the appendix is an integral part of certificate of accreditation no. … · 2020. 9. 2. · (Čsn...

The Appendix is an integral part of

Certificate of Accreditation No. 478/2020 of 27/07/2020

Accredited entity according to ČSN EN ISO/IEC 17025:2018:

“AGRO-LA“, spol. s r.o. Laboratory Centre

Jiráskovo předměstí 630, Jindřichův Hradec III, 377 01 Jindřichův Hradec

of 12

The Laboratory has a flexible scope of accreditation permitted as detailed in the Annex.

Updated list of activities provided within the required flexible scope of accreditation is available in

the laboratory from the Laboratory Centre Manager.

The Laboratory is qualified to carry out independent sampling.

Tests:

Ordinal

number 1 Test procedure/method name

Test procedure/method

identification 2 Tested object

1 Determination of turbidity

by nephelometry

SOP 1

(ČSN EN ISO 7027-1)

Drinking, raw, bottled,

surface, bathing water

2 Determination of the sum of

calcium

and magnesium (Ca+Mg) by

titration

SOP 2

(ČSN ISO 6059) Drinking, raw, bottled,

surface, waste water

3* Determination of pH

by potentiometric method

SOP 3

(ČSN ISO 10523)


surface, waste, bathing water

4 Determination of acid

neutralizing capacity (ANC)

by titration

SOP 4-1

(ČSN EN ISO 9963-1,

ČSN EN ISO 9963-2)

Drinking, raw, surface water

5 Determination of electrical

conductivity

SOP 5

(ČSN EN 27888)



6 Determination of ammonium

by spectrophotometry

and determination of

ammonia nitrogen by

calculation

SOP 6

(ČSN ISO 7150-1)



7 Determination of iron (Fe)


SOP 7

(ČSN 83 0520 – 21:1976,

ČSN 83 0530 – 27:1976)



8 Determination of chemical

oxygen demand with

permanganate (COD-Mn) by

titration

SOP 8

(ČSN EN ISO 8467) Drinking, raw, bottled,


9 Determination of chloride

by titration

SOP 9

(ČSN ISO 9297)



10 Determination of sulphate by

capillary

isotachophoresis

SOP 10

(Recman manual)



11 Determination of nitrate

spectrometric method

with 2,6 – dimethylphenol

(modification in photometric

test-tubes),

determination of nitrate

nitrogen, inorganic and total

nitrogen by calculation

SOP 11

(ČSN 75 7455,

ČSN ISO 7890-1:1995)








of 12

Ordinal




12 Determination of nitrite


and determination of nitrite

nitrogen by calculation

SOP 12

(ČSN EN 26777)



13 Determination of manganese

(Mn)


SOP 13

(ČSN 83 0520-2:1976)



14 Determination of chemical

oxygen demand with

dichromate (CODCr) by

titration

SOP 14

(ČSN ISO 6060 including

Change Z1)

Surface, waste water

15 Determination of

biochemical oxygen demand

after n days (BODn) by

oxygen probe

SOP 15

(ČSN EN 1899-1,

ČSN EN 1899-2)

Surface, waste water

16 Determination of suspended

solids (SS) by gravimetry

SOP 16

(ČSN EN 872)

Drinking, raw, surface,

waste water

17 Determination of dissolved

solids (DS) by gravimetry

SOP 17

(ČSN 75 7346)



18 Determination of phosphorus

(P) by spectrophotometry

SOP 19

(ČSN EN ISO 6878)



19 Determination of phosphates


and determination of

phosphate phosphorus by

calculation

SOP 20

(ČSN EN ISO 6878)



20 Determination of elements

(Ca, Mg)

by flame AAS method

SOP 21

(ČSN ISO 7980)




(Na, K)

by flame AAS method

SOP 22

(ČSN ISO 9964-3)



22* Determination of dissolved

oxygen

– electrochemical method

with a membrane or

luminescence probe

SOP 26

(ČSN EN ISO 5814)



23 Determination of colour


SOP 30

(ČSN EN ISO 7887)



24* Determination of temperature SOP 36

(ČSN 75 7342)



25* Determination of redox

potential (ORP)

SOP 35

(ČSN 75 7367)

