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TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING

TestAmerica St. Louis

TestAmerica Laboratories, Inc.

ANALYTICAL REPORT

REVISED

PROJECT NO. 1991-~35-11/o02

Honeywell Ponds

Lot #: F9E010213

Sean Chisek

Andrews Engineering, Inc.3300 Ginger Creek DriveSpr~gfield, IL 62711

TEST1\MKRICA LABORATORIES I INC.

January 7 I 2010

LOT # F9E070213-REVISED13715 Rider Trail North Earth (itv. MO 63045 t@) ~14.JgR.RSnn faY ~14.?QR.R7'i7 www.t~~tamt!rl~ain~_tom

1 of 57

F9E070213 (4): E-74 LOWERF9E070213 (5): E-67 LOWERF9E070213 (6): E-65 LOWER


Case NarrativeLOT NUMBER: F9E070213

Revised

This report contains the analytical results for the six samples received under chain of custody by STLSt. Louis on May 6. 2009. These samples are associated with your Honeywell Ponds project

The analytical results included in this report meet all applicable quality control procedure requirementsexcept as noted on the following page~

The test results in this report meet all NELAP requirements for parameters in which accreditations areheld by STL St. Louis. Any exceptions to NELAP requirements are noted in the case narrative. Thecase narrative is an integral part of this report.

All chemical analysis results are based upon sample as received, wet weight, unless noted otherwise.All radiochemistry results are based upon sample as dried and ground with the exception of tritium,unless requested wet weight by the client.

This report is revised to report Chemistry data on a wet-weight basis~

observationsINonconformances

Reference the chain of custody and condition upon receipt report for any variations on receipt conditionsand temperature of samples on receipt.

Cation Exchange Capacity

Batch 9133197:The samples were analyzed at a dilution due to high concentrations of target analytes~ The reportinglimit has been adjusted for the dilution since no analysis at a lesser dilution was performed.Affected Samples:F9E070213 (1): E-65 UPPER F9E070213 (6): E-65 LOWER

Gamma Spectroscopy

The presence of Thorium 234/Uranium 238 indicate the presence of Proactinium 234m. TheProactinium 234m results were calculated above the MDA in the samples, however, the results maybe biased high due to the low abundance at keyline 1001.3 keV.Affected Samples:F9E070213 (1): E-65 UPPERF9E070213 (2): E-67 UPPERF9E070213 (3): E-74 UPPER

Reactive Cyanide

LCS/MS recoveries for Reactive cyanide are outside the established QC limits. AU results are nondetect for this batch. Since this test is semi-qualitative no further action is required.Affected Samples:F9E070213 (6): E-65 LOWER

OT # F9E070213-REVISED 2 of 57


TCLP Preparation

Due to limited sample volume, a reduced sample amount was used for the TCLP extraction. The 20:1leachate:sample ratio was maintained.Affected Samples:F9E070213 (1): E-65 UPPER F9E070213 (6): E-65 LOWER

Trace ICP Metals

Batch 9131193:The sample was analyzed at a dilution due to high concentrations of target analytes. The reportinglimit has been adjusted for the dilution since no analysis at a lesser dilution was performed.Affected Samples:F9E070213 (5): E-67 LOWER

There were no nonconformances or observations noted with any other analysis on this lot.

LOT # F9E070213-REVISED 3 of 57


METIIODSSUMMAKY

P9B070213

PARAMETER

Bulk DensityCation-Exchange CapacityChlorideGamma Spectroscopy - Radium-226 & HitsIsotopic Thorium by Alpha SpectroscopyIsotopic Uranium by Alpha SpectroscopyMercury in Liquid Waste (Manual Cold-Vapor)Method D2216 Percent H20 Dry 105 Degrees C, weighPaint Filter TestReactive CyanideReactive SulfideSoil and Waste pHSulfideTotal Organic CarbonTrace Inductively Coupled Plasma (Iep) MetalsTrace Inductively Coupled Plasma (Iep) Metals

References:

ASTM D-5057-90SW846 9081MCAWW 300. OA

EML GA-Ol-R MODEML A-OI-R MODEML A-01-R MODSW846 7470AASTM Mois·ture,SW846 9095SW846 7.3.3SW846 7.3~4

SW846 9045CMCAWW 376.1SW846 9060SW846 6010BSW846 6010B

PREPARATIONMETHOD

ASTM D-5057-90SW846 9081MCAWW 300. OA

SW846 1311/7470. ASTM ASTM 2216

SW846 9095SW846 7.3.3SW846 7.3.4SW846 DI-LEACHAMCAWW 376.1SW846 9060

SW846 1311/3010

ASTM

EML

MCAWW

SW846

Annual Book.Of ASTM Standards.

"ENVIRONMENTAL MEASUREMENTS LABORATORY PROCEDURES MANUAL"

HASL-300 28TH EDITION! VOLUME I and II DEPARTMENT OF ENERGY

"Methods for Chemical Analysis of Water and Wastes" I

EPA-600/4-79-020, March 1983 and subsequent revisions.

"Test Methods for Evaluating Solid Waste, Physical/ChemicalMethods", Third Edition, November 1986 and its updates.



SAMPLE SUMMARY

F9E07·0213

wo # SAMPLE# CLIENT SAMPLE ID

LCJNP 001 E-65 UPPER.LCJPG 002 E-67 UPPERLCJPM 003 E-74 UPPERLCJPV 004 E-74 LOWERLCJP3 005 E-67 LOWERLCJP6 006 E-65 LOWER

NOTE(S) :

- The analytical results of the samples listed above are presented on the following pages•

• All calculations arc performed before rounding lQ avoid round-off errors in calculated results.

• Results noted as ttND II were not detected at or above the stated limit.

- This report must not be reproduced t excepl in full, without the written approval of the laboratory.

- Results for the following. parameters are never reported on a dry weight basis: colort corrosivity, density, tlashpoint, ignitability ~ layers~ od~r,

paint filter test, pH t porosity pressure, reactivity I redox potential, specifiC gravity, spot testS7 solids, solubility, temperature, viscosity t and weight_

OT # F9E070213-REVISED

SAMPLED SAMP

DATE TIME

05/04/09 14:0005/05/09 10:1505/06/09 10:3005/06/09 10:3005/05/09 10:15.05/04/09 14: 00

5 of 57


An~ews Engineering J Inc.

Client Sample ID: E-65 UPPER

TOTAL Metals

Lot-sample i ... : F9E070213-001Date Sampled.. _: 05/04/09 14:00 Date Received•• : 05/06/09'Moisture..•.• : 48

Matrix••.•... : SOLID

WORKORDER #RESULTPARAMETER

REPORTING PREPARATION-LIMIT UNITS METHOD ·ANALYSIS DATE------- ------ ----- ---------

Dilution Factor: 1

Prep Batch I ... : 9131193Uranium 121 50.0 mg/kg SW846 6010B

Analysis Time .. : 19:44

05/12-05/15/09 LCJNP1A3


Andrews Engineering, Inc.


TCLP Metals


Lot-~le I ... : F9E070213-001Date ~led..• : 05/04/09 14:00Leach Date..... : 05/13/09

Date Received.• : 05/06/09Leach Batch I .. : P913310

Matrix••••••. : SOLID

REPORTING PREPARATION- WORKPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #

Prep Batch I ... : 9134386Silver ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJNPIAJ

Dilution Factor: 1 Analysis Time .. : 00:19

Arsenic 427 20.0 ug/L SWB46 6010B 05/14-05/16/09 LCJNPLAKDilution Factor: 1 Analysis Time .. : 00:19

Barium 60.0 B,J 100 ug/L SW846 6010B 05/14-05/16/09 LCJNPlALDilution Factor: 1 Analysis Time .. : 00:19

Cadmium ND 10.0 ug/L SW846 60l0B 05/14-05/16/09 LCJNP1AMDilution Factor: 1 Analysis Time .. : 00:19

Chromium NO 20.0 ug/L SW846 GOlOB 05/14-05/l6/09 LCJNPIANDilution Factor: 1 Analysis Time .. : 00:19

Lead ND 40.0 ug/L SW846 GOlOB 05/14-05/16/09 LCJNP1APDilution Factor: 1 Analysis Time .. : 00:19

Selenium ND 30.0 ug/L SW846 6010B 05/14-05/16/09 LCJNP~Q


Analysis performed in accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311

B Estimated resull:. Result is less than RL.

J Method blank contamination. The associated method blank contains the target analyte at a reportable level.

Dilution Factor: 1

Prep BatCh I ... : 9139074Mercury ND

NOTE(S) :

1.0 ug/L SW846 7470AAnalysis Time .. : 13:21

05/19/09 LCJNP1AR




Client Sample ID: E-65 UPPER·

General Chemistry

Lot-Sample i : F9E070213-001Date S~led : 05/04/09 14:00'MOisture.•.•• : 48

Work Order # •.• : LCJNPDate Received.. : 05/06/09

Matrix••••.•.•• : SOLID

PARAMETERpH (solid)

RESULT12.4

Dilution Factor: 1

PREPBATCH #9132177

cation Exchangecapacity

10.2 2.5 meq/1DOg SW846 9081 05/15-05/20/09 9133197


Dilution Factor: 1

Chloride 18.3 J 2.0 mg/kg MCAWW 300. OA


06/01-06/02/09 9152365

Density

Paint Filter Test

1.5 g/mLDilution Factor: 1

No unitsDilution Factor: 1

ASTM D-S057-90Analysis Time .. : 00:00

SW846 9095Analysis Time .. : 00:00

06/02/09

05/09/09

9153158

9131058

Percent Moisture 48.3 0.10 '"Dilution Factor: 1

ASTM MOisture. % 05/09-05/11/09 9131062Analysis Time .. : 00:00

'rotal OrganicCarbon

0.77 B 2.0 g/kg SW846 9060 OS/21/09 9141537

Dilution Factor: 1 Analysis Time .. : ~3:38

Dilution Factor: 1

Total Sulfide

NOTE (S) :

ND 10.0 mg/kg MCAWW 376.1ADalysis Time .. : 00:00

06/02/09 9152376

RL Reporting Limit

J Method blank contamination. The associated method blank contains the target anaIyte at a reporlable level.

