testaiti erica south burlington, vti certify that this data package is in compliance with the terms...

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Superfund Records Center SITE: H&A? (B^dl-hod BREAK : X - "?- a OTHER ^ 0 7 ̂ (?

TestAiti erica South Burlington, VT

/ . •

Sample Data Summary Package

SDG: JNB070

SDMS DocID 507930

TestAmerica Burlington Data Qualifier Definitions

Organic ;

U: Compound analyzed but not detected at a concentration above the reporting limit.

J: Estimated value.

N: Indicates presumptive evidence of a compound. This flag is used only for tentatively identified compounds (TICs) where the identification of a compound is based on a mass spectral library search.

P; SW-846: The relative percent difference for detected concentrations between two , GC columns is greater than 40%. Unless otherwise specified the higher of the two values is reported on the Form I.

CLP SOW: Greater than 25% difference for detected concentrations between two GC columns. Unless otherwise specified the lower of the two values is reported on the Form I.

C: Pesticide result whose identification has been confirmed by GC/MS. ^

B: Analyte is found in the sample and the associated method blank. The flag is used for tentatively identified compounds as well as positively identified compounds.

E: Compounds whose concentrations exceed the upper limit of the calibration range of the instrument for that specific analysis.

D: Concentrations identified from analysis ofthe sample at a secondary dilution.

A: Tentatively identified compound is a suspected aldol condensation product.

X,Y,Z: Laboratory defined flags that may be used alone or combined, as needed. If used, the description of the flag is defined in the project narrative.

Inorganic/Metals

E: Reported value is estimated due to the presence of interference.

N: Matrix spike sample recovery is not within control limits.

* Duplicate sample analysis is not within control limits.

B: The result reported is, less than the reporting limit but greater than the instrument detection limit.

U: Analyte was analyzed for but not detected above the reporting limit.

Method Codes:

P ICP-AES MS ICP-MS CV Cold Vapor AA AS Semi-Automated Spectrophotometric

FQA009:02.18.08:4 tesfAmerica Burlington - .

Jacobs C O C # .x:-H0038 t J A - H o o z t f CHAIN-OF-CUSTODY RECORD m 6 Otis Park Drive, Suite 200; Bourne, MA 02532-3870 Phone: (508)-743-0214 Fax:(508)743-9177 r Project Name: New Bedford Harbor Laboratory: TestAmerica (formerly Severn Trent - Burlington) >.

Project Number: 35BG0603. ' * Point of contact: Jim Madison • • * M • • WBS Code: A0807003 . Ship to: ' . 30 Community Drive, Suite 11; South Burlinton, VT (05403)

TCLP Analyses: TCLP Metals + Cu; TCLP SVOCs, TCLP VOCs.

Relinquished by:fS/g/rSfujrp;fl iJipateT "'TinM ^aceiye^y^fSigpatu iv)^ *A&s8m&% * * ^ r '%Date~«il ., Ttmei

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mmmmmmmmmmmmmmamm w^mm^mm ŝmmmBm^mmm&miMm^mm

TestAmerica

THE LEADER IN ENVIRONMENTAL TESTING

Sample Data Summary - Wet Chemistry

WET CHEMISTRY i.

Sample Report Summary Client Sample No.

NB-H003801

Lab Name: TestAmerica Burl ington Contract: 35-BG06-03 SDG No.: JNB070

Lab Code: TALVT Case No.: 24045 Lab Sample ID: 763326

Matrix: SOLID Client: JACEN3 Date Received: 08/09/08

% Solids: 70.4 ' • •. <

Analytical Analytical Method Parameter Run Date Batch Units _DE_ _RL_ Cone. -Qual_

IN623 Solids, Percent . 08/12/08 N/A 1.0 70.4

Printed on: 08/14/08 11:26 AM

WET CHEMISTRY Sample Report Summary

Client Sample No.

NB-H003802

Lab Name: TestAmerica Burl ington Contract: 35-BG06-03 SDG No.: JNB070



% Solids: 69.0

Analytical Analytical Method Parameter Run Date : Batch Units JJE_ _RL_ Cone. _QuaL_

IN623 Solids, Percent 08/12/08 N/A 1.0 69.0

Printed on: 08/14/08 11:26 AM


Client Sample No.

NB-H003803

Lab Name: TestAmerica Burlington Contract: 35-BG06-03 SDG No.: JNB070



% Solids: 65.0

Method Parameter Analytical Run Date

Analytical Batch Units _DE_ _RL_ Cone, _QuaL


Printed on: 08/14/08 11:26 AM


Client Sample No.

NB-H003804

Lab Name: TestAmerica Burlington Contract: 35-BG06-03 SDG No.: JNB070



% Solids: 60.5

Analytical Analytical Method Parameter Run Date Batch Units _DE_ _RL_ Cone. _QuaL_


Printed on: 08/14/08 11:26 AM

TestAmerica

THE LEADER IN ENVIRONMENTAL TESTING

Sample Data Summary - Metals

i

i

USEPA-CLP FORMS

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Dab Name: T e s - A m e r i c a B u r l i n g t o n C o n t r a c t : 24045

Lab Code: STLV Case N o . ; 2 4 0 4 5 SAS N o . : SDG No. : JNB070

SOW No.

EPA Sample No.

NB-H003801 NB-H003802 NB-H003803 NB-H003803D

NB-H003803S

NB-H003804

Lab Sample ID.

763327

763330

763333

763333DF

763333MS

763336

Were ICP Interolemant corrections applied? Y E S Yes/No

Were ICP background corrections applied? YES Yes/No

If yes-were raw data generated before

application of background corrections? Yes/No NO

Comments:

I certify that this data package Is In compliance with the terms and conditions of the

contract, both technically and for completeness, for other than the conditions- detailed

above. Release of the data contained in this hardcopy data package and in the computer-readable data

submitted on diskette has been authorized by the Laboratory

Manager or the Manager's designee, as verified by the following signature.

Signature: Name:

Titles Date:

COVER PAGE - IN

USEPA-CLP FORMS

INORGANIC ANALYSES DATA SHEET EPA SAMPLE NO.

NB-H003801

Lab Name: TestAmeriea Burlington . Contract 24045

Lab Code: STLV Case No. : 24045 SAS Noo. : SDG No.: JNB070

Matrix (soil/water) TCLP EXT Lab Sample ID: 763327

Level (low/med): LOW Date Received: 08/09/08 ,. .

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight) UG/L

CAS No. Analyte Concentration C Q M ,

7440-22-4 Silver ' 0.53 Pu

7440-38-2 Arsenic' 11.9-1 | P

7440-39-3 Barium 103 |B |E P

7440-43-9 Cadmium 0.13 |U | P

7440-47-3 Chromium 13.3 | |E P

7440-50-8 Copper 446 | | P

7439-97-6 Mercury 1.0 |u | ,. CV

7439-92-1 Lead 4.2 |B | P

7782-49-2 ' Selenium 12.7 |B | P

Color Before: light brown Clarity Before: clear Texture:

Color After: colorless Clarity After: clear Artifacts:

Comments:

Form I - IN

USEPA-CLP FORMS -l-

INORGANIC ANALYSES DATA SHEET EPA SAMPLE NO.

NB-H003802

Lab Name:

Lab Code:

TestAmeriea Burlington . .

STLV Case No.: 24045

Contract: 24045

SAS No.: SDG No.: JNB070

TCLP EXT Matrix (soil/water) ;•

Level (low/med): LOW

Lab Sample ID:

Date Received:

763330

08/09/08

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L

CAS No. Analyte Concentration C Q M

7440-22-4 Silver ' 0.53 U P

7440-38-2 Arsenic 18.9 P 7440-39-3 Barium 184 B E P .7440^43-9 Cadmium '. 0.13 U P 7440-47-3 Chromium 3.9 B E P 7440-50-8 Copper 187 P

7439-97-6 Mercury 1.0 U CV

7439-92-1 Lead 5.9 B P 1 7782-49-2 Selenium •9-9. B P 1

Color Before: light brown Clarity Before: 'clear Texture:


Comments:

Form I - IN

USEPA-CLP FORMS - 1

INORGANIC ANALYSES DATA SHEET

EPA SAMPLE NO.

NB-H003803

Lab Name: TestAmeriea Burlington C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case No . : 24045 SAS No. : SDG N o . : JNB070

Matrix (soil/water) TCLP EXT Lab Sample ID: 7 6 3 3 3 3

Level (low/med): LOW Date Rece ived : 0 8 / 0 9 / 0 8

% S o l i d s : 0 . 0

C o n c e n t r a t i o n U n i t s (ug/L o r mg/kg d ry weigh t ) UG/L

CAS No. Analyte Concentration C 2 M

7440-22-4 Silver 0. 97 B P |

7440-38-2 Arsenic 17.5 P |

7440-39-3 Barium 113 B E P 1 7440-43-9 Cadmium 0.13 U P |

.7440-47-3 Chromium 11.7 E P |

7440-50-8 Copper 403 - P |

7439-97-6 Mercury 1.0 U CV |

. 7439-92-1 Lead 4.6 B P |

7782-49-2 Selenium 10.9 B P (

Color B e f o r e : l i g h t b r o w n . ( C l a r i t y Be fo re : c l e a r T e x t u r e :

Color A f t e r : c o l o r l e s s C l a r i t y A f t e r : c l e a r A r t i f a c t s :

Comments:

Formal - IN

USEPA-CLP FORMS -1

INORGANIC ANALYSES DATA SHEET

Lab Name:

Lab Code:

T e s t A m e r i e a

STLV

B u r l i n g t o n

Case No. 24045

Contract:

SAS No.

24045

Matrix (soil/water)


TCLP EXT Lab Sample ID:

Date Received:

% Solids: 0.0

Concentration Units (ug/L or mg/kg dry weight):

CAS No.

7440-22-4

7440-38-2

7440-39-3

7440-43-9

7440-47-3

7440-50-8

7439-97-6

7439-92-1

7782-49-2

Analyte Concentration C

Silver •1-5 B

Arsenic 15.4 |

Barium 158 |B

Cadmium 0.13 |U

Chromium 12.4 |

Copper M 373 1 Mercury 1.0 |u Lead 4.3 |B

Selenium 11.9 |B

EPA SAMPLE NO.

NB-H003804

SDG No.: JNB070

763336

08/09/08

UG/L

Q M

P

P

E P

P .

E P

P.

• CV

p

p

Color Before: light brown Clarity Before: clear Texture:


Comments:

Form I - IN

USEPA-CLP FORMS

2A

INITIAL AND CONTINUING CALIBRATION VERIFICATION

Lab Name:

Lab Code:

Tes tAmeriea

STLV

B u r l i n g t o n

Case No . ; 24045

C o n t r a c t : 2 4 0 4 5

SAS No . : SDG No.: JNB070

Initial Calibration Source: Inorganic Ventures/Fisher

Continuing Calibration Source: SPEX/Fisher

Concentration Units: ug/L

I n i t i a l C a l i b r a t i o n C o n t i n u i n g C a l i b r a t i o n

Ana ly t e

M e r c u r y

True

3.0(

Found %R(1)

3 . 0 2 | 1 0 0 . 7

True

5 . 0 |

Found %R(1)

5 . 0 4 | l 0 0 . 8 |

Found %R(1)

5 . 0 7 ) 1 0 1 . 4

M

cv

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

Form II (Part 1) - IN

USEPA-CLP FORMS

2A INITIAL AND CONTINUING CALIBRATION VERIFICATION

Lab Name: T e s t A m e r i e a B u r l i n g t o n C o n t r a c t : 24045

Lab Code: STLV Case N o . : 24045 SAS N o . : SDG N o . : JNB070

i n i t i a l C a l i b r a t i o n Source : I n o r g a n i c V e n t u r e s / F i s h e r

C o n t i n u i n g c a l i b r a t i o n S o u r c e : S P E X / F i s h e r

( Concentration Units: ug/L

I n i t i a l C a l i b r a t i o n C o n t i n u i n g C a l i b r a t i o n

A n a l y t e True . Found %R(1) True Found %R(1) Found %R(1) M

S i l v e r ( 5 0 0 . 0 | 4 7 1 . 8 0 [ 9 4 . 4 1 0 0 . 0 | 9 4 . 7 2 | 9 4 . 7 ( 9 5 . 7 4 | 9 5 . 7 P