Bathing water






of 12

Ordinal




26 Determination of free

chlorine and total chlorine,

with N,N-diethyl-1,4-

phenylenediamine

by titration and determination

of bound chlorine by

calculation

SOP 25

(ČSN ISO 7393-1)

Drinking water, bathing

water

27* Determination of free and

total chlorine

using commercial analytical

set MERCK/HACH

and determination of bound

chlorine by calculation

SOP 25-1

(MERCK/HACH firm

publication)


water

28 Determination of organic

nitrogen (N-org.) by Kjeldahl

method – volumetric method

SOP 33-1

(ČSN EN 25663)

Raw, surface and waste

water


(Pb, Ni, Cd, Cr, Fe, Mn, Al,

Cu, Zn)

by flame AAS method

SOP 38-1

(ČSN 757385,

ČSN EN 1233,

ČSN EN ISO 12020,

ČSN ISO 8288,

ČSN EN ISO 5961)




(Pb, Ni, Cd, Cr, Fe, Mn, Cu,

Zn)

by flame AAS method

SOP 38-2

(ČSN 757385,

ČSN EN 1233,

ČSN ISO 8288,

ČSN EN ISO 5961)

Vegetable materials,

feedstuffs


(Pb, Ni, Cd, Cr, Cu, Zn)

by flame AAS method

SOP 38-3

(ČSN EN 1233,

ČSN EN ISO 5961)

Soils, sludge, sediments,

waste


(V, As, Mo, Be) by flameless

AAS method

SOP 40

(ČSN EN ISO 15586)


waste

33 Determination of mercury

(Hg)

by a single purpose analyzer

SOP 23

(ČSN 75 7440)


surface, waste water,

vegetable materials,

feedstuffs, soils, sludge,

sediments, waste

34 Determination of dry matter

and ash by gravimetry and

determination of moisture

content and loss on ignition

by calculation

SOP 39-1

(ČSN ISO 11465)

Vegetable materials,

feedstuffs

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of 12

Ordinal




35 Determination of dry matter and ash by gravimetry and determination of moisture content and loss on ignition by calculation

SOP 39-2 (ČSN ISO 11465)

Soils, sludge, sediments, fertilizers, waste

36 Determination of elements (Mg, K, Ca, Na) by flame AAS method

SOP 41 (JPP ZK I chap. 7, JPP AR chap. 3, ČSN 46 7092-12: 1998, ČSN 46 7092-14: 1998, ČSN 46 7092-15)

Vegetable materials, feedstuffs

37 Determination of elements (Mg, K, Ca) by flame AAS method

SOP 42 (JPP AP I chap. 3)

Soils

38 Determination of elements (Mg, K, Ca, Na) by flame AAS method

SOP 42-1 (JPP AR chap. 3, JPP AP II chap. 3.3., ČSN 46 7092-12:1998, ČSN 46 7092-13,1998, ČSN 46 7092-14:1998, ČSN 46 7092-15, ČSN EN 13657, JPP AP II chap. 3.2.1)

Soils, sludge, sediments

39 Determination of phosphorus (P) by spectrophotometry

SOP 43-1 (JPP ZK I chap. 7, JPP AR chap. 3, ČSN 46 7092-11)

Vegetable materials, feedstuffs


SOP 43-2 (JPP AP I chap. 3)

Soils


SOP 43-3 (JPP AP I chap. 3.1.2., ČSN EN ISO 6878, ČSN EN 13657, JPP AP II chap. 3.2.1)


42 Determination of pH by potentiometric method

SOP 44 (JPP AP I chap. 2.3, ČSN ISO 10523, ČSN ISO 10390)


43* Preliminary determination of odour

SOP 45 (ČSN 75 7340)

Drinking, raw, bottled water

44* Preliminary determination of taste

SOP 46 (ČSN 75 7340)

Drinking water, bottled water

45 Determination of base neutralizing capacity (BNC) by titration

SOP 4-2 (ČSN 75 7372)

Drinking, raw, surface water






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Ordinal




46 Determination of silver (Ag)

by flame AAS method

SOP 47

(ČSN 75 7400)




(Pb, Ni, Cd, Cr, V, As, Al,

Be, Mo, Ba, Se, Sb, Co) by

flameless AAS method

SOP 87

(ČSN EN ISO 15586)



