twickenham pond stormwater management facilities rehabilitation project … · 2020. 9. 15. · the...
TRANSCRIPT
City Of Richmond Hill Project File Report
Twickenham Stormwater Management Facilities Rehabilitation
APPENDIX D
Sediment and Water Quality
Analyses
TMIG PROJECT NUMBER 19179
August 30 2019
The Municipal Infrastructure Group (TMIG)
8800 Dufferin Street Suite 200
Vaughan Ontario L4K 0C5
Attention Steve Hollingworth Director of Stormwater Management
Re Sediment and Water Sampling Memo ndash Twickenham Pond
Project No 20-202649
Introduction
Groundwater Environmental Management Services Inc (GEMS) has been retained by The
Municipal Infrastructure Group (TMIG) to collect and analyze representative water and sediment
samples taken from Twickenham Pond The project site is located within Twickenham Park east
of Bathurst Street just north of Canyon Hill Avenue in Richmond Hill Ontario
Field Sample Collection
GEMS was on site August 15 2019 to collect representative samples for both sediment and water
from Twickenham Pond Two (2) staff members were on site to facilitate the collection which
was done from safe locations along the banks of the pond A ponar dredge sampler spade
andor shovel was used to collect sediment samples as well as the standard collection of
water samples using laboratory provided sampling containers Standard quality assurance
and quality control practices were observed and standard chain of custody command
practices were used to submit samples to the laboratory All samples were submitted to an
accredited laboratory for analysis (Bureau Vertias)
Three (3) samples from Twickenham Pond were taken for sediment the following chemical
parameters were chosen and analyzed based on typical stormwater management pond sediment
buildup
bull Petroleum hydrocarbons (F2-F4) (PHCs) plus benzene toluene ethylbenzene and
xylenes (BTEX) metals and inorganics volatile organic compounds (VOCs) polycyclic
aromatic hydrocarbons (PAHs) and pH
Sediment and Water Sampling Memo August 30 2019
Page 2
In addition one (1) sediment sample from the pond was also analyzed for Toxicity Characteristic
Leaching Procedure (TCLP) for the purposes of off-site disposal as registered receivers require
the completion of this analysis prior to acceptance of any soil or sediment material
Three (3) surface water samples from the pond were taken the following parameters were analyzed
bull Surface Water Rapid Chemical Analysis Package (RCAp) Total Suspended Solids
(TSS) and Volatile Organic Compounds (VOC)s
All sample locations are shown on the figures provided in Appendix 1
Summary of Results
The following results were found within Twickenham Pond
Sediment samples were labelled TH1 TH2 and TH3 with the TCLP sample labelled TH (taken at the same location as the TH2 sediment sample)
The only reported exceedance for sediment in all three (3) sample locations was found in TH2 for F4 (C34-C50 Hydrocarbons)
The TCLP sample showed no toxic levels for any parameters within the sample Therefore the sample is considered non-hazardous
Water quality results from Twickenham Pond are also labelled as TH1 TH2 and TH3 Results were compared to both Ontario Regulation 153 and Provincial Water Quality Objectives (PWQO) exceedances were found when compared to both criteria
All sample exceedances and detections can be found in Tables 1 2 3 and 4 while the full summary of the lab results can be found in Appendix 2
Table 1 Soil Sample Exceedances
Analysis Parameter Units Criteria
1 Criteria
2 TH1 TH2 TH3
F2-F4 Hydrocarbons
F4 (C34-C50 Hydrocarbons)
ugg 120 5600 ND 140 ND
Table 2 TCLP Detections
OReg 558 TCLP Inorganics
Parameter Units Criteria TH
Inorganics Leachable Fluoride (F-) mgL 150 042
Metals Leachable Barium (Ba) mgL 100 06
Leachable Boron (B) mgL 500 02
Sediment and Water Sampling Memo August 30 2019
Page 3
Table 3 Water Quality Exceedances (OrsquoReg 15304)
Analysis Parameter Units Criteria 1 TH1 TH2 TH3
Total Copper ugL 5 13 35 16
OrsquoReg 15304 Total Lead ugL 19 51 21 059
Total Vanadium ugL 39 11 51 29
Table 4 Water Quality Exceedances (PWQO)
Analysis Parameter Units Criteria 2 TH1 TH2 TH3
PWQO
Total Phosphorus mgL 001 2 047 037
Total Cobalt ugL 09 31 12 ND
Total Copper ugL 5 13 35 16
Total Iron ugL 300 8300 2900 1100
Total Lead ugL 5 51 21 059
Total Vanadium ugL 6 11 51 29
Total Zinc ugL 30 48 88 ND
Total Suspended Solids mgL 25 730 230 100
While PWQO does not have a specific criteria for TSS the Canadian Council of Ministers of the Environment (CCME) recommend a maximum increase of 25mgL above background water quality for short-term exposure
Conclusions and Closure
The w ater quality was completed for the pu rposes of dewatering the po nd prior to any sediment
removal The Total Suspended Solids (TSS) levels within the pond were high which is an indicator
of poor water quality Sample locations TH2 (230 mgL) and TH3 (100 mgL) reported high TSS
levels while TH1 reported much higher levels at 730 mgL The results are likely skewed higher
as a result of the algae content in the water at the t ime of sampling As a result of the high TSS
filtration would be required should the pond need to be dewatered for future maintenance andor
clean out purposes It is also anticipated that the exceedances for the metals parameters are a
result of high TSS For dewatering purposes the water from the pond will need to be filtered prior
to entering the natural environment
Only F4 hydrocarbons were found at sediment sample location TH2 within Twickenham Pond
TH2 was found to exceed the Table 1 criteria limits but it meets the Table 3 criteria Only three
shoreline samples were able to be taken safely and feasibly this excludes the center of the pond
where more sediment accumulation could result in additional exceedances as such it cannot be
guaranteed that all other sediment within the pond meets either criteria Further sampling may
be required if the sediment is to be used on site or at a new location otherwise the sediment
should be disposed of at a registered landfill or receiving site capable of accepting Table 3
material It is expected that there will be exceedances above Table 1 criteria at other locations
within the pond due to the exceedance observed at sampling location TH2
_____________________ __ _________________________ ___
Sediment and Water Sampling Memo August 30 2019
Page 4
Based on the results of the TCLP the tested parameters meet the Ontario Regulation 558 (as
amended) for non-hazardous material and do not need to be disposed of at a hazardous waste
disposal location While the material can be brought to a commercial site to be used (as the
sample did meet Table 3 criteria limits) it is not recommended as it could create structural
limitations due to the water content within the material Significant drying and mixing would be
required to reuse the material on a site capable of accepted Table 3 material As such GEMS
recommends bringing the removed material to a landfill for disposal
This report was prepared by GEMS for TMIG as part of the Twickenham Pond Rehabilitation
Schedule B Municipal Class Environmental Assessment The report provides a summary of the
sediment and surface water conditions in Twickenham Pond Conclusions are based solely on
the collected and available information Any use by which a third party makes of this report or
any reliance on or decisions to be made based on it are the sole responsibility of such third
parties
We trust that this report will meet your current requirements Please do not hesitate to contact the undersigned should you have any questions or require additional information
Yours truly Groundwater Environmental Management Services Inc
Prepared By
Joelle Pecora BA Cert Ecol Rest Junior EcologistTechnician
Reviewed By
Kim Logan PGeo (Limited) QPESA PBiol Senior Ecologist and Project Manager
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
August 30 2019
The Municipal Infrastructure Group (TMIG)
8800 Dufferin Street Suite 200
Vaughan Ontario L4K 0C5
Attention Steve Hollingworth Director of Stormwater Management
Re Sediment and Water Sampling Memo ndash Twickenham Pond
Project No 20-202649
Introduction
Groundwater Environmental Management Services Inc (GEMS) has been retained by The
Municipal Infrastructure Group (TMIG) to collect and analyze representative water and sediment
samples taken from Twickenham Pond The project site is located within Twickenham Park east
of Bathurst Street just north of Canyon Hill Avenue in Richmond Hill Ontario
Field Sample Collection
GEMS was on site August 15 2019 to collect representative samples for both sediment and water
from Twickenham Pond Two (2) staff members were on site to facilitate the collection which
was done from safe locations along the banks of the pond A ponar dredge sampler spade
andor shovel was used to collect sediment samples as well as the standard collection of
water samples using laboratory provided sampling containers Standard quality assurance
and quality control practices were observed and standard chain of custody command
practices were used to submit samples to the laboratory All samples were submitted to an
accredited laboratory for analysis (Bureau Vertias)
Three (3) samples from Twickenham Pond were taken for sediment the following chemical
parameters were chosen and analyzed based on typical stormwater management pond sediment
buildup
bull Petroleum hydrocarbons (F2-F4) (PHCs) plus benzene toluene ethylbenzene and
xylenes (BTEX) metals and inorganics volatile organic compounds (VOCs) polycyclic
aromatic hydrocarbons (PAHs) and pH
Sediment and Water Sampling Memo August 30 2019
Page 2
In addition one (1) sediment sample from the pond was also analyzed for Toxicity Characteristic
Leaching Procedure (TCLP) for the purposes of off-site disposal as registered receivers require
the completion of this analysis prior to acceptance of any soil or sediment material
Three (3) surface water samples from the pond were taken the following parameters were analyzed
bull Surface Water Rapid Chemical Analysis Package (RCAp) Total Suspended Solids
(TSS) and Volatile Organic Compounds (VOC)s
All sample locations are shown on the figures provided in Appendix 1
Summary of Results
The following results were found within Twickenham Pond
Sediment samples were labelled TH1 TH2 and TH3 with the TCLP sample labelled TH (taken at the same location as the TH2 sediment sample)
The only reported exceedance for sediment in all three (3) sample locations was found in TH2 for F4 (C34-C50 Hydrocarbons)
The TCLP sample showed no toxic levels for any parameters within the sample Therefore the sample is considered non-hazardous
Water quality results from Twickenham Pond are also labelled as TH1 TH2 and TH3 Results were compared to both Ontario Regulation 153 and Provincial Water Quality Objectives (PWQO) exceedances were found when compared to both criteria
All sample exceedances and detections can be found in Tables 1 2 3 and 4 while the full summary of the lab results can be found in Appendix 2
Table 1 Soil Sample Exceedances
Analysis Parameter Units Criteria
1 Criteria
2 TH1 TH2 TH3
F2-F4 Hydrocarbons
F4 (C34-C50 Hydrocarbons)
ugg 120 5600 ND 140 ND
Table 2 TCLP Detections
OReg 558 TCLP Inorganics
Parameter Units Criteria TH
Inorganics Leachable Fluoride (F-) mgL 150 042
Metals Leachable Barium (Ba) mgL 100 06
Leachable Boron (B) mgL 500 02
Sediment and Water Sampling Memo August 30 2019
Page 3
Table 3 Water Quality Exceedances (OrsquoReg 15304)
Analysis Parameter Units Criteria 1 TH1 TH2 TH3
Total Copper ugL 5 13 35 16
OrsquoReg 15304 Total Lead ugL 19 51 21 059
Total Vanadium ugL 39 11 51 29
Table 4 Water Quality Exceedances (PWQO)
Analysis Parameter Units Criteria 2 TH1 TH2 TH3
PWQO
Total Phosphorus mgL 001 2 047 037
Total Cobalt ugL 09 31 12 ND
Total Copper ugL 5 13 35 16
Total Iron ugL 300 8300 2900 1100
Total Lead ugL 5 51 21 059
Total Vanadium ugL 6 11 51 29
Total Zinc ugL 30 48 88 ND
Total Suspended Solids mgL 25 730 230 100
While PWQO does not have a specific criteria for TSS the Canadian Council of Ministers of the Environment (CCME) recommend a maximum increase of 25mgL above background water quality for short-term exposure
Conclusions and Closure
The w ater quality was completed for the pu rposes of dewatering the po nd prior to any sediment
removal The Total Suspended Solids (TSS) levels within the pond were high which is an indicator
of poor water quality Sample locations TH2 (230 mgL) and TH3 (100 mgL) reported high TSS
levels while TH1 reported much higher levels at 730 mgL The results are likely skewed higher
as a result of the algae content in the water at the t ime of sampling As a result of the high TSS
