true simultaneous elemental analysis … dragon_for_metals.pdf• nickel, cobalt, copper based...
TRANSCRIPT
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S8 DRAGON
Truly Simultaneous X-ray Fluorescence (XRF)
for Precise, High-speed Elemental Analysis in Metals
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19.01.2012 2
New truly simultaneous XRF S8 DRAGON
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New truly simultaneous XRF S8 DRAGON
19.01.2012 3
• Truly simultaneous XRF spectrometer combining single element channels with the new Multielement ChannelTM
• Covers almost the whole periodic table from C upwards in one run in less than 40 seconds
• 4 kW high excitation power
• Unmatched precision for all relevant elements in metal production and foundries
• Footprint more than 25% smaller compared to traditional instrument
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S8 DRAGON Multielement Channel
19.01.2012 4
• Essential Benefits of the unique Multielement Channel TM
• Elemental fingerprinting
• Identification and Analysis of all elements from Na upwards
• Analytical flexibility
• Contaminations can be traced
• Analysis of non-routine samples
• Upgrading of analytical methods with additional elements in minutes - no further installation of new hardware
• Dual-mode data acquisition
• Internal Backup for data safety with a second internal source
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19. Januar 2012 5
Simultaneous XRF Spectrometer for Metal Applications
Customer for process labs in metallurgy: Buy an analytical tool – dedicated analyzer for specific tasks: Primary focus on analytical specifications • Element list with accuracy and precision • Limited number of materials (alloy types) Second focus on reliability: • Instrument uptime • References • Service and application support • Analytical technology of no or less concern
Different Story: S8 DRAGON – focus on analytical specs S8 LION – focus on analytical technologies
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S8 DRAGON Brochure
19.01.2012 6
• Accuracy
• Example Copper based alloy with CRM and calibration
• Precision
• Example with Nickel, explanation of traditional single element channels SEC
• Detection
• Explanation of USP Multielementchannel
• Ease of use
• TouchControl
• Uptime guaranteed
• SampleCare, S8 Tools
• Teamwork
• Automation with Bruker OES
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19.01.2012 7
S8 DRAGON Applications
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Brass and Bronze
• Analysis of major elements: Fe, Ni, Co,…
• Analysis of expensive components with best precision
• Analysis of wide material ranges in combination with OES
Market price Nickel:
19.01.2012 8
S8 DRAGON Copper based alloys
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Stand. Cu(%) Pb(%) Fe(%) Sn(%) Al(%) Mn(%) Ni(%) Si(%) Zn(%)
45-343 58,87 0,45 0,42 0,042 1,73 2,13 0,073 0,63 35,676
45-361 57,85 0,47 0,39 0,053 1,58 1,96 0,15 0,6 37,049
45-378 57,82 0,72 0,38 0,063 1,61 2,01 0,169 0,57 36,639
45-381 58,39 0,59 0,19 0,067 1,05 2,12 2,09 0,3 34,832
45-388 58,32 0,63 0,1 0,055 1,1 1,96 2,43 0,061 34,985
45-393 58,79 0,67 0,08 0,043 1,02 1,87 2,46 0,084 34,534
15-059 58,27 1,83 0,089 0,1 0,028 0,024 0,035 0,011 39,998
15-060 58,74 1,69 0,085 0,094 0,018 0,016 0,03 0,011 39,798
15-151 58,12 1,84 0,087 0,091 0,006 0,005 0,027 0,002 40,204
19.01.2012 9
S8 DRAGON Copper based alloys - Calibration
• Measurement of 9 elements parallel with Single Element Channels and the Multielement Channel
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S8 DRAGON Calibration
19.01.2012 10
Single
Element
Channel
Multielement
Channel
Element Calibration Dev.
(%)
Calibration Dev.
(%)
Al 0,017 0,014
Si 0,014 0,031
Mn 0,018 0,018
Fe 0,007 0,014
Ni 0,012 0,029
Cu 0,14 0,14
Zn 0,08 0,13
Sn 0,005
Pb 0,014 0,032
Comparison of Calibration Curves :
Nickel with fixed single element channels
Mangan with Mutilelement Channel
No limitation of linear range
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S8 DRAGON Copper based alloys
19.01.2012 11
Parallel measurement in Dual Mode acquisition,
means internal backup of Single Element Channels
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S8 DRAGON Copper based alloys
19.01.2012 12
Dual Mode Acquisition:
• Elemental fingerprinting with the Multielement Channel
• Tracking of contaminations
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Cu Pb Fe Sn Al Mn Ni Si Zn
SEC SEC SEC SEC SEC SEC SEC SEC SEC
MV(%) 57,869 0,481 0,390 0,062 1,563 1,934 0,153 0,609 37,050
Abs.
