,l VIAL

Sv'or AMivCRi :_. Z TER fOLYi LITER PJL.Y1 LIT-R POLY

Depth:, .../X_......

Samp L c-r z : _ __y'\f.

L I MERURRJ..EBL • JL-:

YE'.LI. JW74 V

77W

Pa/. #:

COOL 4C |COOL 4C

COOL 4Ci.,aci.. 4CCOOL 4C

VGASEMI-VOLPESTICIDESTCT METALSTUT MERCURYNITRATE

Aliquots:_

CUMMCMIG Gl: F I EM.' PERSONNELDATE/TtMEWELL 1_

> .' •• ;. .;; •:.•sa* Tc^ of ^.-a.^/«4v

iy,crtounLi.ituio;TEMP. ° C //.SAUN *,

r-.UILL> SHEETU.'o. E;-IVlRi!NI"ll/NlV,L PRUTK'.JT TON AUENCY. REGION VII

ENV1RUNMENTAL J-tr-V ILL!, >>K'. :;S RiNSTUN KD. KANSAS C1TV, K'J 66115

SiLocation: i..?,: i, ,nu IL 1 A

Si te Number: X7bi Lo L-odu: n/c

: Collected: YR: i;6 MO: //. Day: /Z^ Time:/33C? Leader: J. CL.F

CMU tf:

FAR", ::

DUST, Rlr - is , : : i., :.;Ei.'lriL,:l , fi^'.ii_ri,

op i 1 t: > ci r r j -: ,;;,,;, •> : -, E .-

:•! .-::--:T : 1 3,-4 L'..-...! -,T

VIAL : LI HI.

1 LITER POLY1 LITER POLY1 LITER POLY

J. L<i&s- ?OLY

Deptt , :

Will FL'YELL' iW

P a r ;

r r : I vf -/;• i -d v toe!

•.O..SL 4LCO!)L 4f;COOL. 4CCL'OL 4CC'JOL 4C

TO

Al

'•/'Lir.SEf-il

TOT METALSTO I MERCURYNITRATE

UK F- ' t t Lu

-.'^c.r i p ti. :JH :

rea--' 7.0

DATE/TIMEWELL

#

- (T9</r FIELD MEASUREMENTS:TE^P. « CSALiN

H20 L'VEL G/4BEGifiEND PURGEH20 LEVFL AFTERSAKPLl TIME /3?>0

r i L-i.oh ! - , N ! , i |-'l";i. I;L'. riLN r.L ENC'Y, RECTUM VII

. KANVIAS r

L'l.JPOilT ! . . . ; , l ' - i : . - |Locat ion; Cri: lAMLJIE i , ,

Si te? Nuifibor: x. 7Si t c:- Code: n,<

: C.oIiL?c:t-d: YR: G-:., !U;: // D.:,y.-// Leader: J . CLE.'iRY

: Jiampl ;? M...ur:b?ji- J-'j'vx'/OOc:.-

: Sainple Hud.:, a. U:: :t i- • c .1 c? cii : c > ^ :: SOIL. D U G T , R I N : , , '; ; b , ; •: E i.) 1 i' 1 E M

: Sample Split i c i. r c 1 :::• a>"< <:••>: ', E i

SMO #: ..j4 __ ._ ... ._ :

/ ~ \: ., (VATER\ 01MER; :

£> ;: Sample Cc:rita.i nzr : Tag L'clor : F:';

40ml VIAL LIME . :8002 AMBER8Ocn AMciER1 LITER FCJLY1 LITER FGLY1 LITER FOLY

i L. + tr- Pct-^

L^rPa^

PURPLE :BLUE :i-)H.[TE :WHIIE :YELLOW :

T.4rJ ^

T^, :Depth: _ / l M . _ _ Pur. tt:.__A'4

Samp 1 E-r 3 : __ _ _/V. ..

•iLiervat i ve : Analysis Requested :

COOL 40 VGA :COOL 4CCOOL 40COOL 4CI.UCL 40COOL 4C

^C,Acfe-MT^ .,.-0

H rc j> H 7 *f

C:<TOL t/'c

SEMI-VOL :PESTICIDES :TOT METALS :TOT MERCURY :NITRATE :

s«LPvP^ ::

m«»r/CHU*.K/^Te. I• •

Al iqncts: __y/v'/f_. _ :

•--- — iCOMMENTS OF FIEu.b FERSOI-4NEL

: Si to -r i Dt i 01 , :

«. tr>7.0 .

fH 7.0

0 ATE ,?TI M E'WELL i W\,\}~

A JGiJU.X'/A S2

LEVEL J/-,BESiU

|I20 LCV'.L >'.

FIELD MEASUREMENTS:TEMP. « C_SALIM •<•._COHOUCfPH ->F;I.TEKED

VOLUME PURGED ~

FiLZL.O SHEETi I.'', i -HVlh- i 'Mr i r r iVM. PI\Glc' ' . ' l TON AUCMCY, RE.Gl(.;:,i '. ! I

E:NVJ.I-:. iN:lh:NTAL 'A.'.- ' • / : Li:- "i D I V . ;:r:, !" M IT: :.H R'..:. KAN: A3 C ITY , K-: 16

bi i-:. N.'ifr::: D! Ji •1(JI !Y L.Ai'-IOf- U.lLo;.. ration: CM Mr, ML I !L I.V.

S i te? N'jmtaor:Lode:

-• ----- -- ••• — --.------•--- — - ——— ...__..... — _.._ t

Collected: YR: 86 MO: // Day:J/_. TimE:_/ViT Leader: J. CLEARY :i :

Sa.T.plQ Number:: J07X7007F SMO #: __y]//4'__ —— .._ :

Sample Media (circle o •'!•:) : / " "\ 'SOIL, L-UST, RINGATE, GEUlnEM 1 , Q- Vnip , OTHER: __._.__._..._._.___.. •

Sample Split ( - i r n 3. D ciu:>: YES (Miy ••

"

: Sample Ccntain^r

: 40ml VIAL: 80oz AMBER: &0c= AMBER: 1 LITER POLY: 1 LITER POLY: 1 LITER POLY

; j»:

•

i.frr- Po^f

Depth : ... // .._

Samp 1 or:;. :

:

::n«

:::

*•

::

....

T aa Crjl or :

L I MEPURPLEh'LUEI'll 1 1 TEWHITEYELLOW

IV.

TAW

Pan

::•

:::

: =:::

»:.._/

p.- t:Si-::-f vati. ve.- : Analysis Requertod :

COOLCOOLCOOLCHGLCUOL.COOL

Z/-I i^^AcMo,C H T6 (

V* ........

4C VGA4C SEMI-VOL ;:4C PESTICIDES :4C TOT METALS =4C TOT MERCURY :4C NITRATE

JH7^| """ :

y»(__ [/tL^t-l^'^Y/C HLo£iO£ /ZULfiiTg- .

Al iq'.tots: _ . < C L _ _ '

M*.. ._...... .._...... .... . .._ . ._.....— :

CUMMEN'l !'] OF FIEi. L< RERSIJI Jr!EL

DATE'TIME '""'//'/ft, -<

vi f -.-•• D : . - : 3 • : : . • - I. o'. '. "-': '•. V'.'ZLL r

HfU/OVA J,LEVEL C/4.

ENDH^Q LCVE! AFTERSAMPLE iiMi.

A.' A

FIELD MEASUREMENTS:TEMP. « C_SALIM "&.JCCfWUCTPHFiLTESEi)PRESERVEDVOLUME

ANALYSIS TYPE: TOTAL METALS <COK. .ACTOR)TITLE: DUPONTLAB: CHEMTECHSAMPLE PREP:__. ANALYST/ENTRY: E40

J09X7001

MATRIX:METHOD: 90REVIEWER: _

UNITS: UB/LCASE: 6562DATE: 12/11/86

COMPOUNDALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKELPOTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINC.CYANIDE

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

48000.60.010.02305.0018.0

220000.11015.096.0

52000.22.0

110000. :1200.

0.21003500.

5.0010.0

12000.10.0N/A

120140

N/A

UU

U

M

U

MUU

UI

I

44000.60.010.0

9802.0038.0

230000.14082.0140100000.31.0

99000.8700.0.2

21017000.

5.0010.0

31000.10.0N/A

140230

N/A

5500. .,U 370. ...U 500

550M 20.0

60.028000.15091020011000.40.08100.2200.

U 1.302900..

M 3200.U 5*00U 80.0

3400000.U 10.0I N/A

1600.380

I N/A

\*•

u

uM

uuH£

.

HUU

UI

I

36000.60.0 U18.07402.00 M

.. 25.0210000.

18013014044000.29.0

100000. .-13000.

0.2 .37610000.

3.80 H10.0 U360000.

10.0 UN/A

160150

N/A

U

I

I

ANALYSIS TYPE: TOTAL METALS (CONTRACTOR)TITLE: DUPONT-LAB4. CHEMTECHSAMPLE PREPJ_. ANALYST/ENTRY: E4o

J09X7005

MATRIX: UAMETHOD: 90REVIEWER:

UNITS: UG/LCASE: 6562DATE: 12/11/86

COMPOUNDALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUM ....CALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKEL;POTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINCCYANIDE

SAMPLE NUMBERS : .

J09X7005D J09X7006 J09X7007F

29000.19014081010.040.0

200000.15090.0120

57000.— - — —— c31P

100000.4300.

0'2.320

11000,5.0040.0

950000.10.0N/A

250540

N/A

U

MU

MM

U

MUU

UI

I

28000.19081.070010.040.0

220000.13070.0110

530AP-,/3T60-V99000.4400.0.2ciiBcn

1 4000 .5.0040.0

820000.10.0N/A

200430

N/A

U

MU

MM

U

MUU

UI

M

I

36000. ,60,0 ..10.04102.0026.0290000.96.041.012062000.28.0110000.3200.0.2

1506800.4.30

10.092000.10.0N/A

140190N/A

:: . ... 200U . 60.0M 10.0

200M .... 5.00.