CNF Contains No Free Liquid

B Estimated result. Result is less than RL.




Client S~le ID: E-67 UPPER

TOTAL Metals

Lot-sample , ..• : F9E070213~002

Date sampled•.. : 05/05/09 10:15 Date Received.. : 05/06/09'Moisture..... : 47

Matr±X .: SOLID

REPORTING PREPARATION-_PARAMET_E_R R_ES_UL_T LIMIT _UN_I_T_S~ l"1E_TH_O_D AN.ALYSIS DATE

WORKORDER #

Dilution Factor: 1

Prep Batch 1_ .. : 9131193Uranium 98 .4:

LOT # F9E070213-REVISED

50.0 mg/kg 8W846 6010BAnalysis Time .. : 19:51

05/12-05/15/09 LCJPG~V

9 of 57



Client Sample In: E-67 UPPER

TCLP Metals

Lot-~le I : F9E07D213-002Date Sampled : 05/05/09 10:15Leach Date••••• : 05/13/09

Date Received.. : 05/06/09Leach Batch # •• : P913310

Matrix•.•.... : SOLID

REPORTING PREPARATION- WORKPARAMETER RESULT LIMIT UNITS METHOD ANALYSIS DATE ORDER #

Prep Batch # ..• : 9134386Silver ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJPG~


Arsenic 300 20 .. 0 ug/L SW846 6010B 05/14-05/16/09 LCJPG1AKDilution Factor: 1 Analysis Time .. : 00:26

Barimn 62.8 B,J 100 ug/L SW846 6010B 05/14-05/16/09 LCJPGlALDilution Factor: 1 Analysis Time .. : 00:26

Cadmium 1.8 B 10.0 ug/L SW846 6010B 05/14-05/16/09 LCJPGLNMDilution Factor: 1 Analysis Time .. : 00:26

Chromium ND 20.0 ug/L SW846 60l0B 05/14-05/16/09 LCJPGlANDilution Factor: 1 Analysis Time .. : 00:26

Lead NO 40.0 ug/L SW846 60l0B 05/14-05/16/09 LCJPG~P


Selenium ND 30.0 ug/L SW846 6010B 05/14-05/16/09 LCJPG1AQDilution Factor: 1 Analysis Time .. : 00:26

Analysis performed in accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1.311

B Estimated resuU. Result is less than RL.


Dilution Factor: 1

LCJPGl..AR05/19/09SW846 7470AAnalysis Time .. : 13:23

ug/L1 .. 0

NOTE (S) :

Prep BatCh I .. a: 9139074Mercury 0 .44 B




Client Sample ID: E-67 UPPER.

General Chemistry

Lot-S~le 1 : F9E070213-002Date S~led : 05/05/09 10:15% MOisture ••••• : 47

Work Order # ... : LCJPGDate Received•. : 05/06/09

Matrix••••..... : SOLID

PREPARATION- PREP

PARAMETER RESULT RL UNITS f'.mTHOD ANALYSIS DATE BATCH #

pH (solid) 12.4 0.10 No Units SW846 9045C 05/12/09 9132177

Dilution Factor: 1 Analysis Time~~: 00:00

Paint Filter Test CNF No Units SW846 9095 05/09/09 9131058Dilution Factor: 1 Analysis Time~.: 00:00

Percent Moisture

NOTR{S) :

RL Reporting Unlit


46.6 0 .. 10 !IiDilution Factor: 1

ASTM Moisture,' 05/09-05/11/09 9131062Analysis Time~~: 00:00


Andrews Engineering, Inc: _


TOTAL Metals

Lot-~le # ... : F9E070213-003Date S~led••• : 05/06/09 10:30 Date Received.. : 05/06/09t MOisture..... : 48


Matrix•••••.• : SOLID

P.ARAMETER RESULTWORKORDER #

Dilution Factor: 1

Prep Batch # ... : 9131193Uranium 83 • 9


50,,0 mg/kg SW846 6010BAnalysis Time .. : 19:57

05/12-05/15/09~V

12 of 57



Client Sample ID: B-74 UPPER

TCLP Metals

Lot-S~le I ... : F9E070213-003Date Sampled••. : 05/06/09 10:30LeaCh Date..... : 05/13/09

Date Received.. : 05/06/09Leach BatCh I .. : P913310

Matrix : SOLID

P.ARA.!liJETER RESULTREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- ---------

WORKORDER #

Prep Batch :JI: ••• : 9134386Silver ND 20.0 ug/L SW846 60l0B 05/14-05/16/09 LCJPM~

Dilution Factor: 1 .Analysis Time .. : 00:32

Arsenic 555 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJPMlAKDilution Factor: 1 Analysis Time .. : 00:32

Barimn 34.0 B,J 100 ug/L SW846 6010B 05/14-05/16/09 LCJPM1ALDilution Factor: 1 Analysis Time .. : 00:32

CadmiUDl 1.3 B 10.0 ug/L SW846 6010B 05/14-05/16/09 LCJBM1AMDilution Factor: 1 Analysis Time .. : 00:32

Chromium 30.3 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJPM1ANDilution Factor: 1 Analysis Time .. : 00:32

Lead ND 40.0 ug/L SW846 6010B 05/14-05/16/09 LCJPM1APDilution Factor: 1 Analysis Time .. : 00:32

Selenium ND 30.0 ug/L SW846 6010B 05/14-05/16/09 LCJPM1AQDilution Factor: 1 Analysis Time .. : 00:32

Analysis performed in accordance with USEPA Toxicity Characteristic Leaching Procedure Method 1311



Dilution Factor = 1

Prep Batch i ... : 9139074Mercury 0.58 B

NOTE(S):

1.0 ug!L SW846 7470AAnalysis Time .. : 13:25

05/19/09 LCJPMJ.AR



Andrews Bngineering, Inc.


General Chemistry

Lot-S~le I ... : F9E070213-003Date sampled•.. : 05/06/09 10:30% Moisture••.•. : 48

Work Order I ... : LCJPMDate Received•. : 05/06/09

Matrix.......•. : SOLID

PREPARATION- PREPPARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH it

pH (solid) 12.5 0.10 No Units S1f846 9045C 05/12/09 9132177Dilution Factor: 1 Analysis Time .. : 00:00

Paint Filter Test CNF No Units SW846 9095 05/09/09 9131058Dilution Factor: 1 Analysis Time .. ~ 00:00

Percent Moisture

NOTE (S) :

RL Reporting Limit


48.4 0.10 ,Dilution Factor: 1

ASTM Moisture, , 05/09-05/11/09 9131062Analysis Time .. : 00:00



Andrews Engineering. Inc.

Client Sample In: E-74 LOtmR

TOTAL Meta1s

Lot-Sample I ... : F9E070213-004Date Sampled••. : 05/06/09 10:30 Date Received.. : 05/06/09'MOisture..... : 48


WORKORDER #RESULTPARAMETER

REPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE------- ------ ----- ------~-----

Dilution Factor: 1

Prep Batch i ... : 9131193uranium. 188 50.0 mg/kg SW846 6010B


05/12-05/15/09 LC~V




Client Sample In: E-74 LOWER

TCLP Meta1s

Lot-Sample D._.: F9E070213-004Date sampled.•. : 05/06/09 10:30LeaCh Date•.... : 05/13/09

Date Received•. : 05/06/09Leach Batch I ... : P913310

Matrix.•..... : SOLID

PARAMETERREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- ---------

WORKORDER #

Prep Batch # ••• : 9134386Silver ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJPV1AJ


Ars~c 88.1 20.0 ug/L SW846 6010B 05/14-05/16/09~Dilution Factor: 1 Analysis Time .. : 00:38

BarilDD. 26.3 B,J 100 ug/L SW846 6010B 05/14-05/16/09 LC~Dilution Factor: 1 Analysis Time .. : 00:38

Cadmium ND 10.0 ug/L SW846 6010B 05/14-05/16/09 LCJPV1AMDilution Factor: 1 Analysis Time .. : 00:38

Chromium ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJPV1ANDilution Factor: 1 Analysis Time .. : 00:38

Lead ND 40.0 ug/L SW846 6010B 05/14-05/16/09 LCJPV1APDilution Factor: 1 Analysis Time .. : 00:38

Selenium ND 30.0 ug/L SW846 6010B 05/14-05/16/09 LCJPVIAQDilution Factor: 1 Analysis Time .. : 00:38

Dilution Factor: 1

Prep Batch i ... : 9139074Mercury ND

NOTE(S):

1.0 ug/L SW846 7470AAnalysis Time .. : 13:27

05/19/09 LCJPV1AR

Analysis performed in accordance with USEPA Toxicity Cbaracteristic Leaching Procedure Method 1311





Andrews Engineering. J:nc .

Client sample ID: E-74 LOWER.

