----middot---middotshy - -----shy-------shy

JIIC

ab

30 1986 Pile 11o a~ost oe-c

Silreaia Site ruatbull ~at Office ~ 1 Acton Kaaaacbuaetta 01720

ampttutiona llr Ja ampogera

ba aurelia lllPS aorbeDt tube aapllng at cap venta

GeDU-Da

lD accordance wltb a requeat by tbe 08 bullbullamp in a letter 4ate4 January 28 1116 GIA baa prepared tbe following outline of a propoae4 air bullent aorbent tube aapllng progr for tbe Bllria alte

( SILRBSIJI VBRl SMPLIRG

The data collected by the weekly vent monitoring using the B-Nu Model PI-101 Photoionizer and the Century OVA-128 Organic Vapor Analyzer will be supplemented by aorbent tube sampling and analysis The sorbent tube analysis will identify the contaminants and quantify their respective concentrations at the

middotmiddot--middotmiddotmiddottime - o~ year -when worat _case bull conditions _ar_e _exp_ecte~--shy(ie optimized volatilization with minimum atmosphericdispersion) GZA will identify the contaminants exiting in the

middot vents and quantify the vent emissions at the three vents containing the highest concentration of contaminants as determined by previous B-Nu and OVA monitoring data The procedure is discussed in detail below

The emissions from air vent 4 will be sampled using a mixed media aorbent tube and analyzed for positive identification The aorbent tube will include 50 mg of each of the followingaorbents

Activated charcoal lenax-GC Silica-gelCbrcmoaorb 101

Samples will be collected using a Gilian Model 113A OT air sampling pump pre-calibrated at 50 ccminute Samples will be collected for four hours yielding a sample volume of 12 litera

Analysis will include thermal desorption into a Finnegan 4021 GCMS with an SP-1000 analytical column The GCMS system will profile th iaaiona but will not giv quantitative data A clescription of the methodology and laboratory quality control data is includ d in aa an attachment

Quantification of tb iaaions from air vent 4 will be don bycollecting a parallel aampl on tand 600 mg activated charcoal tubes using tb e as pling criteria as d scribed above tor the GCMS profile s ple

t

d aorbed with purified carbon disulfide interterenc ) and analysed by Go-rto The the analysis ia co pound d pend nt but A ll-liter sampl olua will yield the ct bl airborne cone ntrations tor benz n

I I

~ I I

I I I

~ I

The previous vent sampling round using the Century OVA-128 indicated the presence of the similar components across a wide range of concentrations GZA will quantitatively analyze the three vents with the highestmiddot observed concentration of vocs

After the profiling and quantification of Vent 4 is completed Vents 6 and 7 will be sampled with tandem 400 mg Tenax thermal I desotpt~on _tubes _ The therm~l _desor~tion tu~es wil~ _ be__des~rbed

by a Foxboro PTD Programmed Thermal Desorber and syringeinjections made into a Hewlett-Packard 3890A Gas Chromatographequipped with a flame ionization detector The analyticalcolumn is a fused silica capillary column 30 m x 053 mm coated with a 265 um thic~ crosslinked methyl silicone gum phase This particular column provides the chemical inertness of fused silica and the sample capacity approaching packed columna which is useful when making gas injections Multiple injections can be made to verify analytical data and optimize GC conditions (ifnecessary)

As in the sampling of Vent 4 the sample volume will be approximately 12 liters with a flow rate of 50 cominute The minimum detectable airborne concentrations for benzene toluene and xylenes based on a splitless injection are as followaa

I

i Benzene oos ppmToluene 004 ppmXylene a 004 ppm

The B-Nu Model PI-101 Photoionizer and the Century OVA-128 Organic Vapor Analyzer will also be used during the aabullplinground Measurements will be bullade at the vent opening and at a distance of 1 foot downwind of the vent both b fore and after the sorbent sampling

A portable bulleteorological monitoring station will be pr sent on-site which will continuously record on chart paper temperatures wind speed and wind direction Barca tric pressurewill be r corded by an on-site barom ter and r lativ humidity by a sling-psychrometer at hourly intervals

2

]gt()OH ~r HO Zl11 H() ()H -tJ 0 ])0-tJ Hl11 lt3 f11H

n 0])111r n on 00 00

-- middotmiddot---- ( shy

-----middot--middot-middot---middotshymiddot APR 1986 ~

Gu ChTCCIIItosrphYIMul SpectraMtry CCIIIS) hIMteiS

Chp1ce or col-n and opersUna CDDd1Uoaa dependent upon a-pounds or 1ntereat

~linamp packed col-n 11 SP 1000 oo 60110 Cabopack I 11 10 a l4bull

TbullperatuN Prosrbull

lletttocl lequence 1 Col TbullPbull 55-c 1M 10 aiD Squerice 2 Col Tap 200-c late eobullc1a1n Sequence 3 Col Tap 200-c lSIIe 999 bold tor 1400 acana