.... _•. 5.00 _..75000. .....

10.0M 50.0

25.0 .64.05.00

5000.^ '•'..'. 15.0'U 0.2

40.05000.

M 5.00U 10.0

5000.U 10.0I N/A

' . 50.020.0

I N/A

UUUUUUUUUUMUUUU

UUUUUUI

UUI

ANALYSIS TYPE: VOLATILE ANALYSESTITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E94

MATRIX: WATERMETHOD:

COMPOUNDCHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACETONECARBON DISULFIDE1,1 DICHLOROETHENE1.1 DICHLOROETHANETRANS-1,2,-DICHLOROETHENECHLOROFORM1,2,DICHLOROETHANE2-BUTANONE1,1,1 TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBROMODICHLOROMETHANE1,1,2,2,-TETRACHLOROETHANE1 ,2-DICHLQROPROPANETRANS-1,3-DICHLOROPROPENETRICHLOROETHENEDIBROMOCHLOROMETHANE1, 1 ,2-TRICHLOROETHANEBENZENECIS-1»3-DICHLOROPROPENE2-CHLQROETHYL VINYL ETHERBROMOFORM2-HEXANONE4-METHYL-2-PENTANONETETRACHLOROETHENETOLUENECHLOROBENZENEETHYL BENZENESTYRENETOTAL XYLENES

J09X7001


SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

10.010.010,010.025.015.05.005.005.005.005.005.0010.05.005.0010.05.005.005.005.005.005.005.005,005.00

10.05.00

10.010.05.005.005.005.005.005.00

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

10.010.010.00.719.021.05.005.005.005,005.005.0010.05.005,0010.05.005.005.005.005.005.005.003.205.0010.05.0010,010.05.005.0010.05.005.005.00

UUUM

UUUUUUUUUUUUUUUUUUUMUUUUUUU

UUU

2502502502509105803600.130130130130130380130130250130130130130130130130130130250130250250130130130130130130

UUUUUU

UUUUUUUUUUUUUUUUUUUUUUUUUUUU

10.010.010.010.08.70

21.05.000.65.005.005.005.0010.05.005.0010.05.005.005.005.005.005.005.0011.05.0010.05.0010.010.05.005.005.005.305.0024.0

UUUUUUUM

UUUUUUUUUUUUUUU

UUUUUUUU

U

ANALYSIS TYPE: VOLATILE ANALYSESTITLE: L.TQTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY:

COMPOUND

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACETONECARBON DISULFIDE1*1 DICHLOROETHENE1.1 DICHLOROETHANETRANS-li2F-DICHLOROETHENECHLOROFORM1»2,DICHLOROETHANE2-BUTANONE1 » 1 » 1 TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBROMODICHLOROMETHANE1»1 ,2»2 , -TETRACHLOROETHANE1 »2-DICHLOROPROPANETRANS-1,3-DICHLOROPROPENETRICHLOROETHENEDIBROMOCHLOROMETHANE1f1» 2-TRICHLOROETHANEBENZENECIS-1»3-DICHLOROPROPENE2-CHLOROETHYL VINYL ETHERBROMOFORM2-HEXANONE4-METHYL-2-PENTANONETETRACHLOROETHENETOLUENECHLOROBENZENEETHYL BENZENESTYRENETOTAL XYLENES

MATRIX: UATER UNITS: UG/LMETHOD: 9302MOi ^ CASE: 6562

ENTRY: E94 REviEWER:\pi/^.^4__/^ DATE: 12/31/86SAMPLE NUMBERS

J09X7005 J09X7005D J09X7006 J09X7007F

100100100100220

1100.1600.50,050.050,050.050.0

21050.050.010050.050.050.050.050.050.050.05.00

50.010050.010010050.0

1700.50.04.50

50.050.0

UUUUUU

UUUUUUUUUUUUUUUUMUUUUUU

UMUU

1001001001003507101100.50.050.050,050,050.014050.050.010050.050.050,050,050.050,050.050.050.010050.010010050.01100.50.050.050.050.0

UUUUUU

UUUUUUUUUUUUUUUUUUUUUUU

UUUU

10.010.010,010,011,026.05.000,55.005.005.005.0013.05.005.0010.05,005.005.005.005.005.005.005.005.0010.05.0010.010.05.005.005.005.005.005.00

UUUUUUUM

UUUUUUUUUUUUUUUUUUUUUUUUUUU

10.010.010.010,045.01200.75.005.005.005.005.007.705.005.0010.05.005.005.005.005.005.005.005.005.0010.05.0010.010.05.001.405.005.005.005.00

\J

UUUU

MUUUUUMUUUUUUUUUUUUUUUUUHUUUU

ANALYSIS TYPE: SEHIVOLATILES (PAGE i>TITLE: L.TOTDZ FARM <DUFONT)LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY:

MATRIX:METHOD:

WATBR

E95


COMPOUND

PHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1»3 DICHLOROBENZENE1»4 DICHLOROBENZENEBENZYL ALCOHOL1,2 DICHLOROBENZENE2-METHYLPHENOLBIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2»4-DIMETHYLPHENOLBENZOIC ACIDBISC2-CHLOROETHQXY) METHANE2»4 DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2»4f6-TRICHLOROPHENOL2y4f5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLFHTHALATEACENAPHTHYLENE3-NITROANILINEACENAPHTHENE2»4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2»4-DINITROTOLUENE

J09X7001

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

20.020.020.020.020.020.020.020.020 .020.020,020.020.020.020.020.010020.020.020.020.020.020.020.020.020.020.010020.010020.020.010020.050.0

20.020.0

UUUUUUUUUUU

, UUUUUUUUUUUUUUUUUUUUUUUUI

UU

20.0

20.020.0

20.0

20.0

20.020.020.020.0

20.0

20.020.020.020.0

20.020.0

20.010020.020.010020.0

20.020.0

IUI

UUI

UI

UI

UUUUIII

UI

UUUUI

UUII

UUUUUUII

UU

13040.040.040.040.040.040.040,040.010040.040.040.040.040.040.096.040.040.040.040,040.040,040.040.040.040.020040.020040.040.020040.050.0

40.040.0

JUUUUUUUUJUUUUUUMUUUUUUUUUUUUUUUUUUI

UU

10.010.010.010.010.010.010.010,010.010.010.010.010.010.010.010.050.010.010,010.010.010.010.010.010.010.010.050.010.050.010.010.050.010.050.0

10.010.0

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUI

UU

ANALYSIS TYPE: SEMIVQLATILES (PAGE 2>TITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E96

MATRIX: UATERMETHOD: 930/2MAREVIEWER:

COMPOUND2»6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHERFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3»3' DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENE.INDENO(1»2F3-CD)PYRENED I B E N Z O < A » H ) A N T H R A C E N EBENZO(G»Hi DPERYLENE

J09X7001


SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

20.020.020.020.010010020.020.020.010020.020.020,020.020.020.040.020,020.020.020.020.020.020.020.020.020.0


20.020.020.020.0100

20.020.020.0

20.020.020.020.020.020.040.020.022020.022.020.020.020.020.020.020.0

UUUUUI

UUUI

UUUUUUUUUUUUUUUUU

40.040.040.040.020020040.040.040.020040.040.040.040.040.040.080.040.040.040.040.040.040.040.040.040.040.0

UUUUUUUUU:UUUUUUUUUUUUUUUUUU

10.010.010.010.050.050.010.010.010.050,010.010.010.010.010.010.020.010.019010.010.010.010.010.010.010.010.0


ANALYSIS TYPE: SEMIVOLATILES (PAGE i>TITLE: L.TQTDZ FARM (DUPONT)LAB: PACIFIC ANALYTICALSAMPLE PREP:___ ANALYST/ENTRY: E95

MATRIX: WATERMETHOD: 93.02MREVIEWER:

COMPOUNDPHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1,3 DICHLOROBENZENEIf 4 DICHLOROBENZENEBENZYL ALCOHOL1,2 DICHLOROBENZENE2-METHYLPHENOLBIS(2-CHLDROISOPROPYL)ETHER4-METHYLPHENOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS<2-CHLOROETHOXY) METHANE2»4 DICHLOROPHENOL1,2f4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2,4, 6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINEACENAPHTHENE2i4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE

J09X7005


SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

12010010010010010010014.0

100320100100100100100100770100100100100100100100 ^100100100500100500100100500100500

100100

UuuuuuMU

UUUUuuuuuuuuuuuuuuuuuuuuI

uu

72.010.010.010.010.010,010.011.010.0

17010.0

" 10.010.010,010.02.60

20,010.010.010.02.50

10.010.010.010. 010.010.050.010.050,010.010.050.010.050.0

10.010.0

UUUUUuuuuuuuMMUUUMUUUUUUUUUUuuuuI

uu

10,010.010.010.010,010.010.010.010.010.010.010.010.010.010.010.050.010,010.010,010.010,010,010.010.010.010.050.010.050.010.010,050.010.050.0

10.010.0

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuI

uu

10.010.010.010.010.010.010.010.010.010.010.010.010.010.010.010.050.010.010.010.010.010.010.010.010.010.010.050.010.050.010.010,050.010.050.0

10.010.0

uuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuuu: uuI

uu

ANALYSIS TYPE: SEMIVOLATILES <PAGE 2)TITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E96

MATRIX: WATERMETHOD: 930REVIEWER:


COMPOUND2»6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHERFLUORENE4-NITROANILINE4i6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE4-BROMQPHENYL PHENYL ETHERHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3>3' DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO(li2f3-CD)PYRENEDIBENZO(AfH)ANTHRACENEBENZO(GiH»I)PERYLENE