General Chemistry

Lot-Sample 1_ •• : F9E070213-004Date Sampled_._: 05/06/09 10:30l Moisture..... : 48

Work Order # ... : LCJl?VDate Received.• : 05/06/09

Matrix_ ... __ ... : SOLID

PREPARATION- PREPPARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH #

pH (solid) 12 .. 6 0.10 No Units SW846 9045C 05/12/09 9132177Dilution Factor~ 1 Analysis Time .. : 00:00

Paint Filter Test CNF No Units SW846 9095 05/09/09 9131058Dilution Factor: 1 Analysis Time .. : 00:00

Percent Moisture

HOTE(S):RL Reporting Limit


48.4 0.10 tDilution Factor: 1

ASTM Moisture,' 05/09-05/11/09 9131062Analysis Time .. : 00:00




Client Sample ID: £-67 LONER

TOTAL Metals

Lot-sample I ... : F9E070213-00SDate Sampled••• : 05/05/09 10:15 Date Received•• : 05/06/09t MOisture..... : 48

Matrix : SOLID

REPORTING PREPARATION- WORK_PARAl'tmTE_R RE_S_UL_T LIMIT _UN_I_T_S ME_T_H_O_D ANALYSIS DATE ORDER #

Dilution Factor: 2

Prep BatCh I ... : 9131193Uranium 1280


100 mg/kg SW846 6010BAnalysis Time .. : 20;10

05/12-05/15/09 LCJP3~V

18 of 57



Client sample m: :£-67 LOWER

TCLP Metals

Lot-~le I : F9E070213-005Date sampled : 05/05/09 10:15LeaCh Date : 05/13/09

Date Received.• : 05/06/09Leach Batch # .. : P913310

Matrix..•.•.• : SOLID

METHODPARAMETERREPORTINGLIMIT UNITS-----

PREPARATIONANALYSIS DATE---------

WORKORDER #

Prep Batch # ... : 9134386Silver ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJP3lAJ

Dilution Factor: i Analysis Time .. : OO~45

Arsenic 104 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJP31AKDilution Factor: 1 Analysis Time .. : 00:45

Barium 50.4 B,J 100 ug/L SW846 60108 05/14-05/16/09 LCJP31ALDilution Factor: 1 Analysis Time .. : ·00:45

Cadmium ND 10.0 ug/L SW846 6010B 05/14-05/16/09 LCJP31AMDilution Factor: 1 Analysis Time .. : 00:45

Chromium ND 20.0 ug/L SW846 6010B 05/14-05/16/09 LCJP31ANDilution Factor: 1 Analysis Time .. : 00:45

Lead ND 40.0 ug/L SW846 6010B 05/14-Q5/16/09 LCJP31APDilution Factor: 1 Analysis Time .. : 00:45

Selenium ND 30.0 ug/L SW846 6010B 05/14-05/16/09 LCJP31AQDilution Factor: 1 Analysis Time .. : 00:45

Analysis performed in accordance with USEPA Toxicity Char4lcteristic Leaching Procedure Method 1311


J Method blank comamination. The associated method blank contains the target analyte at a reportable level.

Dilution Factor: 1

LCJP31AR05/19/09SW846 7470AAnalysis Time .. : 13:29

ug/L1.0

NOTE(S) :

Prep BatCh 1 __ .: 9139074

Mercury ND




Client Samp1e ID: E-67 LOWER

General Chemistry

Lot-Sample I ... : F9E070213-00SDate S~led•.• : 05/05/09 10:15% Moisture••.•• : 48

Work Order i ... : LCJP3Date Received•• : 05/06/09

Matrix : SOLID

PREPARATION- PREP

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH #



Paint Filter Test CNF No Units SW846 9095 05/09/09 9131058


Percent Moisture

HQTE(S) :

RL Reporting Limit


47.9 0.10 "Dilution Factor: 1

ASTM MOisture, t 05/09-05/11/09 9131062Analysis Time .. : 00:00


Andrews Engineering, Inc ..

Client sample ID: :8-65 LOWER

TOTAL Meta1s

Lot-Sample i ... : F9E070213-006Date Sampled••. : 05/04/09 14:00 Date Received•. : 05/06/09, Moisture..... : 50


Matrix : SOLID

PARAMETER RESULTWORKORDER #

Dilution Factor: 1

Pr~ BatCh # ... : 9131193Uranium 391 50.0 .mg/kg SW846 6010B


05/12-05/15/09 LCJP61A5


------------------------------~----


.Andrews Engineering, Inc.

Client Sample In: B-65 LOWER

TCLP Metals

Lot-Sample i : F9E070213-006Date Sampled : 05/04/09 14:00LeaCh Date : 05/13/09

Date Received.. : 05/06/09Leach Batch I ... : P913310

Matrix..•.... : SOLID

PARAMETER RESULTREPORTING PREPARATION-LIMIT UNITS METHOD ANALYSIS DATE----- ---------

WORKORDER #

Analysis performed in accordance with USEPA Toxicity Characteristic Leachjng Procedure Method 1311



2040 ug/L SW846 GOlOB 05/14-05/16/09 LCJP61AMDilution Factor: 1 Analysis Time .. : 00:51

20.0 ug/L SW846 60l0B 05/14-05/16/09 LCJP61ANDilution Factor: 1 Analysis Time .. ; 00:51

100 ug!L SW846 601DB 05/14-05/16/09 LOJP61APDilution Factor: 1 Analysis Time .. : 00:51

10.0 ug/L SW846 GOlOB 05/14-05/16/09 LCJP61AQDilution Factor: 1 Analysis Time .. : 00:51

20.0 ug/L SW84"6 GOlOB 05/14-05/16/09 LCJP61ARDilution Factor: 1 Analysis Time .. : 00:51

40.0 ug/L SW846 GOlOB 05/14-05/16/09 LCJP61ATDilution Factor: 1 Analysis Time .. : 00:51

30.0 ug/L SW846 6010B 05/14-05/16/09 LCJP61AUDilution Factor: 1 Analysis Time .. : 00:51

Dilution Factor: 1

LCJP61AV05/19/09SW846 7470AAnalysis Time .. : 13:31

ug/L1.0

NQTE(S) :

Prep BatCh i ... : 9134386Silver ND

Prep BatCh I ... : 9139074Mercury 0 .24 B

Arsenic 128

Barium 54.3 B,J

Cadmium ND

Chromium ND

Lead ND

Selenium


TestArnerica St. Louis

Andrews Engineering, Inc ..

Client Sample m: E-65 LOWER

General Chemistry

Lot-sample I ... : F9E070213-006Date Sampled..• : 05/04/09 14:00'Moisture..... : 50

Work Order i ... : LCJP6Date Received•• : 05/06/09

Matrix........• : SOLID

PREPARATION- PREP

PARAMETER RESULT RL UNITS METHOD ANALYSIS DATE BATCH #


Dilution Factor: 1 Analysis Time ... : 00:00

Cation Exchange 9.1 2.5 meq/lOOg 8W846 9081 0'5/15-05/20/09 9133197Capacity


Chloride 24.3 J 2.0 mg/kg MCAIiIf 300.0A 06/01-06/02/09 9152365Dilution Factor: 1 Analysis Time .. : 00:00

Density 1.3 g/mL ASTM D-5057-90 06/02/09 9153158

Dilution Factor: 1 Analysis ~ime .. : 00:00

Paint Filter Test CNF No Units SW846 9095 05/09/09 9131058Dilution Factor: 1 Analysis Time .. : 00:00

Percent Moisture 50.1 0.10 %Dilution Factor: 1

ASTM MOisture, , 05/09-05/11/09 9131062Analysis Time .. : 00:00

Dilution Factor: 1

Reactive Cyanide ND 0.25 mg/kg SW846 7 .. 3.3Analysis Time .. : 00:00

OS/25-05/26/09 9145035

RL Reporting Umit



Dilution Factor: 1

Dilution Factor: 1

9141537

9145034

9152376

OS/21/09

OS/25/09

06/02/09

SW846 9060


MCAWW 376.1Analysis Time .. : 00:00

SW846 7.3.4Analysis Time .. : 00:00

mg/kg

mg/kg

g/kg

10.0

2.0

22.2Dilution Factor: 1

ND

2.7

ND

Total OrganicCarbon

ROTE (S) :

Total Sulfide

Reactive Sulfide



METHOD BLANK REPORT

TOTAL Metals

Client Lot I ... : F9E070213 Matrix•••..•... : SOLID

REPORTING PREPARATION-_PARAMET_E_R R_E_S_U_L_T LIMIT ....;..UN__I_T..;..S ME_TH_O_D_----- ANALYSIS DATE

WORKORDER #

MB Lot-Sample #: F9EII0000-193 Prep Batch # ... : 9131193Uranium ND 50.0 mg/kg SW846 6010B

Dilution Factor: 1

Analysis Time .. ~ 13:17

:HOTE(S) :

Calculations are performed before rounding to avoid round-off errors in calculated results.


05/12-05/14/09 LCP951AA

24 of 57

METHOD BI..d\NX REPORT

TCLP Metals

Client Lot I ... : F9E070213


·Matrix.•••••••• : SOLID

PARAMETER RESULTREPORTINGLIMIT UNITS----- l"tETHOD

WORKORDER i

MB Lot-Sample #: F9E130000-303 Prep Batch #~ •• : 9139074Leach Date..... : 05/13/09 Leach BatCh I .. : P913310Mercury NO 1.0 ug/L SW846 7470A

Dilution Factor: 1


05/19/09 LCXAF1AJ

MB Lot-Sample I: F9E130000-303 Prep BatCh fi ..• : 9134386Leach Date.•... : 05/13/09 Leach Batch ft .• : P913310Arsenic ND 20.0 ug/L SW846 6010E

Dilution Factor: 1


05/14-05/15/09 LCXAF1AC

Barium 3.9 B 100 ug/LDilution Factor: 1


SW846 6010B 05/14-05/15/09 LCXAF1AD

Cadmium ND 10.0 ug/L SW846 6010B 05/14-05/15/09 LCXAF1AE

Lead 3.6 B 40.0 ug/L 8W846 6010B 05/14-05/15/09 LCXAF1AGDilution Factor: 1


Selenium ND 30 .. 0 ug/L SW846 6010B 05/14-05/15/09 LCXAFIAHDilution Factor: 1




Chromium

Silver

NOTE(S) :

