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Underground Storage Tank Closure Report Myersville BP/Crown 9486 Myersville Road Myersville, MD 21773

AEC Project Number: 06-170 MDE Case No. : 90-1304FR

MDE Facility ID Number: 1139

Prepared for:

Maryland Department of the Environment Attn: Rob Hill

Oil Control Program 1800 Washington Boulevard, Suite 620

Baltimore, Maryland 21230-1719

And

Ali Kazemzadeh AKJK, LLC

2035 Chesapeake Road Annapolis, MD 21409

Prepared by:

Advantage Environmental Consultants, LLC

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794

January 27, 2015

8610 Washington Blvd Suite 217 Jessup, MD 20794 Phone: 301.776.0500 Fax: 301.776.1123

January 27, 2015 Mr. Rob Hill Maryland Department of the Environment Oil Control Program, Remediation Division 1800 Washington Boulevard, Suite 620 Baltimore, Maryland 21230-1719 Re: Underground Storage Tank Closure

Myersville BP/Crown 9486 Myersville Road Myersville, MD 21773 AEC Project Number: 06-170 MDE Case No. : 90-1304FR MDE Facility ID Number: 1139 Dear Mr. Hill: Advantage Environmental Consultants, LLC (AEC) is pleased to submit our underground storage tank (UST) closure report to the Maryland Department of the Environment (MDE) on behalf of AKJK, LLC for environmental services performed at the above referenced property (i.e., the Site). AEC was contracted by AKJK to perform environmental oversight for the removal of three 8,000-gallon and one 6,000-gallon USTs located at the Site. As directed by the MDE, AEC collected soil samples from the UST tank field, below the product piping, and below each dispenser. The UST system removal activities were conducted between December 15 and December 18, 2014. Based on the absence of liquid phase hydrocarbons, laboratory analytical results of soil samples collected from the UST tank field, below product piping, and below dispensers and the removal of approximately 327 tons of impacted materials, AEC concludes that limited residual petroleum contamination exists in these areas of the Site. The owner of the property stated that he is switching from well water to city water. After the water is switched over, it is our professional opinion that the identified subsurface impact does not currently pose a human health exposure or environmental risk (i.e. lack of Potable wells and other exposure pathways). Therefore, AEC respectfully requests that the MDE close Case No. 90-1304FR. If you have any questions regarding information in this report or if we can be of further assistance, please contact AEC at (301) 776-0500.

8610 Washington Blvd Suite 217 Jessup, MD 20794 Phone: 301.776.0500 Fax: 301.776.1123

Sincerely, Advantage Environmental Consultants, LLC Nathan Edwards Michael J. Robertson, P.G. Staff Scientist Principal CC: Mr. Ali Kazemzadeh, AKJK, LLC

TABLE OF CONTENTS

1.0 INTRODUCTION .................................................................................................. 1

1.1 Project Introduction and Scope .................................................................. 1

1.2 Site Location and Topography ................................................................... 1

2.0 UST REMOVAL ACTIVITIES ............................................................................... 2

3.0 SOIL SAMPLING RESULTS ................................................................................ 3

4.0 CONCLUSIONS AND RECOMMENDATIONS .................................................... 6

APPENDICES APPENDIX A - FIGURES FIGURE 1: SITE VICINITY MAP FIGURE 2: SITE PLAN FIGURE 3: SAMPLE LOCATION MAP FIGURE 4: DISPENSER AND TANK FIELD LINE SOIL QUALITY MAP FIGURE 5: TANK PIT SOIL QUALITY MAP APPENDIX B - TANK CLEANING AND DISPOSAL MANIFEST APPENDIX C - PHOTO LOG APPENDIX D - SOIL MANIFEST APPENDIX E - MDE TANK REMOVAL/ABANDONMENT DIRECTIVE APPENDIX F - LABORATORY ANALYTICAL RESULTS AND CHAIN-OF-CUSTODY DOCUMENTATION

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 1

1.0 INTRODUCTION 1.1 Project Introduction and Scope AEC was contracted by AKJK, LLC to perform excavation oversight for the removal of three 8,000-gallon and one 6,000-gallon underground storage tanks (USTs) located at 9486 Myersville Road, Myersville, MD 21773 (herein after referred to as the “Site”). The USTs were located on the southern portion of the Site. Mr. Rob Hill of the Maryland Department of the Environment (MDE) was present to inspect portions of the UST system removal and to issue the Tank Removal/Abandonment directive. As directed by the MDE, AEC collected twenty soil samples from the sidewalls and bottom of the tank field, two samples from beneath the product piping, and one sample from beneath each dispenser. 1.2 Site Location and Topography The Site is located at 9486 Myersville Road, Myersville, Maryland. Based on the USGS Middletown, MD 7.5 Minute Series Topographic Quadrangle dated 2014, the Site is located approximately 600 feet above mean sea level (msl). The Site vicinity has a steep topographic gradient towards the west in the direction of Grindstone Run, which is located approximately 750 feet west of the Site. A Site Vicinity Map is included as Figure 1 in Appendix A. A Site Plan depicting the Site features and the UST excavation location is included as Figure 2 in Appendix A. The Site is located in a commercial area of Myersville, Maryland. The Site is bordered to the south and west by Cat construction equipment lot; to the east by Myersville Road; and, to the North by Milt Summers Road. Across the road to the north is a vacant field. Across the road to the east is a standalone Middletown Valley bank.

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 2

2.0 UST REMOVAL ACTIVITIES

AKJK, LLC contracted AEC to perform UST excavation oversight for the removal of three 8,000-gallon and one 6,000-gallon USTs. According to the facility summary MDE documentation, the USTs were 25 years old. Service Station Repair Inc. conducted the removal activities and began removal on December 15, 2014 by first excavating concrete and pea gravel overlying the USTs. A photoionization detector (PID) was used to scan the soils and pea gravel for volatile organic compounds (VOCs) in the UST excavation area. Pea gravel taken from 0-5 feet below ground surface (bgs) exhibited no elevated PID readings. Strong odors and elevated PID reading were noted from pea gravel and soil from 5-15 feet bgs. PID readings for soils beneath the USTs ranged from 0.0 to a maximum of 1,500 parts per million (ppm). Soils that exhibited PID readings or odor were stockpiled on and covered with poly sheeting to await disposal at an approved facility. The excavated, petroleum impacted soil was taken to Clean Earth in Hagerstown, Maryland. Approximately 327 tons of impacted materials were removed from the Site. Groundwater was encountered in the UST excavation at approximately thirteen-feet bgs. Photographs of the UST removal activities are included as Appendix C. The USTs were emptied prior to removal activities of all residual petroleum. A copy of the water and product disposal manifest is included in Appendix B. The USTs were removed from the excavation and inspected for perforations and cracks. All tanks were in good condition with no perforations or cracks observed. The UST disposal forms are included in Appendix B. AEC noted that the top of existing monitoring well 2 (EMW-2) casing was broken by the removal activities. Service Station Repair will sand down the broken casing, making a functional monitoring well. For future groundwater sampling events, AEC will need to resurvey the top of the monitoring well casings. As directed by the MDE, AEC collected twenty soil samples (five from Tank 1, five from Tank 2, five from Tank 3, and five from Tank 4) from the excavation sidewalls approximately eleven-feet bgs, and two-feet below each tank (approximately 16-feet bgs). In addition, two soil samples were collected below the product piping and one sample was collected from below each dispenser. A map depicting soil sample locations within the UST system excavation is included as Figure 3 in Appendix A.

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 3

3.0 SAMPLING RESULTS The soil samples collected on December 18, 2014 were immediately placed on ice and hand-delivered under chain-of-custody to Maryland Spectral Services of Baltimore, Maryland for laboratory analyses. All soil samples were analyzed for the following: Total Petroleum Hydrocarbons (TPH) Gasoline Range Organics (GRO) and Diesel Range Organics (DRO) via EPA Analytical Method 8015B and VOCs via EPA Analytical Method 8260. The results of the laboratory analysis are summarized in the table below:

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 4

Table 1 Soil Sample Laboratory Results Myersville BP/ Crown Samples collected 12/18/2014

Sample B T E X MTBE Naphthalene

TPH GRO

TPH DRO (Date)

Sample 1 BDL BDL BDL 10.8 J BDL 25.5 0.59 31.0

Sample 2 BDL BDL BDL BDL BDL BDL 0.25 17.8

Sample 3 BDL BDL BDL 7.1 J BDL 15.1 9.04 40.0

Sample 4 BDL BDL BDL BDL BDL 19.8 3.49 213

Sample 5 BDL BDL BDL BDL BDL 24.0 19.8 370

Sample 6 BDL BDL BDL BDL BDL BDL 81.9 1140

Sample 7 32.9 38.3 50.5 652 14.1 J 298 10.5 60.8

Sample 8 BDL BDL 17.9 J 115 BDL 459 19.2 72.9

Sample 9 BDL BDL BDL BDL BDL BDL 26.0 98.3

Sample 10 BDL 4.9 J 10.1 32.5 BDL 60.4 13.4 149

Sample 11 BDL 5.4 J 14.4 26.8 5.1 J 66.8 15.6 169

Sample 12 BDL BDL 44.2 48.4 J BDL 157 25.6 202

Sample 13 BDL BDL BDL BDL BDL BDL BDL BDL

Sample 14 BDL BDL BDL BDL BDL BDL BDL 22.1

Sample 15 BDL BDL BDL 7.2 J BDL 4.5 J 0.35 21.9

Sample 16 BDL BDL BDL BDL BDL BDL BDL BDL

Sample 17 BDL BDL BDL BDL BDL BDL BDL BDL

Sample 18 BDL BDL BDL 11.3 J BDL 23.1 0.21 12.1

Sample 19 BDL BDL BDL BDL BDL BDL BDL 19.5

Sample 20 BDL BDL BDL BDL BDL BDL BDL 11.1

Sample 21 BDL BDL BDL BDL BDL BDL BDL BDL

Sample 22 BDL BDL BDL BDL BDL BDL BDL 17.8

Sample 23 BDL BDL BDL BDL BDL BDL BDL BDL

Sample 24 BDL BDL BDL BDL BDL BDL BDL 38.7

MEAT Non- Residential Cleanup

52,000 8,200,000 10,000,000 20,000,000 720,000 2,000,000 620 620

BTEX= Benzene, Toluene, Ethylbenzene, total Xylenes TPH-GRO = Total Petroleum Hydrocarbons Gasoline Range Organics TPH-DRO = Total Petroleum Hydrocarbons Diesel Range Organics TPH-DRO and GRO results are in parts per million or mg/Kg VOC results are in parts per billion or µg/Kg J= Detected but below the reporting limit; therefore, result is an estimated concentration (CLP J-Flag) BDL = Below Detection Limits MTBE = methyl-tertiary butyl-ether MDE Standards (Maryland Environmental Assessment Technology (MEAT) for Leaking Underground Storage Tanks, Revised February 2003)

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 5

Based on the laboratory analytical results, several petroleum constituents were detected in soil samples collected from the bottom of the tank field, beneath the dispensers, and beneath the product piping. Laboratory analytical results for sample 6 indicate levels of TPH DRO above the MDE Maryland Environmental Assessment Technology (MEAT) Leaking Underground Storage Tank standards. All other detected analytes were below MDE MEAT Leaking underground storage tank standards (regulatory standards). Laboratory analytical results for Sample 1, Sample 2, Sample 3, Sample 4, Sample 5, Sample 6, Sample 7, Sample 8, Sample 9, Sample 10, Sample 11, Sample 12, Sample 13, Sample 14, Sample 15, Sample 18, Sample 19, Sample 20, Sample 22 and Sample 24 indicate analytes above laboratory detection limits, but below regulatory standards. Laboratory analytical results for Sample 16, Sample 17, Sample 21 and Sample 23 indicate that all analytes were below laboratory detection limits (BDL).

Myersville BP/ Crown –Myersville, MD January 27, 2015 AEC Project No.: 06-170 Page 6

4.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the absence of liquid phase hydrocarbons, laboratory analytical results for samples collected from the UST excavation, below the product piping and dispensers and the removal of approximately 327 tons of impacted materials, AEC concludes that limited residual petroleum contamination exists in these areas of the Site. The owner of the AKJK, LLC stated that they are switching this property from well water to city water. After the water is switched over, it is our professional opinion that the identified subsurface impact does not currently pose a human health exposure or environmental risk (i.e. lack of Potable wells and other exposure pathways). Therefore, AEC respectfully requests that the MDE close Case No. 90-1304FR.

