teknokroma capillary columns
TRANSCRIPT
7TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Fig. 1. Verification of Hydrothermal Treatment
1 - 2-Octanone 5 - 2,6-Dimethylphenol2 - C-10 6 - 2,6-Dimethylaniline3 - 1-Octanol 7 - C-124 - C-11 8 - C-13
2
1
4
5
63
7 8
Fig. 2. Deactivation Stage (Intermediate Test)
1 - 2-Octanone2 - C-103 - 1-Octanol4 - C-115 - 2,6-Dimethylphenol6 - 2,6-Dimethylaniline7 - C-128 - C-13
Teknokroma Capillary ColumnsTeknokroma has been at the forefront of chromatographic developments in Spain.From its beginnings at 1979, and in order to find the right solutions to the widearray of analytical problems that appear daily in a laboratory, Teknokroma hasalways been involved in the Spanish and European market, not only with columnsfrom the leading world manufactures, but also of those of our own manufacture.
A few years ago, Teknokroma introduced the basic line of high resolution capillarycolumns (Teknokroma columns) which were very well received in the market.Due to the on going research effort carried out by our Research Department incollaboration with the Consejo Superior de Investigaciones Científicas (CSIC) andthe Instituto Químico de Sarriá (IQS) and the support obtained from various publicadministrations (CDTI, CIDEM, MINER and FCTAC) we have been able tocontinuously update and expand our product line with other stationary phases.
All of our columns are manufactured according to a strict established protocol,and within the ISO 9001:2000 quality rules.
Stage 1:Stage 1:Stage 1:Stage 1:Stage 1: Hydrothermal treatmentStage 2:Stage 2:Stage 2:Stage 2:Stage 2: Deactivation processStage 3:Stage 3:Stage 3:Stage 3:Stage 3: Wetting, bonding and crosslinkingStage 4:Stage 4:Stage 4:Stage 4:Stage 4: Quality control
Stage 1: Hydrothermal Treatment
Teknokroma starts its manufacturing process with the selection of the best possiblefused silica tubing. This tube presents an extremely reduced tolerance of internaldiameters and has a polyimide outer coating capable of withstanding the highesttemperatures without loss of its flexible mechanical characteristics. Each one of thebatches of silica used in the process is conveniently characterized as an essentialstep to set the Hydrothermal Treatment conditions (Fig. 1) that will give rise to asurface containing a high and constant density of silanol groups, which will laterbe properly deactivated.
This treatment is indispensable, as the different capillary tubing manufacturedbatches present a very low and irregularly distributed silanol group density due tothe high temperature manufacturing process (~2000ºC).
Stage 2: Deactivation process
The deactivation process, which is different for each type of stationary phase, iscarefully controlled (fig. 2), ensuring that the tubing surface has acquired thenecessary chemical inertness and surface tension in order to be able to proceedwith the second stage of stationary phase deposition. This step also facilitates theintroduction of specific functional groups on the tubing wall which are very usefulfor the later binding of the stationary phase or to give the columns a given endpoint characteristics.
Stage 3: Wetting, bonding and crosslinking
Stationary phase selection for optimum wetting of the column is a critical point inregards to column quality. Teknokroma uses extremely pure polymers for itsphases, in order to guarantee that our columns will respond to the requirementsthat our customers expect in terms of efficiency, reproducibility, stability andminimal bleeding.
The polymers used are carefully fractionated to eliminate the low molecular weightcomponents and trace catalyst. This results in a higher thermal stability and lowerbleeding. Then, these polymers are tested by means of spectroscopic (FTIR, UV,NMR), chromatographic (GPC) techniques and by differential thermal analysis.Fig. 3 shows the molecular exclusion chromatography of the polymer TRB-5 withits corresponding thermogravimetric curve in Fig. 4.
The crosslinking and bonding of the stationary phase is achieved by avoiding theuse of peroxides which are the cause of many of the problems related to residualactivity due to phase degradation and thermal instability exhibited in numerousimported columns.
TKG 1095
Fig. 3. GPC Chromatogram of TRB-5 polymer
TKG 1097
TKG 1096
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
8 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Fig. 4 DTA curve of TRB-5 polymer
Fig. 5 Quality Control Test
Column: TBR-5TBR-5TBR-5TBR-5TBR-5, 60m x 0.25 mm ID x 0.25 µm.Carrier gas: He, 25 psi.Oven: 110°C (Isothermal).Injection: 1µl, split. (1:100:250ºC)Concentration: Approx. 5ng of each compound on columnDetector: FID, 250°C
Peak Name1 - 2-Octanone2 - C-103 - 1-Octanol4 - C-115 - 2,6-Dimethylphenol6 - 2,6-Dimethylaniline7 - C-128 - C-13
Fig. 6. GROB test
Column: TRB-5TRB-5TRB-5TRB-5TRB-5, 30m x 0.25 mm ID x 0.25 µm.Carrier gas: He, 12 psi.Injection: 1µl, split, (1:100), 260ºCDetector: FID, 280°C
Peak Name1 - 2,3-Butanediol2 - C-103 - 1-Octanol4 - 2,6-Dimethylphenol5 - C-116 - Nonanal7 - 2-Ethylhexanoic acid8 - 2,6-Dimethylaniline9 - E-1010 - Dicyclohexylamine11 - E-1112 - E-12
TKG 1099 TKG 1100
The fact that a given stationary phase is crosslinked and/or chemically bonded tothe capillary tube inner wall allows, if necessary, the recovery or regeneration ofan accidentally contaminated column by washing it with the adequate series ofsolvents.
Stage 4. Quality Control
S E L E C T P R O V E N Q U A L I T Y
When you buy a Teknokroma capillary column you receive a product designed andmanufactured in our laboratory with the aim to help you solve your analyticalproblems and which meets all of our quality criteria.At the same time you obtain from our Technical Department at Teknokroma theassurance that we will be at your side to help you with all the problems andconcerns experience in the lab.Remember that each column is individually tested and the accompanying test datais the proof that the column meets our quality specifications and thus we expect itto meet your demands. Each one of the columns obtained by this process isrigorously controlled by means of a strict Quality Control Test (fig. 5 and 6), whichensures that you will receive a guaranteed quality product.
Stationary Phase
The selection of the ideal column for a given analysis may look like a complexproblem since we need to be right on the selection of the polarity of the stationaryphase as well as column length, internal diameter and film thickness.The polarity of the stationary phase is chosen depending on the kind of compoundsyou wish to separate. Non polar phases, such as TRB-1 and TRB-5, separate com-pounds by their boiling points. Intermediate polarity phases such as TRB-WAX, TRB-1701, combine retention by boiling point with the more selective interactionthrough hydrogen bridges or dipolar moments, etc., and thus provide a higherselectivity. The principal mechanisms of polar phases such as TR-CN100(Cyanosilicone with 100% of cyano propyl groups) lie in the dipole-dipoleinteractions between the functional groups of the stationary phase and those fromthe substances to be separated. These type of phases retain polar compounds morethan non polar ones.
In general, non polar phases are more thermally stable than the polar phases. Inother words, the higher the column polarity, the lower its thermal stability. Most ofthe Teknokroma columns are cross-linked, which results in high thermal stability.The cross-linking in a stationary phase produces slight changes in thephysicochemical characteristics of the phase as well as in its polarity relative to theuncross-linked phase. Thus TEKNOKROMA also offers in its catalog columns withnon bonded phases that show the selectivity of the original phase (for instanceTR-SE30, TR-SE54, TR-20M, etc.).
Length
The efficiency of a chromatographic column (number of theoretical plates permeter) is a function of its length. The standard length used for most of theseparations is 25-30 meters. With this length one can obtain a high efficiency withrelative short times of analysis. Columns of 15m are used for rapid controlanalyses, reaction monitoring, etc. as well as for the chromatography of highmolecular weight substances while columns of 50-60 m, 100 m or 150 m areused for very complex samples. Teknokroma exclusively manufactures a 150 mcolumn for detail analyses of petroleum and essential oil hydrocarbons. As ageneral rule, we can say that in a constant temperature chromatographic analysis,the number of theoretical plates and analysis time are directly proportional to thecolumn length while resolution is directly proportional to the square root of thetheoretical plates. Thus, we need to take into account that when we double columnlength, its resolution only increases by 40% whereas analysis time doubles.
Teknokroma Capillary Columns
TKG 1098
9
TKG 1101
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Internal Diameter
The column internal diameter is inversely proportional to its separation power. Thesmaller the diameter, the larger the efficiency and thus a higher resolution but atthe same time the loading capacity decreases.For samples containing a large number of substances where you may need a givenresolution, it is recommended to use small internal diameter columns (0.20-0.25mm) and for samples with a high range of concentrations higher internal diametercolumns are recommended (0.32-0.53 mm) since these larger diameters allow forthe injection of a higher sample amount.
Columns of 0.53 mm ID (semicapillary) have a loading capacity similar to that ofpacked columns, which they replace in many analyzes, with better resolution,higher chemical inertness and lower analysis time.The 0.32-0-53 mm ID columns can be used with either the injector for capillarycolumns or with the packed column injector, due to the high flow-rates at whichthey can operate.
In the increasingly used GC-MS systems it is recommended to work with small IDcolumns (0.10mm, 0.15mm, 0.18mm, 0.20 mm and 0.22 mm) so as not toexceed the capacity of the vacuum system. Recently, capillary columns of 0.1 mmID have appeared on the market. These generate high plate numbers or, in otherwords, to reduce analysis time without losing resolution. The high efficiency ofthese columns (7000-10000 plates/meter) allows the resolution of complexsamples using shorter column lengths, thus with very short analysis times, with theresulting cost reduction for the laboratory. Evidently, their loading capacity is alimiting factor and in order to obtain the best performance from these columns weneed to take into account instrumental factors (injector-detector).
Film Thickness
The film thickness of the stationary phase deposited inside the capillary columnexerts an influence on the number of effective theoretical plates that can beobtained with the column for a given separation, on its loading capacity, on thebleed level and on the elution temperature of a compound.A film thickness of 0.25-0.32 mm is the standard thickness allowing for acompromise between loading capacity and resolution; and for the injection ofsamples with a wide volatility range.
Thick films increase retention of the most volatile components whereas thin filmsprovide faster elution at lower temperatures.As a general rule, thin films (0.1 mm) must be used for compounds with a highmolecular weight such as triglycerides, antioxidants, etc., which have elutiontemperatures over 300°C. Thick films must be used for low boiling substancesbecause thick films increase the interaction between the substances and thestationary phase. Specifically, 3-5 µm films are used to separate solvents, gases,and very volatile substances at room temperature or lower.
When the thickness of the stationary phase increases, thermal stability decreases,and thus the bleed level is higher which will limit the maximum operatingtemperature of the column.
The β factor defines the relation between the column internal diameter and thestationary phase thickness, thereby helping you to select the most appropriatecolumn for your analysis.
In addition, the β factor allows for the easy exchange of columns since, for a givenanalysis with the same stationary phase, similar β factors will result in the sameor very similar retention times and capacity factors. Of course, this implies takinginto account the column loading capacity (phase thickness and internal diameter).
Factor ββββββββββ Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:Column suitable for the separation of:
>400 High molecular weight compounds100 - 400 All purpose use<100 Volatile compounds of low molecular weight
Bleed Level
The bleed level of stationary phase from a capillary column is the parameter whichwill determine the level of sensitivity in a given assay. It is directly related to theamount of stationary phase in the column and thus with the film thickness. It alsoincreases exponentially with temperature (fig.7).
A low bleed level will allow you to work without problems with the whole range ofmodern high sensitivity detectors and at the same time will result in lesscontamination. This will also allow the quantification of high boiling point or highmolecular weight compounds which are analyzed by means of high temperaturegradients.
Teknokroma Capillary Columns
Fig. 7. Bleed level (GROB test)
Column: TRB-5TRB-5TRB-5TRB-5TRB-5,15m x 0.25mm ID x 0.25µm.Carrier gas: He, 6 psi.Injection: 1µl, split. (1:100), 280ºCDetector: FID, 350°C
Bleed level (FID) <4pA (325°C)
325ºC
1 0
Stationary Phase Cross Reference (Table 1)
Maximum Efficiency
All manufacturing stages for capillary columns have been optimized in order to beable to offer our customers columns of very high efficiency.
Maximum Reproducibility
When you select a Teknokroma column for your analyses you can be assured thateach of the steps in the production process has been thoroughly controlled toensure that there are no deviations from the established quality parameters. All ofthe steps incorporate the maximum possible automation procedures.This translates into a high reproducibility level with regards to the chromatographicperformance of our columns.
Teknokroma Capillary Columns
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
AMORKONKET AMORKONKET AMORKONKET AMORKONKET AMORKONKET
,RUFLUSBRT,SM1-BRT,th1-BRT,1-BRT,051LORTEP-BRT,LORTEP-BRT
03-ES,7882-BRT,ANOP2.05.BRT
NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP NOITISOPMOCESAHP
enaxolisyloplyhtemid%001
TNELIGA TNELIGA TNELIGA TNELIGA TNELIGA
1-ARTLU,101PH,1-PH7882-BD,th1-BD,1-BD
OCLEPUS OCLEPUS OCLEPUS OCLEPUS OCLEPUS
1-YTIUQE,1-BPSRUFLUS1-BPS
KETSER KETSER KETSER KETSER KETSER
7882-xtR,1-xtR
NAIRAV NAIRAV NAIRAV NAIRAV NAIRAV
BC5LIS-PCSMBC5LIS-PC
EGS EGS EGS EGS EGS
1-PB
HCETLLA HCETLLA HCETLLA HCETLLA HCETLLA
1-TA
XERDAUQ XERDAUQ XERDAUQ XERDAUQ XERDAUQ
1-700
ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU ERUTUCNEMONPSU
83G,2G,1G
,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT ,SM5-BRT,th5-BRT,5-BRT,ENIMA5-BRT,LORETS-BRT45-ES,72G-BRT,526.5-BRT
lynehpid%5-lyhtemid%59enaxolisylop
5-BD,2-ARTLU,5-PH5-SAP,th5-BD,526.5-BD
5-YTIUQE.5-BPS,5-CAS.5-ETP
MTQ5-ETP
,5-ITX,5-xtRSM5-xtR
BC8LIS-PC 5-PB 5-TA 2-700 63G,72G
5X.ateM 5X.ateM 5X.ateM 5X.ateM 5X.ateM lynehpid%5-lyhtemid%59enelynehplisylop
SM5-BD.AT5-PH 5-NDM SMliS5-xtR BC8LIS-PCSM/deelBwoL
5-XPB sm5-TA SM5-700
34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT 34G-BRT,426-BRT,1031-BRT %49-lynehplyporponayc%6enaxolisyloplyhtemid
426-PH,1031-PH426-BD,1031-BD
1031-BPS34G-IVO
,1031-xtR426-xtR
426-XPB 426-TA 34G
41-BRT 41-BRT 41-BRT 41-BRT 41-BRT lyhtemid%68-lynehpid%41enaxolisylop
BC31LIS-PC
02-BRT 02-BRT 02-BRT 02-BRT 02-BRT lyhtemid%08-lynehpid%02enaxolisylop
LOCOV.02-BPS 02-TA 7-700 23G.82G
53-BRT 53-BRT 53-BRT 53-BRT 53-BRT lyhtemid%56-lynehpid%53enaxolisylop
53-BD.53-PH 53-BPS 53-xtR ,53-XPB806-XPB
53-TA 11-700 24G
1071-BRT 1071-BRT 1071-BRT 1071-BRT 1071-BRT %68-lynehplyporponayc%41enaxolisyloplyhtemid
1071-SAP.1071-PH1071-BD
1071-BPS 1071-xtR BC91LIS-PC 01-PB 1071-TA 1071-700
522-BRT 522-BRT 522-BRT 522-BRT 522-BRT %05-lynehplyporponayc%05enaxolisyloplyhtemid
522-BD.522-PH 522-xtR BC34LIS-PC 522-PB 522-TA 522-700 91G.7G
GAP-BRT GAP-BRT GAP-BRT GAP-BRT GAP-BRT %05-enelyhteylop%05locylqenelyporpylop
GAP
PAFF-BRT PAFF-BRT PAFF-BRT PAFF-BRT PAFF-BRT roflocylgenelyhteylopdetaertsdnuopmoccidica
PAFF-BD.PAFF-PH 0001-PS.LOKUN BD-XAWLIBATS BC85XAW-PC 12-PB ,0001-TAPAFF
PAFF-700 53G.52G
05-BRT 05-BRT 05-BRT 05-BRT 05-BRT lyhtemid%05-lynehpid%05enaxolisylop
,71-BD,+05-PH806-BD
.05-BPS0522-BPS
05-xtR BC42LIS-PC 05-TA 71-700 3G
th05-BRT th05-BRT th05-BRT th05-BRT th05-BRT lyhtemid%05-lynehpid%05enaxolisylop
th71BD 56-xtR BC-BAT TH56-700 71G
05F-BRT 05F-BRT 05F-BRT 05F-BRT 05F-BRT lyporporoulfirt%05enaxolisyloplyhtem%05
002-BD.012-BD 002-xtR 012-TA 012-700 6G
XAW-BRT XAW-BRT XAW-BRT XAW-BRT XAW-BRT locylgenelyhteylop%001 ,XAW-BDXAWONNI.M02-PHrteXAW-BD
01XAWOCLEPUSM02xawobraC
XAWLIBATS BC25XAW-PC 02-PB XAW-TA WC-700 ,61G,51G,41G93G.02G
BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT BD-XAW-BRT roflocylgenelyhteylopdetaertsdnuopmoccisab
xaWcisaB-PH,MAC enimA-xawobraC BC15XAW-PC
xaW.ateM xaW.ateM xaW.ateM xaW.ateM xaW.ateM locylgenelyhteylop%001 XAW-BD,XAW-PH BC75XAW-PC
agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT agemO-XAW-BRT locylgenelyhteylop%001 XAWAGEMO XAWEMAF
001NC-RT 001NC-RT 001NC-RT 001NC-RT 001NC-RT lyporponaycsib%001enaxolisylop
0432-PS 0432-tR 88LIS-PC
LOSERC-RT LOSERC-RT LOSERC-RT LOSERC-RT LOSERC-RT esahpdednobnonyrateirporp LOSERC-PC
71-BRT 71-BRT 71-BRT 71-BRT 71-BRT lyhtemid%05-lynehpid%05enaxolisylop
71-PH 3G
COV.ateM COV.ateM COV.ateM COV.ateM COV.ateM esahpdednobyrateirporp COV-PH,2.205-BD LOCOV 2.205-xtR
806-BRT 806-BRT 806-BRT 806-BRT 806-BRT esahpdednobyrateirporp 806-PH 806-BPS 806-PB
PECT-RT PECT-RT PECT-RT PECT-RT PECT-RT enaporp)yxohteonayc(sirt-3,2,1 PECT PECT-tR PECT-PC
InterInterInterInterInternal diameter (mm)nal diameter (mm)nal diameter (mm)nal diameter (mm)nal diameter (mm) Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)Theoretical Plates (N/m)0,10 7.000 - 9.0000,20 4.700 - 5.5000,25 3.300 - 4.6000,32 2.700 - 3.7000,53 1.400 - 2.200
Wide Stationary Phase Selection
Teknokroma incorporates in its catalogue a selection of capillary columns preparedwith the stationary phases most commonly used in the field of gas chromatography(Table 1).
11
TRB-1
Column: TRB-1TRB-1TRB-1TRB-1TRB-1, P/N TR-111226Dimensions: 25m x 0.15mm x 1.2µmInjection: 1µL Test SP-4-7300, split 1:100, 280ºCCarrier gas: H2, constant pressure 22 psi (151.6 KPa).Oven program: 145ºC (isothermal)Detector: FID, 300ºC
Peak Name
1 Methylene chloride2 2-Octanone3 C-104 1-Octanol5 2,6-Dimethylphenol6 C-117 2,6-Dimethylaniline8 C-12
TKG 1102
TRB-1
100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase100% Dimethyl polysi loxane, bonded and crossl inked phase
• 100% Dimethylpolysiloxane.• Non-polar phase• Column for general use• High thermal stability• Ideal column for the analysis of petrochemical products and industrial solvents
Structure of Poly(dimethyl)siloxane
Si OOCH3
CH3
m
TRB-1
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent PhaseTRB-1 Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-1,HP101,ULTRA-1, DB-1Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SPB-1, EQUITY-1Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1, Rtx -2887VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 5 CBS G ES G ES G ES G ES G E: BP-1.A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1Macherey-Nagel:Macherey-Nagel:Macherey-Nagel:Macherey-Nagel:Macherey-Nagel: OPTIMA-1
TRB-1
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,100,100,100,100,10 10 0,10 -60 to 325/350 TR-110141TR-110141TR-110141TR-110141TR-11014110 0,40 -60 to 320/340 TR-110441TR-110441TR-110441TR-110441TR-110441
20 0,10 -60 to 325/350 TR-110181TR-110181TR-110181TR-110181TR-110181
20 0,40 -60 to 320/340 TR-110481TR-110481TR-110481TR-110481TR-110481
0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-113B89TR-113B89TR-113B89TR-113B89TR-113B89
15 0,15 -60 to 325/350 TR-111319TR-111319TR-111319TR-111319TR-111319
15 0,35 -60 to 325/350 TR-110319TR-110319TR-110319TR-110319TR-11031915 0,50 -60 to 325/350 TR-110519TR-110519TR-110519TR-110519TR-110519
25 0,15 -60 to 325/350 TR-111329TR-111329TR-111329TR-111329TR-11132925 0,33 -60 to 325/350 TR-113329TR-113329TR-113329TR-113329TR-113329
25 0,35 -60 to 325/350 TR-110329TR-110329TR-110329TR-110329TR-110329
25 0,50 -60 to 325/350 TR-110529TR-110529TR-110529TR-110529TR-11052930 0,15 -60 to 325/350 TR-111339TR-111339TR-111339TR-111339TR-111339
30 0,35 -60 to 325/350 TR-110339TR-110339TR-110339TR-110339TR-110339
30 0,50 -60 to 325/350 TR-110539TR-110539TR-110539TR-110539TR-11053950 0,15 -60 to 325/350 TR-111359TR-111359TR-111359TR-111359TR-111359
50 0,33 -60 to 325/350 TR-113359TR-113359TR-113359TR-113359TR-113359
50 0,35 -60 to 325/350 TR-110359TR-110359TR-110359TR-110359TR-11035950 0,50 -60 to 325/350 TR-110559TR-110559TR-110559TR-110559TR-110559
60 0,15 -60 to 325/350 TR-111369TR-111369TR-111369TR-111369TR-111369
60 0,50 -60 to 325/350 TR-110569TR-110569TR-110569TR-110569TR-110569
0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-110112TR-110112TR-110112TR-110112TR-110112
15 0,25 -60 to 325/350 TR-110212TR-110212TR-110212TR-110212TR-110212
15 0,50 -60 to 325/350 TR-110512TR-110512TR-110512TR-110512TR-11051215 1,00 -60 to 325/340 TR-111012TR-111012TR-111012TR-111012TR-111012
25 0,10 -60 to 325/350 TR-110122TR-110122TR-110122TR-110122TR-110122
25 0,25 -60 to 325/350 TR-110222TR-110222TR-110222TR-110222TR-11022225 0,50 -60 to 325/350 TR-110522TR-110522TR-110522TR-110522TR-110522
25 1,00 -60 to 320/340 TR-111022TR-111022TR-111022TR-111022TR-11102230 0,10 -60 to 325/350 TR-110132TR-110132TR-110132TR-110132TR-110132
30 0,25 -60 to 325/350 TR-110232TR-110232TR-110232TR-110232TR-110232
30 0,50 -60 to 325/350 TR-110532TR-110532TR-110532TR-110532TR-11053230 1,00 -60 to 320/340 TR-111032TR-111032TR-111032TR-111032TR-111032
50 0,10 -60 to 325/350 TR-110152TR-110152TR-110152TR-110152TR-110152
50 0,25 -60 to 325/350 TR-110252TR-110252TR-110252TR-110252TR-11025250 0,50 -60 to 325/350 TR-110552TR-110552TR-110552TR-110552TR-110552
50 1,00 -60 to 320/340 TR-111052TR-111052TR-111052TR-111052TR-111052
60 0,10 -60 to 325/350 TR-110162TR-110162TR-110162TR-110162TR-11016260 0,25 -60 to 325/350 TR-110262TR-110262TR-110262TR-110262TR-110262
60 0,50 -60 to 325/350 TR-110562TR-110562TR-110562TR-110562TR-110562
60 1,00 -60 to 325/350 TR-111062TR-111062TR-111062TR-111062TR-111062
100 1,00 -60 to 325/350 TR-111092TR-111092TR-111092TR-111092TR-111092105 1,00 -60 to 325/350 TR-1110K2TR-1110K2TR-1110K2TR-1110K2TR-1110K2
0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-110113TR-110113TR-110113TR-110113TR-110113
15 0,25 -60 to 325/350 TR-110213TR-110213TR-110213TR-110213TR-11021315 0,50 -60 to 325/350 TR-110513TR-110513TR-110513TR-110513TR-110513
15 1,00 -60 to 325/350 TR-111013TR-111013TR-111013TR-111013TR-111013
15 3,00 -60 to 280/300 TR-113013TR-113013TR-113013TR-113013TR-11301325 0,10 -60 to 325/350 TR-110123TR-110123TR-110123TR-110123TR-110123
25 0,25 -60 to 325/350 TR-110223TR-110223TR-110223TR-110223TR-110223
25 0,50 -60 to 325/350 TR-110523TR-110523TR-110523TR-110523TR-110523
1 2
Structure of Poly(dimethyl)siloxane
Si OOCH3
CH3
m
TRB-1ht
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,10 -60 a 395 TR-610112
30 0,10 -60 a 395 TR-610132
0,320,320,320,320,32 15 0,10 -60 a 390 TR-610113
30 0,10 -60 a 390 TR-610133
TRB-1ht
Column: Retention Gap (intermediate polarity) 5m x 0.53mm(TR-200055) + TRB-1htTRB-1htTRB-1htTRB-1htTRB-1ht ( TR-610113)Dimensions: 15m x 0.32mm x 0.10µmInjection: 0.3µL Poliwax 655 (0.1% in CS2), on column (sec. cool 30 s), 280ºCCarrier gas: H2, constant flow 2mL/minOven temperature: 50ºC(2 min) @ 15ºC/min to 380ºC(5 min)Detector: FID, 390ºC
380ºC380ºC380ºC380ºC380ºC<10 pA<10 pA<10 pA<10 pA<10 pA
TKG 1103
TRB-1htTRB-1ht
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane• Non-polar phase• Produced specially for high temperature analyses (Max.temp. 400ºC).• Fused silica tubing with polyimide coating for high temperatures.• Uses: analysis of compounds with high boiling point, triglycerides, waxes, etc.
TRB-1
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent PhaseTRB-1ht Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-1htR e s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Stx-1HTA l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1 ht
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
25 1,00 -60 to 325/350 TR-111023TR-111023TR-111023TR-111023TR-111023
25 3,00 -60 to 280/300 TR-113023TR-113023TR-113023TR-113023TR-11302330 0,10 -60 to 325/350 TR-110133TR-110133TR-110133TR-110133TR-110133
30 0,25 -60 to 325/350 TR-110233TR-110233TR-110233TR-110233TR-110233
30 0,50 -60 to 325/350 TR-110533TR-110533TR-110533TR-110533TR-11053330 1,00 -60 to 325/350 TR-111033TR-111033TR-111033TR-111033TR-111033
30 3,00 -60 to 280/300 TR-113033TR-113033TR-113033TR-113033TR-113033
50 0,10 -60 to 325/350 TR-110153TR-110153TR-110153TR-110153TR-11015350 0,25 -60 to 325/350 TR-110253TR-110253TR-110253TR-110253TR-110253
50 0,50 -60 to 325/350 TR-110553TR-110553TR-110553TR-110553TR-110553
50 1,00 -60 to 325/350 TR-111053TR-111053TR-111053TR-111053TR-11105350 3,00 -60 to 280/300 TR-113053TR-113053TR-113053TR-113053TR-113053
60 0,10 -60 to 325/350 TR-110163TR-110163TR-110163TR-110163TR-110163
60 0,25 -60 to 325/350 TR-110263TR-110263TR-110263TR-110263TR-11026360 0,50 -60 to 325/350 TR-110563TR-110563TR-110563TR-110563TR-110563
60 1,00 -60 to 325/350 TR-111063TR-111063TR-111063TR-111063TR-111063
60 3,00 -60 to 280/300 TR-113063TR-113063TR-113063TR-113063TR-11306360 5,00 -60 to 260/280 TR-115063TR-115063TR-115063TR-115063TR-115063
0,530,530,530,530,53 10 2,65 -60 to 300/310 TR-112645TR-112645TR-112645TR-112645TR-11264515 0,10 -60 to 320/340 TR-110115TR-110115TR-110115TR-110115TR-110115
15 0,50 -60 to 320/340 TR-110515TR-110515TR-110515TR-110515TR-110515
15 1,50 -60 to 310/330 TR-111515TR-111515TR-111515TR-111515TR-11151515 3,00 -60 to 270/290 TR-113015TR-113015TR-113015TR-113015TR-113015
15 5,00 -60 to 270/290 TR-115015TR-115015TR-115015TR-115015TR-115015
15 7,00 -60 to 260/280 TR-117015TR-117015TR-117015TR-117015TR-11701525 0,10 -60 to 320/340 TR-110125TR-110125TR-110125TR-110125TR-110125
25 0,50 -60 to 320/340 TR-110525TR-110525TR-110525TR-110525TR-110525
25 1,50 -60 to 310/330 TR-111525TR-111525TR-111525TR-111525TR-11152525 3,00 -60 to 270/290 TR-113025TR-113025TR-113025TR-113025TR-113025
25 5,00 -60 to 270/290 TR-115025TR-115025TR-115025TR-115025TR-115025
30 0,10 -60 to 320/340 TR-110135TR-110135TR-110135TR-110135TR-11013530 0,50 -60 to 320/340 TR-110535TR-110535TR-110535TR-110535TR-110535
30 0,88 -60 to 310/330 TR-110835TR-110835TR-110835TR-110835TR-110835
30 1,50 -60 to 310/330 TR-111535TR-111535TR-111535TR-111535TR-11153530 2,65 -60 to 270/290 TR-112635TR-112635TR-112635TR-112635TR-112635
30 3,00 -60 to 270/290 TR-113035TR-113035TR-113035TR-113035TR-113035
30 5,00 -60 to 270/290 TR-115035TR-115035TR-115035TR-115035TR-11503530 7,00 -60 to 260/280 TR-117035TR-117035TR-117035TR-117035TR-117035
50 0,10 -60 to 320/340 TR-110155TR-110155TR-110155TR-110155TR-11015550 0,50 -60 to 320/340 TR-110555TR-110555TR-110555TR-110555TR-110555
50 1,50 -60 to 310/330 TR-111555TR-111555TR-111555TR-111555TR-111555
50 3,00 -60 to 270/290 TR-113055TR-113055TR-113055TR-113055TR-11305550 5,00 -60 to 270/290 TR-115055TR-115055TR-115055TR-115055TR-115055
60 0,10 -60 to 320/340 TR-110165TR-110165TR-110165TR-110165TR-110165
60 0,50 -60 to 320/340 TR-110565TR-110565TR-110565TR-110565TR-11056560 1,50 -60 to 310/330 TR-111565TR-111565TR-111565TR-111565TR-111565
60 3,00 -60 to 270/290 TR-113065TR-113065TR-113065TR-113065TR-113065
60 5,00 -60 to 270/290 TR-115065TR-115065TR-115065TR-115065TR-11506560 7,00 -60 to 240/260 TR-117065TR-117065TR-117065TR-117065TR-117065
100 3,00 -60 to 270/290 TR-113095TR-113095TR-113095TR-113095TR-113095
105 3,00 -60 to 270/290 TR-1130K5TR-1130K5TR-1130K5TR-1130K5TR-1130K5
13
Structure of Poly(dimethyl)siloxane Si OOCH3
CH3
m
TRB-1ms
Column: TRB-1msTRB-1msTRB-1msTRB-1msTRB-1ms, P/N TR-510262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1µL Test MX5 (10 to 20 ng/comp. on column), split 1:100, 280ºCCarrier gas: H2, constant pressure 25 psi (172 KPa).Oven temperature: 100ºC @ 6ºC/min to 325ºC(5 min)Detector: FID, 340ºC
Peak Name
1 Methylene chloride2 1,2-Hexanediol3 Nitroso-di-n-propylamine4 Benzoic acid5 C-146 2,4-Dinitrophenol7 4-Nitrophenol8 4-Nitroaniline9 Pentachlorophenol10 Carbazole11 C-2012 C-2113 C-2214 Benzo(b)fluoranthene15 Benzo(k)fluoranthene
TKG 1104
TRB-1msTRB-1ms
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane.