filtration would be required should the pond need to be dewatered for future maintenance andor
clean out purposes It is also anticipated that the exceedances for the metals parameters are a
result of high TSS For dewatering purposes the water from the pond will need to be filtered prior
to entering the natural environment
Only F4 hydrocarbons were found at sediment sample location TH2 within Twickenham Pond
TH2 was found to exceed the Table 1 criteria limits but it meets the Table 3 criteria Only three
shoreline samples were able to be taken safely and feasibly this excludes the center of the pond
where more sediment accumulation could result in additional exceedances as such it cannot be
guaranteed that all other sediment within the pond meets either criteria Further sampling may
be required if the sediment is to be used on site or at a new location otherwise the sediment
should be disposed of at a registered landfill or receiving site capable of accepting Table 3
material It is expected that there will be exceedances above Table 1 criteria at other locations
within the pond due to the exceedance observed at sampling location TH2
_____________________ __ _________________________ ___
Sediment and Water Sampling Memo August 30 2019
Page 4
Based on the results of the TCLP the tested parameters meet the Ontario Regulation 558 (as
amended) for non-hazardous material and do not need to be disposed of at a hazardous waste
disposal location While the material can be brought to a commercial site to be used (as the
sample did meet Table 3 criteria limits) it is not recommended as it could create structural
limitations due to the water content within the material Significant drying and mixing would be
required to reuse the material on a site capable of accepted Table 3 material As such GEMS
recommends bringing the removed material to a landfill for disposal
This report was prepared by GEMS for TMIG as part of the Twickenham Pond Rehabilitation
Schedule B Municipal Class Environmental Assessment The report provides a summary of the
sediment and surface water conditions in Twickenham Pond Conclusions are based solely on
the collected and available information Any use by which a third party makes of this report or
any reliance on or decisions to be made based on it are the sole responsibility of such third
parties
We trust that this report will meet your current requirements Please do not hesitate to contact the undersigned should you have any questions or require additional information
Yours truly Groundwater Environmental Management Services Inc
Prepared By
Joelle Pecora BA Cert Ecol Rest Junior EcologistTechnician
Reviewed By
Kim Logan PGeo (Limited) QPESA PBiol Senior Ecologist and Project Manager
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Sediment and Water Sampling Memo August 30 2019
Page 2
In addition one (1) sediment sample from the pond was also analyzed for Toxicity Characteristic
Leaching Procedure (TCLP) for the purposes of off-site disposal as registered receivers require
the completion of this analysis prior to acceptance of any soil or sediment material
Three (3) surface water samples from the pond were taken the following parameters were analyzed
bull Surface Water Rapid Chemical Analysis Package (RCAp) Total Suspended Solids
(TSS) and Volatile Organic Compounds (VOC)s
All sample locations are shown on the figures provided in Appendix 1
Summary of Results
The following results were found within Twickenham Pond
Sediment samples were labelled TH1 TH2 and TH3 with the TCLP sample labelled TH (taken at the same location as the TH2 sediment sample)
The only reported exceedance for sediment in all three (3) sample locations was found in TH2 for F4 (C34-C50 Hydrocarbons)
The TCLP sample showed no toxic levels for any parameters within the sample Therefore the sample is considered non-hazardous
Water quality results from Twickenham Pond are also labelled as TH1 TH2 and TH3 Results were compared to both Ontario Regulation 153 and Provincial Water Quality Objectives (PWQO) exceedances were found when compared to both criteria
All sample exceedances and detections can be found in Tables 1 2 3 and 4 while the full summary of the lab results can be found in Appendix 2
Table 1 Soil Sample Exceedances
Analysis Parameter Units Criteria
1 Criteria
2 TH1 TH2 TH3
F2-F4 Hydrocarbons
F4 (C34-C50 Hydrocarbons)
ugg 120 5600 ND 140 ND
Table 2 TCLP Detections
OReg 558 TCLP Inorganics
Parameter Units Criteria TH
Inorganics Leachable Fluoride (F-) mgL 150 042
Metals Leachable Barium (Ba) mgL 100 06
Leachable Boron (B) mgL 500 02
Sediment and Water Sampling Memo August 30 2019
Page 3
Table 3 Water Quality Exceedances (OrsquoReg 15304)
Analysis Parameter Units Criteria 1 TH1 TH2 TH3
Total Copper ugL 5 13 35 16
OrsquoReg 15304 Total Lead ugL 19 51 21 059
Total Vanadium ugL 39 11 51 29
Table 4 Water Quality Exceedances (PWQO)
Analysis Parameter Units Criteria 2 TH1 TH2 TH3
PWQO
Total Phosphorus mgL 001 2 047 037
Total Cobalt ugL 09 31 12 ND
Total Copper ugL 5 13 35 16
Total Iron ugL 300 8300 2900 1100
Total Lead ugL 5 51 21 059
Total Vanadium ugL 6 11 51 29
Total Zinc ugL 30 48 88 ND
Total Suspended Solids mgL 25 730 230 100
While PWQO does not have a specific criteria for TSS the Canadian Council of Ministers of the Environment (CCME) recommend a maximum increase of 25mgL above background water quality for short-term exposure
Conclusions and Closure
The w ater quality was completed for the pu rposes of dewatering the po nd prior to any sediment
removal The Total Suspended Solids (TSS) levels within the pond were high which is an indicator
of poor water quality Sample locations TH2 (230 mgL) and TH3 (100 mgL) reported high TSS
levels while TH1 reported much higher levels at 730 mgL The results are likely skewed higher
as a result of the algae content in the water at the t ime of sampling As a result of the high TSS
filtration would be required should the pond need to be dewatered for future maintenance andor
clean out purposes It is also anticipated that the exceedances for the metals parameters are a
result of high TSS For dewatering purposes the water from the pond will need to be filtered prior
to entering the natural environment
Only F4 hydrocarbons were found at sediment sample location TH2 within Twickenham Pond
TH2 was found to exceed the Table 1 criteria limits but it meets the Table 3 criteria Only three
shoreline samples were able to be taken safely and feasibly this excludes the center of the pond
where more sediment accumulation could result in additional exceedances as such it cannot be
guaranteed that all other sediment within the pond meets either criteria Further sampling may
be required if the sediment is to be used on site or at a new location otherwise the sediment
should be disposed of at a registered landfill or receiving site capable of accepting Table 3
material It is expected that there will be exceedances above Table 1 criteria at other locations
within the pond due to the exceedance observed at sampling location TH2
_____________________ __ _________________________ ___
Sediment and Water Sampling Memo August 30 2019
Page 4
Based on the results of the TCLP the tested parameters meet the Ontario Regulation 558 (as
amended) for non-hazardous material and do not need to be disposed of at a hazardous waste
disposal location While the material can be brought to a commercial site to be used (as the
sample did meet Table 3 criteria limits) it is not recommended as it could create structural
limitations due to the water content within the material Significant drying and mixing would be
required to reuse the material on a site capable of accepted Table 3 material As such GEMS
recommends bringing the removed material to a landfill for disposal
This report was prepared by GEMS for TMIG as part of the Twickenham Pond Rehabilitation
Schedule B Municipal Class Environmental Assessment The report provides a summary of the
sediment and surface water conditions in Twickenham Pond Conclusions are based solely on
the collected and available information Any use by which a third party makes of this report or
any reliance on or decisions to be made based on it are the sole responsibility of such third
parties
We trust that this report will meet your current requirements Please do not hesitate to contact the undersigned should you have any questions or require additional information
Yours truly Groundwater Environmental Management Services Inc
Prepared By
Joelle Pecora BA Cert Ecol Rest Junior EcologistTechnician
Reviewed By
Kim Logan PGeo (Limited) QPESA PBiol Senior Ecologist and Project Manager
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Sediment and Water Sampling Memo August 30 2019
Page 3
Table 3 Water Quality Exceedances (OrsquoReg 15304)
Analysis Parameter Units Criteria 1 TH1 TH2 TH3
Total Copper ugL 5 13 35 16
OrsquoReg 15304 Total Lead ugL 19 51 21 059
Total Vanadium ugL 39 11 51 29
Table 4 Water Quality Exceedances (PWQO)
Analysis Parameter Units Criteria 2 TH1 TH2 TH3
PWQO
Total Phosphorus mgL 001 2 047 037
Total Cobalt ugL 09 31 12 ND
Total Copper ugL 5 13 35 16
Total Iron ugL 300 8300 2900 1100
Total Lead ugL 5 51 21 059
Total Vanadium ugL 6 11 51 29
Total Zinc ugL 30 48 88 ND
Total Suspended Solids mgL 25 730 230 100
While PWQO does not have a specific criteria for TSS the Canadian Council of Ministers of the Environment (CCME) recommend a maximum increase of 25mgL above background water quality for short-term exposure
Conclusions and Closure
The w ater quality was completed for the pu rposes of dewatering the po nd prior to any sediment
removal The Total Suspended Solids (TSS) levels within the pond were high which is an indicator
of poor water quality Sample locations TH2 (230 mgL) and TH3 (100 mgL) reported high TSS
levels while TH1 reported much higher levels at 730 mgL The results are likely skewed higher
as a result of the algae content in the water at the t ime of sampling As a result of the high TSS
filtration would be required should the pond need to be dewatered for future maintenance andor
clean out purposes It is also anticipated that the exceedances for the metals parameters are a
result of high TSS For dewatering purposes the water from the pond will need to be filtered prior
to entering the natural environment
Only F4 hydrocarbons were found at sediment sample location TH2 within Twickenham Pond
TH2 was found to exceed the Table 1 criteria limits but it meets the Table 3 criteria Only three
shoreline samples were able to be taken safely and feasibly this excludes the center of the pond
where more sediment accumulation could result in additional exceedances as such it cannot be
guaranteed that all other sediment within the pond meets either criteria Further sampling may
be required if the sediment is to be used on site or at a new location otherwise the sediment
should be disposed of at a registered landfill or receiving site capable of accepting Table 3
material It is expected that there will be exceedances above Table 1 criteria at other locations
within the pond due to the exceedance observed at sampling location TH2
_____________________ __ _________________________ ___
Sediment and Water Sampling Memo August 30 2019
Page 4
Based on the results of the TCLP the tested parameters meet the Ontario Regulation 558 (as
amended) for non-hazardous material and do not need to be disposed of at a hazardous waste
disposal location While the material can be brought to a commercial site to be used (as the
sample did meet Table 3 criteria limits) it is not recommended as it could create structural
limitations due to the water content within the material Significant drying and mixing would be
required to reuse the material on a site capable of accepted Table 3 material As such GEMS
recommends bringing the removed material to a landfill for disposal
This report was prepared by GEMS for TMIG as part of the Twickenham Pond Rehabilitation
Schedule B Municipal Class Environmental Assessment The report provides a summary of the
sediment and surface water conditions in Twickenham Pond Conclusions are based solely on
the collected and available information Any use by which a third party makes of this report or
any reliance on or decisions to be made based on it are the sole responsibility of such third
parties
We trust that this report will meet your current requirements Please do not hesitate to contact the undersigned should you have any questions or require additional information
Yours truly Groundwater Environmental Management Services Inc
Prepared By
Joelle Pecora BA Cert Ecol Rest Junior EcologistTechnician
Reviewed By
Kim Logan PGeo (Limited) QPESA PBiol Senior Ecologist and Project Manager