48 Determination of cobalt (Co)

by flame AAS method

SOP 88

(ČSN ISO 8288,

TNV 75 9335,

ČSN EN 13657,

ČSN EN ISO 15587-1

ČSN EN ISO 15587-2,

GBS work manual)


waste

49* Determination of ozone

using HACH commercial

analytical set

SOP 425

(HACH firm publication)


water

50 Determination of volatile

organic compounds18) by gas

chromatography method with

mass detection (GC-MS) and

∑BTEX, ∑xylenes and

∑THM by calculation from

measured values

SOP 405

(ČSN EN ISO 10301)


surface and waste water

51 Determination of polycyclic

aromatic hydrocarbons19) by

gas chromatography method

with mass detection (GC-

MS) and ∑ PAH by

calculation from measured

values

SOP 404

(ČSN 75 7554)



52 Determination of

organochlorine pesticides20)

by gas chromatography

method with mass detection

(GC-MS)

and ∑ of pesticide substances

by calculation from measured

values

SOP 428

(ČSN EN ISO 6468)



53 Determination of nitrogen

(N) and nitrogenous

substances (NL) by Kjeldahl

method

SOP 55-1

(JPP ARM chap. 3.1.2.,

JPP ARM chap. 2.1.2.,

ČSN 46 7092-4,

ČSN EN 25663)

Feedstuffs, vegetable

material






of 12

Ordinal




54 Determination of proteins by Kjeldahl method

SOP 55-2 (PLZK, DL and P I chap. 2.1, JPP AR chap. 3, ČSN 46 7092-4, ČSN 46 7092-27, ČSN EN 25663)

Feedstuffs, vegetable material

55 Determination of nitrogen (N) by Kjeldahl method

SOP 55-3 (JPP AP III chap. 2.1.4., ČSN 46 7092-4., ČSN EN 25663)

Fertilizers, soils, sludge, sediments

56 Determination of fats by Soxhlet method by gravimetry

SOP 52 (PLZK,DL and P I chap. 3.1., ČSN 46 7092-7)


57 Determination of fibre content by gravimetry

SOP 53 (JPP MCHR P HKO I chap. 15, ČSN ISO 6541)


58 Determination of hydrocarbons C10 to C40 by gas chromatography method with flame ionization detector (GC-FID)

SOP 406 (ČSN EN ISO 9377-2, Change Z1)

Drinking, raw, bottled, surface and waste water

59 Determination of total organic carbon (TOC) and dissolved organic carbon (DOC) by infrared spectrometry method

SOP 430 (ČSN EN 1484)

Drinking, raw, bottled, surface, waste, bathing water

60 Determination of nitrogen – determination of bound nitrogen (TNb) after oxidation to nitrogen oxides by chemiluminescence detection

SOP 431 (ČSN EN 12260)

Drinking, raw, bottled, surface, waste, bathing water

61 Determination of the threshold odour number and threshold flavour number

SOP 432 (ČSN EN 1622)


62 Determination of hydrocarbons C10 to C40 by gas chromatography method with flame ionization detector (GC-FID)

SOP 417 (ČSN EN ISO 16703, ČSN EN 14039)

Soils, sludge, sediments, waste

63 Determination of the content of nitrogen (N) using an analyzer by Dumas method and nitrogenous substances (NL) and proteins by calculation from measured values

SOP 434 (ČSN EN 16634-1, JPP AR chap. 3.1.)

Feedstuffs, vegetable materials, soils, sludge, sediments

64-100 Reserved






of 12

Ordinal




101 Detection and enumeration of Escherichia coli and coliform bacteria by Colilert method

SOP 101-2 (ČSN EN ISO 9308-2)

Drinking, raw, bottled, surface, bathing water

102 Detection and enumeration of Escherichia coli and coliform bacteria by culture method

SOP 101-3 (ČSN ISO 4832, ČSN ISO 16649-2)

Food industry products, feedstuffs

103 Enumeration of Escherichia coli and coliform bacteria by swab method

SOP 101-4 (ČSN ISO 4832, ČSN ISO 16649-2)

Swabs from the environment and equipment

104 Detection and enumeration of Escherichia coli and coliform bacteria by membrane filtration method.

SOP 101-5 (ČSN EN ISO 9308-1)

Drinking, bottled, pool water

105 Detection and enumeration of mesophilic bacteria by culture method

SOP 102 (ČSN 75 7841)