• These columns, with a selectivity identical to the TRB-1, fulfil column bleedspecifications that make them compatible with analysis of trace componentswith GC/MS. Therefore, the standard column of 30 m x 0.25 mm x 0.25 µmhas a guaranteed maximum bleed of 4 pA at 325 °C.
• Great chemical inertness towards active constituents and excellent thermalstability.
• Improved signal/noise ratio, which enables greater sensitivity to be obtainedwith the MS, ECD, NPD, SCD, etc. detectors and provides greater precision inquantitative analysis at trace levels.
• Less column bleed means less detectors contamination and greater speed inconditioning columns.
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent PhaseTRB-1ms Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-1MS, DB-1MSRe s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1msVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 5 CB MSA l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1 MS
TRB-1ms
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-5133B9TR-5133B9TR-5133B9TR-5133B9TR-5133B915 0,33 -60 to 325/350 TR-513319TR-513319TR-513319TR-513319TR-513319
25 0,33 -60 to 325/350 TR-513329TR-513329TR-513329TR-513329TR-513329
30 0,33 -60 to 325/350 TR-513339TR-513339TR-513339TR-513339TR-51333950 0,33 -60 to 325/350 TR-513359TR-513359TR-513359TR-513359TR-513359
60 0,33 -60 to 325/350 TR-513369TR-513369TR-513369TR-513369TR-513369
0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-510112TR-510112TR-510112TR-510112TR-51011215 0,25 -60 to 325/350 TR-510212TR-510212TR-510212TR-510212TR-510212
15 1,00 -60 to 325/350 TR-511012TR-511012TR-511012TR-511012TR-51101230 0,10 -60 to 325/350 TR-510132TR-510132TR-510132TR-510132TR-510132
30 0,25 -60 to 325/350 TR-510232TR-510232TR-510232TR-510232TR-510232
30 1,00 -60 to 325/350 TR-511032TR-511032TR-511032TR-511032TR-51103260 0,10 -60 to 325/350 TR-510162TR-510162TR-510162TR-510162TR-510162
60 0,25 -60 to 325/350 TR-510262TR-510262TR-510262TR-510262TR-510262
60 1,00 -60 to 325/350 TR-511062TR-511062TR-511062TR-511062TR-511062
1 4
Structure of Poly(dimethyl)siloxane
Si OOCH3
CH3
m
TRB-Petrol
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane.
• Column for analyzing complex mixtures of hydrocarbons according to theASTM regulations (American Society for Testing and Materials).
• Sufficient resolution power to undertake PNA, PONA and PIANO analysis.
TRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent PhaseTRB-Pet ro l Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-PetroSupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: Petrocol DH
TRB-PetrolInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 100 0,50 -60 to 300/320 TR-110592TR-110592TR-110592TR-110592TR-110592
TRB- SULFUR
Column: TRB-SULFURTRB-SULFURTRB-SULFURTRB-SULFURTRB-SULFUR, 30 m x 0.32 mm x 4.0 µmMercaptans
Peak Names
1- SH22- Methyl mercaptan3- Ethyl mercaptan4- 2-propylmercaptan5- Terbutyl mercaptan6- Methyl ethyl sulfide7- 1-propylmercaptan8- 2-butyl mercaptan9- T.H.T.
Structure of Poly(dimethyl)siloxane
Si OOCH3
CH3
m
TKG 1105
TRB-Sulfur
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane.
• Column specially designed for the analysis of sulphurous compounds(in natural gas, petrol derivates, wines, beer, etc.)
• Guaranteed thermal stability, with low column bleed.
TRB-Petrol
TRB-Sulfur
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent PhaseTRB-Su l fu r Equ iva lent Phase
Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SPB-1 SULFUR
TRB-SulfurInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 30 4,00 -60 to 270/290 TR-114033TR-114033TR-114033TR-114033TR-114033
15
TRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent PhaseTRB-Pet ro .150 Equ iva lent Phase
Supelco: Supelco: Supelco: Supelco: Supelco: Petrocol DH 150.
TRB-Petro.150InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 150 1,00 -60 to 300/320 TR-1110G2TR-1110G2TR-1110G2TR-1110G2TR-1110G2
Si OOCH3
CH3
m
Structure of Poly(dimethyl)siloxane
TRB-PETROL
Column: TRB-PETROLTRB-PETROLTRB-PETROLTRB-PETROLTRB-PETROL, 100m x 0.25mm x 0.50µm TR 110592Temperature: 60ºC (isothermal)Injector: 260ºCCarrier gas: H2, 34 psiInjection: Test for hydrocarbons, split (1:100)Detector: FID, 260º
tr (min.) Compound
6.39 n-Hexane7.70 Benzene8.03 Cyclohexane9.37 n-Heptane12.47 Toluene16.02 n-Octane22.93 m-Xylene23.08 p-Xylene30.83 n-Nonane
TKG 1106
TRB-Petrol
TRB-Petro. 150TRB-Petro.150
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane.
• Maximum resolution for hydrocarbon analysis
• Detailed hydrocarbon analysis.
• Volatiles in essential oil and beverages
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
1 6 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-Petro.150
TRB-PETRO.15O
Column: TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150TRB-PETRO.150, P/N TR-I110G2Dimensions: 150m x 0.25mm x 1.0µmInjection: 0.1µ1 unleaded gasoline,split 100:1 @ 280°CCarrier gas: He, 75psi (517 kPa) @ 35°COven program: 35°C(hold 135 min.) to 200°C @ 2°C/min. (hold 20 min)Detector: FID @ 280°C
1. n-Butane2. Isopentane3. n-Pentane4. 2,2-Dimethylbutane5. Cyclopentane6. 2,3-Dimethylbutane7. 2-Methylpentane8. 3-Methylpentane9. n-Hexane10. 2,4-Dimethylpentane
11. Benzene12. 2-Methylhexane13. 2,3-Dimethylpentane14.3-Methylhexane15. 2,2,4- Trimethylpentane16. n-Heptane17.2,5-Dimethylhexane18. 2,4-Dimethylhexane19.2,3,4-Trimethylpentane20. Toluene
21. 2,3,3- Trimethylpentane22. 2,3-Dimethylhexane23. 2-Methylheptane24. 3-Methylheptane25.2-Methyl-1-heptene26. n-Octane27. Ethylbencene28. m-Xylene29. p-Xylene30. o-Xylene
17
TKG 1107
31. 1-Nonene32. n-Nonane33. Isopropylbenzene34. 3,3,5- Trimethylheptane35. 2,4,5- Trimethylheptane36. n-propylbenzene37.1-Methyl-3-ethylbenzene38. 1-Methyl-4-ethylbenzene39.1,3,5-Trimethylbenzene40. 3,3,4- Trimethylheptane
41. 1-Methyl-2-ethylbenzene42. 1,2,4- Trimethylbenzene43. Isobuthylbenzene44. sec-Buthylbenzene45. n-Decane .46. 1,2,3- Trimethylbenzene47.lndane48. 1,3-Diethylbenzene49. n-Butylbenzene50.1,4-Dimethyl-2-ethylbenzene
51. 1,3- Dimethyl-4-ethylbenzene52. 1,2-Dimethyl-4-ethylbenzene53. 1,2,4,5- Tetramethylbenzene54.1,2,3,5-Tetramethylbenzene55. Naphthalene56.2-Methylnaphthalene57.1-Methylnaphthalene58. Dimethylnaphthalenes
TRB-Petro.150
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
1 8
TRB-50.2PONA
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane.
• Column designed for the complete analysis of PONA hydrocarbons (P-Paraffins, O-Olefins, N-Naphthenes and A-Aromatics) in petrol-derived productsaccording to the ASTM regulations, method D5134.
Structure of Poly(dimethyl)siloxane Si OOCH3
CH3
m
TRB-50.2PONAInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 50 0,50 -60 to 320/340 TR-110559TR-110559TR-110559TR-110559TR-110559
Si OOCH3
CH3
m
TRB-2887InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,530,530,530,530,53 10 2,65 -60 to 340/360 TR-192645TR-192645TR-192645TR-192645TR-192645
Structure of Poly(dimethyl)siloxane
TRB-2887
Column: TRB-2887TRB-2887TRB-2887TRB-2887TRB-2887, P/N TR-192645Dimensions: 10m x 0.53mm x 2.65µmInjection: 1µL standard RS-31222, split 1:10, 300ºCCarrier gas: H2, constant pressure 5 psi (34.4 KPa)Oven temperature: 40ºC @ 15ºC/min to 350ºC(5 min)Detector: FID, 360ºC. Baseline not compensed
Peak Name
1 n-hexane (C-6)2 n-heptane (C-7)3 n-octane (C-8)4 n-nonane (C-9)5 n-decane (C-10)6 n-undecane (C-11)7 n-dodecane (C-12)8 n-tetradecane (C-14)9 n-hexadecane (C-16)10 n-octadecane (C-18)11 n-eicosane (C-20)12 n-tetracosane (C-24)13 n-octacosane (C-28)14 n-dotriacontane( C-32)15 n-hexatriacotane (C-36)16 n-tetracontane (C-40)17 n-tetratetracontane (C-44)TKG 1108
TRB-2887
100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.100% Dimethyl polysi loxane, bonded and crossl inked phase.
• 100% Dimethylpolysiloxane
• Designed specifically for simulated distillation according to the ASTM methodD2887.
TRB-50.2PONA
TRB-2887
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent PhaseTRB-50.2PONA. Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-PONASupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: Petrocol DH 50.2Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-1 PONAVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL PONA CBS G ES G ES G ES G ES G E: BP-1 PONA
TRB-2887 Equ iva lent PhaseTRB-2887 Equ iva lent PhaseTRB-2887 Equ iva lent PhaseTRB-2887 Equ iva lent PhaseTRB-2887 Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: DB-2887Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: PETROCOL-2887Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: Rtx-2887
19
TRB-5
(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• It is the most versatile and universal stationary phase in the gaschromatography analysis field.
• The low percentage of phenyl in the polymer structure gives it a characteristicaffinity towards the compounds with aromatic rings. This phase, the mostpopular one, due to its great thermal stability and chemical inertness is thestationary phase of choice for any type of analysis.
• It allows the analysis of acidic and basic compounds.
• It is ideal for the analysis in the environmental field. Analysis of dioxines,PCB´s, PCT´s, polyaromatic compounds, phenols, herbicides, organochlorinatedand organophosphorus pesticides, aromatic hydrocarbons, solvents, drugs,oils, etc...
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB-5
Column: TRB-5TRB-5TRB-5TRB-5TRB-5, P/N TR-120232Dimensions: 30m x 0.25mm x 0.25µmInjection: 1µL chlorinated pesticides mixture, splitless @230ºC (25-270 ppb on column)Carrier gas: H2, constant pressure 12 psi (87.7 KPa) 150ºCOven temperature: 150ºC to 225ºC@ 2ºC/min (10 min.)Detector: ECD, 310ºC
Peak Name
1. 2,4,5,6-tetrachloro-m-xylene2. γ-BHC3. δ-BHC4. heptachlor5. aldrin6. β-BHC7. δ-BHC
8. heptachlor epoxide9. endosulfan I10. γ-chlordane11.α-chlordane12. 4,4´- DDE13. dieldrin14. endrin15. 4,4´- DDD
16. endosulfan II17. 4,4´- DDT18. endrin aldehyde19. endosulfan sulfate20. methoxychlor21. endrin ketone22. decachlorobiphenyl
TKG 1109
TRB-5
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
2 0 TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-5InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,100,100,100,100,10 10 0,10 -60 to 325/350 TR-120141TR-120141TR-120141TR-120141TR-120141
10 0,40 -60 to 320/350 TR-120441TR-120441TR-120441TR-120441TR-12044120 0,10 -60 to 325/350 TR-120181TR-120181TR-120181TR-120181TR-120181
20 0,40 -60 to 320/350 TR-120481TR-120481TR-120481TR-120481TR-120481
0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-1233B9TR-1233B9TR-1233B9TR-1233B9TR-1233B915 0,15 -60 to 325/350 TR-121319TR-121319TR-121319TR-121319TR-121319
15 0,35 -60 to 325/350 TR-120319TR-120319TR-120319TR-120319TR-120319
15 0,50 -60 to 325/350 TR-120519TR-120519TR-120519TR-120519TR-12051925 0,15 -60 to 325/350 TR-121329TR-121329TR-121329TR-121329TR-121329
25 0,33 -60 to 325/350 TR-123329TR-123329TR-123329TR-123329TR-123329
25 0,35 -60 to 325/350 TR-120329TR-120329TR-120329TR-120329TR-12032925 0,50 -60 to 325/350 TR-120529TR-120529TR-120529TR-120529TR-120529
30 0,15 -60 to 325/350 TR-121339TR-121339TR-121339TR-121339TR-121339
30 0,35 -60 to 325/350 TR-120339TR-120339TR-120339TR-120339TR-12033930 0,50 -60 to 325/350 TR-120539TR-120539TR-120539TR-120539TR-120539
50 0,15 -60 to 325/350 TR-121359TR-121359TR-121359TR-121359TR-121359
50 0,33 -60 to 325/350 TR-123359TR-123359TR-123359TR-123359TR-12335950 0,35 -60 to 325/350 TR-120359TR-120359TR-120359TR-120359TR-120359
50 0,50 -60 to 325/350 TR-120559TR-120559TR-120559TR-120559TR-120559
60 0,15 -60 to 325/350 TR-121369TR-121369TR-121369TR-121369TR-12136960 0,35 -60 to 325/350 TR-120369TR-120369TR-120369TR-120369TR-120369
60 0,50 -60 to 325/350 TR-120569TR-120569TR-120569TR-120569TR-120569
0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-120112TR-120112TR-120112TR-120112TR-120112
15 0,25 -60 to 325/350 TR-120212TR-120212TR-120212TR-120212TR-120212
15 0,50 -60 to 325/350 TR-120512TR-120512TR-120512TR-120512TR-12051215 1,00 -60 to 320/350 TR-121012TR-121012TR-121012TR-121012TR-121012
25 0,10 -60 to 325/350 TR-120122TR-120122TR-120122TR-120122TR-120122
25 0,25 -60 to 325/350 TR-120222TR-120222TR-120222TR-120222TR-12022225 0,50 -60 to 325/350 TR-120522TR-120522TR-120522TR-120522TR-120522
25 1,00 -60 to 320/350 TR-121022TR-121022TR-121022TR-121022TR-121022
30 0,10 -60 to 325/350 TR-120132TR-120132TR-120132TR-120132TR-12013230 0,25 -60 to 325/350 TR-120232TR-120232TR-120232TR-120232TR-120232
30 0,50 -60 to 325/350 TR-120532TR-120532TR-120532TR-120532TR-120532
30 1,00 -60 to 320/350 TR-121032TR-121032TR-121032TR-121032TR-12103250 0,10 -60 to 325/350 TR-120152TR-120152TR-120152TR-120152TR-120152
50 0,25 -60 to 325/350 TR-120252TR-120252TR-120252TR-120252TR-120252
50 0,50 -60 to 325/350 TR-120552TR-120552TR-120552TR-120552TR-12055250 1,00 -60 to 320/350 TR-121052TR-121052TR-121052TR-121052TR-121052
60 0,10 -60 to 325/350 TR-120162TR-120162TR-120162TR-120162TR-120162
60 0,25 -60 to 325/350 TR-120262TR-120262TR-120262TR-120262TR-12026260 0,50 -60 to 325/350 TR-120562TR-120562TR-120562TR-120562TR-120562
60 1,00 -60 to 325/350 TR-121062TR-121062TR-121062TR-121062TR-121062
0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-120113TR-120113TR-120113TR-120113TR-120113
15 0,25 -60 to 325/350 TR-120213TR-120213TR-120213TR-120213TR-120213
15 0,50 -60 to 325/350 TR-120513TR-120513TR-120513TR-120513TR-12051315 1,00 -60 to 325/350 TR-121013TR-121013TR-121013TR-121013TR-121013
15 3,00 -60 to 280/350 TR-123013TR-123013TR-123013TR-123013TR-123013
25 0.10 -60 to 325/350 TR-120123TR-120123TR-120123TR-120123TR-120123
TRB-5TRB-5InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 25 0,25 -60 to 325/350 TR-120223TR-120223TR-120223TR-120223TR-120223
25 0,50 -60 to 325/350 TR-120523TR-120523TR-120523TR-120523TR-12052325 1,00 -60 to 325/350 TR-121023TR-121023TR-121023TR-121023TR-121023
25 3,00 -60 to 280/350 TR-123023TR-123023TR-123023TR-123023TR-123023
30 0,10 -60 to 325/350 TR-120133TR-120133TR-120133TR-120133TR-12013330 0,25 -60 to 325/350 TR-120233TR-120233TR-120233TR-120233TR-120233
30 0,50 -60 to 325/350 TR-120533TR-120533TR-120533TR-120533TR-120533
30 1,00 -60 to 325/350 TR-121033TR-121033TR-121033TR-121033TR-12103330 3,00 -60 to 280/350 TR-123033TR-123033TR-123033TR-123033TR-123033
50 0,10 -60 to 325/350 TR-120153TR-120153TR-120153TR-120153TR-120153
50 0,25 -60 to 325/350 TR-120253TR-120253TR-120253TR-120253TR-12025350 0,50 -60 to 325/350 TR-120553TR-120553TR-120553TR-120553TR-120553
50 1,00 -60 to 325/350 TR-121053TR-121053TR-121053TR-121053TR-121053
50 3,00 -60 to 280/350 TR-123053TR-123053TR-123053TR-123053TR-12305360 0,10 -60 to 325/350 TR-120163TR-120163TR-120163TR-120163TR-120163
60 0,25 -60 to 325/350 TR-120263TR-120263TR-120263TR-120263TR-120263
60 0,50 -60 to 325/350 TR-120563TR-120563TR-120563TR-120563TR-12056360 1,00 -60 to 325/350 TR-121063TR-121063TR-121063TR-121063TR-121063
60 3,00 -60 to 280/350 TR-123063TR-123063TR-123063TR-123063TR-123063
0,530,530,530,530,53 10 2,65 -60 to 270/290 TR-122645TR-122645TR-122645TR-122645TR-12264515 0,10 -60 to 320/340 TR-120115TR-120115TR-120115TR-120115TR-120115
15 0,50 -60 to 320/340 TR-120515TR-120515TR-120515TR-120515TR-12051515 1,50 -60 to 310/330 TR-121515TR-121515TR-121515TR-121515TR-121515
15 3,00 -60 to 270/290 TR-123015TR-123015TR-123015TR-123015TR-123015
15 5,00 -60 to 270/290 TR-125015TR-125015TR-125015TR-125015TR-12501525 0,10 -60 to 320/340 TR-120125TR-120125TR-120125TR-120125TR-120125
25 0,50 -60 to 320/340 TR-120525TR-120525TR-120525TR-120525TR-120525
25 1,50 -60 to 310/330 TR-121525TR-121525TR-121525TR-121525TR-12152525 3,00 -60 to 270/290 TR-123025TR-123025TR-123025TR-123025TR-123025
25 5,00 -60 to 270/290 TR-125025TR-125025TR-125025TR-125025TR-125025
30 0,10 -60 to 320/340 TR-120135TR-120135TR-120135TR-120135TR-12013530 0,50 -60 to 320/340 TR-120535TR-120535TR-120535TR-120535TR-120535
30 0,88 -60 to 310/330 TR-120835TR-120835TR-120835TR-120835TR-120835
30 1,50 -60 to 310/330 TR-121535TR-121535TR-121535TR-121535TR-12153530 2,65 -60 to 270/290 TR-122635TR-122635TR-122635TR-122635TR-122635
30 3,00 -60 to 270/290 TR-123035TR-123035TR-123035TR-123035TR-123035
30 5,00 -60 to 270/290 TR-125035TR-125035TR-125035TR-125035TR-12503550 0,10 -60 to 320/340 TR-120155TR-120155TR-120155TR-120155TR-120155
50 0,50 -60 to 320/340 TR-120555TR-120555TR-120555TR-120555TR-120555
50 1,50 -60 to 310/330 TR-121555TR-121555TR-121555TR-121555TR-12155550 3,00 -60 to 270/290 TR-123055TR-123055TR-123055TR-123055TR-123055
50 5,00 -60 to 270/290 TR-125055TR-125055TR-125055TR-125055TR-12505560 0,10 -60 to 320/340 TR-120165TR-120165TR-120165TR-120165TR-120165
60 0,50 -60 to 320/340 TR-120565TR-120565TR-120565TR-120565TR-120565
60 1,50 -60 to 310/330 TR-121565TR-121565TR-121565TR-121565TR-12156560 3,00 -60 to 270/290 TR-123065TR-123065TR-123065TR-123065TR-123065
60 5,00 -60 to 270/290 TR-125065TR-125065TR-125065TR-125065TR-125065
TRB-5 Equ iva lent PhaseTRB-5 Equ iva lent PhaseTRB-5 Equ iva lent PhaseTRB-5 Equ iva lent PhaseTRB-5 Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx-5, Rtx XTIAgilent/JWAgilent/JWAgilent/JWAgilent/JWAgilent/JW: HP-5, Ultra-2, DB-5, DB-5.625Supelco:Supelco:Supelco:Supelco:Supelco: SPB-5, PTE-5, SAC-5, Equity-5
Chromapack/VChromapack/VChromapack/VChromapack/VChromapack/Varianar ianar ianar ianar ian: CP-SIL8CBAlltechAl ltechAl ltechAl ltechAl ltech: AT-5Macherey-NagelMacherey-NagelMacherey-NagelMacherey-NagelMacherey-Nagel: OPTIMA-5QuadrexQuadrexQuadrexQuadrexQuadrex: 007-2SGESGESGESGESGE: BP-5
21
IRGANOX 1010
Column: TRB-5ht, TRB-5ht, TRB-5ht, TRB-5ht, TRB-5ht, 15m X 0,25 mm X 0,10 µm, P/N TR-620112Injection: 1µ1 (Irganox 1010, 12mg/ml chloroform), split (1:60), 370ºCCarrier gas: H2, 6psi (41,3 kPa)Oven temp.: 150°C to 380ºC (10 min.) @ 30°C/min.Detector: FID to 390°C
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TKG 1110
Sterols
Column: TRB-Sterol, TRB-Sterol, TRB-Sterol, TRB-Sterol, TRB-Sterol, 30m X 0,22 mm X 0,22 µm, P/N TR-182238Oven Temp.: 265ºCInjector: 280ºCCarrier gas: H2, 18 psi (124 kPa)Injection: 0,5 µl sterols standard, (25 mg/ml.) split(1:100)Detector: FID 300°C
TKG 1111
TRB-5ht/Inox-5htTRB-5ht/Inox-5ht
(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• Produced specially for analysis at high temperature up to 400ºC.
• Fused silica tube covered with polyimide, resistant to high temperatures, orstainless steel tube (specially deactivated).
• Excellent symmetry for compounds with high boiling points.
• Preferably used for the analysis of waxes, triglycerides, sterol esters,polyoxyethylenated alcohols, etc.
TRB-5ht/Inox-5htInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,10 -60 to 395 TR-620112TR-620112TR-620112TR-620112TR-620112
30 0,10 -60 to 395 TR-620132TR-620132TR-620132TR-620132TR-620132
0,320,320,320,320,32 15 0,10 -60 to 390 TR-620113TR-620113TR-620113TR-620113TR-62011330 0,10 -60 to 390 TR-620133TR-620133TR-620133TR-620133TR-620133
TRB-SterolTRB-Sterol
(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• Column specifically designed for the analysis of complex mixtures of sterols,from either animal or plant origin.
• Deactivation method of the capillary tube wall, developed by Teknokroma,that guarantees a high chemical inertness a low bleeding level and allows theanalysis of sterols without derivatization.
• The column is specifically tested for sterols.
TRB-5-SterolInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,220,220,220,220,22 30 0,22 -60 to 325-350 TR-182238TR-182238TR-182238TR-182238TR-182238
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent PhaseTRB-5ht/Inox -5ht Equ iva lent Phase
Agi lentAgi lentAgi lentAgi lentAgi lent: DB-5ht
TRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent PhaseTRB-Ste ro l Equ iva lent Phase
SupelcoSupelcoSupelcoSupelcoSupelco: SAC-5
2 2
TRB-5ms
TRB-5ms
(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.(95%) Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• The TRB-5ms Column uses the same stationary phase as TRB-5, but thepolymer synthesis process, the capillary deactivation technique and thebonding and crosslinking procedures have been optimized to obtain theminimum possible bleeding level and an exceptional chemical inertness.
• The bleeding specifications for a column of 30m x 0,25 mm x 0,25 µm(P/N 520232) inidcate that it is lower than 4 pA at 325ºC.
• Column recommended to work with any selective detector.
• Ideal column to connect with a mass detector. Its ultra-low bleeding joined toits high chemical inertness allows for a better signal/noise ratio (highersensitivity level), and therefore better detection and quantification of samplecomponents at low concentrations.
TRB -5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent PhaseTRB-5ms Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx 5msAgli lent/JWAgli lent/JWAgli lent/JWAgli lent/JWAgli lent/JW: : : : : HP-5MSSupelcoSupelcoSupelcoSupelcoSupelco: PTE-5, Equity-5Macherey-NagelMacherey-NagelMacherey-NagelMacherey-NagelMacherey-Nagel: OPTIMA-5VVVVVarianar ianar ianar ianar ian: CP-Sil8-MS
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-5MSInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 12 0,33 -60 to 325-350 TR-5233B9TR-5233B9TR-5233B9TR-5233B9TR-5233B9
15 0,33 -60 to 325-350 TR-523319TR-523319TR-523319TR-523319TR-523319
25 0,33 -60 to 325-350 TR-523329TR-523329TR-523329TR-523329TR-523329
30 0,33 -60 to 325-350 TR-523339TR-523339TR-523339TR-523339TR-523339
50 0,33 -60 to 325-350 TR-523359TR-523359TR-523359TR-523359TR-523359
60 0,33 -60 to 325-350 TR-523369TR-523369TR-523369TR-523369TR-523369
0,250,250,250,250,25 15 0,10 -60 to 325-350 TR-520112TR-520112TR-520112TR-520112TR-520112
15 0,25 -60 to 325-350 TR-520212TR-520212TR-520212TR-520212TR-520212
15 1,00 -60 to 325-350 TR-521012TR-521012TR-521012TR-521012TR-521012
30 0,10 -60 to 325-350 TR-520132TR-520132TR-520132TR-520132TR-520132
30 0,25 -60 to 325-350 TR-520232TR-520232TR-520232TR-520232TR-520232
30 1,00 -60 to 325-350 TR-521032TR-521032TR-521032TR-521032TR-521032
60 0,10 -60 to 325-350 TR-520162TR-520162TR-520162TR-520162TR-520162
60 0,25 -60 to 325-350 TR-520262TR-520262TR-520262TR-520262TR-520262
60 1,00 -60 to 325-350 TR-521062TR-521062TR-521062TR-521062TR-521062
0,320,320,320,320,32 15 0,10 -60 to 325-350 TR-520113TR-520113TR-520113TR-520113TR-520113
15 0,25 -60 to 325-350 TR-520213TR-520213TR-520213TR-520213TR-520213
15 0,50 -60 to 325-350 TR-520513TR-520513TR-520513TR-520513TR-520513
15 1,00 -60 to 325-350 TR-521013TR-521013TR-521013TR-521013TR-521013
30 0,10 -60 to 325-350 TR-520133TR-520133TR-520133TR-520133TR-520133
30 0,25 -60 to 325-350 TR-520233TR-520233TR-520233TR-520233TR-520233
30 0,50 -60 to 325-350 TR-520533TR-520533TR-520533TR-520533TR-520533
30 1,00 -60 to 325-350 TR-521033TR-521033TR-521033TR-521033TR-521033
60 0,10 -60 to 325-350 TR-520163TR-520163TR-520163TR-520163TR-520163
60 0,25 -60 to 325-350 TR-520263TR-520263TR-520263TR-520263TR-520263
60 0,50 -60 to 325-350 TR-520563TR-520563TR-520563TR-520563TR-520563
60 1,00 -60 to 325-350 TR-521063TR-521063TR-521063TR-521063TR-521063
0,530,530,530,530,53 15 0,50 -60 to 320-340 TR-520515TR-520515TR-520515TR-520515TR-520515
15 1,00 -60 to 320-340 TR-521015TR-521015TR-521015TR-521015TR-521015
15 1,50 -60 to 310-330 TR-521515TR-521515TR-521515TR-521515TR-521515
30 0,50 -60 to 320-340 TR-520535TR-520535TR-520535TR-520535TR-520535
30 1,00 -60 to 320-340 TR-521035TR-521035TR-521035TR-521035TR-521035
30 1,50 -60 to 310-330 TR-521535TR-521535TR-521535TR-521535TR-521535
23
Peak Name
1. Methylene chloride2. 1,2-Hexanediol3. Nitroso-di-n-propylamine4. Benzoic acid5. C-146. 2,4-Dinitrophenol7. 4-Nitrophenol8. 4-Nitroaniline9. Pentachlorophenol10. Carbazole11. C-2012. C-2113. C-2214. Benzo(b)fluoranthene15. Benzol(k)fluoranthene16. Benzo(ghi)perylene
Test MX5
Column: TRB-5ms, TRB-5ms, TRB-5ms, TRB-5ms, TRB-5ms, P/N TR-520232Dimensions: 30 m x 0,25 mm x 0,25 µmInjection: 1µ1, split (1:100), 5 to 10 ng/comp. on column, 280ºCCarrier gas: H2, 12 psi (87,7 kPa)Oven temp.: 100°C to 325ºC (5 min.) @ 6°C/min.Detector: FID to 300°CSample: Test MX5
Injection of 1ng/peak on columnExceptional symmetry
Excellent resolution
Bleedinglevel <2pA
TKG 1112
TRB-5msThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetrThe TRB-5MS column has an excellent resolution and symmetry in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thaty in all its polarity range, for neutral, acid and basic compounds. All these substances thatappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPappear in the analysis of semivolati le traces (for example, EPA official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.A official methods) can be analyzed in only one column.
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
2 4
Amines Test
Column: TRB-5AmineTRB-5AmineTRB-5AmineTRB-5AmineTRB-5Amine, P/N TR-210532Dimensions: 30 m x 0.25 mm x 0.50 µmInjection: 1 µL (split 1:50), 280ºCCarrier gas: H2, 12 psi (87.7 kPa).Oven temperature: 100ºC to 280ºC (5 min.) @ 20ºC/min.Detector: FID, 300ºCSample: Test SP-48278 (500ng/µl)
Peak Name
1 Methyl tert-butyl ether2 Benzylamine3 n-Octylamine4 n-Nonylamine5 2,4-Dimethylaniline6 2,6-Dimethylaniline7 n-Decylamine8 C-159 C-1610 C-1711 Tri-n-hexylamine12 C-1813 C-20
TKG 1113
TRB-5AmineTRB-5Amine
9595959595% % % % % Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• Column specially designed for the analysis of amines.
• Basic deactivation of the column surface with reagents synthetized in ourlaboratories, that jointly with the crosslinking method have permitted theminimization of the absorption level and tailing of basic compounds, like thealkylamines, alcoholamines, basic pharmaceuticals, aromatic amines, etc.
• Selectivity and thermal stability equivalent to the TRB-5 columns.