ND

Dilution Factor: 1


20.0 ug/LDilution Factor: 1


20.0 ug/LDilution Factor: 1


SW846 60l0B

SW846 6010B

05/14-05/15/09 LCXAF1AF

05/14-05/15/09 LCXAF1AA


· TestAmerica St. Louis

METHOD BLANK REPORT

General Chemistzy

Client Lot I ... : F9E070213 Matrix............ : SOLID

REPORTING PREPAR.A.TION- PREPP.ARAJvIETER RESULT LIMIT UNITS IvIETHOD ANALYSIS DATE BATCH #Cation Exchange Work Order #: LCWVMlAA MB Lot-Sample #: F9E130000-197

CapacityND 0.50 meq/1OOg SW846 9081 05/15-05/20/09 9133197

Dilution Factor: 1


Chloride Work Order #: LD6PP1AA ME Lot-Sample #: F9F01OOOO-3650.24 B 2.0 mg/kg MCAJfW 300.0A 06/01-06/02/09 9152365

Dilution Factor: 1


Reactive Cyanide Work Order #: LDN3J1AA MB Lot-Sample #: F9E250000-035NO 0.25 mg/kg SW846 7.3.3 OS/25-05/26/09 9145035

Dilution Factor: 1


Reactive Sulfide Work Order #: LDN3H1AA MB Lot-Sample #: F9E2S0000-034ND 22.2 mg/kg SW846 7.3 .. 4 OS/25/09 9145034

Dilution Factor: 1


Total Organic Work Order #: LDH7D1AA MB Lot-Sample #: D9E210000-S37Carbon

ND 2.0 g!kg SW846 9060 OS/21/09 9141537Dilution Factor~ 1


Total Sulfide

NOTE (S) :

ND

Work Order #: LD5R11AA ME Lot-Sample #: F9F010000-37610.0 mg/kg MCAWW 376.1 06/02/09 9152376

Dilution Factor: 1Analysis Time .. : 00:00

Calculations are performed before rounding to avoid round·off errors in calculated resul[S.


OT # F9E070213-REVISED 26 of 57


LABORATORY CONTROL SAMPLE EVALUATION REPORT

TOTAL Metals

. Client Lot I. __ : F9E07D213 Matrix.•.•••••• : SOLID

PARAMETERPERCENTRECOVERY

RECOVERY

LIMITSPREPARATION-

M_E_T_H_O_D ANALYSIS DATE WORK ORDER #

LCS Lot-S~le#: F9Ell0000-l93 Pr~ Batch #_._: 9131193Uranium 106 (80 - 120) SW846 60l0B 05/12-05/14/09 LCP951AC

Dilution Factor: 1

NOTE (8) :

Calculations are pcrfonned before rounding to avoid round-off errors in calculated results.



27 of 57


LABORATORY CONTROL SAMPLE EYALUATIOB REPORT

TCLP Metals

Client Lot I ... : F9E070213 Matrix..••••••. : SOLID

PARAMETER

PERCENTRECOVERY

RECOVERY

LIMITSPREPARATION

_ME_T-H-O-D------ ANALYSIS DATE WORK ORDER #

LeS Lot-sampleD: F9E140000-386 Prep Batch I ... : 9134386Silver 97 (80 - 120) SW846 60l0B 05/14-05/15/09 LC2PT~


Arsenic 111 (BO - 120) SW846 601GB 05/14-05/15/09 LC2PTlACDilution Factor: 1 Analysis Time .. : 23:28

Barium 113 (80 - 120) SW846 6010B 05/14-05/15/09 LC2PT1ADDilution Factor: 1 Analysis Time .. : 23:28

Cadmium 110 (80 - 120) SW846 60l0B 05/14-05/15/09 LC2PT1AE


Chromium 107 (80 - 120) SW846 6010B 05/14-05/15/09 LC2PTIAFDilution Factor: 1 Analysis Time .. : 23:28

Lead 108 (80 ... 120) SW846 6010B 05/14-05/15/09 LC2PT1AGDilution Factor~ 1 Analysis Time .. : 23:28

Selenium 111 (80 - 120) SW846 6010B 05/14-05/15/09 LC2PT1AHDilution Factor: 1 Analysis Time .. : 23:28

LCS Lot-Sample#: F9E190000-0i4 Prep Batch # ... : 9139074Mercury 94 (80 - 120) SW846 7470A

Dilution Factor: 1

NOTE(S) :



05/19/09Analysis Time .. : 13:04

LC9481AA

28 of 57



General Cheai.stry

Lot-S~le # ... : F9E070213 Matrix••....... : SOLID

PERCENTPARAMETER RECOVERYTotal Organic

Carbon

RECOVERY RPD PREPARATI ON- PREPLIMITS RPD LIMITS _ME_T....;H~O...;,D ANALYSIS DATE BATCH #

WO#:LDH7D~C-LCS/LDH7D~-LCSD LCS Lot-Sample#: D9E210000-537

6958

(46 - 130)

(46 - 130) 17SW846 9060

(0-20) SW846 9060OS/21/09OS/21/09

9141537

9141537

ROTE (8) :

Dilution Factor: 1 Arialysis Time .. : 13:16





General Chemistry

Client Lot I ... : F9E070213 Matrix•.•••.••• : SOLID

PREPARATION- PREPANALYSIS DATE BATCH #

LCS Lot-Sample#: F9E120000-17705/12/09 9132177

RECOVERY

LIMITS METHOD---------Work Order #: LC9E71AA

(99 - 101) SW846 9045C100

PERCENTRECOVERYPARAMETER

pH (solid)


Chloride95

Work Order #: LD6PPIAC Les Lot-Sample#: F9FOIOOOO-365(90 - 110) MCAWW 300.0A 06/01-06/02/09 9152365Dilution Factor: 1 Analysis Time .. : 00:00

Reactive cyanide0.0

Work Order #: LDN3J1AC(10 - 75) SW846 7.3.3

Les Lot-Sample#: F9E250000-035OS/25-05/26/09 9145035


Reactive Sulfide27

Work Order #: LDN3H1AC(10 - 128) SW846 7.3.4

LCS Lot-Sample#: F9E250000-034OS/25/09 9145034

Dilution Factor: 1 A?alysis Time .. : 00:00

Total Sulfide97

Work Order #: LD5RllAC(90 - 110) MCAWW 376.1

Les Lot-Sample#: F9FOIOOOO-37606/02/09 9152376


NOTE(S) :

Calculaoons are performed before rounding to avoid round·off errors in calculated results.



MATRIX SPIKE SAMPLE EVALUATION REPORT

TOTAL Metals

Client Lot I ... : F9E070213Date Sampled••• : 05/04/09 13:15 Date Received•• : 05/06/09

Matrix.••...... : SOLID

PARAMETERPERCENT RECOVERY

RECOVERY LIMITSRPD PREPARATION-

RPD ~IMITS _ME_TH_O_D ANALYSIS DATE

WORKORDER #

Uranium 115 (75 - 125) SW846 6010B102 (75 - 125) 5.6 (0-30) SW846 6010B

Dilution Factor: 1


MS Lot-~le I: F9E070159-001 Prep BatCh #.~.: 9131193'Moisture..... : 4505/12-05/14/09 LCH811AE05/12-05/14/09 LCHBI1AF

NOTE(S) :




MATRIX SPIKE SAMPLE DATA REPORT

TOTAL Metals

Client Lot # ••• : F9E070213Date S~led... : 05/04/09 13:15 Date Received•• : 05/06/09

Matrix•. _._ .. _.: SOLID

SA1'1PLE SPIKE MEASRDPARAMETER AMOUNT Al\1T .AMOUNT---- UNITS

PERCNT PREPARATION-RECVRY RPD METHOD ANALYSIS DATE-------

WORKORDER #

MS Lot-S~le #: F9E070159-001 ~ Batch I ... : 9131193, Moisture_ •••• : 45

Uranium111

111100100

226213

mg/kgmgjkg

11.5102

SW846 6010B5.6 SW846 60l0B

05/12-05/14/09 LCH81lAE05/12-05/14/09 LCH811AF

NOTE (8) :

Dilution Factor: 1


Calculations are performed before rounding to avoid round-off errors in calculated resuhs.




TCLP Metals

Client Lot I ... : F9E070213Date 8amp1ed••• : 04/27/09 14:25 Date Received.. : 05/01/09

Matrix..•..•..• : SOLID

PARAMETERPERCENT RECOVERYRECOVERY LIMITS

RPDRPD LIMITS

PREPARATION-_ME_TH_O~D ~~_ ANALYSIS DATE

WORKORDER #

MS Lot-~le I: F9E010256-001 Prep BatCh t ... : 9134386LeaCh Date ..... : 05/13/09 LeaCh BatCh # .. : P913310Arsenic 104 (75 - 125) SWB46 6010B

103 (75 - 125) 0.97 (O-20) SW846 60l0BDilution Factor: 1Analysis Time .. : 23:47

05/14-05/15/09 LA7D6~3

05/14-05/15/09 LA7D6lA4

Barium 113112

(75 - 125)(75 - 125) . 0.93 (0-20)

Dilution Factor: 1


SW846 60l0BSW846. 6010B

05/14-05/15/09 LA7D61A505/14-05/15/09 LA7D61A6

Cadmium 97

96(75 - 125)

(75 - 125) 1.0SW846 6010B

(0-20) SW846 60l0B05/14-05/15/09 LA7D61A705/14-05/15/09 LA7D61A8

MS Lot-Sample #: F9E010256-001Leach Date..... : 05/13/09

Prep Batch # ... : 9139074Leach Batch :ft •• : P913310(Continued on next page)

Chromium

Lead

Selenium

Silver

9696

9796

9998

107106


(75 - 125)(75 - 125) 0 .. 82 (0-20)

Dilution Factor: 1


(75 - 125)( 75 - 125) 0 .. 66 ( 0 - 20)

Dilution Factor: 1


(75 - 125)(75 - 125) 0.58 (0-20)

Dilution Factor: 1


(75 - 125)(75 - 125) 0.72 (0-20)