APPENDIX A

FIGURES

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794

Phone: 301-776-0500 Fax: 301-776-1123

Figure 1 – Site Vicinity Map

9486 Myersville Road

Myersville, MD 21773

January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

North

SITE

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794 Phone: 301-776-0500 Fax: 301-776-1123 January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

N Legend = Site Location Figure 2 – Site Plan

9486 Myersville Road

Myersville, MD 21773

Store

Canopy

USTs

50 Feet

Milt Summers Road

= Excavation Location

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794 Phone: 301-776-0500 Fax: 301-776-1123 January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

N Legend = Site Location Figure 3a – Sample Location Map

9486 Myersville Road

Myersville, MD 21773

= Sample Location

Store

Canopy

USTs

50 Feet

Milt Summers Road

Sample 2

Sample 6

Sample 1

Sample 5

Sample 4

Sample 3

Sample 8

Sample 12

Sample 7

Sample 11

Sample 10

Sample 9

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794 Phone: 301-776-0500 Fax: 301-776-1123 January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

N Legend = Site Location Figure 3b – Sample Location Map

9486 Myersville Road

Myersville, MD 21773

Store

50 Feet

Milt Summers Road

= Sample Location

= Sidewall Sample Location

Sample 20

Sample 19

Sample 14

Sample 13

Sample 17

Sample 18

Sample 16

Sample 15

Sample 21

Sample 24

Sample 22

Sample 23

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794 Phone: 301-776-0500 Fax: 301-776-1123 January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

N Legend = Site Location Figure 4a – Dispenser and Tank

Field Soil Quality Map

9486 Myersville Road

Myersville, MD 21773

Store

Canopy

50 Feet

Milt Summers Road - TPH DRO = Total Petroleum Hydrocarbons

Diesel Range Organics

- TPH GRO = Total Petroleum Hydrocarbons

Gasoline Range Organics

- Bold values exceed MDE Standards

(Maryland Environmental Assessment

Technology (MEAT) for Leaking Underground

Storage Tanks, Revised February 2003)

- J = Laboratory estimated value

Sample 1

Total Xylenes – 10.8 J µg/kg

Naphthalene – 25.5 µg/kg

TPH GRO -- 0.59 mg/kg

TPH DRO - - 31.0 mg/kg

Sample 12

Ethylbenzene – 44.2 µg/kg

Total Xylenes – 48.4 J µg/kg

Naphthalene – 157 µg/kg

TPH GRO -- 25.6 mg/kg

TPH DRO -- 202 mg/kg

Sample 11

Toluene – 5.4 J µg/kg

Ethylbenzene – 14.4 µg/kg

Total Xylenes – 26.8 µg/kg

MTBE - 5.1 J µg/kg

Naphthalene – 66.8 µg/kg

TPH GRO -- 15.6 mg/kg

TPH DRO -- 169 mg/kg

Sample 10

Toluene – 4.9 J µg/kg

Ethylbenzene – 10.1 µg/kg

Total Xylenes – 32.5 µg/kg

Naphthalene – 60.4 µg/kg

TPH GRO -- 13.4 mg/kg

TPH DRO -- 149 mg/kg

Sample 7

Benzene - 32.9 µg/kg

Toluene – 38.3 µg/kg

Ethylbenzene – 50.5 µg/kg

Total Xylenes – 652 µg/kg

MTBE - 14.1 J µg/kg

Naphthalene – 298 µg/kg

TPH GRO -- 10.5 mg/kg

TPH DRO -- 60.8 mg/kg

Sample 6

TPH GRO -- 81.9 mg/kg

TPH DRO -- 1140 mg/kg

Sample 5

Naphthalene – 24.0 µg/kg

TPH GRO -- 19.8 mg/kg

TPH DRO -- 370 mg/kg

Sample 4

Naphthalene – 19.8 µg/kg

TPH GRO -- 3.49 mg/kg

TPH DRO -- 213 mg/kg

Sample 3

Total Xylenes – 7.1 J µg/kg

Naphthalene – 15.1 µg/kg

TPH GRO -- 9.04 mg/kg

TPH DRO -- 40.0 mg/kg

Sample 2

TPH GRO -- 0.25 mg/kg

TPH DRO -- 17.8 mg/kg

Sample 9

TPH GRO -- 26.0 mg/kg

TPH DRO -- 98.3 mg/kg

Sample 8

Ethylbenzene – 17.9 J µg/kg

Total Xylenes – 115 µg/kg

Naphthalene – 459 µg/kg

TPH GRO -- 19.2 mg/kg

TPH DRO -- 72.9 mg/kg

8610 Washington Boulevard, Suite 217 Jessup, Maryland 20794 Phone: 301-776-0500 Fax: 301-776-1123 January 2015

AEC Project No.: Report Date: Drawn By:

06-170 NAE

N Legend = Site Location Figure 4b – Dispenser and Tank

Field Soil Quality Map

9486 Myersville Road

Myersville, MD 21773

Store

50 Feet

Milt Summers Road

= Sample Location

= Sidewall Sample Location

Sample 13

All analytes BDL

Sample 17

All analytes BDL

Sample 16

All analytes BDL

Sample 1

All analytes BDL

Sample 3

All analytes BDL

Sample 4

TPH DRO -- 38.7 mg/kg

Sample 2

TPH DRO -- 17.8 mg/kg

Sample 20

TPH DRO -- 11.1 mg/kg

Sample 19

TPH DRO -- 19.5 mg/kg

Sample 18

Total Xylenes – 11.3 J µg/kg

Naphthalene – 23.1 µg/kg

TPH GRO -- 0.21 mg/kg

TPH DRO -- 12.1 mg/kg

Sample 15

Total Xylenes – 7.2 J µg/kg

Naphthalene – 4.5 J µg/kg

TPH GRO -- 0.35 mg/kg

TPH DRO -- 21.9 mg/kg

Sample 14

TPH DRO -- 22.1 mg/kg

APPENDIX B

TANK CLEANING AND DISPOSAL MANIFEST

APPENDIX C

PHOTO LOG

Photograph 2: Product line removal

Photograph 1: UST removal activities

Photograph 3: Removed Tank

Photograph 4: Removed Tank

Photograph 5: Removed Tanks

Photograph 6: Piping and disperser removal

Photograph 7: Broken well casing on EMW-1

Photograph 8: Excavation Site

APPENDIX D

SOIL MANIFESTS

APPENDIX E

MDE TANK REMOVAL/ABANDONMENT DIRECTIVE

APPENDIX F

LABORATORY ANALYTICAL RESULTS AND CHAIN-OF-CUSTODY DOCUMENTATION

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

VELAP ID 460040

Advantage Environmental Consultants, LLC

RE: MYERSVILLE CROWN

Jessup, MD 20794

8610 Baltimore Washington Blvd, Suite 217

Michael Robertson

Will Brewington

Staff Chemist

Enclosed are the results of analyses for samples received by the laboratory on 12/18/14 16:30.

Maryland Spectral Services, Inc. is a National Environmental Laboratory Accreditation Program (NELAP)

accredited laboratory. Certification status for analytes included in this report will be provided upon request.

Please visit our website at www.mdspectral.com for a complete listing of our NELAP accreditations.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

29 December 2014

Page 1 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

Client Sample ID Laboratory ID Matrix Date Sampled Date ReceivedAlternate Sample ID

TANK PIT 1 4121820-01 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 2 4121820-02 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 3 4121820-03 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 4 4121820-04 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 5 4121820-05 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 6 4121820-06 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 7 4121820-07 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 8 4121820-08 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 9 4121820-09 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 10 4121820-10 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 11 4121820-11 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT 12 4121820-12 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT N1 4121820-13 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT N2 4121820-14 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT E1 4121820-15 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT E2 4121820-16 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT S1 4121820-17 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT S2 4121820-18 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT W1 4121820-19 12/18/14 00:00 12/18/14 16:30Soil

TANK PIT W2 4121820-20 12/18/14 00:00 12/18/14 16:30Soil

CANOPY 1 4121820-21 12/18/14 00:00 12/18/14 16:30Soil

CANOPY 2 4121820-22 12/18/14 00:00 12/18/14 16:30Soil

CANOPY 3 4121820-23 12/18/14 00:00 12/18/14 16:30Soil

CANOPY 4 4121820-24 12/18/14 00:00 12/18/14 16:30Soil

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 2 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 1

4121820-01 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 13:17Acetone 11.5ug/kg dry 1 WB11.5

73.6 12/19/14 12/19/14 13:17tert-Amyl alcohol (TAA) 57.5ug/kg dry 1 WB57.5

ND 12/19/14 12/19/14 13:17tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Benzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Bromobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Bromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Bromodichloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Bromoform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Bromomethane 5.7ug/kg dry 1 WB5.7

96.1 12/19/14 12/19/14 13:17tert-Butanol (TBA) 57.5ug/kg dry 1 WB57.5

ND 12/19/14 12/19/14 13:172-Butanone (MEK) 11.5ug/kg dry 1 WB11.5

3.0 12/19/14 12/19/14 13:17n-Butylbenzene 5.7J ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17sec-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17tert-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Carbon disulfide 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Carbon tetrachloride 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Chlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Chloroethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 13:17Chloroform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Chloromethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 13:172-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:174-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Dibromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2-Dibromoethane (EDB) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Dibromomethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,3-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,4-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Dichlorodifluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1-Dichloroethene 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 3 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 1

4121820-01 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 13:17cis-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17trans-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Dichlorofluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,3-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:172,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17cis-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17trans-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Diisopropyl ether (DIPE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Ethylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Hexachlorobutadiene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:172-Hexanone 11.5ug/kg dry 1 WB11.5

ND 12/19/14 12/19/14 13:17Isopropylbenzene (Cumene) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:174-Isopropyltoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:174-Methyl-2-pentanone 11.5ug/kg dry 1 WB11.5

ND 12/19/14 12/19/14 13:17Methylene chloride 11.5ug/kg dry 1 WB11.5

25.5 12/19/14 12/19/14 13:17Naphthalene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17n-Propylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Styrene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Tetrachloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Toluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2,3-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2,4-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1,1-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,1,2-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Trichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:171,2,3-Trichloropropane 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 4 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 1

4121820-01 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

48.1 12/19/14 12/19/14 13:171,2,4-Trimethylbenzene 5.7ug/kg dry 1 WB2.3

24.6 12/19/14 12/19/14 13:171,3,5-Trimethylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:17Vinyl chloride 5.7ug/kg dry 1 WB2.3

5.7 12/19/14 12/19/14 13:17o-Xylene 5.7J ug/kg dry 1 WB2.3

5.1 12/19/14 12/19/14 13:17m- & p-Xylenes 5.7J ug/kg dry 1 WB2.3

12/19/14 12/19/14 13:1780-120 108 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 13:1781-117 97 %Surrogate: Toluene-d8

12/19/14 12/19/14 13:1774-121 93 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

0.59 12/22/14 12/22/14 11:35Gasoline-Range Organics 0.11mg/kg dry 1 ECM0.11

12/22/14 12/22/14 11:3585-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

31.0 12/18/14 12/20/14 06:12Diesel-Range Organics 9.2mg/kg dry 1 CMK9.2

12/18/14 12/20/14 06:1270-130 108 %Surrogate: o-Terphenyl

PERCENT SOLIDS

87 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 5 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 2

4121820-02 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 13:50Acetone 11.6ug/kg dry 1 WB11.6

ND 12/19/14 12/19/14 13:50tert-Amyl alcohol (TAA) 58.1ug/kg dry 1 WB58.1

ND 12/19/14 12/19/14 13:50tert-Amyl methyl ether (TAME) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Benzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Bromobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Bromochloromethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Bromodichloromethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Bromoform 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Bromomethane 5.8ug/kg dry 1 WB5.8

ND 12/19/14 12/19/14 13:50tert-Butanol (TBA) 58.1ug/kg dry 1 WB58.1

ND 12/19/14 12/19/14 13:502-Butanone (MEK) 11.6ug/kg dry 1 WB11.6

ND 12/19/14 12/19/14 13:50n-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50sec-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50tert-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Carbon disulfide 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Carbon tetrachloride 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Chlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Chloroethane 5.8ug/kg dry 1 WB5.8

ND 12/19/14 12/19/14 13:50Chloroform 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Chloromethane 5.8ug/kg dry 1 WB5.8

ND 12/19/14 12/19/14 13:502-Chlorotoluene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:504-Chlorotoluene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2-Dibromo-3-chloropropane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Dibromochloromethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2-Dibromoethane (EDB) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Dibromomethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,3-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,4-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Dichlorodifluoromethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1-Dichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2-Dichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1-Dichloroethene 5.8ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 6 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 2

4121820-02 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 13:50cis-1,2-Dichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50trans-1,2-Dichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Dichlorofluoromethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,3-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:502,2-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50cis-1,3-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50trans-1,3-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Diisopropyl ether (DIPE) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Ethyl tert-butyl ether (ETBE) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Ethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Hexachlorobutadiene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:502-Hexanone 11.6ug/kg dry 1 WB11.6

ND 12/19/14 12/19/14 13:50Isopropylbenzene (Cumene) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:504-Isopropyltoluene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Methyl tert-butyl ether (MTBE) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:504-Methyl-2-pentanone 11.6ug/kg dry 1 WB11.6

ND 12/19/14 12/19/14 13:50Methylene chloride 11.6ug/kg dry 1 WB11.6

ND 12/19/14 12/19/14 13:50Naphthalene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50n-Propylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Styrene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1,1,2-Tetrachloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1,2,2-Tetrachloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Tetrachloroethene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Toluene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2,3-Trichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2,4-Trichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1,1-Trichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,1,2-Trichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Trichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Trichlorofluoromethane (Freon 11) 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,2,3-Trichloropropane 5.8ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 7 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 2

4121820-02 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 13:501,2,4-Trimethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:501,3,5-Trimethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50Vinyl chloride 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50o-Xylene 5.8ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 13:50m- & p-Xylenes 5.8ug/kg dry 1 WB2.3

12/19/14 12/19/14 13:5080-120 107 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 13:5081-117 99 %Surrogate: Toluene-d8

12/19/14 12/19/14 13:5074-121 93 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

0.25 12/22/14 12/22/14 12:11Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/22/14 12/22/14 12:1185-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

17.8 12/18/14 12/20/14 06:39Diesel-Range Organics 9.3mg/kg dry 1 CMK9.3

12/18/14 12/20/14 06:3970-130 100 %Surrogate: o-Terphenyl

PERCENT SOLIDS

86 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 8 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 3

4121820-03 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 14:24Acetone 11.8ug/kg dry 1 WB11.8

109 12/19/14 12/19/14 14:24tert-Amyl alcohol (TAA) 58.8ug/kg dry 1 WB58.8

ND 12/19/14 12/19/14 14:24tert-Amyl methyl ether (TAME) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Benzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Bromobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Bromochloromethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Bromodichloromethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Bromoform 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Bromomethane 5.9ug/kg dry 1 WB5.9