J09X7005

SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

10.010,010.010.050.050.010.010.010.050.010.010.010.010,010.010.020.010.010.010.010.010.010,010.010.010.010.0

uuuuuuuuuuuuuuuuuuuuuuuuuuu

10.010.010.010.050.050.010.010.010,013.010.010.010.010.010.010.020.010.010.010.010.010.010.010.010,010.010.0

uuuuuuuuuMuuuuuuuuuuuuuuuuu

10,010,010.010.050.050.010,010,010,050.010.010.010.0"10.010.010.020.010.010.010.010.010.010,010.010.010.010.0

uuuuuuuuuuu

. uu

;uuuuuuuuuuuuuu

10.01.20

10.010.050.050.010.010.010.050,010.010,00.7

.10.010.010,020.010.0

10010.010.010.010.010.010.010.010.0

uMuuuuuuuuuu

MuuuuuMuuuuuuuu

ANALYSIS TYPE: PESTICIDESTITLE: L.TOTDZ FARM (DUPONDLAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E97

MATRIX: WATERMETHOD: #302MoiREVIEWER:

COMPOUNDALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHCHEPTACHLORALDRINHEPTACHLOR EPOXIDEENDOSULFAN IDIELDRIN4i4'-DDEENDRINENDOSULFAN II4t4'-DDDENDRIN ALDEHYDEENDOSULFAN SULFATE4>4'-DDTENDRIN KETONEMETHOXYCHLORCHLORDANETOXAPHENEAROCLOR-1016ARQCLOR-1221AROCLOR-1232AROCLOR-1242AROCLOR-1248AROCLOR-1254AROCLQR-1260


SAMPLE NUMBERS ,;

J09X7001 J09X7002 J09X7003 J09X7004

0.10.10.10.10.10.10. 10.10.20.20.20.20.20.20.20.20.21.001 .002.001,001.001.001.001.002.002.00

UUUUUUUUUUUUUUUUU

UUUUUUUUUU

0.050.050,050,050,050.050.050.050.10.10.10.10.10.10.10.10.10.50.51.000,50.50.50.50.51.001.00

UUUUUUUUUUUUUUUUUUU

UUUUUU

UU

5.005,005.005.000.050.050.050.050.1 .0.10,10.10.10.10.10.10.10.50,51.000.50.50,50.50,51.001.00

UUUU

UUUUU

J U ,

•."'.'UUUUUUUU

; uU

uuuuu

uu

0.050,050.050.050.050.050.050.050.10.10.10,10,10.10.10.10.10.50.51,000.50.50.50.50.51.001.00

Uuuuuuuuuuuuuuuuuuu

uuuuuu

uu

ANALYSIS TYPE: PESTICIDESTITLE: L.TOTHZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP*.____ ANALYST/ENTRY: E97

MATRIX: WATERMETHOD: 930REVIEWER: .Ml4^-


COMPOUNDALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHCHEPTACHLORALDRINHEPTACHLOR EPOXIDEENDOSULFAN IDIELDRIN4*4'-DDEENDRINENDOSULFAN II4f4'-DDDENDRIN ALDEHYDEENDOSULFAN SULFATE4»4'-DDTENDRIN KETONEMETHOXYCHLORCHLORDANETOXAPHENEAROCLOR-1016AROCLOR-1221AROCLOR-1232AROCLOR-1242AROCLOR-124BAROCLOR-1254AROCLOR-1260

J09X700;

SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

5.005.005.005.000.050.050.050.050.10. 10.10,10.10.10.10.10.10.50.51.000.50.50.50.50.55.601.00

UUUU

UUUUUUUUUUUUUUU

UUUUUU

JU

5.005.005.005.000.050.050.050,050.10.10,10.10.10.10.10.10.10.50,51,000.50.50.50,50.55.601.00

UUUU

UUUUUUUUUUUUUUU

UUUUUU

J-U

0,050.050,050.050.050.050.050.050,10.10.10.10,10.10.10,10,10.50.51.000.50.50.50.50.51.001,00

UUUUUUUUUUUU

; u, u

uuuuu

uu

: Uuuu

uu

0.050.050.050.050.050.050.050.050.10.10.10.10.10.10.10.10.10.50.51.000.50.50.50,50.51.001.00

UUUUUUUUUUUuuuuuuuu

uuuuuu

uu

TITLE: L.TOTDZ FARM(DUPONT) MATRI X : WATERLAB: PACIFIC ANALYTICAL METHOD: 9302M01ANALYST/ENTRY: LT REVIEWER: KIRCHM

UNITS: UG/LCASE: 6562DATE: 12-31-86

TENTATIVELY IDENTIFIED COMPOUNDS

SAMPLE NO.

J09X7001J09X7001J09X7001JO9X7001J09X7001JO9X7001JO9X7002J09X7003JO9X70O3JO9X7O03J09X7003JO9X7003J09X7003JO9X7003J09X7003

J09X7003JO9X70O4J09X7004JO9X7O04J09X7004

J09X70O4J09X7004JO9X7005JO9X7005JO9X7005J09X7005J09X7005J09X7005J09X70O5J09X7005J09X7002J09X7004J09X7004J09X7005J09X7005J09X7005

COMPOUND NAME** FRACTION EST. CONC.*

NOTHING SIGNIFICANT FOUND VOA2,5,8.11,14-PENTAOXAHEXADECAN-16-OL BNA2,2-(2-METHOXYETHOXY)ETHOXY-ETHANOL BNA2,5,8,11,14-PENTAOXYPENTADECANE2--ETHOXY-l-METHOXYETHOXY)-ETHENE5-METHYL-l,4-HEXADIENENOTHING SIGNIFICANT FOUNDNOTHING SIGNIFICANT FOUND1,3,5,7,9-PENTATHIECANE1,2,4-TRITHIOLANE1,2,4,6-TETRATHIEPANE1,3,5,7-TETRATHIOCANEBENZENEACETIC ACID1,3,5-TRITHIANE1-CYCLOHEXEN-l-OL, 2,6-DIMETHYL-ACETATETETRADECANOIC ACIDTETRAHYDROFURAN2,2(2-METHOXYETHOXY)ETHOXY ETHANOL2,5,8,11,14-PENTAOXAPENTADECAN-16-OLBNABENZOIC ACID,3,5-BIS(1,1-DIMETHYL-ETHYD4-HYHEXADECANOIC ACID1,4-DIMETHYL BENZENE2-PROPANETHIOL1,2,4-TRITHIOLANE1,2,4,6-TETRATHIEPANE1,3,5,7-TETRATHIOCANEBENZENEPROPANOIC ACIDBENZENEACETIC ACID2,5-DIMETHYL-BENZENEBUTANOIC ACID2-METHYL-FENTANOIC ACID2 UNKNOWN COMPOUNDS4 UNKNOWN HYDROCARBONS3 UNKNOWN COMPOUNDS

• UNKNOWN COMPOUNDS1 UNKNOWN HYDROCARBON4 UNKNOWN COMPOUNDS

BNABNABNABNABNAVGAVOABNABNABNABNABNABNA

BNABNAVOABNA.BNA

BNABNABNAVOABNABNABNABNABNABNABNABNABNABNAVOABNABNAVOfir

216212602420

935270564O4B29521112994

472328

19586484132

16 -102O50

2120124012801120540320340

20-45646-35212-216160-17060

2OO420-344020000

JJJJJ

JJJJJJ

JJJ — *JJ

JJJJJJJJJJJJJJJ<iy-»-JJJ _

*This is a crude estimation based on response relative to aninternal standard. An authentic standard has not been run.

**The compounds were identified using a library search routine.Authentic standards have not been analyzed to veri-fy compound massspectra and retention times.

TITLE: L.TDTDZ FARM(DUPDNT)MATRIX:LAB: PACIFIC ANALYTICAL METHOD:ANALYST/ENTRY: LT REVIEWE;

WATER93CV2M01

KIRCHMER



SAMPLE NO. COMPOUND NAME** FRACTION EST. CONC.*

JO9X7OO5DJ09X7005DJ09X7005DJ09X7005DJO9X70O5DJ09X7005D

J09X7005DJ09X7005DJ09X7005DJO9X7O05DJ09X70O5DJO9X70O5DJ09X7006J09X7006J09X7006J09X7007FJ09X7007FJO9X7007FJ09X7007FJO9X7O05DJ09X70O5DJO9X7006J 09X7007

TEJRAHYnROEJJRAN-.. - . _1,2,4-TRITHIOLANE1,3,5-TRITHIANE1 , 2, 4, 6-TETRATHIEPANEBENZENEACETIC ACID3-CYCLOHEXENE-l-METHANOL, ALPHA, ALPHA4-TR1,3,5, 7-TETRATHIOCANEHEXANOIC ACID3-METHYL PENTANOIC ACID1,3,5-TRITHIANE2, 5-DIMETHYL-BENZENEBUTANOIC ACIDPENTANOIC ACIDNOTHING SIGNIFICANT FOUND2-2 (2-METHOXYETHOXY) ETHOXYETHANOL2,5,8, 11, 14-PENTAOXYHEXADECAN-16-OLTR I CHLOROFLUOROMETHANEHEXANEDIOIC ACID, DIOCTYL ESTER2 HEPTENAL <Z>-2-CYCLOHEXENE-l-ONE7 UNKNOWN COMPOUNDS1 UNKNOWN HYDROCARBON1 UNKNOWN HYDROCARBON1 UNKNOWN HYDROCARBON

VOABNABNABNABNA

BNAVOABNABNABNABNABNAVOABNABNAVOABNABNABNABNABNABNABNA

LQSBfiL .802710690490

39O338298296220

-•' 172160

30305

4002814

22-572-• 30

3660

J " -iJJJJJJJJJ ' . cJJJJJJJJJJ •JJ


##The compounds were identified using a library search routine.Authentic standards have not been analysed to veri-fy compound massspectra and retention times.