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
_____________________ __ _________________________ ___
Sediment and Water Sampling Memo August 30 2019
Page 4
Based on the results of the TCLP the tested parameters meet the Ontario Regulation 558 (as
amended) for non-hazardous material and do not need to be disposed of at a hazardous waste
disposal location While the material can be brought to a commercial site to be used (as the
sample did meet Table 3 criteria limits) it is not recommended as it could create structural
limitations due to the water content within the material Significant drying and mixing would be
required to reuse the material on a site capable of accepted Table 3 material As such GEMS
recommends bringing the removed material to a landfill for disposal
This report was prepared by GEMS for TMIG as part of the Twickenham Pond Rehabilitation
Schedule B Municipal Class Environmental Assessment The report provides a summary of the
sediment and surface water conditions in Twickenham Pond Conclusions are based solely on
the collected and available information Any use by which a third party makes of this report or
any reliance on or decisions to be made based on it are the sole responsibility of such third
parties
We trust that this report will meet your current requirements Please do not hesitate to contact the undersigned should you have any questions or require additional information
Yours truly Groundwater Environmental Management Services Inc
Prepared By
Joelle Pecora BA Cert Ecol Rest Junior EcologistTechnician
Reviewed By
Kim Logan PGeo (Limited) QPESA PBiol Senior Ecologist and Project Manager
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Appendix 1
Sample Locations
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
ll Ave
plusmn
TH1 TH2
TH3
Canyon HiClient
Groundwater Environmental Drawn By Twickenham Pond Sampling Management Services Inc Checked ByJPKL Legend ht tp wwwgemservicesinccom TMIG
Date Title Sample Locations Source Sample Locations August 2019 ial Phot
Scale Figure No Project No EMAC Drone AerNAD 1983 Zone 17N
o 0 5 10 20
Meters 1 20-202649
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Appendix 2
Laboratory Analysis ndash Soil and Surface Water Results
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Soil Samples Received 4
Date Date Analyses Quantity Extracted Analyzed Laboratory Method Reference
Methylnaphthalene Sum 3 NA 20190821 CAM SOP-00301 EPA 8270D m Hot Water Extractable Boron 3 20190817 20190819 CAM SOP-00408 R153 Ana Prot 2011 13-Dichloropropene Sum 3 NA 20190820 EPA 8260C m Free (WAD) Cyanide 2 20190816 20190819 CAM SOP-00457 OMOE E3015 m Free (WAD) Cyanide 1 20190819 20190820 CAM SOP-00457 OMOE E3015 m Cyanide (WAD) in Leachates 1 NA 20190820 CAM SOP-00457 OMOE 3015 m Conductivity 3 20190820 20190820 CAM SOP-00414 OMOE E3530 v1 m Hexavalent Chromium in Soil by IC (1) 1 20190816 20190820 CAM SOP-00436 EPA 30607199 m Hexavalent Chromium in Soil by IC (1) 2 20190819 20190820 CAM SOP-00436 EPA 30607199 m Petroleum Hydrocarbons F2-F4 in Soil (2) 3 20190817 20190818 CAM SOP-00316 CCME CWS m Fluoride by ISE in Leachates 1 20190820 20190820 CAM SOP-00449 SM 23 4500-F- C m Strong Acid Leachable Metals by ICPMS 3 20190817 20190819 CAM SOP-00447 EPA 6020B m Total Metals in TCLP Leachate by ICPMS 1 20190819 20190819 CAM SOP-00447 EPA 6020B m Moisture 3 NA 20190816 CAM SOP-00445 Carter 2nd ed 512 m Nitrate(NO3) + Nitrite(NO2) in Leachate 1 NA 20190820 CAM SOP-00440 SM 23 4500-NO3INO2B PAH Compounds in Soil by GCMS (SIM) 3 20190817 20190817 CAM SOP-00318 EPA 8270D m pH CaCl2 EXTRACT 1 20190817 20190819 CAM SOP-00413 EPA 9045 D m pH CaCl2 EXTRACT 2 20190820 20190820 CAM SOP-00413 EPA 9045 D m Sodium Adsorption Ratio (SAR) 3 NA 20190822 CAM SOP-00102 EPA 6010C TCLP - Solids 1 20190816 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Extraction Fluid 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP - Initial and final pH 1 NA 20190817 CAM SOP-00401 EPA 1311 Update I m TCLP Zero Headspace Extraction 1 20190819 20190820 CAM SOP-00430 EPA 1311 m Volatile Organic Compounds and F1 PHCs 3 NA 20190819 CAM SOP-00230 EPA 8260C m VOCs in ZHE Leachates 1 20190820 20190820 CAM SOP-00228 EPA 8260C m
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
Page 1 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859761 Version 5 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543 All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Soils are reported on a dry weight basis unless otherwise specified (2) All CCME PHC results met required criteria unless otherwise stated in the report The CWS PHC methods employed by Bureau Veritas Laboratories conform to all prescribed elements of the reference method and performance based elements have been validated All modifications have been validated and proven equivalent following ldquoAlberta Environmentrsquos Interpretation of the Reference Method for the Canada-Wide Standard for Petroleum Hydrocarbons in Soil Validation of Performance-Based Alternative Methods September 2003rdquo Documentation is available upon request Modifications from Reference Method for the Canada-wide Standard for Petroleum Hydrocarbons in Soil-Tier 1 Method F2F3F4 data reported using validated cold solvent extraction instead of Soxhlet extraction
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 10 6283251 Inorganics
Conductivity mScm 057 07 016 0002 6288679 016 0002 6288679 Moisture - - 18 10 6283805 Available (CaCl2) pH pH - - 678 6288884 WAD Cyanide (Free) ugg 0051 0051 ND 001 6284895 Chromium (VI) ugg 066 10 ND 02 6286837 Metals
Hot Water Ext Boron (B) ugg - 15 0096 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 ND 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 14 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 ND 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 60 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 20 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 30 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 32 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 31 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 ND 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 027 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
Page 3 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL485 KNL485
Sampling Date 20190815
0920 20190815
0920
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL QC Batch TH1
Lab-Dup RDL QC Batch
Acid Extractable Vanadium (V) ugg 86 86 13 50 6285799 Acid Extractable Zinc (Zn) ugg 290 340 15 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 4 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Client Project P19-464 Report Date 20190829
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Calculated Parameters
Sodium Adsorption Ratio NA 24 50 15 6283251 11 6283251 Inorganics
Conductivity mScm 057 07 019 6288679 037 0002 6288679 Moisture - - 16 6283805 27 10 6283805 Available (CaCl2) pH pH - - 754 6288884 744 6285951 WAD Cyanide (Free) ugg 0051 0051 ND 6284895 ND 001 6287313 Chromium (VI) ugg 066 10 ND 6286837 ND 02 6285097 Metals
Hot Water Ext Boron (B) ugg - 15 0085 6285828 020 0050 6285828 Acid Extractable Antimony (Sb) ugg 13 75 ND 6285799 ND 020 6285799 Acid Extractable Arsenic (As) ugg 18 18 13 6285799 10 10 6285799 Acid Extractable Barium (Ba) ugg 220 390 49 6285799 23 050 6285799 Acid Extractable Beryllium (Be) ugg 25 5 031 6285799 021 020 6285799 Acid Extractable Boron (B) ugg 36 120 ND 6285799 ND 50 6285799 Acid Extractable Cadmium (Cd) ugg 12 12 ND 6285799 ND 010 6285799 Acid Extractable Chromium (Cr) ugg 70 160 13 6285799 92 10 6285799 Acid Extractable Cobalt (Co) ugg 21 22 47 6285799 31 010 6285799 Acid Extractable Copper (Cu) ugg 92 180 95 6285799 64 050 6285799 Acid Extractable Lead (Pb) ugg 120 120 79 6285799 36 10 6285799 Acid Extractable Molybdenum (Mo) ugg 2 69 ND 6285799 ND 050 6285799 Acid Extractable Nickel (Ni) ugg 82 130 98 6285799 60 050 6285799 Acid Extractable Selenium (Se) ugg 15 24 ND 6285799 ND 050 6285799 Acid Extractable Silver (Ag) ugg 05 25 ND 6285799 ND 020 6285799 Acid Extractable Thallium (Tl) ugg 1 1 0078 6285799 0055 0050 6285799 Acid Extractable Uranium (U) ugg 25 23 039 6285799 043 0050 6285799 Acid Extractable Vanadium (V) ugg 86 86 22 6285799 19 50 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 5 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 METALS amp INORGANICS PKG (SOIL)
BV Labs ID KNL489
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Moisture - - 24 10 6283805
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
BV Labs ID KNL487 KNL489
Sampling Date 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH2 QC Batch TH3 RDL QC Batch
Acid Extractable Zinc (Zn) ugg 290 340 27 6285799 25 50 6285799 Acid Extractable Mercury (Hg) ugg 027 18 ND 6285799 ND 0050 6285799
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 6 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 PAHS (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 RDL TH3 RDL QC Batch
Calculated Parameters
Methylnaphthalene 2-(1-) ugg 059 34 ND ND 00071 ND 00071 6283128 Polyaromatic Hydrocarbons
Acenaphthene ugg 0072 58 ND ND 00050 ND 00050 6285832 Acenaphthylene ugg 0093 017 ND ND 00050 ND 00050 6285832 Anthracene ugg 016 074 ND ND 00050 ND 00050 6285832 Benzo(a)anthracene ugg 036 063 00057 00061 00050 ND (1) 0030 6285832 Benzo(a)pyrene ugg 03 03 00076 00090 00050 ND 00050 6285832 Benzo(bj)fluoranthene ugg 047 078 0015 00098 00050 ND 00050 6285832 Benzo(ghi)perylene ugg 068 78 00082 0012 00050 ND 00050 6285832 Benzo(k)fluoranthene ugg 048 078 ND ND 00050 ND 00050 6285832 Chrysene ugg 28 78 00087 ND 00050 ND 00050 6285832 Dibenz(ah)anthracene ugg 01 01 ND ND 00050 ND 00050 6285832 Fluoranthene ugg 056 069 0022 0014 00050 ND 00050 6285832 Fluorene ugg 012 69 ND ND 00050 ND 00050 6285832 Indeno(123-cd)pyrene ugg 023 048 00073 00085 00050 ND 00050 6285832 1-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 2-Methylnaphthalene ugg 059 34 ND ND 00050 ND 00050 6285832 Naphthalene ugg 009 075 ND ND 00050 ND 00050 6285832 Phenanthrene ugg 069 78 00066 00078 00050 ND 00050 6285832 Pyrene ugg 1 78 0018 0013 00050 ND 00050 6285832 Surrogate Recovery ()
D10-Anthracene - - 94 93 91 6285832 D14-Terphenyl (FS) - - 94 93 90 6285832 D8-Acenaphthylene - - 96 96 95 6285832
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected (1) DL was raised due to matrix interference
Page 7 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Calculated Parameters
13-Dichloropropene (cis+trans) ugg 005 0083 ND ND ND 0050 6283042 Volatile Organics
Acetone (2-Propanone) ugg 05 28 ND ND ND 050 6283972 Benzene ugg 002 017 ND ND ND 0020 6283972 Bromodichloromethane ugg 005 13 ND ND ND 0050 6283972 Bromoform ugg 005 026 ND ND ND 0050 6283972 Bromomethane ugg 005 005 ND ND ND 0050 6283972 Carbon Tetrachloride ugg 005 012 ND ND ND 0050 6283972 Chlorobenzene ugg 005 27 ND ND ND 0050 6283972 Chloroform ugg 005 017 ND ND ND 0050 6283972 Dibromochloromethane ugg 005 94 ND ND ND 0050 6283972 12-Dichlorobenzene ugg 005 43 ND ND ND 0050 6283972 13-Dichlorobenzene ugg 005 6 ND ND ND 0050 6283972 14-Dichlorobenzene ugg 005 0097 ND ND ND 0050 6283972 Dichlorodifluoromethane (FREON 12) ugg 005 25 ND ND ND 0050 6283972 11-Dichloroethane ugg 005 11 ND ND ND 0050 6283972 12-Dichloroethane ugg 005 005 ND ND ND 0050 6283972 11-Dichloroethylene ugg 005 005 ND ND ND 0050 6283972 cis-12-Dichloroethylene ugg 005 30 ND ND ND 0050 6283972 trans-12-Dichloroethylene ugg 005 075 ND ND ND 0050 6283972 12-Dichloropropane ugg 005 0085 ND ND ND 0050 6283972 cis-13-Dichloropropene ugg 005 0083 ND ND ND 0030 6283972 trans-13-Dichloropropene ugg 005 0083 ND ND ND 0040 6283972 Ethylbenzene ugg 005 15 ND ND ND 0020 6283972 Ethylene Dibromide ugg 005 005 ND ND ND 0050 6283972 Hexane ugg 005 34 ND ND ND 0050 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 8 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methylene Chloride(Dichloromethane) ugg 005 096 ND ND ND 0050 6283972 Methyl Ethyl Ketone (2-Butanone) ugg 05 44 ND ND ND 050 6283972 Methyl Isobutyl Ketone ugg 05 43 ND ND ND 050 6283972 Methyl t-butyl ether (MTBE) ugg 005 14 ND ND ND 0050 6283972 Styrene ugg 005 22 ND ND ND 0050 6283972 1112-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 1122-Tetrachloroethane ugg 005 005 ND ND ND 0050 6283972 Tetrachloroethylene ugg 005 23 ND ND ND 0050 6283972 Toluene ugg 02 6 ND ND ND 0020 6283972 111-Trichloroethane ugg 005 34 ND ND ND 0050 6283972 112-Trichloroethane ugg 005 005 ND ND ND 0050 6283972 Trichloroethylene ugg 005 052 ND ND ND 0050 6283972 Trichlorofluoromethane (FREON 11) ugg 025 58 ND ND ND 0050 6283972 Vinyl Chloride ugg 002 0022 ND ND ND 0020 6283972 p+m-Xylene ugg - - ND ND ND 0020 6283972 o-Xylene ugg - - ND ND ND 0020 6283972 Total Xylenes ugg 005 25 ND ND ND 0020 6283972 F1 (C6-C10) ugg 25 65 ND ND ND 10 6283972 F1 (C6-C10) - BTEX ugg 25 65 ND ND ND 10 6283972 F2-F4 Hydrocarbons