288 12/19/14 12/19/14 14:24tert-Butanol (TBA) 58.8ug/kg dry 1 WB58.8

ND 12/19/14 12/19/14 14:242-Butanone (MEK) 11.8ug/kg dry 1 WB11.8

49.6 12/19/14 12/19/14 14:24n-Butylbenzene 5.9ug/kg dry 1 WB2.4

54.6 12/19/14 12/19/14 14:24sec-Butylbenzene 5.9ug/kg dry 1 WB2.4

4.0 12/19/14 12/19/14 14:24tert-Butylbenzene 5.9J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Carbon disulfide 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Carbon tetrachloride 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Chlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Chloroethane 5.9ug/kg dry 1 WB5.9

ND 12/19/14 12/19/14 14:24Chloroform 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Chloromethane 5.9ug/kg dry 1 WB5.9

ND 12/19/14 12/19/14 14:242-Chlorotoluene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:244-Chlorotoluene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2-Dibromo-3-chloropropane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Dibromochloromethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2-Dibromoethane (EDB) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Dibromomethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,3-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,4-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Dichlorodifluoromethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1-Dichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2-Dichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1-Dichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24cis-1,2-Dichloroethene 5.9ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 9 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 3

4121820-03 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 14:24trans-1,2-Dichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Dichlorofluoromethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,3-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:242,2-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24cis-1,3-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24trans-1,3-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Diisopropyl ether (DIPE) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Ethyl tert-butyl ether (ETBE) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Ethylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Hexachlorobutadiene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:242-Hexanone 11.8ug/kg dry 1 WB11.8

ND 12/19/14 12/19/14 14:24Isopropylbenzene (Cumene) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:244-Isopropyltoluene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Methyl tert-butyl ether (MTBE) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:244-Methyl-2-pentanone 11.8ug/kg dry 1 WB11.8

ND 12/19/14 12/19/14 14:24Methylene chloride 11.8ug/kg dry 1 WB11.8

15.1 12/19/14 12/19/14 14:24Naphthalene 5.9ug/kg dry 1 WB2.4

4.5 12/19/14 12/19/14 14:24n-Propylbenzene 5.9J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Styrene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1,1,2-Tetrachloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1,2,2-Tetrachloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Tetrachloroethene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Toluene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2,3-Trichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2,4-Trichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1,1-Trichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,1,2-Trichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Trichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Trichlorofluoromethane (Freon 11) 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:241,2,3-Trichloropropane 5.9ug/kg dry 1 WB2.4

12.6 12/19/14 12/19/14 14:241,2,4-Trimethylbenzene 5.9ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 10 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 3

4121820-03 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

6.1 12/19/14 12/19/14 14:241,3,5-Trimethylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 14:24Vinyl chloride 5.9ug/kg dry 1 WB2.4

3.0 12/19/14 12/19/14 14:24o-Xylene 5.9J ug/kg dry 1 WB2.4

4.1 12/19/14 12/19/14 14:24m- & p-Xylenes 5.9J ug/kg dry 1 WB2.4

12/19/14 12/19/14 14:2480-120 87 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 14:2481-117 106 %Surrogate: Toluene-d8

12/19/14 12/19/14 14:2474-121 113 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

9.04 12/22/14 12/22/14 13:26Gasoline-Range Organics 0.59mg/kg dry 5 ECM0.59

12/22/14 12/22/14 13:2685-115 107 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

40.0 12/18/14 12/20/14 07:06Diesel-Range Organics 9.4mg/kg dry 1 CMK9.4

12/18/14 12/20/14 07:0670-130 91 %Surrogate: o-Terphenyl

PERCENT SOLIDS

85 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 11 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 4

4121820-04 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 14:57Acetone 11.4ug/kg dry 1 WB11.4

121 12/19/14 12/19/14 14:57tert-Amyl alcohol (TAA) 56.8ug/kg dry 1 WB56.8

ND 12/19/14 12/19/14 14:57tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Benzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Bromobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Bromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Bromodichloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Bromoform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Bromomethane 5.7ug/kg dry 1 WB5.7

242 12/19/14 12/19/14 14:57tert-Butanol (TBA) 56.8ug/kg dry 1 WB56.8

ND 12/19/14 12/19/14 14:572-Butanone (MEK) 11.4ug/kg dry 1 WB11.4

27.2 12/19/14 12/19/14 14:57n-Butylbenzene 5.7ug/kg dry 1 WB2.3

18.4 12/19/14 12/19/14 14:57sec-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57tert-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Carbon disulfide 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Carbon tetrachloride 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Chlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Chloroethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 14:57Chloroform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Chloromethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 14:572-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:574-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Dibromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2-Dibromoethane (EDB) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Dibromomethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,3-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,4-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Dichlorodifluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1-Dichloroethene 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 12 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 4

4121820-04 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 14:57cis-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57trans-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Dichlorofluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,3-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:572,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57cis-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57trans-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Diisopropyl ether (DIPE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Ethylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Hexachlorobutadiene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:572-Hexanone 11.4ug/kg dry 1 WB11.4

ND 12/19/14 12/19/14 14:57Isopropylbenzene (Cumene) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:574-Isopropyltoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:574-Methyl-2-pentanone 11.4ug/kg dry 1 WB11.4

ND 12/19/14 12/19/14 14:57Methylene chloride 11.4ug/kg dry 1 WB11.4

19.8 12/19/14 12/19/14 14:57Naphthalene 5.7ug/kg dry 1 WB2.3

4.5 12/19/14 12/19/14 14:57n-Propylbenzene 5.7J ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Styrene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Tetrachloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Toluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2,3-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2,4-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1,1-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,1,2-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Trichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:571,2,3-Trichloropropane 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 13 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 4

4121820-04 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

7.8 12/19/14 12/19/14 14:571,2,4-Trimethylbenzene 5.7ug/kg dry 1 WB2.3

3.9 12/19/14 12/19/14 14:571,3,5-Trimethylbenzene 5.7J ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57Vinyl chloride 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57o-Xylene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 14:57m- & p-Xylenes 5.7ug/kg dry 1 WB2.3

12/19/14 12/19/14 14:5780-120 92 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 14:5781-117 102 %Surrogate: Toluene-d8

12/19/14 12/19/14 14:5774-121 101 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

3.49 12/22/14 12/22/14 14:03Gasoline-Range Organics 0.57mg/kg dry 5 ECM0.57

12/22/14 12/22/14 14:0385-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

213 12/18/14 12/20/14 07:33Diesel-Range Organics 18.2mg/kg dry 2 CMK18.2

12/18/14 12/20/14 07:3370-130 95 %Surrogate: o-Terphenyl

PERCENT SOLIDS

88 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 14 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 5

4121820-05 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

25.5 12/19/14 12/19/14 15:30Acetone 12.2ug/kg dry 1 WB12.2

209 12/19/14 12/19/14 15:30tert-Amyl alcohol (TAA) 61.0ug/kg dry 1 WB61.0

ND 12/19/14 12/19/14 15:30tert-Amyl methyl ether (TAME) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Benzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Bromobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Bromochloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Bromodichloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Bromoform 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Bromomethane 6.1ug/kg dry 1 WB6.1

302 12/19/14 12/19/14 15:30tert-Butanol (TBA) 61.0ug/kg dry 1 WB61.0

ND 12/19/14 12/19/14 15:302-Butanone (MEK) 12.2ug/kg dry 1 WB12.2

96.0 12/19/14 12/19/14 15:30n-Butylbenzene 6.1ug/kg dry 1 WB2.4

61.3 12/19/14 12/19/14 15:30sec-Butylbenzene 6.1ug/kg dry 1 WB2.4

2.6 12/19/14 12/19/14 15:30tert-Butylbenzene 6.1J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Carbon disulfide 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Carbon tetrachloride 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Chlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Chloroethane 6.1ug/kg dry 1 WB6.1

ND 12/19/14 12/19/14 15:30Chloroform 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Chloromethane 6.1ug/kg dry 1 WB6.1

ND 12/19/14 12/19/14 15:302-Chlorotoluene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:304-Chlorotoluene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2-Dibromo-3-chloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Dibromochloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2-Dibromoethane (EDB) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Dibromomethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,3-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,4-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Dichlorodifluoromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1-Dichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2-Dichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1-Dichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30cis-1,2-Dichloroethene 6.1ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 15 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 5

4121820-05 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 15:30trans-1,2-Dichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Dichlorofluoromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,3-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:302,2-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30cis-1,3-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30trans-1,3-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Diisopropyl ether (DIPE) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Ethyl tert-butyl ether (ETBE) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Ethylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Hexachlorobutadiene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:302-Hexanone 12.2ug/kg dry 1 WB12.2

ND 12/19/14 12/19/14 15:30Isopropylbenzene (Cumene) 6.1ug/kg dry 1 WB2.4

4.7 12/19/14 12/19/14 15:304-Isopropyltoluene 6.1J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Methyl tert-butyl ether (MTBE) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:304-Methyl-2-pentanone 12.2ug/kg dry 1 WB12.2

ND 12/19/14 12/19/14 15:30Methylene chloride 12.2ug/kg dry 1 WB12.2

24.0 12/19/14 12/19/14 15:30Naphthalene 6.1ug/kg dry 1 WB2.4

7.3 12/19/14 12/19/14 15:30n-Propylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Styrene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1,1,2-Tetrachloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1,2,2-Tetrachloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Tetrachloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Toluene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2,3-Trichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2,4-Trichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1,1-Trichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,1,2-Trichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Trichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30Trichlorofluoromethane (Freon 11) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:301,2,3-Trichloropropane 6.1ug/kg dry 1 WB2.4

7.5 12/19/14 12/19/14 15:301,2,4-Trimethylbenzene 6.1ug/kg dry 1 WB2.4

4.5 12/19/14 12/19/14 15:301,3,5-Trimethylbenzene 6.1J ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 16 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 5

4121820-05 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 15:30Vinyl chloride 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30o-Xylene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 15:30m- & p-Xylenes 6.1ug/kg dry 1 WB2.4

12/19/14 12/19/14 15:3080-120 86 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 15:3081-117 105 %Surrogate: Toluene-d8

12/19/14 12/19/14 15:3074-121 106 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

19.8 12/22/14 12/22/14 21:21Gasoline-Range Organics 0.61mg/kg dry 5 ECM0.61

12/22/14 12/22/14 21:21 S-0785-115 120 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

370 12/18/14 12/20/14 08:01Diesel-Range Organics 29.3mg/kg dry 3 CMK29.3

12/18/14 12/20/14 08:0170-130 119 %Surrogate: o-Terphenyl

PERCENT SOLIDS

82 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 17 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 6

4121820-06 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/26/14 12/26/14 20:33Acetone 1600ug/kg dry 125 ECM1600

ND 12/26/14 12/26/14 20:33tert-Amyl alcohol (TAA) 8010ug/kg dry 125 ECM8010

ND 12/26/14 12/26/14 20:33tert-Amyl methyl ether (TAME) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Benzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Bromobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Bromochloromethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Bromodichloromethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Bromoform 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Bromomethane 801ug/kg dry 125 ECM801

ND 12/26/14 12/26/14 20:33tert-Butanol (TBA) 8010ug/kg dry 125 ECM8010

ND 12/26/14 12/26/14 20:332-Butanone (MEK) 1600ug/kg dry 125 ECM1600

ND 12/26/14 12/26/14 20:33n-Butylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33sec-Butylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33tert-Butylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Carbon disulfide 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Carbon tetrachloride 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Chlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Chloroethane 801ug/kg dry 125 ECM801

ND 12/26/14 12/26/14 20:33Chloroform 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Chloromethane 801ug/kg dry 125 ECM801

ND 12/26/14 12/26/14 20:332-Chlorotoluene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:334-Chlorotoluene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2-Dibromo-3-chloropropane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Dibromochloromethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2-Dibromoethane (EDB) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Dibromomethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2-Dichlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,3-Dichlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,4-Dichlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Dichlorodifluoromethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1-Dichloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2-Dichloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1-Dichloroethene 801ug/kg dry 125 ECM321

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 18 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 6

4121820-06 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/26/14 12/26/14 20:33cis-1,2-Dichloroethene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33trans-1,2-Dichloroethene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Dichlorofluoromethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2-Dichloropropane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,3-Dichloropropane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:332,2-Dichloropropane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1-Dichloropropene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33cis-1,3-Dichloropropene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33trans-1,3-Dichloropropene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Diisopropyl ether (DIPE) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Ethyl tert-butyl ether (ETBE) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Ethylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Hexachlorobutadiene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:332-Hexanone 1600ug/kg dry 125 ECM1600

ND 12/26/14 12/26/14 20:33Isopropylbenzene (Cumene) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:334-Isopropyltoluene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Methyl tert-butyl ether (MTBE) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:334-Methyl-2-pentanone 1600ug/kg dry 125 ECM1600

ND 12/26/14 12/26/14 20:33Methylene chloride 1600ug/kg dry 125 ECM1600

ND 12/26/14 12/26/14 20:33Naphthalene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33n-Propylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Styrene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1,1,2-Tetrachloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1,2,2-Tetrachloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Tetrachloroethene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Toluene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2,3-Trichlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2,4-Trichlorobenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1,1-Trichloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,1,2-Trichloroethane 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Trichloroethene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Trichlorofluoromethane (Freon 11) 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,2,3-Trichloropropane 801ug/kg dry 125 ECM321

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 19 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 6

4121820-06 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/26/14 12/26/14 20:331,2,4-Trimethylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:331,3,5-Trimethylbenzene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33Vinyl chloride 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33o-Xylene 801ug/kg dry 125 ECM321

ND 12/26/14 12/26/14 20:33m- & p-Xylenes 801ug/kg dry 125 ECM321

12/26/14 12/26/14 20:3380-120 93 %Surrogate: 1,2-Dichloroethane-d4

12/26/14 12/26/14 20:3381-117 97 %Surrogate: Toluene-d8

12/26/14 12/26/14 20:3374-121 97 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