MaxiJIB tperatu1e 210bullt lDjectpr 210bullt Separator 235bullt

I Manifold eobull--goec Cabould Dtver exceed wa tperatuN Vb1le 1D openUoo)

carrier Bel1B now Rate 25-30 alla1Dute lit mdertlow lilbt appeera dur1Damp nm reduce DPeNtiDI flow amW UDCIIIflow iadicator

DO loopr 1ilbta) middot Scope c Scope aode Data SJS shyMode EI-SEP Electron tneru 70V llliuioo Current 050shyScan Rate 3S350 Mil (ltcaic ttau UDita) Jb1a MJ

dependilll upoo aoleaalll veilbta or ccapouDdl ot inteNSt UP 195 HC l)(IIR ooo

Bold l1M TOP 000 10nCI4 005 MCo

Cbeck blcJcamp10Und before beampinniftamp aalJaibull ot -pta

acqmre a calibration tor worlc1albull~ Nail st MCUUJmiddot

lple PNpUon

1 Precl aWDl steel traps wUb -p a Men middot c 2ll fl=ial shy ~-~lal

J Attach a clHn epty trap to bt u~a1 middot-rluon into tbt t1QS Wodc

) raquo1v rt t bell flow ttumiddot~h U and 5 na Tbt ~ oven ahOIlG be cool a 1 tht tnP to tht ataoaphe bull

lHII OHzr HO ZITI H(1 (IH-z 0 ~n-x HITI ltI ITIH

n 0~ 111r n on 00 00

0

( SILRBSIJI VBRl SMPLIRG

The data collected by the weekly vent monitoring using the B-Nu Model PI-101 Photoionizer and the Century OVA-128 Organic Vapor Analyzer will be supplemented by aorbent tube sampling and analysis The sorbent tube analysis will identify the contaminants and quantify their respective concentrations at the

middotmiddot--middotmiddotmiddottime - o~ year -when worat _case bull conditions _ar_e _exp_ecte~--shy(ie optimized volatilization with minimum atmosphericdispersion) GZA will identify the contaminants exiting in the

middot vents and quantify the vent emissions at the three vents containing the highest concentration of contaminants as determined by previous B-Nu and OVA monitoring data The procedure is discussed in detail below

The emissions from air vent 4 will be sampled using a mixed media aorbent tube and analyzed for positive identification The aorbent tube will include 50 mg of each of the followingaorbents

Activated charcoal lenax-GC Silica-gelCbrcmoaorb 101

Samples will be collected using a Gilian Model 113A OT air sampling pump pre-calibrated at 50 ccminute Samples will be collected for four hours yielding a sample volume of 12 litera

Analysis will include thermal desorption into a Finnegan 4021 GCMS with an SP-1000 analytical column The GCMS system will profile th iaaiona but will not giv quantitative data A clescription of the methodology and laboratory quality control data is includ d in aa an attachment

Quantification of tb iaaions from air vent 4 will be don bycollecting a parallel aampl on tand 600 mg activated charcoal tubes using tb e as pling criteria as d scribed above tor the GCMS profile s ple

t

d aorbed with purified carbon disulfide interterenc ) and analysed by Go-rto The the analysis ia co pound d pend nt but A ll-liter sampl olua will yield the ct bl airborne cone ntrations tor benz n

I I

~ I I

I I I

~ I

The previous vent sampling round using the Century OVA-128 indicated the presence of the similar components across a wide range of concentrations GZA will quantitatively analyze the three vents with the highestmiddot observed concentration of vocs

After the profiling and quantification of Vent 4 is completed Vents 6 and 7 will be sampled with tandem 400 mg Tenax thermal I desotpt~on _tubes _ The therm~l _desor~tion tu~es wil~ _ be__des~rbed

by a Foxboro PTD Programmed Thermal Desorber and syringeinjections made into a Hewlett-Packard 3890A Gas Chromatographequipped with a flame ionization detector The analyticalcolumn is a fused silica capillary column 30 m x 053 mm coated with a 265 um thic~ crosslinked methyl silicone gum phase This particular column provides the chemical inertness of fused silica and the sample capacity approaching packed columna which is useful when making gas injections Multiple injections can be made to verify analytical data and optimize GC conditions (ifnecessary)