Dev.
(%) 0,012 0,0005 0,0005 0,0003 0,003 0,0012 0,0004 0,0007 0,02
MultiCh MultiCh MultiCh SEC MultiCh MultiCh MultiCh MultiCh MultiCh
MV(%) 57,875 0,447 0,410 0,062 1,527 1,944 0,120 0,605 37,175
Abs.
Dev.
(%)
(%)
0,104 0,0202 0,009 0,0003 0,056 0,0207 0,0063 0,0149 0,10
19.01.2012 13
S8 DRAGON Copper based alloys
• Long term precision test for copper based alloys
• Best alignment of accuracy between both technologies
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Excellent alignment of SEC and
Multielement Channel (MEC):
• Accuracy of elements is perfectly matching customer expectations
• Precision is within the requirement of the process engineers
Unique advantages with Dual Mode Data Acquisition:
• Fingerprinting of additional elements by MEC
• Second dataset as backup for SEC
• Continuous consistency check between MEC and SEC results
19.01.2012 14
S8 DRAGON Copper based alloys
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S8 DRAGON Steel
19.01.2012 15
Elements to be analyzed: Si, P, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, As, Zr, Nb, Mo, Sn, Ta, W, Pb (19)
• Measurement time = 40s, plus handling
• Dual Mode acquisition with Multielement Channel and 15 SEC
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Mn KA1 Minor
Range: 0 – 1,2 %
RMS = 0,01%
19.01.2012 16
Steel Calibration S8 DRAGON for Mn
Mn KA1 Major
Range: 0 – 19,5 %
RMS = 0,07%
• Two ranges with automatic switch depending on intensity
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Concentration
[%]
RSM
[%]
LLD
[PPM]
Comment
Si KA1 0 – 4,1 0.056 350 Multielement
Channel
P KA1 0 – 0.1 0.004 2
Ti KA1 0 – 2.2 0,08 3
V KA1 0 – 9.7 0.15 3
Cr KA1 0 – 30 0,07 2
Mn KA1 0 – 2 0,01 3 Two ranges
0 – 20 0,07
Fe KA1 50 – 100 0,8 Multielement
Channel
Co KA1 0 – 2 0,02 2 Two ranges
0 -10 0,02
Ni KA1 0 – 6,2 0,008 2 Two ranges
0 – 35 0,06
19.01.2012 17
Precision Test for Steel 40 s measurement time - Dual Mode
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Concentration
[%]
RSM
[%]
LLD
[PPM]
Comment
Cu KA1 0 – 3,3 0,02 2
Zn KA1 0 – 0,1 0,004 16 Multielement
Channel
As KB1 0 – 0,1 0,002 6
Zr KA1 0 – 0,1 0,007 10
Nb KA1 0 – 1,1 0,01 75 Multielement
Channel
Mo KA1 0 – 0,3 0,003 1 Two ranges
0 – 3,2 0,013
Sn KA1 0 – 0,2 0,002 4
Ta LB1 0 – 0,3 0,008 12
W LA1 0 – 11 0,06 6 Two ranges
0 – 20 0,10
Pb LA1 0 – 1,1 0,009 3
19.01.2012 18
Precision Test for Steel 40 s measurement time - Dual Mode
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Raw Materials in Metal Production with the S8 DRAGON
19.01.2012 19
Mineral processing
• Iron Ore
• with the S8 DRAGON 4 kW
• Time to result:
• 56 sec per sample
• Sample throughput:
• at least 60 samples/h
• Same configuration than Steel
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Conc. Range
[%]
Calib. Std. Dev.
[%]
LOD [3s, 30s]
[ppm]
Sample
[%]
RSD. 30s
[%]
Mg 0.01 – 3.01 0.21 3 0,18 0,25
Al 0.08 – 1,3 0.05 2 0,39 0,24
Si 0.2 - 20.0 0.99 3 3,49 0,08
P 0.002 - 0.2 0.002 1 0,007 0,001
Ca 0.01 - 0.03 0.001 1 0,05 1,01
Ti 0.04 - 0.15 0.01 1 0,04 0,91
Mn 0.02 - 5.3% 0.005 2 < 2PPM n.a.
Fe Matrix - - - -
19.01.2012 20
Raw Materials in Metal Production with the S8 DRAGON
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Low alloy steel with one smart combination of SEC and Multielmentchannel:
• 19 elements in 40 s measurement time
• Excellent precision
• Best Accuracy
• Additional analysis of iron ore and slags
• Monitoring of process materials to track contaminations
19.01.2012 21
S8 DRAGON Steel
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19.01.2012 22
S8 DRAGON Technology
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S8 DRAGON Setup
19.01.2012 23
• The new S8 DRAGON spectrometers are the unique full simultaneous XRF models for the complete element range on the market with most modern technology!