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB-5AmineInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,50 -60 to 300/315 TR-210512TR-210512TR-210512TR-210512TR-21051215 1,00 -60 to 300/315 TR-211012TR-211012TR-211012TR-211012TR-21101230 0,50 -60 to 300/315 TR-210532TR-210532TR-210532TR-210532TR-21053230 1,00 -60 to 300/315 TR-211032TR-211032TR-211032TR-211032TR-21103260 0,50 -60 to 300/315 TR-210562TR-210562TR-210562TR-210562TR-21056260 1,00 -60 to 300/315 TR-211062TR-211062TR-211062TR-211062TR-211062
0,320,320,320,320,32 15 0,50 -60 to 300/315 TR-210513TR-210513TR-210513TR-210513TR-21051315 1,00 -60 to 300/315 TR-211013TR-211013TR-211013TR-211013TR-21101315 1,50 -60 to 290/305 TR-211513TR-211513TR-211513TR-211513TR-21151330 0,50 -60 to 300/315 TR-210533TR-210533TR-210533TR-210533TR-21053330 1,00 -60 to 300/315 TR-211033TR-211033TR-211033TR-211033TR-21103330 1,50 -60 to 290/305 TR-211533TR-211533TR-211533TR-211533TR-21153360 0,50 -60 to 300/315 TR-210563TR-210563TR-210563TR-210563TR-21056360 1,00 -60 to 300/315 TR-211063TR-211063TR-211063TR-211063TR-21106360 1,50 -60 to 290/305 TR-211563TR-211563TR-211563TR-211563TR-211563
0,530,530,530,530,53 15 1,00 -60 to 290/305 TR-211015TR-211015TR-211015TR-211015TR-21101515 3,00 -60 to 280/295 TR-213015TR-213015TR-213015TR-213015TR-21301530 1,00 -60 to 290/305 TR-211035TR-211035TR-211035TR-211035TR-21103530 3,00 -60 to 280/295 TR-213035TR-213035TR-213035TR-213035TR-21303560 1,00 -60 to 290/305 TR-211065TR-211065TR-211065TR-211065TR-21106560 3,00 -60 to 280/295 TR-213065TR-213065TR-213065TR-213065TR-213065
TRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent PhaseTRB-5Amine Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx-5AmineSupelcoSupelcoSupelcoSupelcoSupelco: PTA-5
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
25
TRB-5. 625
TRB-5.625InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-2633B9TR-2633B9TR-2633B9TR-2633B9TR-2633B925 0,33 -60 to 325/350 TR-263329TR-263329TR-263329TR-263329TR-26332950 0,33 -60 to 325/350 TR-263359TR-263359TR-263359TR-263359TR-263359
0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-260112TR-260112TR-260112TR-260112TR-26011215 0,25 -60 to 325/350 TR-260212TR-260212TR-260212TR-260212TR-26021215 0,50 -60 to 325/350 TR-260512TR-260512TR-260512TR-260512TR-26051215 1,00 -60 to 325/350 TR-261012TR-261012TR-261012TR-261012TR-26101230 0,10 -60 to 325/350 TR-260132TR-260132TR-260132TR-260132TR-26013230 0,25 -60 to 325/350 TR-260232TR-260232TR-260232TR-260232TR-26023230 0,50 -60 to 325/350 TR-260532TR-260532TR-260532TR-260532TR-26053230 1,00 -60 to 325/350 TR-261032TR-261032TR-261032TR-261032TR-26103260 0,10 -60 to 325/350 TR-260162TR-260162TR-260162TR-260162TR-26016260 0,25 -60 to 325/350 TR-260262TR-260262TR-260262TR-260262TR-260262
0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-260113TR-260113TR-260113TR-260113TR-26011315 0,25 -60 to 325/350 TR-260213TR-260213TR-260213TR-260213TR-26021315 0,50 -60 to 325/350 TR-260513TR-260513TR-260513TR-260513TR-26051315 1,00 -60 to 325/350 TR-261013TR-261013TR-261013TR-261013TR-26101330 0,10 -60 to 325/350 TR-260133TR-260133TR-260133TR-260133TR-26013330 0,25 -60 to 325/350 TR-260233TR-260233TR-260233TR-260233TR-26023330 0,50 -60 to 325/350 TR-260533TR-260533TR-260533TR-260533TR-26053330 1,00 -60 to 325/350 TR-261033TR-261033TR-261033TR-261033TR-26103360 0,10 -60 to 325/350 TR-260163TR-260163TR-260163TR-260163TR-260163
0,530,530,530,530,53 15 1,50 -60 to 320/340 TR-261515TR-261515TR-261515TR-261515TR-26151530 0,50 -60 to 320/340 TR-260535TR-260535TR-260535TR-260535TR-26053530 1,00 -60 to 310/330 TR-261035TR-261035TR-261035TR-261035TR-26103560 0,25 -60 to 325/350 TR-260263TR-260263TR-260263TR-260263TR-260263
TRB-5. 625
9595959595% % % % % Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• Specially manufactured column to fulfil the level of inertness required by theEPA methods for the analysis of semivolatile compounds, designed formethods 625, 1625, 8270 and CLP protocols.
• Inertness and minimum absorption for acidic, basic and neutral compounds.
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB-G27
TRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent PhaseTRB-5. 625 Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx-XTI-5SupelcoSupelcoSupelcoSupelcoSupelco: PTE-5Agilent:Agi lent:Agi lent:Agi lent:Agi lent: DB.5.625
TRB-G27InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,530,530,530,530,53 30 5,00 -60 to 270/290 TR-175035TR-175035TR-175035TR-175035TR-175035
TRB-G27
9595959595% % % % % Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.Dimethyl-(5%) diphenylpolysi loxane, bonded and crossl inked phase.
• Column which fulfils the specifications of the American Pharmacopea (USP),for the test of organic volatile impurities (OVI) in pharmaceutical products.Methods <USP 467>.
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB -G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent PhaseTRB-G27 Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx-G27SupelcoSupelcoSupelcoSupelcoSupelco: G27
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
2 6
Peak Name
1 Methanol2 Ethanol3 Acetonitrile4 Acetone5 Isopropanol6 Ethyl ether7 Methylene chloride8 n-Propanol9 Methyl ethyl ketone (MEK)10 n-Hexane11 Ethyl acetate12 Chloroform13 Tetrahydrofuran (THF)14 Cyclohexane15 1,2-Dicholoroethane16 Benzene17 Carbon tetrachloride18 n-Butanol19 n-Heptane20 Trichloroethylene21 1,4-Dioxane22 Pyridine23 Toluene24 Dimethylformamide (DMF)25 p-Xylene26 m-Xylene27 o-Xylene
Residual solvents in Pharmaceutical Products
Column: TRB-G27TRB-G27TRB-G27TRB-G27TRB-G27, 30 m x 0,53 mm x 5,0 µm, P/N TR-175035Injectioon: 220ºC, (split 1:80), 5 m phenylmethyl deactivated retention gapCarrier Gas: He, 4,5 psi (31kPa), 35 cm/s. to 35ºCOven Temp: 35ºC (10 min.) to 100ºC @ 5º C/min. to 240ºC (5 min.) @ 25ºC/min.Detector: FID@ 250ºCSample: 0,02 µl solvent mixture
TKG 1114
TRB-G27
Meta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent PhaseMeta.X5 Equ iva lent Phase
RestekRestekRestekRestekRestek: Rtx-5Sil MSAgilent/JWAgilent/JWAgilent/JWAgilent/JWAgilent/JW::::: DB.5 MS, HP-5TASupelco:Supelco:Supelco:Supelco:Supelco: MDN-5Chromopack/VChromopack/VChromopack/VChromopack/VChromopack/Varian: arian: arian: arian: arian: CP-SIL8CB MSAlltech: AT-5msQuadrex: Quadrex: Quadrex: Quadrex: Quadrex: 007-5MSSGE:SGE:SGE:SGE:SGE: BPX-5
Meta.X5Meta.X5
Silphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedSilphenylene phase, selectivity similar to TRB-5, bonded and crossl inkedphase.phase.phase.phase.phase.
• Choice column for the analysis of semivolatile compounds with GC ,EM.
• Polymer synthesis designed and developed by scientists at Teknokroma.
• Selectivity similar to TRB-5.
• New generation of column incorporates arylene groups in the polymerstructure, and this improves the thermal stability, reduces the bleeding leveland provides optimal resolution for aromatic compounds.
• Manufacturing procedures of this Teknokroma column guarantees maximalinertness and minimal bleeding level.
• Quality control test (MX5) that guarantees total inertness and optimal signal/noise ratio (S/N) for the more active compounds that normally sufferadsorption problems, like 2,4-dinitropherol, 4 nitroaniline andpentachlorophenol.
Structure of Polysiloxane containing p-silphenylene
SiSiCH3
CH3CH3
CH3OO Si
R1O
R2x y
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
27
Compare Column Bleed Levels
Increase of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofIncrease of the base l ine level (bleeding) produced by the degradation ofthe stationarthe stationarthe stationarthe stationarthe stationary phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.y phase when the temperature increases.
Column: Meta.X5Meta.X5Meta.X5Meta.X5Meta.X5, 30 m X 0,25 mm X 0,25 µm, P/N TR-820232Injection: 100ºC,Carrier Gas: H2, 12 psi (82,7 kPa)Oven Temp: 100ºC to 325ªC (5 min.) @ 20º C/min.Detector: FID@ 340ºC
Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)Bleeding level lower than 1pA at 325ºC (limit<4pA)
Peak Name
1 Meta.X52 Manufacturer A3 Manufacturer B4 Manufacturer C
pA
TKG 1115
Meta.X5InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 12 0,33 -60 to 325/350 TR-8233B9TR-8233B9TR-8233B9TR-8233B9TR-8233B925 0,33 -60 to 325/350 TR-823329TR-823329TR-823329TR-823329TR-82332950 0,33 -60 to 325/350 TR-823359TR-823359TR-823359TR-823359TR-823359
0,250,250,250,250,25 15 0,10 -60 to 325/350 TR-820112TR-820112TR-820112TR-820112TR-82011215 0,25 -60 to 325/350 TR-820212TR-820212TR-820212TR-820212TR-82021215 0,50 -60 to 325/350 TR-820512TR-820512TR-820512TR-820512TR-82051215 1,00 -60 to 325/350 TR-821012TR-821012TR-821012TR-821012TR-82101230 0,10 -60 to 325/350 TR-820132TR-820132TR-820132TR-820132TR-82013230 0,25 -60 to 325/350 TR-820232TR-820232TR-820232TR-820232TR-82023230 0,50 -60 to 325/350 TR-820532TR-820532TR-820532TR-820532TR-82053230 1,00 -60 to 325/350 TR-821032TR-821032TR-821032TR-821032TR-82103260 0,10 -60 to 325/350 TR-820162TR-820162TR-820162TR-820162TR-82016260 0,25 -60 to 325/350 TR-820262TR-820262TR-820262TR-820262TR-820262
0,320,320,320,320,32 15 0,10 -60 to 325/350 TR-820113TR-820113TR-820113TR-820113TR-82011315 0,25 -60 to 325/350 TR-820213TR-820213TR-820213TR-820213TR-820213
Meta.X5
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 15 0,50 -60 to 325/350 TR-820513TR-820513TR-820513TR-820513TR-82051315 1,00 -60 to 325/350 TR-821013TR-821013TR-821013TR-821013TR-82101330 0,10 -60 to 325/350 TR-820133TR-820133TR-820133TR-820133TR-82013330 0,25 -60 to 325/350 TR-820233TR-820233TR-820233TR-820233TR-82023330 0,50 -60 to 325/350 TR-820533TR-820533TR-820533TR-820533TR-82053330 1,00 -60 to 325/350 TR-821033TR-821033TR-821033TR-821033TR-82103360 0,10 -60 to 325/350 TR-820163TR-820163TR-820163TR-820163TR-82016360 0,25 -60 to 325/350 TR-820263TR-820263TR-820263TR-820263TR-820263
0,530,530,530,530,53 15 0,50 -60 to 320/340 TR-820515TR-820515TR-820515TR-820515TR-82051515 1,00 -60 to 320/340 TR-821015TR-821015TR-821015TR-821015TR-82101515 1,50 -60 to 320/340 TR-821515TR-821515TR-821515TR-821515TR-82151530 0,50 -60 to 320/340 TR-820535TR-820535TR-820535TR-820535TR-82053530 1,00 -60 to 320/340 TR-821035TR-821035TR-821035TR-821035TR-82103530 1,50 -60 to 310/330 TR-821535TR-821535TR-821535TR-821535TR-821535
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
2 8
Signal/Noise ratio
The reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueThe reduction of bleeding level to the minimum possible valueallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature whenallows the detection of trace compounds at high temperature wheninterinterinterinterinterferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.ferences in the identif ication process are minimized.
Column: Meta.X5 Meta.X5 Meta.X5 Meta.X5 Meta.X5, P/N TR-820232Dimensions: 30m x 0.25mm x 0,25 µmInjection:1,0 µL (splitless, 1 min.) 300ºCCarrier gas: He, 12 ml/min. constant flow.Oven temperature: 60ºC (1 min.) to 320º (15 min.) @30ºC/min.Detector: MSD(SIM), transfer line 300ºCSample: DCB/n-Hexane
Signal/Noise ratioSignal/Noise ratioSignal/Noise ratioSignal/Noise ratioSignal/Noise ratio
S/N = 831ng of Decachlorobiphenyl (DCB)
time TKG 1116
Meta.X5
Separation of aromatic polycyclic hydrocarbons (EPA Method 610)
Column: Meta.X5 Meta.X5 Meta.X5 Meta.X5 Meta.X5, P/N TR-820232Dimensions: 30m x 0.25mm x 0,50 µmInjection:0,3 µL (splitless, 1´) 300ºCCarrier gas: H2, 16 PSI (110,2 kPa). Cte.Oven temperature: 40ºC (1 min.) to 200º @ 20ºC/min to 310ºC (5 min.)@4ºC/minDetector: FID, 340ºCSample: Test PAH (aprox. 12ng/comp. in column)
Peak Name
1 Naphathalene2 Acenaphthylene3 Acenaphthene4 Fluorene5 Phenanthrene6 Anthracene7 Fluoranthene8 Pyrene9 Chrysene10 Benz (a) anthracene11 Benz (b) fluoranthene12 Benz (k) fluoranthene13 Benz (a) pyrene14 Indeno (1,2,3-cd) pyrene15 Dibenzo (ah) anthracene16 Benzo (ghi) perylene
All cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peaksAll cr it ical pair peakswell separatedwell separatedwell separatedwell separatedwell separated
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TKG 1117
29
TRB-1301
9494949494% % % % % Dimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• (6%)Cyanopropyl-phenyl-(94%)dimethylpolysiloxane.
• Ideal column for analyzing mixtures of acidic and basic compounds with awide range of polarity.
• This column of intermediate polarity is very useful for analyzing pesticides andherbicides.
TRB-1301InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,25 -20 to 280/300 TR-600212TR-600212TR-600212TR-600212TR-60021215 1,00 -20 to 260/280 TR-601012TR-601012TR-601012TR-601012TR-60101230 0,25 -20 to 280/300 TR-600232TR-600232TR-600232TR-600232TR-60023230 1,00 -20 to 260/280 TR-601032TR-601032TR-601032TR-601032TR-60103260 0,25 -20 to 280/300 TR-600262TR-600262TR-600262TR-600262TR-60026260 1,00 -20 to 260/280 TR-601062TR-601062TR-601062TR-601062TR-601062
0,320,320,320,320,32 15 0,25 -20 to 280/300 TR-600213TR-600213TR-600213TR-600213TR-60021315 1 00 -20 to 260/280 TR-601013TR-601013TR-601013TR-601013TR-60101330 0,25 -20 to 280/300 TR-600233TR-600233TR-600233TR-600233TR-60023330 1,00 -20 to 260/280 TR-601033TR-601033TR-601033TR-601033TR-60103360 0,25 -20 to 280/300 TR-600263TR-600263TR-600263TR-600263TR-60026360 1,00 -20 to 260/280 TR-601063TR-601063TR-601063TR-601063TR-601063
0,530,530,530,530,53 15 1,00 -20 to 260/280 TR-601015TR-601015TR-601015TR-601015TR-60101530 1,00 -20 to 260/280 TR-601035TR-601035TR-601035TR-601035TR-60103560 1,00 -20 to 260/280 TR-601065TR-601065TR-601065TR-601065TR-601065
TRB-1301
Column: TRB-1301TRB-1301TRB-1301TRB-1301TRB-1301, P/N TR-601032Dimensions: 30m x 0.25mm x 1.0µmInjection: 0.5µL standard SP-4-7301 (500 ng/mL), split 1:50, 260ºCCarrier gas: H2, constant pressure 12 psi (82.7 KPa).Oven temperature: 165ºCDetector: FID, 280ºC
Peak Name
1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 C-127 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-1310 C-14
TRB-1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent PhaseTRB -1301 Equ iva lent Phase
Agi lentAgi lentAgi lentAgi lentAgi lent: HP-1301, HP-624, DB-1301, DB-624SupelcoSupelcoSupelcoSupelcoSupelco: SPB-1301, OVI-G43RestekRestekRestekRestekRestek: Rtx-1301, Rtx-624SGESGESGESGESGE: BPX-624AlltechAl ltechAl ltechAl ltechAl ltech: AT-624
TRB-1301
Structure of Poly(dimethylcyanopropylphenyl)siloxane
Si OO SiCH3
CH3
CH2)3CN
O(
m n
TKG 1118
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
3 0
Structure of Poly(dimethylcyanopropylphenyl)siloxane
Si OO SiCH3
CH3
CH2)3CN
O(
m n
TRB-624
Column: TRB-624TRB-624TRB-624TRB-624TRB-624, P/N TR-601462Dimensions: 60m x 0.25mm x 1.4µmInjection: 1µL solvents mixture, split 1:100 (20-600 ng/comp.), 260ºCCarrier gas: H2, constant pressure 25 psi (172.3 KPa).Oven temperature: 50ºC(5min) @ 6ºC/min to 220ºCDetector: FID, 280ºC
Peak Name
1- Diethylether2- Acetone3- Methyl acetate4- Vinyl acetate5- MEK6- Ethyl acetate7- Tetrahydrofuran8- Cyclohexane9- Benzene10- Isopropyl acetate11- 2-Pentanone
12- 3-Pentanone13- Propyl acetate14- Pyridine15- Toluene16- Isobutyl acetate17- Butyl acetate18- Ethyl benzene19- m-Xylene/p-Xylene20- o-Xylene21- Diisobutylketone22- Nitrobenzene
TRB-624TRB-624
9494949494% % % % % Dimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• (6%) Cyanopropyl-phenyl - (94%) dimethylpolysiloxane.
• Column developed specially for environmental analysis of volatile compounds(“Volatile Priority Pollutants”).
• Column perfectly compatible with EPA methods 501.3, 502.2, 524.2, 601,602, 8010, 8015, 8020, 8221, 8240 and 8260.
• Excellent inertness against active compounds.
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TKG 1119
TRB -624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent PhaseTRB-624 Equ iva lent Phase
Agilent: HP-1301, HP-624, DB-1301, DB-624Supelco: SPB-1301, OVI-G43Restek: Rtx-1301, Rtx-624SGE: BPX-624Alltech: AT-624
TRB-624InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 25 1,12 -20 to 240/260 TR-601129TR-601129TR-601129TR-601129TR-6011290,250,250,250,250,25 30 1,40 -20 to 240/260 TR-601432TR-601432TR-601432TR-601432TR-601432
60 1,40 -20 to 240/260 TR-601462TR-601462TR-601462TR-601462TR-6014620,320,320,320,320,32 30 1,80 -20 to 240/260 TR-601833TR-601833TR-601833TR-601833TR-601833
60 1,80 -20 to 240/260 TR-601863TR-601863TR-601863TR-601863TR-6018630,530,530,530,530,53 30 3,00 -20 to 240/260 TR-603035TR-603035TR-603035TR-603035TR-603035
60 3,00 -20 to 240/260 TR-603065TR-603065TR-603065TR-603065TR-60306575 3,00 -20 to 240/260 TR-603075TR-603075TR-603075TR-603075TR-603075
105 3,00 -20 to 240/260 TR-6030K5TR-6030K5TR-6030K5TR-6030K5TR-6030K5
31
TRB-624
Column: TRB-624TRB-624TRB-624TRB-624TRB-624, P/N TR-601462Dimensions: 60m x 0.25mm x 1.4µmInjection: 0.2µL, split 1:5, 260ºCCarrier gas: He,constant pressure 25 psi (172.3 KPa).Oven temperature: 40ºC(8min) @7ºC/min to 160ºC(5min)Detector: FID, 280ºC
Peak Name
1- Heptane (isomers mixture)2- Acetone3- Tetrahydrofuran4- Ethyl acetate5- Isopropyl acetate6- Methanol7- MEK8- Isopropanol9- Ethanol10- n-Propyl acetate11- MIBK12- n-Propanol13- Toluene14- Butyl acetate15- Methoxypropanol16- Methoxypropyl acetate
TRB-624
TKG 1120
TRB-G43
9494949494% % % % % Dimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andDimethyl-(6%) cyanopropylphenyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• (6%) Cyanopropyl-phenyl - (94%) dimethylpolysiloxane (USP G43).
• Fulfils the specifications of the American (USP) and European (EP)pharmacopoeia for the analysis of residual solvents (OVI) in pharmaceuticalproducts, USP method <467> and EP method 2.4.24.
• Column with chemical inertness and low bleed guaranteed.
• Specially tested for complete separation of the five solvents regulated byUSP Method 467.
• For this analysis, pharmacopoeia recommends the use of a guard column of5m (P/N TR-200055) to trap the non-volatile impurities in the sample.
TRB-G43
Structure of Poly(dimethylcyanopropylphenyl)siloxane
Si OO SiCH3
CH3
CH2)3CN
O(
m n
Peak Name
1- Methanol2- 1,2-Dichloroethene3- Acetonitrile4- Methylene chloride5- n-Hexane6- Cis-1,2-dichloroethene7- Nitromethane8- Chloroform9- Cyclohexane10- 1,1,1-Trichloroethane11- Carbon tetrachloride12- Benzene13- 1,2-Dimethoxyethane14- 1,2-Dichloroethane
15- Trichloroethylene16- Methylcyclohexane17- 1,4-Dioxane18- Pyridine19- Toluene20- 2-Hexanone21- Chlorobenzene22- Dimethylformamide23- Ethylbenzene24- m-Xylene25- p-Xylene26- o-Xylene27- N,N-dimethylacetamide28- 1,2,3,4-Tetrahydronaphthalene
TRB-G43
Column: TRB-G43TRB-G43TRB-G43TRB-G43TRB-G43, P/N TR-163035Dimensions: 30m x 0.53mm x 3.0µmInjection:, split 1:2, 250ºC, 5m x 0.53mm intermediate polarity column (TR-200055)Sample: 0.5 mL headspace 80ºC (2t static head space sampler) 28 Class 1 Mix and Class 2 Mix A, Mix B residual solvents at the regulatory limit concentration.Carrier gas: He, constant pressure 4.8 psi (33.1 KPa), 35 cm/s (40ºC)Oven temperature: 40ºC(20min) @ 10ºC/min to 240ºC(10min)Detector: FID, 250ºC
TKG 1121
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
3 2
TRB-G43
Column: TRB-G43TRB-G43TRB-G43TRB-G43TRB-G43, P/N TR-163035Dimensions: 30m x 0.53mm x 3.0µmInjection: 1mL headspace (2t static head space sampler), split 1:2 (liner1 mm ID), 5m x 0.53mm intermediate polarity precolumn (TR-200055),100 µL standard vial 20 mL + 5 mL H2O + 1g sodium sulfate, 140ºCCarrier gas: He, constant pressure 7 psi (48.2 KPa).Oven temperature: 40ºC(20min) @ 35ºC/min to 240ºC(20min)Detector: FID, 260ºC
Peak Name
1- Methylene chloride 600 ppm2- Chloroform 60 ppm3- Benzene 2 ppm4- Trichloroethylene 80 ppm5- 1,4-Dioxane 380 ppm
TRB-G43
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TKG 1122
TRB-G43InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,530,530,530,530,53 30 3,00 -20 to 240/260 TR-163035TR-163035TR-163035TR-163035TR-163035
TRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent PhaseTRB-G43 Equ iva lent Phase
Agi lentAgi lentAgi lentAgi lentAgi lent: HP-1301, HP-624, DB-1301, DB-624Supelco:Supelco:Supelco:Supelco:Supelco: SPB-1301, OVI-G43Restek:Restek:Restek:Restek:Restek: Rtx-1301, Rtx-624SGE: SGE: SGE: SGE: SGE: BPX-624Alltech:Al ltech:Al ltech:Al ltech:Al ltech: AT-624USP Nomenclature: G43
33
TRB-14
Column: TRB-14TRB-14TRB-14TRB-14TRB-14, P/N TR-801263Dimensions: 60m x 0.32mm x 1.2µmInjection: 0.1µL Amines mixture (0.02-0.2% in Acetonitrile),split 1:25, 200ºCCarrier gas: He, constant pressure 14 psi (96.5 Kpa)Oven temperature: 40ºC(2min) @ 10ºC/min to 250ºCDetector: FID, 280ºC
Peak Name
1 Methylamine2 Acetonitrile3 Diethylamine4 Triethylamine
1
2
4
3
TRB-14TRB-14
(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inked(14%) Diphenyl -(86%) dimethylpolysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.
• (14%) Diphenyl- (86%) dimethylpolysiloxane.
• Column of intermediate polarity without cyanopropyl groups in its structure.
• Chemical inertness and low bleed guaranteed.
• Confirmation column alongside TRB-1 and TRB-5.
TRB-14InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,20 -20 to 300/330 TR-802112TR-802112TR-802112TR-802112TR-802112
15 0,40 -20 to 300/330 TR-800412TR-800412TR-800412TR-800412TR-80041215 1,20 -20 to 300/330 TR-801212TR-801212TR-801212TR-801212TR-801212
30 0,20 -20 to 300/330 TR-802132TR-802132TR-802132TR-802132TR-80213230 0,40 -20 to 300/330 TR-800432TR-800432TR-800432TR-800432TR-800432
30 1,20 -20 to 300/330 TR-801232TR-801232TR-801232TR-801232TR-801232
60 0,20 -20 to 300/330 TR-802162TR-802162TR-802162TR-802162TR-80216260 0,40 -20 to 300/330 TR-800462TR-800462TR-800462TR-800462TR-800462
60 1,20 -20 to 300/330 TR-801262TR-801262TR-801262TR-801262TR-801262
0,320,320,320,320,32 15 0,20 -20 to 300/330 TR-802113TR-802113TR-802113TR-802113TR-80211315 0,40 -20 to 300/330 TR-800413TR-800413TR-800413TR-800413TR-800413
15 1,20 -20 to 300/330 TR-801213TR-801213TR-801213TR-801213TR-801213
30 0,20 -20 to 300/330 TR-802133TR-802133TR-802133TR-802133TR-80213330 0,40 -20 to 300/330 TR-800433TR-800433TR-800433TR-800433TR-800433
30 1,20 -20 to 300/330 TR-801233TR-801233TR-801233TR-801233TR-801233
60 0,20 -20 to 300/330 TR-802163TR-802163TR-802163TR-802163TR-80216360 0,40 -20 to 300/330 TR-800463TR-800463TR-800463TR-800463TR-800463
60 1,20 -20 to 300/330 TR-801263TR-801263TR-801263TR-801263TR-801263
0,530,530,530,530,53 15 1,00 -20 to 300/330 TR-801015TR-801015TR-801015TR-801015TR-80101515 2,00 -20 to 300/330 TR-802015TR-802015TR-802015TR-802015TR-802015
30 1,00 -20 to 300/330 TR-801035TR-801035TR-801035TR-801035TR-801035
30 2,00 -20 to 300/330 TR-802035TR-802035TR-802035TR-802035TR-802035
60 1,00 -20 to 300/330 TR-801065TR-801065TR-801065TR-801065TR-801065
60 2,00 -20 to 300/330 TR-802065TR-802065TR-802065TR-802065TR-802065
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TKG 1123
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-14 Equ iva lent PhaseTRB-14 Equ iva lent PhaseTRB-14 Equ iva lent PhaseTRB-14 Equ iva lent PhaseTRB-14 Equ iva lent Phase
VVVVVarian:arian:arian:arian:arian: CP-SIL 13 CB
3 4
TRB-20
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,25 -20 to 300/320 TR-200212TR-200212TR-200212TR-200212TR-20021215 1,00 -20 to 280/300 TR-201012TR-201012TR-201012TR-201012TR-201012
30 0,25 -20 to 300/320 TR-200232TR-200232TR-200232TR-200232TR-200232
30 1,00 -20 to 280/300 TR-201032TR-201032TR-201032TR-201032TR-20103260 0,25 -20 to 300/320 TR-200262TR-200262TR-200262TR-200262TR-200262
60 1,00 -20 to 280/300 TR-201062TR-201062TR-201062TR-201062TR-201062
0,320,320,320,320,32 15 0,25 -20 to 300/320 TR-200213TR-200213TR-200213TR-200213TR-20021315 1,00 -20 to 280/300 TR-201013TR-201013TR-201013TR-201013TR-201013
30 0,25 -20 to 300/320 TR-200233TR-200233TR-200233TR-200233TR-200233
30 1,00 -20 to 280/300 TR-201033TR-201033TR-201033TR-201033TR-20103360 0,25 -20 to 300/320 TR-200263TR-200263TR-200263TR-200263TR-200263
60 1,00 -20 to 280/300 TR-201063TR-201063TR-201063TR-201063TR-201063
0,530,530,530,530,53 15 0,50 -20 to 260/280 TR-200515TR-200515TR-200515TR-200515TR-20051515 1,00 -20 to 260/280 TR-201015TR-201015TR-201015TR-201015TR-201015
30 0,50 -20 to 260/280 TR-200535TR-200535TR-200535TR-200535TR-20053530 1,00 -20 to 260/280 TR-201035TR-201035TR-201035TR-201035TR-201035
60 0,50 -20 to 260/280 TR-200565TR-200565TR-200565TR-200565TR-200565
60 1,00 -20 to 260/280 TR-201065TR-201065TR-201065TR-201065TR-201065
TRB-20
(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inked(20%) Diphenyl-(80%) Dimethylpolysi l ioxane, bonded and crossl inkedphase.phase.phase.phase.phase.
• (20%) Diphenyl-(80%) dimethylpolysiloxane.
• Column of intermediate polarity without cyanopropyl groups in its structure
• Excellent confirmation column.
TRB-20
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Peak Name
1- Methanol2- Acetaldehyde3- Ethanol4- Isopropanol5- Acetone6- n-Propanol
Retention time
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB-20
Column: TRB-20TRB-20TRB-20TRB-20TRB-20, P/N TR-203035Dimensions: 30m x 0.53mm x 3.0µmInjection: Alcohols in blood, 0.5 µL Head Space, split 5:1, 200ºCCarrier gas: He, constant pressure 10 psi (69Kpa)Oven temperature: 40ºC (isothermal)Detector: FID, 200ºC
TKG 1124
TRB-20 Equ iva lent PhaseTRB-20 Equ iva lent PhaseTRB-20 Equ iva lent PhaseTRB-20 Equ iva lent PhaseTRB-20 Equ iva lent Phase
Supelco:Supelco:Supelco:Supelco:Supelco: SPB-20, VOCOLAlltechAl ltechAl ltechAl ltechAl ltech: AT-20Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-502
35
TRB-35TRB-35
(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inked(35%) Diphenyl (65%) Dimethylpolysi l ioxane, bonded and crossl inkedphase.phase.phase.phase.phase.
• (35%) Diphenyl-(65%) dimethylpolysiloxane.
• Column of intermediate polarity without cyanopropyl groups in its structure.
• Excellent confirmation column.
TRB -35 Equ iva lent PhaseTRB-35 Equ iva lent PhaseTRB-35 Equ iva lent PhaseTRB-35 Equ iva lent PhaseTRB-35 Equ iva lent Phase
Agilent: Agi lent: Agi lent: Agi lent: Agi lent: HP-35, DB-35Supelco:Supelco:Supelco:Supelco:Supelco: SPB-35RestekRestekRestekRestekRestek: Rtx-35SGE:SGE:SGE:SGE:SGE: BPX-35AlltechAl ltechAl ltechAl ltechAl ltech: AT-35Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-11
TRB-35InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,15 -20 to 300/320 TR-351312TR-351312TR-351312TR-351312TR-351312
15 0,25 -20 to 300/320 TR-350212TR-350212TR-350212TR-350212TR-35021230 0,15 -20 to 300/320 TR-351332TR-351332TR-351332TR-351332TR-351332
30 0,25 -20 to 300/320 TR-350232TR-350232TR-350232TR-350232TR-35023260 0,15 -20 to 300/320 TR-351362TR-351362TR-351362TR-351362TR-351362
60 0,25 -20 to 300/320 TR-350262TR-350262TR-350262TR-350262TR-350262
0,320,320,320,320,32 15 0,15 -20 to 300/320 TR-351313TR-351313TR-351313TR-351313TR-35131315 0,25 -20 to 300/320 TR-350213TR-350213TR-350213TR-350213TR-350213
15 0,50 -20 to 290/310 TR-350513TR-350513TR-350513TR-350513TR-350513
30 0,15 -20 to 300/320 TR-351333TR-351333TR-351333TR-351333TR-35133330 0,25 -20 to 300/320 TR-350233TR-350233TR-350233TR-350233TR-350233
30 0,50 -20 to 290/310 TR-350533TR-350533TR-350533TR-350533TR-350533
60 0,15 -20 to 300/320 TR-351363TR-351363TR-351363TR-351363TR-35136360 0,25 -20 to 300/320 TR-350263TR-350263TR-350263TR-350263TR-350263
60 0,50 -20 to 290/310 TR-350563TR-350563TR-350563TR-350563TR-350563
0,530,530,530,530,53 15 0,50 -20 to 260/280 TR-350515TR-350515TR-350515TR-350515TR-35051515 1,00 -20 to 260/280 TR-351015TR-351015TR-351015TR-351015TR-351015
30 0,50 -20 to 260/280 TR-350535TR-350535TR-350535TR-350535TR-350535
30 1,00 -20 to 260/280 TR-351035TR-351035TR-351035TR-351035TR-35103560 0,50 -20 to 260/280 TR-350565TR-350565TR-350565TR-350565TR-350565
60 1,00 -20 to 260/280 TR-351065TR-351065TR-351065TR-351065TR-351065
1
2
3
4 5
67
8
9
10 11
TRB-35
Column: TRB-35TRB-35TRB-35TRB-35TRB-35, P/N TR-350535Dimensions: 30m x 0.53mm x 0.5µmInjection: 1 µL Grob Test, split 1:25, 260ºCCarrier gas: H2, constant pressure 3 psi (20.7 Kpa)Oven temperature: 40ºC @ 6ºC/min to 280ºC(5min)Detector: FID, 260ºC
Peak Name
1 Methylene chloride2 2,3-Butanediol3 C-104 C-115 1-Octanol6 Nonanal7 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-10 FAME10 C-11 FAME11 C-12 FAME
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TKG 1125
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
3 6
TRB-1701TRB-1701
(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded and(14%) Cyanopropyphenyl-(86%) dimethyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• (14%) Cyanopropyl-phenyl- (86%)dimethylpolysiloxane.