A r s e n i c 2 5 0 . 0| 2 5 5 . 9 0 | 1 0 2 . 4 1 0 0 . 0 | 1 0 4 . 30| 1 0 4 . 3 , 1 0 4 . 3 0 1 1 0 4 . 3 P

B a r i u m 5 0 0 . 0| 4 9 7 . 7 0 | 9 9 . 5 2 0 0 . 0 | 1 9 4 . 3 0 | 9 7 . 2 { 1 9 4 . 7 0 | 9 7 . 4 P

Cadmium 5 0 0 . 0| 4 8 8 . 2 0 | 9 7 . 6 1 0 0 , 0 | 9 7 . 2 0 | 9 7 . 2 | . . 9 6 . 5 3 ) 9 6 . 5 P

Chromium 5 0 0 . 0 4 8 7 . 2 0 | 9 7 . 4 2 0 0 . 0 | 1 8 9 . 7 0 ) 9 4 . 8 | 1 8 8 . 3 0 { 9 4 . 2 P

C o p p e r 5 0 0 . 0 | 462 .10 ] 9 2 . 4 2 0 0 . 0 | 1 7 9 . 0 0 ) 8 9 . 5 | 1 7 9 . 6 0 | 8 9 . 8 P

L e a d 1 0 0 0 . o | 9 8 2 . 90| 9 8 . 3 4 0 0 . 0 | 3 9 2 . 5 0 ) 9 8 . 1 3 9 0 . 7 0 97 . 7 P

S e l e n i u m 2 5 0 . 0| 2 5 4 . 50| 1 0 1 . 8 1 0 0 . 0 1 0 6 . 2 0 1 0 6 . 2 1 0 0 . 1 0 | 1 0 0 . 1 P



USEPA-CLP FORMS

2A INITIAL AND CONTINUING CALIBRATION VERIFICATION

Lab Name:

Lab Code:

Tes tAmer iea

STLV

B u r l i n g t o n

Case N o . : 24045

C o n t r a c t : 2 4 0 4 5

SAS N o . : SDG No.: JNB070

Initial Calibration Source: Inorganic Ventures/Fisher i . ' •

Continuing Calibration Source: SPEX/Fisher

Concentration Units: ug/L

I n i t i a l C a l i b r a t i o n Con t inu ing C a l i b r a t i o n

A n a l y t e

S i l v e r

A r s e n i c

Barium

Cadmium

Chromium

Copper

Lead Se len ium

' True

• •

11111

1

1

Found %R(1)

M M

1 1

• 1 1

1 1

True

1 0 0 . 0 |

1 0 0 . 0 |

2 0 0 . 0 |

1 0 0 . 0 |

2 0 0 . 0 )

2 0 0 . 6 |

. 4 0 0 . 0 |

1 0 0 . 0 |

- A ' • Found %R(1) Found

95 .69) 9 5 . 7 |

103 .80 ) 1 0 3 ; 8 | M

194 .50 ) 9 7 . 2

96 .42) 9 6 . 4

187 .20) 9 3 . 6 )

180 .00 ) 9 0 . 0 )

396 .60 ) 9 9 . 2 X

103 .00) 1 0 3 . 0 |

/ %R(1)

|

|

|

|

|

|

|

|

M

P

P

P

P

P

P

F

P



USEPA-CLP FORMS

2B-IN

CRDL STANDARD FOR A A AND ICP


Lab Code: STLV Case No . : 2 4 0 4 5 SAS No . : SDG No. : JNB070

AA CRDL S t a n d a r d S o u r c e :

ICP CRDL S t a n d a r d S o u r c e : I n o r g a n i c V e n t u r e s

C o n c e n t r a t i o n U n i t s : ug/L

CRDL S t a n d a r d f o r ICP In i . t i a l F i n a l

A n a l y t e True Foundy %R True Found %R Found %R

S i l v e r 1 0 . 0 1 0 , 6 2 1 0 6 . 2 A r s e n i c 1 0 . 0 1 1 . 6 4 1 1 6 . 4

B a r i u m

' . • I ' • . - • •

2 0 0 . 0 1 9 3 . 8 0 9 6 . 9

Cadmium 5 . 0 5 . 1 1 1 0 2 . 2

Chromium 1 0 . 0 9 . 9 1 9 9 . 1

C o p p e r 2 5 . 0 2 2 . 7 8 9 1 . 1

L e a d ) 1 0 . 0 8 . 9 1 8 9 . 1

S e l e n i u m 3 5 X 3 7 . 6 0 1 0 7 . 4 • 1 " •

C o n t r o l L i m i t s : no l i m i t s have been e s t a b l i s h e d by EPA a t t h i s t ime

Form I IB- IN ". I

USEPA-CLP FORMS

3

BLANKS

Lab Name: TestAmeriea Burlington Contract: 24045

Lab Code: STLV Case No.: 24045 SAS No. : • SDG No. : JNB070

Preparation Blank Matrix (soil/water): TCLP EXT

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L

A n a l y t e

M e r c u r y

* I n i t i a l Cal ib . Blank (ug/L)

. G 0 . 1 U

1

Con t inu ing C a l i b r a t i o n Blank (ug/L)

C 2 . C 3

0 . 1 | U | 0 . 1 ) U|

' C

|

P r e p a r a t i o n Blank

1.000 |

C

u

M

CV

Form III - IN

USEPA-CLP FORMS

3.

BLANKS


Lab Code: STLV Case No.: 24045 SAS No.: SDG No. JNB070

Preparation Blank Matrix (soil/water): TCLP EXT

Preparation Blank Concentration'Units (ug/L or mg/kg): UG/L

I n i t i a l C o n t i n u i n g C a l i b r a t i o n Cal ib . P r e p a r a t i o n

Blank (ug/L) Blanic Blank (ug/L) A n a l y t e 1 c 3 MC 2 c C

S i l v e r 1 . 3 B ; 0 . 6 | B | 0 . 5 ) U| 0 , 5 Iu '. 0 . 8 7 9 | B . P A r s e n i c 4 . 1 B 2 . 8 | B | 4 . 9 ) B| 1 . 4 u -- 3 . 7 7 7 | B P B a r i u m 1 . 7 U 1 . 7 | U | 2 . 2 ) B| - 5 . 0 " IB 3 . 3 9 0 | B P Cadmium 0 . 1 B 0 ; 2 | B | 5 - 0 . 2 1 8 ) - 0 . 3 IB - 0 ; 3 5 8 | B P Chromium 0 . 1 U 0 . 1 | U | 0 . 2 ) B| - 0 . 1 IB 0 . 9 5 0 ) B P C o p p e r 0 . 5 U 0 . 5 | U | ' 0 . 5 ) U| 0 . 5 1 3 . 3 6 0 | B PIu L e a d 1 . 7 B 3 . 2 | B | 1 . 3 B| 1 . 9 | B 8 . 0 0 0 | B P

S e l e n i u m , 4 . 3 B 6 . 1 | B 1 .8 B| 4 . 5 IB 1 1 . 4 7 0 ) B P

Form III - IN

C

USEPA-CLP FORMS

ICP INTERFERENCE CHECK SAMPLE

Lab Name: T e s t A m e r i e a B u r l i n g t o n C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case No. : 2 4 0 4 5 SAS N o . :

ICP ID Number: TJA ICAP 7 ICS S o u r c e :

C o n c e n t r a t i o n U n i t s : ug/L

True Initial Found

Analyte Sol.A Sol.AB Sol.A Sol.AB y %R

Silver 0 202 1 195.2| 96.6

Arsenic 0 106 ,5 104.3) 98.4

Barium 0 485 6 483.7 99.7

Cadmium 0 993 2 970.2) 97.7

Chromium 0 490 1 481; 3 | 98.2,

Copper 0 488 1 459.9) 94.2

Lead 0 55 0 . 50.0 90.9

Selenium 0 49 3 49.6 101.2

SDG No. JNB070 A

I n o r g a n i c V e n t u r e s

Final Found

Sol.A Sol.AB %R

^

Form IV - IN

USEPA-CLP FORMS

. 5 A •

SPIKE SAMPLE RECOVERY

SAMPLE NO.

NB-H003803S


Lab Coda: STLV Case No.: 24045 SAS No.: SDG No. JNB070

M a t r i x ( s o i l / w a t e r ) : TCLP EXT Level ( low/mad); LOW

% S o l i d s f o r Sample: 0 .0 - •

C o n c e n t r a t i o n U n i t s (ug/L or mg/kg d r y w e i g h t ) : TH3/T,

C o n t r o l Spiked Sample Sample Sp ikeA n a l y t e L imi t %R R e s u l t (SSR) C R e s u l t (SR) C Added (SA) %R > Q H

S i l v e r 50 - 150 3 9 6 . 9 0 0 0 0 . 9 7 1 1 | B 5 0 0 . 0 0 7 9 . 2 P | A r s e n i c •• 50 - 150 8 9 9 . 1 0 0 0 1 7 . 4 9 0 0 ) 1 0 0 0 . 0 0 8 8 . 2 P B a r i u m 50 - 150 1 7 1 1 . 0 0 0 0 1 1 2 . 9 0 0 0 | B 2 0 0 0 . 0 0 7 9 . 9 P Cadmium 50 - 150 4 6 . 2 1 0 0 0 . 1 3 0 0 | u 5 0 . 0 0 9 2 . 4 P Chromium 50 - 150 1 7 8 , 7 0 0 0 1 1 . 7 2 0 0 ) 2 0 0 . 0 0 8 3 , 5 P C o p p e r ^50 - 150 5 7 2 . 8 0 0 0 4 0 2 . 9 0 0 0 ) 2 5 0 . 0 0 6 8 . 0 P M e r c u r y 50 - 150 6 . 2 8 0 0 1 . 0 0 0 0 | u 1 0 . 0 0 6 2 . 8 CV L e a d 50 - 150 4 6 4 . 3 0 0 0 4 . 5 8 3 0 | B 5 0 0 . 0 0 9 1 . 9 P S e l e n i u m 50 - 150 1 6 8 0 . 0 0 0 0 1 0 . 9 0 0 0 | B 2 0 0 0 . 0 0 8 3 . 5 P

Coimnont. s •

Form V (PART X) - IN

USEPA-CLP FORMS

5B / •

POST DIGEST SPIKE SAMPLE RECOVERY SAMPLE NO.

NB-H003803A

Lab Name: T e s t A m e r i e a B u r l i n g t o n Contract : 24045

Lab Code: STLV Case No.: 24045 SAS No.: • • SDG No. : JNB070

Matrix ( s o i l / w a t e r ) : TCLP EXT Level (low/mad): LOW

|

|

|

|

Ana ly t e

S i l v e r

A r s e n i c

B a r i u m

Cadmium

Chromium

C o p p e r

L e a d

S e l e n i u m

C o n t r o l L imi t %R

C o n c e n t r a t i o n U n i t s : ug /L

Spiked Sample . R e s u l t (SSR) C

3 5 . 8 4

5 4 . 2 8

1 9 3 1 . 0 0

4 6 . 5 1

1 9 7 . 2 0

6 2 9 . 7 0

2 6 . 8 3

6 2 . 6 3

Sample R e s u l t ' ( S R )

0 . 9 7

' 1 7 . 4 9

1 1 2 . 9 0

0 . 1 3

1 1 . 7 2

402.-90

4 . 5 8

1 0 . 9 0

C

B

B

U

B

B

Spike Added(SA)

5 0 , 0

4 0 . 0

2 0 0 0 . 0

5 0 . 0

2 0 0 . 0

2 5 0 . 0

2 0 . 0

5 0 . 0

%R

6 9 . 7

9 2 . 0

9 0 . 9

9 3 . 0

9 2 . 7

9 0 . 7

1 1 1 . 2

1 0 3 . 5

_ M

P

P

P

P

P

P

P

P

Comments:

Form V (PART 2) - IN

USEPA-CLP FORMS

DUPLICATES

SAMPLE NO.