81.9 12/24/14 12/24/14 21:18Gasoline-Range Organics 16.0mg/kg dry 125 ECM16.0

12/24/14 12/24/14 21:1885-115 96 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

1140 12/18/14 12/20/14 08:28Diesel-Range Organics 103mg/kg dry 10 CMK103

12/18/14 12/20/14 08:2870-130 115 %Surrogate: o-Terphenyl

PERCENT SOLIDS

78 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 20 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 7

4121820-07 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 18:52Acetone 61.0ug/kg dry 5 WB61.0

ND 12/22/14 12/22/14 18:52tert-Amyl alcohol (TAA) 305ug/kg dry 5 WB305

ND 12/22/14 12/22/14 18:52tert-Amyl methyl ether (TAME) 30.5ug/kg dry 5 WB12.2

32.9 12/22/14 12/22/14 18:52Benzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Bromobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Bromochloromethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Bromodichloromethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Bromoform 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Bromomethane 30.5ug/kg dry 5 WB30.5

329 12/22/14 12/22/14 18:52tert-Butanol (TBA) 305ug/kg dry 5 WB305

ND 12/22/14 12/22/14 18:522-Butanone (MEK) 61.0ug/kg dry 5 WB61.0

55.8 12/22/14 12/22/14 18:52n-Butylbenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52sec-Butylbenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52tert-Butylbenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Carbon disulfide 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Carbon tetrachloride 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Chlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Chloroethane 30.5ug/kg dry 5 WB30.5

ND 12/22/14 12/22/14 18:52Chloroform 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Chloromethane 30.5ug/kg dry 5 WB30.5

ND 12/22/14 12/22/14 18:522-Chlorotoluene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:524-Chlorotoluene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2-Dibromo-3-chloropropane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Dibromochloromethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2-Dibromoethane (EDB) 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Dibromomethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2-Dichlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,3-Dichlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,4-Dichlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Dichlorodifluoromethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1-Dichloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2-Dichloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1-Dichloroethene 30.5ug/kg dry 5 WB12.2

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 21 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 7

4121820-07 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 18:52cis-1,2-Dichloroethene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52trans-1,2-Dichloroethene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Dichlorofluoromethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2-Dichloropropane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,3-Dichloropropane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:522,2-Dichloropropane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1-Dichloropropene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52cis-1,3-Dichloropropene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52trans-1,3-Dichloropropene 30.5ug/kg dry 5 WB12.2

21.3 12/22/14 12/22/14 18:52Diisopropyl ether (DIPE) 30.5J ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Ethyl tert-butyl ether (ETBE) 30.5ug/kg dry 5 WB12.2

50.5 12/22/14 12/22/14 18:52Ethylbenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Hexachlorobutadiene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:522-Hexanone 61.0ug/kg dry 5 WB61.0

12.4 12/22/14 12/22/14 18:52Isopropylbenzene (Cumene) 30.5J ug/kg dry 5 WB12.2

16.5 12/22/14 12/22/14 18:524-Isopropyltoluene 30.5J ug/kg dry 5 WB12.2

14.1 12/22/14 12/22/14 18:52Methyl tert-butyl ether (MTBE) 30.5J ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:524-Methyl-2-pentanone 61.0ug/kg dry 5 WB61.0

ND 12/22/14 12/22/14 18:52Methylene chloride 61.0ug/kg dry 5 WB61.0

298 12/22/14 12/22/14 18:52Naphthalene 30.5ug/kg dry 5 WB12.2

27.7 12/22/14 12/22/14 18:52n-Propylbenzene 30.5J ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Styrene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1,1,2-Tetrachloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1,2,2-Tetrachloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Tetrachloroethene 30.5ug/kg dry 5 WB12.2

38.3 12/22/14 12/22/14 18:52Toluene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2,3-Trichlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2,4-Trichlorobenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1,1-Trichloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,1,2-Trichloroethane 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Trichloroethene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Trichlorofluoromethane (Freon 11) 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:521,2,3-Trichloropropane 30.5ug/kg dry 5 WB12.2

1160 12/22/14 12/22/14 18:521,2,4-Trimethylbenzene 30.5ug/kg dry 5 WB12.2

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 22 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 7

4121820-07 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

406 12/22/14 12/22/14 18:521,3,5-Trimethylbenzene 30.5ug/kg dry 5 WB12.2

ND 12/22/14 12/22/14 18:52Vinyl chloride 30.5ug/kg dry 5 WB12.2

209 12/22/14 12/22/14 18:52o-Xylene 30.5ug/kg dry 5 WB12.2

443 12/22/14 12/22/14 18:52m- & p-Xylenes 30.5ug/kg dry 5 WB12.2

12/22/14 12/22/14 18:5280-120 99 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 18:5281-117 100 %Surrogate: Toluene-d8

12/22/14 12/22/14 18:5274-121 104 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

10.5 12/22/14 12/22/14 15:16Gasoline-Range Organics 0.61mg/kg dry 5 ECM0.61

12/22/14 12/22/14 15:1685-115 111 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

60.8 12/18/14 12/20/14 08:55Diesel-Range Organics 9.8mg/kg dry 1 CMK9.8

12/18/14 12/20/14 08:5570-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS

82 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 23 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 8

4121820-08 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 19:25Acetone 57.5ug/kg dry 5 WB57.5

ND 12/22/14 12/22/14 19:25tert-Amyl alcohol (TAA) 287ug/kg dry 5 WB287

ND 12/22/14 12/22/14 19:25tert-Amyl methyl ether (TAME) 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Benzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Bromobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Bromochloromethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Bromodichloromethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Bromoform 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Bromomethane 28.7ug/kg dry 5 WB28.7

521 12/22/14 12/22/14 19:25tert-Butanol (TBA) 287ug/kg dry 5 WB287

ND 12/22/14 12/22/14 19:252-Butanone (MEK) 57.5ug/kg dry 5 WB57.5

270 12/22/14 12/22/14 19:25n-Butylbenzene 28.7ug/kg dry 5 WB11.5

93.9 12/22/14 12/22/14 19:25sec-Butylbenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25tert-Butylbenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Carbon disulfide 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Carbon tetrachloride 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Chlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Chloroethane 28.7ug/kg dry 5 WB28.7

ND 12/22/14 12/22/14 19:25Chloroform 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Chloromethane 28.7ug/kg dry 5 WB28.7

ND 12/22/14 12/22/14 19:252-Chlorotoluene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:254-Chlorotoluene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2-Dibromo-3-chloropropane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Dibromochloromethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2-Dibromoethane (EDB) 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Dibromomethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2-Dichlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,3-Dichlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,4-Dichlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Dichlorodifluoromethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1-Dichloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2-Dichloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1-Dichloroethene 28.7ug/kg dry 5 WB11.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 24 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 8

4121820-08 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 19:25cis-1,2-Dichloroethene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25trans-1,2-Dichloroethene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Dichlorofluoromethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2-Dichloropropane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,3-Dichloropropane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:252,2-Dichloropropane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1-Dichloropropene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25cis-1,3-Dichloropropene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25trans-1,3-Dichloropropene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Diisopropyl ether (DIPE) 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Ethyl tert-butyl ether (ETBE) 28.7ug/kg dry 5 WB11.5

17.9 12/22/14 12/22/14 19:25Ethylbenzene 28.7J ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Hexachlorobutadiene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:252-Hexanone 57.5ug/kg dry 5 WB57.5

27.4 12/22/14 12/22/14 19:25Isopropylbenzene (Cumene) 28.7J ug/kg dry 5 WB11.5

35.2 12/22/14 12/22/14 19:254-Isopropyltoluene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Methyl tert-butyl ether (MTBE) 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:254-Methyl-2-pentanone 57.5ug/kg dry 5 WB57.5

ND 12/22/14 12/22/14 19:25Methylene chloride 57.5ug/kg dry 5 WB57.5

459 12/22/14 12/22/14 19:25Naphthalene 28.7ug/kg dry 5 WB11.5

118 12/22/14 12/22/14 19:25n-Propylbenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Styrene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1,1,2-Tetrachloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1,2,2-Tetrachloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Tetrachloroethene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Toluene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2,3-Trichlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2,4-Trichlorobenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1,1-Trichloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,1,2-Trichloroethane 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Trichloroethene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Trichlorofluoromethane (Freon 11) 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:251,2,3-Trichloropropane 28.7ug/kg dry 5 WB11.5

912 12/22/14 12/22/14 19:251,2,4-Trimethylbenzene 28.7ug/kg dry 5 WB11.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 25 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 8

4121820-08 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

256 12/22/14 12/22/14 19:251,3,5-Trimethylbenzene 28.7ug/kg dry 5 WB11.5

ND 12/22/14 12/22/14 19:25Vinyl chloride 28.7ug/kg dry 5 WB11.5

38.1 12/22/14 12/22/14 19:25o-Xylene 28.7ug/kg dry 5 WB11.5

76.9 12/22/14 12/22/14 19:25m- & p-Xylenes 28.7ug/kg dry 5 WB11.5

12/22/14 12/22/14 19:2580-120 97 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 19:2581-117 100 %Surrogate: Toluene-d8

12/22/14 12/22/14 19:2574-121 106 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

19.2 12/23/14 12/23/14 12:24Gasoline-Range Organics 0.57mg/kg dry 5 ECM0.57

12/23/14 12/23/14 12:2485-115 113 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

72.9 12/18/14 12/20/14 09:22Diesel-Range Organics 9.2mg/kg dry 1 CMK9.2

12/18/14 12/20/14 09:2270-130 100 %Surrogate: o-Terphenyl

PERCENT SOLIDS

87 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 26 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 9

4121820-09 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/26/14 12/26/14 21:06Acetone 1440ug/kg dry 125 ECM1440

ND 12/26/14 12/26/14 21:06tert-Amyl alcohol (TAA) 7180ug/kg dry 125 ECM7180

ND 12/26/14 12/26/14 21:06tert-Amyl methyl ether (TAME) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Benzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Bromobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Bromochloromethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Bromodichloromethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Bromoform 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Bromomethane 718ug/kg dry 125 ECM718

ND 12/26/14 12/26/14 21:06tert-Butanol (TBA) 7180ug/kg dry 125 ECM7180

ND 12/26/14 12/26/14 21:062-Butanone (MEK) 1440ug/kg dry 125 ECM1440

ND 12/26/14 12/26/14 21:06n-Butylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06sec-Butylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06tert-Butylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Carbon disulfide 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Carbon tetrachloride 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Chlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Chloroethane 718ug/kg dry 125 ECM718

ND 12/26/14 12/26/14 21:06Chloroform 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Chloromethane 718ug/kg dry 125 ECM718

ND 12/26/14 12/26/14 21:062-Chlorotoluene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:064-Chlorotoluene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2-Dibromo-3-chloropropane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Dibromochloromethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2-Dibromoethane (EDB) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Dibromomethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2-Dichlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,3-Dichlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,4-Dichlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Dichlorodifluoromethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1-Dichloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2-Dichloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1-Dichloroethene 718ug/kg dry 125 ECM287

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 27 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 9

4121820-09 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/26/14 12/26/14 21:06cis-1,2-Dichloroethene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06trans-1,2-Dichloroethene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Dichlorofluoromethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2-Dichloropropane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,3-Dichloropropane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:062,2-Dichloropropane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1-Dichloropropene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06cis-1,3-Dichloropropene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06trans-1,3-Dichloropropene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Diisopropyl ether (DIPE) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Ethyl tert-butyl ether (ETBE) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Ethylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Hexachlorobutadiene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:062-Hexanone 1440ug/kg dry 125 ECM1440

ND 12/26/14 12/26/14 21:06Isopropylbenzene (Cumene) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:064-Isopropyltoluene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Methyl tert-butyl ether (MTBE) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:064-Methyl-2-pentanone 1440ug/kg dry 125 ECM1440

ND 12/26/14 12/26/14 21:06Methylene chloride 1440ug/kg dry 125 ECM1440

ND 12/26/14 12/26/14 21:06Naphthalene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06n-Propylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Styrene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1,1,2-Tetrachloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1,2,2-Tetrachloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Tetrachloroethene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Toluene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2,3-Trichlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2,4-Trichlorobenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1,1-Trichloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,1,2-Trichloroethane 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Trichloroethene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Trichlorofluoromethane (Freon 11) 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,2,3-Trichloropropane 718ug/kg dry 125 ECM287

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 28 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 9

4121820-09 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

361 12/26/14 12/26/14 21:061,2,4-Trimethylbenzene 718J ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:061,3,5-Trimethylbenzene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06Vinyl chloride 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06o-Xylene 718ug/kg dry 125 ECM287

ND 12/26/14 12/26/14 21:06m- & p-Xylenes 718ug/kg dry 125 ECM287

12/26/14 12/26/14 21:0680-120 93 %Surrogate: 1,2-Dichloroethane-d4

12/26/14 12/26/14 21:0681-117 98 %Surrogate: Toluene-d8

12/26/14 12/26/14 21:0674-121 95 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

26.0 12/24/14 12/24/14 21:56Gasoline-Range Organics 14.4mg/kg dry 125 ECM14.4

12/24/14 12/24/14 21:5685-115 94 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

98.3 12/18/14 12/20/14 09:49Diesel-Range Organics 9.2mg/kg dry 1 CMK9.2

12/18/14 12/20/14 09:4970-130 102 %Surrogate: o-Terphenyl

PERCENT SOLIDS

87 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 29 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 10

4121820-10 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

30.5 12/19/14 12/19/14 17:11Acetone 11.5ug/kg dry 1 WB11.5

215 12/19/14 12/19/14 17:11tert-Amyl alcohol (TAA) 57.5ug/kg dry 1 WB57.5

ND 12/19/14 12/19/14 17:11tert-Amyl methyl ether (TAME) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Benzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Bromobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Bromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Bromodichloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Bromoform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Bromomethane 5.7ug/kg dry 1 WB5.7