Dilution Factor: 1


SW846 6010BSW846 6010B

SW846 6010BSW846 6010B

SW846 6010BSW846 60l0B

SW846 6010BSW846 6010B

05/14-05/15/09 LA7D61A905/14-05/15/09 LA7D61CA

05/14-05/15/09 LA7D61CC05/14-05/15/09 LA7D61CD

05/14-05/15/09 LA7D61CE05/14-05/15/09 LA7D6lCF

05/14-05/15/09 LA7D61Al05/14-05/15/09 LA7D61A2



TCLP Metals

Client Lot •... : F9E070213Date samp1ed .•• : 04/27/09 14:25 Date Received•. : 05/01/09


Matrix••....... : SOLID

PARAMETERMercury

PERCENTRECOVERY7876

RECOVERY

LIMITS RPD(70 - 130)

(70 - 130) 1 .. 6

RPD

LIMITS

(0-20)

METHODSW846 7470ASW846 7470A

WORKORDER #LA7D61CGLA7D61CH

NOTE(S) :

Dilution Factor: 1



LOT # F9E070213-REVISED . 34 of 57



TCLP Metals

Client Lot 1: ••• : F9E070213 Matrix......... : SOLIDDate Sampled••• : 04/27/09 14:25 Date Received~.: 05/01/09

SAMPLE SPIKE MEASRD PERCNT PREPARATION- WORKPARAMETER .AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD ANALYSIS DATE ORDER #

MS Lot-Sample I: F9E010256-001 Prep Batch # ... : 9134386Leach Date•. _.• : 05/13/09 Leach Batch # •• : P913310

Arsenic146 2000 2230 ug/L 104 SWB46 6010B 05/14-05/15/09 LA7D61A31.46 2000 2200 ug/L 103 0.97 SW846 60l0B 05/14-05/15/09 LA7D61A4

Dilution Factor: 1


Barium57.7 2000 2320 ug/L 113 SW846 60l0B 05/14-05/15/09 LA7D61A5

57.7 2000 2300 ug/L 112 0.93 SW846 60l0B 05/14-05/15/09 LA7D61A6Dilution Factor: '1

Analysis Time w ~ : 23:47

CadmiumND 2000 1930 ug/L 97 SW846 6010B 05/14-05/15/09 LA7D61A7

ND 2000 1910 ug/L 96 1.0 SW846 6010B 05/14-05/15/09 LA7D61A8Dilution Factor: 1


ChromiumNO 2000 1930 ug/L 96 SW846 6010B 05/14-05/15/09 LA7D61A9ND 2000 1910 ug/L 96 0.82 SW846 60l0B 05/14-05/15/09 LA7D61CA

Dilution Factor: 1


LeadND 2000 1940 ug/L 97 SW846 GOlOB 05/14-05/15/09 LA7D61CCND 2000 1920 ug/L 96 0.66 SW846 60l0B 05/14-05/15/09 LA7D61CD

Dilution Factor: 1

Analysis Time. 4 : 23:47

SeleniumND 2000 1980 ug/L 99 SW846 6010B 05/14-05/15/09 LA7D61CEND 2000 1970 ug/L 98 0.5B SWB46 6010B 05/14-05/15/09 LA7D61CF

Dilution Factor: 1


SilverND 200 213 ug/L 107 SW846 6010B 05/14-05/15/09 LA7D61AlND 200 212 ug/L 106 0.72 SW846 6010B 05/14-05/15/09 LA7D61A2

Dilution Factor: 1


MS Lot-Sample #: F9E010256-001 Prep Batch :It ..... : 9139074Leach Date ..... : 05/13/09 Leach Batch :If: .... : P913310

LOT # F9E070213-REVISED (Continued on next page) 35 of 57


MATRIX. SPIKE SAMPLE DATA REPORT

TCLP Meta1s

Client Lot I ... : F9E070213Date S~led. __ : 04/27/09 14:25 Date Received.. : 05/01/09

Matrix..•...... : SOLID

SAMPLE SPIKE MEASRD PERCNT PREPARATION-P.ARAIv1ETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD .ANALYSIS DATE---- ------ -------Mercury

NOTE (S) :

ND

ND

25.025.0

19.4 ug/L 7819.1 ug/L 76


SWB46 7470A1.6 SWB46 7470A

05/19/0905/19/09

WORKORDER #

LA7D61CGLA7D61CH

Calculations are performed before rounding to avoid. round-off errors in calculated results.


· .. __._-._.__ .- ------



General Chemistry

Client Lot I : F9E070213Date Sampled : 05/12/09 10:24 Date Received .• : 05/13/09

Matrix.•..•...• : SOLID

Total OrganicCarbon

WO#: LCQ4T1AD-MS/LCQ4T1AE-MSD

PARAMETERPERCENT RECOVERYRECOVERY LIMITS

RPD PREPARATION- PREP

RPD LIMITS ME__TH_O_D_~~__ ANALYSIS DATE BATCH #'MOisture..... : 3.5

ME Lot-Sample #: D9E1I0164-011

HOTE(S) :

101101

(46 - 130)

(46 - 130) 0.08 (0-20)

Dilution Factor: 1Analysis Time.. : ~3:26

SW846 9060SW846 9060

OS/21/09OS/21/09

91415379141537

Calculations are perfonned before rounding to avoid round-off errors in calculated results.

N Spiked analyte recovery is outside stated control limits.




General Chemistry·

Client Lot I ... : F9E070213Date Sampled.~_: 05/12/09 10:24 Date Received.. : 05/13/09

Matrix : SOLID

SAMPLE SPIKE MEASRD

PARAMETER AMOUNT AMT AMOUNT----- UNITS

Total OrganicCarbon

PREPARATION- PREP_ME_T_H_O_D ANALYSIS DATE BATCH #

% Moisture••••. : 3.5WO#: LCQ4TIAD-MS/LCQ4T1AE-MSD MS Lot-Sample #: D9El10164-011

ND

ND120120

122122

g/kgg/kg

101101

SW846 90600.08 SW846 9060

OS/21/09OS/21/09

91415379141537

ROTE (S):

Dilution Factor: 1



N Spiked analytc recovery is outside stated control limits.




General Chemistry

Client Lot I ... : F9EO?0213Date S~led.•• : 05/04/09 14:00 Date Received•. : 05/06/09

Matrix : SOLID

Percnt Moisture: 45PERCENT

PARAMETER RECOVERYChloride

104

RECOVERY PREPARATION- PREPLIMITS _ME_TH_O_D ANALYSIS DATE BATCH #Work Order # ... : LCJNPIA9 MS Lot-Sample #: F9E070213-001{90 - 110} MCAWW 300.0A 06/01-06/02/09 9152365Dilution Factor: 1 Analysis Time .. : 00:00

Reactive Cyanide0.0

Work Order # ... : LCJP6~9 MS Lot-Sample #: F9E070213-006(10 - 45) SW846 7.3.3 OS/25-05/26/09 9145035Dilution Factor: 1 Analysis Time .. : 00:00

Reactive Sulfide22 N

Work Order # ... : LCJP6~7

(10 - 121) SW846 7.3.4MS Lot-Sample #: F9E070213-006

OS/25/09 9145034Dilution Factor~ 1 Analysis Time .. : 00:00

Total Sulfide98 N

Work Order # ... : LC1M61A4(O.o- 0.0) MCAWW 376.1

MS Lot-Sample #: F9E140145-00206/02/09 9152376

NOTE (S) :

Dilution Factor: 1 Analysis Time .. ~ 00:00


N Spiked analyte recovery is outside stated control limits.




General Chemist:ry

Client Lot I : F9E070213Date sampled : 05/04/09 14:00 Date Received•• : 05/06/09·

Matrix__ ......• : SOLID

Percnt Moisture: 45

SAMPLE SPIKEPARAMETER AMOUNT AMT

Chloride18.3 20.0

MEASURED PERCENT PREPARATION- PREPAMOUNT UNITS RECOVERY METHOD ANALYSIS DATE BATCH #

Work Order #••• : LCJNP1A9 MS Lot-Sample #: F9E070213-00139.2 mg/kg 104 MCAWW 300.0A 06/01-06/02/09 9152365


Reactive CyanideND 6.25

Work Order # ... : LCJP61A9mg/kg 0.0

MS Lot-Sample #: F9E070213-006SW846 7.3.3 OS/25-05/26/09 9145035


Reactive SulfideND 200

Work Order # .•• : LCJP61A744.5 N mg/kg 22

ME Lot-Sample #: F9E070213-006SW846 7.3.4 OS/25/09 9145034

Dilution Factor: 1 Analysis Time •. : 00:00

Total SulfideND 1000

Work Order # ... : LCIM61A4980 N mg/kg 98

MS Lot-Sample #: F9E140145-002MCAWW 376.1 06/02/09 9152376

NOTE(S) :



N Spiked analyte recovery is outside stated conlrollimits.