NB-H003803D

Lab Name:

Lab Code:

TestAmeriea Burlington

STLV Case No.: 24045

Contract: 24045

SAS No. SDG No. : JNB070


Matrix (soil/water): TCLP EXT

% Solids for Duplicate: 0.0 % Solids for Sample: Q.Q

Concentration Units (ug/L or mg/kg dry weight) UG/L

Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q M

Silver 0.9711 B 0.5300 U 200.0 P

Arsenic 10.0 17.4900 15.3700 12.9 P

Barium 112.9000 B 114.5000 B 1.4 P

Cadmium 0.1300 U 0.1300 U P

Chromium 10.0 11.7200 11.2900 3.7 P

Copper 402.9000 393.1000 2.5 P

Mercury 1.0000 U 1.0000 U CV

Lead 4.5830 B 4.3780 B 4.6 p

Selenium 10.9000 . B 12.3100 B 12.1 p

Form VI - DJ

USEPA-CLP FORMS

LABORATORY CONTROL SAMPLE

Lab Name: T e s t A m e r i e a B u r l i n g t o n C o n t r a c t : . 2 4 0 4 5

Lab Code: STLV Case No. : 2 4 0 4 5 SAS N o . : SDG N o . : JNB070

S o l i d LCS S o u r c e :

Aqueous LCS S o u r c e : I n o r g a n i c V e n t u r e s

Aqueous (ug/L) Solid (mg/kg)

Analyte True Found %R True Found C Limits %R,

Mercury 1.0 0.93 93.0 1 1 1

Form VI I - IN

USEPA-CLP FORMS

LABORATORY CONTROL SAMPLE


Lab Code: STLV . Case No. : . 2 4 0 4 5 SAS No . : SDG No.: JNB070

Solid LCS Source:

Aqueous LCS Source: Inorganic Ventures

Aqueous (ug/L) Solid (mg/kg)

Analyte True Found %R True Found C Limits %R

Silver 500.0 426.90 85.4 1 1

Arsenic 1050.0 977.20 93.1 1

Barium 500.0 443.00 88.6 1

- • •Cadmium 525.0 457.50 87.1 1

Chromium 500.0 436.00 87.2 1

Copper 500.0 418.30 83.7 |... 1

Lead 1015.0 907.50 89.4 • X 1 • Selenium 525.0 468.80 89.3 1 1

Form VII - IN

USEPA-CLP FORMS

ICP SERIAL DILUTIONS •J

SAMPLE NO.

N B - H 0 0 3 8 0 3 L


Lab C o d e : STLV C a s e N o . : 2 4 0 4 5 SAS N o . : SDG N o . : J N B 0 7 0

Matrix (soil/water): TCLP EXT L e v e l ( l o w / m e d ) : LOW

A n a l y t e

S i l v e r

A r s e n i c

B a r i u m

Cadmium

Chromium

C o p p e r

L e a d

S e l e n i u m

C o n c e n t r a t i o n

I n i t i a l Sample R e s u l t ( I )

C

0 . 9 7

1 7 . 4 9

1 1 2 . 9 0

0 . 1 3

1 1 . 7 2

4 0 2 . 9 0

4 . 5 8

1 0 . 9 0

B

B

U

(

B

B

U n i t s : ug/L

S e r i a l D i l u t i o n R e s u l t (S)

1

c 5 . 1 2 | B

2 1 . 4 . 6 J B

1 2 9 . 2 0 | B

0 . 6 5 | U

1 3 . 0 0 | B

4 0 4 . 6 0 )

4 . 2 5 | U

1 0 . 1 1 ) B

% D i f f e r ence

4 2 7 . 8

2 2 . 7

1 4 . 4

1 0 . 9

0 . 4

1 0 0 . 0

7 . 2

Q

E

E

M

P

P ,

P

P

P

P.

P

P

Form IX - IN

USF,PA-rT,P FORMS

10

INSTRUMENT DETECTION LIMITS (QUARTERLY)


Lab Code: STLV Case N o . : 24045 SAS N o . : SDG No. : JNB070

ICP ID Number:

Flame AA ID Number:

Furnace AA ID Number:

Leeman

.

H v d r a AA (2 )

_ ^

D a t e : 0 7 / 0 1 / 0 8

Wave BackCRDL IDL Ana ly t e l e n g t h ground M

(ug/L) (ug/L) (ma)

Mercury 2 5 3 . 7 0 0 . 2 0 . 1 CV

Comments:

Form X - IN

TISFPA-CTP F O R M S

10

INSTRUMENT DETECTION LIMITS (QUARTERLY)

Lab Name: Tes tAmer iea B u r l i n g t o n C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case N o . : 24045 SAS N O . :

ICP ID Number: TJA ICAP 7 Date: 07/01/08

Flame AA ID Number:

Furnace AA ID Number:

Analyte Wavelength (nm)

Background CRDL

(ug/L)

Silver 328.068 10 Arsenic 189.042 10 Barium. 493.409 200

Cadmium 226.502 . 5 .

Chromium 267.716 10

Copper 324.754 25 Lead 220.353 10 Selenium 196.026 35

SDG NO. JNB070

IDL

(ug/L)

0.5

1.4

1.7

0.1

0.1

0.5

0.9

1.6

M

P

P

P

P

P

P

P

P

Comments:

Form X - IN

USEPA-CLP FORMS

11A

ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)


Lab Code: STLV Case No. 24045 SAS No. : SDG No. : JNB070

ICP ID Number: TJA ICAP 7 Date : 0 7 / 1 1 / 0 8

Wave

Interelement Correction Factors for:

Analyte length (nm) Al Ca Fe Mg Ag

Aluminum 308.215 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Antimony 206.838 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Arsenic 189.042 0.0000000 0.0000000 0,0000000 0.0000000 0.0000000

Barium 493.409 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Beryllium 313.042 0.0000000 0.0000000 0.0000000 . 0.0000000 0.0000000 J

Boron 249.678 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Cadmium 226.502 0.0000000 0.0000000 o.Ooooooo 0.0000000 0.0000000

Calcium 317.933 -0.0001324 0.0000000 0.0000000 0.0000000 0.0000000

Chromium 267.716 0.0000000 0.0000000 0.0020050 0.0000000 0.0000000

Cobalt 228.616 0.0000000 0.0000000 0.0819380 o.ooooooo 0.0000000

Copper 324.754 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Iron 271.441 -0.0001158 0.0000000 0.0000000 0.0001830 0.0000000

Lead 220.353 0.0000000 0.0000000 0.0000000 0.0000000 .0.0000000

Magnesium 279.079 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Manganese , 257.610 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Molybdenum 202.030 0.0541914 0.0031140 0.0025280 0.0113110 0.0000000

Nickel 231.604' 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Phosphorus 178.287 0.0000000. 0.0000000 0.0000000 0.0000000 0.0000000

Potassium 766.491 0.0000000 0.0000000 0.0000000 0.0000000 a. ooooooo Selenium 196.026 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Silver 328.068 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Sodium 330.232 0.0000000 0.0000000 . 0.0000000 0.0000000 0.0000000

Strontium 421.552 0. 0000000 0.0000000 0.0000000 0.0000000 0.0000000

Thallium 190.864 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Tin 189.989 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Titanium 334.941 0.ooooooo 0.0000000 0.0000000 0.0035760 -0.0001310

Vanadium 292.402 0.0000000 0.0000000 0.0060410 0.0000000 0.0000000

Zinc 206.200 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Comments:

Form XI (PART 1) IN

USEPA-CLP FORMS

11A



Lab Code: STLV Case No. : 2 4 0 4 5 SAS N o . : SDG No. : JNB070

ICP ID Number; TJA ICAP 7 D a t e : 0 7 / 1 1 / 0 8

Analyte

Wavelength (nm) As


B Be Cd Co

Aluminum 308.215 0.0000076 0.0000000 0.0000000 0.0000000 0.0000000

Antimony 206.838 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000.

Arsenic 189.042 0.0000000 0.0000000 0.0000000 0.0046300 0.0000000

Barium 493.409 0.0000000 0.0000000 0.0000000) 0,0000000) 0.0004100

Beryllium 313.042 0.0003440: 0.0000000 : 0-0000000 0.0000000 0.0000000

Boron 249.678 0.0000000 0.0000000 0,0000000. o.ooooooo) 0.0000000

Cadmium 226.502 0.0000000 0.0000000 0.0000000) 0.O000000| -0>0002790

Calcium 317,933 0.0000000 0.0000000 0.0000000 0.0000000) 0.0000000

Chromium 267.716 -0.0123310 0.ooooooo 0.0000000 0.0000000' 0.0001180 Cobalt 228.616 0.0000000 ! 0.0000000 0-0000000 O.OOOOOOO) 0.0000000

Copper 324.754 0.0000000 0.0000000 0.0000000 O.OOOOOOO) 0.0000000

Iron 271.441 -0.0000108 0.0000000 0,0000000 0.0000000 0.0000000

Lead 220.353 0.0000000 0.0000000 0.0000000 0.0000000) 0.0000000

Magnesium 279.079 •0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Manganese 257.610 0.0000000 0,0000000 0.0000000 0,0000000) 0.0000000

Molybdenum 202.030 0,0000000 0.0381560 0.0000000) 0,0000000 -0.0016570

Nickel 231.604 0.0000000 0.0000000 0.0000000) 0.0000000 0.0001170

Phosphorus 178.287 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Potassium 766.491 0.0000000 o.ooooooo o.ooooooo| 0.ooooooo o.ooooooo Selenium 196.026 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Silver 328.068 0,0000000 0.0000000 o.ooooooo 0.0000000 0.0000000 Sodium 330.232 0.0000000 0.0000000 0.0000000 | 0.0000000 0.0000000

Strontium 421.552 0.0000000 0.0000000 .0.0000000 ( o.ooooooo 0.0000000

Thallium 190.864 0.0000000 0.0000000. 0.0000000) 0.0000000 0.0000000

Tin 189.989 0.0000000 0.0000000 0.0000000 0.0000000) 0.0000000

Titanium 334.941 0.0000000 0.0000000 -0.0005960 O.OOOOOOO) 0.0017470

Vanadium 292.402 0.0000000 0.0000000 0.0004350 0.0000550 ' 0.0000000

Zinc 206.200 0.0000000 0.0000000 ,0.0000000 0.0000000 0.0000000

Comments:

Form XI (PART 2) - IN

USEPA-CLP FORMS

11A


Lab Name: T e s t A m e r i e a B u r l i n g t o n , , C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case N o . : 2 4 0 4 5 SAS No. : SDG No. : JNB070

ICP ID. Number: TJA ICAP 7 Da te : 0 7 / 1 1 / 0 8

Analyte

Wavelength (nm) Cr


Cu Mn r Na Ni

Aluminum 308.215 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Antimony 206.838 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Arsenic 189.042 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Barium 493.409 0.0000000 >0.0000000 0.0000000 0.0000000 0.0000000

Beryllium 313.042 -0.0002710 0.0000000 0.0000000 0.0000000 0.0000000

Boron 249.678 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Cadmium 226.502 0.0000000 0.0000000 0.0000000 o.ooooooo 0.0000000 Calcium 317.933 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Chromium 267.716 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Cobalt 228.616 0.0000000 o.ooooooo 0.0000000 0.0000000 0.0000000 Copper 324.754 0.0000000 0.0000000 0.0000000 0.0000000 "- 0.0000000

Iron 271.441 0.0000000 0.0000120 0.0000000 0.0000000 0.0000580

Lead 220.353 0.0000000 0.0000000 0.0000000 ,0.0000000 0.0000000

Magnesium 279.079 0.ooooooo 0.0000000 0.0000180 0.0000000 0.0000000 Manganese 257.610 0.0001480 0.0000000 0.0000000 0.0000000 0.0000000

Molybdenum 202.030 -0.0020110 0.0004000 0.0000000 0.0000000 0.0004250

Nickel 231.604 -0.0001510 0.0000000 0.0000000 0.0000000 0.0000000

Phosphorus 178.287 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Potassium. 766.491 o.ooooooo 0.0000000 0.0000000 . 0'. ooooooo 0,0000000 Selenium 196.026 0.0000000 0.0000000 0.0000000 o.ooooooo 0.0000000 Silver 328.068 0.0000000 .0.0000000 0.0000000 0.0000000 . 0.0000000

Sodium 330.232 /-O.OOOOOOO 0.0000000 0.0000000 0.0000000 0.0000000

Strontium 421.552 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Thallium 190.864 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Tin 189.989 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Titanium 334.941 0.0000000 -0.0003370 0.0000000 0.0000000 0.0000000

Vanadium 292,402 0.0000000 -0.0002870 0.0000000 0.0000000 0.0000000

Zinc 206.200 0.0000000 0.0000000 0.0000000 0.0000000 0,0000000

Comments:


USEPA-CLP FORMS

11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)

Lab Name: T e s t A m e r i e a B u r l i n g t o n ; C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case No. : 2 4 0 4 5 SAS N o . : SDG No . : JNB070

ICP ID Number: TJA ICAP 7 Da t e : 0 7 / 1 1 / 0 8

Wave

Interelement Correction Factors for: length

Analyte (nm) Pb Sb Se Si Tl

Aluminum 308.215 -0_. 0000570 0.0000000 0.0000190 0.0000000 , 0.0000000

Antimony 206.838 0.0000000 0.0000000 0.0000000 0.0007570 0.0000000

Arsenic 189.042 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Barium 493.409 0.0000000 0.0000000 0,0000000 0.0000000 0.0000000

Beryllium 313.042 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Boron 249.678 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Cadmium 226.502 0.0000000 0.0000000 0.0000000 0.0008870 o.ooooooo

Calcium 317.933 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Chromium _ 267.716 0.0000000 0.0130170 0.0000000 0.0033900 0.0001210

Cobalt 228.616 o.ooooooo 0.0000000 0.0000000 0.0000000 0.0053,640

Copper 324.754 -0.0001350 0.0000000 0.0000000 0.0000000 0.0000000

Iron 271.441 0.0000180 0.0000470 0.0000310 0.0000000 o.ooooooo

Lead 220.353 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Magnesium 279.079 0.0000030 0.0000000 >'0.0000000 0.0000000 0.0000000

Manganese 257.610 0.0000000 0.0000000. 0.0008470 0.0000000 0.0017310

Molybdenum 202.030 -0.0029500 -0.0008470 0.0002350 0.0000000 0.0000000

Nickel v 231.604 0.0000560 -0.0001980 0.0000000 0.0000000 0.0000000

Phosphorus 178.287 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Potassium 766.491 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Selenium 196.026 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Silver 328.068 0.0000000 .0.0000000 0.0000000 0.0000000 0.0000000

Sodium 330,232 0.0000000 0.0000000 0.0000000 0.0000000 . 0.0000000.