• Intermediate polarity column of wide use.
• Historically used in the analysis of pesticides.
TRB-1701InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 15 0,20 -20 to 280/280 TR-132119TR-132119TR-132119TR-132119TR-132119
30 0,20 -20 to 280/280 TR-132139TR-132139TR-132139TR-132139TR-13213960 0,20 -20 to 280/280 TR-132169TR-132169TR-132169TR-132169TR-132169
0,250,250,250,250,25 15 0,25 -20 to 280/280 TR-130212TR-130212TR-130212TR-130212TR-130212
15 0,50 -20 to 270/280 TR-130512TR-130512TR-130512TR-130512TR-13051215 1,00 -20 to 260/280 TR-131012TR-131012TR-131012TR-131012TR-131012
30 0,10 -20 to 280/280 TR-130132TR-130132TR-130132TR-130132TR-130132
30 0,25 -20 to 280/280 TR-130232TR-130232TR-130232TR-130232TR-13023230 0,50 -20 to 270/280 TR-130532TR-130532TR-130532TR-130532TR-130532
30 1,00 -20 to 260/280 TR-131032TR-131032TR-131032TR-131032TR-131032
60 0,10 -20 to 280/280 TR-130162TR-130162TR-130162TR-130162TR-13016260 0,25 -20 to 280/280 TR-130262TR-130262TR-130262TR-130262TR-130262
60 0,50 -20 to 270/280 TR-130562TR-130562TR-130562TR-130562TR-130562
60 1,00 -20 to 260/280 TR-131062TR-131062TR-131062TR-131062TR-131062
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-1701
Column: TRB-1701TRB-1701TRB-1701TRB-1701TRB-1701, P/N TR-131565Dimensions: 60m x 0.53mm x 1.5µmInjection: 1 µL standard SP-4-7301, split 1:50, 260ºCCarrier gas: H2, constant pressure 6.2 psi (42.7 Kpa)Oven temperature: 130ºCDetector: FID, 280ºC
Peak Name
1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 C-127 2,6-Dimethylphenol9 C-138 2,6-Dimethylaniline10 C-14
TRB-225
(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded and(50%) Cyanopropylphenyl - (50%) dimethyl polysi loxane, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• (50%) Cyanopropylphenyl - (50%) dimethyl polysiloxane.
• Medium/high polarity column.
• Excellent for separating cis-trans isomers of FAMES and sugar derivatives.
Structure of Poly(dimethylcyanopropylphenyl)siloxane
Si OO SiCH3
CH3
CH2)3CN
O(
m n
TRB-225
TKG 1126
TRB -225 Equ iva lent PhaseTRB-225 Equ iva lent PhaseTRB-225 Equ iva lent PhaseTRB-225 Equ iva lent PhaseTRB-225 Equ iva lent Phase
Agilent: Agilent: Agilent: Agilent: Agilent: HP-225, DB-225RestekRestekRestekRestekRestek: Rtx-225VVVVVarian:arian:arian:arian:arian: CP-SIL 43 CBSGE:SGE:SGE:SGE:SGE: BP-225AlltechAl ltechAl ltechAl ltechAl ltech: AT-225Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-225
Structure of Poly(dimethylcyanopropylphenyl)siloxane
Si OO SiCH3
CH3
CH2)3CN
O(
m n
TRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent PhaseTRB -1701 Equ iva lent Phase
Agilent: Agilent: Agilent: Agilent: Agilent: HP-1701, PAS-1701, DB-1701Supelco:Supelco:Supelco:Supelco:Supelco: SPB-1701RestekRestekRestekRestekRestek: Rtx-1701VVVVVarianar ianar ianar ianar ian: CP-SIL 19 CBSGE:SGE:SGE:SGE:SGE: BP-10AlltechAl ltechAl ltechAl ltechAl ltech: AT-1701Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-1701
37
TRB-225
Column: TRB-225TRB-225TRB-225TRB-225TRB-225, P/N TR-251332Dimensions: 30m x 0.25mm x 0.15µmInjection: 1 µL standard SP-4-7301, split 1:50, 260ºCCarrier gas: H2, constant pressure 12 psi (82.7 Kpa)Oven temperature: 110ºCDetector: FID, 280ºC
Peak Name
1 Methylene chloride2 C-103 C-114 C-125 2-Octanone6 C-137 1-Octanol8 C-149 2,6-Dimethylphenol10 2,6-Dimethylaniline
TRB-225 TRB-50TRB-50
(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inked(50%) Diphenyl-(50%) dimethyl polysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.
• (50%) Diphenyl-(50%) dimethyl polysiloxane.
• Medium polarity column.
• Excellent column for confirmation of TRB-5 analyses.
TRB-50InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,15 0 to 300/320 TR-501312TR-501312TR-501312TR-501312TR-50131215 0,25 0 to 300/320 TR-500212TR-500212TR-500212TR-500212TR-500212
15 0,50 0 to 290/310 TR-500512TR-500512TR-500512TR-500512TR-500512
30 0,15 0 to 300/320 TR-501332TR-501332TR-501332TR-501332TR-501332
30 0,25 0 to 300/320 TR-500232TR-500232TR-500232TR-500232TR-500232
30 0,50 0 to 290/310 TR-500532TR-500532TR-500532TR-500532TR-500532
60 0,15 0 to 300/320 TR-501362TR-501362TR-501362TR-501362TR-501362
60 0,25 0 to 300/320 TR-500262TR-500262TR-500262TR-500262TR-500262
60 0,50 0 to 290/310 TR-500562TR-500562TR-500562TR-500562TR-500562
0,320,320,320,320,32 15 0,15 0 to 300/320 TR-501313TR-501313TR-501313TR-501313TR-501313
15 0,25 0 to 300/320 TR-500213TR-500213TR-500213TR-500213TR-500213
15 0,50 0 to 290/310 TR-500513TR-500513TR-500513TR-500513TR-500513
30 0,15 0 to 300/320 TR-501333TR-501333TR-501333TR-501333TR-501333
30 0,25 0 to 300/320 TR-500233TR-500233TR-500233TR-500233TR-500233
30 0,50 0 to 290/310 TR-500533TR-500533TR-500533TR-500533TR-500533
60 0,15 0 to 300/320 TR-501363TR-501363TR-501363TR-501363TR-501363
60 0,25 0 to 300/320 TR-500263TR-500263TR-500263TR-500263TR-500263
60 0,50 0 to 290/310 TR-500563TR-500563TR-500563TR-500563TR-500563
0,530,530,530,530,53 15 0,50 0 to 270/290 TR-500515TR-500515TR-500515TR-500515TR-500515
15 1,00 0 to 260/280 TR-501015TR-501015TR-501015TR-501015TR-501015
30 0,50 0 to 270/290 TR-500535TR-500535TR-500535TR-500535TR-500535
30 1,00 0 to 260/280 TR-501035TR-501035TR-501035TR-501035TR-501035
60 0,50 0 to 270/290 TR-500565TR-500565TR-500565TR-500565TR-500565
60 1,00 0 to 260/280 TR-501065TR-501065TR-501065TR-501065TR-501065
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TKG 1127
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-50 Equ iva lent PhaseTRB-50 Equ iva lent PhaseTRB-50 Equ iva lent PhaseTRB-50 Equ iva lent PhaseTRB-50 Equ iva lent Phase
Agilent: Agi lent: Agi lent: Agi lent: Agi lent: HP-50, +DB-17, DB-608SupelcoSupelcoSupelcoSupelcoSupelco: SPB-50, SPB-2250RestekRestekRestekRestekRestek: Rtx-50VVVVVarian:arian:arian:arian:arian: CP-SIL 24 CBAlltechAl ltechAl ltechAl ltechAl ltech: AT-50Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-17
TRB-225InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 15 0,20 40 to 220/240 TR-252119TR-252119TR-252119TR-252119TR-252119
30 0,20 40 to 220/240 TR-252139TR-252139TR-252139TR-252139TR-252139
0,250,250,250,250,25 15 0,15 40 to 220/240 TR-251312TR-251312TR-251312TR-251312TR-251312
15 0,25 40 to 220/240 TR-250212TR-250212TR-250212TR-250212TR-250212
30 0,15 40 to 220/240 TR-251332TR-251332TR-251332TR-251332TR-25133230 0,25 40 to 220/240 TR-250232TR-250232TR-250232TR-250232TR-250232
0,320,320,320,320,32 15 0,15 40 to 220/240 TR-251313TR-251313TR-251313TR-251313TR-251313
15 0,25 40 to 220/240 TR-250213TR-250213TR-250213TR-250213TR-25021330 0,15 40 to 220/240 TR-251333TR-251333TR-251333TR-251333TR-251333
30 0,25 40 to 220/240 TR-250233TR-250233TR-250233TR-250233TR-250233
0,530,530,530,530,53 15 1,00 40 to 200/220 TR-251015TR-251015TR-251015TR-251015TR-251015
30 1,00 40 to 200/220 TR-251035TR-251035TR-251035TR-251035TR-251035
3 8
Structure of Poly(dimethyldiphenyl)siloxane
m n
Si OO SiCH3
CH3O
TRB-50ht
Column: TRB-50htTRB-50htTRB-50htTRB-50htTRB-50ht, P/N TR-531312Dimensions: 15m x 0.25mm x 0.15mmInjection: 0.2mL Triglycerides Palm Oil in Isooctane(50 mg/mL), split 1:12Carrier gas: H2, constant pressure, 9psi (56 KPa)Oven temperature: 340ºC(1min)@0.5ºC/min to 355ºC(5min)Injector: 380ºC (high temperature septum)Detector: FID, 380ºC
Peak Name
1 D322 D343 D364 MPP5 MOM6 PPP7 MOP8 MLP9 PPS10 POP11 MOO12 PLP13 MLO14 PSS15 POS16 POO17 PLS18 PLO19 PLL20 SOS21 SOO22 OOO23 SLO24 OLO25 OLL26 SOA27 AOO
12
3
4
5
610
7
8
9
11
1314
15
16
17
18
19 2021
22
2324
25 26 27
12
Structure of Poly(methyltrifluoroproyl)siloxane
n
(CH2)2CF3
O Si OCH3
TKG 1128
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-50htTRB-50ht
(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase(50%) Diphenyl-(50%) dimethylpolysi loxane, bonded and crossl inked phase
• (50%) Diphenyl-(50%) dimethylpolysiloxane.
• Medium polarity column with high thermal stability.
• Best column for triglycerides analysis.
TRB-F50(50%) T(50%) T(50%) T(50%) T(50%) Trif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedrif luoropropyl-(50%) Methylpolysi loxane, bonded and crossl inkedphase.phase.phase.phase.phase.
• (50%) Trifluoropropyl-(50%) Methylpolysiloxane.
• High polarity column.
• Column designed for the EPA 609 and 8140 methods.
TRB -50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent PhaseTRB-50ht Equ iva lent Phase
Agilent: Agi lent: Agi lent: Agi lent: Agilent: DB17htRestekRestekRestekRestekRestek: Rtx-65VVVVVarian:arian:arian:arian:arian: TAB-CBQuadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-65HT
TRB-50htInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,10 50 to 370 TR-530112TR-530112TR-530112TR-530112TR-530112
15 0,15 50 to 370 TR-531312TR-531312TR-531312TR-531312TR-531312
30 0,10 50 to 370 TR-530132TR-530132TR-530132TR-530132TR-530132
30 0,15 50 to 370 TR-531332TR-531332TR-531332TR-531332TR-531332
TRB-F50InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,15 45 to 240/260 TR-571312TR-571312TR-571312TR-571312TR-57131215 0,25 45 to 240/260 TR-570212TR-570212TR-570212TR-570212TR-570212
15 0,50 45 to 240/260 TR-570512TR-570512TR-570512TR-570512TR-570512
30 0,15 45 to 240/260 TR-571332TR-571332TR-571332TR-571332TR-57133230 0,25 45 to 240/260 TR-570232TR-570232TR-570232TR-570232TR-570232
30 0,50 45 to 240/260 TR-570532TR-570532TR-570532TR-570532TR-570532
0,320,320,320,320,32 15 0,15 45 to 240/260 TR-571313TR-571313TR-571313TR-571313TR-57131315 0,25 45 to 240/260 TR-570213TR-570213TR-570213TR-570213TR-570213
15 0,50 45 to 240/260 TR-570513TR-570513TR-570513TR-570513TR-570513
30 0,15 45 to 240/260 TR-571333TR-571333TR-571333TR-571333TR-57133330 0,25 45 to 240/260 TR-570233TR-570233TR-570233TR-570233TR-570233
30 0,50 45 to 240/260 TR-570533TR-570533TR-570533TR-570533TR-570533
0,530,530,530,530,53 15 1,00 45 to 220/240 TR-571015TR-571015TR-571015TR-571015TR-571015
30 1,00 45 to 220/240 TR-571035TR-571035TR-571035TR-571035TR-571035
39
TRB-F50
Column: TRB-F50TRB-F50TRB-F50TRB-F50TRB-F50, P/N TR-570533Dimensions: 30m x 0.32mm x 0.5µmInjection: 1µL standard SP-4-7301 (500 ng/mL comp), split 1:50, 260ºCCarrier gas: H2, constant pressure, 7psi (48.2 KPa)Oven temperature: 100ºCDetector: FID, 280ºC Peak Name
1 Methylene chloride2 C-103 C-114 C-125 1-Octanol6 C-137 2-Octanone8 2,6-Dimethylphenol9 C-1410 2,6-Dimethylaniline
12
3
4
56
8
7
9
10
TRB-PAG
Column: TRB-PTRB-PTRB-PTRB-PTRB-PAGAGAGAGAG, P/N TR-550232Dimensions: 30m x 0.25mm x 0.25µmInjectionn: 1 µL Test Grob, split 1:25, 260ºCCarrier gas: H2, constant pressure 11 psi(75.8 Kpa)Oven temperature: 40ºC @ 6ºC/min to230ºC(5min)Detector: FID, 260ºC
1
2
3
4
5 6
7
9
1011
8
12
Peak Name
1 C-102 C-113 Nonanal4 2,3-Butanediol5 1-Octanol6 C-10 FAME7 Dicyclohexylamine8 2,6-Dimethylaniline9 C-11 FAME10 2,6-Dimethylphenol11 C-12 FAME12 2-Ethyl hexanoic acid
TKG 1129
TKG 1130
TRB-F50
50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylen50% Polyethylene -50% polypropylene e e e e glycol, glycol, glycol, glycol, glycol, bonded and bonded and bonded and bonded and bonded and crosslinkedcrosslinkedcrosslinkedcrosslinkedcrosslinked phase. phase. phase. phase. phase.
• (50%) Polyethylene-(50%) polypropylene glycol.
• Phase polarity slightly lower than TRB-WAX due to the inclusion of groups ofpropylene oxide.
• Polarity similar to UCON phase.
TRB-PAG
TRB-PAGInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,25 30 to 220/230 TR-550212TR-550212TR-550212TR-550212TR-550212
30 0,25 30 to 220/230 TR-550232TR-550232TR-550232TR-550232TR-55023260 0,25 30 to 220/230 TR-550262TR-550262TR-550262TR-550262TR-550262
0,320,320,320,320,32 15 0,25 30 to 220/230 TR-550213TR-550213TR-550213TR-550213TR-550213
30 0,25 30 to 220/230 TR-550233TR-550233TR-550233TR-550233TR-55023360 0,25 30 to 220/230 TR-550263TR-550263TR-550263TR-550263TR-550263
0,530,530,530,530,53 15 0,50 30 to 220/230 TR-550515TR-550515TR-550515TR-550515TR-550515
30 0,50 30 to 220/230 TR-550535TR-550535TR-550535TR-550535TR-55053560 0,50 30 to 220/230 TR-550565TR-550565TR-550565TR-550565TR-550565
Structure of Poly(ethylenepropylene)glycol
CH2 CH2 OOm
CH2 CH2 OCH2 n
TTTTT e k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m ae k n o k r o m a C a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a rC a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent PhaseTRB-F50 Equ iva lent Phase
Agilent: Agi lent: Agi lent: Agi lent: Agilent: DB-210, DB-200RestekRestekRestekRestekRestek: Rtx-200Alltech:Al ltech:Al ltech:Al ltech:Al ltech: AT-210Quadrex:Quadrex:Quadrex:Quadrex:Quadrex: 007-210
TRB -PTRB -PTRB -PTRB -PTRB -PAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent PhaseAG Equ iva lent Phase
Supe l c oSupe l c oSupe l c oSupe l c oSupe l c o: PAG
4 0
TKG 1131
TRB-WAXTRB-WAX
(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.(100%) polyethylene glycol, bonded and cross- l inked phase.
• 100% Polyethylene glycol (PEG).
• High polarity column.
• Wide range of working temperatures and high thermal stability (270º C)
• Ideal for separating alcohols, aldehydes, ketones and aromatic isomers (BTX)
Structure of Polyethylene glycol
CH2 CH2 OOm
TRB-WAXInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,100,100,100,100,10 10 0,10 40 to 260/270 TR-140141TR-140141TR-140141TR-140141TR-140141
10 0,20 40 to 260/270 TR-142141TR-142141TR-142141TR-142141TR-142141
20 0,10 40 to 260/270 TR-140181TR-140181TR-140181TR-140181TR-140181
20 0,20 40 to 260/270 TR-142181TR-142181TR-142181TR-142181TR-142181
0,200,200,200,200,20 15 0,20 40 to 260/270 TR-142119TR-142119TR-142119TR-142119TR-142119
15 0,40 40 to 260/270 TR-140419TR-140419TR-140419TR-140419TR-140419
30 0,20 40 to 260/270 TR-142139TR-142139TR-142139TR-142139TR-142139
30 0,40 40 to 260/270 TR-140439TR-140439TR-140439TR-140439TR-140439
60 0,20 40 to 260/270 TR-142169TR-142169TR-142169TR-142169TR-142169
60 0,40 40 to 260/270 TR-140469TR-140469TR-140469TR-140469TR-140469
0,250,250,250,250,25 15 0,10 40 to 260/270 TR-140112TR-140112TR-140112TR-140112TR-140112
15 0,25 40 to 260/270 TR-140212TR-140212TR-140212TR-140212TR-140212
15 0,50 40 to 260/270 TR-140512TR-140512TR-140512TR-140512TR-140512
30 0,10 40 to 260/270 TR-140132TR-140132TR-140132TR-140132TR-140132
30 0,25 40 to 260/270 TR-140232TR-140232TR-140232TR-140232TR-140232
30 0,50 40 to 260/270 TR-140532TR-140532TR-140532TR-140532TR-140532
30 1,00 40 to 260/270 TR-141032TR-141032TR-141032TR-141032TR-141032
60 0,10 40 to 260/270 TR-140162TR-140162TR-140162TR-140162TR-140162
60 0,25 40 to 260/270 TR-140262TR-140262TR-140262TR-140262TR-140262
60 0,50 40 to 260/270 TR-140562TR-140562TR-140562TR-140562TR-140562
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 15 0,10 40 to 260/270 TR-140113TR-140113TR-140113TR-140113TR-140113
15 0,25 40 to 260/270 TR-140213TR-140213TR-140213TR-140213TR-140213
15 0,50 40 to 260/270 TR-140513TR-140513TR-140513TR-140513TR-140513
30 0,10 40 to 260/270 TR-140133TR-140133TR-140133TR-140133TR-140133
30 0,25 40 to 260/270 TR-140233TR-140233TR-140233TR-140233TR-140233
30 0,50 40 to 260/270 TR-140533TR-140533TR-140533TR-140533TR-140533
50 1,20 40 to 230/240 TR-141253TR-141253TR-141253TR-141253TR-141253
60 0,10 40 to 260/270 TR-140163TR-140163TR-140163TR-140163TR-140163
60 0,25 40 to 260/270 TR-140263TR-140263TR-140263TR-140263TR-140263
60 0,50 40 to 260/270 TR-140563TR-140563TR-140563TR-140563TR-140563
60 1,00 40 to 230/240 TR-141063TR-141063TR-141063TR-141063TR-141063
60 1,20 40 to 230/240 TR-141263TR-141263TR-141263TR-141263TR-141263
100 1,00 40 to 230/240 TR-141093TR-141093TR-141093TR-141093TR-141093
0,530,530,530,530,53 10 1,00 40 to 240/250 TR-141045TR-141045TR-141045TR-141045TR-141045
15 1,00 40 to 240/250 TR-141015TR-141015TR-141015TR-141015TR-141015
30 1,00 40 to 240/250 TR-141035TR-141035TR-141035TR-141035TR-141035
30 1,33 40 to 240/250 TR-141735TR-141735TR-141735TR-141735TR-141735
30 2,00 40 to 240/250 TR-142035TR-142035TR-142035TR-142035TR-142035
60 1,00 40 to 240/250 TR-141065TR-141065TR-141065TR-141065TR-141065
60 2,00 40 to 240/250 TR-142065TR-142065TR-142065TR-142065TR-142065
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
TRB-WAX
Column: TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX, P/N TR-140262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Test SP-4-7302 (500 ng/mL comp.),split 1:25, 260ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 155ºC (Isothermal)Detector: FID, 280ºC
Peak Name
1 Methylene chloride2 2-Octanone3 C-154 1-Octanol5 C-166 C-177 C-188 2,6-Dimethylaniline9 2,6-Dimethylphenol10 C-20
TRB -WTRB -WTRB -WTRB -WTRB -WAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-20M, INNOWAX, DB-WAX, DBWAXetrS upe l c oSupe l c oSupe l c oSupe l c oSupe l c o: SUPELCOWAX-10, Carbowax 20MRe s t e kRe s t e kRe s t e kRe s t e kRe s t e k: STABILWAXVVVVVa r i aa r i aa r i aa r i aa r i an: CP-WAX 52CBS G ES G ES G ES G ES G E: BP-20A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-WAX
41
TRB-FFAP
Column: TRB-FFTRB-FFTRB-FFTRB-FFTRB-FFAPAPAPAPAP, P/N TR-150262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Test SP-4-7302 (500 ng/mL comp.),split 1:100, 260ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 155ºCDetector: FID, 280ºC Peak Name
1 Methylene chloride2 2-Octanone3 C-154 1-Octanol5 C-166 C-177 C-188 2,6-Dimethylaniline9 2,6-Dimethylphenol10 C-20
TKG 1132
TRB-FFAPInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 15 0,30 40 to 240/250 TR-152119TR-152119TR-152119TR-152119TR-15211930 0,30 40 to 240/250 TR-152139TR-152139TR-152139TR-152139TR-152139
60 0,30 40 to 240/250 TR-152169TR-152169TR-152169TR-152169TR-152169
0,250,250,250,250,25 15 0,25 40 to 240/250 TR-150212TR-150212TR-150212TR-150212TR-15021230 0,25 40 to 240/250 TR-150232TR-150232TR-150232TR-150232TR-150232
60 0,25 40 to 240/250 TR-150262TR-150262TR-150262TR-150262TR-150262
0,320,320,320,320,32 15 0,25 40 to 240/250 TR-150213TR-150213TR-150213TR-150213TR-15021315 0,50 40 to 240/250 TR-150513TR-150513TR-150513TR-150513TR-150513
30 0,25 40 to 240/250 TR-150233TR-150233TR-150233TR-150233TR-150233
30 0,50 40 to 240/250 TR-150533TR-150533TR-150533TR-150533TR-15053360 0,25 40 to 240/250 TR-150263TR-150263TR-150263TR-150263TR-150263
60 0,50 40 to 240/250 TR-150563TR-150563TR-150563TR-150563TR-150563
0,530,530,530,530,53 15 0,50 40 to 240/250 TR-150515TR-150515TR-150515TR-150515TR-150515
15 1,00 40 to 230/240 TR-151015TR-151015TR-151015TR-151015TR-151015
30 0,50 40 to 240/250 TR-150535TR-150535TR-150535TR-150535TR-15053530 1,00 40 to 230/240 TR-151035TR-151035TR-151035TR-151035TR-151035
60 0,50 40 to 240/250 TR-150565TR-150565TR-150565TR-150565TR-150565
60 1,00 40 to 230/240 TR-151065TR-151065TR-151065TR-151065TR-151065
TRB-FFAP
TRB-FFAP
Polyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andPolyethylene glycol esterif ied with nitroterephtalic acid, bonded andcrossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.crossl inked phase.
• 100% Polyethylene glycol (PEG) esterified with nitroterephthalic acid.
• Ideal for analysis of free acids (without derivatization), phenols and glycols.
• High thermal stability (250ºC)
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Structure of Polyethylene glycol
CH2 CH2 OOm
TRB -FFTRB -FFTRB -FFTRB -FFTRB -FFAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent PhaseAP Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-FFAP, DB-FFAPSupe l c oSupe l c oSupe l c oSupe l c oSupe l c o: NUKOL, SP-1000Re s t e kRe s t e kRe s t e kRe s t e kRe s t e k: STABILWAX-DAVVVVVa r i aa r i aa r i aa r i aa r i an: CP-WAX 58 CBS G ES G ES G ES G ES G E: BP-21A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h :A l l t e c h : AT-1000, FFAPQuad r e xQuad r e xQuad r e xQuad r e xQuad r e x: 007-FFAP
4 2
TRB-WAX.DB
Column: TRB-WTRB-WTRB-WTRB-WTRB-WAX.AX.AX.AX.AX.DBDBDBDBDB, P/N TR-932162Dimensions: 60m x 0.25mm x 0.20µmInjection: 1 µL Test SP-4-8278 (500 ng/mL comp.), split1:50, 260ºCCarrier gas: H2, constantpressure 24 psi (168 Kpa)Oven temperature: 120ºC (isothermal)Detector: FID, 280ºC
Peak Name1 Tert-butylmethylether2 N-octylamine3 N-nonylamine4 C-155 N-decylamine6 C-167 Benzylamine8 C-179 Tri-n-hexylamine10 C-1811 2,6-Dimethylaniline12 2,4-Dimethylaniline13 C-20
TKG 1133
TRB-WAXOmega
TRB-WAX. DB
(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.(100%) Polyethylene glycol, nonbonded phase.
• 100% basic deactivated Polyethylene glycol (PEG).
• Excellent for analysing basic nonderivatized compounds
• Ideal for separating amines and nitrosamines.
Structure of Polyethylene glycol
CH2 CH2 OOm
TRB -WTRB -WTRB -WTRB -WTRB -WAX .AX .AX .AX .AX .D BD BD BD BD B Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: CAM, HP-BasicWaxVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-WAX 51SupelcoSupelcoSupelcoSupelcoSupelco: Carbowax-AmineRestekRestekRestekRestekRestek: Stabilwax-DB
TRB-WAX.DBInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,20 60 to 210/220 TR-932112TR-932112TR-932112TR-932112TR-932112
15 0,25 60 to 210/220 TR-930212TR-930212TR-930212TR-930212TR-930212
30 0,20 60 to 210/220 TR-932132TR-932132TR-932132TR-932132TR-93213230 0,25 60 to 210/220 TR-930232TR-930232TR-930232TR-930232TR-930232
30 0,50 60 to 210/220 TR-930532TR-930532TR-930532TR-930532TR-930532
60 0,20 60 to 210/220 TR-932162TR-932162TR-932162TR-932162TR-932162
0,320,320,320,320,32 15 0,25 60 to 210/220 TR-930213TR-930213TR-930213TR-930213TR-930213
30 0,25 60 to 210/220 TR-930233TR-930233TR-930233TR-930233TR-93023330 0,50 60 to 210/220 TR-930533TR-930533TR-930533TR-930533TR-930533
30 1,00 60 to 210/220 TR-931033TR-931033TR-931033TR-931033TR-931033
60 1,00 60 to 210/220 TR-931063TR-931063TR-931063TR-931063TR-931063
0,530,530,530,530,53 15 1,00 60 to 210/220 TR-931015TR-931015TR-931015TR-931015TR-931015
30 0,50 60 to 210/220 TR-930535TR-930535TR-930535TR-930535TR-93053530 1,00 60 to 210/220 TR-931035TR-931035TR-931035TR-931035TR-931035
30 1,50 60 to 210/220 TR-931535TR-931535TR-931535TR-931535TR-931535
60 1,00 60 to 210/220 TR-931065TR-931065TR-931065TR-931065TR-931065
(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.(100%) Polyethylene glycol, bonded and crossl inked phase.
• 100% Polyethylene glycol (PEG).
• High polarity column
• Specially designed for analysis of Omega 3 and Omega 6 fatty acids methylesters.
Structure of Polyethylene glycol
CH2 CH2 OOm
TRB-WAXOmegaInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 30 0,25 40 to 260/270 TR-840232TR-840232TR-840232TR-840232TR-840232
0,320,320,320,320,32 30 0,25 40 to 260/270 TR-840233TR-840233TR-840233TR-840233TR-840233
0,530,530,530,530,53 30 0,50 40 to 260/270 TR-840535TR-840535TR-840535TR-840535TR-840535
TRB-WAX.DB
TRB -WTRB -WTRB -WTRB -WTRB -WAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t PhaseAXOmega Equ iva len t Phase
SupelcoSupelcoSupelcoSupelcoSupelco: OmegawaxRestekRestekRestekRestekRestek: Famewax
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
43
TRB-WAXOmega
Column: TR-WTR-WTR-WTR-WTR-WAXOmegaAXOmegaAXOmegaAXOmegaAXOmega, P/N TR-840233Dimensions: 30m x 0.32mm x 0.25µmInjection: 1µL test SP-4-8476, split 1:90, 250ºCCarrier gas: H2, 9.5 psi (65.4 KPa)Oven temperature: 200ºC (Isothermal)Detector: FID, 260ºC
Peak Name
1- C14:02- C16:03- C18:04- C18:1n95- C18:1n76- C18:2n67- C18:4n38- C20:09- C20:5n3 (EPA)10- C22:011- C21:5n312- C23:013- C22:5n314- C24:015- C22:6n3 (DHA)16- C24:1n9
12
3
4
6
57
8
9 EP
A
1011
12
13 14 16
15 D
HA
TKG 1134
Meta.WAX
TRB-WAXOmega
(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.(100%) Polyethylene glycol, bonded and cross- l inked phase.
• 100% Polyethylene glycol (PEG).
• High polarity column.
• Minimum operating temperature 20º C.
• Designed for analyzing volatiles in alcoholic beverages.
• Excellent symmetry for aldehyde and glycol peaks.
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Structure of Polyethylene glycol
CH2 CH2 OOm
Meta.WAXInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,10 20 to 240/250 TR-810112TR-810112TR-810112TR-810112TR-81011215 0,25 20 to 240/250 TR-810212TR-810212TR-810212TR-810212TR-810212
15 0,50 20 to 240/250 TR-810512TR-810512TR-810512TR-810512TR-810512
30 0,10 20 to 240/250 TR-810132TR-810132TR-810132TR-810132TR-81013230 0,25 20 to 240/250 TR-810232TR-810232TR-810232TR-810232TR-810232
30 0,50 20 to 240/250 TR-810532TR-810532TR-810532TR-810532TR-810532
60 0,20 20 to 240/250 TR-812162TR-812162TR-812162TR-812162TR-81216260 0,25 20 to 240/250 TR-810262TR-810262TR-810262TR-810262TR-810262
0,320,320,320,320,32 15 0,25 20 to 240/250 TR-810213TR-810213TR-810213TR-810213TR-81021315 0,50 20 to 240/250 TR-810513TR-810513TR-810513TR-810513TR-810513
15 1,00 20 to 230/240 TR-811013TR-811013TR-811013TR-811013TR-811013
30 0,25 20 to 240/250 TR-810233TR-810233TR-810233TR-810233TR-81023330 0,50 20 to 240/250 TR-810533TR-810533TR-810533TR-810533TR-810533
30 1,00 20 to 230/240 TR-811033TR-811033TR-811033TR-811033TR-811033
60 0,25 20 to 240/250 TR-810263TR-810263TR-810263TR-810263TR-81026360 0,50 20 to 240/250 TR-810563TR-810563TR-810563TR-810563TR-810563
60 0,64 20 to 240/250 TR-816463TR-816463TR-816463TR-816463TR-81646360 1,00 20 to 230/240 TR-811063TR-811063TR-811063TR-811063TR-811063
0,530,530,530,530,53 15 1,20 20 to 230/240 TR-811215TR-811215TR-811215TR-811215TR-811215
30 1,20 20 to 230/240 TR-811235TR-811235TR-811235TR-811235TR-811235
Me ta .WMeta .WMeta .WMeta .WMeta .WAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent PhaseAX Equ iva lent Phase
Ag i l e n tA g i l e n tA g i l e n tA g i l e n tA g i l e n t: HP-WAX, DB-WAXVVVVVa r i a na r i a na r i a na r i a na r i a n: CP-WAX 57 CBRestekRestekRestekRestekRestek: Rtx-WAX
4 4
TKG 1135
TR-CN100(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase(100%) Cyanopropyl polysi loxane, nonbonded phase
• 100% Cyanopropyl polysiloxane.