TITLE: DUPONTLAB: CHEMTECHANALYST/ENTRY: LT

MATRIX: WATERMETHOD: SEE * BELOWREVIEWER: GCS iff

UNITS: MG/LCASE: SAS2564GTE: 12-11-86

SAMPLE NO. CHLORIDE SULFATE NITRATE SULFIDE ALKALINITY

J09X7001J09X7002JO9X7OO3J09X70O4J09X7005J09X7005DJ09X7006J09X7007F

12.019.0

66025927017026.03.0

53.911.917.7

10039.93211717.3

5.050.02U0.02U

0.02U0.02U0.02U330.02U

l.OU1 . OU "

169

l.OU2.93.3i.ou ; •;1 . OU

"•?' :"

262642883O7402250,2280

:* 1844 -•: 6.0

* METHOD'NOS.:

CHLORIDE -SULFATE -NITRATE -SULFIDE -

ALKALINITY -

3251W033751W033531W023761WO131O1WO1

Case No.: 6562 Laboratory : Chemtech

Contract No.: SOW 785 Method No.: 9001M07

SMO No-.: MGD050-MGD058 Activity No.: 009X7

Site : Dupont Matrix : Water

We have reviewed the above case. The following are our findings:

1. Analysis was requested for the contract inorganic totalmetals fraction only.

2. Iron was reported in the field blank sample, J09X7007F/MGD056. Sample results were all greater than five times theblank level for iron, therefore no qualifications were made basedon the blank rules.

3. Antimony exceeded MES recovery control limits, but above30%. Since no positive responses were recorded in the samplesfor antimony, no qualifications were made on the sample data forantimony.

4. A performance evaluation audit was introduced as sampleJ09X7008P/MGD057. All metals were correctly identified althoughiron was quantitated at 2.5 times the spiked concentration.

Case No.: SAS 2564G«

Contract No.: NA

Laboratory : Chemtech

Method Nos.: 3251W03, 3751W03,3531W02, 3761W01, 3101W01

SMO No.: MGD050-058 Activity No.: J09X7



1. Analyses were requested for chloride, sulfate, nitrate,sulfide and total alkalinity. The audit sample, MGD057, was notrequested to be analyzed for sulfide.

2. Initial and continuing calibrations and calibrationverification solution analyses along with blank, duplicate andmatrix spike results were all satisfactory.

3. The field blank sample, J09X7007F/MGD056, was reported tohave insignificant amounts of chloride and total alkalinitycompared with sample results. This field blank did have sulfatereported at the concentration level of the performance evaluationaudit (J09X7008P/MGD057) true value. Since sulfate was reportedas a non-detect in the audit for sulfate, and sulfate, chlorideand alkalinity are analyzed from the same sample container, andchloride and alkalinity audit results are acceptable, it appearsthe laboratory has switched the field blank and audit samples forsulfate analysis. The data were not qualified by the blank rulesbecause of the high probability of a sample mixup. All otheraudit sample parameters were correctly identified.

f UNITED STATES ENVIRONMENTAL PROTECTION AGENREGION 7

25 FUNSTON ROADKANSAS CITY, KANSAS 66115

''cj Other:

Date:

MEMORANDUM

SUBJECT: Data Transmittal for Activity #: 0 0 S X ^7Site Description: Qunfc^cb LQ.W^^;\\

FROM: Robert D. Kleopfer, Ph.D.Acting Chief, Laboratory Branch', ENSV

TO: Robert L. MorbyChief, Superfund Branch, WSTM

ATTN: _____________________

Attached is the data transmittal for the above referenced site.

This should be considered a __ Partial __ Corrected _ Complete

data transmittal (completes transmittal of ____________). If you

have any questions or comments, please contact D. Simmons at 236-3881.

Attachments

cc: Data File

U.S.FIELD SHEETPROTECTION AGENCY, REGION VII

!'.;•,• . 2;= F:L:NSTGN RD. KANSAS CITY, KG

b:i he Name: DUrCN'l LANDFILLLocatior,: CAi lANUHL IA

Site Number: .<'/Site Code: n/;

: Collected: YR: 86 Mu:.//.. Day:..//...

: Sample Number : JO9X7oO:lX«

: S^rrip 1 e Modi a (ci r c 11 on..--.:• > :: SO 11- , DUS T, RI N^AT E . :DLD I !''ENT ,•

: ./v.i.'ip \. o Sp Jib (c ]. i ::: .1. u

Leader: J. CLEAPY

SMO #:

TER) OTI IER:

: Sample Container : Tag Color :

40ml VIALSOoz AMBER80oz AM3ER1 LITER POLY1 LITER POLY1 LITER POLY

i l~i4r,- PL-UV

Df'pth: /V4

Samplers: _f^A

a

LIME :PURPLE :BLUE :WHITE :WHITE :YELLOW :

;::

F- in #:|

Prese r v ative : An a lysis R e q u e stc d :

COOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4CCOOL 4C ,

toot yc.

H.tJA.. Al]

VOA :SEMI-VOL :PESTICIDES ,:TOT METALS .:TOT MERCURY :NITRATE :

K/ rfr/cW/.0«>.3£/Wr£ •'

Lquots: s^-A ;

;COMMENTS OF PIELJ PERSONNEL

DATE/TIME/'A/<?£>'V.'cLL * AAW- /: Site Dt/scn p t i on :

: MW-lPELD MEASUREMENT!TEMP. ° C_SAL.N '

.MfcNIi:y/,r"iii«Uj'OVA-L3 AgHiNU/Gv'A-CM2U LEVEL

I CM-PC

FIELD SHEETu.s. GMvn:i:rMLin.".L. F -ROTLLTIOM AGENCY, REGION vn

i•••'... iiFpA'tuES D:I.V.. 25 FL.'NSTUN RD. KANS)A3 CITY, KS

: Site Mama: DUPQN 1 L.ANi:-FH..!_: Location: CAMANCHL

Collected: YR: 86

Sample Number:

S impl o Mcidia (ci re !.SOIL, DUG 1 , RINV

Sample Spl it ici r r i

1,-,

MO : ._//. Day : _//_ .Time: /_?£

J 09X7002 SMO

fj our • : /"" ^-~\IEi. bEDIiiEN! , AjATERy

c: c - i i ' . • : YIFS /NU^

: Sample Container : Tag Color : Preservative

::::::••

•

:.

:

••

:

.

:

.

: o

: j

40ml VIAL :QOoz AMBER :GOoz AMBER :i. LITER POLY ":1 LITER POLY :1 1.. I TER F-OLY :j, L,J(i- ^>oi.Y

:

:

J, Lt-t-fr~~ poL Y %

Depth: ^^

Sampler^: X^A

.

f 'Gi-

•:' i tc L'oscr i p :. ;. on :

/V\*V <L_

Hnvetfi. f'J,i>rW fo fv-f-ff^ C«4.c t.-c( 7 o.H rwt4p,- ck*r^^ *"*" 3 i &.^

i;.<''o' ^JCi( -fcp,,^ Tsr" C-( ?TC.i'

LIME : COOL 4CPURPLE : COOL 4CBLUE : COOL 4CWl-l ITE : COOL 4CL'!i! l !E : COGL AC\ELLGW : COOL 40

n

'-. /y'(..rH TO ^M 7 "7

T4H ; (Tpc6 ty*C

Pan #: x/'/4 Al

: :

! ' J

MLH1L] OF I'lELD PERSONNEL

DATE/TIME '%/4fe - /TOWELL v SitU'2.

t J"^lC]> ~IQQ_'L-^•IJG / £ -vv,\.HJ A/.P. w/« &m-£'EL U/4 20.52- '

BEGIN PUfJCt /Z . /O7u END PURGE /ZZJT

,«.tl HZO LEVEL AFTER ZS.CS"'

Sits Number: ,<7Site Code: n/a

_ . .

Leader: J. CLEARY

#: ._ /!/A- — — .- -

OTHER :_ .___ . . _. . . . . . „__. .

: Analysis Requested


- -\-

***i,v.t,/fMe*./^Lf^

iquots: yv'A

FIELD MEASUREMENTS:TEuP. « C ?.CS.\LIN *. C. 7J" cCOHJUCT UMMOS ,fcm 9 ?O

,.» M ^. i 'FILTERED YE9fN0rRESEAvEDtiL^/^O ^.li-f-^fVOLUME PURCEO ^^.^$"^//««SAlMLLUS SluFJATUntJ

:

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FIELD SHEETU.S. ENVIRONMENTAL.. PROTECT I ON AGENCY, REGION VII

ENVIRONMENTAL SERVERS DIV. 25 FUNSTON PP. KANSAS CITY, KS 661M

:*•

Site Name: Dl.JPONTLocation: CAMANU

LANDFILL. Site Number: X7 :HE. I A Site Code: n/a :

Collected: YR: 86 MO :...//.. Day: ,/ r Time: / -C Leader: J. CLEARY

Sample Number: JO^X/003 SMO #: ._//& _._...._ _

•«

:

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'ii.J3.mp 1 '••:-? Mod c a ( c 1 1SOIL, DLISI , RIN

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40ml VIAL :8002 AMBER :80oz AMBER :1 LITER POLY :1 LITER POLY :.1 LITER POLY :1 Lt-itr- PeLy :

;::

1 L<T££ fci-Y ::

Depth : _ .fiJo

£-3.mpl er s : yV

r. 1 (.:• •:;!.;; ' : ^ -^••:;iilL. !i-:.LLi.''j.hEI'li', (WfiTtLh^ OTHER:

•••i ••: o:ik- > : Y£-.-L; /Co)

Tag Lnl or : Preservative : Analysis Requested :

LIME : COOL ,4C VOA '•PURPLE : COOL 4C SEMI-VOLBLUE : COOL 4C PESTICIDESWHITE : COOL 4C TOT METALSWHITE : COOL 4C TOT MERCURYYELLOW : COOL 4C NITRATET4«4 :**4 ?,«c ^ceixrt 0 <;

;. f\k« OH rc^M 71 ' ' ":

TH<\\ : (.Pci U 6f_ #)L) * <ji+ / /. ' V L«,ur/ r cP .; '. n # : A/ A- _ Al i quot s : _/l/4.