Drinking, raw, bottled, surface water

106 Detection and enumeration of psychrophilic bacteria by culture method

SOP 103 (ČSN 75 7842)


107 Detection and enumeration of intestinal enterococci - Part 2: membrane filtration method

SOP 104-1 (ČSN EN ISO 7899-2)


108 Detection and enumeration of enterococci by smear method

SOP 104-2 (AHEM No. 7/2001)


109 Detection and enumeration of Clostridium perfringens (including spores) by membrane filtration method.

SOP 106-1 (Annex No. 6 to Regulation No. 252/2004 Coll., as amended)


110 Detection and enumeration of the spores of sulphite-reducing anaerobes (Clostridia) – Part 2: membrane filtration method

SOP 106-2 (ČSN EN 26461-2)


111 Enumeration of Clostridium perfringens and detection and enumeration of sulphite-reducing anaerobes (clostridia) by culture

SOP 106-4 (ČSN EN ISO 7937, ČSN ISO 15213)

Food industry products, feedstuffs

112 Enumeration of Clostridium perfringens and detection and enumeration of sulphite-reducing anaerobes (clostridia) by smear method

SOP 106-5 (ČSN EN ISO 7937, ČSN ISO 15213)

Swabs from the environment and equipment






of 12

Ordinal




113 Detection and enumeration of

Staphylococcus aureus by

culture method

SOP 107-1

(ČSN ISO 6888:1994,

ČSN EN ISO 6888-1)



114 Enumeration of

Staphylococcus aureus and

coagulase-positive

staphylococci by culture

method

SOP 107-2

(ČSN ISO 6888:1994,

ČSN EN ISO 6888-1)

Food industry products,

feedstuffs

115 Enumeration of

Staphylococcus aureus and

coagulase-positive

staphylococci by swab

method

SOP 107-3

(ČSN ISO 6888:1994,

ČSN EN ISO 6888-1)

Swabs from the environment

and equipment


Pseudomonas aeruginosa by

membrane filtration method

SOP 108

(ČSN EN ISO 16 266)




thermotolerant coliform

bacteria and Escherichia coli

by culture method

SOP 109-1

(CSN 75 7835)




thermotolerant coliform

bacteria by culture

SOP 109-2

(AHEM No. 7/2001)


119 Enumeration of culturable

microorganisms

a) at 22°C

b) at 36°C

by culture method

SOP 114

(ČSN EN ISO 6222)



120 Biological analysis –

Determination of abioseston

by microscopic method

SOP 112

(ČSN 75 7713)


121 Biological analysis –

Determination of

microscopic image

SOP 113

(ČSN 75 7712)


122 Enumeration of total

microorganisms by culture

method

SOP 122-1



feedstuffs

123 Enumeration of total

microorganisms by swab

method

SOP 122-2



and equipment

124 Enumeration of yeasts and

moulds by culture method

SOP 153-1

(ČSN ISO 6611,

ČSN ISO 7698:1996,

ČSN ISO7954:1994)


feedstuffs






of 12

Ordinal




125 Enumeration of yeasts and

moulds by swab method

SOP 153-2

(ČSN ISO 6611,

ČSN ISO 7698:1996,

ČSN ISO7954:1994)


and equipment

126 Enumeration of Bacillus

cereus

by culture method

SOP 124

(ČSN EN ISO 7932)


feedstuffs

127 Detection and enumeration

of Listeria sp. and Listeria

monocytogenes by culture method

SOP 120


ČSN EN ISO 11290-2)


feedstuffs

128 Detection of Salmonella spp.

by culture method

SOP 105-1

(AHEM No. 7/2001)


biowaste


by culture method

SOP 105-2

(ČSN ISO 19250)




by culture method

SOP 105-3

(ČSN EN ISO 6579,

ČSN EN ISO 6785:2009)

Food products


by swab method

SOP 105-4

(ČSN EN ISO 6579,

ČSN EN ISO 6785:2009)


and equipment


Legionella spp. by membrane

filtration method

SOP 115-1

(ČSN EN ISO 11731)

Drinking and surface water,

bathing water


Legionella spp. by swab

method

SOP 115-2

(ČSN EN ISO 11731)


and equipment

134 Enumeration of mucific

bacteria Leuconostoc by

culture

SOP 118

(ČSN 56 0095)