• Column of maximum polarity.
• Designed for separating fatty acids methyl esters (FAMEs)
• High selectivity towards cis-trans isomers of FAMEs.
TR-CN100InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 15 0,20 0 to 240/250 TR-882112TR-882112TR-882112TR-882112TR-88211230 0,20 0 to 240/250 TR-882132TR-882132TR-882132TR-882132TR-882132
60 0,20 0 to 240/250 TR-882162TR-882162TR-882162TR-882162TR-882162
0,320,320,320,320,32 15 0,20 0 to 240/250 TR-882113TR-882113TR-882113TR-882113TR-882113
30 0,20 0 to 240/250 TR-882133TR-882133TR-882133TR-882133TR-882133
60 0,20 0 to 240/250 TR-882163TR-882163TR-882163TR-882163TR-882163
0,530,530,530,530,53 15 0,20 0 to 225/250 TR-882115TR-882115TR-882115TR-882115TR-882115
30 0,20 0 to 225/250 TR-882135TR-882135TR-882135TR-882135TR-882135
60 0,20 0 to 225/250 TR-882165TR-882165TR-882165TR-882165TR-882165
TR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent PhaseTR -CN100 Equ iva lent Phase
SupelcoSupelcoSupelcoSupelcoSupelco: SP-2340, SP-2380RestekRestekRestekRestekRestek: Rt-2340, Rt-2330VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-SIL 88
Meta.WAX
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
Meta.WAX
Column: Meta.WMeta.WMeta.WMeta.WMeta.WAXAXAXAXAX, P/N TR-810532Dimensions: 30m x 0.25mm x 0.5µmInjection: 1µL Standard Alcohols, split 1:25, 260ºCCarrier gas: He, 12 psi (82.7 KPa)Oven temperature: 35ºC(10min) @ 8ºC/min to 220ºC (15min)Detector: FID, 260ºC
Peak Name
1- Acetaldehyde2- Methyl acetate3- Acetal4- Ethyl acetate5- Methanol6- Ethanol7- Ethyl butyrate8- 2-Butanol9- n-Propanol10- Isobutanol11- 1-Butanol12- 4-Methyl-2-pentanol (I. St.)13- Ethyl hexanoate14- 2-Methyl-1-butanol15- 3-Methyl-1-butanol16- Hexanol17- Ethyl lactate18- Ethyl octanoate19- Benzaldehyde20- Ethyl nonanoate21- Ethyl decanoate22- 4-Ethylphenol
Structure of Poly(biscyanopropyl)siloxane
n(CH2)3CN
(CH2)3CN
Si OO
n
45
TR-CN100
Column: TR-CN100TR-CN100TR-CN100TR-CN100TR-CN100, P/N TR-882162Dimensions: 60m x 0.25mm x 0.20µmInyection: 1µL SP-47885 FAMES (10 mg/mL), split 1:100, 260ºCCarrier gas: He, 20.15 cm/s to 185ºCOven temperature: 90ºC(7min) @ 5ºC/min to 240ºC(15min)Detector: FID, 260ºC
Peak Name
1- Butyric acid methyl ester (C4:0)2- Caproic acid methyl ester (C6:0)3- Caprylic acid methyl ester (C8:0)4- Capric acid methyl ester (C10:0)5- Undecanoic acid methyl ester (C11:0)6- Lauric acid methyl ester (C12:0)7- Tridecanoic acid methyl ester (C13:0)8- Myristic acid methyl ester (C14:0)9- Myristoleic acid methyl ester (C14:1)10- Pentadecanoic acid methyl ester (C15:0)11- Cis-10-pentadecenoic acid methyl ester (C15:1)12- Palmitic acid methyl ester (C16:0)13- Palmitoleic acid methyl ester (C16:1)14- Heptadecanoic acid methyl ester (C17:0)15- Cis-10-heptadecenoic acid methyl ester (C17:1)16- Stearic acid methyl ester (C18:0)17- Oleic acid methyl ester (C18:1n9c)18- Elaidic acid methyl ester (C18:1n9t)
19- Linoleic acid methyl ester (C18:2n6c)20- Linolelaidic acid methyl ester (C18:2n6t)21- γ-Linolenic acid methyl ester (C18:3n6)22- Linolenic acid methyl ester (C18:3n3)23-Arachidic acid methyl ester (C20:0)24- Cis-11-eicosenoic acid methyl ester (C20:1)25- Cis-11,14-eicosadienoic acid methyl ester (C20:2)26- Cis-8,11,14-eicosatrienoic acid methyl ester (C20:3n6)27- Cis-11,14,17-eicosatrienoic acid methyl ester (C20:3n3)28- Arachidonic acid methyl ester (C20:4n6)29- Cis-5,8,11,14,17-eicosapentaenoic acid methyl ester (C20:5n3)30- Heneicosanoic acid methyl ester (C21:0)31- Behenic acid methyl ester (C22:0)32- Erucic acid methyl ester (C22:1n9)33- Cis-13,16-docosadienoic acid methyl ester (C22:2)34- Cis-4,7,10,13,16,19-docosahexaenoic acid methyl ester(C22:6n3)35- Tricosanoic acid methyl ester (C23:0)36- Lignoceric acid methyl ester (C24:0)37- Nervonic acid methyl ester (C24:1)
1
23
4
5
6
8
8
910
11
12
1314
15
16
18
2019
10
17
21
24
22
25
30
31
26
32 28+3
5
33
36
29
37
34
TKG 1136
TR-CN100
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
4 6
TR-CRESOL
Column: TR-CRESOLTR-CRESOLTR-CRESOLTR-CRESOLTR-CRESOL, P/N TR-712162Dimensions: 60m x 0.25mm x 0.20µmInjection: 1 µL standard Cresols (5000 ng/mL comp.), split 1:25, 150ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 130ºCDetector: FID, 150ºC Peak Name
1 Methylene chloride2 Phenol3 o-Cresol4 2,6-Xylenol5 p-Cresol6 m-Cresol7 o-Ethylphenol8 2,4-Xylenol9 2,5-Xylenol10 2,3-Xylenol11 p-Ethylphenol12 m-Ethylphenol13 3,5-Xylenol14 3,4-Xylenol
1
23
4 5
6
7
8
9
101112
13
14
1
2
3
TR-17
Column: TR-17TR-17TR-17TR-17TR-17 P/N TR-502045Dimensions: 10m X 0,53 mm X 2.0 µmInjector: 260ºCCarrier gas: He, 6.5 psiInjection: 1ml standard, split (1:4)Oven Temperature: 180ºCDetector: FID, 280ºC
Peak Name
1- o-toluensulphonamide2- p-toluensulphonamide3 caffeine
TKG 1137 TKG 1138
TR-CRESOL TR-17TR-CRESOL
PropietarPropietarPropietarPropietarPropietary nonbonded phase.y nonbonded phase.y nonbonded phase.y nonbonded phase.y nonbonded phase.
• Stationary phase of perfectly defined purity.
• Column specially designed for analysis of phenolic compounds (phenols,cresylic acids).
• Derivatization of phenolic compounds is not required to obtain suitableresolution.
• Resolves m-cresol/p-cresol and 2.4-xylenol/2.5-xylenol pairs, which are notseparated with other columns used for this analysis such as TRB-5 andTRB-WAX .
TR-CRESOLInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 30 0,20 130 TR-712132TR-712132TR-712132TR-712132TR-712132
60 0,20 130 TR-712162TR-712162TR-712162TR-712162TR-712162
m n
Si OO SiCH3
CH3O
Structure of Poly(dimethyldiphenyl)siloxane
TR-17
PolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxanePolymethylphenylsiloxane
• Polymethylphenylsiloxane.
• Recommended by pharmacopoeia for determining the impurities of sodiumsaccharin (o-p-toluenesulphonamides).
TR-17InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,530,530,530,530,53 10 2,0 0 to 220/240 TR-502045TR-502045TR-502045TR-502045TR-502045
TR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent PhaseTR -CRESOL Equ iva lent Phase
VVVVVa r i a na r i a na r i a na r i a na r i a n: CP-CRESOL
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s
TR-17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent PhaseTR -17 Equ iva lent Phase
Agilent:Agi lent:Agi lent:Agi lent:Agi lent: HP-17
47
1
2
3
4
56
78
9
Meta.VOC
Column: Meta .VOCMeta .VOCMeta .VOCMeta .VOCMeta .VOC, P/N TR-941863Dimensions: 60m x 0.32mm x 1.8µmInjection: 1 µL Test SP-4-8423(500 ng/mL comp.), split 1:100, 280ºCCarrier gas: H2, constant pressure15psi (103.4 Kpa)Oven temperature: 150ºCDetector: FID, 280ºC Peak Name
1 Methylene chloride2 C-103 2-Octanone4 C-115 1-Octanol6 2,6-Dimethylphenol7 2,6-Dimethylaniline8 C-139 C-14
TKG 1139
Meta.VOCMeta.VOC
ProprietarProprietarProprietarProprietarProprietary bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.
• Developed for analysis of volatile organic compounds (VOC)
• Intermediate polarity column.
Meta.VOCInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,200,200,200,200,20 10 1,20 -20 to 240/250 TR-941249TR-941249TR-941249TR-941249TR-941249
0,250,250,250,250,25 30 1,50 -20 to 240/250 TR-941532TR-941532TR-941532TR-941532TR-941532
60 1,50 -20 to 240/250 TR-941562TR-941562TR-941562TR-941562TR-941562
0,320,320,320,320,32 60 1,80 -20 to 240/250 TR-941863TR-941863TR-941863TR-941863TR-941863
60 3,00 -20 to 240/230 TR-943063TR-943063TR-943063TR-943063TR-943063
0,530,530,530,530,53 30 3,00 -20 to 240/230 TR-943035TR-943035TR-943035TR-943035TR-943035
60 3,00 -20 to 240/230 TR-943065TR-943065TR-943065TR-943065TR-943065
105 3,00 -20 to 240/230 TR-9430K5TR-9430K5TR-9430K5TR-9430K5TR-9430K5
TRB-608
ProprietarProprietarProprietarProprietarProprietary bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.y bonded and crossl inked phase.
• Specifically designed for analysing chlorinated pesticides and PCBs
• Designed for the EPA 508, 608 and 8080 methods.
TRB-608InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 30 0,25 -20 to 300/310 TR-360232TR-360232TR-360232TR-360232TR-360232
0,530,530,530,530,53 15 0,50 -20 to 290/300 TR-360515TR-360515TR-360515TR-360515TR-360515
30 0,50 -20 to 290/300 TR-360535TR-360535TR-360535TR-360535TR-360535
TRB-608
TRB 608
Column: TRB-608TRB-608TRB-608TRB-608TRB-608, P/N TR-360232Dimensions: 30m x 0.25mm x 0.25mmInjection: 1 µL Grob Test, split 1:100, 280ºCCarrier gas: H2, constant pressure11 psi (75.8 Kpa)Oven temperature: 40ºC @ 6ºC/minto 300ºC(5min)Detector: FID, 340ºC
Meta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent PhaseMeta.VOC Equ iva lent Phase
Agilent:Agi lent:Agi lent:Agi lent:Agi lent: DB-502.2, HP-VOCSupelco:Supelco:Supelco:Supelco:Supelco: VOCOLRestek:Restek:Restek:Restek:Restek: Rtx-502.2
TRB-608 Equ iva lent PhaseTRB-608 Equ iva lent PhaseTRB-608 Equ iva lent PhaseTRB-608 Equ iva lent PhaseTRB-608 Equ iva lent Phase
Agilent:Agi lent:Agi lent:Agi lent:Agi lent: HP-608Supelco:Supelco:Supelco:Supelco:Supelco: SPB-608SGE:SGE:SGE:SGE:SGE: BP-608
1
2 34
5
6
7
8
910 11
Peak Name
1 Methylene chloride2 2,3-Butanediol3 C-104 C-115 1-Octanol6 Nonanal7 2,6-Dimethylphenol8 2,6-Dimethylaniline9 C-10 FAME10 C-11 FAME11 C-12 FAME
TKG 1140
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s - - - - - S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r yyyyyTTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s
4 8
Peak Name
1 Isooctane2 C-113 C-124 Benzene5 C-136 Toluene7 Ethylbenzene8 p-Xylene9 Cumene
TR-TCEP
Column: TR-TCEPTR-TCEPTR-TCEPTR-TCEPTR-TCEP, P/N TR-960462Dimensions: 60m x 0.25mm x 0.40µmInjection: 1 µL standard (20 ng/mL comp.), split 1:50, 170ºCCarrier gas: H2, constant pressure 24 psi (165 Kpa)Oven temperature: 110ºCDetector: FID, 170ºC
Meta.WAX 400
Column: Meta.WMeta.WMeta.WMeta.WMeta.WAX 400AX 400AX 400AX 400AX 400, P/N TR-402153Dimensions: 50m x 0.32mm x 0.20µmInjection: 1µL standard (split 1:50), 175ºCCarrier gas: He, 11 psi (75.8 Kpa)Oven Temperature: 30ºC(5 min.) @ 4ºC/min to 60ºC(10 min.)Detector Temperature: FID, 175ºC
Peak Name
1 Acetaldehyde2 Ethyl Acetate3 Methanol4 Ethanol5 2-Butanol6 n-Propanol7 Allyl alcohol8 2-Methyl-1-propanol (isobutanol)9 1-Butanol10 2-Methyl-1-butanol (amyl alcohol)11 3-Methyl-1-butanol (isoamyl alcohol)
TR-TCEP
1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase1, 2, 3-tr is (2-cyanoethoxy) propane, nonbonded phase
• High polarity column.
• Column for analysis of alcohols in gasoline.
• Separation of the aliphatic hydrocarbons up to C12 in aromatics.
Meta.WAX 400
100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.100% Polyethylene glycol (PEG), nonbonded phase.
• Column designed for analysis of volatiles in alcoholic beverages and solvents.
• Maximum resolution of amylic alcohols.
• High number of plates even at very low temperature (<20ºC)
TR-TCEP
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s - - - - - S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r S p e c i a l f o r I n d u s t r yyyyy
Meta.WAX 400
Structure of Polyethyleneglycol CH2 CH2 OOm
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n sy C o l u m n s - S p e c i a l t y C o l u m n s
TKG 1141TKG 1142
TR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent PhaseTR -TCEP Equ iva lent Phase
Supelco:Supelco:Supelco:Supelco:Supelco: TCEPRestekRestekRestekRestekRestek: Rt-TCEPVVVVVarian: ar ian: ar ian: ar ian: ar ian: CP-TCEP
Me ta .WMeta .WMeta .WMeta .WMeta .WAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent PhaseAX 400 Equ iva lent Phase
VVVVVarian: arian: arian: arian: arian: CP Carbowax 400
TR-TCEPInterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 30 0,40 0 to 135 TR-960432TR-960432TR-960432TR-960432TR-960432
60 0,40 0 to 135 TR-960462TR-960462TR-960462TR-960462TR-960462
Meta.WAX 400InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength FilmFilmFilmFilmFilm TTTTTempempempempemp ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) Thickness (Thickness (Thickness (Thickness (Thickness (mmmmmm)m)m)m)m) l imits (°C)l imits (°C)l imits (°C)l imits (°C)l imits (°C) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 50 0,20 0 to 60/80 TR-402153TR-402153TR-402153TR-402153TR-402153
49
Fig. 9. Lemon oil in a 100 µµµµµm column
Column TRB-5, 10m x 0,1 mm ID X 0,33 µm
Fig. 8. Lemon oil in a conventional column
Column TRB-1, 50m x 0,25 mm ID X 0,33 µm
10 minutes
Teknokroma Microbore Columns (0,1mm ID)• MINIMUM BLEED LEVEL (approximately 10 times less than that of a
conventional column of 0.25 mm ID).
• HIGH ANALYTICAL SPEED (the analysis are approximately 3 times faster than aconventional column of 0.25 mm ID).
These columns of 100 µm internal diameter also enable them to be connected to aconventional chromatograph fitted with a SPLIT/SPLITLESS injector, and due to itsgreat efficiency (~7,000-10,000 plates/m) and its reduced diameter, theanalysis can be undertaken with greater speed compared to standard capillarycolumns, without loss of peak resolving power. Having such a high level ofefficiency enables the analysis of complex mixtures, with a large number ofcomponents. The standard length is 10 metres (Fig. 8 and Fig. 9).
Limiting factors
1. WORKING PRESSURE (GAS FLOW)
With microbore columns the working pressures are higher so that more precautionsshould be taken regarding gas leaks from the injector cavity or with ferrules.
At optimed pressure the carrier gas flow is low (H2~0.2cc/min, He ~0.1cc/min),which is good for working with mass detectors, since it does not exceed itsemptying capacity. Not optimizing these parameters may cause losses in peakresolution.
2. SAMPLE CAPACITY
In these columns with a small diameter the sample that can be injected is muchsmaller than with a column with a conventional diameter. Its sample capacity isaround ten times less than that of a column of 0.25 mm ID.
3. INJECTOR
The columns of 0.1 mm ID are compatible with the injection techniques in Split-splitless. It is not recommended to work with direct or on-column injection.The glass liners, with internal diameters of 2-4 mm, are not the most suitablesince, due to their large dead volume, and the fact that one is working with smallgas carrying flows, it is difficult for there to be a correct sweep in the injectionzone. This transforms into an enlarging of peaks, with the subsequent loss ofresolution (especially for liners of 4 mm). It is highly recommended to work withliners of 0.75-1 mm diameter.
Working with this type of small volume liner, along with the microbore columns,means that one must be extremely careful with the purity of the samples that areinjected. The samples must be clean and the non-volatile residues must beminimised in order to avoid contaminations that cause absorption of analytes,decompositions, the appearance of ghost peaks, etc.
4. DETECTOR
The gas flows of the detector must be optimised for working with the microborecolumns. It is possible that in some detectors the auxiliary gas flow(make up) willhave to be increased in order to minimise its dead volume and enable the correctsweep of the compounds that leave the column at very low flow levels.Since the peaks elute very fast and are very narrow (the peak widths are generallyless than 1 s) it is necessary to work at very high speeds on the electrometer andwith fast integration so that the quantification of the peaks is correct.The small volume of these columns means that the stationary phase quantitydeposited in them is very small compared to a conventional column. This, alongwith the low flow levels with which it works, causes the bleed level (proportionalto the quantity of the phase and flow) to be minimal, even at high temperatures,thus favouring the signal/noise ratio and contributing to the detectors not gettingcontaminated.
TKG 1143
TKG 1144
40 minutes
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r e C o l u m n sC o l u m n sC o l u m n sC o l u m n sC o l u m n s
Teknokroma Microbore columns of 100 µmPhasePhasePhasePhasePhase Length (m)Length (m)Length (m)Length (m)Length (m) (df µm)(df µm)(df µm)(df µm)(df µm) P/NP/NP/NP/NP/NTRB-1TRB-1TRB-1TRB-1TRB-1 10 0.1 TR-110141TR-110141TR-110141TR-110141TR-110141
10 0.4 TR-110441TR-110441TR-110441TR-110441TR-11044120 0.1 TR-110181TR-110181TR-110181TR-110181TR-11018120 0.4 TR-110481TR-110481TR-110481TR-110481TR-110481
TRB-5TRB-5TRB-5TRB-5TRB-5 10 0.1 TR-120141TR-120141TR-120141TR-120141TR-12014110 0.4 TR-120441TR-120441TR-120441TR-120441TR-12044120 0.1 TR-120181TR-120181TR-120181TR-120181TR-12018120 0.4 TR-120481TR-120481TR-120481TR-120481TR-120481
TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX 10 0.1 TR-140141TR-140141TR-140141TR-140141TR-14014110 0.2 TR-142141TR-142141TR-142141TR-142141TR-14214120 0.1 TR-140181TR-140181TR-140181TR-140181TR-14018120 0.2 TR-142181TR-142181TR-142181TR-142181TR-142181
5 0
TKG 1145
Teknokroma Microbore Columns
TRB-WAX
Column: TRB-WTRB-WTRB-WTRB-WTRB-WAXAXAXAXAX, P/N TR-140141Dimensions: 10m x 0.10mm x 0.10µmInjection: 1µL standard FAMES, (200ng/comp), split 1:50, 280ºCCarrier gas: H2, constant pressure 50 psi (344.5 Kpa)Oven temperature: 40ºC(1min) @ 25ºC/min to 195ºC @ 3ºC/min to 205ºC @ 8ºC/min to 230ºC(1min)Detector: FID, 280ºC
20 Linolelaidic acid methyl ester (C18:2n6t)21 γ-Linolenic acid methyl ester (C18:3n6)22 Linolenic acid methyl ester (C18:3n3)23 Arachidic acid methyl ester (C20:0)24 Cis-11-eicosenoic acid methyl ester (C20:1)25 Cis-11,14-eicosadienoic acid methyl ester (C20:2)26 Cis-8,11,14-eicosatrienoic acid methyl ester (C20:3n6)27 Heneicosanoic acid methyl ester (C21:0)28 Cis-11,14,17-eicosatrienoic acid methyl ester (C20:3n3)29 Arachidonic acid methyl ester (C20:4n6)30 Cis-5,8,11,14,17-eicosapentaenoic acid methyl ester (C20:5n3)31 Behenic acid methyl ester (C22:0)32 Erucic acid methyl ester (C22:1n9)33 Cis-13,16-docosadienoic acid methyl ester (C22:2)34 Tricosanoic acid methyl ester (C23:0)35 Lignoceric acid methyl ester (C24:0)36 Cis-4,7,10,13,16,19-docosahexaenoic acid methyl ester (C22:6n3)37 Nervonic acid methyl ester (C24:1)
Peak Name
1 Butyric acid methyl ester (C4:0)2 Caproic acid methyl ester (C6:0)3 Caprylic acid methyl ester (C8:0)4 Capric acid methyl ester (C10:0)5 Undecanoic acid methyl ester (C11:0)6 Lauric acid methyl ester (C12:0)7 Tridecanoic acid methyl ester (C13:0)8 Myristic acid methyl ester (C14:0)9 Myristoleic acid methyl ester (C14:1)10 Pentadecanoic acid methyl ester (C15:0)11 Cis-10-pentadecenoic acid methyl ester (C15:1)12 Palmitic acid methyl ester (C16:0)13 Palmitoleic acid methyl ester (C16:1)14 Heptadecanoic acid methyl ester (C17:0)15 Cis-10-heptadecenoic acid methyl ester (C17:1)16 Stearic acid methyl ester (C18:0)17 Oleic acid methyl ester (C18:1n9c)18 Elaidic acid methyl ester (C18:1n9t)19 Linoleic acid methyl ester (C18:2n6c)
1
2
34
5
6
7
8
12
910
11 1314
15
16
17, 18
1920
2122
23
24
25
26
27
2829
30
31
32
33
34
35
36-37Excellent Resolution
in 12 minutes
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r ey C o l u m n s - M i c r o b o r e C o l u m n sC o l u m n sC o l u m n sC o l u m n sC o l u m n s
51
TKG 1147
Custom Capillary ColumnsTeknokroma also provides you with the possibility of working with nonbonded andbonded custom capillary columns, which are still described today in officialmethods, or which appear in the scientific bibliography. We can supply you withthese columns in the size and phase thickness that you require for a similar priceas our standard Teknokroma columns. As an example:
TR-101 - 100% polydimethylsiloxane phase(“silicone fluid”).
TR-SE-30 - 100% polydimethylsiloxane phase.
TR-SE-52 - 5% phenyl -95% dimethylpolysiloxane phase.
TR-SE-54 - 5% phenyl-1% vinyl-94% dimethylpolysiloxane phase.
TR-20M - polyethylene glycol 100% (Carbowax 20M) phase.
We can also supply you with columns for inverse gas chromatography, used for thecharacterisation of polymers. Teknokroma can coat your polymer in our fused silicacolumn.
F O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TF O R O T H E R P H A S E S N O T I N C L U D E D I N T H I S L I S TC O N TC O N TC O N TC O N TC O N T A C T O U RA C T O U RA C T O U RA C T O U RA C T O U R T E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E PT E C H N I C A L D E P A RA RA RA RA R T M E N TT M E N TT M E N TT M E N TT M E N T
TRB-240
Column: TRB-240 TRB-240 TRB-240 TRB-240 TRB-240 (OV-240-OH), P/N TR-240262Dimensions: 60m x 0.25mm x 0.25µmInjection: 1 µL Grob Test, split 1:25, 260ºCCarrier gas: H2, constant pressure 11 psi (75.8 Kpa)Oven temperature: 40ºC @ 6ºC/min to 260ºC(5min)Detector: FID, 260ºC
Peak Name
1 Methylene chloride2 C-103 C-114 2,3-Butanediol5 Nonanal6 1-Octanol7 C-10 FAME8 2,6-Dimethylaniline9 C-11 FAME10 2,6-Dimethylphenol11 C-12 FAME
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o my C o l u m n s - C u s t o m
5 2
NON POLAR
Methyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarMethyl deactivated, suitable for pentane/hexane and other non polarsolvents.solvents.solvents.solvents.solvents.
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 3x1 TR-100012TR-100012TR-100012TR-100012TR-100012
1X5 TR-100052TR-100052TR-100052TR-100052TR-100052
1X10 TR-100042TR-100042TR-100042TR-100042TR-100042
1X20 TR-100082TR-100082TR-100082TR-100082TR-100082
0,320,320,320,320,32 3x1 TR-100013TR-100013TR-100013TR-100013TR-100013
1X5 TR-100053TR-100053TR-100053TR-100053TR-100053
1X10 TR-100043TR-100043TR-100043TR-100043TR-100043
1X20 TR-100083TR-100083TR-100083TR-100083TR-100083
0,530,530,530,530,53 3x1 TR-100015TR-100015TR-100015TR-100015TR-100015
1X5 TR-100055TR-100055TR-100055TR-100055TR-100055
1X10 TR-100045TR-100045TR-100045TR-100045TR-100045
1X20 TR-100085TR-100085TR-100085TR-100085TR-100085
UNIVERSAL PRESS FIT CONNECTORS
DeactivatedDeactivatedDeactivatedDeactivatedDeactivated DescriptionDescriptionDescriptionDescriptionDescriptionUniversalUniversalUniversalUniversalUniversal
TR-33001TR-33001TR-33001TR-33001TR-33001 Universal Press Fit 12pk
TR-33002TR-33002TR-33002TR-33002TR-33002 Universal Press Fit Angled Y/unit
Guard Columns (Retention Gap)
NON POLAR
MEDIUM POLAR (INTERMEDIATE)
POLAR
AQUASAFE
BASE-DEACTIVATED
MEDIUM POLAR (INTERMEDIATE)
Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,Phenyl-methyl deactivated, USP (467) suitable for methylene chloride,hexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solventshexane, toluene, and a wide range of similar solvents
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 3x1 TR-200012TR-200012TR-200012TR-200012TR-200012
1X5 TR-200052TR-200052TR-200052TR-200052TR-200052
1X10 TR-200042TR-200042TR-200042TR-200042TR-200042
1X20 TR-200082TR-200082TR-200082TR-200082TR-200082
0,320,320,320,320,32 3x1 TR-200013TR-200013TR-200013TR-200013TR-200013
1X5 TR-200053TR-200053TR-200053TR-200053TR-200053
1X10 TR-200043TR-200043TR-200043TR-200043TR-200043
1X20 TR-200083TR-200083TR-200083TR-200083TR-200083
0,530,530,530,530,53 3x1 TR-200015TR-200015TR-200015TR-200015TR-200015
1X5 TR-200055TR-200055TR-200055TR-200055TR-200055
1X10 TR-200045TR-200045TR-200045TR-200045TR-200045
1X20 TR-200085TR-200085TR-200085TR-200085TR-200085
G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )
53
Guard Columns (Retention Gap)
Teknokroma Metal Capillary ColumnsStainless steel Teknokroma columns (TR-INOX)
• Chemical inertness comparable to that of fused silica• Bonded and crosslinked• Ideal for chromatographs in industrial control processes• Practically unbreakable• Enables the use of high analysis temperatures
Teknokroma can supply you with Teknokroma stainless steel columns with a 0.53mm internal diameter and with an external diameter similar to that of fused silicasemi-capillary columns, enabling you to use the same standard ferrules of0.8 mm ID.
These columns are available with our most popular stationary phases.To order a metallic column simply add the prefix INOX at the end of thecorresponding reference to the column in the catalog.
For example: TRB-2887 of 10m x 0.53 mm x 2.65µm P/N TR-192645P/N TR-192645P/N TR-192645P/N TR-192645P/N TR-192645With stainless steel tube, 10m x 0.53 mm x 2.65µm P/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOXP/N TR-192645INOX
5-inch column cage
For columns that have to be placed in the oven of the 6850 chromatograph, thecolumn must be rolled up in a 5 inch cage.To order a column in a 5 inch cage you just need to add a 5 to the end of thecatalog number of the corresponding column.
For example: TRB-5, 30m x 0.25 mm x 0.25µm P/N TR-120232P/N TR-120232P/N TR-120232P/N TR-120232P/N TR-120232With 5 inch cage, TRB-5, 30m x 0.25 mm x 0.25µm P/N TR-1202325P/N TR-1202325P/N TR-1202325P/N TR-1202325P/N TR-1202325
POLAR
Polyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widePolyethylene glycol deactivated, suitable for methanol, water and a widerange of similar polar solvents.range of similar polar solvents.range of similar polar solvents.range of similar polar solvents.range of similar polar solvents.
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 3x1 TR-300012TR-300012TR-300012TR-300012TR-300012
1X5 TR-300052TR-300052TR-300052TR-300052TR-300052
1X10 TR-300042TR-300042TR-300042TR-300042TR-300042
1X20 TR-300082TR-300082TR-300082TR-300082TR-300082
0,320,320,320,320,32 3x1 TR-300013TR-300013TR-300013TR-300013TR-300013
1X5 TR-300053TR-300053TR-300053TR-300053TR-300053
1X10 TR-300043TR-300043TR-300043TR-300043TR-300043
1X20 TR-300083TR-300083TR-300083TR-300083TR-300083
0,530,530,530,530,53 3x1 TR-300015TR-300015TR-300015TR-300015TR-300015
1X5 TR-300055TR-300055TR-300055TR-300055TR-300055
1X10 TR-300045TR-300045TR-300045TR-300045TR-300045
1X20 TR-300085TR-300085TR-300085TR-300085TR-300085
AQUASAFE
ProprietarProprietarProprietarProprietarProprietary deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.y deactivation suitable for water direct aqueous injections.