As in the sampling of Vent 4 the sample volume will be approximately 12 liters with a flow rate of 50 cominute The minimum detectable airborne concentrations for benzene toluene and xylenes based on a splitless injection are as followaa

I

i Benzene oos ppmToluene 004 ppmXylene a 004 ppm

The B-Nu Model PI-101 Photoionizer and the Century OVA-128 Organic Vapor Analyzer will also be used during the aabullplinground Measurements will be bullade at the vent opening and at a distance of 1 foot downwind of the vent both b fore and after the sorbent sampling

A portable bulleteorological monitoring station will be pr sent on-site which will continuously record on chart paper temperatures wind speed and wind direction Barca tric pressurewill be r corded by an on-site barom ter and r lativ humidity by a sling-psychrometer at hourly intervals

2

]gt()OH ~r HO Zl11 H() ()H -tJ 0 ])0-tJ Hl11 lt3 f11H

n 0])111r n on 00 00

-- middotmiddot---- ( shy

-----middot--middot-middot---middotshymiddot APR 1986 ~

Gu ChTCCIIItosrphYIMul SpectraMtry CCIIIS) hIMteiS

Chp1ce or col-n and opersUna CDDd1Uoaa dependent upon a-pounds or 1ntereat

~linamp packed col-n 11 SP 1000 oo 60110 Cabopack I 11 10 a l4bull

TbullperatuN Prosrbull

lletttocl lequence 1 Col TbullPbull 55-c 1M 10 aiD Squerice 2 Col Tap 200-c late eobullc1a1n Sequence 3 Col Tap 200-c lSIIe 999 bold tor 1400 acana

MaxiJIB tperatu1e 210bullt lDjectpr 210bullt Separator 235bullt

I Manifold eobull--goec Cabould Dtver exceed wa tperatuN Vb1le 1D openUoo)

carrier Bel1B now Rate 25-30 alla1Dute lit mdertlow lilbt appeera dur1Damp nm reduce DPeNtiDI flow amW UDCIIIflow iadicator

DO loopr 1ilbta) middot Scope c Scope aode Data SJS shyMode EI-SEP Electron tneru 70V llliuioo Current 050shyScan Rate 3S350 Mil (ltcaic ttau UDita) Jb1a MJ

dependilll upoo aoleaalll veilbta or ccapouDdl ot inteNSt UP 195 HC l)(IIR ooo

Bold l1M TOP 000 10nCI4 005 MCo

Cbeck blcJcamp10Und before beampinniftamp aalJaibull ot -pta

acqmre a calibration tor worlc1albull~ Nail st MCUUJmiddot

lple PNpUon

1 Precl aWDl steel traps wUb -p a Men middot c 2ll fl=ial shy ~-~lal

J Attach a clHn epty trap to bt u~a1 middot-rluon into tbt t1QS Wodc

) raquo1v rt t bell flow ttumiddot~h U and 5 na Tbt ~ oven ahOIlG be cool a 1 tht tnP to tht ataoaphe bull

lHII OHzr HO ZITI H(1 (IH-z 0 ~n-x HITI ltI ITIH

n 0~ 111r n on 00 00

0

I I I

~ I

The previous vent sampling round using the Century OVA-128 indicated the presence of the similar components across a wide range of concentrations GZA will quantitatively analyze the three vents with the highestmiddot observed concentration of vocs

After the profiling and quantification of Vent 4 is completed Vents 6 and 7 will be sampled with tandem 400 mg Tenax thermal I desotpt~on _tubes _ The therm~l _desor~tion tu~es wil~ _ be__des~rbed

by a Foxboro PTD Programmed Thermal Desorber and syringeinjections made into a Hewlett-Packard 3890A Gas Chromatographequipped with a flame ionization detector The analyticalcolumn is a fused silica capillary column 30 m x 053 mm coated with a 265 um thic~ crosslinked methyl silicone gum phase This particular column provides the chemical inertness of fused silica and the sample capacity approaching packed columna which is useful when making gas injections Multiple injections can be made to verify analytical data and optimize GC conditions (ifnecessary)

As in the sampling of Vent 4 the sample volume will be approximately 12 liters with a flow rate of 50 cominute The minimum detectable airborne concentrations for benzene toluene and xylenes based on a splitless injection are as followaa

I

i Benzene oos ppmToluene 004 ppmXylene a 004 ppm

The B-Nu Model PI-101 Photoionizer and the Century OVA-128 Organic Vapor Analyzer will also be used during the aabullplinground Measurements will be bullade at the vent opening and at a distance of 1 foot downwind of the vent both b fore and after the sorbent sampling