F2 (C10-C16 Hydrocarbons) ugg 10 150 ND ND ND 10 6285827 F3 (C16-C34 Hydrocarbons) ugg 240 1300 ND 68 ND 50 6285827 F4 (C34-C50 Hydrocarbons) ugg 120 5600 ND 140 ND 50 6285827 Reached Baseline at C50 ugg - - Yes No Yes 6285827 Surrogate Recovery ()
o-Terphenyl - - 94 92 90 6285827 4-Bromofluorobenzene - - 99 100 99 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil ND = Not detected
Page 9 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 153 VOCS BY HS amp F1-F4 (SOIL)
BV Labs ID KNL485 KNL487 KNL489
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
D10-o-Xylene - - 95 99 113 6283972 D4-12-Dichloroethane - - 106 105 106 6283972 D8-Toluene - - 95 95 94 6283972
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Soil - ResidentialParklandInstitutionalIndustrialCommercialCommunity Property Use Criteria-2 Ontario Reg 15304 (Amended April 15 2011) Table 3 Full Depth Generic Site Condition Standards in a Non-Potable Ground Water Condition Soil - ResidentialParklandInstitutional Property Use - Medium and Fine Textured Soil
Page 10 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP INORGANICS PACKAGE (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
Inorganics
Leachable Fluoride (F-) mgL 042 010 6289140 Leachable WAD Cyanide (Free) mgL ND 0010 6289152 Leachable Nitrite (N) mgL ND 010 6289151 Leachable Nitrate (N) mgL ND 10 6289151 Leachable Nitrate + Nitrite (N) mgL ND 10 6289151 Metals
Leachable Arsenic (As) mgL ND 02 6286668 Leachable Barium (Ba) mgL 06 02 6286668 Leachable Boron (B) mgL 02 01 6286668 Leachable Cadmium (Cd) mgL ND 005 6286668 Leachable Chromium (Cr) mgL ND 01 6286668 Leachable Lead (Pb) mgL ND 01 6286668 Leachable Mercury (Hg) mgL ND 0001 6286668 Leachable Selenium (Se) mgL ND 01 6286668 Leachable Silver (Ag) mgL ND 001 6286668 Leachable Uranium (U) mgL ND 001 6286668
RDL = Reportable Detection Limit QC Batch = Quality Control Batch ND = Not detected
Page 11 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
OREG 558 TCLP LEACHATE PREPARATION (SOIL)
BV Labs ID KNL484 KNL484
Sampling Date 20190815
0930 20190815
0930
COC Number 731714-01-01 731714-01-01
UNITS TH TH
Lab-Dup RDL QC Batch
Inorganics
Final pH pH 567 570 6284200 Initial pH pH 883 886 6284200 TCLP - Solids 100 100 02 6284021 TCLP Extraction Fluid NA FLUID 2 FLUID 2 6284024
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
OREG 558 TCLP VOLATILE ORGANICS HS (SOIL)
BV Labs ID KNL484
Sampling Date 20190815
0930
COC Number 731714-01-01
UNITS TH RDL QC Batch
ChargePrep Analysis
Amount Extracted (Wet Weight) (g) NA 25 NA 6287197 Volatile Organics
Leachable Benzene mgL ND 0020 6288814 Leachable Carbon Tetrachloride mgL ND 0020 6288814 Leachable Chlorobenzene mgL ND 0020 6288814 Leachable Chloroform mgL ND 0020 6288814 Leachable 12-Dichlorobenzene mgL ND 0050 6288814 Leachable 14-Dichlorobenzene mgL ND 0050 6288814 Leachable 12-Dichloroethane mgL ND 0050 6288814 Leachable 11-Dichloroethylene mgL ND 0020 6288814 Leachable Methylene Chloride(Dichloromethane) mgL ND 020 6288814 Leachable Methyl Ethyl Ketone (2-Butanone) mgL ND 10 6288814 Leachable Tetrachloroethylene mgL ND 0020 6288814 Leachable Trichloroethylene mgL ND 0020 6288814 Leachable Vinyl Chloride mgL ND 0020 6288814 Surrogate Recovery ()
Leachable 4-Bromofluorobenzene 96 6288814 Leachable D4-12-Dichloroethane 106 6288814 Leachable D8-Toluene 88 6288814
RDL = Reportable Detection Limit QC Batch = Quality Control Batch NA = Not Applicable ND = Not detected
Page 13 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL484 TH Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Cyanide (WAD) in Leachates SKALCN 6289152 NA 20190820 Gnana Thomas
Fluoride by ISE in Leachates ISE 6289140 20190820 20190820 Surinder Rai
Total Metals in TCLP Leachate by ICPMS ICP1MS 6286668 20190819 20190819 Prempal Bhatti
Nitrate(NO3) + Nitrite(NO2) in Leachate LACH 6289151 NA 20190820 Chandra Nandlal
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
TCLP Zero Headspace Extraction 6287197 20190819 20190820 Walt Wang
VOCs in ZHE Leachates GCMS 6288814 20190820 20190820 Blair Gannon
BV Labs ID KNL484 Dup Collected 20190815 Sample ID TH Shipped
Matrix Soil Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
TCLP - Solids BAL 6284021 20190816 20190817 Jian (Ken) Wang
TCLP - Extraction Fluid 6284024 NA 20190817 Jian (Ken) Wang
TCLP - Initial and final pH PH 6284200 NA 20190817 Jian (Ken) Wang
BV Labs ID Sample ID
Matrix
KNL485 TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL485 Dup TH1 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Conductivity
Instrumentation
AT
Batch
6288679
Extracted
20190820
Date Analyzed
20190820
Analyst
Kazzandra Adeva
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 14 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL487 TH2 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6284895 20190816 20190819 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6286837 20190819 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6288884 20190820 20190820 Surinder Rai
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Methylnaphthalene Sum CALC 6283128 NA 20190821 Automated Statchk
Hot Water Extractable Boron ICP 6285828 20190817 20190819 Archana Patel
13-Dichloropropene Sum CALC 6283042 NA 20190820 Automated Statchk
Free (WAD) Cyanide TECH 6287313 20190819 20190820 Barbara Kalbasi Esfahani
Conductivity AT 6288679 20190820 20190820 Kazzandra Adeva
Hexavalent Chromium in Soil by IC ICSPEC 6285097 20190816 20190820 Rupinder Sihota
Petroleum Hydrocarbons F2-F4 in Soil GCFID 6285827 20190817 20190818 Prabhjot Gulati
Strong Acid Leachable Metals by ICPMS ICPMS 6285799 20190817 20190819 Daniel Teclu
Moisture BAL 6283805 NA 20190816 Amitoj Singh Uppal
PAH Compounds in Soil by GCMS (SIM) GCMS 6285832 20190817 20190817 Bibin Alias Paul
pH CaCl2 EXTRACT AT 6285951 20190817 20190819 Neil Dassanayake
Sodium Adsorption Ratio (SAR) CALCMET 6283251 NA 20190822 Automated Statchk
Volatile Organic Compounds and F1 PHCs GCMSFD 6283972 NA 20190819 Denis Reid
BV Labs ID Sample ID
Matrix
KNL489 Dup TH3 Soil
Collected Shipped
Received
20190815
20190815
Test Description
Moisture
Instrumentation
BAL
Batch
6283805
Extracted
NA
Date Analyzed
20190816
Analyst
Amitoj Singh Uppal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 15 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 16 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283805 6283972
6283972
GYA DR1
DR1
RPD [KNL489-01] Matrix Spike
Spiked Blank
Moisture 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene F1 (C6-C10) 4-Bromofluorobenzene D10-o-Xylene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane
20190816 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819 20190819
12 105 129 100 104 102 85 83 96 98 85 83 83 94 86 86 89 88 85 87 87 80 86 84 85 93 79 88 86 81
100 97 77 85 92 93 84 83 87 99 87 97 90 86 82
108 105 105 99
103 73 87 86
20 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 140 60 - 130 60 - 140 60 - 140 60 - 140 60 - 130 60 - 130
Page 17 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Bromoform 20190819 96 60 - 130 Bromomethane 20190819 96 60 - 140 Carbon Tetrachloride 20190819 88 60 - 130 Chlorobenzene 20190819 84 60 - 130 Chloroform 20190819 86 60 - 130 Dibromochloromethane 20190819 95 60 - 130 12-Dichlorobenzene 20190819 88 60 - 130 13-Dichlorobenzene 20190819 89 60 - 130 14-Dichlorobenzene 20190819 93 60 - 130 Dichlorodifluoromethane (FREON 12) 20190819 92 60 - 140 11-Dichloroethane 20190819 89 60 - 130 12-Dichloroethane 20190819 88 60 - 130 11-Dichloroethylene 20190819 90 60 - 130 cis-12-Dichloroethylene 20190819 82 60 - 130 trans-12-Dichloroethylene 20190819 89 60 - 130 12-Dichloropropane 20190819 87 60 - 130 cis-13-Dichloropropene 20190819 82 60 - 130 trans-13-Dichloropropene 20190819 85 60 - 130 Ethylbenzene 20190819 80 60 - 130 Ethylene Dibromide 20190819 88 60 - 130 Hexane 20190819 89 60 - 130 Methylene Chloride(Dichloromethane) 20190819 83 60 - 130 Methyl Ethyl Ketone (2-Butanone) 20190819 77 60 - 140 Methyl Isobutyl Ketone 20190819 88 60 - 130 Methyl t-butyl ether (MTBE) 20190819 77 60 - 130 Styrene 20190819 86 60 - 130 1112-Tetrachloroethane 20190819 95 60 - 130 1122-Tetrachloroethane 20190819 91 60 - 130 Tetrachloroethylene 20190819 88 60 - 130 Toluene 20190819 85 60 - 130 111-Trichloroethane 20190819 91 60 - 130 112-Trichloroethane 20190819 92 60 - 130 Trichloroethylene 20190819 90 60 - 130 Trichlorofluoromethane (FREON 11) 20190819 100 60 - 130 Vinyl Chloride 20190819 124 60 - 130 p+m-Xylene 20190819 87 60 - 130 o-Xylene 20190819 83 60 - 130 F1 (C6-C10) 20190819 90 80 - 120
6283972 DR1 Method Blank 4-Bromofluorobenzene 20190819 101 60 - 140 D10-o-Xylene 20190819 100 60 - 130 D4-12-Dichloroethane 20190819 100 60 - 140 D8-Toluene 20190819 95 60 - 140 Acetone (2-Propanone) 20190819 ND
RDL=050 ugg
Benzene 20190819 ND RDL=0020
ugg
Bromodichloromethane 20190819 ND RDL=0050
ugg
Bromoform 20190819 ND RDL=0050
ugg
Bromomethane 20190819 ND RDL=0050
ugg
Page 18 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Carbon Tetrachloride 20190819 ND ugg RDL=0050
Chlorobenzene 20190819 ND ugg RDL=0050
Chloroform 20190819 ND ugg RDL=0050
Dibromochloromethane 20190819 ND ugg RDL=0050
12-Dichlorobenzene 20190819 ND ugg RDL=0050
13-Dichlorobenzene 20190819 ND ugg RDL=0050
14-Dichlorobenzene 20190819 ND ugg RDL=0050
Dichlorodifluoromethane (FREON 12) 20190819 ND ugg RDL=0050
11-Dichloroethane 20190819 ND ugg RDL=0050
12-Dichloroethane 20190819 ND ugg RDL=0050
11-Dichloroethylene 20190819 ND ugg RDL=0050
cis-12-Dichloroethylene 20190819 ND ugg RDL=0050
trans-12-Dichloroethylene 20190819 ND ugg RDL=0050
12-Dichloropropane 20190819 ND ugg RDL=0050
cis-13-Dichloropropene 20190819 ND ugg RDL=0030
trans-13-Dichloropropene 20190819 ND ugg RDL=0040
Ethylbenzene 20190819 ND ugg RDL=0020
Ethylene Dibromide 20190819 ND ugg RDL=0050
Hexane 20190819 ND ugg RDL=0050
Methylene Chloride(Dichloromethane) 20190819 ND ugg RDL=0050
Methyl Ethyl Ketone (2-Butanone) 20190819 ND ugg RDL=050
Methyl Isobutyl Ketone 20190819 ND ugg RDL=050
Methyl t-butyl ether (MTBE) 20190819 ND ugg RDL=0050
Styrene 20190819 ND ugg RDL=0050
1112-Tetrachloroethane 20190819 ND ugg RDL=0050
1122-Tetrachloroethane 20190819 ND ugg RDL=0050
Tetrachloroethylene 20190819 ND ugg RDL=0050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 19 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 ND ugg RDL=0020
111-Trichloroethane 20190819 ND ugg RDL=0050
112-Trichloroethane 20190819 ND ugg RDL=0050
Trichloroethylene 20190819 ND ugg RDL=0050
Trichlorofluoromethane (FREON 11) 20190819 ND ugg RDL=0050
Vinyl Chloride 20190819 ND ugg RDL=0020
p+m-Xylene 20190819 ND ugg RDL=0020
o-Xylene 20190819 ND ugg RDL=0020
Total Xylenes 20190819 ND ugg RDL=0020
F1 (C6-C10) 20190819 ND ugg RDL=10
F1 (C6-C10) - BTEX 20190819 ND ugg RDL=10
6283972 DR1 RPD Acetone (2-Propanone) 20190819 NC 50 Benzene 20190819 NC 50 Bromodichloromethane 20190819 NC 50 Bromoform 20190819 NC 50 Bromomethane 20190819 NC 50 Carbon Tetrachloride 20190819 NC 50 Chlorobenzene 20190819 NC 50 Chloroform 20190819 NC 50 Dibromochloromethane 20190819 NC 50 12-Dichlorobenzene 20190819 NC 50 13-Dichlorobenzene 20190819 NC 50 14-Dichlorobenzene 20190819 NC 50 Dichlorodifluoromethane (FREON 12) 20190819 NC 50 11-Dichloroethane 20190819 NC 50 12-Dichloroethane 20190819 NC 50 11-Dichloroethylene 20190819 NC 50 cis-12-Dichloroethylene 20190819 NC 50 trans-12-Dichloroethylene 20190819 NC 50 12-Dichloropropane 20190819 NC 50 cis-13-Dichloropropene 20190819 NC 50 trans-13-Dichloropropene 20190819 NC 50 Ethylbenzene 20190819 NC 50 Ethylene Dibromide 20190819 NC 50 Hexane 20190819 NC 50 Methylene Chloride(Dichloromethane) 20190819 NC 50 Methyl Ethyl Ketone (2-Butanone) 20190819 NC 50 Methyl Isobutyl Ketone 20190819 NC 50 Methyl t-butyl ether (MTBE) 20190819 NC 50 Styrene 20190819 NC 50 1112-Tetrachloroethane 20190819 NC 50 1122-Tetrachloroethane 20190819 NC 50 Tetrachloroethylene 20190819 NC 50
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 20 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Toluene 20190819 049 50 111-Trichloroethane 20190819 NC 50 112-Trichloroethane 20190819 NC 50 Trichloroethylene 20190819 094 50 Trichlorofluoromethane (FREON 11) 20190819 NC 50 Vinyl Chloride 20190819 NC 50 p+m-Xylene 20190819 NC 50 o-Xylene 20190819 NC 50 Total Xylenes 20190819 NC 50 F1 (C6-C10) 20190819 NC 30 F1 (C6-C10) - BTEX 20190819 NC 30