Food products


Enterobacteriaceae

by culture method

SOP 126-1

(ČSN ISO 21528-2)


feedstuffs


Enterobacteriaceae

by swab method

SOP 126-2

(ČSN ISO 21528-2)


and equipment


Paenibacillus larvae by

culture method

SOP 128

(OIE Terrestrial Manual 2008,

chapter 2.2.2, American

foulbrood of honey bees)

Honey, pulp, wax

138-200 Reserved

1 Asterisk at the ordinal number identifies the tests, which the Laboratory is qualified to carry out outside the

permanent laboratory premises.






of 12

2 If the document identifying the test procedure is dated, only these specific procedures are used. If the

document identifying the test procedure is not dated, the latest edition of the specified procedure is used

(including any changes).

Annex:

Flexible scope of accreditation

Ordinal numbers of tests

1 - 63

The Laboratory is allowed to modify the test methods listed in the Annex within the specified scope of

accreditation provided the measuring principle is observed. The flexible approach to the scope of

accreditation cannot be applied to the tests not included in the Annex.

Sampling:

Ordinal

number Sampling procedure name Sampling

procedure identification1 Sampled object

201 Drinking water sampling SOP 205


ČSN EN ISO 5667-3,

ČSN ISO 5667-5,

ČSN ISO 5667-11,


ČSN EN ISO 19458,

Regulation No. 252/2004 Coll.)

Drinking, raw water

202 Waste water sampling

manually, by an automatic

sampler

SOP 210


ČSN EN ISO 5667-3,

ČSN ISO 5667-10,

ČSN ISO 5667-11,


ČSN EN ISO 19458)

Waste water

203

Manual sampling of surface

water

SOP 211


ČSN EN ISO 5667-3,

ČSN ISO 5667-4,

ČSN EN ISO 5667-6,


ČSN EN ISO 19458)

Surface water






of 12

Ordinal

number Sampling procedure name Sampling

procedure identification1 Sampled object

204 Bathing water sampling SOP 206


ČSN EN ISO 5667-3,

ČSN ISO 5667-4,

ČSN ISO 5667-5,

ČSN EN ISO 5667-6,


ČSN EN ISO 19458,

Regulation No. 238/2011 Coll.,

as amended)

Bathing water

205 Sampling of sludge, sediments SOP 207

(CSN EN ISO 5667-1,

CSN EN ISO 5667-3,

CSN EN ISO 5667-14,

ČSN EN ISO 19458,

Regulation No. 294/2005 Coll.,

Regulation No. 382/2001 Coll.)

Sludge, sediments

206 Sampling of swabs for

microbiological analysis

SOP 119

(ČSN 56 0100,

article 145 - 1968)

Food industry facilities

207 Sampling of soils SOP 213

(UKZUZ Guideline No.

51/OBKP,

Regulation No. 75/2010,

ČSN EN ISO 5667-1,

ČSN EN ISO 5667-3,

ČSN ISO 5667-12

ČSN EN ISO 5667-14)

Soils

208 Waste sampling SOP 214

(MoE CR Guideline for waste

sampling, MoE CR Bulletin No.

4/2008)

Waste

209 Sampling of food, raw materials

and feedstuffs

SOP 215

(Regulation 339/2001 Coll.,

Regulation 211/2004 Coll.,

EC No. 152/2009,

ČSN 56 0080:1983,

ČSN 56 0130-2,

ČSN 56 0520-2,

ČSN ISO 3100-1:2001,

ČSN EN ISO 707,

ČSN 56 0512-2:1995,

ČSN 56 0290-2,

ČSN EN ISO 6497,

ČSN 46 2200-2)

Food and raw materials for the

production of food, feedstuffs

and raw materials for the

production of feedstuffs

1 If the document identifying the sampling procedure is dated, only these specific procedures are used. If the

document identifying the sampling procedure is not dated, the latest edition of the specified procedure is used

(including any changes)






of 12

3) JPP AP I, II, III: Uniform working procedures, Analysis of soils I, II, III

JPP AR: Uniform working procedures, Analysis of vegetable material

JPP ZK I: Uniform working procedures, laboratory testing of feedstuffs, complements and premixes I

JPP ÚKZÚZ: Central Institute for Supervising and Testing in Agriculture in Brno - Uniform Working