Strontium 421.552 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Thallium 190.864 0.0000000 0.0000000 o.ooooooo 0.0000000 0.0000000

Tin 189.989 O.OOOOOOO -0.0059460 0.0000000 0.0000000 0.0000000

Titanium 334.941 -0.0005950 -0.0001800 0.0000000 >0.0071290 -0.0012330

Vanadium 292.402. -0.0000370 -0.0030990 0.0000000 ,0.0020480 0.000336,0

Zinc 206,200 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000

Comments:

Form XI (PART 2) IN

USEPA-CLP FORMS

11A



Lab Code: STLV Case No. ; 24045 SAS No . : SDG No. JNB070

ICP ID Number: TJA ICAP 7 Da t e : 0 7 / 1 1 / 0 8

Wave

Interelement Correction Factors for: length

Analyte (nm) • V Zn X

Aluminum 308.215 0.0000000 0.0000120 L 1 1 r-Antimony 206.838 0.0000000 0.0000000

Arsenic 189.042 0.0000000 0.0000000

Barium 493.409 0.0000000 0.0000000 1

Beryllium 313.042 0.0000000 0.0000000 1 1 Boron 249.678 0.0000000 O.ooooooo ' 1 1 Cadmium 226.502 0.0000000 0.0000000 1 1 Calcium 317.933 0.0000000 0.0000000

Chromium 267.716 0.0000000 0.0000000 1 Cobalt 228.616 •0.0000000 0.0000000 1 Copper 324.754 0.0000000 0.0003930 1 1 Iron 271.441 0.0000340 0.0000670 1 Lead 220.353 0.0000000 0.0000000 1 1 Magnesium 279.079 0.0000000 0.0000350 1 Manganese 257.610 0.0000000 :0.0000000

Molybdenum . 202.030 -0.0197980 -0.0001260

Nickel 231.604 0.0000000 0.0047210

Phosphorus 178.287 0.0000000 0.0000000 1 Potassium 766.491 0.0000000 0.0000000 ; v, - • 1 . . , Selenium 196.026 0.0000000 0.0000000 1 Silver 328.068 0.0000000 0.0000000 1 Sodium 330.232 0.0000000 0.0000000 1 Strontium 421.552 0.0000000 0.0000000

Thallium 190.864 0.0000000 0.0000000

Tin 189.989 .0.0000000 0.0000000

Titanium 334.941 0.0014890 -0.0006710 1 Vanadium 292.402 0.0000000 0.0000000 1 Zinc 206.200 0.0000000 0.0000000 1

Comments:


USEPA-CLP FORMS

• n

ICP LINEAR RANGES (QUARTERLY)


Lab Code: STLV Case No.: 24045 SAS N o . : '

ICP ID Number: TJA ICAP 7 Da t e : 07/01/08

Integ.

Concentration Time

(ug/L) Analyte (Sec.)

Silver 20.00 500.0

Arsenic 20.00 2000.0

Barium 20.00 4000.0

Cadmium 60.00 2000.0

Chromium 20.00 4000.0

Copper 20.00 4000.0

Lead 20.00 4000.0

Selenium 20.00 2000.0

SDG No. : JNB070

M

|P

|P

P

|P

|P

|P

|P

|P

Comments:

Form XII - IN

USEPA-CLP FORMS

13

PREPARATION LOG

Lab Name: T e s t A m e r i e a B u r l i n g t o n ___ C o n t r a c t : 2 4 0 4 5

Lab Code: STLV Case N o . : 2 4 0 4 5 SAS N o . : SDG N o . : JNB070

Method: CV

EPA Preparation . Initial Volume Volume Sample No. Date mL (mL)

LCSW081508B 08/15/08 50.0 50.0 MB081308G 08/15/08 5.00 50.0 NB-H003801 08/15/08 5.00 50.0 NB-H003802, 08/15/08 5.00 50,0 NB-H003803 08/15/08 5.00 50.0 NB-H003803D 08/15/08 5.00 50,0 NB-H003803S ' 08/15/08 5.00 50.0 NB-H003804 08/15/08 5.00 50.0

Form X I I I - IN

USEPA-CLP FORMS

13

PREPARATION LOG

Lab Name: TestAmeriea• B u r l i n g t o n Contract: 24045 •

Lab Code: STLV Case No.: 24045 SAS No.: SDG No.: JNB070

Method: P

EPA Preparation Initial Volume Volume Sample No. Oate mL (mL)

LCSW081508A 08/15/08 100.0 100.0 MBLK081308G 08/15/08 100.00 100.0 NB-H003801 08/15/08 100.00 . 100.0 NB-H003802 08/15/08 100.00 100.0 NB-H003803 08/15/08 100.00 100.0 NB-H003803D 08/15/08 100.00 100.0 NB-H003803S 08/15/08 100.00 100.0 NB-H003804 08/15/08 100.00 100.0

Form XIII - IN

USEPA-CLP FORMS

14

ANALYSIS RUN LOG

Lab Name: TestAmeriea Burlington C o n t r a c t : 24045

Lab Code: STLV Case N o . : 24045 SAS N o . : SDG N o . : JNB070

I n s t r u m e n t ID Number: TJA ICAP 7 Method:

End D a t e : 0 8 / 1 5 / 0 8 S t a r t D a t e : 0 8 / 1 5 / 0 8

EPA Analytes

Sample No.

D/F Time % R A L

S B

A S

B A

B E

c D c A

c R

c o

C

u F E

p B

M

o M N

H

o N I

K s E

A G

N A

T L

V z N

c N

SO 1.00 1735 X X X X X X X X

STD7 1.00 1739

STD8 1.00 1743 X X X

STD4 1.00 1747 X X X X X

. ICV ( 1.00 17 51 X X X X X X X X

ICB 1.00 1754 X X X X X X X X

ICSA 1.00 1758 X X X X 1* X X X ICSAB 1.00 1802 X X X X X X X X

CRI 1.00 1806 X X X X X X

USEPA-CLP FORMS

14

ANALYSIS RUN LOG

Lab Name: T e s t A m e r i e a B u r l i n g t o n C o n t r a c t : 24045

Lab Code; STLV Case No . : 2 4 0 4 5 SAS No . : SDQ N o . : JNB070

I n s t r u m e n t ID Number: Leeman H y d r a AA (2) Method: CV

End D a t e : 0 8 / 1 8 / 0 8 S t a r t D a t e : 0 8 / 1 8 / 0 8

EPA Analytes

Sample D/F Time % R

A S A B B C C C C C F P M M H N K S A N T V Z C

No. L B S A E D A R O U E B G N Q I E Q A L N N

SO 1.00 1211 X

SO. 2 1.00 . 1214 X

SO.5 1.00 ,1217 X

SI 1.00 1219 X

S5 1.00 1222 X

S10 1.00 1224 X

ICV 1.00 1226 X

ICB 1.00 1228 X

CCV 1.00 1230 X

CCB 1.00 1232 X

ZZZZZZ 1.00 1234

LCSW08I508B 1.00 1237 - X

MB08130BQ 1.00 1239 X

NB-H003801 1.00 1241 X

NB-H003802 1.00 1243 X

NB-H003804 1.00 1245 X

NB-K003803 1.00 1247 X

NB-H003803S 1.00 1249 X

NB-H003803D 1.00 1251 X

CCV 1.00 1253 X

CCB 1.00 1255 X

Form XIV - IN

TestAmeriGa

. THE LEADER IN ENVIRONMENTAL TESTING

Sample Data Summary - 8260B TCLP

FORM 1 . .JACEN3. SAMPLE NO.

VOLATILE ORGANICS ANALYSIS DATA SHEET

NB-H003801

Lab Name:,TESTAMERICA BURLINGTON Contract: 24045.


Matrix: (soil/water). WATER Lab Sample ID.: .763 3 28

Sample wt/vol: . 5.000- (g/mL) ML Lab File ID: 763328

Level: (low/med) LOW Date Received: 08/09/08

% Moisture: not dec. Date Analyzed: 08/14/08

GC Column: CAP '- ID: 0.53 (mm) Dilution Factor.; 8.8

Soil Extract Volume: (uL) Soil Aliquot Volume: (UL)

CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

•75-01-4--- Vinyl Chloride 9.8 J 75-35-4 • - ! , 1-Dichloroethene •• 44 U 78.-93-3 2-Butanone 44 U 6 7,-66-3-- : Chloroform 44 U 56-23-5 Carbon Tetrachloride 44 U 71-43-2 Benzene 44 U 107-06-2 --1,2-Dichloroethane - : 44 U 79-01-6 ----Trichloroethene .. 1600 127-18-4 . Tetrachloroethene 62 108-90-7----- Chlorobenzene 44 U;

FORM I VOA

FORM 1 JACEN3 SAMPLE NO.VOLATILE'ORGANICS ANALYSIS DATA SHEET.

NB-H003802

-Lab Name: TESTAMERICA BURLINGTON Contract: 24045

Lab CodeXSTLV Case No.: 24045 SAS No.: " SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: 763331

Sample wt/vol: 5.000 (g/mL) ML Lab File ID: 763331


% Moisture: not dec. ' Date Analyzed: 08/14/08

GC Column: CAP ID: 0.53 (mm) Dilution Factor: 8.8

Soil Extract Volume: (uL) Soil Aliquot Volume: (uL)



75-01-4- — -Vinyl Chloride_ 25 J 75-35-4 — 1,1-Dichloroethene 44 U 78-93-3-.-- — 2-Butanone_ •' • 87 B 67-66-3 • --Chloroform 44 U 56-23-5 Carbon Tetrachloride_ 44 U ... 71-43-2 Benzene 44 U 107-06-2- — — 1;2-Dichloroethane_ ' 44 U 79-01-6- — —Trichloroethene__ 15000 E 127-18-4 • --Tetrachloroethene 140 108-90-7 —Chlorobenzene 44 U

FORM I VOA

FORM 1 JACEN3 SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA-SHEET

NB-H003802DL Lab Name:, TESTAMERICA BURLINGTON Contract: 24045 '

Lab Code: STLV Case No.: 24045/ SAS No.: SDG No.,:-- JNB070

Matrix: (soil/water) WATER Lab Sample,ID: 763 3 31D1



% Moisture: not dec. ._ Date Analyzed: 08/15/08

GC Column: CAP ID: 0.53 (mm) Dilution Factor: 122.0

Soil Extract Volume: (uL) .Soil Aliquot Volume: (UL)

CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

75-01-4----- Vinyl Chloride 610 U 75-3 5-4 . 1,1-Dichloroethene 610 u 78-93-367-66-3

-2-Butanone --^Chloroform

. 610 610

UU 56-23-5 -Carbon Tetrachloride. 610 U 71-43-2 Benzene •; 610 U 107-06.-2--. 1,2-Dichloroethane 610 U 79-01-6 — . '-Trichloroethene 23000 D

. 127-18-4 Tetrachloroethene 130 DJ 108-90-7 ---Chlorobenzene. 610 U

FORM I VOA

FORM 1 JACEN3 SAMPLE NO.