350 12/19/14 12/19/14 17:11tert-Butanol (TBA) 57.5ug/kg dry 1 WB57.5

ND 12/19/14 12/19/14 17:112-Butanone (MEK) 11.5ug/kg dry 1 WB11.5

118 12/19/14 12/19/14 17:11n-Butylbenzene 5.7ug/kg dry 1 WB2.3

58.9 12/19/14 12/19/14 17:11sec-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11tert-Butylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Carbon disulfide 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Carbon tetrachloride 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Chlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Chloroethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 17:11Chloroform 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Chloromethane 5.7ug/kg dry 1 WB5.7

ND 12/19/14 12/19/14 17:112-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:114-Chlorotoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2-Dibromo-3-chloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Dibromochloromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2-Dibromoethane (EDB) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Dibromomethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,3-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,4-Dichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Dichlorodifluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2-Dichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11cis-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 30 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 10

4121820-10 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 17:11trans-1,2-Dichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Dichlorofluoromethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,3-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:112,2-Dichloropropane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11cis-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11trans-1,3-Dichloropropene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Diisopropyl ether (DIPE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Ethyl tert-butyl ether (ETBE) 5.7ug/kg dry 1 WB2.3

10.1 12/19/14 12/19/14 17:11Ethylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Hexachlorobutadiene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:112-Hexanone 11.5ug/kg dry 1 WB11.5

16.7 12/19/14 12/19/14 17:11Isopropylbenzene (Cumene) 5.7ug/kg dry 1 WB2.3

10.7 12/19/14 12/19/14 17:114-Isopropyltoluene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Methyl tert-butyl ether (MTBE) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:114-Methyl-2-pentanone 11.5ug/kg dry 1 WB11.5

ND 12/19/14 12/19/14 17:11Methylene chloride 11.5ug/kg dry 1 WB11.5

60.4 12/19/14 12/19/14 17:11Naphthalene 5.7ug/kg dry 1 WB2.3

63.5 12/19/14 12/19/14 17:11n-Propylbenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Styrene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1,1,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1,2,2-Tetrachloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Tetrachloroethene 5.7ug/kg dry 1 WB2.3

4.9 12/19/14 12/19/14 17:11Toluene 5.7J ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2,3-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2,4-Trichlorobenzene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1,1-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,1,2-Trichloroethane 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Trichloroethene 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:11Trichlorofluoromethane (Freon 11) 5.7ug/kg dry 1 WB2.3

ND 12/19/14 12/19/14 17:111,2,3-Trichloropropane 5.7ug/kg dry 1 WB2.3

87.3 12/19/14 12/19/14 17:111,2,4-Trimethylbenzene 5.7ug/kg dry 1 WB2.3

34.3 12/19/14 12/19/14 17:111,3,5-Trimethylbenzene 5.7ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 31 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 10

4121820-10 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 17:11Vinyl chloride 5.7ug/kg dry 1 WB2.3

10.7 12/19/14 12/19/14 17:11o-Xylene 5.7ug/kg dry 1 WB2.3

21.8 12/19/14 12/19/14 17:11m- & p-Xylenes 5.7ug/kg dry 1 WB2.3

12/19/14 12/19/14 17:1180-120 109 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 17:1181-117 107 %Surrogate: Toluene-d8

12/19/14 12/19/14 17:1174-121 108 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

13.4 12/23/14 12/23/14 13:00Gasoline-Range Organics 0.57mg/kg dry 5 ECM0.57

12/23/14 12/23/14 13:0085-115 112 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

149 12/18/14 12/20/14 10:16Diesel-Range Organics 9.2mg/kg dry 1 CMK9.2

12/18/14 12/20/14 10:1670-130 102 %Surrogate: o-Terphenyl

PERCENT SOLIDS

87 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 32 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 11

4121820-11 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

33.4 12/19/14 12/19/14 17:44Acetone 12.2ug/kg dry 1 WB12.2

278 12/19/14 12/19/14 17:44tert-Amyl alcohol (TAA) 61.0ug/kg dry 1 WB61.0

ND 12/19/14 12/19/14 17:44tert-Amyl methyl ether (TAME) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Benzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Bromobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Bromochloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Bromodichloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Bromoform 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Bromomethane 6.1ug/kg dry 1 WB6.1

488 12/19/14 12/19/14 17:44tert-Butanol (TBA) 61.0ug/kg dry 1 WB61.0

ND 12/19/14 12/19/14 17:442-Butanone (MEK) 12.2ug/kg dry 1 WB12.2

97.5 12/19/14 12/19/14 17:44n-Butylbenzene 6.1ug/kg dry 1 WB2.4

49.1 12/19/14 12/19/14 17:44sec-Butylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44tert-Butylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Carbon disulfide 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Carbon tetrachloride 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Chlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Chloroethane 6.1ug/kg dry 1 WB6.1

ND 12/19/14 12/19/14 17:44Chloroform 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Chloromethane 6.1ug/kg dry 1 WB6.1

ND 12/19/14 12/19/14 17:442-Chlorotoluene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:444-Chlorotoluene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2-Dibromo-3-chloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Dibromochloromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2-Dibromoethane (EDB) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Dibromomethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,3-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,4-Dichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Dichlorodifluoromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1-Dichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2-Dichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1-Dichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44cis-1,2-Dichloroethene 6.1ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 33 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 11

4121820-11 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 17:44trans-1,2-Dichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Dichlorofluoromethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,3-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:442,2-Dichloropropane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44cis-1,3-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44trans-1,3-Dichloropropene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Diisopropyl ether (DIPE) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Ethyl tert-butyl ether (ETBE) 6.1ug/kg dry 1 WB2.4

14.4 12/19/14 12/19/14 17:44Ethylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Hexachlorobutadiene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:442-Hexanone 12.2ug/kg dry 1 WB12.2

19.0 12/19/14 12/19/14 17:44Isopropylbenzene (Cumene) 6.1ug/kg dry 1 WB2.4

10.0 12/19/14 12/19/14 17:444-Isopropyltoluene 6.1ug/kg dry 1 WB2.4

5.1 12/19/14 12/19/14 17:44Methyl tert-butyl ether (MTBE) 6.1J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:444-Methyl-2-pentanone 12.2ug/kg dry 1 WB12.2

ND 12/19/14 12/19/14 17:44Methylene chloride 12.2ug/kg dry 1 WB12.2

66.8 12/19/14 12/19/14 17:44Naphthalene 6.1ug/kg dry 1 WB2.4

66.0 12/19/14 12/19/14 17:44n-Propylbenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Styrene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1,1,2-Tetrachloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1,2,2-Tetrachloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Tetrachloroethene 6.1ug/kg dry 1 WB2.4

5.4 12/19/14 12/19/14 17:44Toluene 6.1J ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2,3-Trichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2,4-Trichlorobenzene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1,1-Trichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,1,2-Trichloroethane 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Trichloroethene 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:44Trichlorofluoromethane (Freon 11) 6.1ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 17:441,2,3-Trichloropropane 6.1ug/kg dry 1 WB2.4

56.7 12/19/14 12/19/14 17:441,2,4-Trimethylbenzene 6.1ug/kg dry 1 WB2.4

25.8 12/19/14 12/19/14 17:441,3,5-Trimethylbenzene 6.1ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 34 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 11

4121820-11 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 17:44Vinyl chloride 6.1ug/kg dry 1 WB2.4

9.2 12/19/14 12/19/14 17:44o-Xylene 6.1ug/kg dry 1 WB2.4

17.6 12/19/14 12/19/14 17:44m- & p-Xylenes 6.1ug/kg dry 1 WB2.4

12/19/14 12/19/14 17:4480-120 112 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 17:4481-117 107 %Surrogate: Toluene-d8

12/19/14 12/19/14 17:4474-121 106 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

15.6 12/23/14 12/23/14 13:37Gasoline-Range Organics 0.61mg/kg dry 5 ECM0.61

12/23/14 12/23/14 13:37 S-0785-115 116 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

169 12/18/14 12/20/14 10:44Diesel-Range Organics 9.8mg/kg dry 1 CMK9.8

12/18/14 12/20/14 10:4470-130 103 %Surrogate: o-Terphenyl

PERCENT SOLIDS

82 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 35 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 12

4121820-12 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

73.6 12/22/14 12/22/14 18:18Acetone 61.7ug/kg dry 5 WB61.7

ND 12/22/14 12/22/14 18:18tert-Amyl alcohol (TAA) 309ug/kg dry 5 WB309

ND 12/22/14 12/22/14 18:18tert-Amyl methyl ether (TAME) 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Benzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Bromobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Bromochloromethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Bromodichloromethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Bromoform 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Bromomethane 30.9ug/kg dry 5 WB30.9

414 12/22/14 12/22/14 18:18tert-Butanol (TBA) 309ug/kg dry 5 WB309

ND 12/22/14 12/22/14 18:182-Butanone (MEK) 61.7ug/kg dry 5 WB61.7

424 12/22/14 12/22/14 18:18n-Butylbenzene 30.9ug/kg dry 5 WB12.3

202 12/22/14 12/22/14 18:18sec-Butylbenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18tert-Butylbenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Carbon disulfide 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Carbon tetrachloride 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Chlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Chloroethane 30.9ug/kg dry 5 WB30.9

ND 12/22/14 12/22/14 18:18Chloroform 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Chloromethane 30.9ug/kg dry 5 WB30.9

ND 12/22/14 12/22/14 18:182-Chlorotoluene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:184-Chlorotoluene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2-Dibromo-3-chloropropane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Dibromochloromethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2-Dibromoethane (EDB) 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Dibromomethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2-Dichlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,3-Dichlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,4-Dichlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Dichlorodifluoromethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1-Dichloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2-Dichloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1-Dichloroethene 30.9ug/kg dry 5 WB12.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 36 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 12

4121820-12 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 18:18cis-1,2-Dichloroethene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18trans-1,2-Dichloroethene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Dichlorofluoromethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2-Dichloropropane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,3-Dichloropropane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:182,2-Dichloropropane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1-Dichloropropene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18cis-1,3-Dichloropropene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18trans-1,3-Dichloropropene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Diisopropyl ether (DIPE) 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Ethyl tert-butyl ether (ETBE) 30.9ug/kg dry 5 WB12.3

44.2 12/22/14 12/22/14 18:18Ethylbenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Hexachlorobutadiene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:182-Hexanone 61.7ug/kg dry 5 WB61.7

70.9 12/22/14 12/22/14 18:18Isopropylbenzene (Cumene) 30.9ug/kg dry 5 WB12.3

36.7 12/22/14 12/22/14 18:184-Isopropyltoluene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Methyl tert-butyl ether (MTBE) 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:184-Methyl-2-pentanone 61.7ug/kg dry 5 WB61.7

ND 12/22/14 12/22/14 18:18Methylene chloride 61.7ug/kg dry 5 WB61.7

157 12/22/14 12/22/14 18:18Naphthalene 30.9ug/kg dry 5 WB12.3

274 12/22/14 12/22/14 18:18n-Propylbenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Styrene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1,1,2-Tetrachloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1,2,2-Tetrachloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Tetrachloroethene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Toluene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2,3-Trichlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2,4-Trichlorobenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1,1-Trichloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,1,2-Trichloroethane 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Trichloroethene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Trichlorofluoromethane (Freon 11) 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:181,2,3-Trichloropropane 30.9ug/kg dry 5 WB12.3

117 12/22/14 12/22/14 18:181,2,4-Trimethylbenzene 30.9ug/kg dry 5 WB12.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 37 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT 12

4121820-12 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

58.8 12/22/14 12/22/14 18:181,3,5-Trimethylbenzene 30.9ug/kg dry 5 WB12.3

ND 12/22/14 12/22/14 18:18Vinyl chloride 30.9ug/kg dry 5 WB12.3

15.4 12/22/14 12/22/14 18:18o-Xylene 30.9J ug/kg dry 5 WB12.3

33.0 12/22/14 12/22/14 18:18m- & p-Xylenes 30.9ug/kg dry 5 WB12.3

12/22/14 12/22/14 18:1880-120 115 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 18:1881-117 102 %Surrogate: Toluene-d8

12/22/14 12/22/14 18:1874-121 100 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

25.6 12/22/14 12/22/14 17:42Gasoline-Range Organics 0.62mg/kg dry 5 ECM0.62

12/22/14 12/22/14 17:42 S-0785-115 137 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

202 12/18/14 12/20/14 11:11Diesel-Range Organics 9.9mg/kg dry 1 CMK9.9

12/18/14 12/20/14 11:1170-130 113 %Surrogate: o-Terphenyl

PERCENT SOLIDS

81 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 38 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N1

4121820-13 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 18:50Acetone 13.3ug/kg dry 1 WB13.3

ND 12/19/14 12/19/14 18:50tert-Amyl alcohol (TAA) 66.7ug/kg dry 1 WB66.7

ND 12/19/14 12/19/14 18:50tert-Amyl methyl ether (TAME) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Benzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Bromobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Bromochloromethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Bromodichloromethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Bromoform 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Bromomethane 6.7ug/kg dry 1 WB6.7

69.6 12/19/14 12/19/14 18:50tert-Butanol (TBA) 66.7ug/kg dry 1 WB66.7

ND 12/19/14 12/19/14 18:502-Butanone (MEK) 13.3ug/kg dry 1 WB13.3

ND 12/19/14 12/19/14 18:50n-Butylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50sec-Butylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50tert-Butylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Carbon disulfide 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Carbon tetrachloride 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Chlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Chloroethane 6.7ug/kg dry 1 WB6.7

ND 12/19/14 12/19/14 18:50Chloroform 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Chloromethane 6.7ug/kg dry 1 WB6.7

