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Latest Revision: 1/16/2018 Page 1 of 5 SWGDRUG.org/monographs.htm alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory generated this monograph using structurally confirmed reference material. N O CH 3 N CH 3 1. GENERAL INFORMATION IUPAC Name: CAS#: Synonyms: Source: Appearance: UV max (nm): N-phenyl- N-[1-(1-phenylpropan-2-yl)piperidin-4-yl]acetamide NA acetyl-α-methyl fentanyl DEA Reference Material Collection white powder NA 2. CHEMICAL AND PHYSICAL DATA 2.1 CHEMICAL DATA Form Chemical Formula Molecular Weight Melting Point ( o C) Base C 22 H 28 N 2 O 336.47 Not Determined HCl C 22 H 28 N 2 O HCl 372.93 Not Determined

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Page 1: The Drug Administration's Special Testing Laboratory ...swgdrug.org/Monographs/alpha-methyl acetyl fentanyl.pdf · Latest Revision: 1/16/2018 SWGDRUG.org/monographs.htm Page 3 of

Latest Revision: 1/16/2018 Page 1 of 5SWGDRUG.org/monographs.htm

alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory

generated this monograph using structurally confirmed reference material.

N

O CH3

N

CH3

1. GENERAL INFORMATION

IUPAC Name:

CAS#:

Synonyms:

Source:

Appearance:

UVmax(nm):

N-phenyl-N-[1-(1-phenylpropan-2-yl)piperidin-4-yl]acetamide

NA

acetyl-α-methyl fentanyl

DEA Reference Material Collection

white powder

NA

2. CHEMICAL AND PHYSICAL DATA

2.1 CHEMICAL DATA

Form Chemical Formula Molecular Weight Melting Point (oC)

Base C22H28N2O 336.47 Not Determined

HCl C22H28N2O HCl 372.93 Not Determined

Page 2: The Drug Administration's Special Testing Laboratory ...swgdrug.org/Monographs/alpha-methyl acetyl fentanyl.pdf · Latest Revision: 1/16/2018 SWGDRUG.org/monographs.htm Page 3 of

Latest Revision: 1/16/2018 Page 2 of 5SWGDRUG.org/monographs.htm

alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory

generated this monograph using structurally confirmed reference material.

3. QUALITATIVE DATA

3.1 NUCLEAR MAGNETIC RESONANCE

Sample Preparation: Dilute analyte to ~12mg/mL in CD3OD containing TMS for 0 ppm reference anddimethylfumarate as quantitative internal standard.

Instrument: 400 MHz NMR spectrometerParameters: Spectral width: at least containing -3 ppm through 13 ppm

Pulse angle: 90o

Delay between pulses: 45 seconds1HNMR: alpha-methyl acetyl fentanyl HCl; lot# 0496094-9; CD3OD; 400MHz

7 6 5 4 3 2 1 0

35213 3 173

TMS

CD3OD

dimethylfumarateCD3ODdimethylfumarate

7.35 7.25

7

3.35 3.25

13

CD3OD

7.55

3

3.60

3 1

1.200

3

1.851.801.75

5

2.25 2.15

2

Page 3: The Drug Administration's Special Testing Laboratory ...swgdrug.org/Monographs/alpha-methyl acetyl fentanyl.pdf · Latest Revision: 1/16/2018 SWGDRUG.org/monographs.htm Page 3 of

Latest Revision: 1/16/2018 Page 3 of 5SWGDRUG.org/monographs.htm

alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory

generated this monograph using structurally confirmed reference material.

3.2 GAS CHROMATOGRAPHY/MASS SPECTROMETRY

Sample Preparation: Dilute analyte ~5 mg/mL into methanol.