SAMPLE DUPLICATE EVALtIATIQR REPORT

General Chemistry

PREP

BATCH #

9131058

Matrix..••.•• : SOLID

RPD PREPARATION-LIMIT METHOD ANALYSIS DATE

SD Lot~Sample #: F9D230347-001(0-0.0) SW846 9095 05/09/09

Analysis Time~~: 00:00

RPD

Work Order I ... : LAM2F-SMPLAM2F-DUP

Date Received.. : 04/23/09

No Units 0Dilution Factor: 1

UNITS-----


PARAM RESULT

Paint Filter Test

Date Samp1ed.•• : 04/21/09 13:05'Moisture..... : 46

DUPLICATERESULT



SAMPLE DUPLICATE EVALUATION REPORT

General Chemistry

Dilution Factor: 1


PREPARATION- PREPMETHOD ANALYSIS DATE BATCH #SD Lot-Sample #: F9E070213-006

(O-O.O) ASTM Moisture, % 05/09-05/~1/09 9131062Analysis Time .. : 00:00

RPD

LIMIT

0.26

RPD

Work Order I ... : LCJP6-SMPLCJP6-DUP


%50.2

Client Lot # •.. : F9E070213

PARAM RESULTPercent Moisture

50.1

Date sampled : 05/04/09 14:00% MOisture : 50

DUPLICATERESULT

Dilution Factor: 1

Reactive CyanideND ND mg/kg o

SD Lot-Sample #: F9E070213-006(0-30) SW846 7.3.3 OS/25-05/26/09 9145035


Dilution Factor: 1

Reactive SulfideND ND mg/kg o

SD Lot-Sample #: F9E070213-006(0-20) SW846 7.3.4 OS/25/09


9145034




General Chemistry

Work Order I ... : LCJNP-SMPLCJNP-DUP

Date Received•. : 05/06/09

Matrix•.•.... : SOLID

PREPARATION- PREP

METHOD ANALYSIS DATE BATCH #SD Lot-Sample #: F9E070213-001MCAWW 300.0A 06/01-06/02/09 9152365

RPDLIMIT

(0-20)0.78

RPD

mg!kg18.5

UNITS-~-~-~


Date Sampled••• : 05/04/09 14:00~ Moisture..... : 48

DUPLICATERESULTPARAM RESULT

Chloride18.3 J


pH (solid)12.4 12.6 No Units 1.7

Dilution Factor: 1

SD Lot-Sample #: F9E070213-001(0-0.0) SW846 9045C 05/12/09


9132177

SD Lot.-Sample #: F9E070213-001


Cation ExchangeCapacity

10.2 9.7 meq/100g 5.8Dilution Factor: 5

(0-30) SW846 9081 05/15-05/20/09 9133197

HOTE(S) :

Calculations are performed before rounding to avoid round~off errors in calculated results.

J Method blank contamination. The associated method blank. contains the target anatyre at a reportable level.




General Chemistry

9152376

Matrix : SOLID

a

RPD PREPARATION- PREPRPD LIMIT METHOD ANALYSIS DATE BATCH #

SD Lot-Sample #: F9E140145-002(0-0.0) MCAWW 376.1 06/02/09

Work Order # ••• : LC1M6-SMPLC1M6-DUP

Date Received•• : 05/13/09

mg/kgND

UNITS-----

C1ient Lot I ... : F9E070213

PARAM RESULT

Total SulfideND

Date S~led... : 05/12/09 10:24, MOisture •.••• : 45

DUPLICATERESULT

Dilution Factor: l Analysis Time .. : 00:00




General Chemistry

9153158

Matrix•.••..• : SOLID

RPD PREPARATION- PREPLIMIT METHOD ANALYSIS DATE BATCH #

SD Lot-Sample #: F9E140145-001(0-0.0) ASTM D-5057-90 06/02/09

RPD

6.5

Work Order i ... : LC1MO-SMPLC1MO-DUP


g/mL1.4

UNITS-----

Client Lot i ... : F9E070213

Date Sampled.•• : 05/12/09 10:15, MOisture..... : 47

DUPLICATERESULTPARAM RESULT

Density1.5





Client SamDle ID: 1-65 UPPER

Radiochemistry

Lab Sample ID: F9E070213-001Work Order: LCJNPMatrix: SOLID

Date Collected:Date Received:

05/04/0905/06/09

14001855

A.. Ol-R MODOS/21/09 OS/29/09 9141383 77

OS/21/09 OS/29/09 9141383 77OS/21/09 OS/29/09 9141383 77

A-Ol-R HODOS/21/09 05/30/09 9141381 87

OS/21/09 05/30/09 9141381 87

OS/21/09 05/30/09 9141381 87

05/11/09 06/01/09 9131396

Yld ,AnalysisDate BatCh I

GA-Ol .. R MOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

PrepDate

'rotaluncert.

Parameter Result Qua.l (2 0+/-) MOe

Gamma Ra~226 &. Hits By DOE GA-Ol0R MOD pCi/gBismuth 214 0.89 0.29 0.33

Lead 212 0.11 U 0.17 0.30

Lead 214 1.12 0.29 0.29

Protactinium 234M 97 21 8

Protactinium 231 -0.02 U 2.4 4.2

Radium (226) 0.89 0.29 0.33

Thorium 232 0.0 U 0.45 0.82

Thorium 234 81.0 9.0 6.0

Uranium 235 4.3 1.0 1.0

--- Other Detected Radionuclides

Potassium 40 5.7 1.9 2.3

Iso URANIUM (SHORT CT) DOE A.. Ql-R MOD pCi/gUranium 234 58.1 5.4 0.2

Uranium 235/236 3.60 0.74 0.21

Uranium 238 60.5 5.7 0.2

Iso THORIUM (SHORT CT) DOE A-Ol-R MOD pCi/gThorium 228 0.01 U 0.12 0.25

Thorium 230 1.04 0.33 0.19

Thorium 232 0.028 U 0.066 0.13

NOTE (S)

Data are incomplete without the case narrative.

MOC is determined by instrument performance only.Bold results are greater tban the MOe




Client Sam~le ID: ~-67 UPPER

Radiochemistry

Lab Sample ID: F9E070213-002Work Order: LCJPGMatrix: SOLID


05/05/0905/06/09

10151855

A-Ol-R MODQ5/21/09 OS/29/09 9141383 58

OS/21/09 OS/29/09 9141383 58

OS/21/09 OS/29/09 9141383 58

A-Ol-R MODOS/21/09 05/30/09 9141381 89

OS/21/09 05/30/09 9141381 89

OS/21/09 05/30/09 9141381 89

05/11/09 06/01/09 9131396

GA-Ol-R MOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 913139605/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

Ylcl ,AnalysisDate EBtch #

prepDate

TotalUncert.

Parameter Result Qual (2 (1+/-) MDC

Gamma Ra-226 & Hits By DOE GA-Ol0R MOD pCi/gBismuth 214 0.61 0.23 0.24

Lead 212 0.09 U 0.13 0.23

Leaa 214 0.73 0.24 0.23


Protactinium 231 0.4 U 1.6 2.9

Radium (226) 0.61 0.23 0.24

Thorium 232 0.01 U 0.39 0.72

Thorium 234 102 8.7 6.0Uraniwn 235 6.01 0.94 0.87


Potassium 40 9.8 2.4 1.6

Iso URANIUM (SHORT CT) DOB A-Ol-R MOD pCi/gUranium 234 88.7 8.2 0.2

Uranium 235/236 4.87 0.9a 0,,11

Uranium 238 95.6 8.8 0.2

Iso THORltlM (SHORT C'r) DOE A-Ol-R HOD pCi/gThorium 228 0.037 U 0.088 0.17

Thorium 230 1.18 0.33 0.12Thorium 232 0.089 U 0.095 0.12

NOTE(S)Data are iDCQ~lete without the case narrative.

MDC is determined by instrument perfo~ce only.Bold results are greater than the Nne




Client SamDle ID: E-74 UPPER

Radiochemistry

Lab Sample ID: F9E070213-003Work Order: LCJPMMatrix: SOLID


05/06/0905/06/09

10301855

A-Ol-R MOD .

OS/21/09 05/30/09 9141381 B7

OS/21/09 05/30/09 9141381 87

OS/21/09 05/30/09 9141381 87

A-Ol-R MODOS/21/09 OS/29/09 9141383 74

OS/21/09 OS/29/09 9141383 7.

OS/21/09 OS/29/09 9141383 74

05/11/09 06/01/09 9131396

GA-Ol-R MOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

OS/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

Yld \1UI.alyai.Date 3atch ,

Prepnate

TotaltrDcert.

Parameter Result Qual (2 a+/-) MDC

Gamma Ra-226 & Hits By DOE GA-010R MOD pCi/gBismuth 214 0.39 U 0.24 0 .. 39

Lead 212 0.05 U 0.15 0.28

Lead 214 0.62 0.21 0.24

Protaotinium 234M 96 20 7


Radium (226) 0.39 U 0.24 0.39

Thorium 232 -0.01 U 0.30 0.56

Thorium 234 77.5 8.6 5.5Uranium 235 4.26 0.82 0.93

-~- Other Detected Radionuclides ---

Potassium 40 8.8 2.2 1.8

Iso URANIUM (SHORT CT) DOE A-Ol-R MOD pCi/guranium 234 57.9 5.4 0.2

Uranium 235/236 3.20 0.69 0.13

Uranium 238 58.2 5.5 0.2

Iso THORIUM (SHORT CT) DOE A-Ol-R MOD pCi/gThorium. 228 0.028 U 0 .. 078 0.16

-rhorium 230 0.93 0.30 0.16Thorium 232 0.028 U 0.071 0.14

NOTE (8)

Data are iucQDPlete without the case narrative.

MOC is determined by instrument perfo~ce only.Bold results are greater than the MDe




Client Sample ID: E-74 LOWER

Radiochemistry

Lab Sample 1D: F9E070213-004Work Order: LCJPV

Matrix: SOLID


05/06/0905/06/09

10301855

A-Ol-R MODOS/21/09 OS/29/09 9141383 43

OS/21/09 OS/29/09 9141383 4305/21/09 OS/29/09 9141383 43

A-Ol-R MODOS/21/09 05/30/09 9141381 89

OS/21/09 05/30/09 9141381 89

OS/21/09 05/30/09 9141381 89

05/11/09 06/01/09 9131396

GA-Ol-R MOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 913139G

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

Yld %AnalysisD&~. BatCh #

PrepDate

TotaltJDcert.