:.A_ ___._„„..__„ .„.._„.___

L'.GMMENTS OF FIL^L.U PEREUNNEL

: EDATE/TIME ('/^,WELL XMvJ-3EPA

HELD MEASUREMENTS:TEMP.SALIH ;

M&^UKLMkrJIA:

."C //, 2. J' *. TL*' ?^rUCTwuMoa/:^ //T,^r J

FIELD SHEET.S. FN"Ir'PNi-0,mL PROTECTION AGENCY, FUSION VII

^!'RV i: Cl-.S D1V.. 2"! !': u'i I5TGN RD. KANSAS CITY, K13 6M

: Bite Namu: DUPQNT I..ANPFILL: Location: CAMr.NCHL LA


: Collected: VR: 86 MU:./A

I Sample Number: JO'-^"

Time:/^^ Loader, J. CLEARY

SM° *' "

..._......_.. Media (circle ana::: SUJ.L, DUST, R1NSATE, bi£DIMIENT, (WATER^,) OTHER:.

:;; .;, ,v, p i •-.:• S [.:• lit (c: i r • c .!. e a:. t • • : Y E S

Container : fag Color : Pr-eservat iv

40ml VIAL.SOo;: AMBEReOcz AMBER1 L.[TER rCJLY1 LITER POLYt LITER POLYJ LiifC

LIMEPURPLEBLUE:WHITEWHITEYE I-LOW

COOL 4CCOOL 4CCOOL 4CCOOL 4Cr:GGL 4CCOOL 4C

VOA ;SEMI-VOLPESTICIDESTOT METALSTUT MERCURYNITRATE

!>t;pt !-.:„.//.

SaiTipl crs:

Par. «:. ...A'/.. _.. Aliquots: _*

•:-. i I; .; ••:'.!•" ••. t :> r: •.

LJ OF F1E1..D PERSONNEL

7 «

DATE.TIME !'WELL /•'

FIELD MEASUREMENTS:TEMP. ° C_SALINCUiiJUCl OMHOS/f,,, /fe/0

PH 7.3H20 IE /EL B/4

ri !'UhCEEMU PJfWEH,?0 LEV- I A.TER.iiAi'.ii'Lc Vi.Vit

FIELD 'SU.13. r^lVlKuNMI.-NIVU PRUTLIUI TON AUENLY, hfGluN VI

ENVIRONMENTAL .-lilW [ LTiS O i V . '-'_-_. n.iNSTUN KD. I .AN^S C I T Y , KG 6/, l l !

: Si i:t- Njune: DLJRuNT L. A:'ir.f [ 1 L: Location: Cf :r-i,'iNi.:Hb 1,',

Si to Ni nl ib or: X".'bi U.- l.odi.-: r,.' ,i

Collected: YFv; 86 i - IU: // . D a y : / /- Ti me: . CU'.,,R",

i1ed:i ..> • -.- 1 r ,;. ; •;• ...n • • -.DUGT , r-:U-.;:.V, IT

Sample Split (ciic'e

r- -nip L c: iiedi ..:• • v i r c. : •;• oil • ' : -—. _SOIL, DUST, r-:U-.;:.V, IT., : >bi.; 1 r:L, 11 . (wV. I LR)

: Sample Lent ru ner : 1 ;-,q L c. 1 , , : RrU .^,/: val i. vt- :

VIAL: .J'.'o; ,'.iMBi;:R: bOoz Mi-iLiER: 1 LITER POLY: 1 LITER ROLY : WHITE: 1 LITER ROLY : YELLOW

: LI ML: PURPLE-:: ULUL: W H I T E ;

fU -~</\' va tV -1 -

l--t,:d .-

4tCOOL 4CCOOL 4CCOOL 4C

> ci

t.-^f^ POL- * TAM

Depth:. . A//4.. .... Ran W:

Gamp I r.;. :

PL-S'I 1TOT METALSTOT MERCURYNITRATE

qi.'.ot = : _ A' n_

-"• L--:•:>•. ; ;. |-j I; i -in :

;fY£

DATE/TIME,WELL #__ERA # .1

Tr./j H20 LEVEL B/4_

//"6-«/vTBEGIN PURGE

'.if.LEVEL AFTER V/>

SAMPLEs ,

F!ELb"MEAS"UP,£M£NTS:' TEMP. « C ^ •A. SALIM v_____A--»

CONDUCT'PH

ES/NO.FILTERED YES/NO A ^PRESERVED YES/NO^ A'-VOLUME PURGED yv-,*

FHl.D SHEETU.S. ENVIRONMENTAL PROTECTION AGuNC.'Y, PEG I UN VII

8ER'-:in.:/-; DIv. 25 FHNGTON IxJ. KANSAS CITY, KS 66115

: Site Name: DUFOMi LANDI ILL.: Location: CAMANCHE IA

te Numb or: X 7Site Code: n/a

Collected: YR: 86 MO: _//... Da- : /^ Ti rna: /3j5£ Leader: J. CLEARY :

Sample Number: JO'.'X7005 BMO

'-.-a.mp.i. ••:•> I '!•..•( j i a (c i r c 1 :? r>r. . • : • ; • :sun... DUG r, RH.H.Y-, ic. s i : ! ' i : ! i i ; _ ! : ! ,

I. 7) Sf:: 1 i <- (C i ;: c.i i, •• ,

11 o ContairiC'i- : T.\c L, 1 or : Pi •••• /at ivK : Anal ysi s Requc-s t(

40ml VIALfJOaj AMBEiS

1 ...; TEZR PCLY1 L i:T.:-< PJLY1 L i T J x POLY

?:cpth:_ _/X*_.

Sampl er 3: _ __

L I ML;-'URFL.!::.BL.L'[-

YG.:..,L ..•'.<:

COOL 40COOL 4CCOOL 4CCOOL 4CUOCL 4CCOC'L 4C

VGASEMI-VOLPESTICIDESTOT METALSTUT MERCURYNITRATE

i quots:_

01- F lE ' .D PEr\SL)NNELDATE/TIME **/n- /*(; --•Qe}4-$~ FIELD MEASUOtENTS:" ~ -—— -WELL * AVW-.r TEMP.'C___^

V.VCZA/O aH20 LEVELBEUiWEND

FILTERED YEPRESERVEDVOLUME

FIELD SHEETU.I?. LNVIRUNMI/NIVW. rROTKiJl IOM AUENCY, REGION VII

ENVIRONMENTAL :-L!-.V I (Ji-/., D J V . ,'S rilNSTHM Rl>. KAN^HS C I T Y , K'J

:: Si !-(..- Nj.mc: L'l ip._iN i ! ,'V-IOr f i I.: Lo;_ =it. 1 on : u; .Mr ,N(._! IL J i-'i

i to Mu.iibcpr: X7Si L_- i..-c.dt--: n .-',

: -::cii locted: YR: f;6 i-iU: //. D a y : / ^ T ime : /33C? Leader: J. CLEAR',

:: -• .?..iip I c hod i ...-. • •_. i i - •_ ; •_• r.,: SOIL, DUST, Rll'-JS, : ! t-.,

• :• :;.,Li; I r i L . ' i I ,

I e Sp L i t . •„ c i r • r 1 e ':::» " • : - > : > E'.-

L'orito.i -:-,--:-r : ") aq L,rjli.:r : Fv c • ~<j\ vat i.

1iiI

.•o: MMBI:!-':

LITER POLYLITER POLYLITER POLY

?oLY

Depth: A/ A

Sampler:,:

: LlrlL

iJLOEU! I.[ TEWH.I FEYELHiW

Pan tf:

.'J..JL

COOLCUOLCOOL£/<*£.1^ ro

4C4L4C^C4C

Re--|t'.:-v-, t o

'-'Or,SEMIPE5TJ.T1S..'ESTOT METALSTOT MERCURY-MI IRATE

OF

[.'•:• i p!;r :JH :

'^ re 8.f(r,

e, f-

DATE/TIME "/Z-/8i, - (T9vr FIELD MEA3UPEMEOTS:WELL * /?i*J-S~_____ T£^P. ° C

SALifJ -

7.0 H20 LZVEL B/4BEGIN PUi?GEEND PURGEH20 LEVFL AFTERSAMPLt TIME.

I M|-!--Fi",

:'.''.;.. :;:;•!','iR-' T | . uill IE! IT.Ml. ^ruvi

FIELDi i -m, L I-RI. i'i:j rn-N AL,! . -MC:Y, RC-OILM vii.;-• ' ' ' , ' , 2';. F M!T-;TMN (•!:;•. KAN- IAS C I T Y , i-:s 6.->:i i ; ';

: : 'C'!LI !.., N:"|[ ri LLocation: Ufii IA MiJ IE I,,

Sit:? N u m b e r : X 7S i t e / Code: n / _

C o l l e c t e d : Y R : 8 : , i l j : ; / / L V , y : / / T i ;

E, a (n p 1;:/ IM. j IT: b (-•:• i - ; J •'..' '-;• x. / 0'. J c

3 a i f: p 1 e M:.-.- d.:. 3. ( c :i r c I ;.::SOIL, DUST, RINLATL, SED .1 i' '!E -I / ,

Sample Sf/ l i t (c i r c 1-:/ r...-,--/; v^'i

l-.eacjor: J . CLEAR','

SHO

0 1 1 -MI.R =

£ .ample? Ccntain^r : Tag Color : R;- ive : Analysis Requested

40ml VIAL8002 AMBER80o:: AM'dER1 LITER PQLY1 LITER POLYi LITER POLY1 Liirr- PCL.^

Gampl ers: __

LIMEPURPLEBLUEWHITEI'JHIILYELLOW

T.ArJ

Pan ti=:

COOL. 4CCOOL 4CCOGL 4CCOQL 4CLOLL 4CCOOL 4C

TO

VGASEMI-VOLPESTICIDESTOT METALSTOT MERCURYNITRATE

Al i quots : __

COMMENT:-:, CF FIELI..- PERSONNEL

: £ i t •.-;• Dt:-u ::r i. ::)t i 01.:

7.0 .

fH — J

DATE/TI.-.KWELL •>

.-;u, e /A 52 /g Q'l£,EL JK

BEGIN ,'L'K.A

!)/0 LCV'.L >'

FIELD MEASUREMENTS:TEMP. °C__ /£..