6284895 BKE Matrix Spike WAD Cyanide (Free) 20190819 82 75 - 125 6284895 BKE Spiked Blank WAD Cyanide (Free) 20190819 91 80 - 120 6284895 BKE Method Blank WAD Cyanide (Free) 20190819 ND
RDL=001 ugg
6284895 BKE RPD WAD Cyanide (Free) 20190819 38 35 6285097 RSU Matrix Spike Chromium (VI) 20190820 NC (1) 70 - 130 6285097 RSU Spiked Blank Chromium (VI) 20190820 99 80 - 120 6285097 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6285097 RSU RPD Chromium (VI) 20190820 NC 35 6285799 DT1 Matrix Spike Acid Extractable Antimony (Sb) 20190819 96 75 - 125
Acid Extractable Arsenic (As) 20190819 101 75 - 125 Acid Extractable Barium (Ba) 20190819 NC 75 - 125 Acid Extractable Beryllium (Be) 20190819 101 75 - 125 Acid Extractable Boron (B) 20190819 96 75 - 125 Acid Extractable Cadmium (Cd) 20190819 102 75 - 125 Acid Extractable Chromium (Cr) 20190819 NC 75 - 125 Acid Extractable Cobalt (Co) 20190819 98 75 - 125 Acid Extractable Copper (Cu) 20190819 96 75 - 125 Acid Extractable Lead (Pb) 20190819 NC 75 - 125 Acid Extractable Molybdenum (Mo) 20190819 102 75 - 125 Acid Extractable Nickel (Ni) 20190819 100 75 - 125 Acid Extractable Selenium (Se) 20190819 101 75 - 125 Acid Extractable Silver (Ag) 20190819 102 75 - 125 Acid Extractable Thallium (Tl) 20190819 96 75 - 125 Acid Extractable Uranium (U) 20190819 99 75 - 125 Acid Extractable Vanadium (V) 20190819 NC 75 - 125 Acid Extractable Zinc (Zn) 20190819 NC 75 - 125 Acid Extractable Mercury (Hg) 20190819 91 75 - 125
6285799 DT1 Spiked Blank Acid Extractable Antimony (Sb) 20190819 105 80 - 120 Acid Extractable Arsenic (As) 20190819 101 80 - 120 Acid Extractable Barium (Ba) 20190819 100 80 - 120 Acid Extractable Beryllium (Be) 20190819 102 80 - 120 Acid Extractable Boron (B) 20190819 101 80 - 120 Acid Extractable Cadmium (Cd) 20190819 100 80 - 120 Acid Extractable Chromium (Cr) 20190819 101 80 - 120 Acid Extractable Cobalt (Co) 20190819 101 80 - 120 Acid Extractable Copper (Cu) 20190819 100 80 - 120 Acid Extractable Lead (Pb) 20190819 104 80 - 120 Acid Extractable Molybdenum (Mo) 20190819 102 80 - 120 Acid Extractable Nickel (Ni) 20190819 100 80 - 120 Acid Extractable Selenium (Se) 20190819 106 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 21 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Silver (Ag) 20190819 103 80 - 120 Acid Extractable Thallium (Tl) 20190819 102 80 - 120 Acid Extractable Uranium (U) 20190819 103 80 - 120 Acid Extractable Vanadium (V) 20190819 100 80 - 120 Acid Extractable Zinc (Zn) 20190819 103 80 - 120 Acid Extractable Mercury (Hg) 20190819 93 80 - 120
6285799 DT1 Method Blank Acid Extractable Antimony (Sb) 20190819 ND ugg RDL=020
Acid Extractable Arsenic (As) 20190819 ND ugg RDL=10
Acid Extractable Barium (Ba) 20190819 ND ugg RDL=050
Acid Extractable Beryllium (Be) 20190819 ND ugg RDL=020
Acid Extractable Boron (B) 20190819 ND ugg RDL=50
Acid Extractable Cadmium (Cd) 20190819 ND ugg RDL=010
Acid Extractable Chromium (Cr) 20190819 ND ugg RDL=10
Acid Extractable Cobalt (Co) 20190819 ND ugg RDL=010
Acid Extractable Copper (Cu) 20190819 ND ugg RDL=050
Acid Extractable Lead (Pb) 20190819 ND ugg RDL=10
Acid Extractable Molybdenum (Mo) 20190819 ND ugg RDL=050
Acid Extractable Nickel (Ni) 20190819 ND ugg RDL=050
Acid Extractable Selenium (Se) 20190819 ND ugg RDL=050
Acid Extractable Silver (Ag) 20190819 ND ugg RDL=020
Acid Extractable Thallium (Tl) 20190819 ND ugg RDL=0050
Acid Extractable Uranium (U) 20190819 ND ugg RDL=0050
Acid Extractable Vanadium (V) 20190819 ND ugg RDL=50
Acid Extractable Zinc (Zn) 20190819 ND ugg RDL=50
Acid Extractable Mercury (Hg) 20190819 ND ugg RDL=0050
6285799 DT1 RPD Acid Extractable Antimony (Sb) 20190819 11 30 Acid Extractable Arsenic (As) 20190819 15 30 Acid Extractable Barium (Ba) 20190819 33 30 Acid Extractable Beryllium (Be) 20190819 18 30 Acid Extractable Boron (B) 20190819 41 30 Acid Extractable Cadmium (Cd) 20190819 16 30 Acid Extractable Chromium (Cr) 20190819 020 30 Acid Extractable Cobalt (Co) 20190819 60 30 Acid Extractable Copper (Cu) 20190819 48 30 Acid Extractable Lead (Pb) 20190819 0081 30
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 22 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Acid Extractable Molybdenum (Mo) 20190819 021 30 Acid Extractable Nickel (Ni) 20190819 53 30 Acid Extractable Selenium (Se) 20190819 NC 30 Acid Extractable Silver (Ag) 20190819 92 30 Acid Extractable Thallium (Tl) 20190819 11 30 Acid Extractable Uranium (U) 20190819 071 30 Acid Extractable Vanadium (V) 20190819 64 30 Acid Extractable Zinc (Zn) 20190819 56 30 Acid Extractable Mercury (Hg) 20190819 80 30
6285827 GUL Matrix Spike o-Terphenyl 20190818 91 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 92 50 - 130 F3 (C16-C34 Hydrocarbons) 20190818 82 50 - 130 F4 (C34-C50 Hydrocarbons) 20190818 84 50 - 130
6285827 GUL Spiked Blank o-Terphenyl 20190818 89 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 94 80 - 120 F3 (C16-C34 Hydrocarbons) 20190818 81 80 - 120 F4 (C34-C50 Hydrocarbons) 20190818 82 80 - 120
6285827 GUL Method Blank o-Terphenyl 20190818 96 60 - 130 F2 (C10-C16 Hydrocarbons) 20190818 ND
RDL=10 ugg
F3 (C16-C34 Hydrocarbons) 20190818 ND RDL=50
ugg
F4 (C34-C50 Hydrocarbons) 20190818 ND RDL=50
ugg
6285827 GUL RPD F2 (C10-C16 Hydrocarbons) 20190818 NC 30 F3 (C16-C34 Hydrocarbons) 20190818 NC 30 F4 (C34-C50 Hydrocarbons) 20190818 NC 30
6285828 APT Matrix Spike Hot Water Ext Boron (B) 20190819 98 75 - 125 6285828 APT Spiked Blank Hot Water Ext Boron (B) 20190819 101 75 - 125 6285828 APT Method Blank Hot Water Ext Boron (B) 20190819 ND
RDL=0050 ugg
6285828 APT RPD Hot Water Ext Boron (B) 20190819 10 40 6285832 PP4 Matrix Spike D10-Anthracene 20190817 93 50 - 130
D14-Terphenyl (FS) 20190817 88 50 - 130 D8-Acenaphthylene 20190817 79 50 - 130 Acenaphthene 20190817 91 50 - 130 Acenaphthylene 20190817 88 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 91 50 - 130 Benzo(a)pyrene 20190817 79 50 - 130 Benzo(bj)fluoranthene 20190817 83 50 - 130 Benzo(ghi)perylene 20190817 78 50 - 130 Benzo(k)fluoranthene 20190817 88 50 - 130 Chrysene 20190817 89 50 - 130 Dibenz(ah)anthracene 20190817 79 50 - 130 Fluoranthene 20190817 93 50 - 130 Fluorene 20190817 93 50 - 130 Indeno(123-cd)pyrene 20190817 84 50 - 130 1-Methylnaphthalene 20190817 99 50 - 130 2-Methylnaphthalene 20190817 88 50 - 130 Naphthalene 20190817 84 50 - 130 Phenanthrene 20190817 85 50 - 130 Pyrene 20190817 93 50 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 23 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6285832 PP4 Spiked Blank D10-Anthracene 20190817 97 50 - 130 D14-Terphenyl (FS) 20190817 94 50 - 130 D8-Acenaphthylene 20190817 89 50 - 130 Acenaphthene 20190817 92 50 - 130 Acenaphthylene 20190817 92 50 - 130 Anthracene 20190817 87 50 - 130 Benzo(a)anthracene 20190817 93 50 - 130 Benzo(a)pyrene 20190817 81 50 - 130 Benzo(bj)fluoranthene 20190817 85 50 - 130 Benzo(ghi)perylene 20190817 80 50 - 130 Benzo(k)fluoranthene 20190817 90 50 - 130 Chrysene 20190817 91 50 - 130 Dibenz(ah)anthracene 20190817 80 50 - 130 Fluoranthene 20190817 94 50 - 130 Fluorene 20190817 94 50 - 130 Indeno(123-cd)pyrene 20190817 86 50 - 130 1-Methylnaphthalene 20190817 100 50 - 130 2-Methylnaphthalene 20190817 89 50 - 130 Naphthalene 20190817 86 50 - 130 Phenanthrene 20190817 87 50 - 130 Pyrene 20190817 94 50 - 130
6285832 PP4 Method Blank D10-Anthracene 20190817 104 50 - 130 D14-Terphenyl (FS) 20190817 101 50 - 130 D8-Acenaphthylene 20190817 90 50 - 130 Acenaphthene 20190817 ND
RDL=00050 ugg
Acenaphthylene 20190817 ND RDL=00050
ugg
Anthracene 20190817 ND RDL=00050
ugg
Benzo(a)anthracene 20190817 ND RDL=00050
ugg
Benzo(a)pyrene 20190817 ND RDL=00050
ugg
Benzo(bj)fluoranthene 20190817 ND RDL=00050
ugg
Benzo(ghi)perylene 20190817 ND RDL=00050
ugg
Benzo(k)fluoranthene 20190817 ND RDL=00050
ugg
Chrysene 20190817 ND RDL=00050
ugg
Dibenz(ah)anthracene 20190817 ND RDL=00050
ugg
Fluoranthene 20190817 ND RDL=00050
ugg
Fluorene 20190817 ND RDL=00050
ugg
Indeno(123-cd)pyrene 20190817 ND RDL=00050
ugg
1-Methylnaphthalene 20190817 ND RDL=00050
ugg
2-Methylnaphthalene 20190817 ND RDL=00050
ugg
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 24 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Naphthalene 20190817 ND ugg RDL=00050
Phenanthrene 20190817 ND ugg RDL=00050
Pyrene 20190817 ND ugg RDL=00050
6285832 PP4 RPD Acenaphthene 20190817 NC 40 Acenaphthylene 20190817 NC 40 Anthracene 20190817 NC 40 Benzo(a)anthracene 20190817 NC 40 Benzo(a)pyrene 20190817 NC 40 Benzo(bj)fluoranthene 20190817 NC 40 Benzo(ghi)perylene 20190817 NC 40 Benzo(k)fluoranthene 20190817 NC 40 Chrysene 20190817 NC 40 Dibenz(ah)anthracene 20190817 NC 40 Fluoranthene 20190817 NC 40 Fluorene 20190817 NC 40 Indeno(123-cd)pyrene 20190817 NC 40 1-Methylnaphthalene 20190817 NC 40 2-Methylnaphthalene 20190817 NC 40 Naphthalene 20190817 NC 40 Phenanthrene 20190817 NC 40 Pyrene 20190817 NC 40
6285951 NYS Spiked Blank Available (CaCl2) pH 20190819 100 97 - 103 6285951 NYS RPD Available (CaCl2) pH 20190819 12 NA 6286668 PBA Matrix Spike Leachable Arsenic (As) 20190819 101 80 - 120
Leachable Barium (Ba) 20190819 NC 80 - 120 Leachable Boron (B) 20190819 100 80 - 120 Leachable Cadmium (Cd) 20190819 103 80 - 120 Leachable Chromium (Cr) 20190819 94 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 100 80 - 120 Leachable Selenium (Se) 20190819 106 80 - 120 Leachable Silver (Ag) 20190819 99 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Leachate Blank Leachable Arsenic (As) 20190819 ND mgL RDL=02
Leachable Barium (Ba) 20190819 ND mgL RDL=02
Leachable Boron (B) 20190819 ND mgL RDL=01
Leachable Cadmium (Cd) 20190819 ND mgL RDL=005
Leachable Chromium (Cr) 20190819 ND mgL RDL=01
Leachable Lead (Pb) 20190819 ND mgL RDL=01
Leachable Mercury (Hg) 20190819 ND mgL RDL=0001
Leachable Selenium (Se) 20190819 ND mgL RDL=01
Leachable Silver (Ag) 20190819 ND mgL RDL=001
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 25 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA Spiked Blank Leachable Arsenic (As) 20190819 101 80 - 120 Leachable Barium (Ba) 20190819 102 80 - 120 Leachable Boron (B) 20190819 95 80 - 120 Leachable Cadmium (Cd) 20190819 100 80 - 120 Leachable Chromium (Cr) 20190819 93 80 - 120 Leachable Lead (Pb) 20190819 95 80 - 120 Leachable Mercury (Hg) 20190819 99 80 - 120 Leachable Selenium (Se) 20190819 101 80 - 120 Leachable Silver (Ag) 20190819 98 80 - 120 Leachable Uranium (U) 20190819 95 80 - 120
6286668 PBA Method Blank Leachable Arsenic (As) 20190819 ND RDL=02
mgL
Leachable Barium (Ba) 20190819 ND RDL=02
mgL
Leachable Boron (B) 20190819 ND RDL=01
mgL
Leachable Cadmium (Cd) 20190819 ND RDL=005
mgL
Leachable Chromium (Cr) 20190819 ND RDL=01
mgL
Leachable Lead (Pb) 20190819 ND RDL=01
mgL
Leachable Mercury (Hg) 20190819 ND RDL=0001
mgL
Leachable Selenium (Se) 20190819 ND RDL=01
mgL
Leachable Silver (Ag) 20190819 ND RDL=001
mgL
Leachable Uranium (U) 20190819 ND RDL=001
mgL
6286668 PBA RPD Leachable Arsenic (As) 20190819 NC 35 Leachable Barium (Ba) 20190819 85 35 Leachable Boron (B) 20190819 58 35 Leachable Cadmium (Cd) 20190819 NC 35 Leachable Chromium (Cr) 20190819 NC 35 Leachable Lead (Pb) 20190819 NC 35 Leachable Mercury (Hg) 20190819 NC 35 Leachable Selenium (Se) 20190819 NC 35 Leachable Silver (Ag) 20190819 NC 35 Leachable Uranium (U) 20190819 NC 35
6286837 RSU Matrix Spike Chromium (VI) 20190820 18 (2) 70 - 130 6286837 RSU Spiked Blank Chromium (VI) 20190820 89 80 - 120 6286837 RSU Method Blank Chromium (VI) 20190820 ND
RDL=02 ugg
6286837 RSU RPD Chromium (VI) 20190820 NC 35 6287313 BKE Matrix Spike WAD Cyanide (Free) 20190820 98 75 - 125 6287313 BKE Spiked Blank WAD Cyanide (Free) 20190820 99 80 - 120 6287313 BKE Method Blank WAD Cyanide (Free) 20190820 ND
RDL=001 ugg
6287313 BKE RPD WAD Cyanide (Free) 20190820 NC 35 6288679 KAD Spiked Blank Conductivity 20190820 104 90 - 110
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 26 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6288679 KAD Method Blank Conductivity 20190820 ND mScm RDL=0002
6288679 KAD RPD [KNL485-01] Conductivity 20190820 16 10 6288814 BG1 Matrix Spike Leachable 4-Bromofluorobenzene 20190820 106 70 - 130
Leachable D4-12-Dichloroethane 20190820 97 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 92 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 85 70 - 130 Leachable 12-Dichlorobenzene 20190820 88 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 89 70 - 130 Leachable 11-Dichloroethylene 20190820 91 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 88 60 - 140 Leachable Tetrachloroethylene 20190820 88 70 - 130 Leachable Trichloroethylene 20190820 94 70 - 130 Leachable Vinyl Chloride 20190820 95 70 - 130