Parameter Re8ul~ Qual (2 0+/-) MOO

Gamma. Ra-226 & Hits By DOE GA-010R MOD pCi/gBismuth 214 0.93 0.39 0.40

Lead 212 0.10 U 0.20 0.35

Lead 214 0.75 0.30 0.33



Radium (226) 0.93 0.39 0.40Thorium 232 0.1 U 0.28 0.53

Thorium 234 239 22 10

Uranium 235 12.4 1.8 1.5


Potassium 40 8.1 2.6 2.2

Iso URANIUM (SHORT CT) DOE A-Ol-R KOD pCi/gUranium 234 173 16 0.5

Uranium 235/236 8.9 1.6 0.5

Uranium 238 177 16 0.6

Iso THORIUM (SHORT CT) DOE A-Ol-R MOD pCi/gThorium 228 0.08 U 0.14 0.24

Thorium 230 1.95 0.45 0.19

Thorium 232 0.071 U 0.089 0.13

NOTE(S)

Data are incomplete wiChout the case narrative.

MOe is dete~ined by instrument performance only.Bola results are greater than the MOe




Client SamDle ID: E-67 LOWER

Radiochemistry

Lab Sample ID; F9E070213-005Work Order: LCJP3Matrix: SOLID


05/05/0905/06/09

10151855

A-Ol-R MODOS/21/09 OS/29/09 9141383 44

OS/21/09 OS/29/09 9141383 44

OS/21/09 OS/29/09 9141383 44

A-Ol-R MODOS/21/09 05/30/09 9141381 90

OS/21/09 05/30/09 9141381 90

OS/21/09 05/30/09 9141381 90

05/11/09 06/01/09 9131396

Yld ,ADaly.iaDate Batch I

GA-Ol-R HOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

prepDate

TotaltJncert.

Parameter Result Qual (20+/-) MOe

Gamma Ra-226 & Hits By DOE GA-Ol0R MOD pCi/sBismuth 214 0.31 U 0.30 0.51

Lead 212 -0.002 U 0.21 0.36

Lead 214 0.73 0.34 0.35


Protactinium 231 1.9 U 2.8 4.7

Radium (226) 0.31 U 0.30 0.51

Thorium 232 -0.10 U 0.40 0.73

Thorium 234 252 22 10

Uranium 235 12.4 1.' 1.5


Potassium 40 6.2 .... 2.2 2.3

Iso URANIUM (SHORT CT) DOE A-Ol-R MOD pCi/gUranium 234 188 17 0.4

Uranium 235/236 8.4 1.5 0.3

Uranium 23 B 194 17 0.3

Iso THORIOM (SHORT CT) DOB A-Ol-R MOD pCi/gThorium 228 -0.015 U 0.079 0.20

Thorium 230 2.28 0.48 0.15

Thorium 232 -0.010 U 0.047 0.15

NOTE(S)Data are incomplete witbout the ease narrative.

MOe is dete~ined by instrument p.rfo~ce only.Bold results are greater than the MOe




Client SamDle ID: E-65 LOWER

Radiochemistry

Lab Sample ID:Work Order:Matrix:

F9E070213-006LCJP6SOLID


05/04/0905/06/09

14001855

A-OI-R MODOS/21/09 OS/29/09 9141383 38

OS/21/09 OS/29/09 9141383 38

OS/21/09 OS/29/09 9141383 38

A-Ol-R MODOS/21/09 05/30/09 9141381 87

OS/21/09 05/30/09 9141381 87

OS/21/09 05/30/09 9141381 87

05/11/09 06/01/09 9131396

Yld 5kb.alysisDate Batc:h ,.

GA-Ol-R MOD05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

05/11/09 06/01/09 9131396

PrepDate

Total'Dncert.

Pa:ram.etezo Result Qual (2 a+/-) MOC

Gamma Ra-226 & Hits By DOE GA-010R MOD pCi/gBismuth 214 0.92 0.35 0.39

Lead 212 0.27 U 0.21 0.30

Lead 214 1.17 0.34 0.37



Radium (226) 0.92 0.35 0.39Thorium 232 0.23 U 0.41 0.70

Thorium 234 332 28 10

Uranium 235 16.6 2.1 1.8

--~ Other Detected Radionuclides

Potassium 40 5.4 1.9 2.4

Iso.URANIUM (SHORT CT) DOE A-Ol-R MOD pCi/;Uranium 234 228 20 0.4

Uranium 235/236 11.4 1.9 0.3

Uranium 238 239 21 0.4

Iso THORIUM (SHORT CT) DOB A-Ol-R MOD pCi/gThorium 228 0.06 U 0.10 0.17

Thorium 230 2.61 0.52 0.12

Thorium 232 0.027 U 0.063 0.12

NOTE(S)

Data are incomplete without the case narrative.

MOe is determined by instrument performance only.Bold results are greater than the MOe


METHOD BLANK REPORT

Radiochemistry


Client Lot ID: F9E070213Matrix: SOLID

:rotal LIID Sample ID

UDcert. Pr:ep ADalysia

Pat:amete:r Result Qual (2 a+/-) !IDe Date Date Batch # Yld \

Gamma Ra-226 & Hits By DOE GA-010R MOD pCi/g GA-Ol-R MOD F9El10000-396B

Bismuth 214 0.030 U 0.045 0.10 05/11/09 06/01/09 9131396

Lead 212 0.074 U 0.059 0.OB5 05/11/09 06/01/09 9131396Lead 214 0.028 U 0.067 0.12 05/11/09 06/01/09 9131396

Protactinium 234M 0.0 U 1.2 4.4 05/11/09 06/01/09 9131396

Protactinium 231 -0.23 U 0.74 1.3 05/11/09 06/01/09 9131396

Radium (226) 0.030 U 0.045 0.10 05/11/09 06/01/09 9131396Thorium 232 0.09 U 0.13 0.21 05/11/09 06/01/09 9131396

Thorium 234 -0.01 U 0.55 1.1 05/11/09 06/01/09 9131396

Uranium 235 -0.02 U 11 0.2 05/11/09 06/01/09 9131396

Iso THORIUM (SHORT C'1') DOE A-Ol-R MOD pCi/g A-Ol-R MOD P9E210000-381BThorium 228 0.005 U 0.023 0.060 OS/21/09 05/31/09 9141381 88

Thorium 230 0.076 0.059 0.047 OS/21/09 05/31/09 9141381 88

Thorium 232 0.0 U 0.0095 0.030 OS/21/09 05/31/09 9141381 88

Iso URANIUM (SHORT CT) DOE A-OI-R MOD pCi/g A... Ol-R MOD F9E210000-383B

Uranium 234 0.0006 U 0.022 0.062 OS/21/09 OS/29/09 9141383 94

Uranium 235/236 0.012 U 0.025 0.034 OS/21/09 OS/29/09 9141383 94

Uranium 238 0.018 U 0.028 0.042 OS/21/09 OS/29/09 9141383 94

NOTE(S)

Data are incomplete without the dass narrative.

MOC is dete~ined using instrument performance onlyBold results are greater than the MDC


Laboratory Control Sample Report

Radiochemistry


Client Lot ID:Matrix:

F9E070213SOLID

-.t'otal Lab Spple ID

Vncert. OC Ccmtrcl

Parameter Spike Amount Result (2 a+/-' MOe % Yld , Ree Limits

Gamma Ra-226 & Hits By DOB GA-010R MOD pCi/g GA-Ol-R MOD F9Bl10000-396C

Radium (226) 12.2 11.1 0.93 0.37 91 (82 - 110)

Thorium 232 9.50 10.1 0.87 0.42 106 (89 - 130)

Bateh #: 9131396 Analysis Date: 06/01/09

Iso THORIUM (SHORT C'X) DOE A-Ol-R MOD pCi/g A-Ol-R MOD F9E210000-381C

Thorium 230 57.4 59.8 6.7 0.4 90 104 (83 - 126)

Batcb i: 9141381 Analysis Date: 05/31/09

Iso URANIUM (SHORT eT) DOE A-Ol-R MOD pCi/g A-Ol-R MOD F9B210000-383C

Uranium 234 19.2 18.0 3.0 0.5 79 94 (69 - 125)

Uranium 238 19.2 17.9 3.0 0.4 79 93 (68 - 121)

Batch #: 9141383 Analysis Date: OS/29/09

NOTE(S)LOT # P~E070213 ~EVIgED

MOC is dete:mined by instrument performance only_.. ~... - ..53 of 57

DUPLICATE EVALUATION REPORT

Radiochemistry


Client Lot ID:Matrix:

F9E070213SOLID

Date Sampled:Date Received:

05/04/09

05/06/09

Total Total QC Sample ID

SAMPLE l1J1cert. DUPLICATE l1Dcert.Parameter Result (2a+/-) , Yld Result (2 u+/-) % Yld Pz:eci.icm

Gamma Ra-226 & Hits By DOE GA-010R MOD pCi/g GA-Ol-R MOD F9E070213-001

Bismuth 214 0.89 0.29 1.01 0.33 13 %RPD

Lead 212 0.11 U 0.17 -0.1 U 67 3700 %RPD

Lead 214 ~.12 0.29 1.03 0.30 B %RPD

Protactinium 231 -0.02 U 2.4 0.7 U 2.2 210 %"RPDProtactinium 234M 97 21 91 25 7 %RPD

Radium (226) 0.89 0.29 1.01 0.33 13 %RPDThorium 232 0.0 U 0.45 -0.02 U 0.39 200 %"RPDThorium 234 81 .. 0 9.0 76.0 7.1 6 %RPD

Uranium 235 4.3 1.0 3.90 0.85 10 %RPD

---Other Dedec~ed Radionuclides---Potassium 40 5.7 1.9 4.7 2.0 19 %RPD

Batch #: 9131396 (Sample) 9131396 (Duplicate)

Iso THORIUM (SHORT CT) DOE A-Ol-R MOD pCi/g A-Ol-R MOD F9E070213-001

Thorium 228 O~Ol U 0.12 87 0.004 U 0.095 84 113 %RPD

Thorium 230 1.04 0.33 87 1.25 0.35 84 18 %RPD

Thorium 232 0.028 U 0.066 87 0.033 U 0.080 84 16 %RPDBatch t. 9141381 (Sample) 9141381 (Duplicate)

Iso URANIUM (SHORT CT) DOE A-Ol-R MOD pCi/g A-Ol-R MOD F9E070213-001

Uranium 234 58.1 5.4 77 63.5 5.9 69 9 %RPDUranium 235/236 3.60 0.74 77 3.50 0 .. 75 69 3 %RPDUranium 238 60.5 5.7 77 67.2 6 .. 3 69 11 %RPD

BateA I: 9141383 (Sample) 9141383 (Dupl icate)

NOTE(S)

Data are incomplete without the case narrative.Calculations are perfor.med before roundiDg to avo14 ~oUD4-cf! er~or 1~ calculated %esults


t-toreSfAmerica St Louisl31t1 Rider Trail North~anlIjCityl MO 63045)ho~314..298-8566 fax 314-298..8566

"e., ~ ~~t fA.--~ J

t\~ Ce-o~4- Z-,

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-3./a-e-Chain of Custody Record

TestAmericaTHE LEADER-IN ENVlnONMENTAL TE6TIt.IG

TestAmerica Laboratories,

~ Client Contact Project Manager: Sean Chisek Site Contact: W. Brines Date: COC No:~ncliBws Engineering. Inc. TellFax: 217-622-3084 Lab Co.tact: T. Romanko Carrier: _ of__ coes~3~Ginger Creek Drive A~alysis Turnaround Time Job No.