CONDUCTPH 'FILTEfiED

. CC ' _

. /

FIEL.O 3HLE.TLI.?:. EMV[R:'MI1kLMTi",l F ' l v J T & L ' l TON AivCNCY, K t . O l i j i V •:. 1

E.Nv'j.:--!.jNiiii::N-rAi.. HU--; [LLS P ' v. :;:':. r i ' l i - j r j ' -J RL>. LAM:AS C T T Y , i- :.; :..'_.

Si re Mam-; DUPUNY L . r 'NO i - r, . 1 . .Los jtior,: L-riMfiMCI !L 1 . i

Si ts Nvmbor: X7Si to Code: n.' =

Collected: YR: 86 MC: _//.... Day:_//_. Time: J ML Leader: J. CLEARY

Sample Number:: JO'?X7007F ShO #:

Sample Media (circle on •.;•:•:SOIL, DUET, RINSiVTl-:, GEDIfiL-M 1 ,

Siifi.pl e '3 p. Lit . ( c i r - r ].;::• oi-,t: > : .'LS

UT i

: Sample Container :

: 40ml VIAL: 80oz AMBER: &0c= AMBER: 1 LITER POLY: 1 LITER POLY: 1 LL'TER POLYi .', -*

" t L*i~-fs~ ^o^~Y: -1-

: Depth: /^A

-, Samplnrz:

1 an Col or :

L I MEPURPLEBLUEWHITE',-iH I T EYELLOW

1 A, .1

"

Pan #:

/vA

fv t.'servati v-e: :

COOL 4CCOOL 4CCOOL 4CCOOL. 4CCOOL. 4CCOOL 4C

McsC H TC (>U 7- J

CCCi- t-f>C-

/v4 Al

Anslvsis R^LlS,t,d :

VGA :SEMI-VOL i:PESTICIDES :TOT METALS :TOT MERCURY :NITRATE ••

L quots : .... /y L ...._. :

;

=:i IT s OF F:LL;::' RURSOiJMEL

:.-! i. O - i. Mn :.

DATE/TIMEWELL r

HfiJ/'JVA JZ___H20 L tvEL C/4BEGIN

FIELD MEASUREf.'ENTS:TEMP. c C A/ASALIK *.CONDUCTPH

"A

END PL^GE. A.-AHXO LEVEL AFfERSAMPLE HMi.

fiLTEREi) YEPRESERVED,VOLO:.;E PLACED

At__Ysis TYPE: TOTAL METALS < .ACTOR)

TITLE: DUPONTLAB: CHEMTECHSAMPLE PREP:__. ANALYST/ENTRY: E4o

J09X7001

MATRIX: WAT,METHOD: 90REVIEWER: _


COMPOUNDALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUMCALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKEL.POTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINC.CYANIDE

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

48000.60.010.0

2305.00

18.0220000.

11015,096.0

52000.22.0

110000.1200.

0.21003500.

5.0010.0

12000.10.0N/A

120140

N/A

UU

U

M

U

MUU

UI

I

44000.60.010.0

9802.00

38.0230000.14082,0140100000.

31.099000.8700,0.2

21017000.

5.0010.0

31000.10.0N/A

140230

N/A

5500. .,U 370- .. ...U 500

550M 20.0

60.028000. ...15091020011000.40.08100.2200.

U 1.302900..

M 3200.U 5.00U 80.0

3400000.U 10.0I N/A

1600.380

I N/A

f

u

uM

U

UM*

MUU

UI

I

36000*60*018.07402.0025.0210000

18013014044000.29.0

100000. ..13000.

0.237010000.

3.8010.0360000

10.0N/A

160150

N/A

U

M

*

U

MU*

UI

I

At_t_Ysis TYPE: TOTAL METALS < NTRACTOR)TITLE: DUPONTLAB: CHEMTECHSAMPLE PREP:_. ANALYST/ENTRY: E4o

J09X7005

MATRIX: UAMETHOD: 90REVIEWER:


COMPOUNDALUMINUMANTIMONYARSENICBARIUMBERYLLIUMCADMIUM ....CALCIUMCHROMIUMCOBALTCOPPERIRONLEADMAGNESIUMMANGANESEMERCURYNICKEL:POTASSIUMSELENIUMSILVERSODIUMTHALLIUMTINVANADIUMZINCCYANIDE

SAMPLE NUMBERS :-.

J09X7005D J09X7006 J09X7007F

29000.19014081010.040.0

200000.15090.0120

57000'• 26_P

100000.4300.^0*2320

11000.5.0040,0

950000.10.0N/A

25(T540

N/A

U

MU

MM

U

MUU

UI

I

28000.19081.070010.040.0

220000.13070.0110

53PJXXKXTL60V99000.4400.0.2

28014000.

5.0040.0

820000.10.0N/A

200430

N/A

U

MU

MM

U

MUU

UI

M

I

36000. .','60 0 ..10.04102,0026.0290000.96.041.012062000.28.0110000.3200.0.2

1506800.4.3010.0

92000.10.0N/A

140190

N/A

1: . /. 200U . 60.0M .. 10.0

200M 5.00 .

... . v 5.00 ...5000.10.0

M 50.025.064.05.00

5000.- . "... 15.0U 0.2

40.0 .5000.

M 5.00U 10.0

5000.U 10.0I N/A

• . 50.020.0

I N/A

UUUUUUUUUUMUUUU

UUUUUUI

UUI

ANALYSIS TYPE: VOLATILE ANALYSESTITLE: L.TOTDZ FARM CDUPONT)LAB: PACIFIC ANALYTICALSAMPLE PREP: ____ ANALYST/ENTRY:

MATRIX:METHOD:

WATER>M01

E94UNITS: UG/LCASE: 6562DATE: 12/31/86

COMPOUND

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACETONECARBON DISULFIDE1,1 DICHLOROETHENEi»i DICHLOROETHANETRANS-1»2»-DICHLOROETHENECHLOROFORM1»2»DICHLOROETHANE2-BUTANONE1»1»1 TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBROMODICHLOROMETHANEIfl,2t2,-TETRACHLOROETHANE1»2-DICHLOROPROPANETRANS-1»3-DICHLOROPROPENETRICHLOROETHENEDIBROMOCHLOROMETHANE1f1f 2-TRICHLOROETHANEBENZENECIS-li3-DICHLOROPROPENE2-CHLOROETHYL VINYL ETHERBROMOFORM2-HEXANONE4-METHYL-2-PENTANONETETRACHLOROETHENETOLUENECHLOROBENZENEETHYL BENZENESTYRENETOTAL XYLENES

J09X7001

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

10,010.010,010.025.015.05.005.005.005.005.005.00

10,05.005.00

10.05.005.005.005.005.005.005.005.005.00

10.05.00

10.010.0

5.005.005.005.005.005.00

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

10.010.010.00.7

19.021.0

5,005.005.005.005.005.00

10.05.005.00

10.05.005.005.005.005.005.005.003.205.00

10.05.00

10,010.0

5.005.00

10,05,005.005.00

UUUM

UUUUUUUUUUUUUUUUUUUMUUUUUUU

UUU

2502502502509105803600.130130130130130380130130250130130130130130130130130130250130250250130130130130130130

UUUUUU

ifUUUUUUU

. UUUUUUUUUUUUUUUUUUUU

10.010.010.010.0

8.7021.0

5.000.65.005.005.005.00

10.05.005.00

10.05.005.005.005.005.005.005.00

11.05.00

10.05.00

10.010.0

5.005.005.005.305.00

24.0

UUUUUUUM

UUUUUUUUUUUUUUU

UUUUUUUU

U

AtffiLYSis TYPE: VOLATILE ANALY^STITLE: L.TOTDZ FARM (DUPONT)LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E94

MATRIX: WATERMETHOD: 93 2 01REVIEWER:


COMPOUND

CHLOROMETHANEBROMOMETHANEVINYL CHLORIDECHLOROETHANEMETHYLENE CHLORIDEACETONECARBON DISULFIDE1.1 DICHLOROETHENE1.1 DICHLOROETHANETRANS-l»2i-DICHLOROETHENECHLOROFORM1,2>DICHLORQETHANE2-BUTANONEl i l f l TRICHLOROETHANECARBON TETRACHLORIDEVINYL ACETATEBRQMODICHLOROMETHANE1»1 » 2.2i-TETRACHLOROETHANE1 > 2-DICHLOROPROPANETRANS-lf3-DICHLOROPROPENETRICHLORQETHENEDIBROMOCHLOROMETHANE1, 1»2-TRICHLQROETHANEBENZENECIS-1,3-DICHLOROPROPENE2-CHLOROETHYL VINYL ETHERBROMOFORM2-HEXANONE4-METHYL-2-PENTANONETETRACHLOROETHENETOLUENECHLOROBENZENEETHYL BENZENESTYRENETOTAL XYLENES

SAMPLE NUMBERS

J09X7005 J09X7005D J09X7006 J09X7007F

1001001001002201100.1600."~~50. 0'50,050,050.050.021050.050,010050.050,050.050.050.050.050.05.0050.010050.010010050.0

1700.50.04.5050.050.0

UUuuuu

"~uuuuuuuuuuuuuuuuMuuuuuuuMuu

1001001001003507101100.50.650.050.050,050.014050,050.010050.050.050,050,050.050.050.050.050,010050.010010050.01100.50.050.050.050.0

UUUUUU_ _Uuuuuuuuuuuuuuuuuuuuuuuuuuu

10.010.010.010,011,026.05,000,55.005.005.005,0013.05.005.0010.05.005.005.005.005.005.005.005.005.0010.05.0010.010.05.005.005.005.005.005.00