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 3x1 TR-310012TR-310012TR-310012TR-310012TR-310012
1X5 TR-310052TR-310052TR-310052TR-310052TR-310052
1X10 TR-310042TR-310042TR-310042TR-310042TR-310042
1X20 TR-310082TR-310082TR-310082TR-310082TR-310082
AQUASAFE (Cont.)InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,320,320,320,320,32 3x1 TR-310013TR-310013TR-310013TR-310013TR-310013
1X5 TR-310053TR-310053TR-310053TR-310053TR-310053
1X10 TR-310043TR-310043TR-310043TR-310043TR-310043
1X20 TR-310083TR-310083TR-310083TR-310083TR-310083
0,530,530,530,530,53 3x1 TR-310015TR-310015TR-310015TR-310015TR-310015
1X5 TR-310055TR-310055TR-310055TR-310055TR-310055
1X10 TR-310045TR-310045TR-310045TR-310045TR-310045
1X20 TR-310085TR-310085TR-310085TR-310085TR-310085
BASE-DEACTIVATED
ProprietarProprietarProprietarProprietarProprietary deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basicy deactivation suitable for analysis of amines and other basiccompoundscompoundscompoundscompoundscompounds
InterInterInterInterInternalnalnalnalnal LengthLengthLengthLengthLength ParParParParPart .t .t .t .t .Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm)Diam.(mm) (m)(m)(m)(m)(m) N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)N°. (P/N)
0,250,250,250,250,25 3x1 TR-320012TR-320012TR-320012TR-320012TR-320012
1X5 TR-320052TR-320052TR-320052TR-320052TR-320052
1X10 TR-320042TR-320042TR-320042TR-320042TR-320042
1X20 TR-320082TR-320082TR-320082TR-320082TR-320082
0,320,320,320,320,32 3x1 TR-320013TR-320013TR-320013TR-320013TR-320013
1X5 TR-320053TR-320053TR-320053TR-320053TR-320053
1X10 TR-320043TR-320043TR-320043TR-320043TR-320043
1X20 TR-320083TR-320083TR-320083TR-320083TR-320083
0,530,530,530,530,53 3x1 TR-320015TR-320015TR-320015TR-320015TR-320015
1X5 TR-320055TR-320055TR-320055TR-320055TR-320055
1X10 TR-320045TR-320045TR-320045TR-320045TR-320045
1X20 TR-320085TR-320085TR-320085TR-320085TR-320085
Columns for the Agilent GC 6850
G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )G u a r d C o l u m n s ( R e t e n t i o n G A P )
5 4
USP Capillary Column EquivalentsEDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG NOITPIRCSEDLARENEG
DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKET DEDNEMMOCERAMORKONKETTNELAVIUQEYRALLIPAC
1G1G1G1G1G lioenaxolisyloplyhtemiD sm1-BRT,1-BRT
2G2G2G2G2G mugenaxolisyloplyhtemiD sm1-BRT,1-BRT
3G3G3G3G3G enaxolisyloplyhtem%05-lynehp%05 05-BRT
5G5G5G5G5G enaxolislyporponayc-3 001NC-RT
8G8G8G8G8G enaxolislyhtemlynehp%01-lyporponayc-3-%09 001NC-RT
9G9G9G9G9G enaxolisyloplynivlyhteM sm1-BRT,1-BRT
41G 41G 41G 41G 41G )0501-159=WM(locylgenelyhteyloP XAW-BRT
51G 51G 51G 51G 51G )0703-0003=WM(locylgenelyhteyloP XAW-BRT
61G 61G 61G 61G 61G )00051=WM(locylgenelyhteyloP XAW-BRT
91G 91G 91G 91G 91G enaxolislyhtemlyporponayc%52-lynehp%52 522-BRT
02G 02G 02G 02G 02G )024-083=WM(locylgenelyhteyloP 004XAW.ateM
52G 52G 52G 52G 52G APTlocylgenelyhteyloP PAFF-BRT
72G 72G 72G 72G 72G enaxolisyloplyhtem%59-lynehp%5 5X.ateM,sm5-BRT,5-BRT
82G 82G 82G 82G 82G enaxolisyloplyhtemid-%57-lynehp%52 02-BRT
23G 23G 23G 23G 23G enaxolisyloplyhtemid-%08-lyhtemlynehp%02 02-BRT
53G 53G 53G 53G 53G dicacilahthperetortiNhtiwlocylgenelyhteyloP PAFF-BRT
63G 63G 63G 63G 63G enaxolisyloplyhtemlynehp%5-lyniv%1 5X.ateM,sm5-BRT,5-BRT
93G 93G 93G 93G 93G )0051=WM(locylgenelyhteyloP XAW-BRT
24G 24G 24G 24G 24G enaxolisyloplyhtemid%56-lynehpid%53 53-BRT
34G 34G 34G 34G 34G enaxolisyloplyhtemid%49-lynehplyporponayc%6 34G-RT,1031-BRT,426-BRT
64G 64G 64G 64G 64G enaxolisyloplyhtemid%68-lynehplyporponayc%41 1071-BRT
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
55
EPA Drinking Water Test MethodsEPA METHODEPA METHODEPA METHODEPA METHOD APPLICATIONAPPLICATIONAPPLICATIONAPPLICATION RECOMMENDEDRECOMMENDEDRECOMMENDEDRECOMMENDED TEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMNTEKNOKROMA CAPILLARY COLUMN PART NUMBERPART NUMBERPART NUMBERPART NUMBER
501.3501.3501.3501.3 Trihalomethanes by GC/MS and SIM TRB-624 30m x 0.53mm x 3.0 mm TR-603035
TRB-624 75m x 0.53mm x 3.0 mm TR-603075
TRB-624 105m x 0.53mm x 3.0 mm TR-6030K5
TRB-624 30m x 0.25mm x 1.0 mm TR-601032
502.2502.2502.2502.2 Vo l a t i l e ha l oge na te d O rg an i c s i n Wat e r b y Pu r ge & Tr a pGC/PID/ELCD
TRB-624 30m x 0.53mm x 3.0 mm TR-603035
503.1503.1503.1503.1 Volatile Aromatics & Unsaturated Organics by Purge & Trap GC TRB-624 30m x 0.53mm x 3.0 mm TR-603035
TRB-624 30m x 0.25mm x 1.4 mm TR-601432
504.1504.1504.1504.1 1,2-Dibromoethane (EDB), 1,2-Dibromo-3-chloropropane TRB-1 30m x 0.32mm x 0.25 mm TR-110233
(DBCP), and 1,2,3-Trichloropropane (123TCP) by GC/MS TRB-624 30m x 0.53mm x 3.0 mm TR-603035
TRB-624 30m x 0.25mm x 1.4 mm TR-601432
505505505505 Organohalide Pesticides & Aroclors by GC/ECD TRB-1 30m x 0.32mm x 1.0 mm TR-111033
TRB-50 30m x 0.32mm x 0.5 mm TR-500533
TRB-50 30m x 0.25mm x 0.25 mm TR-500232
507507507507 Nitrogen & Phosphorous containing Pesticides in Water TRB-5 30m x 0.25mm x 0.25 mm TR-120232
by GC/NPD TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232
TRB-1701 30m x 0.25mm x 0.25 mm TR-130233
508508508508 Chlorinated Pesticides in Water by GC/MS TRB-5 30m x 0.25mm x 0.25 mm TR-120232
TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232
TRB-1701 30m x 0.25mm x 0.25 mm TR-130233
513513513513 2,3,7,8-Tetrachlorodibenzo-p-dioxin by GC/MS TRB-5ms 60m x 0.25mm x 0.10 mm TR-520162
515.2515.2515.2515.2 Determination of chlorinated acids in water using TRB-1 30m x 0.32mm x 0.25 mm TR-110233
liquid-solid extraction and GC/ECD TRB-5 30m x 0.32mm x 0.25 mm TR-120233
TRB-1701 30m x 0.32mm x 0.25 mm TR-130233
TRB-5ms 30m x 0.32mm x 0.25 mm TR-520233
524.2524.2524.2524.2 Measurement of purgeable organic compounds in water TRB-624 30m x 0.25mm x 1.4 mm TR-601432
by Purge & Trap capillary column GC/MS TRB-624 30m x 0.53mm x 3.0 mm TR-603035
TRB-624 75m x 0.53mm x 3.0 mm TR-603075
TRB-624 60m x 0.32mm x 1.8 mm TR-601863
525525525525 Capillary column GC/MS Organic compounds in drinking waterby liquid-solid extraction
TRB-5 30m x 0.32mm x 0.25 mm TR-120233
TRB-5ms 30m x 0.25mm x 0.25 mm TR-520232
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
5 6
EPA Solid Waste Test MethodsDOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP
0108 0108 0108 0108 0108 scinagroelitalovdetanegolaH 426-BRT 0.3xmm35.0xm57 mm 570306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
5108 5108 5108 5108 5108 scinagroelitalovdetanegolaH-noN 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
1208/0208 1208/0208 1208/0208 1208/0208 1208/0208 cinagroelitalovcitamorA 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
1308/0308 1308/0308 1308/0308 1308/0308 1308/0308 elirtinoteca,elirtinolyrca,nielorcA 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
1408/0408 1408/0408 1408/0408 1408/0408 1408/0408 slonehP 5-BRT 5.1xmm35.0xm03 mm 535121-RT
sm5-BRT 52.0xmm52.0xm03 mm 232025-RT
1608/0608 1608/0608 1608/0608 1608/0608 1608/0608 sretseetalahthP 1-BRT 5.1xmm35.0xm51 mm 515111-RT
sm1-BRT 4.0xmm52.0xm03 mm 234015-RT
0808 0808 0808 0808 0808 sBCPdnasedicitsepenirolhconagrO 5-BRT 5.1xmm35.0xm03 mm 535121-RT
sm5-BRT 5.0xmm52.0xm03 mm 235025-RT
2808/1808 2808/1808 2808/1808 2808/1808 2808/1808 rolhcorAsasBCPdnasedicitsepenirolhconagrO 5-BRT 5.1xmm35.0xm03 mm 535121-RT
1071-BRT 0.1xmm35.0xm03 mm 530131-RT
1908/0908 1908/0908 1908/0908 1908/0908 1908/0908 senotekscilcycdnascitamoraortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT
sm5-BRT 5.0xmm52.0xm03 mm 235025-RT
0018 0018 0018 0018 0018 snobracordyhcitamoraraelcunyloP 5-BRT 52.0xmm23.0xm03 mm 332021-RT
sm5-BRT 52.0xmm23.0xm03 mm 332025-RT
1218/0218 1218/0218 1218/0218 1218/0218 1218/0218 snobracordyhdetanirolhC 1-BRT 0.1xmm23.0xm03 mm 330111-RT
sm1-BRT 0.1xmm23.0xm03 mm 330115-RT
0418 0418 0418 0418 0418 sedicitsepsurohpsohponagrO 1-BRT 5.1xmm23.0xm03 mm 535111-RT
1071-BRT 0.1xmm35.0xm03 mm 530131-RT
1-BRT 52.0xmm52.0xm03 mm 232011-RT
1418 1418 1418 1418 1418 sedicitsepsurohpsohponagrO 5-BRT 5.1xmm35.0xm51 mm 515121-RT
sm5-BRT 52,0xmm52.0xm51 mm 212025-RT
1518/0518 1518/0518 1518/0518 1518/0518 1518/0518 sedicibrehdetanirolhC 5-BRT 0.1xmm35.0xm52 mm 520121-RT
1071-BRT 0.1xmm35.0xm03 mm 530131-RT
sm5-BRT 52,0xmm52.0xm51 mm 232025-RT
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
57
DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP
0428 0428 0428 0428 0428 scinagroelitalovrofSM/CG 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 0.3xmm35.0xm57 mm 570306-RT
426-BRT 0.3xmm35.0xm501 mm 5K0306-RT
426-BRT 0.1xmm52.0xm03 mm 230106-RT
0528 0528 0528 0528 0528 scinagroelitalov-imesrofSM/CG sm5-BRT 05,0xmm52.0xm03 mm 235025-RT
0628 0628 0628 0628 0628 seuqinhcetyrallipacscinagroelitalovrofdohtemSM/CG 426-BRT 0,3xmm35.0xm03 mm 530306-RT
426-BRT 0,3xmm35.0xm57 mm 570306-RT
426-BRT 0,3xmm35.0xm501 mm 5K0306-RT
426-BRT 0,1xmm52.0xm03 mm 230106-RT
0728 0728 0728 0728 0728 seuqinhcetyrallipacscinagroelitalov-imesrofdohtemSM/CG 5-BRT 0,1xmm52.0xm03 mm 230121-RT
sm5-BRT 0,1xmm52.0xm03 mm 230125-RT
0828 0828 0828 0828 0828 dnasnixoid-p-oznebiddetanirolhcylopfosisylanAsnarufoznebiddetanirolhcylop
5-BRT 52,0xmm52.0xm03 mm 232021-RT
sm5-BRT 52,0xmm52.0xm06 mm 261025-RT
DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP
106 106 106 106 106 snobracolahelbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 0.3xmm35.0xm57 mm 570306-RT
426-BRT 0.3xmm35.0xm501 mm 5K0306-RT
426-BRT 0.1xmm52.0xm03 mm 230106-RT
206 206 206 206 206 scitamoraelbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 0.3xmm35.0xm501 mm 5K0306-RT
426-BRT 0.1xmm52.0xm03 mm 230106-RT
306 306 306 306 306 elirtinolyrcadnanielorcA 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 0.1xmm52.0xm03 mm 230106-RT
506/406 506/406 506/406 506/406 506/406 senidiznebdnaslonehP sm5-BRT 4.1xmm35.0xm03 mm 534125-RT
sm5-BRT 52.0xmm52.0xm03 mm 232025-RT
606 606 606 606 606 sretseetalahthP 5-BRT 5.1xmm35.0xm51 mm 515121-RT
sm5-BRT 52.0xmm52.0xm03 mm 232025-RT
EPA Solid Waste Test Methods
EPA Waste Water Test Methods
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
5 8
DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE DOHTEMAPE NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA NOITACILPPA DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER DEDNEMMOCER NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET NMULOCYRALLIPACAMORKONKET REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP REBMUNTRAP
606 606 606 606 606 sretseetalahthP 5-BRT 5.1xmm35.0xm51 mm 515121-RT
sm5-BRT 52.0xmm52.0xm03 mm 232025-RT
706 706 706 706 706 senimasortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT
sm5-BRT 05.0xmm52.0xm03 mm 235025-RT
806 806 806 806 806 sBCPdnasedicitsepenirolhconagrO 5-BRT 0.1xmm35.0xm05 mm 550121-RT
sm5-BRT 21.0xmm52.0xm05 mm 257025-RT
906 906 906 906 906 enorohposidnascitamoraortiN 5-BRT 5.1xmm35.0xm03 mm 535121-RT
sm5-BRT 5.0xmm52.0xm03 mm 235025-RT
016 016 016 016 016 snobracordyHcitamorAcilcycyloP 5-BRT 52.0xmm23.0xm03 mm 332021-RT
sm5-BRT 01.0xmm23.0xm03 mm 331025-RT
116 116 116 116 116 srehteolaH 5-BRT 5.1xmm35.0xm51 mm 515121-RT
sm5-BRT 05.0xmm52.0xm03 mm 235025-RT
216 216 216 216 216 snobracordyhdetanirolhC 5-BRT 0.1xmm23.0xm03 mm 330121-RT
sm5-BRT 0.1xmm52.0xm03 mm 230125-RT
316 316 316 316 316 nixoid-p-oznebidorolhcartet-8,7,3,2 sm5-BRT 01.0xmm52.0xm06 mm 261025-RT
516 516 516 516 516 sedicibrehdetanirolhC 1071-BRT 0.1xmm35.0xm03 mm 530131-RT
1071-BRT 52.0xmm52.0xm03 mm 232031-RT
916 916 916 916 916 sedicibrehenizairT 05-BRT 0.1xmm35.0xm03 mm 530105-RT
05-BRT 05.0xmm52.0xm03 mm 235005-RT
426 426 426 426 426 selbaegruP 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 0.3xmm35.0xm57 mm 570306-RT
426-BRT 0.3xmm35.0xm501 mm 5K0306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
526 526 526 526 526 sdicadnaslartuen/esaB sm5-BRT 52.0xmm23.0xm03 mm 332025-RT
sm1-BRT 52.0xmm52.0xm03 mm 232015-RT
086 086 086 086 086 tnemides/liosdnaretawnisBCPdnasedicitseP 5-BRT 52.0xmm23.0xm03 mm 332021-RT
sm5-BRT 52.0xmm23.0xm03 mm 332025-RT
4261 4261 4261 4261 4261 SM/CGnoitulidepotosiybsdnuopmoccinagroelitaloV 426-BRT 0.3xmm35.0xm03 mm 530306-RT
426-BRT 4.1xmm52.0xm03 mm 234106-RT
5261 5261 5261 5261 5261 noitulidepotosiybsdnuopmoccinagroelitalovimeS 5-BRT 52.0xmm52.0xm03 mm 232021-RT
sm5-BRT 52.0xmm52.0xm03 mm 232025-RT
3561 3561 3561 3561 3561 noitalycaSMutis-niybretawetsawnislonehpdetanirolhCSM/deelbwolCGdna
5-BRT 52.0xmm23.0xm03 mm 332021-RT
sm5-BRT 52.0xmm23.0xm03 mm 332025-RT
EPA Waste Water Test Methods
TTTTT e k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a re k n o k r o m a C a p i l l a r y C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n sy C o l u m n s
59
Packed Columns
NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS TROPPUSDILOS EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU
htraesuoeciliS tropocliS brosomorhC PHW A1S
dehsaw-esabdna-dicahtobdnaA1Ssadetaert,htraesuoeciliS tropocliS WBW BA1S
,dehsaw-dica,Cº009evobarednibyalcahtiwdenrubrodeniclac,kcirberifdehsurCdezinalisebyam
brosomorhC SCDMDWAP C1S
htraesuoecilisdetaertnU brosomorhC WANW SN1S
nag/2m05nahtsselfoaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS4.0-3.0foretemaiderop.eva µµµµµ m
brosomorhC 101 2S
g/2m006ot005foaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS5700.0foretemaiderop.evadna µµµµµ m
peseyaH kcaparoPQ Q 3S
lanimonagnivahspuorgN-dna0-citamorahtiwremylopocenezneblynivid-enerytS6700.0foretemaiderop.evadnag/2m006ot004foaeraecafrus µµµµµ m
peseyaH kcaparoPR R 4S
hsem06-04,remylopenelyhteroulfartetthgiewralucelomhgiH brosomorhC T 5S
dnag/2m053-052foaeraecafruslanimonhtiwremylopocenezneblynivid-enerytS1900.0foretemaiderop.eva µµµµµ m
brosomorhC kcaparoP,201 peseyaH, 6S
g/2m21foaeraecafruslanimonagnivahnobracdezitihparG kcalBobraC 7S
enezneblynividenerytsdnaenidiryp-lyniv-4foremylopoC peseyaH kcaparoP,S S 8S
edixoenelynehp-p-lynehpid-6,2nodesabremylopsuoroP xaneT AT 9S
enezneblynividdnaetirtinolyrcaforemylopocdeknil-ssorcylhgiH peseyaH C 01S
llamshtiwdeifidom,g/2m001foaeraecafruslanimonagnivahnobracdezitihparGdnuopmoclocylgenelyhteylopdnamutalortepfostnuoma
kcalBobraC 0051tR%3021/08B 11S
G g/2m001foaeraecafruslanimonagnivahnobracdezitihpar kcalBobraC B 21S
- Solid Supports for USP Methods
TTTTT e k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n s
6 0
These columns have been used for the last 50 years in all kinds of analyses forgas chromatography.
"Packed colum use today is understandable due to the wide range of solid supportpackings available and to their high on-column sample capacity. These aspectsmake packed columns quite versatile for a wide range of applications".
"Today Packed columns are still demostrating their utility in the solution of manyanalytical problems where it is not necessary to use the high resolution of capillarycolumns".
"Teknokroma has packed columns since its beginnings and have always provided awide range and latest advantages in this area of gas chromatography. Within thesenew advances we showcase the latest advance in micro-packed columns (0,75mmand 1,00mm ID) and new bonded phase packings".
WE CAN SUPPLWE CAN SUPPLWE CAN SUPPLWE CAN SUPPLWE CAN SUPPLY YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!Y YOU ANY K IND OF COLUMNS. . . JUST ASK FOR THEM!
TTTTTubingubingubingubingubing ExterExterExterExterExternal Diameter (OD)nal Diameter (OD)nal Diameter (OD)nal Diameter (OD)nal Diameter (OD) InterInterInterInterInternal Diameter (ID)nal Diameter (ID)nal Diameter (ID)nal Diameter (ID)nal Diameter (ID)
Glass 1/4’’ 2mm, 3mm and 4 mm
Stainless Steel 1/4 ’’ and 1/8’’ 4mm, 3mm and 2 mm
Silcosteel 1/4’’ and 1/8’’ 5.2mm and 2 mm
1/16’’ 0.75mm and 1 mm
Nickel, Teflon and Copper 1/8’’ 2 mm
ChromatographChromatographChromatographChromatographChromatograph ConfigurationConfigurationConfigurationConfigurationConfiguration TTTTTubingubingubingubingubing DimmensionsDimmensionsDimmensionsDimmensionsDimmensions PhasePhasePhasePhasePhase SupporSupporSupporSupporSupportttttModelModelModelModelModel (%)(%)(%)(%)(%) (mesh)(mesh)(mesh)(mesh)(mesh)
Agllient 5890 ON-Column Glass 1.8m x 1/4’’ OD 3% Chromosorb W-HP
X 2mm ID SE-30 80/100 mesh
Columns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anColumns can be delivered pre-conditioned or conditioned and proved at anextra cost (please inquire).extra cost (please inquire).extra cost (please inquire).extra cost (please inquire).extra cost (please inquire).
To order a packed column it is necessary to supply the following parameters:
TTTTT e k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n s
Packed Columns
TTTTT e k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n s
NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU
TAhcetllA MT 0001- 052/05 53G
nozeipA L 003/05 -
nozeipA M 003/05 -
43enotneB 081/0 -
)FECB(edimamrof)lyhteonayC-2(-sib-N,N 521/02 -
)TBMB(enidiulot-p-ib-’a,a-)enedilyznebyxohteM-p(-sib-N,N 051 -
)AEEB(etapidA)lyhteyxohte-2(-siB 051 -
)AEMB(etapidA)lyhteyxohtem-2(-siB 051 -
xawobraC 004 001/02 02G
xawobraC 045 571/04 93G
xawobraC 006 521/02 -
xawobraC 0001 051/04 41G
xawobraC 0541 571/05 -
xawobraC 0533 002/06 51G
xawobraC 0006 002/06 -
xawobraC M02 522/06 61G
xawobraC 22222 APT-M0 052/06 52G
)lyhteM(ktsc053,002-CD 052/02 -
)lyhteM(ktsc005,002-CD 052/02 -
)lyhehP-%52(,055-CD 522/02 82G
lisxeD CG003 004/05 33G
etaelaMlytub-n-iD 05/02 -
etalahthplyced-n-iD 571/01 -
etacabes)lyxehlyhte-2(iD 521/0 11G
etapidAlocylgenelyhteiD 012/02 -
etaniccuSlocylgenelyhteiD 002/02 4G
lorecylgiD 001/02 -
etanofluslyhtemiD-4,2 05/0 -
etalahthPlynoniD 051/02 -
etalahthPlycedosiiD 051/02 42G
etapidAlocylgenelyhtE 012/001 -
etaniccuSlocylgenelyhtE 012/001 -
134-CFdaroulF 002/04 -
PAFF 052/05 53G
52-41lionobracolaH 051 -
lapegI 036-OC 002/03 -
lapegI )lonyxonoN(088-OC 002/001 13G
lapegI 099-OC 002/001 -
F-leK 01.oNliO 001 -
etaniccuSlocylglytnepoeN 032/05 12G
VO MT )muglyhteM(1- 053/001 2G
61
Packed Columns
PACKED COLUMNS
Column: 5% Carbowax 20M CarboBlack B/AW, 80/120 meshDimensions: 2m x 1/8" OD X 2mm ID, (Silcosteel)Injection: 1 µl standard, 175ºCCarrier Gas: He, 15mL/minOven temperature: 60ºC(6min) @ 10ºC/min to150ºC(7min)Detector: FID, 175ºC
Peak Name
1- Acetaldehyde2- Methanol3- Acetone4- Ethyl formate5- Ethanol6- Ethyl acetate7- n-Propanol8- Secbutanol9- Isobutanol10- Acetic acid11- Amyl alcohol12- Isoamyl alcohol13- n-Amyl alcohol14- Propionic acid
NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED NOITPIRCSED )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT )Cº(STIMILT EDOCPSU EDOCPSU EDOCPSU EDOCPSU EDOCPSU
VO MT )lynehp%05(71- 053/02 3G
VO MT )lynehp%05(lyniV-71- +003 -
VO MT )lynehp%57(52- 003 71G
VO MT )diulflyhteM(101- 053/02 1G
VO MT )lyporporoulfirT%05(012- +572/02 6G
VO MT )lyhtemlyporponayc%52,lynehp%52(522- +052/02 91G
VO MT )lyllaonayciD(572- +052 -
VO MT 1071- 052/0 -
β,β β,β β,β β,β β,β elirtinoiporpidyxO- 57/0 -
etaniccuSenimalonahteidlynehP 032/0 21G
etapidalocylgenelyhteyloP 522/0 32G
enimienelyhteyloP 571/0 -
421-SO)sgnir5(rehtelynehpyloP 002/0 -
831-SO)sgnir6(rehtelynehpyloP 522/0 -
locylgenelyporpyloP 051/0 -
enimienelyporpyloP 002/0 -
)lyporporoulfirT%05(1-FQ 052/02 -
)muglyhteM(03-ES 003/57 -
)edargCG(03-ES 003/57 2G
)lynehP%5(25-ES 003/05 72G
)lyniV%1,lynehP%5(45-ES 003/05 63G
elirtinocabeS 051 -
raliS )enociliSlynehPlyporponayC%05(PC5 052/05 7G
raliS )enociliSlynehPlyporponayC%09(PC9 052/05 8G
raliS )enociliSlyporponayC%001(C01 052/05 5G
lotibroS 051/001 31G
0021-PS 002/52 -
)enocilislyhteM(0012-PS 053/0 1G
)enaxolislynehplyporponaycyloP(0032-PS 572/02 7G
enaxolis)lynehplyporponayc-%02-lyporponaycsib-%08(yloP(0332-PS 572/52 8G
)enaxolislyporponaycsibyloP(0432-PS 572/52 5G
enelauqS 051/02 -
XOREPUS )WM000.000.4(4 003 -
XOREPUS )WM000.02(M02 052/06 -
)EPECT(lotirhtyreatnePdetalyhteonaycarteT 051/03 -
)DEEHT(enimaiDenelyhtelyhteyxordyharteT 521 -
)PECT(enaporp)yxohteonayc-2(-sirT-3,2,1 081/02 -
notirT 001-X 002/0
notirT )lonahteyxohteyloPyxonehplytcO(503-X 052/02 -
)289W-CU(89-WCU +003/08 9G
)locylGenelyklayloP(X-0081-BLNOCU 002 81G
dimasreV 009 572 -
For other stationarFor other stationarFor other stationarFor other stationarFor other stationary phases please inquirey phases please inquirey phases please inquirey phases please inquirey phases please inquire
TKG 1146
TTTTT e k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n se k n o k r o m a P a c k e d C o l u m n s
6 2
17 mm17 mm17 mm17 mm17 mm12.7 mm12.7 mm12.7 mm12.7 mm12.7 mm11.5 mm11.5 mm11.5 mm11.5 mm11.5 mm11 mm11 mm11 mm11 mm11 mm10 mm10 mm10 mm10 mm10 mm9.5 mm9.5 mm9.5 mm9.5 mm9.5 mm9 mm9 mm9 mm9 mm9 mm5 mm5 mm5 mm5 mm5 mm
Measure Guideyour old septum here
GC Septa
CenterGuideTM Septa for Improved Performance
• Center point guides the needle for easy penetration.• Reduce needle bending• Precision molding assures accurate fit• Available in selected sizes of our premium septa• Improves injection life in some applications
The CenterGuideTM design is currently available in many sizes of our septa SeptaSeptaSeptaSeptaSeptaBTOBTOBTOBTOBTOTMTMTMTMTM, Maratahon, Maratahon, Maratahon, Maratahon, MaratahonTMTMTMTMTM and Advanced Green and Advanced Green and Advanced Green and Advanced Green and Advanced GreenTMTMTMTMTM.....
Septum Size ChartInstrInstrInstrInstrInstrumentumentumentumentument Septum sizeSeptum sizeSeptum sizeSeptum sizeSeptum size
(mm)(mm)(mm)(mm)(mm)
Agilent (HP)Agilent (HP)Agilent (HP)Agilent (HP)Agilent (HP)
5880A, 5890, 6890, 6850 11
5700, 5880 9.5/10
On-Column Injection 5
CE InstrCE InstrCE InstrCE InstrCE Instruments (TMQ)uments (TMQ)uments (TMQ)uments (TMQ)uments (TMQ)
TRACE GC 17
Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)Finnigan (TQM)
GC 9001 9.5
GCQ 9.5
GCQ w/TRACE 17
QCQ 9.5
TRACE 2000 9.5
Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)Fisons/Carlo Erba (TQM)
8000 Series 17
InstrInstrInstrInstrInstrumentumentumentumentument Septum sizeSeptum sizeSeptum sizeSeptum sizeSeptum size(mm)(mm)(mm)(mm)(mm)
PerkinElmerPerkinElmerPerkinElmerPerkinElmerPerkinElmer
Sigma Series 11
900, 990 11
8000 Series 11
Auto SYS 11
Auto SYS XL 11
Pye/UnicamPye/UnicamPye/UnicamPye/UnicamPye/UnicamAll models 7
ShimadzuShimadzuShimadzuShimadzuShimadzuAll models Plug
VVVVVarianarianarianarianarianInjector Type:
Varian Packed Column 9.5/10
Split/splitless
Varian 1078/1079 10/11
Varian 1177 9
Varian 1075/1077 11
Septa BTO TM ( Bleed and Temperature Optimized )
• Extended Temperature Range , Low Bleed• Maximum Temperature 400 ºC in most instruments• Virtually eliminates injection-port sticking• Pre-conditioned; packaged in glass to prevent contamination• Each batch GC-FID tested• Ideal for use with low bleed “Mass Spec” capillary columns
This septa has a excellent performance. You can use this septa at 400 ºC with most modern GCs, for some models 375 ºC isthe maximum; for 17 mm injectors the maximum is 300 ºC. When you need a septa that you need to use with hightemperature and low bleed this is the septa you should use.The BTO Septa has been optimized to reduce injection port adhesion. Is a ideal septa for trace analysis, high injection porttemperature.The BTO Septa are pre-conditioned and packages in glass to prevent contamination.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K298787TR-K298787TR-K298787TR-K298787TR-K298787 5 mm Septa BTO for HP OCI port “Center Guide” 50TR-K298705TR-K298705TR-K298705TR-K298705TR-K298705 9,5 mm 3/8” Septa BTO 50TR-K298745TR-K298745TR-K298745TR-K298745TR-K298745 10 mm Septa BTO 50TR-K298717TR-K298717TR-K298717TR-K298717TR-K298717 11mm 7/16” Septa BTO “Center Guide” 50TR-K298775TR-K298775TR-K298775TR-K298775TR-K298775 11,5 mm Septa BTO for Varian 50TR-K298725TR-K298725TR-K298725TR-K298725TR-K298725 12,7 mm 1/2" Septa BTO 50TR-K298815TR-K298815TR-K298815TR-K298815TR-K298815 17 mm Septa BTO 50
Cylindrical for Shimadzu InstrumentsTR-K298735TR-K298735TR-K298735TR-K298735TR-K298735 Plug Type Septa BTO for Shimadzu 50
CenterGuide Septa Advanced GreenTM
G C S e p t aG C S e p t aG C S e p t aG C S e p t aG C S e p t a
63
17 mm17 mm17 mm17 mm17 mm12.7 mm12.7 mm12.7 mm12.7 mm12.7 mm11.5 mm11.5 mm11.5 mm11.5 mm11.5 mm11 mm11 mm11 mm11 mm11 mm10 mm10 mm10 mm10 mm10 mm9.5 mm9.5 mm9.5 mm9.5 mm9.5 mm9 mm9 mm9 mm9 mm9 mm5 mm5 mm5 mm5 mm5 mm
Measure Guideyour old septum here
GC SeptaMarathon Septa TM (The premium Septa for Autosamplers)
• Outstanding Lifetime• Premium Septum for autosamplers• Ideal for Overnight Runs• Up to 400 injections per Septum• Maximum Temperature 350 ºC• Soft, 45 Durometer, Easy On Autosampler Needles
The septa Marathon, has developed and advanced GC septum for autosampler use, with significantly longer life. The Marathonseptum typically achieves 400 injections without failure, when used with a rounded-tip (HP-style) needles and autosampler orneedle guide. Now you can make extended autosampler runs without fear of sample loss, caused by blow-back of leakingcarrier gas. The Marathon septum is also ideal for standard manual-injection GC and GC/MS.It is packaged in glass vials.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K239587TR-K239587TR-K239587TR-K239587TR-K239587 5 mm Marathon for HP OCI port “Center Guide” 25TR-K239188TR-K239188TR-K239188TR-K239188TR-K239188 9,5 mm 3/8” Marathon 25TR-K239287TR-K239287TR-K239287TR-K239287TR-K239287 11mm 7/16” Marathon “Center Guide” 25TR-K239788TR-K239788TR-K239788TR-K239788TR-K239788 11,5 mm Marathon for Varian 25TR-K239388TR-K239388TR-K239388TR-K239388TR-K239388 12,7 mm 1/2" Marathon 25TR-K239688TR-K239688TR-K239688TR-K239688TR-K239688 17 mm Marathon 25
Cylindrical for Shimadzu InstrumentsTR-K239488TR-K239488TR-K239488TR-K239488TR-K239488 Plug Type Marathon for Shimadzu 25
Septa Advanced Green 3TM
• True Long-Life, High Temperature Green Septum• More injections per Septum• Reduced Injection Port Sticking• Maximum Temperature 350 ºC
The Septum Advanced Green 3 was specifically created to combine significantly longer injection life, low bleed and lowinjection port adhesion. The result is a green septum good for general purpose use.The septum are packaged in glass vials for high purity.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K246525TR-K246525TR-K246525TR-K246525TR-K246525 5 mm Advanced Green 3TM for HP OCI port “Center Guide” 50TR-K246124TR-K246124TR-K246124TR-K246124TR-K246124 9,5 mm 3/8” Advanced Green 3TM 50TR-K246225TR-K246225TR-K246225TR-K246225TR-K246225 11mm 7/16” Advanced Green 3TM “Center Guide” 50TR-K246724TR-K246724TR-K246724TR-K246724TR-K246724 11,5 mm Advanced Green 3TM for Varian 50TR-K246324TR-K246324TR-K246324TR-K246324TR-K246324 12,7 mm 1/2" Advanced Green 3TM 50TR-K246624TR-K246624TR-K246624TR-K246624TR-K246624 17 mm Advanced Green 3TM 50
Cylindrical for Shimadzu InstrumentsTR-K246424TR-K246424TR-K246424TR-K246424TR-K246424 Plug Type Advanced Green 3TM for Shimadzu 50
G C S e p t aG C S e p t aG C S e p t aG C S e p t aG C S e p t a
6 4
Septa 77TM
This is our high-quality septum, suitable for most applications. It has been the standard septum in GC and GC/MS labs foryears. Septa 77 features low bleed with excellent resealing capability and good temperature endurance. Septa 77 is carefullyprocessed, then packaged in glass bottles for purity. Maximum temperature is 300 ºC, except in 17 mm injection ports,270ºC.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K237785TR-K237785TR-K237785TR-K237785TR-K237785 5 mm Septa 77 for HP 5880/90 OCI Port 50TR-K237765TR-K237765TR-K237765TR-K237765TR-K237765 6 mm Septa 77 for Hitachi (4,5 mm thick) 50TR-K237755TR-K237755TR-K237755TR-K237755TR-K237755 1/4" Septa 77 50TR-K237705TR-K237705TR-K237705TR-K237705TR-K237705 9,5 mm 3/8” Septa 77 50TR-K237745TR-K237745TR-K237745TR-K237745TR-K237745 10mm Septa 77 50TR-K237715TR-K237715TR-K237715TR-K237715TR-K237715 7/16” Septa 77 50TR-K237725TR-K237725TR-K237725TR-K237725TR-K237725 12,7 mm 1/2" Septa 77 50
Cylindrical for Shimadzu InstrumentsTR-K237735TR-K237735TR-K237735TR-K237735TR-K237735 Plug Type Septa 77 for Shimadzu 50
MicrosepTM Septa F-174 Medium-Performance Septum
This is a good -performance silicone septum faced on side with a layer of TFE teflon. Thickness is approximately 3 mm. Thecolor is White/yellow . Sold in packages of 50.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K230905TR-K230905TR-K230905TR-K230905TR-K230905 9,5 mm 3/8” Microsep Septa F-174 100TR-K230115TR-K230115TR-K230115TR-K230115TR-K230115 11 mm 7/16” Microsep Septa F-174 100TR-K230125TR-K230125TR-K230125TR-K230125TR-K230125 12,5 mm 1/2” Microsep Septa F-174 100
Tekno Blue Septa (Economy Blue Septa)
The septa Tekno Blue are designed for non-demanding, routine applications. They are easy to penetrate, with a durometerrating of 40-45. These septa can be used up to 200-250 ºC and are suitable for 90 % of all GC analysis. Made from silicone.The package is for 100 pieces.