6288814 BG1 Spiked Blank Leachable 4-Bromofluorobenzene 20190820 107 70 - 130 Leachable D4-12-Dichloroethane 20190820 99 70 - 130 Leachable D8-Toluene 20190820 104 70 - 130 Leachable Benzene 20190820 88 70 - 130 Leachable Carbon Tetrachloride 20190820 89 70 - 130 Leachable Chlorobenzene 20190820 88 70 - 130 Leachable Chloroform 20190820 84 70 - 130 Leachable 12-Dichlorobenzene 20190820 89 70 - 130 Leachable 14-Dichlorobenzene 20190820 92 70 - 130 Leachable 12-Dichloroethane 20190820 91 70 - 130 Leachable 11-Dichloroethylene 20190820 90 70 - 130 Leachable Methylene Chloride(Dichloromethan 20190820 82 70 - 130 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 96 60 - 140 Leachable Tetrachloroethylene 20190820 86 70 - 130 Leachable Trichloroethylene 20190820 93 70 - 130 Leachable Vinyl Chloride 20190820 97 70 - 130
6288814 BG1 Method Blank Leachable 4-Bromofluorobenzene 20190820 95 70 - 130 Leachable D4-12-Dichloroethane 20190820 106 70 - 130 Leachable D8-Toluene 20190820 88 70 - 130 Leachable Benzene 20190820 ND mgL
RDL=0020
Leachable Carbon Tetrachloride 20190820 ND mgL RDL=0020
Leachable Chlorobenzene 20190820 ND mgL RDL=0020
Leachable Chloroform 20190820 ND mgL RDL=0020
Leachable 12-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 14-Dichlorobenzene 20190820 ND mgL RDL=0050
Leachable 12-Dichloroethane 20190820 ND mgL RDL=0050
Leachable 11-Dichloroethylene 20190820 ND mgL RDL=0020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 27 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Leachable Methylene Chloride 20190820 ND mgL (Dichloromethane) RDL=020
Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 ND mgL RDL=10
Leachable Tetrachloroethylene 20190820 ND mgL RDL=0020
Leachable Trichloroethylene 20190820 ND mgL RDL=0020
Leachable Vinyl Chloride 20190820 ND mgL RDL=0020
6288814 BG1 RPD Leachable Carbon Tetrachloride 20190820 NC 30 Leachable Chlorobenzene 20190820 NC 30 Leachable Chloroform 20190820 NC 30 Leachable 12-Dichlorobenzene 20190820 NC 30 Leachable 14-Dichlorobenzene 20190820 NC 30 Leachable 12-Dichloroethane 20190820 NC 30 Leachable 11-Dichloroethylene 20190820 NC 30 Leachable Methylene Chloride(Dichloromethan 20190820 NC 30 Leachable Methyl Ethyl Ketone (2-Butanone) 20190820 NC 30 Leachable Tetrachloroethylene 20190820 NC 30 Leachable Trichloroethylene 20190820 NC 30 Leachable Vinyl Chloride 20190820 NC 30
6288884 SAU Spiked Blank Available (CaCl2) pH 20190820 100 97 - 103 6288884 SAU RPD Available (CaCl2) pH 20190820 016 NA 6289140 SAU Matrix Spike Leachable Fluoride (F-) 20190820 93 80 - 120 6289140 SAU Leachate Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU Spiked Blank Leachable Fluoride (F-) 20190820 95 80 - 120 6289140 SAU Method Blank Leachable Fluoride (F-) 20190820 ND mgL
RDL=010
6289140 SAU RPD Leachable Fluoride (F-) 20190820 52 25 6289151 C_N Matrix Spike Leachable Nitrite (N) 20190820 106 80 - 120
Leachable Nitrate (N) 20190820 92 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 95 80 - 120
6289151 C_N Leachate Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N Spiked Blank Leachable Nitrite (N) 20190820 95 80 - 120 Leachable Nitrate (N) 20190820 100 80 - 120 Leachable Nitrate + Nitrite (N) 20190820 99 80 - 120
6289151 C_N Method Blank Leachable Nitrite (N) 20190820 ND mgL RDL=010
Leachable Nitrate (N) 20190820 ND mgL RDL=10
Leachable Nitrate + Nitrite (N) 20190820 ND mgL RDL=10
6289151 C_N RPD Leachable Nitrite (N) 20190820 NC 25 Leachable Nitrate (N) 20190820 NC 25 Leachable Nitrate + Nitrite (N) 20190820 NC 25
6289152 GTO Matrix Spike Leachable WAD Cyanide (Free) 20190820 99 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 28 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6289152 GTO Leachate Blank Leachable WAD Cyanide (Free) 20190820 ND RDL=0010
mgL
6289152 GTO Spiked Blank Leachable WAD Cyanide (Free) 20190820 108 80 - 120 6289152 GTO Method Blank Leachable WAD Cyanide (Free) 20190820 ND
RDL=00020 mgL
6289152 GTO RPD Leachable WAD Cyanide (Free) 20190820 NC 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
Leachate Blank A blank matrix containing all reagents used in the leaching procedure Used to determine any process contamination
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
(1) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
(2) The matrix spike recovery was below the lower control limit This may be due in part to the reducing environment of the sample The matrix spike was reanalyzed to confirm result
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 29 of 31
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 30 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-SoilRes Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH2 KNL487-02 F4 (C34-C50 Hydrocarbons) 120 140 50 ugg
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Reg15304 T3-SoilRes-FM Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID No Exceedences
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 31 of 31 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
Sample Matrix Water Samples Received 3
Analyses Quantity Extracted Analyzed Laboratory Method Reference
Alkalinity 2 NA 20190816 CAM SOP-00448 SM 23 2320 B m Alkalinity 1 NA 20190817 CAM SOP-00448 SM 23 2320 B m Carbonate Bicarbonate and Hydroxide 3 NA 20190819 CAM SOP-00102 APHA 4500-CO2 D Chloride by Automated Colourimetry 3 NA 20190819 CAM SOP-00463 SM 4500-Cl E m Conductivity 2 NA 20190816 CAM SOP-00414 SM 23 2510 m Conductivity 1 NA 20190817 CAM SOP-00414 SM 23 2510 m Hardness (calculated as CaCO3) 3 NA 20190822 CAM SOP SM 2340 B
001020040800447 Lab Filtered Metals Analysis by ICP 3 20190817 20190821 CAM SOP-00408 EPA 6010D m Total Metals Analysis by ICPMS 3 NA 20190820 CAM SOP-00447 EPA 6020B m Total Ammonia-N 3 NA 20190819 CAM SOP-00441 USGS I-2522-90 m Nitrate (NO3) and Nitrite (NO2) in Water (1) 3 NA 20190817 CAM SOP-00440 SM 23 4500-NO3INO2B pH 2 20190816 20190816 CAM SOP-00413 SM 4500H+ B m pH 1 20190816 20190817 CAM SOP-00413 SM 4500H+ B m Orthophosphate 3 NA 20190820 CAM SOP-00461 EPA 3651 m Sat pH and Langelier Index ( 20C) 3 NA 20190822 Sat pH and Langelier Index ( 4C) 3 NA 20190822 Sulphate by Automated Colourimetry 3 NA 20190819 CAM SOP-00464 EPA 3754 m Total Dissolved Solids (TDS calc) 3 NA 20190822 Total Organic Carbon (TOC) (2) 3 NA 20190820 CAM SOP-00446 SM 23 5310B m Total Phosphorus (Colourimetric) 3 20190819 20190819 CAM SOP-00407 SM 23 4500 P B H m Total Suspended Solids 3 20190816 20190819 CAM SOP-00428 SM 23 2540D m Turbidity 3 NA 20190816 CAM SOP-00417 SM 23 2130 B m Volatile Organic Compounds in Water 3 NA 20190817 CAM SOP-00228 EPA 8260C m
Date Date
Remarks
Bureau Veritas Laboratories are accredited to ISOIEC 17025 for specific parameters on scopes of accreditation Unless otherwise noted procedures used by BV Labs are based upon recognized Provincial Federal or US method compendia such as CCME MELCC EPA APHA
All work recorded herein has been done in accordance with procedures and practices ordinarily exercised by professionals in BV Labs profession using accepted testing methodologies quality assurance and quality control procedures (except where otherwise agreed by the client and BV Labs in writing) All
Page 1 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Your Project P19-464 Your COC 731714-01-01
Attention Kim Logan
Groundwater Environmental Management Services Inc 8800 Dufferin St Suite 303 Concord ON CANADA L4K 0C5
Report Date 20190829 Report R5859712 Version 4 - Revision
CERTIFICATE OF ANALYSIS ndash REVISED REPORT BV LABS JOB B9M6739 Received 20190815 1543
data is in statistical control and has met quality control and method performance criteria unless otherwise noted All method blanks are reported unless indicated otherwise associated sample data are not blank corrected Where applicable unless otherwise noted Measurement Uncertainty has not been accounted for when stating conformity to the referenced standard
BV Labs liability is limited to the actual cost of the requested analyses unless otherwise agreed in writing There is no other warranty expressed or implied BV Labs has been retained to provide analysis of samples provided by the Client using the testing methodology referenced in this report Interpretation and use of test results are the sole responsibility of the Client and are not within the scope of services provided by BV Labs unless otherwise agreed in writing BV Labs is not responsible for the accuracy or any data impacts that result from the information provided by the customer or their agent
Solid sample results except biota are based on dry weight unless otherwise indicated Organic analyses are not recovery corrected except for isotope dilution methods Results relate to samples tested When sampling is not conducted by BV Labs results relate to the supplied samples tested This Certificate shall not be reproduced except in full without the written approval of the laboratory Reference Method suffix ldquomrdquo indicates test methods incorporate validated modifications from specific reference methods to improve performance
RPDs calculated using raw data The rounding of final results may result in the apparent difference (1) Values for calculated parameters may not appear to add up due to rounding of raw data and significant figures (2) Total Organic Carbon (TOC) present in the sample should be considered as non-purgeable TOC
Encryption Key
Please direct all questions regarding this Certificate of Analysis to your Project Manager Jolanta Goralczyk Project Manager Email JolantaGoralczykbvlabscom Phone (905)817-5751 ==================================================================== BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Total Cover Pages 2 Page 2 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Calculated Parameters
Bicarb Alkalinity (calc as CaCO3) mgL - - 69 10 65 64 10 6283246 Calculated TDS mgL - - 300 10 280 280 10 6281853 Carb Alkalinity (calc as CaCO3) mgL - - ND 10 14 17 10 6283246 Hardness (CaCO3) mgL - - 65 10 55 56 10 6283317 Langelier Index ( 20C) NA - - -0363 -00200 00810 6282088 Langelier Index ( 4C) NA - - -0611 -0270 -0169 6282089 Saturation pH ( 20C) NA - - 828 838 837 6282088 Saturation pH ( 4C) NA - - 852 863 862 6282089 Inorganics
Total Ammonia-N mgL - - 0076 0050 ND ND 0050 6284192 Conductivity umhocm - - 570 10 550 550 10 6283837 Total Organic Carbon (TOC) mgL - - 60 050 24 30 050 6287105 Orthophosphate (P) mgL - - ND 0010 ND ND 0010 6284176 pH pH - 6585 791 836 845 6283843 Total Phosphorus mgL - 001 20 01 047 037 002 6286958 Dissolved Sulphate (SO4) mgL - - 49 10 49 32 10 6284173 Turbidity NTU - - 270 01 130 130 01 6283731 Alkalinity (Total as CaCO3) mgL - - 70 10 66 66 10 6283830 Dissolved Chloride (Cl-) mgL 790 - 130 10 120 120 10 6284166 Nitrite (N) mgL - - ND 0010 ND ND 0010 6283744 Nitrate (N) mgL - - ND 010 ND ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 20 005 16 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 37 005 34 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 3 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 89 05 84 86 05 6285868 Total Aluminum (Al) ugL - - 3800 50 1400 370 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 3 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 RDL TH2 TH3 RDL QC Batch
Total Antimony (Sb) ugL 15 20 063 050 ND ND 050 6287085 Total Arsenic (As) ugL 13 100 45 10 26 30 10 6287085 Total Barium (Ba) ugL 610 - 180 20 34 32 20 6287085 Total Beryllium (Be) ugL 05 11 ND 050 ND ND 050 6287085 Total Boron (B) ugL 1700 200 44 10 40 41 10 6287085 Total Cadmium (Cd) ugL 05 02 012 010 ND ND 010 6287085 Total Calcium (Ca) ugL - - 32000 200 40000 20000 200 6287085 Total Chromium (Cr) ugL 11 - 82 50 ND ND 50 6287085 Total Cobalt (Co) ugL 38 09 31 050 12 ND 050 6287085 Total Copper (Cu) ugL 5 5 13 10 35 16 10 6287085 Total Iron (Fe) ugL - 300 8300 100 2900 1100 100 6287085 Total Lead (Pb) ugL 19 5 51 050 21 059 050 6287085 Total Magnesium (Mg) ugL - - 7100 50 5800 4100 50 6287085 Total Manganese (Mn) ugL - - 1300 20 500 710 20 6287085 Total Molybdenum (Mo) ugL 23 40 10 050 084 093 050 6287085 Total Nickel (Ni) ugL 14 25 67 10 28 14 10 6287085 Total Potassium (K) ugL - - 5700 200 3800 3500 200 6287085 Total Selenium (Se) ugL 5 100 ND 20 ND ND 20 6287085 Total Silicon (Si) ugL - - 6300 50 3800 2100 50 6287085 Total Silver (Ag) ugL 03 01 ND 010 ND ND 010 6287085 Total Sodium (Na) ugL 490000 - 100000 100 97000 96000 100 6287085 Total Strontium (Sr) ugL - - 170 10 140 110 10 6287085 Total Thallium (Tl) ugL 05 03 ND 0050 ND ND 0050 6287085 Total Titanium (Ti) ugL - - 150 50 64 14 50 6287085 Total Vanadium (V) ugL 39 6 11 050 51 29 050 6287085 Total Zinc (Zn) ugL 160 30 48 50 88 ND 50 6287085