NB-H0O3803.

Lab Name: TESTAMERICA BURLINGTON. . Contract: 24045

Lab Code: STLV Case No.: 24045 . SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER •. Lab Sample ID:. 7633 34


Level: (low/med) LOW Date Received: 08/09/0,8

% Moisture: not dec. Date Analyzed: ,08/14/08

GC Column: CAP ID: 0.53 (mm) Dilution Factor:'8.8



CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

75-01-4- -Vinyl Chloride_ 62

75-3.5-4 -j- - -1,1-Dichloroethene . 44

.78-93-3 2-Butanone . .' • • 84

67-66-3- Chloroform -44

56-23-5 -Carbon Tetrachloride_ . 44

71-43-2 -- -Benzene 44

107-06-2---- -- --1,2-Dichloroethane 44

79-01-6 - ---Trichlproethene 14000

127-18-4 - ---Tetrachloroethene_ 240

108-90-7---- Chlorobenzene 8.8

FORM I VOA

. FORM 1 JACEN3 SAMPLE NO.


NB-H003803DL

Lab Name: TESTAMERICA BURLINGTON Contract: 2404 5

Lab Code: STLV Case No.': 24045 SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: 763 3 34D1

• i

" ~ v • •

Lab File ID: 76333413

Sample wt/vol: 5.00 0 (g/mL) ML

Date Received: 08/09/08

Level: (low/med) LOW

Date Analyzed: 08/15/08

% Moisture: not dec. __

Dilution Factor: 176.0

GC Column: CAP ID: 0.53 (mm)

Soil Aliquot Volume: (uL)

Soil Extract Volume: y (uL)


CAS NO. COMPOUND (ug/L or .ug/Kg) UG/L

75-01-4- -Vinyl Chloride

75-35-4------ • -1,1-Dichloroethene_

78-93-3 - •.-2-Butanone ' X

67-66-3 -Chloroform

56-23-5--. •-Carbon Tetrachloride_

71-43-2 •-Benzene

107-06-2- 1,2-Dichloroethane_

79-01-6- -Trichloroethene

12 7-18 -.4-. Tetrachloroethene

108-O0-7—'-- Chlorobenzene

FORM T VOA

FORM 1 JACEN3 SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET

NB-H003804 Lab Name:. TESTAMERICA. BURLINGTON Contract: 24045,


Matrix: (soil/water) WATER. Lab Sample ID: 76333 7

Sample,wt/vol: 5.000 (g/mL) ML Lab File ID: 76333712

Level: (low/med)/ LOW Date Received: 08/09/08


GC Column: CAP ID: 0.53 (mm) Dilution Factor:. 8.8

Soil Extract Volume: (uL) Soil Aliquot Volume: :_ (uL)

CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L

75-01-4 — V i n y l Chloride 2 1 J 75-35-4 •1,l-Dichloroethene_ 4 4 U . 78-93-3 • 2 -Butanone 4 4 U 67-66-3 •Chloroform 4 4 U 56-23-5 Carbon Tetrachloride_ 4 4 u 71-43-2- •---Benzene 4 4 u • 107-06-2---79-01-6

1,2-Dichloroethane_ -Trichloroethene

4 4 660

u 127-18-4 Tetrachloroethene - 25 J 108-90-7 • Chlorobenzene 4 4 u

FORM I VOA

FORM 1 , CLIENT SAMPLE NO.


MBLK814 08NA

Lab Name: TESTAMERICA BURLINGTON Contract:'24045

Lab Code: STLV " Case No.: 24045 SAS No.: SDG No.: JNB070 '

Matrix: (soil/water) WATER . Lab Sample ID:. MBLK81408NA

Sample wt/vol: 5.000 (g/mL) ML • Lab File ID: ' NPSB05

Level: (low/med) LOW' Date Received:


GC Column:'CAP ID:. 0.53 (mm) Dilution-Factor: 1.0


•CONCENTRATION UNITS:

CAS NO. COMPOUND (ug/L or ug/Kg) UG/L.

,75-01-4--- — -Vinyl Chloride_ 5 . 0 U 75-35-4 1,l-Dichloroethene_ • 5 . 0 •u 78-93-3 — 2 -Butanone , 5 . 0 U 67-66-3---- Chloroform 5 . 0 U 56-23-5---- Carbon Tetrachloride_ 5 . 0 U 71-43-2 , •---Benzene 5 . 0 U 107-06-2 1,2-Dichloroethane_ 5 . 0 U 79-01-6-1 -Trichloroethene 5 . 0 U 127-18-4 Tetrachloroethene 5 . 0 U 108-90-7 Chlorobenzene 5 . 0 U

FORM I VOA

- FORM 1 CLIENT SAMPLE NO.


MBLK81508NA

Lab, Name: TESTAMERICA BURLINGTON . Contract: 24045'

Lab Code: STLV Case No.: 24045 SAS No.': - SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: MBLK815 08NA

Sample wt/vol: 5.000 (g/mL) ML Lab File ID: ' NPSB04B

Level: . (low/med) LOW \Date Received:

% Moisture: not dec. •Date Analyzed: 08/15/08

GC Column: CAP ID: 0.53- (mm) Dilution Factor: 1.0

Soil Extract Volume: (uL) Soil Aliquot Volume: (uL')


CAS NO; COMPOUND (ug/L or ug/Kg) UG/L Q

75-01-4 — --Vinyl. Chloride 5.0 U

75-35-4 ----1,1-Dichloroethene 5.0 U

78-93-3 2-Butanone •'5.0 U

67-66-3--- Chloroform -5.0 U -..

56-23-5 ---Carbon Tetrachloride 5.0 U

71-43-2 Benzene 5.0 U

107-06-2--- 1,2-Dichloroethane 5.0 U

79-01-6 -Trichloroethene 0.99 J

12 7-18-4 Tetrachloroethene / 5.0 U

108-90-7 ;- -Chlorobenzene 5.0 u

FORM I VOA

file:///Date

FORM 1 . -CLIENT SAMPLE NO.

.VOLATILE ORGANICS ANALYSIS DATA SHEET

ZB08130801

Lab Name: TESTAMERICA BURLINGTON . Contract: 24045


Matrix: (soil/water) WATER • \ Lab Sample ID: ZB08130801

Sample wt/vol: 5.000 (g/mL) ML Lab File ID: ZB0813 01 '

Level: (low/med) LOW Date Received:


GC Column: CAP , ID:.0.53 (mm) Dilution Factor: 1.0.

Soil Extract Volume:- (uL) y Soil Aliquot Volume: (iiL)



75-01-4 Vinyl Chloride 5.0 U 75-35-4 1,1-Dichloroethene 5.0 U 78-93-3 2-Butanone 7 2.9 J. 67-66-3--- Chloroform . > 5.0 U' 56-23-5 -----Carbon Tetrachloride 5.-0 U 71-43-2 • --Benzene 5.0 U 107-06-2 -1, 2-Dichloroethane 5.0 U 79-01-6 Trichloroethene ' .5.0 U 127-18-4 Tetrachloroethene 5.0 U 108-90-7--. Chlorobenzene 5.0 U

FORM I VOA

http:ID:.0.53

FORM 1 CLIENT. SAMPLE NO.


NA081408LCS

Lab Name: TESTAMERICA BURLINGTON .Contract: 24045

Lab Code: STLV Case No.: 24045 SAS No.. : SDG No--. : JNB07 0

Matrix: (soil/water) WATER Lab Sample ID: NA081408LCS

Sample wt/vol: 5.000 (g/mL) ML Lab File ID: NPS050Q

Level: •' (low/med) LOW Date Received:

% Moisture:, not dec. , Date Analyzed: 08/14/08

. • ' . - • • > .

GC Column:- CAP ID: 0.53 (mm) Dilution Factor: 1.0

Soil Extract Volume: (uL) ' Soil Aliquot Volume: (uL)



75-01-4 -Vinyl Chloride_ 54

75-35-4 ----1,l-Dichloroethene_ 51

78-93-3- — — — — 2 -Butanone 63

;67-66-3----- - Chloroform 52

56-23-5----- — Carbon Tetrachloride_ 53

71-43-2 ----Benzene 53

107-06-2 1,2-Dichloroethane_ 51

79-01-6 — - - - -Trichloroethene^^ 53

127-18-4- Tetrachloroethene 54

108-90-7 — — Chlorobenzene 51

FORM I VOA

FORM 1 CLIENT SAMPLE NO.

VOLATILE ORGANICS ANALYSIS'DATA SHEET

NA0814 08LCSD

Lab Name: TESTAMERICA BURLINGTON .Contract: 24045

Lab Code: STLV . Case No.: 24045 SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: NA081408LCSD

Sample wt/vol: .5.000 (g/mL) ML Lab File ID: NPS0 50Q2 .

-Level: (low/med) LOW Date Received:

% Moisture: not dec. ' - Date Analyzed: 08/14/08

GC Column: CAP ID: 0.53 (mm) ' Dilution Factor: 1.0

Soil Extract Volume: (uL) . Soil Aliquot Volume: (uL)



75-01-4 Vinyl Chloride • " 5 6

75-35-4 1,1 -Di chloroethene. 51

78-93-3 ---2-Butanone 66

67-66-3-- Chloroform 52

56-23-5 ---Carbon Tetrachloride 53

71-43-2--1 Benzene 52

107-06-2--- 1,2-Dichloroethane 52

79-01-6--- Trichloroethene . 5 2

127-18-4- — ; -Tetrachloroethene ,52

108-90-7- : Chlorobenzene 51

FORM I VOA



NA081508LCS

Lab Name: TESTAMERICA BURLINGTON Contract: 24045.

Lab Code: STLV Case No!: 24045 SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: NA081508LCS

Sample wt/vol: . 5.000 (g/mL) • ML Lab File ID: NPS050BQ

Level: (low/med) LOW. Date Received: ___


-GC Column: CAP ID: 0.53 (mm) Dilution Factor: 1.0




75-01-4 -Vinyl Chloride 54

75-35-4 1,1-Dichloroethene 50

78-93-3 2-Butanone 50

67-66-3- Chloroform/' 51

56-23-5- --Carbon Tetrachloride • ,52

71-43-2- — Benzene 52

107-06-2 1,-2 -Dichloroethane 51

79-01-6 Trichloroethene 53 B

127-18-4 ---Tetrachloroethene 52

108-90-7- --Chlorobenzene 50

1 • •

FORM I VOA

... FORM. 1 -• -•-. JACEN3 "SAMPLE NO.^


NB-H0 03 803DLMS

Lab Name: TESTAMERICA BURLINGTON Contract: 24045

I

SDG No.: JNB070 Lab Code:, STLV Case No.: 24045 SAS No.:

Lab Sample ID: 763334D1MS Matrix: (soil/water) WATER

Lab File ID: 763334M3 Sample wt/vol: 5.000 (g/mL) ML •

Date Received: 08/09/08 Level: -• (low/med) LOW

Date Analyzed: 08/15/08 % Moisture: not dec. •

Dilution Factor: 176.0. GC Column: CAP ID: 0.53 (mm)

Soil Aliquot Volume: (uL) Soil Extract Volume:. (uL)



75-01-4-- -Vinyl Chloride 9700 D 75-35-4 . 1,1-Dichloroethene : 8500 D. 78-93-3 — 2-Butanone 8600 DB 67-66-3-- -Chloroform 8700 D 56-23-5 :-Carbon Tetrachloride 8900 D 71-43-2-- Benzene 8800 D ' 107-06-2 '-—.1,2-Dichloroethane. 8700 D 79'-01-6 Trichloroethene ' 32000 D . 127-18-4 — ---Tetrachloroethene 9300 D 1.08-90-7-- • Chlorobenzene 9200 D

FORM I VOA

. FORM 2.

WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY



CLIENT SMC1 SMC2 SMC3 OTHER TOT SAMPLE NO. (DCE)# (TOL)# (BFB)# (DCB)#. OUT

01 NA081408LCS 98 10 0 99 96 0 02 NA08140 8LCSD 100 99 •98- 96 0 03 MBLK814 08NA • 101, 95 .101 97 0 04 ZB08130801 101 98 101 •96 0 05 NB-H003801 101 99 100 96 0 06 NB-H003802 102 97 100 96 0 07 NB-H003803 100 .93 102 100 0 08 NA081508LCS 98 * 99 99 96 0 09 MBLK81508NA 100 99 104 97 0 10 NB-H003804 101 98 99 97 0 11 NB-H003802DL ,89 95 102 99 0 .12 NB-H003803DL 99 94 100 97 . 0 13 NB-H003803DL 96 97 98 94 0 14 15. 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30

QC LIMITS SMC1 (DCE) = l,2-Dichloroethane-d4 (70-125)

SMC2 (TOL) = Toluene -_d8 (85-120)

SMC3 (BFB) = Bromofluorobenzene (85-120)

OTHER(DCB) = 1,2-Dichlorobenzene-d4, ' (85-120)

# Column to be used to flag recovery values

•Values outside of contract required QC limits

D System Monitoring Compound diluted out

page 1 of 1 FORM II VOA

FORM- .3 .

WATER VOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY


Lab Code: STLV Case No.: 24045 SAS No.: SDG No.: JNB070'

Matrix Spike - JACEN3 Sample No.: NB-H00380

COMPOUND

Vinyl Chloride

1,1-Dichloroethene

2-Butanone

Chloroform

.Carbon Tetrachloride

Benzene

1, 2-Dichloroethane

Tri chloroethene

Tetrachloroethene

Chlorobenzene.

SPIKE

ADDED

(ug/L)

8800

8800

8800

8800

8 800

8800

• 8800

8800

8800

8800

,SAMPLE

CONCENTRATION.

(ug/L)

0-0

o.o '•

0.0 .

0.0

0.0

0.0

0.0

23000

240

0.0

MS

CONCENTRATION

(ug/L)

9700

8500 :

8600 ••

8700s

8900 '

8800

8700

32000

9300

9200

MS %

REC #

110

96

98

99

101.

100

99

102

103

104

QC.

LIMITS

REC.

70-135

80-125

50-150

85-120

80-120

85-120

80-125

85-120

85-120

85-120

# Column to be used to flag recovery and RPD values with an asterisk

* Values outside of QC limits • c

RPD: 0 out of 0 outside limits

Spike Recovery: 0 out of 10 outside limits

COMMENTS:

FORM III VOA

FORM 3

WATER VOLATILE LAB CONTROL SAMPLE

Lab Name: TESTAMERICA BURLINGTON - Contract: 24045

Lab Code: STLV Case No.: 24045 SAS No. : SDG No.: JNB070

Matrix Spike - Sample No.: NA081408LCS

SPIKE SAMPLE LCS LCS QC. ADDED . . CONCENTRATION CONCENTRATION a. LIMITS

COMPOUND (ug/L) /(ug/L) (ug/L) REC # REC.

Vinyl Chloride 1,1-Di'chloroethene

. y so , 50 ,

' ' 54 51

' 108 102

70-135 80-125

2-Butanone 50 63 . 126 50-150 Chloroform 50 52 104 85-120 Carbon Tetrachloride 50 53 106 80-120 Benzene 50 53 106 85-120 1,2-Dichloroethane 50 51 -,- 102 80-125 Trichloroethene 50 53 106 85-120 Tetrachloroethene 50 54 l 108 85-120 Chlorobenzene 50 51 102 85-120

SPIKE LCSD •LCSD ADDED . CONCENTRATION % "5 • QC LIMITS

COMPOUND (ug/L) _ (ug/L) REC # .RPD # RPD REC.

Vinyl Chloride 50 , 56 112 4 30 70-135 1,1-Dichloroethene 50 51 102 0 30 80-125 2-Butanone 50 66 132 5 30 50-150 Chloroform 50 52 104 < 0 30 8 5-12 0 Carbon Tetrachloride . 50 53. 106 0 30 80-120 Benzene 50 52 104 2 3 0 85-120 1,2-Dichloroethane -50 52 104 2 3 0 80-125 Trichloroethene 50 52 104 2 30 85-120 Tetrachloroethene 50 52 104 . 4 30 85-120 Chlorobenzene 50 ' 51 102 0 3 0 ,85-120

# Column to be used to flag recovery and.RPD values with an asterisk

* Values outside oftQC limits

RPD: 0 out of'10 outside limits


COMMENTS: •

X

FORM III VOA

FORM 3

WATER VOLATILE LAB CONTROL SAMPLE


Lab Code: STLV Case No.: 24045 SAS No.: SDG No. iJNB07 0

Matrix Spike - ^ Sample No.: NA081508LCS

QC.

LIMITS

REC.

======

70-135

80-125

50-150

85-120

.80-120

85-120

80-125

85-120

'85-120

85-120

SPIKE

.ADDED

COMPOUND • (ug/L) .

======================== =========

Vinyl Chloride 50

1,1-Dichloroethene 50

2-Butanone , 5 0

Chloroform 50

Carbon Tetrachloride , 50

Benzene > 50

1,2-Dichloroethane 50

Trichloroethene 50

Tetrachloroethene 50

Chlorobenzene 50

SAMPLE LCS

CONCENTRATION CONCENTRATION

(ug/L)- , (ug/L)

= = == == === = = ============== =

54 •

50

50

51

52

52

51

53

52

N 50

LCS

o, o

REC #

======

108

100

100

102

104

104

102

106

104

10 0

# Column to be used, to flag recovery and RPD values with an asterisk

* Values outside of QC limits ,

RPD: '0 out of 0 outside limits


COMMENTS: ,

FORM III VOA

. FORM 4 CLIENT SAMPLE NO.

VOLATILE METHOD BLANK.SUMMARY

MBLK814 08NA


Lab Code:. STLV Case No.: 24045 SAS No.: SDG No.: JNB070 ~> ' " ' . ' ' , • .

Lab File ID:NPSB05 Lab Sample ID: MBLK81408NA

Date Analyzed: 08/14/08 • Time Analyzed: 1311

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N "

Instrument ID:. N . ' . - . - ^

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:

01

02

03

04

05

06

07

08

09

10

11

12

13

14

15

16

17

18

19

20

21

22

2 3

24

25

26

27

28

29

30

LAB LAB TIME

SAMPLE NO. SAMPLE ID FILE ID ANALYZED

NA0814 08LCS. NA081408LCS NPS050Q , 1110

NA0 814 0 8LCSD NA081408LCSD ' NPS050Q2 1211

>.

v

^

14 '

^ ; . .

COMMENTS:

page 1 of 1

FORM IV VOA

FORM 4. CLIENT SAMPLE NO.

VOLATILE METHOD BLANK SUMMARY

MBLK81508NA


Lab Code: STLV Case No.-: .24045 SAS No.: SDG No.: JNB070

Lab File ID: NPSB04B ' Lab Sample ID: MBLK81508NA

Date Analyzed': 08/15/08 Time Analyzed: 1104.

GC Column: CAP ID: 0.53 (mm) - Heated Purge: (Y/N) N

Instrument ID: N ^

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:'

01

02

03

04

05

06

07

08

09

10

11

12

13

14

15

16

17

18

19

20

21

22

23

24

25

26

27

28

29

30

COMMENTS;

page 1 of 1 ,

SAMPLE NO.

NA081508LCS

-

!

. LAB.

SAMPLE ID

NA081508LCS

• ' . . - '

,

LAB

' FILE ID

NPS050BQ

f - . •

FORM IV VOA

TIME

ANALYZED

0 933


VOLATILE METHOD BLANK SUMMARY

ZB0813.0801

Lab Name: TESTAMERICA BURLINGTON • Contract: 24045

Lab Code: STLV -, Case No.: 24045 SAS No.: SDG No.: JNB070

Lab File ID: ZB081301 •• . Lab Sample ID: ZB08130801

Date Analyzed: 08/14/08 . Time Analyzed: 1340

GC Column:.CAP ID: 0.53 (mm) Heated Purge: (Y/N) N

Instrument ID: N

THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS and MSD:

LAB LAB TIME

SAMPLE NO. .-• SAMPLE ID FILE ID ANALYZED

01 NB-H003801 763328 763328 14l7

02 NB-H003802 763331 763331 1447

03 NB-H003803 763334 763334 1517

04 NB-H003804 763337 76333712 1149

05 NB-H003802DL •763331D1.-. 76333112 1218

06 NB-H003803DL 763334D1 76333413 1419

07 NB-H003803DL 763 3 34D1MS 763334M3 1449

08

09 10

11

12

13

14

15 -,

16

17

18

- •

19

20

21 . '

22

23

24

25

,26

27

28

29

30

COMMENTS;

page 1 of 1

FORM'IV VOA

FORM 5 •' • • , , ' • VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

. ' • BROMOFLUOROBENZENE (BFB). i


Lab Code: STLV- Case No.-: 24045 SAS. No.: , SDG No.: JNB070

Lab File ID: NPS01PV BFB Injection Date: 08/14/08

Instrument ID: N BFB Injection Time: 0 70 9

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N

. • . • • • • . % RELATIVE m/e . ION ABUNDANCE CRITERIA ABUNDANCE

50 15.0 - 40.0%'Of mass 95 25.7 75 30.0 - 60.0% of mass 95 5,1.9 95 Base Peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.7

173 Less than 2.0% of mass 174 0.0 ( 0.0)1 174 50.0 - 120.0% of mass 95 , 54 .7 175 5.0 - 9.0% of mass 174 4.1 ( 7.4) 1 176 95.0 - 101.0% of mass 174 53 .8 ( 98 .3) 1 177 5.0 - 9.0% of mass 176 3 .7 ( 6.8)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:

EPA LAB LAB DATE TIME SAMPLE NO. SAMPLE ID FILE -ID ANALYZED ANALYZED

01 VSTD005 VSTD005 NPQ005V 08/14/08 0753 02 VSTD02 0 VSTD020 NPS020V 08/14/08 0823 . 03 VSTD050 VSTD050 • NPQ050V 08/14/08 0853 , 04 VSTD100 VSTD100 NPS100V 08/14/08 0923 05 VSTD200 VSTD200 NPS200V 08/14/08 0953 06 NA0814 08LCS NA081408LCS NPS050Q . . , 08/14/08 1110 07 NA081408LCSD NA081408LCSD NPS050Q2 08/14/08 1211 08 MBLK814 08NA MBLK81408NA NPSB05 08/14/08 1311 09 ZB08.130801 : ZB08130801 ZB081301 08/14/08 1340 10 NB-H003801 763328 763328 08/14/08 1417 11 NB-H003802 763331 763331 08/14/08 -144 7 12 NB-H003803 763334 763334 08/14/08 1517 • 13 14 15 16 17 18 19 20 21 22

page 1 of 1

FORM V VOA

^ FORM .5 -. . . - >

VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK

BROMOFLUOROBENZENE (BFB)

Lab Name: TESTAMERICA BURLINGTON Contract: 24 04 5

Lab Code:• STLV Case No.: 24045 SAS No.: SDG No.: JNB0 7 0

Lab File ID: NPS02PV , BFB Injection Date: 08/15/08

Instrument ID: N BFB Injection Time: 0818

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N

% RELATIVE 'm/e ION ABUNDANCE CRITERIA , ABUNDANCE

• 50- 15.0 - 40.0%'of mass 95 26.5 75 30.0 - 60.0% of mass 95 51.8 95 Base Peak, 100% relative abundance. 100.0 . 96 5.0;- 9.0% of mass 95 6.0

173 Less than 2 ..0% of mass 174 0.0 ( 0.0)1 174 50.0 - 120.0% of mass 95 j 56.3 175 5.0 - 9.0% of mass 174 4.1 ( 7.4)1 176 95.0 ' 101.0%-of mass 174 55.2 ( 98.1)1 177 5.0 - 9.0% of mass 176 3.9 ( 7.0)2

1-Value is % mass 174 2-Value is % mass 176

THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS:

EPA LAB LAB DATE TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED ANALYZED

01 VSTD050 VSTD050 NPQ050BV , 08/15/08 0903 02 NA081508LCS NA081508LCS NPS050BQ 08/15/08 0933 03 MBLK81508NA MBLK81508NA NPSB04B 08/15/08 1104 04 NB-H0038 04 763.337 76333712 08/15/08 1149 05 NB-H003802DL 763331D1 76333112 08/15/08 1218 06 NB-H003803DL 763334D1 76333413'. 08/15/08 . 1419 07 NB-H003803DL 763334D1MS 763334M3 08/15/08 144 9' 08 09 10 11 , 12 13

^ •

14 . v 15 16 17 18 -19 20 21

>, ' - •

22 •

page 1 of ,1 FORM V VOA

6A

VOLATILE ORGANICS INITIAL CALIBRATION DATA


Lab Code: STLV Case No.: 24045 SAS No.: C SDG No.: JNB070

Instrument ID: N Calibration Date(s): 08/14/08- 08/14/08

Heated Purge: (Y/N) N Calibration Time(s): -0753 0953

GC Column: CAP . ID: 0.53 (mm).