A portable bulleteorological monitoring station will be pr sent on-site which will continuously record on chart paper temperatures wind speed and wind direction Barca tric pressurewill be r corded by an on-site barom ter and r lativ humidity by a sling-psychrometer at hourly intervals

2

]gt()OH ~r HO Zl11 H() ()H -tJ 0 ])0-tJ Hl11 lt3 f11H

n 0])111r n on 00 00

-- middotmiddot---- ( shy

-----middot--middot-middot---middotshymiddot APR 1986 ~

Gu ChTCCIIItosrphYIMul SpectraMtry CCIIIS) hIMteiS

Chp1ce or col-n and opersUna CDDd1Uoaa dependent upon a-pounds or 1ntereat

~linamp packed col-n 11 SP 1000 oo 60110 Cabopack I 11 10 a l4bull

TbullperatuN Prosrbull

lletttocl lequence 1 Col TbullPbull 55-c 1M 10 aiD Squerice 2 Col Tap 200-c late eobullc1a1n Sequence 3 Col Tap 200-c lSIIe 999 bold tor 1400 acana

MaxiJIB tperatu1e 210bullt lDjectpr 210bullt Separator 235bullt

I Manifold eobull--goec Cabould Dtver exceed wa tperatuN Vb1le 1D openUoo)

carrier Bel1B now Rate 25-30 alla1Dute lit mdertlow lilbt appeera dur1Damp nm reduce DPeNtiDI flow amW UDCIIIflow iadicator

DO loopr 1ilbta) middot Scope c Scope aode Data SJS shyMode EI-SEP Electron tneru 70V llliuioo Current 050shyScan Rate 3S350 Mil (ltcaic ttau UDita) Jb1a MJ

dependilll upoo aoleaalll veilbta or ccapouDdl ot inteNSt UP 195 HC l)(IIR ooo

Bold l1M TOP 000 10nCI4 005 MCo

Cbeck blcJcamp10Und before beampinniftamp aalJaibull ot -pta

acqmre a calibration tor worlc1albull~ Nail st MCUUJmiddot

lple PNpUon

1 Precl aWDl steel traps wUb -p a Men middot c 2ll fl=ial shy ~-~lal

J Attach a clHn epty trap to bt u~a1 middot-rluon into tbt t1QS Wodc

) raquo1v rt t bell flow ttumiddot~h U and 5 na Tbt ~ oven ahOIlG be cool a 1 tht tnP to tht ataoaphe bull

lHII OHzr HO ZITI H(1 (IH-z 0 ~n-x HITI ltI ITIH

n 0~ 111r n on 00 00

0

-- middotmiddot---- ( shy

-----middot--middot-middot---middotshymiddot APR 1986 ~

Gu ChTCCIIItosrphYIMul SpectraMtry CCIIIS) hIMteiS

Chp1ce or col-n and opersUna CDDd1Uoaa dependent upon a-pounds or 1ntereat

~linamp packed col-n 11 SP 1000 oo 60110 Cabopack I 11 10 a l4bull

TbullperatuN Prosrbull

lletttocl lequence 1 Col TbullPbull 55-c 1M 10 aiD Squerice 2 Col Tap 200-c late eobullc1a1n Sequence 3 Col Tap 200-c lSIIe 999 bold tor 1400 acana

MaxiJIB tperatu1e 210bullt lDjectpr 210bullt Separator 235bullt

I Manifold eobull--goec Cabould Dtver exceed wa tperatuN Vb1le 1D openUoo)

carrier Bel1B now Rate 25-30 alla1Dute lit mdertlow lilbt appeera dur1Damp nm reduce DPeNtiDI flow amW UDCIIIflow iadicator

DO loopr 1ilbta) middot Scope c Scope aode Data SJS shyMode EI-SEP Electron tneru 70V llliuioo Current 050shyScan Rate 3S350 Mil (ltcaic ttau UDita) Jb1a MJ

dependilll upoo aoleaalll veilbta or ccapouDdl ot inteNSt UP 195 HC l)(IIR ooo

Bold l1M TOP 000 10nCI4 005 MCo

Cbeck blcJcamp10Und before beampinniftamp aalJaibull ot -pta

acqmre a calibration tor worlc1albull~ Nail st MCUUJmiddot

lple PNpUon

1 Precl aWDl steel traps wUb -p a Men middot c 2ll fl=ial shy ~-~lal

J Attach a clHn epty trap to bt u~a1 middot-rluon into tbt t1QS Wodc

) raquo1v rt t bell flow ttumiddot~h U and 5 na Tbt ~ oven ahOIlG be cool a 1 tht tnP to tht ataoaphe bull