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 4 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RCAP - SURFACE WATER (WATER)
BV Labs ID KNL490
Sampling Date 20190815
0940
COC Number 731714-01-01
UNITS Criteria Criteria-2 TH3
Lab-Dup RDL QC Batch
Inorganics
Nitrite (N) mgL - - ND 0010 6283744 Nitrate (N) mgL - - ND 010 6283744 Metals
Dissolved Calcium (Ca) mgL - - 17 005 6285868 Dissolved Magnesium (Mg) mgL - - 35 005 6285868 Dissolved Potassium (K) mgL - - 3 1 6285868 Dissolved Sodium (Na) mgL 490 - 86 05 6285868
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Lab-Dup = Laboratory Initiated Duplicate Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 5 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
RESULTS OF ANALYSES OF WATER
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS TH1 RDL TH2 RDL TH3 RDL QC Batch
Inorganics
Total Suspended Solids mgL 730 100 230 25 100 17 6284213
RDL = Reportable Detection Limit QC Batch = Quality Control Batch
Page 6 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Volatile Organics
Acetone (2-Propanone) ugL 2700 - ND ND ND 10 6283608 Benzene ugL 05 100 ND ND ND 020 6283608 Bromodichloromethane ugL 2 200 ND ND ND 050 6283608 Bromoform ugL 50 60 ND ND ND 10 6283608 Bromomethane ugL 089 09 ND ND ND 050 6283608 Carbon Tetrachloride ugL 02 - ND ND ND 020 6283608 Chlorobenzene ugL 05 15 ND ND ND 020 6283608 Chloroform ugL 2 - ND ND ND 020 6283608 Dibromochloromethane ugL 2 40 ND ND ND 050 6283608 12-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 13-Dichlorobenzene ugL 05 25 ND ND ND 050 6283608 14-Dichlorobenzene ugL 05 4 ND ND ND 050 6283608 Dichlorodifluoromethane (FREON 12) ugL 590 - ND ND ND 10 6283608 11-Dichloroethane ugL 05 200 ND ND ND 020 6283608 12-Dichloroethane ugL 05 100 ND ND ND 050 6283608 11-Dichloroethylene ugL 05 40 ND ND ND 020 6283608 cis-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 trans-12-Dichloroethylene ugL 16 200 ND ND ND 050 6283608 12-Dichloropropane ugL 05 07 ND ND ND 020 6283608 cis-13-Dichloropropene ugL 05 - ND ND ND 030 6283608 trans-13-Dichloropropene ugL 05 7 ND ND ND 040 6283608 Ethylbenzene ugL 05 8 ND ND ND 020 6283608 Ethylene Dibromide ugL 02 5 ND ND ND 020 6283608 Hexane ugL 5 - ND ND ND 10 6283608 Methylene Chloride(Dichloromethane) ugL 5 100 ND ND ND 20 6283608 Methyl Ethyl Ketone (2-Butanone) ugL 400 400 ND ND ND 10 6283608 Methyl Isobutyl Ketone ugL 640 - ND ND ND 50 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 7 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VOLATILE ORGANICS BY GCMS (WATER)
BV Labs ID KNL486 KNL488 KNL490
Sampling Date 20190815
0920 20190815
0930 20190815
0940
COC Number 731714-01-01 731714-01-01 731714-01-01
UNITS Criteria Criteria-2 TH1 TH2 TH3 RDL QC Batch
Methyl t-butyl ether (MTBE) ugL 15 200 ND ND ND 050 6283608 Styrene ugL 05 4 ND ND ND 050 6283608 1112-Tetrachloroethane ugL 11 20 ND ND ND 050 6283608 1122-Tetrachloroethane ugL 05 70 ND ND ND 050 6283608 Tetrachloroethylene ugL 05 50 ND ND ND 020 6283608 Toluene ugL 08 08 ND ND ND 020 6283608 111-Trichloroethane ugL 05 10 ND ND ND 020 6283608 112-Trichloroethane ugL 05 800 ND ND ND 050 6283608 Trichloroethylene ugL 05 20 ND ND ND 020 6283608 Trichlorofluoromethane (FREON 11) ugL 150 - ND ND ND 050 6283608 Vinyl Chloride ugL 05 600 ND ND ND 020 6283608 p+m-Xylene ugL - 2 ND ND ND 020 6283608 o-Xylene ugL - 40 ND ND ND 020 6283608 Total Xylenes ugL 72 - ND ND ND 020 6283608 Surrogate Recovery ()
4-Bromofluorobenzene - - 93 93 93 6283608 D4-12-Dichloroethane - - 114 115 111 6283608 D8-Toluene - - 89 89 89 6283608
No Fill No Exceedance
Grey Exceeds 1 criteria policylevel
Black Exceeds both criterialevels
RDL = Reportable Detection Limit QC Batch = Quality Control Batch Criteria Ontario Reg 15304 (Amended April 15 2011) Table 1 Full Depth Background Site Condition Standards Ground Water - All Types of Property Uses Criteria-2 Ontario Provincial Water Quality Objectives Ref to MOEE Water Management document dated Feb1999 ND = Not detected
Page 8 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL486 TH1 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID Sample ID
Matrix
KNL488 TH2 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190816 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190816 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190816 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 9 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
TEST SUMMARY
BV Labs ID Sample ID
Matrix
KNL490 TH3 Water
Collected Shipped
Received
20190815
20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Alkalinity AT 6283830 NA 20190817 Surinder Rai
Carbonate Bicarbonate and Hydroxide CALC 6283246 NA 20190819 Automated Statchk
Chloride by Automated Colourimetry KONE 6284166 NA 20190819 Deonarine Ramnarine
Conductivity AT 6283837 NA 20190817 Surinder Rai
Hardness (calculated as CaCO3) 6283317 NA 20190822 Automated Statchk
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Total Metals Analysis by ICPMS ICPMS 6287085 NA 20190820 Matthew Ritenburg
Total Ammonia-N LACHNH4 6284192 NA 20190819 Mazin Wakai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
pH AT 6283843 20190816 20190817 Surinder Rai
Orthophosphate KONE 6284176 NA 20190820 Alina Dobreanu
Sat pH and Langelier Index ( 20C) CALC 6282088 NA 20190822 Automated Statchk
Sat pH and Langelier Index ( 4C) CALC 6282089 NA 20190822 Automated Statchk
Sulphate by Automated Colourimetry KONE 6284173 NA 20190819 Deonarine Ramnarine
Total Dissolved Solids (TDS calc) CALC 6281853 NA 20190822 Automated Statchk
Total Organic Carbon (TOC) TOCVNDIR 6287105 NA 20190820 Mandeep Kaur
Total Phosphorus (Colourimetric) LACHP 6286958 20190819 20190819 Nimarta Singh
Total Suspended Solids BAL 6284213 20190816 20190819 Mandeep Kaur
Turbidity AT 6283731 NA 20190816 Kazzandra Adeva
Volatile Organic Compounds in Water GCMS 6283608 NA 20190817 Blair Gannon
BV Labs ID KNL490 Dup Collected 20190815 Sample ID TH3 Shipped
Matrix Water Received 20190815
Test Description Instrumentation Batch Extracted Date Analyzed Analyst
Lab Filtered Metals Analysis by ICP ICP 6285868 20190817 20190821 Suban Kanapathippllai
Nitrate (NO3) and Nitrite (NO2) in Water LACH 6283744 NA 20190817 Amanpreet Sappal
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Page 10 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
GENERAL COMMENTS
Each temperature is the average of up to three cooler temperatures taken at receipt
Package 1 83degC
Revised Report (20190829) Split report
Revised Report (20190828) Regulatory criteria have been revised
Revised Report (20190826) Regulatory criteria have been amended as per clients request
Results relate only to the items tested
Page 11 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283608
6283608
BG1
BG1
Matrix Spike
Spiked Blank
4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene Chloroform Dibromochloromethane 12-Dichlorobenzene 13-Dichlorobenzene 14-Dichlorobenzene Dichlorodifluoromethane (FREON 12) 11-Dichloroethane 12-Dichloroethane 11-Dichloroethylene cis-12-Dichloroethylene trans-12-Dichloroethylene 12-Dichloropropane cis-13-Dichloropropene trans-13-Dichloropropene Ethylbenzene Ethylene Dibromide Hexane Methylene Chloride(Dichloromethane) Methyl Ethyl Ketone (2-Butanone) Methyl Isobutyl Ketone Methyl t-butyl ether (MTBE) Styrene 1112-Tetrachloroethane 1122-Tetrachloroethane Tetrachloroethylene Toluene 111-Trichloroethane 112-Trichloroethane Trichloroethylene Trichlorofluoromethane (FREON 11) Vinyl Chloride p+m-Xylene o-Xylene 4-Bromofluorobenzene D4-12-Dichloroethane D8-Toluene Acetone (2-Propanone) Benzene Bromodichloromethane Bromoform Bromomethane Carbon Tetrachloride Chlorobenzene
20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817 20190817
104 103 103 118 94 95
109 107 88 92 88
104 94 89 96
105 90
100 94 89 91 91 99
109 90
104 97 88
125 122 88 98 99
110 85 88 89
103 93 99
102 97 92
104 100 106 102 93 94
104 103 91 93
70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130 70 - 130 60 - 140 70 - 130 70 - 130
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 12 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Chloroform 20190817 89 70 - 130 Dibromochloromethane 20190817 102 70 - 130 12-Dichlorobenzene 20190817 93 70 - 130 13-Dichlorobenzene 20190817 91 70 - 130 14-Dichlorobenzene 20190817 98 70 - 130 Dichlorodifluoromethane (FREON 12) 20190817 111 60 - 140 11-Dichloroethane 20190817 91 70 - 130 12-Dichloroethane 20190817 97 70 - 130 11-Dichloroethylene 20190817 96 70 - 130 cis-12-Dichloroethylene 20190817 89 70 - 130 trans-12-Dichloroethylene 20190817 93 70 - 130 12-Dichloropropane 20190817 89 70 - 130 cis-13-Dichloropropene 20190817 92 70 - 130 trans-13-Dichloropropene 20190817 98 70 - 130 Ethylbenzene 20190817 91 70 - 130 Ethylene Dibromide 20190817 100 70 - 130 Hexane 20190817 100 70 - 130 Methylene Chloride(Dichloromethane) 20190817 87 70 - 130 Methyl Ethyl Ketone (2-Butanone) 20190817 110 60 - 140 Methyl Isobutyl Ketone 20190817 112 70 - 130 Methyl t-butyl ether (MTBE) 20190817 87 70 - 130 Styrene 20190817 101 70 - 130 1112-Tetrachloroethane 20190817 100 70 - 130 1122-Tetrachloroethane 20190817 104 70 - 130 Tetrachloroethylene 20190817 89 70 - 130 Toluene 20190817 89 70 - 130 111-Trichloroethane 20190817 93 70 - 130 112-Trichloroethane 20190817 100 70 - 130 Trichloroethylene 20190817 95 70 - 130 Trichlorofluoromethane (FREON 11) 20190817 103 70 - 130 Vinyl Chloride 20190817 104 70 - 130 p+m-Xylene 20190817 99 70 - 130 o-Xylene 20190817 97 70 - 130
6283608 BG1 Method Blank 4-Bromofluorobenzene 20190817 96 70 - 130 D4-12-Dichloroethane 20190817 109 70 - 130 D8-Toluene 20190817 90 70 - 130 Acetone (2-Propanone) 20190817 ND ugL
RDL=10
Benzene 20190817 ND ugL RDL=020
Bromodichloromethane 20190817 ND ugL RDL=050
Bromoform 20190817 ND ugL RDL=10
Bromomethane 20190817 ND ugL RDL=050
Carbon Tetrachloride 20190817 ND ugL RDL=020
Chlorobenzene 20190817 ND ugL RDL=020
Chloroform 20190817 ND ugL RDL=020
Dibromochloromethane 20190817 ND ugL RDL=050
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 13 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
12-Dichlorobenzene 20190817 ND ugL RDL=050
13-Dichlorobenzene 20190817 ND ugL RDL=050
14-Dichlorobenzene 20190817 ND ugL RDL=050
Dichlorodifluoromethane (FREON 12) 20190817 ND ugL RDL=10
11-Dichloroethane 20190817 ND ugL RDL=020
12-Dichloroethane 20190817 ND ugL RDL=050
11-Dichloroethylene 20190817 ND ugL RDL=020
cis-12-Dichloroethylene 20190817 ND ugL RDL=050
trans-12-Dichloroethylene 20190817 ND ugL RDL=050
12-Dichloropropane 20190817 ND ugL RDL=020
cis-13-Dichloropropene 20190817 ND ugL RDL=030
trans-13-Dichloropropene 20190817 ND ugL RDL=040
Ethylbenzene 20190817 ND ugL RDL=020
Ethylene Dibromide 20190817 ND ugL RDL=020
Hexane 20190817 ND ugL RDL=10
Methylene Chloride(Dichloromethane) 20190817 ND ugL RDL=20
Methyl Ethyl Ketone (2-Butanone) 20190817 ND ugL RDL=10
Methyl Isobutyl Ketone 20190817 ND ugL RDL=50
Methyl t-butyl ether (MTBE) 20190817 ND ugL RDL=050
Styrene 20190817 ND ugL RDL=050
1112-Tetrachloroethane 20190817 ND ugL RDL=050
1122-Tetrachloroethane 20190817 ND ugL RDL=050
Tetrachloroethylene 20190817 ND ugL RDL=020
Toluene 20190817 ND ugL RDL=020
111-Trichloroethane 20190817 ND ugL RDL=020
112-Trichloroethane 20190817 ND ugL RDL=050
Trichloroethylene 20190817 ND ugL RDL=020
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 14 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Trichlorofluoromethane (FREON 11) 20190817 ND ugL RDL=050
Vinyl Chloride 20190817 ND ugL RDL=020
p+m-Xylene 20190817 ND ugL RDL=020
o-Xylene 20190817 ND ugL RDL=020
Total Xylenes 20190817 ND ugL RDL=020
6283608 BG1 RPD Acetone (2-Propanone) 20190817 NC 30 Benzene 20190817 NC 30 Bromodichloromethane 20190817 020 30 Bromoform 20190817 NC 30 Bromomethane 20190817 NC 30 Carbon Tetrachloride 20190817 NC 30 Chlorobenzene 20190817 NC 30 Chloroform 20190817 053 30 Dibromochloromethane 20190817 42 30 12-Dichlorobenzene 20190817 NC 30 13-Dichlorobenzene 20190817 NC 30 14-Dichlorobenzene 20190817 NC 30 Dichlorodifluoromethane (FREON 12) 20190817 NC 30 11-Dichloroethane 20190817 049 30 12-Dichloroethane 20190817 NC 30 11-Dichloroethylene 20190817 079 30 cis-12-Dichloroethylene 20190817 043 30 trans-12-Dichloroethylene 20190817 NC 30 12-Dichloropropane 20190817 NC 30 cis-13-Dichloropropene 20190817 NC 30 trans-13-Dichloropropene 20190817 NC 30 Ethylbenzene 20190817 NC 30 Ethylene Dibromide 20190817 NC 30 Hexane 20190817 NC 30 Methylene Chloride(Dichloromethane) 20190817 NC 30 Methyl Ethyl Ketone (2-Butanone) 20190817 NC 30 Methyl Isobutyl Ketone 20190817 NC 30 Methyl t-butyl ether (MTBE) 20190817 NC 30 Styrene 20190817 NC 30 1112-Tetrachloroethane 20190817 NC 30 1122-Tetrachloroethane 20190817 NC 30 Tetrachloroethylene 20190817 NC 30 Toluene 20190817 12 30 111-Trichloroethane 20190817 044 30 112-Trichloroethane 20190817 NC 30 Trichloroethylene 20190817 049 30 Trichlorofluoromethane (FREON 11) 20190817 NC 30 Vinyl Chloride 20190817 NC 30 p+m-Xylene 20190817 NC 30 o-Xylene 20190817 NC 30 Total Xylenes 20190817 NC 30