LAB FILE ID: RRF5 =NPQ005V . RRF20 =NPS020V •

RRF50 =NPQ050V RRF100=NPS100V ' RRF200=NPS200V •

r , • • • - . • •

O

COMPOUND RRFS RRF20 RRF50 RRF100 RRF2 00 RRF RSD

Vinyl Chloride • '* 0.531 0.534 0.526 0.512 0 .493 0.519 3.2* 1,1-Dichloroethene **' 0.380 • 0.3 6-5 0.360 0.354 0.340 0.3 60 4.1* 2-Butanone .* * 0.034 0'. 034 0.035 0.035 0.034 0.034 2.3* Chloroform *' 0.853 0.848 0.855 0.843 0.822 '0.844 1.6* Carbon Tetrachloride '" 0.587 0.602 0.606 0.611 0.614 0.604 1.7* Benzene *̂ 1.013. 0.998 0.997 ; 0.983 0.941 0,. 986 2.8* 1,2-Dichloroethane *k 0.544 ,0.53 9 0.542 0 . 53 9 0.533 0.539 0.8* Trichloroethene *" 0.564 0.549 0.560 0 . 558 0.554 0.557 1.0* Tetrachloroethene , • - "* 0.514 0.492 0.4 98 0.491 0.494 0.498 1.9* Chlorobenzene i " 1.026 0.974 1. 024 0.981 1.015 1.004 2 .4*

• 111,2-Dichloroethane-d4 * 0.466 0.439 0.450 0.451 0.446 0.450

2.2* Toluene-d8 * 1.253 1.225A 1.242 1.231 1.234 1.237 0.9* Bromofluorobenzene * 1.555 1.610 1.647 1.6 90 1.74 5 1.649

- 4.4* 1,2-Dichlorobenzene-d4 *" 0.985 . 0.917 0.922 0.929 0.950 0.941 2.9*

'

'

'

' •\

- • <

'

. r , <

* Compounds with required minimum RRF and maximim %RSD values,

• All other compounds must meet a minimim RRF of 0.010.

FORM VI VOA 3/90

. FORM 7 - ,

VOLATILE CONTINUING CALIBRATION,CHECK

Lab Name': , TESTAMERICA BURLINGTON Contract: 24045

Lab- Code: STLV Case No. 24045 SAS No.: SDG No.: JNB070

Instrument ID: N Calibration Date: 08/15/08 Time: 0903

Lab File ID: NPQ050BV Init. Calib. Date(s): 08/14/08 08/14/08

Heated Purge;- (Y/N) N Init. Calib. Times:' 0753 0953

GC Column: CAP ID: 0.53 (mm)

-' COMPOUND . "• M •'

Vinyl Chloride . 1,1-Dichloroethene 2-Butanone Chloroform Carbon Tetrachloride Benzene 1,2-Dichloroethane Trichloroethene Tetrachloroethene Chlorobenzene • . ;

1,2-Dichloroethane-d4 Toluene-d8 Bromofluorobenzene 1,2-Dichlorobenzene-d4

RRF RRF50 MIN RRF %D

MAX %D

0.519 0.360 0.034 0.844 0.604 0.986 0.539 0.557 0.498 1.004

.0.52 7 . 0.354 0.034 0.83 9 0.599 0.986 0.532 0.573 0.491 0.968 ' 0.3

1.5 1.7 0.0 0.6 0.8 -0.0 1.3

. 2.9 1.4 3.6

20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0

0.450 1.237 1.649 0.941

0.435 1.212 1.622 0.904

3.3 2.0 1.6 3.9

20.0 20.0 20.0 20.0

FORM VII VOA

FORM 8

VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY


Lab Code: STLV •Case No.: 24045 SAS No.: SDG No.: JNB070

Lab File ID (Standard) :. NPQ050V Date Analyzed: 08/14/08

Instrument ID: N Time Analyzed: 08 53

GC Column: CAP ID: 0.53 (mm) Heated Purge: (Y/N) N .'

IS1 IS2(CBZ) IS3(DCB)

AREA # RT, # . AREA # RT # AREA # RT #

12 HOUR STD 2629572 10.26 2588694 16.19 1355970 20.30

UPPER LIMIT 5259144 .10.76 5177388 16.69 2711940 20.80

LOWER LIMIT 1314786 9.76 1294347 15.69 677985 19.80

CLIENT

SAMPLE NO.

/ •

01 NAO81408LCS 2 672494 10.27 2634511 16.19 1396192 20.3002 NAO81408LCSD 2604431 10.27 2598826 16.19. 1365846 20.30

03 MBLK814 08NA 2 501531: 10.26 2590454 16.19 13 072 96 20.32

04 ZB08130801 2476448 10.26 2502 009 16.19 1317922 20.31

05 NB-H003801 2473944 y 10.24 2470843 16.19 - 1320284 20.30

06 NB-H003802 . 2442056 "10.24 2477356 16.18 1329347 .. 2 0.30

07 NB-H003803 2473770, 10.27 2565120 16.19 1290226 20.31

08 . j. . i

09

10

11

12 1

.13

.14 . i

15

16

17

18

19 ' .

20

21

22

151 = Fluorobenzene

152 ^(CBZ) = Chlorobenzene-d5

153 (DCB) = l,4-Dichlorobenzene-d4

AREA UPPER LIMIT = +100% of internal standard area

AREA LOWER LIMIT = - 50% of internal standard area

RT UPPER LIMIT = + 0,50 minutes of internal standard RT

RT LOWER LIMIT = - 0.50 minutes of internal standard RT -,.

# Column used' to flag values outside QC limits with an asterisk.

* Values outside of QC limits. '

page 1 of 1

FORM VIII VOA

• FORM 8 . •

VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY

Lab Name: TESTAMERICA BURLINGTON Contract: 24045.

Lab Code: STLV Case No.: 24045 ' SAS No.: . SDG No.: JNB070

Lab File ID (Standard): NPQ050BV Date Analyzed: 08/15/08

Instrument ID: N ' Time Analyzed: 0903

GC Column: CAP ID: 0.53 (mm), Heated Purge: (Y/N) N

IS1 IS2(CBZ) . IS3(DCB)

AREA #. RT # AREA # • RT ; # ^ AREA • # RT #

12 HOUR STD 2.633792 10.28 2660955 16.19 1400961 20.30

UPPER LIMIT 5267584 10.78. 5321910 16.69 2801922 20.80

LOWER LIMIT 1316896 9.78 1330478 15.69 700,480. .19.80

CLIENT

SAMPLE NO. X

01 NA081508LCS 2634307 10.29 2 609244 16.19 1367530 20.30 02 MBLK81508NA 2547149 10.28'. 2509270 16.15 .1291124 20.27 03 NB-H003804 2528363 10.26 2558473 16.17 . 1357130 20.28 04 NB-H003 8 02DL 2835010 10.28 2594838 16.19 1323706 20.30

. 05 NB-H003803DL 2504429 10.27 2507956 16.19 1297759 20.31 06 NB-H003803DL 2523437 10.25 ' 2460365 16.20 1357978 20.31

,07 ' 08 09 10 11 12 i 13 14 15 • • .c

. 16 17 .18 / 19 20 -21 22 \ -

151 = Fluorobenzene

152 (CBZ) = Chlorobenzene-d5

153 (DCB) = l,4-Dichlorobenzene-d4

AREA,UPPER LIMIT = +100% of internal standard area

AREA LOWER LIMIT = - 50% of internal standard area"

RT UPPER LIMIT = + 0.50 minutes of internal standard RT

RT LOWER LIMIT-= - 0.50 minutes of internal standard RT

# Column used to flag values outside QC limits with an asterisk.

* Values outside of QC limits.

page 1 of 1

FORM VIII VOA

estAmerica

•.•mm

THE LEADER IN ENVIRONMENTAL TESTING • X

Sample Data Summary - 8270C TGLP

Semivolatile

FORM.1 JACEN3 SAMPLE NO.

SEMIVOLATILE ORGANICS, ANALYSIS DATA SHEET

NB-H003801

Lab Name: TESTAMERICA BURLINGTON Contract: 24045>

Lab Code: STLV Case No.: 24045 SAS No.: SDG No. : JNB.070


Sample wt/vol: 200.0 (g/mL) ML Lab File ID: .763327


X

% Moisture: X decanted: (Y/N)

Date Extracted:08/18/08

Concentrated Extract Volume: 1000(uL)

Date Analyzed: 08/18/08

Injection Volume: .2.0(uL)

Dilution Factor: 1.0

GPC Cleanup: , (Y/N) N pH: ._


GAS NO. COMPOUND (ug/L or ug/Kg) UG/L

110-86-1 •Pyridine_

106-46-7 1,4-Dichlorobenzene_

95-48-7- •• 2-Methylphenol . .

106-44-5- 4-Methylphenol .

67-72-1 '• --- -Hexachloroethane

98-95-3---------Nitrobenzene

87-68-3----- Hexachlorobutadiene

88-06-2 2,4,6-Trichlorophenol_

95-95-4 ----2,4,5-Trichlorophenol_

121-14-2 ----2,4-Dinitrotoluene

118-74-1 Hexachlorobenzene

87-86-5--------Pehtachlorophenol

FORM I SV


SEMIVOLATILE ORGANICS, ANALYSIS DATA SHEET

.NB-H003802

Lab Name: TESTAMERICA'BURLINGTON Contract: 24045



Sample wt/vol: 200.0 (g/mL) ML Lab File ID: 763330 ,


% Moisture: decanted: (Y/N)_ Date Extracted:08/18/08

Concentrated Extract Volume: ' 1000(uL) Date Analyzed: 08/18/08

Injection Volume: 2.0(uL) Dilution Factor.: 1.0

GPC Cleanup: (Y/N) N , "" pH:


CAS NO. COMPOUND (ug/L or ug/Kg)* UG/L

110-86-1- Pyridine 19 J

106-46-7 1, 4 -Dichlorobenzene 37 J

95-48-7--. 2-Methylphenol 50 U

: 106-44-5 --4-MethylphenoI 17 J . 67-72-1---- Hexachloroethane 50 U 98-95-3- Nitrobenzene 50 U 87-68-3--- --Hexachlorobutadiene 50 U 88-06-2 --2,4,6-Trichlorophenol 50 U 95-95-4--' - - - - 2 . , 4,5-Trichlofophenol 130 U 121-14-2 2,4-Dinitrotoluene 50 u

118-74-1 Hexachlorobenzehe 50 u

87-86-5 Pentachlorophenol 130 u

FORM I SV

FORM . 1 ; JACEN3 SAMPLE NO.

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

NB-H003803



Matrix: (soil/water) WATER Lab Sample ID: 763 33 3 ,

Sample wt/vol: , 200.0 (g/mL) ML Lab. File ID:. 763 3 33

Level: (low/med) LOW .' Date Received: 08/09/08

% Moisture: decanted: (Y/N) Date Extracted:08/18/08

Concentrated Extract Volume: 1000(uL) Date Analyzed:'08/18/08

Injection Volume: 2.0(uL) Dilution Factor:.1.0

GPC. Cleanup: •.. (Y/N) N pH:



110-86-1--- Pyridine_

106-46-7--- — 1,4 -Di chlorobenzehe_

95-48-7---- •- -2-Methylphenol_

106-44-5 —4-Methylphenol_

67-72-1 -Hexachlorbethane_

98-95-3---- -Nitrobenzene

87-68-3 —Hexachlorobutadiene

88-06-2---- —2,4,6-Trichlorophenol_

95-95-4 X-r —2,4,5-Trichlorophenol_

121-14-2--- — 2,4-Dinitrotoluene

118-74-1--- •--Hexachlorobenzene

87-86-5 • --Pentachlorophenol_

FORM I SV

FORM,1 JACEN3 SAMPLE,NO.