Two basic configurations
• S8 DRAGON 3K
• S8 DRAGON 4K
with
• TouchControl
• SampleCare
• EasyLoad
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Up to 15 Single Element Channels plus
Multielement Channel:
Crystals
• Optimized bent crystals for each element with high resolution and sensitivity
• Individually temperature controlled
Attenuators (up to 6)
• Automated absorbers
• for high dynamic ranges
Detectors
• Proportional and Scintillation counters for optimum detection
19.01.2012 24
S8 DRAGON Single Element Channel
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S8 DRAGON The optimal solution - Less Is More
19.01.2012 25
• Best analytical performance
with max 15 channels plus
Multi Element Channel:
• Highest intensity due to most compact beam path (close coupling of tube-sample-detector)
• Stable vacuum due to small volume of sample and spectrometer chamber with pre-evacuation step
• Less channels
offer more performance
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S8 DRAGON Multielement Channel
19.01.2012 26
XFlash technology of Bruker
• 4th generation Silicon Drift Detector (SDD)
High transmission window
• Unique energy resolution
• 129 eV FWHM
• @ Mn K
• @ 100 000 cps
Unmatched count rates
• up to 300 000 cps input count rate
• up to 100 000 cps output count rate
• without resolution degradation
Peltier cooled
• Maintenance free
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S8 DRAGON TouchControl
19.01.2012 27
• Easiest operation due to intuitive touch screen interface: Three steps to accurate results
• Select sample position and application
• Enter sample ID
• Press “Measure”
• No operator training required
• Island mode: Reliable operation in rough environments (no PC)
• Unmatched Data Safety: Routine analysis is separated from advanced tasks like calibration, evaluation, and extended reporting
• Online language switch with huge selection
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S8 DRAGON SampleCare
19.01.2012 28
Accurate positioning of the sample surface:
• no tolerances in tube-to-sample distance
Pre-evacuation step:
• separation of sample and spectrometer chamber for highest vacuum stability
• Compact vacuum system
Shortest time-to-result:
• Preloading position with internal sample changer
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S8 DRAGON SampleCare
19.01.2012 29
Essential Hardware Components for precision and reliability
Tube-above-sample geometry:
• No contamination and damage of the X-ray tube window
• No damages of flow counter foils
The S8 DRAGON is not affected by:
• Sample failures
• Dust from pressed powder samples
• e.g. analyzing slag samples
Reliability by design
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Sample Handling:
Sample cups
• 8 positions stand alone
40 mm steel rings
• 12 positions stand alone
• 9 positions - ONLINE
51.5 mm steel rings
• 10 positions stand alone
• 8 positions – ONLINE
Bare samples with a diameter of
• e.g. 33 mm - (cylindric)
• Thickness: max. 30 mm
• Weight: max 500g
19.01.2012 30
S8 DRAGON EasyLoad
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Connection path
19.01.2012 31
Standalone operation in rough environments
• connection via TCP/IP for data exchange:
• 1 TCP/IP port
• 2 USB ports
Maximum uptime
• no PC with keyboard, mouse and monitor required for instrument operation
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S8 DRAGON Teamwork to Perfection
19.01.2012 32
• Automated sample transport and pickup at the back of the unit
• Interface for belt connection or robot
• Sample Magazine accessible for non routine samples from the front
• Easy and simple integration path to automated sample preparation:
• AXSCOM Interface
• TCP/IP Connection
• Link to Bruker OES
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Summary
19.01.2012 33
The S8 DRAGON delivers:
• Best accuracy
• Ultimate Precision
• Shortest time to result
… for Rapid Process Control in:
• Iron
• Steel
• Nickel, Cobalt, Copper based alloys
• Aluminum
Elemental fingerprinting
• Analytical flexibility
• Dual-mode data acquisition
• Internal Backup for data safety with a second internal source
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• Group 1: S8 DRAGON USER
• Producers of single materials: Sim-XRF for metals and Slags
• Iron and low alloy steel
• Copper
• Aluminium
• Group 2: S8 DRAGON USER
• Producers of wide range of materials: Sim-XRF plus OES for metals and evtl. slags and raw materials
• Brass
• Bronze
• high alloy steel
• Group 3: NON S8 DRAGON USER
• Producers of wide range of materials : only Sim-XRF for metals and Slags
• Stainless Steel
S8 DRAGON Sales opportunities
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• 14.3.2011 Launch of the S8 DRAGON @ PittCon
• SAP: ready, part of the M8 Konfigurator
• Brochure: printed, available for download
• Press release
• Web page ready
• Sales Platform
• Powerpoint for distribution
• 1.5.2011 AIST in US