ND 12/19/14 12/19/14 18:502-Chlorotoluene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:504-Chlorotoluene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2-Dibromo-3-chloropropane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Dibromochloromethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2-Dibromoethane (EDB) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Dibromomethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2-Dichlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,3-Dichlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,4-Dichlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Dichlorodifluoromethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1-Dichloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2-Dichloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1-Dichloroethene 6.7ug/kg dry 1 WB2.7

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 39 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N1

4121820-13 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 18:50cis-1,2-Dichloroethene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50trans-1,2-Dichloroethene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Dichlorofluoromethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2-Dichloropropane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,3-Dichloropropane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:502,2-Dichloropropane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1-Dichloropropene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50cis-1,3-Dichloropropene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50trans-1,3-Dichloropropene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Diisopropyl ether (DIPE) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Ethyl tert-butyl ether (ETBE) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Ethylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Hexachlorobutadiene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:502-Hexanone 13.3ug/kg dry 1 WB13.3

ND 12/19/14 12/19/14 18:50Isopropylbenzene (Cumene) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:504-Isopropyltoluene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Methyl tert-butyl ether (MTBE) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:504-Methyl-2-pentanone 13.3ug/kg dry 1 WB13.3

ND 12/19/14 12/19/14 18:50Methylene chloride 13.3ug/kg dry 1 WB13.3

ND 12/19/14 12/19/14 18:50Naphthalene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50n-Propylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Styrene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1,1,2-Tetrachloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1,2,2-Tetrachloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Tetrachloroethene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Toluene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2,3-Trichlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2,4-Trichlorobenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1,1-Trichloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,1,2-Trichloroethane 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Trichloroethene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Trichlorofluoromethane (Freon 11) 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,2,3-Trichloropropane 6.7ug/kg dry 1 WB2.7

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 40 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N1

4121820-13 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 18:501,2,4-Trimethylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:501,3,5-Trimethylbenzene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50Vinyl chloride 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50o-Xylene 6.7ug/kg dry 1 WB2.7

ND 12/19/14 12/19/14 18:50m- & p-Xylenes 6.7ug/kg dry 1 WB2.7

12/19/14 12/19/14 18:5080-120 93 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 18:5081-117 102 %Surrogate: Toluene-d8

12/19/14 12/19/14 18:5074-121 96 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/22/14 12/22/14 18:19Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/22/14 12/22/14 18:1985-115 102 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

ND 12/18/14 12/20/14 11:38Diesel-Range Organics 10.7mg/kg dry 1 CMK10.7

12/18/14 12/20/14 11:3870-130 105 %Surrogate: o-Terphenyl

PERCENT SOLIDS

75 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 41 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N2

4121820-14 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/26/14 12/26/14 18:28Acetone 11.6ug/kg dry 1 WB11.6

ND 12/26/14 12/26/14 18:28tert-Amyl alcohol (TAA) 58.1ug/kg dry 1 WB58.1

ND 12/26/14 12/26/14 18:28tert-Amyl methyl ether (TAME) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Benzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Bromobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Bromochloromethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Bromodichloromethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Bromoform 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Bromomethane 5.8ug/kg dry 1 WB5.8

ND 12/26/14 12/26/14 18:28tert-Butanol (TBA) 58.1ug/kg dry 1 WB58.1

ND 12/26/14 12/26/14 18:282-Butanone (MEK) 11.6ug/kg dry 1 WB11.6

ND 12/26/14 12/26/14 18:28n-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28sec-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28tert-Butylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Carbon disulfide 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Carbon tetrachloride 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Chlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Chloroethane 5.8ug/kg dry 1 WB5.8

ND 12/26/14 12/26/14 18:28Chloroform 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Chloromethane 5.8ug/kg dry 1 WB5.8

ND 12/26/14 12/26/14 18:282-Chlorotoluene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:284-Chlorotoluene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2-Dibromo-3-chloropropane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Dibromochloromethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2-Dibromoethane (EDB) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Dibromomethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,3-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,4-Dichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Dichlorodifluoromethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1-Dichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2-Dichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1-Dichloroethene 5.8ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 42 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N2

4121820-14 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/26/14 12/26/14 18:28cis-1,2-Dichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28trans-1,2-Dichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Dichlorofluoromethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,3-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:282,2-Dichloropropane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28cis-1,3-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28trans-1,3-Dichloropropene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Diisopropyl ether (DIPE) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Ethyl tert-butyl ether (ETBE) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Ethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Hexachlorobutadiene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:282-Hexanone 11.6ug/kg dry 1 WB11.6

ND 12/26/14 12/26/14 18:28Isopropylbenzene (Cumene) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:284-Isopropyltoluene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Methyl tert-butyl ether (MTBE) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:284-Methyl-2-pentanone 11.6ug/kg dry 1 WB11.6

14.8 12/26/14 12/26/14 18:28Methylene chloride 11.6L ug/kg dry 1 WB11.6

ND 12/26/14 12/26/14 18:28Naphthalene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28n-Propylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Styrene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1,1,2-Tetrachloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1,2,2-Tetrachloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Tetrachloroethene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Toluene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2,3-Trichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2,4-Trichlorobenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1,1-Trichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,1,2-Trichloroethane 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Trichloroethene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Trichlorofluoromethane (Freon 11) 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,2,3-Trichloropropane 5.8ug/kg dry 1 WB2.3

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 43 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT N2

4121820-14 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/26/14 12/26/14 18:281,2,4-Trimethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:281,3,5-Trimethylbenzene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28Vinyl chloride 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28o-Xylene 5.8ug/kg dry 1 WB2.3

ND 12/26/14 12/26/14 18:28m- & p-Xylenes 5.8ug/kg dry 1 WB2.3

12/26/14 12/26/14 18:2880-120 120 %Surrogate: 1,2-Dichloroethane-d4

12/26/14 12/26/14 18:2881-117 96 %Surrogate: Toluene-d8

12/26/14 12/26/14 18:2874-121 84 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/26/14 12/26/14 17:03Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/26/14 12/26/14 17:0385-115 91 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

22.1 12/18/14 12/20/14 12:05Diesel-Range Organics 9.3mg/kg dry 1 CMK9.3

12/18/14 12/20/14 12:0570-130 99 %Surrogate: o-Terphenyl

PERCENT SOLIDS

86 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 44 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E1

4121820-15 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

39.6 12/19/14 12/19/14 19:24Acetone 13.0ug/kg dry 1 WB13.0

510 12/19/14 12/19/14 19:24tert-Amyl alcohol (TAA) 64.9ug/kg dry 1 WB64.9

ND 12/19/14 12/19/14 19:24tert-Amyl methyl ether (TAME) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Benzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Bromobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Bromochloromethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Bromodichloromethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Bromoform 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Bromomethane 6.5ug/kg dry 1 WB6.5

917 12/19/14 12/19/14 19:24tert-Butanol (TBA) 64.9ug/kg dry 1 WB64.9

ND 12/19/14 12/19/14 19:242-Butanone (MEK) 13.0ug/kg dry 1 WB13.0

ND 12/19/14 12/19/14 19:24n-Butylbenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24sec-Butylbenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24tert-Butylbenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Carbon disulfide 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Carbon tetrachloride 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Chlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Chloroethane 6.5ug/kg dry 1 WB6.5

ND 12/19/14 12/19/14 19:24Chloroform 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Chloromethane 6.5ug/kg dry 1 WB6.5

ND 12/19/14 12/19/14 19:242-Chlorotoluene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:244-Chlorotoluene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2-Dibromo-3-chloropropane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Dibromochloromethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2-Dibromoethane (EDB) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Dibromomethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2-Dichlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,3-Dichlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,4-Dichlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Dichlorodifluoromethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1-Dichloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2-Dichloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1-Dichloroethene 6.5ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 45 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E1

4121820-15 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 19:24cis-1,2-Dichloroethene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24trans-1,2-Dichloroethene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Dichlorofluoromethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2-Dichloropropane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,3-Dichloropropane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:242,2-Dichloropropane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1-Dichloropropene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24cis-1,3-Dichloropropene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24trans-1,3-Dichloropropene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Diisopropyl ether (DIPE) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Ethyl tert-butyl ether (ETBE) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Ethylbenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Hexachlorobutadiene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:242-Hexanone 13.0ug/kg dry 1 WB13.0

ND 12/19/14 12/19/14 19:24Isopropylbenzene (Cumene) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:244-Isopropyltoluene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Methyl tert-butyl ether (MTBE) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:244-Methyl-2-pentanone 13.0ug/kg dry 1 WB13.0

ND 12/19/14 12/19/14 19:24Methylene chloride 13.0ug/kg dry 1 WB13.0

4.5 12/19/14 12/19/14 19:24Naphthalene 6.5J ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24n-Propylbenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Styrene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1,1,2-Tetrachloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1,2,2-Tetrachloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Tetrachloroethene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Toluene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2,3-Trichlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2,4-Trichlorobenzene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1,1-Trichloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,1,2-Trichloroethane 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Trichloroethene 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Trichlorofluoromethane (Freon 11) 6.5ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:241,2,3-Trichloropropane 6.5ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 46 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E1

4121820-15 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 19:241,2,4-Trimethylbenzene 6.5ug/kg dry 1 WB2.6

4.7 12/19/14 12/19/14 19:241,3,5-Trimethylbenzene 6.5J ug/kg dry 1 WB2.6

ND 12/19/14 12/19/14 19:24Vinyl chloride 6.5ug/kg dry 1 WB2.6

4.4 12/19/14 12/19/14 19:24o-Xylene 6.5J ug/kg dry 1 WB2.6

2.8 12/19/14 12/19/14 19:24m- & p-Xylenes 6.5J ug/kg dry 1 WB2.6

12/19/14 12/19/14 19:2480-120 92 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 19:2481-117 102 %Surrogate: Toluene-d8

12/19/14 12/19/14 19:2474-121 98 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

0.35 12/22/14 12/22/14 18:55Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/22/14 12/22/14 18:5585-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

21.9 12/18/14 12/20/14 12:32Diesel-Range Organics 10.4mg/kg dry 1 CMK10.4

12/18/14 12/20/14 12:3270-130 99 %Surrogate: o-Terphenyl

PERCENT SOLIDS

77 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 47 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E2

4121820-16 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 19:57Acetone 11.9ug/kg dry 1 WB11.9

ND 12/19/14 12/19/14 19:57tert-Amyl alcohol (TAA) 59.5ug/kg dry 1 WB59.5

ND 12/19/14 12/19/14 19:57tert-Amyl methyl ether (TAME) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Benzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Bromobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Bromochloromethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Bromodichloromethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Bromoform 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Bromomethane 6.0ug/kg dry 1 WB6.0

ND 12/19/14 12/19/14 19:57tert-Butanol (TBA) 59.5ug/kg dry 1 WB59.5

ND 12/19/14 12/19/14 19:572-Butanone (MEK) 11.9ug/kg dry 1 WB11.9

ND 12/19/14 12/19/14 19:57n-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57sec-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57tert-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Carbon disulfide 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Carbon tetrachloride 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Chlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Chloroethane 6.0ug/kg dry 1 WB6.0

ND 12/19/14 12/19/14 19:57Chloroform 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Chloromethane 6.0ug/kg dry 1 WB6.0

ND 12/19/14 12/19/14 19:572-Chlorotoluene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:574-Chlorotoluene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2-Dibromo-3-chloropropane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Dibromochloromethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2-Dibromoethane (EDB) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Dibromomethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,3-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,4-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Dichlorodifluoromethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1-Dichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2-Dichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1-Dichloroethene 6.0ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 48 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E2

4121820-16 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 19:57cis-1,2-Dichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57trans-1,2-Dichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Dichlorofluoromethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,3-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:572,2-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57cis-1,3-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57trans-1,3-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Diisopropyl ether (DIPE) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Ethyl tert-butyl ether (ETBE) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Ethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Hexachlorobutadiene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:572-Hexanone 11.9ug/kg dry 1 WB11.9

ND 12/19/14 12/19/14 19:57Isopropylbenzene (Cumene) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:574-Isopropyltoluene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Methyl tert-butyl ether (MTBE) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:574-Methyl-2-pentanone 11.9ug/kg dry 1 WB11.9

ND 12/19/14 12/19/14 19:57Methylene chloride 11.9ug/kg dry 1 WB11.9

ND 12/19/14 12/19/14 19:57Naphthalene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57n-Propylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Styrene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1,1,2-Tetrachloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1,2,2-Tetrachloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Tetrachloroethene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Toluene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2,3-Trichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2,4-Trichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1,1-Trichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,1,2-Trichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Trichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Trichlorofluoromethane (Freon 11) 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,2,3-Trichloropropane 6.0ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 49 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT E2

4121820-16 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 19:571,2,4-Trimethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:571,3,5-Trimethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57Vinyl chloride 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57o-Xylene 6.0ug/kg dry 1 WB2.4

ND 12/19/14 12/19/14 19:57m- & p-Xylenes 6.0ug/kg dry 1 WB2.4

12/19/14 12/19/14 19:5780-120 91 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 19:5781-117 104 %Surrogate: Toluene-d8

12/19/14 12/19/14 19:5774-121 95 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/22/14 12/22/14 19:32Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/22/14 12/22/14 19:3285-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

ND 12/18/14 12/20/14 13:00Diesel-Range Organics 9.5mg/kg dry 1 CMK9.5

12/18/14 12/20/14 13:0070-130 95 %Surrogate: o-Terphenyl

PERCENT SOLIDS

84 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 50 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S1

4121820-17 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 20:31Acetone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 20:31tert-Amyl alcohol (TAA) 62.5ug/kg dry 1 WB62.5

ND 12/19/14 12/19/14 20:31tert-Amyl methyl ether (TAME) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Benzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Bromobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Bromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Bromodichloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Bromoform 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Bromomethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 20:31tert-Butanol (TBA) 62.5ug/kg dry 1 WB62.5