6283731 KAD Spiked Blank Turbidity 20190816 95 85 - 115
Page 15 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6283731 KAD Method Blank Turbidity 20190816 ND NTU RDL=01
6283731 KAD RPD Turbidity 20190816 28 20 6283744 ASP Matrix Spike [KNL490-01] Nitrite (N) 20190817 104 80 - 120
Nitrate (N) 20190817 93 80 - 120 6283744 ASP Spiked Blank Nitrite (N) 20190817 106 80 - 120
Nitrate (N) 20190817 95 80 - 120 6283744 ASP Method Blank Nitrite (N) 20190817 ND mgL
RDL=0010
Nitrate (N) 20190817 ND mgL RDL=010
6283744 ASP RPD [KNL490-01] Nitrite (N) 20190817 NC 20 Nitrate (N) 20190817 NC 20
6283830 SAU Spiked Blank Alkalinity (Total as CaCO3) 20190816 95 85 - 115 6283830 SAU Method Blank Alkalinity (Total as CaCO3) 20190816 ND mgL
RDL=10
6283830 SAU RPD Alkalinity (Total as CaCO3) 20190816 23 20 6283837 SAU Spiked Blank Conductivity 20190816 102 85 - 115 6283837 SAU Method Blank Conductivity 20190816 ND umhocm
RDL=10
6283837 SAU RPD Conductivity 20190816 016 25 6283843 SAU Spiked Blank pH 20190816 102 98 - 103 6283843 SAU RPD pH 20190816 049 NA 6284166 DRM Matrix Spike Dissolved Chloride (Cl-) 20190819 107 80 - 120 6284166 DRM Spiked Blank Dissolved Chloride (Cl-) 20190819 104 80 - 120 6284166 DRM Method Blank Dissolved Chloride (Cl-) 20190819 ND mgL
RDL=10
6284166 DRM RPD Dissolved Chloride (Cl-) 20190819 039 20 6284173 DRM Matrix Spike Dissolved Sulphate (SO4) 20190819 114 75 - 125 6284173 DRM Spiked Blank Dissolved Sulphate (SO4) 20190819 104 80 - 120 6284173 DRM Method Blank Dissolved Sulphate (SO4) 20190819 ND mgL
RDL=10
6284173 DRM RPD Dissolved Sulphate (SO4) 20190819 51 20 6284176 ADB Matrix Spike Orthophosphate (P) 20190820 105 75 - 125 6284176 ADB Spiked Blank Orthophosphate (P) 20190820 101 80 - 120 6284176 ADB Method Blank Orthophosphate (P) 20190820 ND mgL
RDL=0010
6284176 ADB RPD Orthophosphate (P) 20190820 NC 25 6284192 MT4 Matrix Spike Total Ammonia-N 20190819 100 75 - 125 6284192 MT4 Spiked Blank Total Ammonia-N 20190819 102 80 - 120 6284192 MT4 Method Blank Total Ammonia-N 20190819 ND mgL
RDL=0050
6284192 MT4 RPD Total Ammonia-N 20190819 16 20 6284213 MKX QC Standard Total Suspended Solids 20190819 101 85 - 115 6284213 MKX Method Blank Total Suspended Solids 20190819 ND mgL
RDL=10
6284213 MKX RPD Total Suspended Solids 20190819 NC 25 6285868 SUK Matrix Spike [KNL490-01] Dissolved Calcium (Ca) 20190821 NC 80 - 120
Dissolved Magnesium (Mg) 20190821 100 80 - 120 Dissolved Potassium (K) 20190821 103 80 - 120 Dissolved Sodium (Na) 20190821 NC 80 - 120
6285868 SUK Spiked Blank Dissolved Calcium (Ca) 20190821 99 80 - 120 Dissolved Magnesium (Mg) 20190821 98 80 - 120 Dissolved Potassium (K) 20190821 101 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 16 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Dissolved Sodium (Na) 20190821 101 80 - 120 6285868 SUK Method Blank Dissolved Calcium (Ca) 20190821 ND
RDL=005 mgL
Dissolved Magnesium (Mg) 20190821 ND RDL=005
mgL
Dissolved Potassium (K) 20190821 NDRDL=1 mgL Dissolved Sodium (Na) 20190821 ND
RDL=05 mgL
6285868 SUK RPD [KNL490-01] Dissolved Calcium (Ca) 20190821 012 25 Dissolved Magnesium (Mg) 20190821 055 25 Dissolved Potassium (K) 20190821 062 25 Dissolved Sodium (Na) 20190821 025 25
6286958 NS3 Matrix Spike Total Phosphorus 20190819 NC 80 - 120 6286958 NS3 QC Standard Total Phosphorus 20190819 93 80 - 120 6286958 NS3 Spiked Blank Total Phosphorus 20190819 100 80 - 120 6286958 NS3 Method Blank Total Phosphorus 20190819 ND
RDL=0004 mgL
6286958 NS3 RPD Total Phosphorus 20190819 14 20 6287085 MRG Matrix Spike Total Aluminum (Al) 20190820 96 80 - 120
Total Antimony (Sb) 20190820 101 80 - 120 Total Arsenic (As) 20190820 98 80 - 120 Total Barium (Ba) 20190820 95 80 - 120 Total Beryllium (Be) 20190820 99 80 - 120 Total Boron (B) 20190820 92 80 - 120 Total Cadmium (Cd) 20190820 98 80 - 120 Total Calcium (Ca) 20190820 NC 80 - 120 Total Chromium (Cr) 20190820 98 80 - 120 Total Cobalt (Co) 20190820 97 80 - 120 Total Copper (Cu) 20190820 97 80 - 120 Total Iron (Fe) 20190820 100 80 - 120 Total Lead (Pb) 20190820 97 80 - 120 Total Magnesium (Mg) 20190820 99 80 - 120 Total Manganese (Mn) 20190820 96 80 - 120 Total Molybdenum (Mo) 20190820 101 80 - 120 Total Nickel (Ni) 20190820 95 80 - 120 Total Potassium (K) 20190820 98 80 - 120 Total Selenium (Se) 20190820 102 80 - 120 Total Silicon (Si) 20190820 95 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 98 80 - 120 Total Strontium (Sr) 20190820 95 80 - 120 Total Thallium (Tl) 20190820 98 80 - 120 Total Titanium (Ti) 20190820 97 80 - 120 Total Vanadium (V) 20190820 99 80 - 120 Total Zinc (Zn) 20190820 99 80 - 120
6287085 MRG Spiked Blank Total Aluminum (Al) 20190820 99 80 - 120 Total Antimony (Sb) 20190820 102 80 - 120 Total Arsenic (As) 20190820 103 80 - 120 Total Barium (Ba) 20190820 96 80 - 120 Total Beryllium (Be) 20190820 101 80 - 120 Total Boron (B) 20190820 96 80 - 120 Total Cadmium (Cd) 20190820 101 80 - 120 Total Calcium (Ca) 20190820 100 80 - 120
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 17 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Chromium (Cr) 20190820 99 80 - 120 Total Cobalt (Co) 20190820 100 80 - 120 Total Copper (Cu) 20190820 99 80 - 120 Total Iron (Fe) 20190820 103 80 - 120 Total Lead (Pb) 20190820 96 80 - 120 Total Magnesium (Mg) 20190820 104 80 - 120 Total Manganese (Mn) 20190820 100 80 - 120 Total Molybdenum (Mo) 20190820 102 80 - 120 Total Nickel (Ni) 20190820 99 80 - 120 Total Potassium (K) 20190820 100 80 - 120 Total Selenium (Se) 20190820 104 80 - 120 Total Silicon (Si) 20190820 97 80 - 120 Total Silver (Ag) 20190820 99 80 - 120 Total Sodium (Na) 20190820 103 80 - 120 Total Strontium (Sr) 20190820 99 80 - 120 Total Thallium (Tl) 20190820 97 80 - 120 Total Titanium (Ti) 20190820 90 80 - 120 Total Vanadium (V) 20190820 102 80 - 120 Total Zinc (Zn) 20190820 105 80 - 120
6287085 MRG Method Blank Total Aluminum (Al) 20190820 ND RDL=50
ugL
Total Antimony (Sb) 20190820 ND RDL=050
ugL
Total Arsenic (As) 20190820 ND RDL=10
ugL
Total Barium (Ba) 20190820 ND RDL=20
ugL
Total Beryllium (Be) 20190820 ND RDL=050
ugL
Total Boron (B) 20190820 ND RDL=10
ugL
Total Cadmium (Cd) 20190820 ND RDL=010
ugL
Total Calcium (Ca) 20190820 ND RDL=200
ugL
Total Chromium (Cr) 20190820 ND RDL=50
ugL
Total Cobalt (Co) 20190820 ND RDL=050
ugL
Total Copper (Cu) 20190820 ND RDL=10
ugL
Total Iron (Fe) 20190820 ND RDL=100
ugL
Total Lead (Pb) 20190820 ND RDL=050
ugL
Total Magnesium (Mg) 20190820 ND RDL=50
ugL
Total Manganese (Mn) 20190820 ND RDL=20
ugL
Total Molybdenum (Mo) 20190820 ND RDL=050
ugL
Total Nickel (Ni) 20190820 ND RDL=10
ugL
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
Page 18 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
Total Potassium (K) 20190820 ND ugL RDL=200
Total Selenium (Se) 20190820 ND ugL RDL=20
Total Silicon (Si) 20190820 ND ugL RDL=50
Total Silver (Ag) 20190820 ND ugL RDL=010
Total Sodium (Na) 20190820 ND ugL RDL=100
Total Strontium (Sr) 20190820 ND ugL RDL=10
Total Thallium (Tl) 20190820 ND ugL RDL=0050
Total Titanium (Ti) 20190820 ND ugL RDL=50
Total Vanadium (V) 20190820 ND ugL RDL=050
Total Zinc (Zn) 20190820 ND ugL RDL=50
6287085 MRG RPD Total Aluminum (Al) 20190820 54 20 Total Antimony (Sb) 20190820 14 20 Total Arsenic (As) 20190820 NC 20 Total Barium (Ba) 20190820 48 20 Total Beryllium (Be) 20190820 NC 20 Total Boron (B) 20190820 24 20 Total Cadmium (Cd) 20190820 54 20 Total Calcium (Ca) 20190820 25 20 Total Chromium (Cr) 20190820 NC 20 Total Cobalt (Co) 20190820 NC 20 Total Copper (Cu) 20190820 49 20 Total Iron (Fe) 20190820 NC 20 Total Lead (Pb) 20190820 12 20 Total Magnesium (Mg) 20190820 077 20 Total Manganese (Mn) 20190820 NC 20 Total Molybdenum (Mo) 20190820 23 20 Total Nickel (Ni) 20190820 36 20 Total Potassium (K) 20190820 21 20 Total Selenium (Se) 20190820 NC 20 Total Silicon (Si) 20190820 24 20 Total Silver (Ag) 20190820 NC 20 Total Sodium (Na) 20190820 26 20 Total Strontium (Sr) 20190820 43 20 Total Thallium (Tl) 20190820 NC 20 Total Titanium (Ti) 20190820 NC 20 Total Vanadium (V) 20190820 13 20 Total Zinc (Zn) 20190820 30 20
6287105 KRM Matrix Spike Total Organic Carbon (TOC) 20190820 92 80 - 120 6287105 KRM Spiked Blank Total Organic Carbon (TOC) 20190820 97 80 - 120 6287105 KRM Method Blank Total Organic Carbon (TOC) 20190820 ND mgL
RDL=050
Page 19 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
QUALITY ASSURANCE REPORT(CONTD)
QAQC Batch Init QC Type Parameter Date Analyzed Value Recovery UNITS QC Limits
6287105 KRM RPD Total Organic Carbon (TOC) 20190820 24 20
NA = Not Applicable
Duplicate Paired analysis of a separate portion of the same sample Used to evaluate the variance in the measurement
Matrix Spike A sample to which a known amount of the analyte of interest has been added Used to evaluate sample matrix interference
QC Standard A sample of known concentration prepared by an external agency under stringent conditions Used as an independent check of method accuracy
Spiked Blank A blank matrix sample to which a known amount of the analyte usually from a second source has been added Used to evaluate method accuracy
Method Blank A blank matrix containing all reagents used in the analytical procedure Used to identify laboratory contamination
Surrogate A pure or isotopically labeled compound whose behavior mirrors the analytes of interest Used to evaluate extraction efficiency
NC (Matrix Spike) The recovery in the matrix spike was not calculated The relative difference between the concentration in the parent sample and the spike amount was too small to permit a reliable recovery calculation (matrix spike concentration was less than the native sample concentration)
NC (Duplicate RPD) The duplicate RPD was not calculated The concentration in the sample andor duplicate was too low to permit a reliable RPD calculation (absolute difference lt= 2x RDL)
Page 20 of 22
Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Groundwater Environmental Management Services Inc Report Date 20190829 Client Project P19-464
VALIDATION SIGNATURE PAGE
The analytical data and all QC contained in this report were reviewed and validated by the following individual(s)
Anastassia Hamanov Scientific Specialist
BV Labs has procedures in place to guard against improper use of the electronic signature and have the required signatories as per ISOIEC 17025 signing the reports For Service Group specific validation please refer to the Validation Signature Page
Page 21 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Microbiology testing is conducted at 6660 Campobello Rd Chemistry testing is conducted at 6740 Campobello Rd
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
BV Labs Job B9M6739 Report Date 20190829
Groundwater Environmental Management Services Inc Client Project P19-464
Exceedence Summary Table ndash Reg15304 T1-GW Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Lead (Pb) 19 51 050 ugL
TH1 KNL486-04 Total Vanadium (V) 39 11 050 ugL
TH2 KNL488-04 Total Lead (Pb) 19 21 050 ugL
TH2 KNL488-04 Total Vanadium (V) 39 51 050 ugL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Exceedence Summary Table ndash Prov Water Quality Obj Result Exceedences
Units DL Result Criteria Parameter BV Labs ID Sample ID TH1 KNL486-04 Total Cobalt (Co) 09 31 050 ugL
TH1 KNL486-04 Total Copper (Cu) 5 13 10 ugL
TH1 KNL486-04 Total Iron (Fe) 300 8300 100 ugL
TH1 KNL486-04 Total Lead (Pb) 5 51 050 ugL
TH1 KNL486-03 Total Phosphorus 001 20 01 mgL
TH1 KNL486-04 Total Vanadium (V) 6 11 050 ugL
TH1 KNL486-04 Total Zinc (Zn) 30 48 50 ugL
TH2 KNL488-04 Total Cobalt (Co) 09 12 050 ugL
TH2 KNL488-04 Total Iron (Fe) 300 2900 100 ugL
TH2 KNL488-03 Total Phosphorus 001 047 002 mgL
TH3 KNL490-04 Total Iron (Fe) 300 1100 100 ugL
TH3 KNL490-03 Total Phosphorus 001 037 002 mgL
The exceedence summary table is for information purposes only and should not be considered a comprehensive listing or statement of conformance to applicable regulatory guidelines
Page 22 of 22 Bureau Veritas Laboratories 6740 Campobello Road Mississauga Ontario L5N 2L8 Tel (905) 817-5700 Toll-Free 800-563-6266 Fax (905) 817-5777 wwwbvlabscom
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-
Page 1 of 1
- Appendix D - Sediment and Water Quality Analyses
-
- GEMS - Sediment and Water Sampling Memo - Twickenham Pond
-
- Appendix 1 - Sample Locations
- Appendix 2 - Laboratory Analysis - Soil and Surface Water Results
-