NB-HO 03 8,04


Lab Code: STLV Case No.: 24045 SAS,No.: SDG No.:.JNB070

Matrix: (soil/water.) WATER Lab Sample ID: 763336

Sample wt/vol: 200.0 (g'/mL) ML Lab File ID: 763336

Level: (low/med) LOW Date Received:- 08/09/08

% Moisture: X • • decanted: (Y/N)' Date Extracted:08/18/08

Concentrated Extract Volume: -1000(uL) Date Analyzed: 08/18/08

Injection'Volume: 2.0(uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pH: _ _



110-86-1- — -Pyridine . •

106-46-7- —1,4-Dichlorobenzene

95-48-7--- — 2-Methylphenol

106-44-5- - 4-MethyIphenol

67-72-1 — - -Hexachloroethane_

98-95-3--- -Nitrobenzene

87-68-3--- Hexachlorobutadiene_

88-06-2 — - —--2,4,6-Trichlorophenol_

95-95-4--- 2,4,5-Trichlorophenol_

121-14-2- 2,4-Dinitfotpluene

118-74,-1-- • Hexachlorobenzene

87-86-5--- • -. Pentachlorophenol

FORM I-SV

FORM 1 STLVT.SAMPLE NO.


MBLK0818O8C

Lab Name: TESTAMERICA BURLINGTON Contract: 24 045.

Lab Code: STLV Case No 24045 SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: MBLK08180 8C

Sample wt/vol: 200.0 (g/mL) ML Lab File ID: B0818C

Level: . (low/med) LOW v Date Received:

% Moisture: decanted: (Y/N) Date Extracted:08/18/08

Concentrated Extract Volume: 1000(uL) Date Analyzed: 08/18/08

Injection Volume: 2.0(uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N X pH



110-86-1 — — - -Pyridine

106-46-7 -1,4-Dichlorobenzene_

95-48-7 '-• -2-Methylphenol

106-44-5 -4-Methylphenol

67-72-1------ -Hexachloroethane

98-95-3 — — - -Nitrobenzene

87-68-3 -Hexachlor6butadiene_

88-06-2- -2,4,6-Trichlorophenol_

95-95-4 — — - -2,4,5-Trichlorophenol_

"121-14-2 -2,4-Diriitrotoluene

118-74-1 — — - -Hexachlorobenzene

87-86-5 ;- - Pent achlorophenol_

FORM I SV

FORM 1 STLVT SAMPLE NO.

SEMIVOLATILE ORGANICS. ANALYSIS DATA SHEET

MBLK082008C


Lab Code: STLV Case No.: 24045 SAS No.: SDG No,: JNB070

/

Matrix: (soil/water) WATER Lab Sample ID A MBLK0 82 0 08C

Sample wt/vol: 200.0 (g/mL) ML . Lab File ID: B0820C


% Moisture: • decanted: (Y/N) _'• Date Extracted:08/20/08

Goncentrated^Extract Volume: 1000(uL) Date Analyzed: 08/21/08


GPC Cleanup: (Y/N) N pH:

CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q

A A . • .• ' ' ' 110-86-1 . Pyridine r . 50 U 106^46-7 . 1,4-Dichlorobenzene 50 U . 95-48-7 — -2-Methylphenol 50 U 106-44-5 --4-Methylphenol 50 U 67-72-1 Hexachloroethane 50 U 98-95-3-- Nitrobenzene 50 U 87-68-3- -Hexachlorobutadiene 50 U 88-06-2 2,4,6-Trichlorophenol ^ 50 U 95-95-4 2,4,5-Trichlorophenol 130 U 121-14-2 2,4-Dinitrotoluene 50 U 118-74-1 :——-Hexachlorobenzene 50 U 87-86-5 Pentachlorophenol 130 U

FORM I SV



NB-H00.3801MS

Lab Name: TESTAMERICA BURLINGTON ' Contract: 24045

Lab Code: STLV '. Case No.: 24045 SAS No.: SDG No.: JNB070

Matrix: (soil/water) WATER Lab Sample ID: 763327MS

Sample wt/vol: '. 200.0 (g/mL) ML Lab File ID: 763327M


% Moisture: decanted: (Y/N)_ Date Extracted:08/20/08



GPC Cleanup- (Y/N) N . pH:


CAS NO. COMPOUND ' (ug/L or ug/Kg)' UG/L

110-86-1 Pyridine 85 106-46-7 1,4-Dichloroberizene 230 95-48-7 •• 2-Methylphenol 210 106-44-5 . 4-Methylphenol 390 67-72-1 Hexachloroethane 220 98-95-3 --Nitrobenzene 240 87-68-3 Hexachlorobutadiene 210 88 06 -2 -2, 4 ,.6 -Trichlorophenol 230 95-95-4- ---2,4,5-Trichlorophenol 240 121-14-2- — —.--2, 4-Dini.trotoluene 210 118-74-1 Hexachlorobenzene 250 87-86-5 : iPentachlorophenol 210

FORM I SV



C081808LCS


Lab Code: STLV Case No.: 24045' SAS No. : • SDG No.: JNB070

> • •

Lab Sample ID: C081808LCS

Matrix: (soil/water) WATER

Lab File ID: Q0818C

Sample wt/vol: 200.0 (g/mL)^ ML

Date Received: Level: , (low/med) LOW

Date Extracted:08/18/08 % Moisture: '•' decanted: (Y/N)

v .



GPC Cleanup: (Y/N) N pH: .

CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

' 110-86-1---- Pyridine 110 106-46 -7 — 1,4-Dichlorobenzene 180 95-48-7 2-Methylphenol ' 210 106-44-5 4-Methylphenol 380 67-72-1 — -Hexachloroethane 160 98-95-3 -Nitrobenzene 210 87-68-3 Hexachlorobutadiene 160 88-06-2- -----2,4,6-Trichlorophenol 220 95-95-4 •' 2, 4, 5-Trichlorophenol •210 121-14-2- 2,4-Dinitrotoluene 240 118-74-1---- Hexachlorobenzene '• v 200 87-86-5 — Pentachlorophenol 150

FORM I SV



C082008LCS

Lab Name: TESTAMERICA BURLINGTON Contract:-24045

Lab Code: STLV Case No.: 24045 SAS NO. : SDG No..: JNB070

Matrix: (soil/water) WATER Lab Sample ID: C082008LCS

.Sample wt/vol: 20 0.0 (g/mL) ML Lab File ID: Q0820C


% Moisture: decanted: (Y/N) _•-. Date Extracted: 08/20/08

Concentrated Extract Volume: 1000(uL) Date. Analyzed: 08/21/08

Injection Volume: -2.0(uL) Dilution Factor: 1.0

GPC Cleanup: (Y/N) N pH :•;___

CONCENTRATION UNITS::


110-86-1 Pyridine 57 106-46-7 -1,4-Dichlorobenzene . 210 95-48-7-- 2-Methylphenol 220 106-44-5 — —4-Methylphenol 400 67-72-1 --Hexachloroethane 210 98-95-3---- Nitrobenzene 240 87-68-3 —Hexachlorobutadiene 190 88-06-2 -----2,4,6-Trichlorophenol 240 95-95-4 2,4, 5-Trichlorophenol 260 121-14-2 —2,4-Dinitrotoluene 250 y 118-74-1 Hexachlorobenzene 230 87-86-5-- Pentachlorophenol 200

FORM I SV

' '• FORM 2

WATER SEMIVOLATILE SURROGATE RECOVERY



STLVT SI S2 S3. S4 S5 S6 S7 S8

SAMPLE NO. (2FP)# (PHL)# (2CP)# (DCB)# (NBZ)# (FBP)# (TBP)# (TPH)#

01 C081808LCS 64 43 89 80 88 83 103 102

02 MBLK081808C 65 44 95 83 92 87 ,. 104 107

03 NB-H003801- 78 52 112 102 110 . 102* 126 118

04 NB-H003802 ,62 42 90 , 82 86 84 100 88

05 NB-H003803 64 43 92 • 82 92 82 101 96

06 NB-H003804 63 43 90 82 91 83 102 91

07 C082008LCS 70 47 97 95 102 98*' 106 95

08 MBLK082008C 63 41 86 84 89 88 95 84r

09 NB-H003 801MS 68 44 93 94 99 97* 92 • 98.

10

11

12 i . '

13

14

15

16 ' ' ' .1

17.

18

19

20

21

22

23

24

25

26

27

28

29

30 * • :

QC LIMITS

51 (2FP) 2-Fluorophenol (3 0-95)

52 (PHL) Phenol-d5 (10- 75)

53 (2CP) 2-Chloropheno.l-d4 (55-120) (advisory)

54 (DCB) l,2-Dichlorobenzene-d4 (55-120). (advisory)

55 (NBZ) Nitrobenzene-d5 (55-125)

56 (FBP) 2-Fluorobiphenyl (30- 95)

57 (TBP) 2,4,6-Tribromophenol (50-135)

58 (TPH) Terphenyl-dl4 (55-145)

# Column to be used to flag recovery values

N * Values outside of contract required QC limits

D Surrogate diluted-out

page 1 of 1 FORM II SV

TOT

OUT

0

0

1

0

0

0

1

' 0

1

FORM 3

WATER SEMIVOLATILE MATRIX SPIKE/MATRIX SPIKE DUPLICATE RECOVERY


Lab Code: STLV Case No.: 24045' SAS No/: SDG No, JNB070

Matrix Spike - JACEN3 Sample No.: NB-H00380

QC.

LIMITS

REG.

10-105

55-125

55-13 0

35-130

50-140

60-135

35-140

55-155

60-140

60-130

55-150

50-165

COMPOUND

Pyridine >

1,4-Dichlorobenzene

2-Methylphenol

4-MethyIphenol

Hexachloroethane

Nitrobenzene -

Hexachlorobut adiene

2,4,6-Trichlorophenol

2 , 4 ,'5-Trichlorophenol

2,4-Dinitrotoluene

Hexachlorobenzene

Pentachlorophenol

SPIKE

ADDED,

(ug/L)

250

250

250

500

250

250

250

250

250

250

250

250

-' SAMPLE

CONCENTRATION

(ug/L)

' 15

18

0.0

6.9

0.0

0.0

0.0

0.0

0.0

' 0.0

' 0 . 0

0.0

MS

CONCENTRATION

(ug/L)

85

230

210

390

220

240

210

230

240

210

250

210

MS

%

REC #

28

85

84

I T 88

96

84

92

96

. 84

100

84


* Values outside of QC limits '

RPD: 0 out ofSpike Recovery:

0 outside limits 0 out of 12 outside

' limitsM

COMMENTS:

FORM III SV

i

) FORM 3

WATER SEMIVOLATILE LAB CONTROL SAMPLE


Lab Code: STLV, Case No:: 24045 . SAS No.: SDG NO.: JNB070

Matrix Spike -.STLVT Sample No.: C081808LCS

• SPIKE SAMPLE •• LCS LCS QC.

o, , ADDED CONCENTRATION CONCENTRATION o LIMITS

COMPOUND (ug/L) ' (ug/L) *• (ug/L) REC # REC.

======================== ========= ============= ============= ====== ======

Pyridine 250 110 . 44 10-105

1,4-Dichlorobenzene 250 . 180 72 55-125

2-Methylphenol 250 210 84 55-130

4-MethyIphenol 500 380 ' 76 35-130

Hexachloroethane 250 160 6-4 50-140

Nitrobenzene 250 210 84 60-135

Hexachlorobutadiene 250 160 64 35-140

2,4,6-Trichlorophenol 250 220 88 55-155

2,4,5-Trichlorophenol 250 210 84 60-140

2,4-Dinitrotoluene 250 240 96 60-130

Hexachlorobenzene 250 200 80 55-150

Pentachlorophenol 250 150 60 50-165

• . i •


* Values outside of QC 1-imits

RPD: 0 out of 0 outside limits


COMMENTS:'' .

FORM III SV

FORM 3

WATER SEMIVOLATILE LAB CONTROL SAMPLE


Lab Code: STLV Case No.: 24045 SAS No.: SDG No.

Matrix Spike - STLVT Sample No-. : C082008LCS

JNB070

LCS '

%

REC #

23

84

88

80

84

96

76

96

104

100

92

80

SPIKE

ADDED

COMPOUND .(ug/L) .

Pyridine 250

1,4-Dichlorobenzene 250

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