ND 12/19/14 12/19/14 20:312-Butanone (MEK) 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 20:31n-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31sec-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31tert-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Carbon disulfide 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Carbon tetrachloride 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Chlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Chloroethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 20:31Chloroform 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Chloromethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 20:312-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:314-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2-Dibromo-3-chloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Dibromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2-Dibromoethane (EDB) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Dibromomethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,3-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,4-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Dichlorodifluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1-Dichloroethene 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 51 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S1

4121820-17 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 20:31cis-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31trans-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Dichlorofluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,3-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:312,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31cis-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31trans-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Diisopropyl ether (DIPE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Ethyl tert-butyl ether (ETBE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Ethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Hexachlorobutadiene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:312-Hexanone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 20:31Isopropylbenzene (Cumene) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:314-Isopropyltoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Methyl tert-butyl ether (MTBE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:314-Methyl-2-pentanone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 20:31Methylene chloride 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 20:31Naphthalene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31n-Propylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Styrene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1,1,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1,2,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Tetrachloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Toluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2,3-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2,4-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1,1-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,1,2-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Trichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Trichlorofluoromethane (Freon 11) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,2,3-Trichloropropane 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 52 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S1

4121820-17 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 20:311,2,4-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:311,3,5-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31Vinyl chloride 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31o-Xylene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 20:31m- & p-Xylenes 6.3ug/kg dry 1 WB2.5

12/19/14 12/19/14 20:3180-120 94 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 20:3181-117 102 %Surrogate: Toluene-d8

12/19/14 12/19/14 20:3174-121 98 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/22/14 12/22/14 20:08Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/22/14 12/22/14 20:0885-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

ND 12/18/14 12/20/14 13:27Diesel-Range Organics 10.0mg/kg dry 1 CMK10.0

12/18/14 12/20/14 13:2770-130 99 %Surrogate: o-Terphenyl

PERCENT SOLIDS

80 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 53 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S2

4121820-18 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/19/14 12/19/14 21:04Acetone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 21:04tert-Amyl alcohol (TAA) 62.5ug/kg dry 1 WB62.5

ND 12/19/14 12/19/14 21:04tert-Amyl methyl ether (TAME) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Benzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Bromobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Bromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Bromodichloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Bromoform 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Bromomethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 21:04tert-Butanol (TBA) 62.5ug/kg dry 1 WB62.5

ND 12/19/14 12/19/14 21:042-Butanone (MEK) 12.5ug/kg dry 1 WB12.5

3.2 12/19/14 12/19/14 21:04n-Butylbenzene 6.3J ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04sec-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04tert-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Carbon disulfide 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Carbon tetrachloride 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Chlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Chloroethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 21:04Chloroform 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Chloromethane 6.3ug/kg dry 1 WB6.3

ND 12/19/14 12/19/14 21:042-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:044-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2-Dibromo-3-chloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Dibromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2-Dibromoethane (EDB) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Dibromomethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,3-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,4-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Dichlorodifluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1-Dichloroethene 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 54 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S2

4121820-18 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/19/14 12/19/14 21:04cis-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04trans-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Dichlorofluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,3-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:042,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04cis-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04trans-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Diisopropyl ether (DIPE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Ethyl tert-butyl ether (ETBE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Ethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Hexachlorobutadiene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:042-Hexanone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 21:04Isopropylbenzene (Cumene) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:044-Isopropyltoluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Methyl tert-butyl ether (MTBE) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:044-Methyl-2-pentanone 12.5ug/kg dry 1 WB12.5

ND 12/19/14 12/19/14 21:04Methylene chloride 12.5ug/kg dry 1 WB12.5

23.1 12/19/14 12/19/14 21:04Naphthalene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04n-Propylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Styrene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1,1,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1,2,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Tetrachloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Toluene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2,3-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2,4-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1,1-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,1,2-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Trichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Trichlorofluoromethane (Freon 11) 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:041,2,3-Trichloropropane 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 55 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT S2

4121820-18 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

25.1 12/19/14 12/19/14 21:041,2,4-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

12.9 12/19/14 12/19/14 21:041,3,5-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/19/14 12/19/14 21:04Vinyl chloride 6.3ug/kg dry 1 WB2.5

8.3 12/19/14 12/19/14 21:04o-Xylene 6.3ug/kg dry 1 WB2.5

3.0 12/19/14 12/19/14 21:04m- & p-Xylenes 6.3J ug/kg dry 1 WB2.5

12/19/14 12/19/14 21:0480-120 93 %Surrogate: 1,2-Dichloroethane-d4

12/19/14 12/19/14 21:0481-117 102 %Surrogate: Toluene-d8

12/19/14 12/19/14 21:0474-121 100 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

0.21 12/22/14 12/22/14 20:45Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/22/14 12/22/14 20:4585-115 103 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

12.1 12/21/14 12/23/14 05:34Diesel-Range Organics 10.0mg/kg dry 1 CMK10.0

12/21/14 12/23/14 05:3470-130 91 %Surrogate: o-Terphenyl

PERCENT SOLIDS

80 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 56 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W1

4121820-19 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 13:51Acetone 12.7ug/kg dry 1 WB12.7

ND 12/22/14 12/22/14 13:51tert-Amyl alcohol (TAA) 63.3ug/kg dry 1 WB63.3

ND 12/22/14 12/22/14 13:51tert-Amyl methyl ether (TAME) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Benzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Bromobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Bromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Bromodichloromethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Bromoform 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Bromomethane 6.3ug/kg dry 1 WB6.3

ND 12/22/14 12/22/14 13:51tert-Butanol (TBA) 63.3ug/kg dry 1 WB63.3

ND 12/22/14 12/22/14 13:512-Butanone (MEK) 12.7ug/kg dry 1 WB12.7

ND 12/22/14 12/22/14 13:51n-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51sec-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51tert-Butylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Carbon disulfide 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Carbon tetrachloride 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Chlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Chloroethane 6.3ug/kg dry 1 WB6.3

ND 12/22/14 12/22/14 13:51Chloroform 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Chloromethane 6.3ug/kg dry 1 WB6.3

ND 12/22/14 12/22/14 13:512-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:514-Chlorotoluene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2-Dibromo-3-chloropropane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Dibromochloromethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2-Dibromoethane (EDB) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Dibromomethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,3-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,4-Dichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Dichlorodifluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2-Dichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1-Dichloroethene 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 57 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W1

4121820-19 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 13:51cis-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51trans-1,2-Dichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Dichlorofluoromethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,3-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:512,2-Dichloropropane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51cis-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51trans-1,3-Dichloropropene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Diisopropyl ether (DIPE) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Ethyl tert-butyl ether (ETBE) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Ethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Hexachlorobutadiene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:512-Hexanone 12.7ug/kg dry 1 WB12.7

ND 12/22/14 12/22/14 13:51Isopropylbenzene (Cumene) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:514-Isopropyltoluene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Methyl tert-butyl ether (MTBE) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:514-Methyl-2-pentanone 12.7ug/kg dry 1 WB12.7

ND 12/22/14 12/22/14 13:51Methylene chloride 12.7ug/kg dry 1 WB12.7

ND 12/22/14 12/22/14 13:51Naphthalene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51n-Propylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Styrene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1,1,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1,2,2-Tetrachloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Tetrachloroethene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Toluene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2,3-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2,4-Trichlorobenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1,1-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,1,2-Trichloroethane 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Trichloroethene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Trichlorofluoromethane (Freon 11) 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,2,3-Trichloropropane 6.3ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 58 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W1

4121820-19 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 13:511,2,4-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:511,3,5-Trimethylbenzene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51Vinyl chloride 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51o-Xylene 6.3ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 13:51m- & p-Xylenes 6.3ug/kg dry 1 WB2.5

12/22/14 12/22/14 13:5180-120 104 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 13:5181-117 103 %Surrogate: Toluene-d8

12/22/14 12/22/14 13:5174-121 86 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 14:50Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/23/14 12/23/14 14:5085-115 99 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

19.5 12/21/14 12/23/14 06:01Diesel-Range Organics 10.1mg/kg dry 1 CMK10.1

12/21/14 12/23/14 06:0170-130 91 %Surrogate: o-Terphenyl

PERCENT SOLIDS

79 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 59 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W2

4121820-20 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 14:25Acetone 12.8ug/kg dry 1 WB12.8

897 12/22/14 12/22/14 14:25tert-Amyl alcohol (TAA) 64.1ug/kg dry 1 WB64.1

ND 12/22/14 12/22/14 14:25tert-Amyl methyl ether (TAME) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Benzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Bromobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Bromochloromethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Bromodichloromethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Bromoform 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Bromomethane 6.4ug/kg dry 1 WB6.4

1460 12/22/14 12/22/14 14:25tert-Butanol (TBA) 64.1E ug/kg dry 1 WB64.1

ND 12/22/14 12/22/14 14:252-Butanone (MEK) 12.8ug/kg dry 1 WB12.8

ND 12/22/14 12/22/14 14:25n-Butylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25sec-Butylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25tert-Butylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Carbon disulfide 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Carbon tetrachloride 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Chlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Chloroethane 6.4ug/kg dry 1 WB6.4

ND 12/22/14 12/22/14 14:25Chloroform 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Chloromethane 6.4ug/kg dry 1 WB6.4

ND 12/22/14 12/22/14 14:252-Chlorotoluene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:254-Chlorotoluene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2-Dibromo-3-chloropropane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Dibromochloromethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2-Dibromoethane (EDB) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Dibromomethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2-Dichlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,3-Dichlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,4-Dichlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Dichlorodifluoromethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1-Dichloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2-Dichloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1-Dichloroethene 6.4ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 60 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W2

4121820-20 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 14:25cis-1,2-Dichloroethene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25trans-1,2-Dichloroethene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Dichlorofluoromethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2-Dichloropropane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,3-Dichloropropane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:252,2-Dichloropropane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1-Dichloropropene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25cis-1,3-Dichloropropene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25trans-1,3-Dichloropropene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Diisopropyl ether (DIPE) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Ethyl tert-butyl ether (ETBE) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Ethylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Hexachlorobutadiene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:252-Hexanone 12.8ug/kg dry 1 WB12.8

ND 12/22/14 12/22/14 14:25Isopropylbenzene (Cumene) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:254-Isopropyltoluene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Methyl tert-butyl ether (MTBE) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:254-Methyl-2-pentanone 12.8ug/kg dry 1 WB12.8

ND 12/22/14 12/22/14 14:25Methylene chloride 12.8ug/kg dry 1 WB12.8

ND 12/22/14 12/22/14 14:25Naphthalene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25n-Propylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Styrene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1,1,2-Tetrachloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1,2,2-Tetrachloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Tetrachloroethene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Toluene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2,3-Trichlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2,4-Trichlorobenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1,1-Trichloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,1,2-Trichloroethane 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Trichloroethene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Trichlorofluoromethane (Freon 11) 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,2,3-Trichloropropane 6.4ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 61 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

TANK PIT W2

4121820-20 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 14:251,2,4-Trimethylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:251,3,5-Trimethylbenzene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25Vinyl chloride 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25o-Xylene 6.4ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 14:25m- & p-Xylenes 6.4ug/kg dry 1 WB2.6

12/22/14 12/22/14 14:2580-120 100 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 14:2581-117 101 %Surrogate: Toluene-d8

12/22/14 12/22/14 14:2574-121 92 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 15:26Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/23/14 12/23/14 15:2685-115 98 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

11.1 12/21/14 12/23/14 06:29Diesel-Range Organics 10.3mg/kg dry 1 CMK10.3

12/21/14 12/23/14 06:2970-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS

78 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 62 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 1

4121820-21 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 14:58Acetone 12.0ug/kg dry 1 WB12.0

ND 12/22/14 12/22/14 14:58tert-Amyl alcohol (TAA) 60.2ug/kg dry 1 WB60.2

ND 12/22/14 12/22/14 14:58tert-Amyl methyl ether (TAME) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Benzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Bromobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Bromochloromethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Bromodichloromethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Bromoform 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Bromomethane 6.0ug/kg dry 1 WB6.0

ND 12/22/14 12/22/14 14:58tert-Butanol (TBA) 60.2ug/kg dry 1 WB60.2

ND 12/22/14 12/22/14 14:582-Butanone (MEK) 12.0ug/kg dry 1 WB12.0

ND 12/22/14 12/22/14 14:58n-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58sec-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58tert-Butylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Carbon disulfide 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Carbon tetrachloride 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Chlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Chloroethane 6.0ug/kg dry 1 WB6.0

ND 12/22/14 12/22/14 14:58Chloroform 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Chloromethane 6.0ug/kg dry 1 WB6.0

ND 12/22/14 12/22/14 14:582-Chlorotoluene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:584-Chlorotoluene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2-Dibromo-3-chloropropane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Dibromochloromethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2-Dibromoethane (EDB) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Dibromomethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,3-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,4-Dichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Dichlorodifluoromethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1-Dichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2-Dichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1-Dichloroethene 6.0ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 63 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 1

4121820-21 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 14:58cis-1,2-Dichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58trans-1,2-Dichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Dichlorofluoromethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,3-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:582,2-Dichloropropane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58cis-1,3-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58trans-1,3-Dichloropropene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Diisopropyl ether (DIPE) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Ethyl tert-butyl ether (ETBE) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Ethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Hexachlorobutadiene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:582-Hexanone 12.0ug/kg dry 1 WB12.0

ND 12/22/14 12/22/14 14:58Isopropylbenzene (Cumene) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:584-Isopropyltoluene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Methyl tert-butyl ether (MTBE) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:584-Methyl-2-pentanone 12.0ug/kg dry 1 WB12.0