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K00500TR-K00500TR-K00500TR-K00500TR-K00500 6,4 mm 1/4" Tekno Blue Septa 100TR-K00510TR-K00510TR-K00510TR-K00510TR-K00510 9,5 mm 3/8” Tekno Blue Septa 100TR-K00520TR-K00520TR-K00520TR-K00520TR-K00520 11 mm 7/16” Tekno Blue Septa 100TR-K00530TR-K00530TR-K00530TR-K00530TR-K00530 12,5 mm 1/2" Tekno Blue Septa 100
Tekno Red Septa (General Purpose Septa)
• The Tekno Red Septa is a very low bleed septa .• Is easy to penetrate• Have a long injection lifetime at 300 ºC• Maximum temperature 350• Durometer hardness is 45-55
ReferencesReferencesReferencesReferencesReferences DiameterDiameterDiameterDiameterDiameter InchInchInchInchInch DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K00300TR-K00300TR-K00300TR-K00300TR-K00300 9,5 mm 3/8” Tekno Red 50TR-K00320TR-K00320TR-K00320TR-K00320TR-K00320 11 mm 7/16” Tekno Red 50TR-K00330TR-K00330TR-K00330TR-K00330TR-K00330 12,5 mm 1/2" Tekno Red 50
GC Septa
G C S e p t aG C S e p t aG C S e p t aG C S e p t aG C S e p t a
65
GC Ferrules
Graphite Ferrules
• The best material for high temperature use.• Upper temperature limit 450ºC• High-purity Graphite minimizes bleed effects and detector interferences in GC• Preferred by capillary GC use• Smoother surface cleanser edges• Perfect sealing material for glass, and fused silica• Reusable if not overtightened• Not recommended for GC/MS connections
FerFerFerFerFerrrrrrules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Short Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDt Style 1/16" for 4890, 5890 and 6890 except MSDReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211165TR-K211165TR-K211165TR-K211165TR-K211165 1/16" to 0.5 mm 0.25 - 0.32 mm id 10TR-K211168TR-K211168TR-K211168TR-K211168TR-K211168 1/16" to 0.8 mm 0.53 mm id 10TR-K211160TR-K211160TR-K211160TR-K211160TR-K211160 1/16" to 1.0 mm 0.53 - 0.65 mm id 10
G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s
Capillary Column Ferrules
GraphiteThe best material for high temperature use. This is also the softest ferrule material, so it seals gas tight without the risk ofbreaking the column. It does not stick to glass at higher temperatures and may be reused or moved along the column severaltimes if not overtightened; seals with finger-tight pressures. Its one-piece design fits both SwangelokTM and ParkerTM fittings,and does not need a back ferrule. Upper temperature limit is 450ºC.
VespelTM/Graphite60% polymide - 40% graphite. This is especially recommended for GC/MS interface applications. Our one-piece design requiresno back ferrule, and can be reused if not over-tightened. Upper temperature limit is 400ºC.
VespelTM
100% high-temperature polymide. VespelTM is fairly hard and tends to stick to glass columns, usually not reusable. One-piecedesign requires no back ferrule. Upper temperature limit is 350ºC.
TeflonTM
These ferrules are made from 100% TeflonTM in a one-piece design that requires no bback ferrule. Almost completely inert, fairlysoft. Upper temperature limit is 250ªC.
Ferrules for Agilent (HP) HP 5890 and 6890Ferrules ending with HP are reducing ferrules designed to fit all inlets and detectors on the HP 5890 and 6890, except theMSD. The MSD should be used with standard 1/16" ferrules, preferably made from Vespel/Graphite.
Ferrules for Thermo Quest/Fisons/CE Instruments.See in pages 66 and 67.
Ferrules for Perkin Elmer Sigma SeriesUse 1/8" ferrules
Ferrules/Capillary Columns0.25 mm id columns use 0.4 mm id ferrules0.32 mm id columns use 0.5 mm id ferrules0.53 mm id columns use 0.8 mm id ferrules
Agilent / Hewlett-Packard - Graphite
Graphite Ferrules
6 6
Graphite Standard FerGraphite Standard FerGraphite Standard FerGraphite Standard FerGraphite Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211104TR-K211104TR-K211104TR-K211104TR-K211104 1/16" to 0.4 mm 0.25 mm id 10TR-K211105TR-K211105TR-K211105TR-K211105TR-K211105 1/16" to 0.5 mm 0.32 mm id 10TR-K211108TR-K211108TR-K211108TR-K211108TR-K211108 1/16" to 0.8 mm 0.53 mm id 10TR-K211110TR-K211110TR-K211110TR-K211110TR-K211110 1/16" to 1.0 mm 0.65 mm id 10
Graphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard FerGraphite 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211124TR-K211124TR-K211124TR-K211124TR-K211124 1/16" 2-hole 0.4mm/0.4mm 0.25 mm id 10TR-K211125TR-K211125TR-K211125TR-K211125TR-K211125 1/16" 2-hole 0.5mm/0.5mm 0.32 mm id 10
Reducing Graphite FerReducing Graphite FerReducing Graphite FerReducing Graphite FerReducing Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211204TR-K211204TR-K211204TR-K211204TR-K211204 1/8" to 0.4 mm 0.25 mm id 10TR-K211205TR-K211205TR-K211205TR-K211205TR-K211205 1/8" to 0.5 mm 0.32 mm id 10TR-K211208TR-K211208TR-K211208TR-K211208TR-K211208 1/8" to 0.8 mm 0.53 mm id 10TR-K211210TR-K211210TR-K211210TR-K211210TR-K211210 1/8" to 1/16" 1/16" od 10TR-K211405TR-K211405TR-K211405TR-K211405TR-K211405 1/4" to 0.5 mm 0.32 mm id 10TR-K211408TR-K211408TR-K211408TR-K211408TR-K211408 1/4" to 0.8 mm 0.53 mm id 10TR-K211420TR-K211420TR-K211420TR-K211420TR-K211420 1/4" to 1/8" 1/8" od 10TR-K211410TR-K211410TR-K211410TR-K211410TR-K211410 1/4" to 1/16" 1/16" od 10
Graphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing FerGraphite 2-Hole Reducing Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211222TR-K211222TR-K211222TR-K211222TR-K211222 1/8" 2 hole 0.5mm/ 0.5mm 0.32 mm id 10
Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Shimadzuules for Shimadzuules for Shimadzuules for Shimadzuules for ShimadzuReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K211500TR-K211500TR-K211500TR-K211500TR-K211500 5 mm for Shimadzu 5 mm od columns 10
Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Carlo Erbaules for Carlo Erbaules for Carlo Erbaules for Carlo Erbaules for Carlo ErbaReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211904TR-K211904TR-K211904TR-K211904TR-K211904 0.4 mm ID for M8 nut 0.25 mm id 10TR-K211905TR-K211905TR-K211905TR-K211905TR-K211905 0.5 mm ID for M8 nut 0.32 mm id 10TR-K211908TR-K211908TR-K211908TR-K211908TR-K211908 0.8 mm ID for M8 nut 0.53 mm id 10
Special ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite FerSpecial ity Graphite Ferrrrrrules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferules for Fisons/CE Cup Ferrrrrru leuleuleuleuleReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211982TR-K211982TR-K211982TR-K211982TR-K211982 Cup Ferrule 0.25 mm ID for M4 nut 0.20 mm id 2TR-K211983TR-K211983TR-K211983TR-K211983TR-K211983 Cup Ferrule 0.35 mm ID for M4 nut 0.25 mm id 2TR-K211984TR-K211984TR-K211984TR-K211984TR-K211984 Cup Ferrule 0.45 mm ID for M4 nut 0.32 mm id 2TR-K211988TR-K211988TR-K211988TR-K211988TR-K211988 Cup Ferrule 0.8 mm ID for M4 nut 0.53 mm id 2TR-K211948TR-K211948TR-K211948TR-K211948TR-K211948 Graphite Liner Seal 8 mm 1
Graphite Straight FerGraphite Straight FerGraphite Straight FerGraphite Straight FerGraphite Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K211100TR-K211100TR-K211100TR-K211100TR-K211100 1/16" 1/16" 10TR-K211200TR-K211200TR-K211200TR-K211200TR-K211200 1/8" 1/8" 10TR-K211400TR-K211400TR-K211400TR-K211400TR-K211400 1/4" 1/4" 10TR-K211600TR-K211600TR-K211600TR-K211600TR-K211600 3/8" 3/8" 10TR-K211800TR-K211800TR-K211800TR-K211800TR-K211800 1/2" 1/2" 5
O-Ring made of VO-Ring made of VO-Ring made of VO-Ring made of VO-Ring made of VitonitonitonitonitonTMTMTMTMTM for Agilent for Agilent for Agilent for Agilent for AgilentReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription pkpkpkpkpkTR-K211973TR-K211973TR-K211973TR-K211973TR-K211973 O-Ring made of Viton for HP 12
GC Ferrules
G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s
1/16"- Graphite Ferrules
Carlo Erba - Graphite for M8 nut
Fisons /Carlo Erba "Cup" Graphite Ferrulefor M4 nut.
8 mm Graphite Liner Seal for Fisons/CE
O-ring made of Viton for Agilent HP
67G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s
VerspelTM / Graphite Ferrules
• Precision drilled (id)• One-piece design no black ferrule• Stable to 400ºC• Recommended for GC/MS interface applications• Can be re-used• 40% graphite, 60% high temp DuPont polymide
FerFerFerFerFerrrrrrules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Shorules for Agilent Short Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDt Style 1/16" for 5890 and 6890 except MSDReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213163TR-K213163TR-K213163TR-K213163TR-K213163 1/16" to 0.3 mm 0.10 mm id 10TR-K213164TR-K213164TR-K213164TR-K213164TR-K213164 1/16" to 0.4 mm 0.25 mm id 10TR-K213165TR-K213165TR-K213165TR-K213165TR-K213165 1/16" to 0.5 mm 0.32 mm id 10TR-K213168TR-K213168TR-K213168TR-K213168TR-K213168 1/16" to 0.8 mm 0.53 mm id 10
VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Fer/Graphite Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213103TR-K213103TR-K213103TR-K213103TR-K213103 1/16" to 0.3 mm - 10TR-K213104TR-K213104TR-K213104TR-K213104TR-K213104 1/16" to 0.4 mm 0.25 mm id 10TR-K213105TR-K213105TR-K213105TR-K213105TR-K213105 1/16" to 0.5 mm 0.32 mm id 10TR-K213108TR-K213108TR-K213108TR-K213108TR-K213108 1/16" to 0.8 mm 0.53 mm id 10TR-K213110TR-K213110TR-K213110TR-K213110TR-K213110 1/16" to 1.0 mm 0.65 mm id 10
VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Fer/Graphite 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213124TR-K213124TR-K213124TR-K213124TR-K213124 1/16" 2-hole 0.4mm/0.4mm 0.25 mm id 10TR-K213125TR-K213125TR-K213125TR-K213125TR-K213125 1/16" 2-hole 0.5mm/0.5mm 0.32 mm id 10
VVVVVespelespelespelespelespelTMTMTMTMTM/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Fer/Graphite Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K213100TR-K213100TR-K213100TR-K213100TR-K213100 1/16" 10TR-K213200TR-K213200TR-K213200TR-K213200TR-K213200 1/8" 10TR-K213400TR-K213400TR-K213400TR-K213400TR-K213400 1/4" 10
Reducing VReducing VReducing VReducing VReducing VespelespelespelespelespelTMTMTMTMTM/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213204TR-K213204TR-K213204TR-K213204TR-K213204 1/8" to 0.4 mm 0.25 mm id 10TR-K213205TR-K213205TR-K213205TR-K213205TR-K213205 1/8" to 0.5 mm 0.32 mm id 10TR-K213208TR-K213208TR-K213208TR-K213208TR-K213208 1/8" to 0.8 mm 0.53 mm id 10TR-K213210TR-K213210TR-K213210TR-K213210TR-K213210 1/8" to 1/16" 1/16" od 10TR-K213405TR-K213405TR-K213405TR-K213405TR-K213405 1/4" to 0.5 mm 0.32 mm id 10TR-K213408TR-K213408TR-K213408TR-K213408TR-K213408 1/4" to 0.8 mm 0.53 mm id 10TR-K213420TR-K213420TR-K213420TR-K213420TR-K213420 1/4" to 1/8" 1/8" od 10
2-Hole Reducing V2-Hole Reducing V2-Hole Reducing V2-Hole Reducing V2-Hole Reducing VespelespelespelespelespelTMTMTMTMTM/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Fer/Graphite Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K213222TR-K213222TR-K213222TR-K213222TR-K213222 1/8" 2-hole 0.5mm/0.5mm 0.32 mm id 10
GC Ferrules
Standard 1/8"- Graphite/VespelTM
Standard 1/4"- Graphite VespelTM
Agilent HP- Graphite/VespelTM
Carlo Erba - Graphite/VespelTM
Standard 1/16"- Graphite/VespelTM
6 8
VespelTM Ferrules
• Upper temperature limit 350ºC• 100% high-temperature DuPont polymide• Precission-drilled id. No imperfections from molding• One-piece design requires no back ferrule• Fairly hard; tends to seal permanently to the column
VVVVVespelespelespelespelespelTMTMTMTMTM Standard Fer Standard Fer Standard Fer Standard Fer Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212103TR-K212103TR-K212103TR-K212103TR-K212103 1/16" to 0.3 mm - 10TR-K212104TR-K212104TR-K212104TR-K212104TR-K212104 1/16" to 0.4 mm 0.25 mm id 10TR-K212105TR-K212105TR-K212105TR-K212105TR-K212105 1/16" to 0.5 mm 0.32 mm id 10TR-K212108TR-K212108TR-K212108TR-K212108TR-K212108 1/16" to 0.8 mm 0.53 mm id 10TR-K212110TR-K212110TR-K212110TR-K212110TR-K212110 1/16" to 1.0 mm 0.65 mm id 10
VVVVVespelespelespelespelespelTMTMTMTMTM 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Fer 2-Hole Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212124TR-K212124TR-K212124TR-K212124TR-K212124 1/16" 2-hole 0.4 mm/0.4 mm 0.25 mm id 10TR-K212125TR-K212125TR-K212125TR-K212125TR-K212125 1/16" 2-hole 0.5 mm/0.4mm 0.32 mm id 10
Reducing VReducing VReducing VReducing VReducing VespelespelespelespelespelTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212204TR-K212204TR-K212204TR-K212204TR-K212204 1/8" to 0.4 mm 0.25 mm id 10TR-K212205TR-K212205TR-K212205TR-K212205TR-K212205 1/8" to 0.5 mm 0.32 mm id 10TR-K212208TR-K212208TR-K212208TR-K212208TR-K212208 1/8" to 0.8 mm 0.53 mm id 10TR-K212210TR-K212210TR-K212210TR-K212210TR-K212210 1/8" to 1/16" 1/16" od 10TR-K212410TR-K212410TR-K212410TR-K212410TR-K212410 1/4" to 1/16" 1/16" od 10TR-K212420TR-K212420TR-K212420TR-K212420TR-K212420 1/4" to 1/8" 1/8" od 10
VVVVVespelespelespelespelespelTMTMTMTMTM 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Fer 2-Hole Reducing Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K212222TR-K212222TR-K212222TR-K212222TR-K212222 1/8" 2-hole 0.5 mm ea 0.32 mm id 10
VVVVVespelespelespelespelespelTMTMTMTMTM Straight Fer Straight Fer Straight Fer Straight Fer Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K212100TR-K212100TR-K212100TR-K212100TR-K212100 1/16" 10TR-K212200TR-K212200TR-K212200TR-K212200TR-K212200 1/8" 10TR-K212400TR-K212400TR-K212400TR-K212400TR-K212400 1/4" 10
GC Ferrules
VespelTM Standard Ferrules
1/16" VespelTM Ferrules: 0.5 mm id,Straight
G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s
69
TeflonTM
• Upper temperature limit 250ºC• 100% Teflon, completely inert• One-piece design requires no back ferrule
TTTTTeflonefloneflonefloneflonTMTMTMTMTM Straight Fer Straight Fer Straight Fer Straight Fer Straight Ferrrrrrules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedules - for tubing with ods as l istedReferencesReferencesReferencesReferencesReferences pkpkpkpkpkTR-K214100TR-K214100TR-K214100TR-K214100TR-K214100 1/16" 10TR-K214200TR-K214200TR-K214200TR-K214200TR-K214200 1/8" 10TR-K214400TR-K214400TR-K214400TR-K214400TR-K214400 1/4" 10
TTTTTeflonefloneflonefloneflonTMTMTMTMTM Standard Fer Standard Fer Standard Fer Standard Fer Standard Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214103TR-K214103TR-K214103TR-K214103TR-K214103 1/16" to 0.3 mm - 10TR-K214104TR-K214104TR-K214104TR-K214104TR-K214104 1/16" to 0.4 mm 0.25 mm id 10TR-K214105TR-K214105TR-K214105TR-K214105TR-K214105 1/16" to 0.5 mm 0.32 mm id 10TR-K214108TR-K214108TR-K214108TR-K214108TR-K214108 1/16" to 0.8 mm 0.53 mm id 10TR-K214110TR-K214110TR-K214110TR-K214110TR-K214110 1/16" to 1.0 mm 0.65 mm id 10
Reducing TReducing TReducing TReducing TReducing Tef lonefloneflonefloneflonTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214204TR-K214204TR-K214204TR-K214204TR-K214204 1/8" to 0.4 mm 0.25 mm id 10TR-K214205TR-K214205TR-K214205TR-K214205TR-K214205 1/8" to 0.5 mm 0.32 mm id 10TR-K214208TR-K214208TR-K214208TR-K214208TR-K214208 1/8" to 0.8 mm 0.53 mm id 10TR-K214210TR-K214210TR-K214210TR-K214210TR-K214210 1/8" to 1/16" 1/16" od 10TR-K214410TR-K214410TR-K214410TR-K214410TR-K214410 1/4" to 1/16" 1/16" od 10TR-K214420TR-K214420TR-K214420TR-K214420TR-K214420 1/4" to 1/8" 1/8" od 10
2-Hole Reducing T2-Hole Reducing T2-Hole Reducing T2-Hole Reducing T2-Hole Reducing Tef lonefloneflonefloneflonTMTMTMTMTM Fer Fer Fer Fer Ferrrrrru lesulesulesulesulesReferencesReferencesReferencesReferencesReferences Capil larCapi l larCapi l larCapi l larCapi l lary Column Fery Column Fery Column Fery Column Fery Column Ferrrrrru leuleuleuleule Fits column IDFits column IDFits column IDFits column IDFits column ID pkpkpkpkpkTR-K214222TR-K214222TR-K214222TR-K214222TR-K214222 1/8" 2-hole 0.5 mm ea 0.32 mm id 10
Ferrule Accesories and Tools
Dry Bit set
High speed steel drills let you drill ferrules to the size you need. The set includes 0.35 mm, 0.4 mm, 0.5 mm, 0.7 mm, 0.8mm, 1.0 mm and 1.2 mm drill bits and pin vise.
DrDrDrDrDry Bit Sety Bit Sety Bit Sety Bit Sety Bit SetReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K206250TR-K206250TR-K206250TR-K206250TR-K206250 Drill Bit Set
Septa Pick
This is useful for removing small pieces of graphite ferrule from the cap and fittings of the column connectors; also removespieces of septa found in threads of the injection port.
Septa PickSepta PickSepta PickSepta PickSepta PickReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205465TR-K205465TR-K205465TR-K205465TR-K205465 Septa Pick
GC Ferrules
Teflon
Septa Pick
G C F e rG C F e rG C F e rG C F e rG C F e r rrrrr u l e su l e su l e su l e su l e s
7 0
Injection Port LinersInjection Port Liners for Capillary GCs
• Fits original equipment• Polysiloxane deactivated borosilicate glass (quartz where noted)• Guaranteed inert phenols, organic acids and bases• Other configurations available on demand
These capillary injection port liners (sleeves) provide a clean, non adsorptivesurface for your sample. Regular replacement of liners eliminates "disappearingpeaks". They also protect your capillary column from potentially harmful non-volatiles that might otherwise deposit on your column.
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208110TR-K208110TR-K208110TR-K208110TR-K208110 2 mm splitless 79 mm 18740-80220 1TR-K208110-10TR-K208110-10TR-K208110-10TR-K208110-10TR-K208110-10 5181-8818 10TR-K208111TR-K208111TR-K208111TR-K208111TR-K208111 2 mm splitless, Quartz 79 mm 5181-8818 1TR-K208111-10TR-K208111-10TR-K208111-10TR-K208111-10TR-K208111-10 18740-80220 10TR-K208112TR-K208112TR-K208112TR-K208112TR-K208112 4 mm split/splitless 79 mm 1TR-K208112-10TR-K208112-10TR-K208112-10TR-K208112-10TR-K208112-10 10TR-K208122TR-K208122TR-K208122TR-K208122TR-K208122 4 mm split/splitless, Quartz 79 mm 1TR-K208122-10TR-K208122-10TR-K208122-10TR-K208122-10TR-K208122-10 10TR-K208113TR-K208113TR-K208113TR-K208113TR-K208113 4 mm split/splitless, with Deactivated Glass Wool 79 mm 19251-60540 1TR-K208113-10TR-K208113-10TR-K208113-10TR-K208113-10TR-K208113-10 10TR-K208114TR-K208114TR-K208114TR-K208114TR-K208114 Split Liner, 4 mm id with Cup 79 mm 18740-80190 1TR-K208114-10TR-K208114-10TR-K208114-10TR-K208114-10TR-K208114-10 10TR-K208115TR-K208115TR-K208115TR-K208115TR-K208115 As above, with OV-1/Chromosorb W-HP 80/100 79 mm 18740-60840 1TR-K208115-10TR-K208115-10TR-K208115-10TR-K208115-10TR-K208115-10 10TR-K208118TR-K208118TR-K208118TR-K208118TR-K208118 Direct Liner, 1.5 mm id 79 mm 18740-80200 1TR-K208118-10TR-K208118-10TR-K208118-10TR-K208118-10TR-K208118-10 10TR-K208129TR-K208129TR-K208129TR-K208129TR-K208129 Single Taper Liner, 2 mm id 79 mm 1TR-K208129-10TR-K208129-10TR-K208129-10TR-K208129-10TR-K208129-10 10TR-K208119TR-K208119TR-K208119TR-K208119TR-K208119 Single Taper Liner, 4 mm id 79 mm 5181-3316 1TR-K208119-10TR-K208119-10TR-K208119-10TR-K208119-10TR-K208119-10 10TR-K208120TR-K208120TR-K208120TR-K208120TR-K208120 As above, with Deactivated Wool 79 mm 5062-3587 1TR-K208120-10TR-K208120-10TR-K208120-10TR-K208120-10TR-K208120-10 10TR-K208116TR-K208116TR-K208116TR-K208116TR-K208116 Double Taper Liner, 4 mm id 79 mm 5181-3315 1TR-K208116-10TR-K208116-10TR-K208116-10TR-K208116-10TR-K208116-10 10
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208130TR-K208130TR-K208130TR-K208130TR-K208130 Universal Packed Inj. Liner, Deactivated 93 mm 5181-3382 1TR-K208130-25TR-K208130-25TR-K208130-25TR-K208130-25TR-K208130-25 10TR-K208132TR-K208132TR-K208132TR-K208132TR-K208132 Universal Packed Inj. Liner, Not Deactivated 93 mm 5080-8732 1TR-K208132-25TR-K208132-25TR-K208132-25TR-K208132-25TR-K208132-25 10
Agilent (HP) Injection Port Liners
For Agilent (HP) Packed Column GCs
I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s
71
Injection Port LinersNote the difference..
Between a properly deactivated liner and a non-deactivated liner. Both phenol runs were performedon the same column and GC under identical conditions except for the liners.
Column:Column:Column:Column:Column: Bonded Trifluoropropyl Polysiloxane0.25 mm I.D. x 30 m x 0.2 mm film
Temp: 50ºC(7min)-270ºCInjector: 225ºCDetector: MSD, Interface temp-290ºCCarrier gas: HE, 30cm/sec
Peaks
1. Phenol2. 2-chronophenol3. 2,4-Dimethylphenol4. 24,-Dichlorophenol5. 2-Nitrophenol6. 4-Chloro-3-methylphenol7. 2,4,6-Trichlorophenol8. 4-Nitrophenol9. Pentachlorophenol10. 2,4-Dinitrophenol11. 4,6-Dinitro-2-methyl phenol
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208330TR-K208330TR-K208330TR-K208330TR-K208330 Universal Flash Injector Liner 73 mm 37-000813-00 1TR-K208330-10TR-K208330-10TR-K208330-10TR-K208330-10TR-K208330-10 10
Varian Packed Injection Port Liners
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208310TR-K208310TR-K208310TR-K208310TR-K208310 Baffle Split Liner 72 mm 01-900109-04 1TR-K208310-10TR-K208310-10TR-K208310-10TR-K208310-10TR-K208310-10 16-000829-00 10TR-K208311TR-K208311TR-K208311TR-K208311TR-K208311 4 mm Open Split Liner 72 mm 16-0008300-00 1TR-K208311-10TR-K208311-10TR-K208311-10TR-K208311-10TR-K208311-10 10TR-K208313TR-K208313TR-K208313TR-K208313TR-K208313 4 mm Open Split Liner, with Deactivated Wool 72 mm 01-900109-01 1TR-K208313-10TR-K208313-10TR-K208313-10TR-K208313-10TR-K208313-10 10TR-K208312TR-K208312TR-K208312TR-K208312TR-K208312 Frit Split Liner 72 mm 01-900109-03 1TR-K208312-10TR-K208312-10TR-K208312-10TR-K208312-10TR-K208312-10 16-000830-01 10TR-K208314TR-K208314TR-K208314TR-K208314TR-K208314 Splitless, Borosilicate Glass 74 mm 01-900109-05 1TR-K208314-10TR-K208314-10TR-K208314-10TR-K208314-10TR-K208314-10 03-949437-90 & 00 10TR-K208315TR-K208315TR-K208315TR-K208315TR-K208315 Splitless, Quartz 74 mm 1TR-K208315-10TR-K208315-10TR-K208315-10TR-K208315-10TR-K208315-10 10TR-K208316TR-K208316TR-K208316TR-K208316TR-K208316 0.5 mm SPI 54 mm 01-900109-06 1TR-K208316-10TR-K208316-10TR-K208316-10TR-K208316-10TR-K208316-10 03-918332-01 10TR-K208318TR-K208318TR-K208318TR-K208318TR-K208318 0.8 mm SPI 54 mm 01-900109-07 1TR-K208318-10TR-K208318-10TR-K208318-10TR-K208318-10TR-K208318-10 03-918332-02 10TR-K208320TR-K208320TR-K208320TR-K208320TR-K208320 Cup Splitter 72 mm 01-900109-02 1TR-K208320-10TR-K208320-10TR-K208320-10TR-K208320-10TR-K208320-10 10TR-K208346TR-K208346TR-K208346TR-K208346TR-K208346 3.4 mm ID x 5 mm OD for 1079 54 mm 1TR-K208346-10TR-K208346-10TR-K208346-10TR-K208346-10TR-K208346-10 10
Varian Capillary Injection Port Liners
I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s
7 2 I n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o rI n j e c t i o n P o r t L i n e r st L i n e r st L i n e r st L i n e r st L i n e r s
Injection Port Liners
Carlo Erba Capillary Injection Port Liner
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208610TR-K208610TR-K208610TR-K208610TR-K208610 Splitless, 2 mm id 79 mm 453 00300 1TR-K208610-10TR-K208610-10TR-K208610-10TR-K208610-10TR-K208610-10 10
Hitachi Capillary Injection Port LinerReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208716TR-K208716TR-K208716TR-K208716TR-K208716 Double Taper Liner 68 mm 1TR-K208716-10TR-K208716-10TR-K208716-10TR-K208716-10TR-K208716-10 10
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208414TR-K208414TR-K208414TR-K208414TR-K208414 Split Liner 14A 99 mm 221-32544 1TR-K208414-10TR-K208414-10TR-K208414-10TR-K208414-10TR-K208414-10 10TR-K208416TR-K208416TR-K208416TR-K208416TR-K208416 Splitless Liner 14A 99 mm 221-32544 1TR-K208416-10TR-K208416-10TR-K208416-10TR-K208416-10TR-K208416-10 10
Shimadzu Capillary Injection Port Liners
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208240TR-K208240TR-K208240TR-K208240TR-K208240 Glass Liner for AutoSystem 112 mm N-610-1048 1TR-K208240-10TR-K208240-10TR-K208240-10TR-K208240-10TR-K208240-10 10TR-K208242TR-K208242TR-K208242TR-K208242TR-K208242 Glass Liner for 8000 Series, Sigma 2000 101 mm 0330-2221 1TR-K208242-10TR-K208242-10TR-K208242-10TR-K208242-10TR-K208242-10 10
Perkin Elmer Packed Injection Port Liners
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208232TR-K208232TR-K208232TR-K208232TR-K208232 Split Liner for Autosystem, 4mm id 92 mm N-610-1052 1TR-K208232-10TR-K208232-10TR-K208232-10TR-K208232-10TR-K208232-10 10TR-K208234TR-K208234TR-K208234TR-K208234TR-K208234 Split Liner for Autosystem, 2 mm id 92 mm N-610-1048 1TR-K208234-10TR-K208234-10TR-K208234-10TR-K208234-10TR-K208234-10 10TR-K208210TR-K208210TR-K208210TR-K208210TR-K208210 PTV Injector 88 mm N-600-2017 1TR-K208210-10TR-K208210-10TR-K208210-10TR-K208210-10TR-K208210-10 10TR-K208212TR-K208212TR-K208212TR-K208212TR-K208212 Dimple Splitter 100 mm 0330-5181 1TR-K208212-10TR-K208212-10TR-K208212-10TR-K208212-10TR-K208212-10 10TR-K208214TR-K208214TR-K208214TR-K208214TR-K208214 Splitless 100 mm 0330-5180 1TR-K208214-10TR-K208214-10TR-K208214-10TR-K208214-10TR-K208214-10 10
Perkin Elmer Capillary Injection Port Liners
Injection Liner Cleaning KitProlong the life of injection port liners and help maintain column efficiency. This kit includes four sizes of nylon brush to cleanmost of liners, and one foot of pipe cleaner for light-duty jobs. The 4 mm and 2 mm diameter brushes clean standard liners.The 1 mm and 0.5 mm diameter brushes can reach inside reversible tapered liners.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205215TR-K205215TR-K205215TR-K205215TR-K205215 Injection Sleeve Cleaning Kit
Fisons Capillary Injection Port LinerReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription LenghtLenghtLenghtLenghtLenght Equivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. NbrEquivalent Cat. Nbr..... PkPkPkPkPkTR-K208612TR-K208612TR-K208612TR-K208612TR-K208612 Split, 5 mm id 105 mm 453 20030 1TR-K208612-10TR-K208612-10TR-K208612-10TR-K208612-10TR-K208612-10 10
73
Maintenance - Kits and Tools
Capillary Survival KitTM
Save 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individuallySave 35% over items bought individually.....