Procedures PLZK, DL and P IÚKZÚZ: Procedures for Laboratory Testing of Feedstuffs, Complements and Premixes I,

ÚKZÚZ Brno, Pavel Šíma et al., 2001

JPP MCHR p HKO I = Uniform working procedures, Methodology of chemical analyzes for quality

evaluation of varieties I ÚKZÚZ Brno, František Novotný, 2000 4) SOP: Standard Operating Procedure 5) TNV: Technical Standard for Waters 6) Reserved 7) Sludge: water treatment sludge, industrial sludge, sedimented mud, pond sedimented sludge, dewatered

sanitized sludge, waste sludge 8) Soils: agricultural, forest, excavation soils, composts, substrates, sands 9) Sediments: natural, industrial sediments 10) AHEM: Acta hygienica, epidemiologica et microbiologica 11) Food products: foodstuffs, feed, food raw materials, biological and plant material 12) Raw water: water for the production of drinking water 13) Waste: solid materials – debris, building materials 14) AAS: Atomic Absorption Spectrometry 15) MoE CR Guideline: Guideline of the Ministry of Environment of the Czech Republic 16) Bathing water – pools and natural bathing places 17) GC – MS: Gas Chromatography – Mass Spectrometry 18) Volatile organic compounds: vinylchloride (i.e. chloroethylene), 1,1-dichloroethylene, dichloromethane,

trans-1,2-dichloroethylene, cis-1,2-dichloroethylene, chloroform (i.e. trichloromethane), 1,2-dichloroethane,

1,1,1-trichloroethane, tetrachloromethane, benzene, 1,2-dichloropropane, trichloroethene,

bromodichloromethane,

cis-1,3-dichloropropene, trans-1,3-dichloropropene, 1,1,2-trichloroethane, toluene, dibromochloromethane,

tetrachloroethene, chlorobenzene, ethylbenzene, ∑xylenes (m+p-xylene, o-xylene), bromoform

(i.e. tribromomethane), styrene, isopropylbenzene, bromobenzene, propylbenzene, 2-chlorobenzene, 4-

chlorotoluene, 1,2,4-trimethylbenzene,

tert-butylbenzene, 1,3,5-trimethylbenzene, sec-butylbenzene, 1,3-dichlorobenzene, 1,4-dichlorobenzene,

p-isopropyltoluene, 1,2-dichlorobenzene, butylbenzene, 1,2,4-trichlorobenzene, 1,2,3-trichlorobenzene,

∑BTEX (benzene, toluene, ethylbenzene, xylenes), ∑THM (trichloromethane, tribromomethane,

dibromochloromethane, bromodichloormethane), dichlorobenzenes (1,2-dichlorobenzene, 1,3-

dichlorobenzene, 1,4-dichlorobenzene), trichlorobenzenes (1,2,3-trichlorobenzene, 1,2,4-trichlorobenzene) 19) Polycyclic Aromatic Hydrocarbons (PAH): naphthalene, acenaphthylene, acenaphthene, fluorene,

phenanthrene, anthracene, fluoranthene, pyrene, benzo(a)pyrene, chrysene, benzo(b)fluoranthene,

benzo(k)fluoranthene, benzo(a)anthracene, indeno(1,2,3cd)pyrene,

dibenzo(a,h)anthracene,benzo(g,h,i)perylene. 20) Pesticides: alachlor, isodrin, pentachlorobenzene, aldrin, 1,2,4,5-tetrachlorobenzene, α-

hexachlorocyclohexane (α-lindan), hexachlorobenzene, β-hexachlorcyclohexane (β-lindan), γ-

hexachlorocyclohexane (γ-lindan),

δ-hexachlorocyclohexane (δ-lindan), ε-hexachlorocyclohexane (ε-lindan), heptachlor, 4,4´-DDE (i.e. p,p-

DDE),

4,4´-DDD (i.e. p,p-DDD), 4,4´-DDT (i.e. p,p-DDT), 2,4´-DDE (i.e. o,p-DDE), 2,4´-DDD (i.e. o,p-DDD),

2,4´-DDT (i.e. o,p-DDT) and methoxychlor 21) GC – FID: Gas Chromatography with Flame Ionization Detection

the appendix is an integral part of certificate of accreditation no. … · 2020. 9. 2. · (Čsn...

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