• 16.5.2011 CETAS in D
• 27.6.2011 GIFA in D
19.01.2012 35
Roadmap
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The perfect combination of
OES and XRF for fast furnace control
The new link
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Bruker Elemental Analysis
19.01.2012 37
• Complete product portfolio for single instrumentation in
• Optical Emission Spectrometry
• Combustion Analysis
• X-ray fluorescence Spectrometry
• for metals
• Foundries
• Small metal production
• Central labs
• Commercial serice labs
• The missing piece for large companies (Thyssen, Arcelor,…) is now available:
• Twin Automation
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Bruker Solution for Fast Furnace Control
19.01.2012 38
Full Automation with
• Sample preparation
• High speed milling
• High speed grinding
• X-ray fluorescence Analysis
• Major and minor elements in less than 40 s
• Optical emission spectrometry
• Traces and light elements
• For fast furnace control
• High analytical speed
• Best precision
• Best accuracy
• Enhanced trace element
• Optimal uptime
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Bruker Automation Market
19.01.2012 39
• Be attractive for major metal producers
• Be competitive versus
• Thermo
• SMS 2000 for OES automation
• SMS 3000 and SMS 3500
for twin automation
• PANalytical + OBLF
• Teamworks
• Be Complete solution provider
• Process Labs
• Central Labs
• R&D Labs
• Service Labs
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• Solutions for
• Cast iron
• Pig iron
• low alloy steel
• high alloy steel
• Copper base
• Nickel base
• Aluminium base
• Container Lab
• Furnace control
• Close to the furnace
• Quickest feedback on the process
• Consistent analytical quality
• Reliable turn-around times
19.01.2012 40
Bruker Automation
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Q8 CORONADO
Q8 MAGELLAN
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High-end Vacuum OES Q8 MAGELLAN
19.01.2012 42
• Vacuum spectrometer with high-resolution optical system
• Optimized for demanding applications
• Latest channel photomultiplier detector technology (CPM)
• Single-spark detection up to 1000 Hz
• Time-resolved spectroscopy
• 750 mm focal length, highest spectral sensitivities, low detection limits
• Up to 128 channels
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Spark Stand for routine operation
19.01.2012 43
• Pneumatic sample holder
• Automatic electrode cleaning (optional)
• Self-centering plate
• Quick-open spark stand plate
• Newly Optimised argon flows
• Ready for automated Sample manipulation
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Typical Nitrogen Performance
19.01.2012 44
Sample 93554-10 3FE 28664 RN 14/36
1 0,0039 0,0072 0,031
2 0,0039 0,0067 0,0303
3 0,0039 0,007 0,0303
4 0,0042 0,0068 0,0297
5 0,0043 0,0077 0,0308
6 0,0038 0,007 0,0306
7 0,004 0,0068 0,0306
8 0,004 0,0069
9 0,0035 0,0071
10 0,004 0,0069
11 0,0038 0,0068
Average 0,0039 0,007 0,0305
SD 0,0002 0,0003 0,0004
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Long Term Stability of Key Elements
19.01.2012 45
0
0,5
1
1,5
2
2,5
3
3,5
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
C
Si
0
0,1
0,2
0,3
0,4
0,5
0,6
0,7
0,8
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15
Mn
P
Cr
Ni
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Q8 CORONADO Twin Automation XRF & OES
19.01.2012 46
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19.01.2012 47
Q8 CORONADO Twin Setup
S8 DRAGON
Q8 MAGELLAN
Milling Machine
Robot Cell
Container Cabin
Sample Entry
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• Double-size Container or
• Laboratory automation
• Free Q8 & S8 configuration
• Flexible workflow definitions
• Integrated backup functionalities
• One-stop shop solution
• Global sales & service coverage
• Joint BE / BAXS approach
19.01.2012 48
Automation Configuration Q8 CORONADO Twin
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19.01.2012 49
Twin-Automation XRF & OES Containerlab
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S8 LION:
• Installation at TPI Polene Thailand, first installation in Asia
• Successful trial period at Lafarge Martes France
• Order and addition to frame agreement due to better performance than Thermo 9800
• Recent orders at Cementos Yura Peru, Oriental Cement India
S8 DRAGON
• Container laboratory with OES and automation in Kalkar
• Trial period at VALE in Brazil for Iron Ore
• First Purchase Order North America at ThyssenKrupp Stainless in Calvert, AL
19.01.2012 50
Bruker AXS Simultaneous XRF
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Satisfied Bruker Users @ Holcim Sehnde
19.01.2012 51
Automation in cement plant Holcim Sehnde Germany with Herzog Sample Prep, Robot, 2 D4 ENDEAVOR, S8 TIGER and S8 LION
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Satisfied Bruker Users @ Holcim Sehnde
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