lHII OHzr HO ZITI H(1 (IH-z 0 ~n-x HITI ltI ITIH

n 0~ 111r n on 00 00

0

t

fmple Preperat1on - contd

4 After 5 aina 11tt tbe trap hw tbe Uiaamp block ad a11011 1t to cool v1tb bel1a flaw tbrouamph 1t

5 When the trap 1a cool place bull lUll ampluool plua 1n tbe unthreaded end or~ trap

6 FUl the trap v1th the bullbullplea cbarcoal tau bulk bullter1al etc qaickly s in bull dvmt fne

1 Place an add1tianal plLJamp in the tbNaded ad ot tbe trap

8 Attach tbe trap to the tberul daorpUca UD1t J)Svert tbe bel1bull flaw tbroulh the trap unit- ampaperature abauld be at 225-c 11M a U nat or Mtbanol to check tbe r1 ~ u t~WPmiddot

Simple ampDalpis - Packed Col

9 acqu1a1t1oo nan ready

10 Separator divert 1a c 11 1M Voltap CFF

PUnt CFF Scope c

12 IDoHD HpbiD DUt ampower tbeYWal duorpt1aa tnp Medle JDto 1Dject1cm port OviD 1a cool and oven door 1a OpeD at tb1l tae ~ta Hptua DUt

13 Tum Hparator d1nrt CFF IMVoltap C

14 lote tbe chanp JD pruaUN on tbe 1cm pup

15 After tbe preuure baa atab1l1sed tum filiMIIt Cll

Check tor leakl and tlaw Scope IIOdet ampIIGlE

lote axypn leu at raquo DCS MUbull nbull at 4 lel1ua peak aheuld be orr acale lampbullt top) OD acope Jon pup 8bould ad appt1C1MtelJ 12x10 bull

16 tum cope IIOde to J)lTamp SYSTIM

en r 11ed tbod 11 (f99)

roUDWita eurrscsent or bull NG tufD ott GtiKS

I I

~ I I

~(I)OH xr HO Zl11 H(1 (IH ~I 0 ~0 ~J Hl11 ltI 111H

0 0~ 111r 0 00 00 00

0

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( duzUon unit trc 1njecUon pan Tbln Uft trap trca ampat1a1 block nampj lDW U ampo cool middot

IC71Ea JR 101 11ft tbt trap trc tbt MatiJtl block vblle tbe _orpUoniiiiit amp atlll 1n tbe SnJecuon port tbia cauae back pruaure ampo eboot ampbe contenta trc tbe trap

QUampmTlTIOJI

lt apec1tlcal1J requuted w v11l qallt1tate tbl ~ teDtathelJ 1dent1tled bJ GCMS a atandard conuiDiDI IIDt or cmpouDda 1a IUrectlJ injeCted SDto tbe ICIKS Quant1tat1on ot tbl AIIIIPlbull 1a llaHd upon tbe -pUon we acb1nt 1801 ducrption ettldeDCJ for ot quant1taUcm we orteD calculate a MI1U ot cCIII)OWMII for uuple aUpbatlc llrdrocarbcma u cme capound tor exaple baane 111 tb1a cue bull aSIIUU IUpclllM tactcn tor aU te 1lld1v1dLal CCIIPoundl

21 he cl--5 llnf5 ouMriel trwpa CD be fi11eamp with -1 aia far llibulll tMting ~tiJMdia tm are filleamp vith Silica get Olarcaal umx m aunJCCGb 101PalaM JIJ with glaa te101 pl191 at ampthe --L 1ft-~ are cl-5 pdar to 8lllcentiJVJ Iaing the ccmMtiaw u far ttwaal d~K~rptian bit -rtin to middot~-~ atpling pcocae4 in 8tap 8

I I

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------- ----NOnCE If the film le Ia laaa clear tban thla SILRESIM CHEMICAL CORPnotice Itmiddotae due to the ADMINISTRATIVE RECORD aualltY of the dOcuent

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2. barcodetext SDMS Doc ID 569092

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1. barcode 569092
2. barcodetext SDMS Doc ID 569092

-shy

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2. barcodetext SDMS Doc ID 569092

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1. barcode 569092
2. barcodetext SDMS Doc ID 569092

I I I

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1. barcode 569092
2. barcodetext SDMS Doc ID 569092

bull

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1. barcode 569092
2. barcodetext SDMS Doc ID 569092