trayed distillation towers: operation, flood mechanisms ... · –punched directly from tray deck...

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Trayed Distillation Towers: Tray Types, Operation and Troubleshooting April 7, 2011 Ray Sowiak Senior Process Engineer Process Engineering Associates, LLC www.ProcessEngr.com Copyright © 2011 Process Engineering Associates, LLC. All rights reserved.

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Page 1: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Trayed Distillation Towers:

Tray Types, Operation and

Troubleshooting

April 7, 2011

Ray Sowiak

Senior Process Engineer

Process Engineering Associates, LLC

www.ProcessEngr.com

Copyright © 2011 Process Engineering Associates, LLC. All rights reserved.

Page 2: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Today‟s Topics

• Introduction: Tray Types

• Distillation Tray Operation

(Fractionation Research, Inc. (FRI) “Film A”)

• Tray Flooding Mechanisms

• Troubleshooting Trayed Tower Flood

• Multipass Flow Balance

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Page 3: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Introduction:

Conventional Tray Types

• Movable or “Floating” Valve

• Fixed Valve

• Sieve

• Bubble Cap

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Page 4: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

V-1 & V-1X Valves

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Page 5: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

“Leg-Type” Moveable Valves

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Page 6: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Rectangular “Float” Valves

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Page 7: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Moveable Valve Characteristics

• Excellent capacity, especially at low pressures

• Very good turndown, valves mitigate “weeping”

• Not recommended in fouling/coking services

• “Tabs” or “dimples” prevent flush seating; valves without these are not recommended

• Valve units can have various thicknesses, typically 16 to 10 gauge

• Use of dual valve weights on a given tray said to improve turndown; usually in pairs of rows

• For rectangular valves, dimples must be on downstream side

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Page 8: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

“ProValve” Fixed Valves

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Page 9: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

VG-0 Deck w/ VG-9 “Push” Valves

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Page 10: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Fixed Valve Characteristics

• Fixed valve trays sacrifice some turndown

flexibility for enhanced fouling resistance

• Two types:

– Punched directly from tray deck (e.g. VG-0, SVG)

– Separate cap piece over a deck orifice (ProValve)

• Better capacity in low pressure services than

equivalent hole size sieve trays

• Most fixed valve types are directional; attention

must be paid during installation

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Page 11: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Sieve Tray

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Page 12: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Sieve Tray Characteristics

• Simple and relatively inexpensive!

• Good efficiency

• 2:1 turndown at low pressures; 3:1 turndown at

higher pressures

• Larger hole sizes (1 to 1½") can be very fouling

resistant

• Very easy to clean when fouled

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Page 13: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Slotted Bubble Cap

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Page 14: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

FRI “Standard” Bubble Cap

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Page 15: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

“Tunnel Caps”

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Page 16: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Bubble Cap Characteristics

• Great performance at low liquid rates, even with

high vapor rates

• Can be turned down to very low vapor rate

without loss of efficiency

• Poor performance at high liquid rates due to

hydraulic gradient

• Reasonable resistance to fouling, but hard to

clean!

• Expensive

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Page 17: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Tray Operation: • A few things to look for:

– Flow regimes (spray, mixed, froth ≡ bubbly)

– Tray flood by “massive entrainment” (jet flood)

– Downcomer backup flood

– Downcomer entrance flood (choke)

– Flood by System Limitation

– Weeping & dumping

• Trays without downcomers (a.k.a “Dual-flow”) – not

typically used in refining

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Page 18: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Four Tray Flood Mechanisms

• Jet flood (entrainment)

• Downcomer flood by backup

• Downcomer top choke

• System limit

• All of these are aggravated by foaming

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Page 19: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Jet Flood (Mech #1)

• Jet flood occurs when the spray or froth reaches

the tray above and liquid is aspirated wholesale

through the vapor-handling elements

• Also known as „entrainment flood‟

• Tends to occur at low pressures (<50 psig)