3prjt gfield, IL 62711 Calendar ( C) or Work Days (W) •

!1~ 87-2334 TAT irdifferent &om Below Standard GJ

~17-;" 87-9495 FAX Cl 2 weeks -e ~ ~ ~ ~ SOG No.U) G) (U!E --

~ CJ 1 week Ja en O:J: oa..c b ::J '0)itEPHoneywell Metropolis Pond Sampling CJ 2 days ~ ! gg i :5 :I ~ fIl ~ .~ ~ ~ 55 ·'0# 91 ..135-11 Cl 1day ;:):;:E > en a.. 8.u:: .> CD C ~ iii:2 if

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Sample Sample Sample #I of 0 Q 0 0 0 0 .!! mX CLt 0 1U :; I! :c 0 0 .Sample IdentiOcatlon Date Time Type Matrix Con'. t- ~ .... t- I- t- LL D.. a. ~ .!! 0 m C) 0 I- I- sample Specific Notes:

f.'-(, Lf 6/'110"1 13:I~'~- )(,X " ~ '. J • I •

J~ -,S' \Affe7l, S/9/00, 1'1:00 A ~ ~ ~I~ ~~~~~~ ~~ 2~£ -~c S'1G1t1: gJ'lO 1\IJ , ~ ~

£ - ,ry V1t'P~,..", ~/$}fJ'I 'IJ:/S~ :f'l J !X IXl" X ~~-~£ -,B b/G1~ IIXX rf:~I'f~£ ...,q 5'ISM I/:l{f) t:l'£ -.?O iG~/IJ? IJ!Zo .~ .xE -~ry {j/~/di J3'LfO l' ~ -E -.,(, 1$U;/#1llf:/t>XX~- ?$;- S/~/r, IS.'Jt; , IX' 1\E - '? I f>/~/#'i 8: DO ~~ )(

1= -"1 2- ~~/'~ g:30 ,~resel'YQtlon Used: 1== Ice, 2== BCI; 3-= H2S04; 4=-HNOJ; 5-NaOH; 6- Other I

tosl'ble Hn'l.tlrd Identljica110n Sample Disposal ( A fee may bu assessed ifsamples are retained longer than 1 month)

::J Non-HQZQrd CJ Flammable .. Skin Irritant Polson B Cl Unknown Cl CJ Return To Client .. Disposal By Lab CJ Archive For Months .-::pl:ciallnstruc:tlonslQC Requirements & Comments: ~

)Iease email [email protected][email protected] i~ /~ 1

~elin~y • ~~ C07ony:.t ~iJP;,:.:I~~ Rece~~n \. lJ I J Company: ~telfime: n.---....~ ~~~~ "r"~r~$ t:1MD9 ~ ~~G..J.Jt....J~ ~-oq 3:'&0 PJ

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resJl\merica St. Louisl37i5 Rider Trail North~rtfflCity, MO 63045]hOM 314..298-8566 fax 314-298-8566

o

Chain of Custody RecordTestAmerica

THE LEADER IN e~VlnONMe.NTALTESTING

TestAmerica Laboratories,

o aleRt Contact IProJect Maoaeer: Sean Chisek Site CODtad: W_ Brines Date: COC No:

\ntiws Engineering, Inc. lTeJlFax: 217-622-3084 Lab Contact: T. Romsnko Carrier: of, COCs

l300>Ginger Creek Drive Analysis Turnaround TIme Job No.

)prWJfield. IL 62711 Calendar ( C) or Work Days (W)

~1~ 87-2334 TATirdiffereutrromBe1owStandard CD

!17~87-9495 FAX CJ 2 weeks -e ~ ~ ~ ~ SDGNo.tn CD ca.... .--r: CJ 1 week .!! 0 () :I: ~.c ~ :; 15

>ite: Honeywell Metropolis Pond Sampling CJ 2 days ~ t 8~ 11 :5 .$ en ~ ! IS ~ :i)0# 91 ..135-11 CJ 1day ..... 1ft :IE > rn a. ~ ~ ~ I CG> en -a a.oC

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~~ ... 7Lf Wfe~ SI'/df /0:'0 I~·~ ~~ ii ,'1 ,-~.t2~~ # -€I" pj'tldtl/2!2fJ ~A

.£,,83'" ~'/tf7 Il:lfS rx ~\t .. 7 i.t Lowell ~/D" If): 3D l.. ~'1 X. X '}\ 3X25lJG£~--c,? Lf!)~ ~~_q IO~/S· X. 1"'- '" ~ 't I/<-~ ,E-'.5'" t.o We'L, ~/ij/" I'I:~ }('.~X XxiX ~IX XXX ,X .JIr .~I1,! 'AI... J~.. _V~·J "" I-L ~ ...J

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Ireservatlon Used: 1= Ice. 2a. HCI; 3- H2SO4; 4=HN03; 5=NaOH; 6= Other

·osslbleHtUard IdentJflcatlon Sample Disposal ( A fee maybe assassed Ifsamples are retained longer thlllJ 1 month)

::J Non-JlazDrd 0 FIQlrlmab11i - SkIn [rritanl Polson B 0 Unknown 0 0 Return To Client - Disposal By Lab 0 Archive For Months ~:pecial InstrodionslQC Req_lremenfs & Comments: m

h)Iease email [email protected]@andrews-eng.com ~

CD

~ ,~... ~~e~v, 'Z:P---C CO~;'~imea ..u Rec;ejv~: "... T/\TJ-.. ~ Company: Da1eJTime: 0

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--------------._--_... _. ---_..


6. ------7. ------8. ------9. ------

]0. ------

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2. ---_-:.-3. --_.....-.--4. -----5. -----

Multiple Packages:

Sample Temperature (s)=**1. (J·7

3,1·o.f'

Other: - _

45'4

Date: tJ5=.tJ~·~9Information

Lot #(8): P7.__'Et._._o ~_

9. _

10, ------------4. --------

5. ------

CONDm?N.UPONRE~E~FORMChent. ~1Ve'/PC iJY~d?i!J9

Quote NO:.PIP9Z>t.P05~COCIRFA No: IZ7J?'/ .

fuili~d~~~~ ~ _

TestAmerica

Shipper: FedEx UPS - DHL Courier

Shipping # (s):*

1. 6: ----_:..---------2. 7. ___.....0-- _

3. 8. ------------

*Numbered shipping Hnes colTe5P:ond to Numbered Sample Temp lines 1(1*Sample must be received at 4DC =2°C.. If not, note contents below. Temperaturevariance' does NOT affect the following: Metals-Liquid or Rad tests- Liquid or SoUds

Condition (Circle "Y" for}'es.!~ for n~.and "N/A!1 for·not ·Jicabl.c)~

1 Y/::) Are there custody seals present on the'

. UI-' cooler? 8. · Y <5) Are there custody seals present on bottles?

Was sample received With proper pHI? (lfnotmake note below

Do custody seals on bottles appear to betam ered with?

Sample received in proper containers?

y9.

11.

10.

· 12, 'Y N tN1h." Headspace in VOA or TOX liquid samples?~ (IfYes, note sample IO's below)

Were contenm ofcooler frisked aftero en,n t but before un ackin ?

Do cllstody seals .on cooler appear to bet ~reCI with?

Sample recejve~ with Chain ofCustod ?

N/A DOeS'the Chain of Custody match r

sam ;le ID's on the containe s?

4.

3.

2.

5.

6. Was sample received broken? 13. Y· N@ Was Internal COCIWorkshare received?

7 Is s$ple volume suffici~nt·for 14 Y N' NI W' H tak b'· aJ i' stA ' 1 b?. anal :~is? " .. as p en y orIgm· e merlea a ·

1.For DOB-AL (pantex. LAN L~ Sandia) sites~ pH ofALL containers received must be verified, EXCEPT VOA. TOX and soils.

Notes:

THIS FORM MUST BE COMPLETED AT THE TIME THE ITEMS ARE BEING CHECKED IN. IF ANY ITEM IS COMPLETED BY SOMEONE OTHER THANTHE iNITIATOR. THEN THAT 'PERSON IS RSQU1REP TO AfPLYTHEIRlNlTlAL AND THE DATE NEXT TO THAT ITEM.

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F9E070213-REVISED " . 57 of 57

Corrective Action:o Client Conta~t Name: ~

o Sample(s) processed t~~ is"o Sample(s) on hold uno!l:Project Management Review:

','

Informed by~ _~~ - _

ff~cle~e~~~:~~~~~ ~~__~~~~_pate: _

testamerica laboratories, inc. - nrc.gov · testamerica st. louis tclp preparation due to limited...

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