UUUUUuuM

UUUUUUUuuuuuuuuuuuuuuuuuuuu

10.010.010.010.045^01200,75.005.005.005.005.007.705.005.0010.05.005.005.005.005.005.005.005.005.0010.05,0010.010*05.001.405.005.005.005.00

UUUU

MUUUUUMUUUUUUUUUUuuuuuuuMUUUu

TYPE: SEMIVOLATILES i>TITLE: L.TOTDZ FARM (DUPONT)LAB: PACIFIC ANALYTICALSAMPLE PREP: ____ ANALYST/ENTRY: E?S

COMPOUNDJ09X7001

MATRIX:METHOD:REVIEWER

UATE\R UNITS: UG/LCASE: 6562DATE: 12/31/86

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

PHENOLBIS(2-CHLOROETHYL) ETHER2-CHLOROPHENOL1.3 DICHLOROBENZENE1.4 DICHLOROBENZENEBENZYL ALCOHOL1,2 DICHLOROBENZENE2-METHYLPHENOLBIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2»4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHOXY) METHANE2,4 DICHLOROPHENOL1,2,4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLQRO-3-METHYLPHENOL2-METHYLNAFHTHALENEHEXACHLOROCYCLOPENTADIENE2,4,6-TRICHLOROPHENOL2,4,5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINEACENAPHTHENE2,4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2,4-DINITROTOLUENE

20.020.020.020.020.020.020.020.020 .020,020,020.020.020.020.020.010020.020.020.020.020.020.020.020.020.020.010020.010020.020.010020.050.0

20.020.0

UUUUUULJUUUUUUUUUUUUUUUUUUUUUUUUUUUUI

UU

20.0

20.020.0

20.0

20.0

20.020.020.020.0

20.0

20.020.020.020.0

20.020.0

20.010020.020.010020.0

20.020.0

IUI

UUI

UI

UI

UUUUIII

UI

UUUUI

UUII

UUUUUUII

UU

13040.040.040,040.040.040.040.040.010040.040.040.040.040.040.096.040.040.040.040.040.040.040.040.040.040.020040.020040.040.020040.050.0

•40.040.0

JUUUUUUUUJUUUUUUMUUUUUUUUUUUUUUUUUUI

UU

10.010.010.010.010.010,010.010.010.010.010.010.010.010.010.010.050,010.010.010.010.010.010.010.010.010.010.050.010.050.010.010.050.010.050.0

10.010.0


UU

ANALYSIS TYPE: SEMIYOLATILES (PAGE 2>TITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E96

MATRIX: WATERMETHOD: 93Q/2MAREVIEWER:

COMPOUND

2r6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHERFLUORENE4-NITROANILINE4,6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3»3' DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS<2-ETHYLHEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENE>INDENO(1»2»3-CD)PYRENEDIBENZO(AiH)ANTHRACENEBENZQ(G»H»I)PERYLENE

J09X7001


SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

20.020.020.020.010010020.020.020.010020.020.020.020.020.020.040.020.020.020.020.020.020.020.020.020.020.0


20.020.020.020.0100

20.020.020.0

20.020.020,020.020.020.040.020.022020.022.020.020.020.020.020.020.0

UUUUUI

UUUI

UUUUUUUUUUUUUUUUU

40.040.040.040.0200.20040.040.040.020040.040.040*040.040.040.080.040.040.040.040.040.040.040.040.040.040.0


10.010.010.010.050.050.010.010.010,050.010.010.010.010.010.010.020.010.019010.010.010.010.010.010.010.010.0


ANALYSIS TYPE: SEMIVOLATILES TP~AGE DTITLE: L.TOTDZ FARM (DUPONT)LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY E95

MATRIX:METHOD:REVIEWER:

WATER

J09X7005COMPOUND

PHENOLBIS<2-CHLOROETHYL> ETHER2-CHLOROPHENOL1»3 DICHLOROBENZENEIt A DICHLOROBENZENEBENZYL ALCOHOL1»2 DICHLOROBENZENE2-METHYLPHENOLBIS(2-CHLOROISOPROPYL)ETHER4-METHYLPHENOLN-NITROSO-DIPROPYLAMINEHEXACHLOROETHANENITROBENZENEISOPHORONE2-NITROPHENOL2,4-DIMETHYLPHENOLBENZOIC ACIDBIS(2-CHLOROETHOXY> METHANE2»4 DICHLOROPHENOLl,2i4-TRICHLOROBENZENENAPHTHALENE4-CHLOROANILINEHEXACHLOROBUTADIENE4-CHLORO-3-METHYLPHENOL2-METHYLNAPHTHALENEHEXACHLOROCYCLOPENTADIENE2»4t6-TRICHLOROPHENOL2i 4»5-TRICHLOROPHENOL2-CHLORONAPHTHALENE2-NITROANILINEDIMETHYLPHTHALATEACENAPHTHYLENE3-NITROANILINEACENAPHTHENE2»4-DINITROPHENOL4-NITROPHENOLDIBENZOFURAN2»4-DINITROTOLUENE


SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

12010010010010010010014.0

100320100100100100100100770100100100100100100100 -100100100500100500100100500100500

100100

UUUUUUMU__„UUUUUU

UUUUUUUUUUUUUUUUUUI

UU

72.010.010,010.010.010.010.011.010.0

17010.010.010.010,010.02.6020.010.010.010.02.5010.010,010.010.010.010.050.010.050.010.010.050.010.050.0

10.010.0

UUUUUU

U

UUUUUMMUUUMUUUUU .UUUUUUUUUI

UU

10,010.010.010.010.010,010.010.010.010.010.010.010,010,010.010.050.010,010.010.010.010.010.010,010.010.010.050.010.050.010,010.050.010.050.0

10,010.0


UU

10.010.010.010.010.010.010.010.010.010.010.010.010.010.010.010.050,010.010.010.010.010.010.010.010.010.010.050.010.050.010.010.050.010.050.0

10.010.0

UUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUUU

' UUI

UU

ANALYSIS TYPE: SEMIYQLATILES TPAGE 2)TITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E96

MATRIX: UATERMETHOD: 930REVIEWER:


COMPOUND2»6-DINITROTOLUENEDIETHYLPHTHALATE4-CHLOROPHENYL PHENYL ETHERFLUORENE4-NITROANILINE4»6-DINITRO-2-METHYLPHENOLN-NITROSODIPHENYLAMINE4-BROMOPHENYL PHENYL ETHERHEXACHLOROBENZENEPENTACHLOROPHENOLPHENANTHRENEANTHRACENEDI-N-BUTYLPHTHALATEFLUORANTHENEPYRENEBUTYL BENZYL PHTHALATE3.3' DICHLOROBENZIDINEBENZO(A)ANTHRACENEBIS(2-ETHYLHEXYL)PHTHALATECHRYSENEDI-N-OCTYL PHTHALATEBENZO(B)FLUORANTHENEBENZO(K)FLUORANTHENEBENZO(A)PYRENEINDENO<1»2»3-CD)PYRENEDIBENZO<A»H)ANTHRACENEBENZO(G,Hi DPERYLENE

J09X7005

SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

10.010.010.010.050.050.010.010.010.050.010.010.010.010.010,010.020.010.010.010.010.010.010.010.010.010.010.0


10.010.010.010.050,050.010.010.010.013.010.010.010.010.010.010,020.010.010.010.010.010.010.010.010.010.010.0

uuuuuuuuuMuuuuuuuuuuuuuuuuu

10.010.010,010.050.050.010.010,010.050,010.010.010.010.010.010.020.010.010.010.010.010.010,010.010.010.010.0


10.01.20

10.010.050.050.010.010.010.050,010.010.00.7

10.010.010.020.010.0

10010. 010.010.010.010,010.010.010.0

uMuuuuuuuuuu

MuuuuuMuuuuuuuu

ANALYSIS TYPE: PESTICIDESTITLE: L.TOTDZ FARM <DUPONT>LAB: PACIFIC ANALYTICALSAMPLE PREP:——_ ANALYST/ENTRY: E97

MATRIX: WATERMETHOD: &302M01REVIEWER!;

COMPOUND

ALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHCHEPTACHLORALDRINHEPTACHLOR EPOXIDEENDOSULFAN IDIELDRIN4»4'-DDEENDRINENDOSULFAN II4»4'-DDDENDRIN ALDEHYDEENDOSULFAN SULFATE4f4'-DDTENDRIN KETONEMETHOXYCHLORCHLORDANETOXAPHENEAROCLOR-1016AROCLOR-1221AROCLOR-1232AROCLOR-1242AROCLOR-1248AROCLOR-1254AROCLOR-1260

J09X7001

4-UNITS: UG/LCASE: 6562DATE: 12/31/86

SAMPLE NUMBERS

J09X7002 J09X7003 J09X7004

0.10.10.10.10.10.10.10.10.20.20.20.20.20.20.20.20.21.001,002,001.001.001.001.001.002.002.00

UUUUUUUUUUUUUUUUU

UUUUUUUUUU

0.050.050.050.050.050.050.050.050.10.10.10.10.10.10.10.10.10.50.51.000,50.50.50.50.51.001.00

UUUUUUUUUUUUUUUUUUU

UUUUUU

UU

5.005.005.005.000.050.050.050,050,10.10.10.10.10.10.10.10.10,5 .0.51.000.50.50*50,50,51.001,00

UUUU

UUUUU

4 uUUUUUUUU

; uUuuuuu

uu

0.050.050.050,050.050.050.050.050,10.10.10.10.10.10.10.10.10.50.51,000,50.50.50.50.51,001.00