• Tray efficiency drops as jet flood is approached

and entrainment picks up

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Page 20: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Efficiency Drop with Entrainment

(Vapor Rate)

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Page 21: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Downcomer Flood (Mech #2)

• Downcomer flood occurs when aerated liquid fills the downcomer and begins backing up onto the tray deck

• Flood can be sudden: tray efficiency is generally not affected as downcomer flood is approached (some cases do show an effic. drop caused by vapor undercarry)

• Downcomer backup is not linear with fluid rates – it increases approx. with the square of rate

• Downcomer flood tends to occur at high liquid rates, e.g. at high pressures

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Page 22: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Downcomer Flood: DC Full of Froth

Downcomer backs up to top of

weir due to a combination of

• Tray pressure drop

• Insufficient disengaging volume

• Head loss thru exit opening

causing fluid friction between

liquid & bubbles or against walls

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Page 23: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Downcomer Choke (Mech #3)

• Downcomer choke occurs when there is not

enough area at the top to admit the frothy liquid

while disengaged vapor is trying to escape

• Like downcomer backup flood, choke occurs

suddenly and without an efficiency drop

• Like backup flood, choke tends to occur at high

liquid rates and high pressures

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Page 24: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

System Limit (Mech #4)

• System limit is the inability of liquid droplets to

fall via gravity in the upflowing vapor stream

• System limit capacity is dictated by fluid rates

and properties. When system limit is controlling,

changes to the active element type or size do

not increase capacity

• System limit tends to govern at high pressures

(>150 psig) and at low pressures (<10 psig)

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Page 25: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

System Limit Flow Pattern

Many of the smaller

droplets cannot fall in the

rising vapor, and are

carried upward

The vapor can even shear

some of the larger droplets

into smaller ones

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Page 26: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Troubleshooting Flooded Towers Basic Questions to Ask

• Start with operating data for a flooding event

– Where is pressure drop before onset of flood?

– Is there a loss in separation before flood occurs?

– Do you believe your instrumentation?

– Did the flooding begin one day (e.g. after upset)?

– Is water getting into your hydrocarbon system?

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Page 27: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Tray Pressure Drop Approaching Jet Flood

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Page 28: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Jet or Downcomer Flood?

• Jet Flood

– As you approach flood, efficiency falls off

– Pressure drop builds

• Downcomer Flood

– Tower floods suddenly, unexpectedly

– No decrease in efficiency or buildup of ΔP before

flood

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Page 29: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Further Troubleshooting Checks

• Do tray ratings – this requires a reasonably well-

matched simulation (for loads & properties)

• Try to get gamma scans at incipient flood

• Better: gamma scans and tray ratings

– Ratings can support or downplay observations

from the gamma scan

– Gamma scan data and rating results can be

assesed alongside operating behaviors for a

multi-faceted view of the problem

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Page 30: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Gamma Scan Lines – Active Area

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Page 31: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Gamma Scan – Well Behaved Tower

Increasing Relative Density

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Page 32: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Gamma Scan – Heavy Entrainment

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Page 33: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Gamma Scan – Foaming

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Page 34: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Multipass Tray Flow Balance

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Page 35: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Flow Splits by ΔP and Weir Load

• Panels act in pairs

• ΔP of panels A+C

must equal B+D

• Weir load affects

liquid hold-up (crest)

• Imbalance in the

flow splits can lead to

premature flood

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Page 36: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

What‟s Wrong with this Tray?

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Page 37: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

Picket Weir at Center Downcomer

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Page 38: Trayed Distillation Towers: Operation, Flood Mechanisms ... · –Punched directly from tray deck ... Bubble Cap Characteristics ... and properties. When system limit is controlling,

How Picket Weirs Work

• Picket weirs increase liquid holdup on tray

• Affect Entrainment

– Greater liquid inventory increases breakup of

vapor jets issuing from active elements

– Breakup of vapor eddies reduces droplet carry-up

(entrainment)

• Affect Pressure Drop

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