Instrument:Column:Carrier Gas:Temperatures:

Agilent gas chromatograph operated in split mode with MS detector HP-5; 30m x 0.25 mm x 0.25 mHelium at 1.5 mL/minInjector: 280oCMSD transfer line: 280oCMS Source: 230oCMS Quad: 150oCOven program:

1) 100oC initial temperature for 1.0 min2) Ramp to 280oC at 12 oC/min3) Hold final temperature for 9.0 min

Injection Parameters: Split Ratio = 25:1, 1 L injectedMS Parameters: Mass scan range: 30-550 amu

Threshold: 250Tune file: stune.uAcquisition mode: scan

Retention Time: 17.005minEI Mass Spectrum: alpha-methyl acetyl fentanyl HCl; lot# 0496094-9

m/z30025020015010050

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4919191 9191919191 9191919191 9191919191 91919191

828282 8282828282 8282828282 8282828282 82828282777777 7777777777 7777777777 7777777777 77777777656565 6565656565 6565656565 6565656565 65656565585858 5858585858 5858585858 5858585858 58585858565656 5656565656 5656565656 5656565656 56565656

555555 5555555555 5555555555 5555555555 55555555434343 4343434343 4343434343 4343434343 43434343424242 4242424242 4242424242 4242424242 42424242EI+

m/z30025020015010050

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919191 9191919191 9191919191 9191919191 91919191848484 8484848484 8484848484 8484848484 84848484

828282 8282828282 8282828282 8282828282 82828282777777 7777777777 7777777777 7777777777 77777777

676767 6767676767 6767676767 6767676767 67676767656565 6565656565 6565656565 6565656565 65656565

585858 5858585858 5858585858 5858585858 58585858565656 5656565656 5656565656 5656565656 56565656

555555 5555555555 5555555555 5555555555 55555555515151 5151515151 5151515151 5151515151 51515151

434343 4343434343 4343434343 4343434343 43434343424242 4242424242 4242424242 4242424242 42424242

EI+

Page 4: The Drug Administration's Special Testing Laboratory ...swgdrug.org/Monographs/alpha-methyl acetyl fentanyl.pdf · Latest Revision: 1/16/2018 SWGDRUG.org/monographs.htm Page 3 of

Latest Revision: 1/16/2018 Page 4 of 5SWGDRUG.org/monographs.htm

alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory

generated this monograph using structurally confirmed reference material.

3.3 INFRARED SPECTROSCOPY (FTIR)

FTIR (Smart Golden Gate ATR Accessory)Instrument: Scan Parameters: Number of scans: 32

Number of background scans: 32Resolution: 4 cm-1

Sample gain: 8Aperture: 150

FTIR ATR (Diamond 1 Bounce): alpha-methyl acetyl fentanyl HCl; lot# 0496094-9

Wavenumber (cm-1)3500 3000 2500 2000 1500

%Tr

ansm

ittan

ce

60

65

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75

80

2455245524552455245524552455245524552455245524552455245524552455245524552455245524552455

2413241324132413241324132413241324132413241324132413241324132413241324132413241324132413

1651165116511651165116511651165116511651165116511651165116511651165116511651165116511651

1595159515951595159515951595159515951595159515951595159515951595159515951595159515951595 1495

149514951495149514951495149514951495149514951495149514951495149514951495149514951495

1487148714871487148714871487148714871487148714871487148714871487148714871487148714871487

1431143114311431143114311431143114311431143114311431143114311431143114311431143114311431

1390139013901390139013901390139013901390139013901390139013901390139013901390139013901390

13811381138113811381138113811381138113811381138113811381138113811381138113811381138113811371137113711371137113711371137113711371137113711371137113711371137113711371137113711371

13081308130813081308130813081308130813081308130813081308130813081308130813081308130813081288128812881288128812881288128812881288128812881288128812881288128812881288128812881288

1236123612361236123612361236123612361236123612361236123612361236123612361236123612361236

1155115511551155115511551155115511551155115511551155115511551155115511551155115511551155

1078107810781078107810781078107810781078107810781078107810781078107810781078107810781078

1030103010301030103010301030103010301030103010301030103010301030103010301030103010301030