ND 12/22/14 12/22/14 14:58Methylene chloride 12.0ug/kg dry 1 WB12.0

ND 12/22/14 12/22/14 14:58Naphthalene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58n-Propylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Styrene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1,1,2-Tetrachloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1,2,2-Tetrachloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Tetrachloroethene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Toluene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2,3-Trichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2,4-Trichlorobenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1,1-Trichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,1,2-Trichloroethane 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Trichloroethene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Trichlorofluoromethane (Freon 11) 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,2,3-Trichloropropane 6.0ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 64 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 1

4121820-21 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 14:581,2,4-Trimethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:581,3,5-Trimethylbenzene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58Vinyl chloride 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58o-Xylene 6.0ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 14:58m- & p-Xylenes 6.0ug/kg dry 1 WB2.4

12/22/14 12/22/14 14:5880-120 111 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 14:5881-117 99 %Surrogate: Toluene-d8

12/22/14 12/22/14 14:5874-121 92 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 16:02Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/23/14 12/23/14 16:0285-115 98 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

ND 12/21/14 12/23/14 06:56Diesel-Range Organics 9.6mg/kg dry 1 CMK9.6

12/21/14 12/23/14 06:5670-130 90 %Surrogate: o-Terphenyl

PERCENT SOLIDS

83 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 65 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 2

4121820-22 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 15:31Acetone 11.8ug/kg dry 1 WB11.8

ND 12/22/14 12/22/14 15:31tert-Amyl alcohol (TAA) 58.8ug/kg dry 1 WB58.8

ND 12/22/14 12/22/14 15:31tert-Amyl methyl ether (TAME) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Benzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Bromobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Bromochloromethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Bromodichloromethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Bromoform 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Bromomethane 5.9ug/kg dry 1 WB5.9

ND 12/22/14 12/22/14 15:31tert-Butanol (TBA) 58.8ug/kg dry 1 WB58.8

ND 12/22/14 12/22/14 15:312-Butanone (MEK) 11.8ug/kg dry 1 WB11.8

ND 12/22/14 12/22/14 15:31n-Butylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31sec-Butylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31tert-Butylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Carbon disulfide 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Carbon tetrachloride 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Chlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Chloroethane 5.9ug/kg dry 1 WB5.9

ND 12/22/14 12/22/14 15:31Chloroform 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Chloromethane 5.9ug/kg dry 1 WB5.9

ND 12/22/14 12/22/14 15:312-Chlorotoluene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:314-Chlorotoluene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2-Dibromo-3-chloropropane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Dibromochloromethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2-Dibromoethane (EDB) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Dibromomethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,3-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,4-Dichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Dichlorodifluoromethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1-Dichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2-Dichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1-Dichloroethene 5.9ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 66 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 2

4121820-22 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 15:31cis-1,2-Dichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31trans-1,2-Dichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Dichlorofluoromethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,3-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:312,2-Dichloropropane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31cis-1,3-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31trans-1,3-Dichloropropene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Diisopropyl ether (DIPE) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Ethyl tert-butyl ether (ETBE) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Ethylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Hexachlorobutadiene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:312-Hexanone 11.8ug/kg dry 1 WB11.8

ND 12/22/14 12/22/14 15:31Isopropylbenzene (Cumene) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:314-Isopropyltoluene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Methyl tert-butyl ether (MTBE) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:314-Methyl-2-pentanone 11.8ug/kg dry 1 WB11.8

ND 12/22/14 12/22/14 15:31Methylene chloride 11.8ug/kg dry 1 WB11.8

ND 12/22/14 12/22/14 15:31Naphthalene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31n-Propylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Styrene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1,1,2-Tetrachloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1,2,2-Tetrachloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Tetrachloroethene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Toluene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2,3-Trichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2,4-Trichlorobenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1,1-Trichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,1,2-Trichloroethane 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Trichloroethene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Trichlorofluoromethane (Freon 11) 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,2,3-Trichloropropane 5.9ug/kg dry 1 WB2.4

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 67 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 2

4121820-22 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 15:311,2,4-Trimethylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:311,3,5-Trimethylbenzene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31Vinyl chloride 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31o-Xylene 5.9ug/kg dry 1 WB2.4

ND 12/22/14 12/22/14 15:31m- & p-Xylenes 5.9ug/kg dry 1 WB2.4

12/22/14 12/22/14 15:3180-120 108 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 15:3181-117 84 %Surrogate: Toluene-d8

12/22/14 12/22/14 15:3174-121 98 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 16:39Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/23/14 12/23/14 16:3985-115 98 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

17.8 12/21/14 12/23/14 07:24Diesel-Range Organics 9.4mg/kg dry 1 CMK9.4

12/21/14 12/23/14 07:2470-130 92 %Surrogate: o-Terphenyl

PERCENT SOLIDS

85 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 68 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 3

4121820-23 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 16:05Acetone 13.2ug/kg dry 1 WB13.2

ND 12/22/14 12/22/14 16:05tert-Amyl alcohol (TAA) 65.8ug/kg dry 1 WB65.8

ND 12/22/14 12/22/14 16:05tert-Amyl methyl ether (TAME) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Benzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Bromobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Bromochloromethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Bromodichloromethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Bromoform 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Bromomethane 6.6ug/kg dry 1 WB6.6

ND 12/22/14 12/22/14 16:05tert-Butanol (TBA) 65.8ug/kg dry 1 WB65.8

ND 12/22/14 12/22/14 16:052-Butanone (MEK) 13.2ug/kg dry 1 WB13.2

ND 12/22/14 12/22/14 16:05n-Butylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05sec-Butylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05tert-Butylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Carbon disulfide 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Carbon tetrachloride 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Chlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Chloroethane 6.6ug/kg dry 1 WB6.6

ND 12/22/14 12/22/14 16:05Chloroform 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Chloromethane 6.6ug/kg dry 1 WB6.6

ND 12/22/14 12/22/14 16:052-Chlorotoluene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:054-Chlorotoluene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2-Dibromo-3-chloropropane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Dibromochloromethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2-Dibromoethane (EDB) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Dibromomethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2-Dichlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,3-Dichlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,4-Dichlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Dichlorodifluoromethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1-Dichloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2-Dichloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1-Dichloroethene 6.6ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 69 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 3

4121820-23 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 16:05cis-1,2-Dichloroethene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05trans-1,2-Dichloroethene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Dichlorofluoromethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2-Dichloropropane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,3-Dichloropropane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:052,2-Dichloropropane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1-Dichloropropene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05cis-1,3-Dichloropropene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05trans-1,3-Dichloropropene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Diisopropyl ether (DIPE) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Ethyl tert-butyl ether (ETBE) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Ethylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Hexachlorobutadiene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:052-Hexanone 13.2ug/kg dry 1 WB13.2

ND 12/22/14 12/22/14 16:05Isopropylbenzene (Cumene) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:054-Isopropyltoluene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Methyl tert-butyl ether (MTBE) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:054-Methyl-2-pentanone 13.2ug/kg dry 1 WB13.2

ND 12/22/14 12/22/14 16:05Methylene chloride 13.2ug/kg dry 1 WB13.2

ND 12/22/14 12/22/14 16:05Naphthalene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05n-Propylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Styrene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1,1,2-Tetrachloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1,2,2-Tetrachloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Tetrachloroethene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Toluene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2,3-Trichlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2,4-Trichlorobenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1,1-Trichloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,1,2-Trichloroethane 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Trichloroethene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Trichlorofluoromethane (Freon 11) 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,2,3-Trichloropropane 6.6ug/kg dry 1 WB2.6

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 70 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 3

4121820-23 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 16:051,2,4-Trimethylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:051,3,5-Trimethylbenzene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05Vinyl chloride 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05o-Xylene 6.6ug/kg dry 1 WB2.6

ND 12/22/14 12/22/14 16:05m- & p-Xylenes 6.6ug/kg dry 1 WB2.6

12/22/14 12/22/14 16:0580-120 110 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 16:0581-117 100 %Surrogate: Toluene-d8

12/22/14 12/22/14 16:0574-121 91 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 17:16Gasoline-Range Organics 0.13mg/kg dry 1 ECM0.13

12/23/14 12/23/14 17:1685-115 99 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

ND 12/21/14 12/23/14 07:51Diesel-Range Organics 10.5mg/kg dry 1 CMK10.5

12/21/14 12/23/14 07:5170-130 83 %Surrogate: o-Terphenyl

PERCENT SOLIDS

76 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 71 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 4

4121820-24 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS)

ND 12/22/14 12/22/14 16:38Acetone 12.3ug/kg dry 1 WB12.3

ND 12/22/14 12/22/14 16:38tert-Amyl alcohol (TAA) 61.7ug/kg dry 1 WB61.7

ND 12/22/14 12/22/14 16:38tert-Amyl methyl ether (TAME) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Benzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Bromobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Bromochloromethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Bromodichloromethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Bromoform 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Bromomethane 6.2ug/kg dry 1 WB6.2

ND 12/22/14 12/22/14 16:38tert-Butanol (TBA) 61.7ug/kg dry 1 WB61.7

ND 12/22/14 12/22/14 16:382-Butanone (MEK) 12.3ug/kg dry 1 WB12.3

ND 12/22/14 12/22/14 16:38n-Butylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38sec-Butylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38tert-Butylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Carbon disulfide 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Carbon tetrachloride 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Chlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Chloroethane 6.2ug/kg dry 1 WB6.2

ND 12/22/14 12/22/14 16:38Chloroform 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Chloromethane 6.2ug/kg dry 1 WB6.2

ND 12/22/14 12/22/14 16:382-Chlorotoluene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:384-Chlorotoluene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2-Dibromo-3-chloropropane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Dibromochloromethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2-Dibromoethane (EDB) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Dibromomethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2-Dichlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,3-Dichlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,4-Dichlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Dichlorodifluoromethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1-Dichloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2-Dichloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1-Dichloroethene 6.2ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 72 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 4

4121820-24 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 16:38cis-1,2-Dichloroethene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38trans-1,2-Dichloroethene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Dichlorofluoromethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2-Dichloropropane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,3-Dichloropropane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:382,2-Dichloropropane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1-Dichloropropene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38cis-1,3-Dichloropropene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38trans-1,3-Dichloropropene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Diisopropyl ether (DIPE) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Ethyl tert-butyl ether (ETBE) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Ethylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Hexachlorobutadiene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:382-Hexanone 12.3ug/kg dry 1 WB12.3

ND 12/22/14 12/22/14 16:38Isopropylbenzene (Cumene) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:384-Isopropyltoluene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Methyl tert-butyl ether (MTBE) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:384-Methyl-2-pentanone 12.3ug/kg dry 1 WB12.3

ND 12/22/14 12/22/14 16:38Methylene chloride 12.3ug/kg dry 1 WB12.3

ND 12/22/14 12/22/14 16:38Naphthalene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38n-Propylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Styrene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1,1,2-Tetrachloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1,2,2-Tetrachloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Tetrachloroethene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Toluene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2,3-Trichlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2,4-Trichlorobenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1,1-Trichloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,1,2-Trichloroethane 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Trichloroethene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Trichlorofluoromethane (Freon 11) 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,2,3-Trichloropropane 6.2ug/kg dry 1 WB2.5

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 73 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

ResultAnalyte Limit (MRL)

Reporting

Prepared Analyzed AnalystNotes DilutionUnits

CANOPY 4

4121820-24 (Soil)

Sample Date: 12/18/14

Quantitation

Limit (LOQ)

VOLATILE ORGANICS BY EPA METHOD 8260B (GC/MS) (continued)

ND 12/22/14 12/22/14 16:381,2,4-Trimethylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:381,3,5-Trimethylbenzene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38Vinyl chloride 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38o-Xylene 6.2ug/kg dry 1 WB2.5

ND 12/22/14 12/22/14 16:38m- & p-Xylenes 6.2ug/kg dry 1 WB2.5

12/22/14 12/22/14 16:3880-120 111 %Surrogate: 1,2-Dichloroethane-d4

12/22/14 12/22/14 16:3881-117 95 %Surrogate: Toluene-d8

12/22/14 12/22/14 16:3874-121 90 %Surrogate: 4-Bromofluorobenzene

GASOLINE RANGE ORGANICS BY EPA 5030/8015B

ND 12/23/14 12/23/14 17:52Gasoline-Range Organics 0.12mg/kg dry 1 ECM0.12

12/23/14 12/23/14 17:5285-115 98 %Surrogate: a,a,a-Trifluorotoluene

DIESEL RANGE ORGANICS BY EPA 3540/8015B

38.7 12/21/14 12/23/14 08:19Diesel-Range Organics 9.9mg/kg dry 1 CMK9.9

12/21/14 12/23/14 08:1970-130 93 %Surrogate: o-Terphenyl

PERCENT SOLIDS

81 12/19/14 12/20/14 08:41Percent Solids % 1 WB

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 74 of 78

Project:

Project Number:

Project Manager:

Reported:06-170

Michael Robertson

MYERSVILLE CROWN

12/29/14 11:31

1500 Caton Center Dr Suite G

Baltimore MD 21227

410-247-7600

www.mdspectral.com

Analytical Results

Notes and Definitions

S-07 Surrogate recovery and/or internal standard area are outside control limits due to sample matrix effect.

L Analyte is a possible laboratory contaminant

J Detected but below the reporting limit; therefore, result is an estimated concentration (CLP J-Flag).

E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered

an estimate (CLP E-flag).

Sample results reported on a dry weight basis

Relative Percent DifferenceRPD

dry

Not ReportedNR

Analyte NOT DETECTED at or above the reporting limitND

Analyte DETECTEDDET

Will Brewington, Staff Chemist

The results in this report apply to the samples analyzed in accordance with the chain of

custody document. This analytical report must be reproduced in its entirety.

As a NELAP accredited laboratory, MSS certifies that all applicable test results meet NELAC requirements. Page 75 of 78

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