Uuuuuuuuuuuuuuuuuuu

uuuuuu

uu

ANALYSIS TYPE: PESTICIDESTITLE: L.TOTDZ FARM <BUPONT>LABt PACIFIC ANALYTICALSAMPLE PREP:____ ANALYST/ENTRY: E97

MATRIX: WATERMETHOD: 930REVIEWER: _


COMPOUNDALPHA-BHCBETA-BHCDELTA-BHCGAMMA-BHCHEPTACHLORALDRINHEPTACHLOR EPOXIDEENDOSULFAN IDIELDRIN4»4'-DDEENDRINENDOSULFAN II4»4'-DDDENDRIN ALDEHYDEENDOSULFAN SULFATE4,4'-DDTENDRIN KETONEMETHOXYCHLORCHLORDANETOXAPHENEAROCLOR-1016AROCLOR-1221AROCLOR-1232AROCLOR-1242AROCLOR-1248AROCLOR-1254AROCLOR-1260

J09X7005

SAMPLE NUMBERS

J09X7005D J09X7006 J09X7007F

5.005.005.005.000.050.050.050.050.10.10.10.10.10.10.10.10.10,50.51.000.50.50.50.50.55.601.00

UUUU

UUUUUUUUUUUUUUU

UUUUUU

JU

5.005.005.005.000.050.050.050.050,10.10.10.10.10.10,10.10,10,50.51.000,50.50.50.50.55.601.00

UUUU

UUUUUUUUUUUUUUU

UUUUUU

J^U

0.050.050.050.050,050.050.050.050.10.10.10.10.10.10.10.10.10.50.51.000.50.50.50.50.51.001.00

UUUUUUUUUUUU

^ U, U

UUUUU

UU

; UUUU

UU

0.050.050.050.050.050.050.050.050.10.10,10.10.10.10.10.10.10.50.51.000.50.50.50.50.51.001.00

UUUUUUUUUUUUUUUUUUU

UUUUUU

UU

TITLE: L.TOTDZ FARM(DUPONT)MATRIX: WATERLAB: PACIFIC ANALYTICAL METHOD: 93O2M01ANALYST/ENTRY: LT REVIEWER: KIRCHM



SAMPLE NO.

JO9X7OO1JO9X7001J09X7001J09X7001J09X7001J09X7O01J09X7OO2JO9X7003JO9X7003J09X7003J09X7003J09X7003J09X7003JO9X7003J09X7O03

J09X70O3JO9X70O4JO9X7O04J09X7O04J09X70O4

J09X70O4J09X7004JO9X7005J09X7005JO9X7005J09X7005J09X7O05J09X7005J09X7005J09X7005J09X7002JO9X7004J09X7004J09X7005J09X7005J09X7005

COMPOUND NAME** FRACTION

NOTHING SIGNIFICANT FOUND VOA2,5,8,11,14-PENTAOXAHEXADECAN-16-OL BNA2,2-(2-METHOXYETHOXY)ETHOXY-ETHANOL BNA2,5,8,11,14-PENTAOXYPENTADECANE BNA2-ETHOXY-l-METHOXYETHOXY)-ETHENE BNA5-METHYL-l,4-HEXADIENE BNANOTHING SIGNIFICANT FOUND VOANOTHING SIGNIFICANT FOUND VOA1,3,5,7,9-PENTATHIECANE BNA1,2,4-TRITHIOLANE BNA1,2,4,6-TETRATHIEPANE BNA1,3,5,7-TETRATHIOCANE BNABENZENEACETIC ACID BNA1,3,5-TRITHIANE BNA1-CYCLOHEXEN-l-OL, 2,6-DIMETHYL-ACETATE BNATETRADECANOIC ACID BNATETRAHYDROFURAN J PA2,2(2-METHOXYETHOXY)ETHOXY ETHANOL BNA2,5,8,11,14-PENTAOXAPENTADECAN-16-OLBNABENZOIC ACID,3,5-BIS(1,1-DIMETHYL-ETHYD4-HY BNAHEXADECANOIC ACID BNA1,4-DIMETHYL BENZENE BNA2-PROPANETHIOL VOA1,2,4-TRITHIOLANE BNA1,2,4,6-TETRATHIEPANE BNA1,3!,5,7-TETRATHIOCANE BNABENZENEPROPANOIC ACID BNABENZENEACETIC ACID BNA2,5-DIMETHYL-BENZENEBUTANOIC ACID BNA2-METHYL-PENTANOIC ACID BNA2 UNKNOWN COMPOUNDS BNA4 UNKNOWN HYDROCARBONS BNA3 UNKNOWN COMPOUNDS BNA& UNKNOWN COMPOUNDS VOA1 UNKNOWN HYDROCARBON BNA4 UNKNOWN COMPOUNDS BNA

Vtoft-

EST.

216212602420

70564O4B29521112994

472328

_19586484 """132

16 -102O50

2120124012801120540320340

20-45646-35212-216160-17060

200420-3440

CONC.*

JJJJJ

JJJJJJ

JJJJJ

JJJJJJJJJJJJJJ

JJJ


**The compounds were identified using a library search routine.Authentic standards have not been analyzed to veri-fy compound massspectra and retention times.

TITLE: L.TDTDZ FARM(DUPDNT)MATRIX: WATERLAB: PACIFIC ANALYTICAL METHOD: 93O2MO1ANALYST/ENTRY: LT REVIEWEFK.iKIRCHMER

SAMPLE NO.

_J09X7005P_JO9X7005DJ09X7005DJ09X7005DJO9X7005DJ09X70O5D

JO9X7O05DJ09X7005DJ09X7005DJO9X7O05DJ09X7005DJ09X70O5DJ09X7006JO9X7006J09X7006JO9X7007FJ09X70O7FJ09X7007FJ09X7007FJ09X7O05DJ09X7005DJO9X7OO6JO9X70O7



COMPOUND NAME**

JETRAHYDROFJJRAN____—_.________1,2,4-TRITHIOLANE1,3,5-TRITHIANE1,2,4,6-TETRATHIEPANEBENZENEACETIC ACID3-CYCLOHEXENE-l-METHANOL,ALPHA,ALPHA4-TR1,3,5,7-TETRATHIOCANEHEXANOIC ACID3-METHYL PENTANOIC ACID1,3,5-TRITHIANE2,5-DIMETHYL-BENZENEBUTANOIC ACIDPENTAND1C ACIDNOTHING SIGNIFICANT FOUND2-2(2-METHOXYETHOXY)ETHOXYETHANOL2,5,8,11,14-PENTAOXYHEXADECAN-16-OLTRICHLOROFLUOROMETHANEHEXANEDIOIC ACID, DIOCTYL ESTER2 HEPTENAL (Z)-2-CYCLOHEX ENE-1-ONE7 UNKNOWN COMPOUNDS1 UNKNOWN HYDROCARBON1 UNKNOWN HYDROCARBON1 UNKNOWN HYDROCARBON

FRACTION EST.CONC.*

VOASNABNABNABNA

iBNAVOABNABNABNABNABNAVOABNABNAVOABNABNABNABNABNABNABNA

IG5BSL.802710690490

39O338298296220172160

30305

4002814

22-572303660

J -JJJJ

JJJJJ

- JJ

JJJJJJJJJJ

#This is a crude estimation based on response relative to aninternal standard. An authentic standard has not been run.

**The compounds were identified using a library search routine.Authentic standards have not been analyzed to verify compound massspectra and retention times.

TITLE: DUPDNTLAB: CHEMTECHANALYST/ENTRY: LT

MATRIX: WATERMETHOD: SEE * BELOWREVIEWER: GCS

UNITS: MG/LCASE: SAS2564G

12-11-86

T-

SAMPLE NO.

J09X7001JO9X7002

J09X7003JO9X7004J09X7005JO9X7005DJ09X7006J09X7007F

CHLORIDE

12.019.0

66025927017026.03.0

SULFATE

53.911.9

17.710039.93211717.3

NITRATE

5.050.02U

0.02U

0.02UO.O2U0.02U330.02U

SULFIDE

l.OU1 . OU

169

l.OU2.93.31 . OU1 . OU

ALKALINITYf- '262642

BB30

7402250228O

1 . 184-j 6.0

« METHOD'NDS. ;

CHLORIDE - 3251W03SULFATE - 3751W03NITRATE - 3531W02SULFIDE - 3761WO1

ALKALINITY - 3101W01

Case No.: 6562 Laboratory : Chemtech

Contract No.: SOW 785 Method No.: 9001M07

SMO No-.: MGD050-MGD058 Activity No.: J09X7



1. Analysis was requested for the contract inorganic totalmetals fraction only.

2. Iron was reported in the field blank sample, J09X7007F/MGD056. Sample results were all greater than five times theblank level for iron, therefore no qualifications were made basedon the blank rules.

3. Antimony exceeded MES recovery control limits, but above30%. Since no positive responses were recorded in the samplesfor antimony, no qualifications were made on the sample data forantimony.

4. A performance evaluation audit was introduced as sampleJ09X7008P/MGD057. All metals were correctly identified althoughiron was quantitated at 2.5 times the spiked concentration.

Case No.: SAS 2564G•

Contract No.: NA

SMO No.: MGD050-058

Laboratory : Chemtech

Method Nos.: 3251W03, 3751W03,3531W02, 3761W01, 3101W01

Activity No.: J09X7



1. Analyses were requested for chloride, sulfate, nitrate,sulfide and total alkalinity. The audit sample, MGD057, was notrequested to be analyzed for sulfide.

2. Initial and continuing calibrations and calibrationverification solution analyses along with blank, duplicate andmatrix spike results were all satisfactory.

3. The field blank sample, J09X7007F/MGD056, was reported tohave insignificant amounts of chloride and total alkalinitycompared with sample results. This field blank did have sulfatereported at the concentration level of the performance evaluationaudit (J09X7008P/MG0057) true value. Since sulfate was reportedas a non-detect in the audit for sulfate, and sulfate, chlorideand alkalinity are analyzed from the same sample container, andchloride and alkalinity audit results are acceptable, it appearsthe laboratory has switched the field blank and audit samples forsulfate analysis. The data were not qualified by the blank rulesbecause of the high probability of a sample mixup. All otheraudit sample parameters were correctly identified.

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