964964964964964964964964964964964964964964964964964964964964964964

930930930930930930930930930930930930930930930930930930930930930930

899899899899899899899899899899899899899899899899899899899899899899

773773773773773773773773773773773773773773773773773773773773773773

756756756756756756756756756756756756756756756756756756756756756756

700700700700700700700700700700700700700700700700700700700700700700

625625625625625625625625625625625625625625625625625625625625625625

598598598598598598598598598598598598598598598598598598598598598598

590590590590590590590590590590590590590590590590590590590590590590

521521521521521521521521521521521521521521521521521521521521521521

451451451451451451451451451451451451451451451451451451451451451451

405405405405405405405405405405405405405405405405405405405405405405

Wavenumber (cm-1)1700 1600 1500 1400 1300 1200 1100 1000 900 800 700

%Tr

ansm

ittan

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60

65

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1651165116511651165116511651165116511651165116511651165116511651165116511651165116511651

1595159515951595159515951595159515951595159515951595159515951595159515951595159515951595 1495

149514951495149514951495149514951495149514951495149514951495149514951495149514951495

14871487148714871487148714871487148714871487148714871487148714871487148714871487148714871452145214521452145214521452145214521452145214521452145214521452145214521452145214521452

1431143114311431143114311431143114311431143114311431143114311431143114311431143114311431

1390139013901390139013901390139013901390139013901390139013901390139013901390139013901390

13811381138113811381138113811381138113811381138113811381138113811381138113811381138113811371137113711371137113711371137113711371137113711371137113711371137113711371137113711371

1336133613361336133613361336133613361336133613361336133613361336133613361336133613361336 1308

1308130813081308130813081308130813081308130813081308130813081308130813081308130813081288128812881288128812881288128812881288128812881288128812881288128812881288128812881288

1250125012501250125012501250125012501250125012501250125012501250125012501250125012501250 1236

123612361236123612361236123612361236123612361236123612361236123612361236123612361236

1155115511551155115511551155115511551155115511551155115511551155115511551155115511551155

1113111311131113111311131113111311131113111311131113111311131113111311131113111311131113

1078107810781078107810781078107810781078107810781078107810781078107810781078107810781078

1049104910491049104910491049104910491049104910491049104910491049104910491049104910491049 1030

103010301030103010301030103010301030103010301030103010301030103010301030103010301030

968968968968968968968968968968968968968968968968968968968968968968964964964964964964964964964964964964964964964964964964964964964964 939

939939939939939939939939939939939939939939939939939939939939939

930930930930930930930930930930930930930930930930930930930930930930

899899899899899899899899899899899899899899899899899899899899899899

872872872872872872872872872872872872872872872872872872872872872872

849849849849849849849849849849849849849849849849849849849849849849 798

798798798798798798798798798798798798798798798798798798798798798

773773773773773773773773773773773773773773773773773773773773773773

756756756756756756756756756756756756756756756756756756756756756756

742742742742742742742742742742742742742742742742742742742742742742

708708708708708708708708708708708708708708708708708708708708708708

700700700700700700700700700700700700700700700700700700700700700700

661661661661661661661661661661661661661661661661661661661661661661

625625625625625625625625625625625625625625625625625625625625625625

598598598598598598598598598598598598598598598598598598598598598598

590590590590590590590590590590590590590590590590590590590590590590

555555555555555555555555555555555555555555555555555555555555555555

521521521521521521521521521521521521521521521521521521521521521521

496496496496496496496496496496496496496496496496496496496496496496 451

451451451451451451451451451451451451451451451451451451451451451

405405405405405405405405405405405405405405405405405405405405405405

Page 5: The Drug Administration's Special Testing Laboratory ...swgdrug.org/Monographs/alpha-methyl acetyl fentanyl.pdf · Latest Revision: 1/16/2018 SWGDRUG.org/monographs.htm Page 3 of

Latest Revision: 1/16/2018 Page 5 of 5SWGDRUG.org/monographs.htm

alpha-methyl acetyl fentanyl The Drug Enforcement Administration's Special Testing and Research Laboratory

generated this monograph using structurally confirmed reference material.

4. ADDITIONAL RESOURCES

No available literature as of 11/15/17