Each kit includes:• Magnifier with built-in light• Slide-Lok tweezers for holding small items; "spacing" the column proper
distances into the injection port, etc.• 15 cm steel ruler• 3 column scribes, for cleanly-cut columns• 2 Universal Unions for joining broken capillary columns• Single-ended pinvise holds drill bits• 3 Drill Bits 0.4 mm, 0.5 mm and 0.8 mm• Multipurpose Septum Pick• Nylon Brushes 1/8", 3/16" and 1/4" od• Open-end wrench, 1/4" + 5/16"• High-temperature string (>400ºC) 25 ft.• Ferrule Remover• Pipecleaners 5 each 1/8" od and 1/4" od
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K-205625TR-K-205625TR-K-205625TR-K-205625TR-K-205625 Capillary Survival Kit
Packed Column Change KitThis has everything you need forhooking up columns in the GC lab. TheColumn Change Kit includes threeratchet wrenches, 7/16", 1/2" and9/16"; one ImpTM Tubing cutter, andone roll of TeflonTM tape, 1/2" x520". The ratchet wrenches are idealfor tight spaces; the ratchet tips can beopened, then snapped closed aroundfittings.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205250TR-K205250TR-K205250TR-K205250TR-K205250 Column Change Kit
Fine Wire KitThe Fine Wire Kit lets you clean manysmall items around the lab; also usefulfor bending into microhooks, other uses.The Kit contains a pin vise, and 30stainless steel wires, 10 each of thefollowing sizes: 0.006", 0.010" and0.020".
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205230TR-K205230TR-K205230TR-K205230TR-K205230 Fine Wire Kit
Needle Cleaning KitThis Kit is specifically designed forcleaning syringes and needles. Itincludes one bottle of organic,biodegradable cleaning solution, and10 each of five different diametertungsten wires, ranging in diameterfrom 0.0035" to 0.0121". Suggestedcleaning procedures are included. Thiskit is especially recommended forcleaning Hamilton Syringes.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K76620TR-K76620TR-K76620TR-K76620TR-K76620 Needle Cleaning Kit
FID Cleaning KitThe Flame Detector Cleaning Kitimproves sensibility while reducingnoise and spikes. Use it to clean boththe jet tip and collector. The FIDCleaning Kit includes everything you´llneed: three jet reamers (0.16", 0.19"and 0.024") with a unique spiraldesign that can clean without
scratching; a mini drill bit (0.0102"), two wire minibrushes, one brass and onestainless steel; and a dua-ended handle for the rearmers and brushes.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205220TR-K205220TR-K205220TR-K205220TR-K205220 FID Cleaning Kit
Injection Port Cleaning KitThis is designed for cleaning all GCInjection ports, including those inShimadzu instruments. Included are threestainless steel brushes, 5mm (forShimadzu), 1/4" and 3/8", and onescraper for removing septum residue.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K206211TR-K206211TR-K206211TR-K206211TR-K206211 Inj. Port Cleaning Kit
Utility Ring StandThis nickel-plated ring stand is usefulfor holding bubble flowmeters, as wellas wide variety of standard labequipment. The support rod is 5/16"od x 20".
Clamps are available separately. Theplastic-coated jaws hold aroundglassware from, 3/8" to 13/8" in
diameter. The small clamp is useful for securing items 3/8" in diameter and less(10 ml and less bubble flowmeters; thermometers). Rotates 360ºC. The RingStand Clamps are made from zinc-platted steel.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205570TR-K205570TR-K205570TR-K205570TR-K205570 Utility Ring StandTR-K205571TR-K205571TR-K205571TR-K205571TR-K205571 Large Ring Stand ClampTR-K205572TR-K205572TR-K205572TR-K205572TR-K205572 Small Ring Stand Clamp
M a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d T o o l so o l so o l so o l so o l s
7 4
Maintenance - Kits and ToolsGlass Tubing Cutter
For shortering glass columns or inserts;other applications involving glasstubing. The hardended steel cutingwheel scores tubing as it is turned;cuts tubing up to 1.5".
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205595TR-K205595TR-K205595TR-K205595TR-K205595 Glass Tubing CutterTR-K2055969TR-K2055969TR-K2055969TR-K2055969TR-K2055969 Spare Cutting Wheels, 5/pk
StopwatchThis 1/00th second Stopwatch hassplit/lap and normal time. It displayshours, minutes, seconds, day, date andmonth. Quartz accuracy. Useful formeasuring gas glow with bubbleflowmeters. Has alarm feauture.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205200TR-K205200TR-K205200TR-K205200TR-K205200 Stopwatch
Adjustable Wrench6 inch or 10 inch. The 6" wrench opensto 15/16" for all common Swage-lokconnectors. The 10" wrench opens to15/16" for standard CGA fittings.Chronomeplated, drop-forged steel.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205586TR-K205586TR-K205586TR-K205586TR-K205586 Adjustable Wrench 6 inchTR-K205588TR-K205588TR-K205588TR-K205588TR-K205588 Adjustable Wrench 10 inch
Ratchet WrenchThe jaws of the Ratchet Whrench open,to slip over fittings already in place.Makes tightering or loosening incramped areas easy. Three sizesavailable: 7/16", 1/2" or 9/16"
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205593TR-K205593TR-K205593TR-K205593TR-K205593 Ratchet Wrench 7/16"TR-K205592TR-K205592TR-K205592TR-K205592TR-K205592 Ratchet Wrench 1/2"TR-K205591TR-K205591TR-K205591TR-K205591TR-K205591 Ratchet Wrench 9/16"
Goose-neck FlashlightIluminates hard-to-reach areas. TheGoose-neck flashlight has a flexible neckwhich can be bent as desired. Includesbatteries.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205628TR-K205628TR-K205628TR-K205628TR-K205628 Goose-neck Flashlight
Jeweler´s ScrewDriversSix flaat-head screwdrivers whithconvenient swivel-top handles. Baldesare from 0.025" to 0.100" in width.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205676TR-K205676TR-K205676TR-K205676TR-K205676 Jeweler´s ScrewDrivers
Allen Wrench SetStandard or Metric. The standard(USA) Allen wrenches come in a set of9, from 0.050" to 3/16". The metricAllen wrenches come in a set of 7,from 1.5mm to 6mm.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205670TR-K205670TR-K205670TR-K205670TR-K205670 Allen Wrench Set StandardTR-K205671TR-K205671TR-K205671TR-K205671TR-K205671 Allen Wrench Set Metric
Micro HookThis is a multi-purpose hook used forpulling O-rings, springs, or septumfragments.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205678TR-K205678TR-K205678TR-K205678TR-K205678 Micro Hook
Magnet on a StickThis is used to pick up small objectssuch as screws and nuts frominstrumet cabinets and circuit boards.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205630TR-K205630TR-K205630TR-K205630TR-K205630 Magnet on a Stick
Threadulator Thread CutterCleans up cross-threated fittings oncolumns, etc.; use with weldedinstrumet fittings to avoide expensivereplacement. Knurled otuter handle forsecure gripping; hardless steel cutter.Available in three sizes.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205638TR-K205638TR-K205638TR-K205638TR-K205638 Threeadulator, 1/16"TR-K205640TR-K205640TR-K205640TR-K205640TR-K205640 Threeadulator, 1/8"TR-K205642TR-K205642TR-K205642TR-K205642TR-K205642 Threeadulator, 1/4"
TeflonTM TapeThis is great for leak-proofing fittings;dry-lubricating joints. Do not use overferrules. Teflon tape comes in rolls of520 inces, 1/2" wide.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205117TR-K205117TR-K205117TR-K205117TR-K205117 Teflon Tape
M a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d T o o l so o l so o l so o l so o l s
75
Maintenance - Kits and ToolsCapillary/HPLC Wrench Set
This set includes 4 wrenches for useon 1/32", 1/16", or 1/8" nuts. Thewrench ends are 3/16", 1/4", 5/16", 3/8" and 7/16".
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205320TR-K205320TR-K205320TR-K205320TR-K205320 Capillary/HPLC Wrench Set
Mirror on a StickThe Mirror on a Stick lets you peeraround corners or tight spaces; alsoused at the outlet of flame detectors;condensation on the mirror indicatesthe flame is lit.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205632TR-K205632TR-K205632TR-K205632TR-K205632 Mirror on a Stick
Open End WrenchesThis set fits most types of fittings.Sizes range from 5/16" to 9/16" in1/16" increments. Made fromchromeplated steel. 5 wrenches.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205622TR-K205622TR-K205622TR-K205622TR-K205622 Open End Wrenches
Lighted MagnifierThis is perfect for inspecting capillaryend cuts and syringe tips. The 11/4"x 11/4 lens magnifiers 4x; smallbifocal insert lens measures 8x. Keepone in your desk. Batteries included.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205648TR-K205648TR-K205648TR-K205648TR-K205648 Lighted Magnifier
Needle-Nose PliersThese are useful for picking up orclamping small parts. Comes with vinylgrips for sure grip.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205626TR-K205626TR-K205626TR-K205626TR-K205626 Needle-Nose Pliers
4-in-1 ScrewdriverComes with two double-ended heads,each with a flat and phillips head. Justflip the end to change the tip.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205624TR-K205624TR-K205624TR-K205624TR-K205624 4-in-1 Screwdriver
Wire Stripper/CrimperUseful for cutting or stripping wire, andcrimping on connectors. For repairs,maintenance, prototyping.
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-K205574TR-K205574TR-K205574TR-K205574TR-K205574 Wire Stripper/Crimper
M a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d TM a i n t e n a n c e - K i t s a n d T o o l so o l so o l so o l so o l s
7 6
Chart Paper
C h a rC h a rC h a rC h a rC h a r t P a p e rt P a p e rt P a p e rt P a p e rt P a p e r
Chart Paper
• High Quality Chart Papers• Available for many popular Integrators and recorders• Buy the Case for Bigger Savings
Papers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett PackardPapers for Hewlett Packard
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K443181TR-K443181TR-K443181TR-K443181TR-K443181 5880A, 3888A 8.5" x 184´, Z-fold blue 5/cs 5080-8778TR-K443182TR-K443182TR-K443182TR-K443182TR-K443182 8.5" x 184´, Z-fold black 5/cs 9270-0658
TR-K443192TR-K443192TR-K443192TR-K443192TR-K443192 5840A, 5880 GC, 8.5" x 184´, Z-fold blue 5/cs 5080-87353380A, 3385A Int.
TR-K443193TR-K443193TR-K443193TR-K443193TR-K443193 1082, 1084 LC 8.5" x 184´, Z-fold black 5/cs
TR-K443194TR-K443194TR-K443194TR-K443194TR-K443194 3392, 3393A Int. 4.2" x 400´, roll blue 2/cs 5080-8800TR-K443195TR-K443195TR-K443195TR-K443195TR-K443195 4.2" x 400´, roll black 2/cs
TR-K443191TR-K443191TR-K443191TR-K443191TR-K443191 3396A 9.5" x 272´, roll, ink jet 4/cs 5181-1219TR-K443179TR-K443179TR-K443179TR-K443179TR-K443179 3396A 8.5" x 230,´ Z-fold ink jet 5/cs 5062-3561
Papers for ShimadzuPapers for ShimadzuPapers for ShimadzuPapers for ShimadzuPapers for Shimadzu
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K441610TR-K441610TR-K441610TR-K441610TR-K441610 CR1A, CR1B 8 3/16" x 170´, roll black 1 roll 221-13391-01TR-K443612TR-K443612TR-K443612TR-K443612TR-K443612 CR3A 8 3/16" x 167´, roll black 10/cs 221-25412-00TR-K441613TR-K441613TR-K441613TR-K441613TR-K441613 CR4A 255 mm x 148", black 1 roll 223-02000-12TR-K443615TR-K443615TR-K443615TR-K443615TR-K443615 CR5A 208 mm x 148", black 10/cs 223-02037-81TR-K441617TR-K441617TR-K441617TR-K441617TR-K441617 CR7A 10 1/6" x 148´ 1 roll 200-91527
Papers for VPapers for VPapers for VPapers for VPapers for Var ianar ianar ianar ianar ian
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K443620TR-K443620TR-K443620TR-K443620TR-K443620 3400/3500/3600 4.3" x 150´, black 2/cs 03-917650TR-K443604TR-K443604TR-K443604TR-K443604TR-K443604 Vista 401/402 8.5" x 184´, Z-fold, black 5/cs 03-906362-0TR-K441599TR-K441599TR-K441599TR-K441599TR-K441599 4270/4290 9.4" x 183´, roll, black 1 roll 00-997096-01
Papers for WPapers for WPapers for WPapers for WPapers for Watersatersatersatersaters
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K441608TR-K441608TR-K441608TR-K441608TR-K441608 730 8.5" x 184´, Z-fold, blue 1 pack 74703
Thermal Paper
77C h a rC h a rC h a rC h a rC h a r t P a p e rt P a p e rt P a p e rt P a p e rt P a p e r
Papers for HitachiPapers for HitachiPapers for HitachiPapers for HitachiPapers for Hitachi
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K443170TR-K443170TR-K443170TR-K443170TR-K443170 234 mm x 160´, black 9/cs 661-7501
Papers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin ElmerPapers for Perkin Elmer
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K441189TR-K441189TR-K441189TR-K441189TR-K441189 LC1-100 283 mm x 100´, Roll, black 1 roll N-625-1026
Papers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra PhysicsPapers for Spectra Physics
ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
TR-K443596TR-K443596TR-K443596TR-K443596TR-K443596 SP-4000 Series 9.4" x 184´, Z-fold, black 5/cs A0022-020TR-K443598TR-K443598TR-K443598TR-K443598TR-K443598 SP-4270, SP-4290 9.4" x 167´, roll, black 10/cs A2157-020
Chromojet, CH1, CH2
Chart Paper
Recorder PaperManufacturerManufacturerManufacturerManufacturerManufacturer ReferencesReferencesReferencesReferencesReferences Model NumberModel NumberModel NumberModel NumberModel Number CharCharCharCharChart Tt Tt Tt Tt Typeypeypeypeype QtyQtyQtyQtyQty..... Manuf. CharManuf. CharManuf. CharManuf. CharManuf. Chart Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbrt Paper Nbr.....
HoustonHoustonHoustonHoustonHouston TR-K443198TR-K443198TR-K443198TR-K443198TR-K443198 D-5000, B-5000 11" X 100´roll, 0-10 English 4/cs EC-103Kipp & ZonenKipp & ZonenKipp & ZonenKipp & ZonenKipp & Zonen TR-K441199TR-K441199TR-K441199TR-K441199TR-K441199 BD111/12, BD40/41 230 mm x 66´, 0-100 1 roll XR-9LinearLinearLinearLinearLinear TR-K441184TR-K441184TR-K441184TR-K441184TR-K441184 1201/1202/1210 230 mm x 83´, roll 1 roll 0100-0026LinearLinearLinearLinearLinear TR-K441186TR-K441186TR-K441186TR-K441186TR-K441186 142/143 120 mm x 100´, roll 1 roll 0100-0011Perkin ElmerPerkin ElmerPerkin ElmerPerkin ElmerPerkin Elmer TR-K441395TR-K441395TR-K441395TR-K441395TR-K441395 56/200/561 276 mm x 100´, roll 1 roll 056-7300
7 8
Gas & Handling Purification
Indicating Oxygen Trap
• High efficiency. Reduces O2 to less than 0,1 ppm• Changes color from bright green to brown when adsorption capacity is depleted• Non-contaminating glass tube
This safe, compact unit has a capacity of 40 cc of pure oxygen; it will removeoxygen from a full 200 ft3 cylinder of helium with purity specification of 99,995 %(assuming 20 % impurity is oxygen; or several cylinders of higher purity helium).The non contaminating, heavy-walled inner glass tube of catalyst is protected fromaccidental breakage by the outer plastic tube.
Maximum pressure is 100 psig. The indicating oxygen trap is delivered in theactive state, filled with high purity helium. It is recommended that the trap bepurged with the gas you will be using. Approximate dimensions: 1 3/8” x 10 1/4”
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202220TR-K202220TR-K202220TR-K202220TR-K202220 Indicating Oxygen Trap 1/8” fittingsTR-K202223TR-K202223TR-K202223TR-K202223TR-K202223 Indicating Oxygen Trap 1/4” fittings
Model 1000 Oxygen Trap
• High capacity, can remove 2.5 liters of O2
• Exceptional efficiency, less than 70 ppb oxygen concentration at the outlet
This is highest capacity oxygen trap, for long term protection of capillary columnstationary phases against oxidation at GC operating temperatures. It is alsorecommended for packed column carrier gases. The Model 1000 has a capacity of2,5 liters of oxygen at room temperature; its capacity is even higher at 100 ºC . Itis also effective for removing sulfur compounds, such as hydrogen sulfide andmercaptans. The Model 1000 is intended for use with non oxidizing gases such asHe, Ar, N2, H2, or CH4, containing less than 1 % oxygen. It will remove oxygen tobelow 70 ppb from these gases at flow rates normally encountered in GC .
The Model 1000 oxygen trap is a high pressure metal cylinder filled with 500 ccof active oxygen adsorbent. The adsorbent binds covalently with oxygen; no gas isgenerated from this reaction. It is delivered in the active state, filled with highpurity helium. It is ready for use, but we recommended that the trap be purgedwith the gas you will be using. Maximum flow rate for nominal pressure drop is 1liter/min; maximum pressure 1000 psig. Approximate dimensions 2” x ¼”including fitting. Weight 3 pounds.
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202200TR-K202200TR-K202200TR-K202200TR-K202200 Model 1000 Oxygen Trap 1/8” fittingsTR-K202202TR-K202202TR-K202202TR-K202202TR-K202202 Model 1000 Oxygen Trap 1/4” fittings
Moisture /Oil / Dust traps
• Recommended for FID supply gases; cleaner gas improves baseline stabilityfor more accurate analysis
• Molecular sieve 5A provide high efficiency drying• Indicating DrieriteTM warns of leaks in the gas stream• Acrylic or glass construction for low permeability; inertness
Big Trap
This removes moisture, oil and dust from wet supply gas before it flow into yourFID detector. It can also be used to purity hydrogen in flame ionization detectors.Maximum pressure is 100 psig . The Big Trap has a 400 cc total volume ofindicating DrieriteTM and molecular sieve 5 A in a clear acrylic tube. The DrieriteTM
changes from blue to pink at 5 % relative humidity to warn of leaks in the gasstream. Our unique O-ring design allows hand removal of the cartridge withoutdisconnecting the fittings from the line, while a plastic insert at each end keeps thepacking from spilling. Available with 1/8” or 1/4” fittings. Dimensions 2 1/4" x17" including fittings.
Oxygen Traps Oxygen Traps
• Recommended for all GC and GC/MS carrier gas• Reduce capillary column phase degradation
Moisture traps, Moisture/ Oil / Dust Traps
• Recommended for detector suply gases• Improves baseline stability
Hydrocarbons Traps
• Recommended for H2 and air detector supply gases• Activated charcoal adsorbent for highly efficient contaminant removal• Can also be used for purge and trap; organic analysis applications.
G a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o n
79
Gas & Handling Purification
Safe Glass Moisture Trap
This filter is designed for use with GC detectors needing very high purity gases,such as electron capture or Hall electrolytic conductivity. Gas contacts only glass,metal and the adsorbents for purity, and the trap may be used in any orientation.An internal screen at each end prevents particulate contamination. The Safe GlassTrap is enclosed in a plastic outer sheath. The outer sheath can be removed toreactivate the inner glass tube by baking under inert gas flow; instructionsincluded. It contains 55 cc total absorbents . Maximum pressure is 100 psig.Dimentions 1 3/8” x 10 1/4”.
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202260TR-K202260TR-K202260TR-K202260TR-K202260 Big Trap 1/8” fittingsTR-K202262TR-K202262TR-K202262TR-K202262TR-K202262 Big Trap 1/4” fittingsTR-K202266TR-K202266TR-K202266TR-K202266TR-K202266 Safe Glass Moisture Trap for ECD 1/8” fittingsTR-K202268TR-K202268TR-K202268TR-K202268TR-K202268 Safe Glass Moisture Trap for ECD 1/4” fittings
Hydrocarbon Trap / CO2 Trap
Model 300 High Pressure Hydrocarbon Trap
This high pressure metal cylinder filled with 500 cc of activated charcoal, one ofthe most effective adsorbents for organics and hydrocarbons. It will remove allhydrocarbons at room temperature except methane, from your FID air and H2 lines,to minimize noise and extraneous peaks in the signal. It is also recommended foruse with purge and trap apparatuses, and with GC carrier gases for trace analyses.Highest efficiency is obtained using flow rates bellow 500cc/min. Frits in each endprevent fines from entering the gas stream. The Model 300 is delivered filled withhigh purity helium; It should be purged before use with the gas you will be using.Maximum pressure is 1000 psig. The Model 300 comes with 1/8" or 1/4" fittings.Approximate dimensions 2" x 14".
Model 100 Safe Glass Hydrocarbon Trap
The Model 100 is designed to provide organics free gas, with an indicator formoisture contamination. The gas contacts only metal or glass for high purity. Itcontains indicating DrieriteTM and activated charcoal; the inner glass tube isprotected by an outer tube of clear plastic. Internal stainless steel screens at end ofthe trap protect against fines entering the gas stream. It can be used in anyorientation without gas channeling. The Trap can be regenerated by heating underinert gas flow after removing the outer plastic guard; instructions included. TheTrap should be purged before use with the gas you will be using . Maximumpressure is 100 psig. The Model 100 is supplied with 1/8" or 1/ 4" fittings.Approximate dimensions 1 3/8" x 10 1/4".
Carbon Dioxide Trap
Remove carbon dioxide from your gas stream with our carbon dioxide Trap. Highcapacity, it will irreversibly bind 100 g of carbon dioxide. Its unique design usesNaOH blended with molecular sieve to scrub out CO2. The reaction produce waterwhich is adsorbed by the molecular sieve. Not recommended for GC use. Whendrown stream water is a concern we recommended using a second moisture trap inline as a safety measure. Maximum pressure for the Carbon Dioxide, trap is 1000psig; approximate dimension 2” x 14”
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionTR-K202330TR-K202330TR-K202330TR-K202330TR-K202330 Model 300 Hydrocarbon Trap 1/8" fittingsTR-K202332TR-K202332TR-K202332TR-K202332TR-K202332 Model 300 Hydrocarbon Trap 1/4" fittingsTR-K202340TR-K202340TR-K202340TR-K202340TR-K202340 Model 100 Safe Glass Hydrocarbon Trap 1/8" fittingsTR-K202342TR-K202342TR-K202342TR-K202342TR-K202342 Model 100 Safe Glass Hydrocarbon Trap 1/4" fittingsTR-K202350TR-K202350TR-K202350TR-K202350TR-K202350 Carbon Dioxide Trap 1/8" fittingsTR-K202352TR-K202352TR-K202352TR-K202352TR-K202352 Carbon Dioxide Trap 1/4" fittings
G a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o nG a s H a n d l i n g & P u r i f i c a t i o n
8 0
Super-Clean Gas Filters
A revolution in gas purifying of GC and GC/MS gases
Unique «POINT-OF-USE» and «SEMI IN-LINE» glass/metal, diffusionproof Super-Clean Gas Filters, purify the delicate carrier and burner gases for your GC and GC/MS system for Hydrocarbons, Oxygen (colour indicated) and Moisture (colourindicated) to better-as 6.0 gas (99,9999%) quality, independent of the originalgas quality.
Analytical advantages of SGT Super-Clean Gas Filters
• Longer lifetime of analytical columns, avoids bleeding, espec. important forMS and ECD.
• Better sensitivity, decreases baseline noise, eliminates spikes.
• Filter-change during analysis within seconds, system stays online.
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81
Spec’s on SGT Super-Clean Gas Filters
• The specified lifetimes are strongly depending of the quality of the incominggas.
• Effectivity: <0.1 ppm at a flowrate of 2 liters/minute
Benefits of the “quick-fit” system:
• Filter replacement within seconds.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.- El iminates GC downtime.
• Tool-less filter replacement.- Easy handling- Easy handling- Easy handling- Easy handling- Easy handling
• Diffusion-proof Baseplate (also during filter replacement).- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.- El iminates analytical disturbance.
• Baseplates can be wall-mounted.- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning- Convenient posit ioning
Standard Configurations
P U R I F I C A T I O N O F C A R R I E R G A S
• Removal of Oxygen, moisture and hydrocarbons for longer column lifetime andcleaner baseline.
• Use a Triple filter on 1-position baseplate.
• Excelent for Carrier gas and ECD, MS applications
SG-F0301SG-F0301SG-F0301SG-F0301SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)SG-B0010SG-B0010SG-B0010SG-B0010SG-B0010 Baseplate for 1 Super Clean Gasfilter
Super-Clean Gas FiltersP U R I F I C A T I O N O F G A S E S F O R F I D
• Removal of moisture and hydrocarbons in the gases of the FID for a betterbaseline.
• 2 Combi filter (Hydrocarbons/moisture) (One for Air & one for Hydrogen)
2u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture).
2u. of SG-B00102u. of SG-B00102u. of SG-B00102u. of SG-B00102u. of SG-B0010 Baseplate for 1 Super Clean Gasfilter
P U R I F I C A T I O N F O R C A R R I E R A N D F I D G A S E S
• The full solution for your GC/FID system
• Use a Triple + 2 Combi filter (One for Air & one for Hydrogen)
1u. of SG-F03011u. of SG-F03011u. of SG-F03011u. of SG-F03011u. of SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)
2u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F02012u. of SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture).
3u. of SG-B00103u. of SG-B00103u. of SG-B00103u. of SG-B00103u. of SG-B0010 Baseplate for 1 Super Clean Gasfilter
H I G H C A P A C I T Y P U R I F I E R S F O R C A R R I E R A N D F I D G A S E S
• Recomended for low quality gases
• Use Ultra Capacity Moisture and Oxygen filters for carrier + 2 Ultra CapacityHydroCarbon filter (One for Air & one for Hydrogen)
1u. of SG-F01011u. of SG-F01011u. of SG-F01011u. of SG-F01011u. of SG-F0101 Moisture filter, standard, ultra capacity
1u. of SG-F01021u. of SG-F01021u. of SG-F01021u. of SG-F01021u. of SG-F0102 Oxygen filter,standard, ultra capacity
2u. of SG-F01032u. of SG-F01032u. of SG-F01032u. of SG-F01032u. of SG-F0103 Hydrocarbons filter,standard, ultra capacity
4u. of SG-B00104u. of SG-B00104u. of SG-B00104u. of SG-B00104u. of SG-B0010 Baseplate for 1 Super Clean Gasfilter
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionSG-B0010SG-B0010SG-B0010SG-B0010SG-B0010 Baseplate for 1 Super Clean GasfilterSG-B0020SG-B0020SG-B0020SG-B0020SG-B0020 Baseplate for 2 filtersSG-B0030SG-B0030SG-B0030SG-B0030SG-B0030 Baseplate for 3 filtersSG-F0101SG-F0101SG-F0101SG-F0101SG-F0101 Moisture filter, standard, ultra capacitySG-F0102SG-F0102SG-F0102SG-F0102SG-F0102 Oxygen filter,standard, ultra capacitySG-F0103SG-F0103SG-F0103SG-F0103SG-F0103 Hydrocarbons filter,standard, ultra capacitySG-F0301SG-F0301SG-F0301SG-F0301SG-F0301 Filter,Triple (O2/Moisture/Hydrocarbons)SG-F0201SG-F0201SG-F0201SG-F0201SG-F0201 Filter,Combi, high capacity, (Hydrocarbons/moisture)SG-F0730SG-F0730SG-F0730SG-F0730SG-F0730 Filter bundle of 3 (Triple + 2x Hydrocarbons/ moisture
Combi)SG-F0740SG-F0740SG-F0740SG-F0740SG-F0740 Filter bundle of 4 (standard : oxygen, moisture +
2x Hydrocarbons)
One position platform
Quick-Fit System
S u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r sS u p e r C l e a n G a s F i l t e r s
8 2
Helium Gas Leak Check
H e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c kH e l i u m G a s L e a c k C h e c k
Helium Gas Leak Check
• Pipe fittings• Welding parts• Pressure regulators
Specifications
Detection Method: Thermal Conductivity DetectorTarget gas: HeliumRange: High/LowSensibility: Minimum Detection Limit 0.01 mL/minDisplay: LCDPower Supply: Rechargeable BatteryOperation Temp: 10-35ºCDimensions: 65 (W) x 37 (D) x 143 (H) mmWeight: 330g approx.Accesories: Recharger AC 100 - 220v
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescriptionGL-2702-1941GL-2702-1941GL-2702-1941GL-2702-1941GL-2702-1941 Helium Gas Leak Detector LD 229GL-XXXXXGL-XXXXXGL-XXXXXGL-XXXXXGL-XXXXX Recharger AC 100 - 220v
83
Teknokroma 2t Head Space Sampler
The Teknokroma 2t Head Space Sampler for Head Space techniquewithin your reach with a low cost and high precision level
The 2t sampler is the first manual system for Static Head Space which allows theapplication of this technique in a quantitative, economical and precise manner.
Now it is possible to use the Static Head Space technique with a manualequipment. the Teknokroma 2t sampler is a low cost, high versatility and easyoperations system. For this reason the Static Head Space technique is beingsuccesfully introduced to laboratories.
The new 2t sampler makes the Head Space technique available to all GasChromatography users.
It complies with all the European CE requirements.
Applications
• Volatiles in pharmaceuticals
• Flavours analysis in food and cosmetic products
• Alcohol and other toxic compounds in blood
• Screening of volatiles in all type of environmental samples (soils, waters,plastics, polymers, etc.)
It is according the Pharmacopeia test:
European Pharmacopeia 4th. (2002). "Gas Chromatography will static head-spaceinjection 2.2.28". "It is possible to use airtight syringes and a conventionalchromatograph".
USP 26(2003 <467> Organic Volatile Impurities: "Proceed as direct underMethod V, except to inject, using a heated gas-tight syringe, 1 ml. of theheadspace".
Technical specifications
Heating temperature Range: up to 120ºC.Variable injection: up to 2,5 ml.Temperature accuracy: +/- 0,5ºCHolds up to 6 vials of: 2, 4, 6, 9, 10, 12, 20, 22 and 27 ml.Sampling time control with accoustic alarm: 1 to 99 secondsEquilibrium time control with accoustic alarm: 1 to 99 minutesStabilization time from 25ºC to 70ºC with1 ml syringe and 6 empty 20 ml vials: 8 minutesSafety temperature: 150ºCPower: 220 +/- 10% VAC.
The F irst Manual SystemFor Stat ic Head Space
TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r
8 4 TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r
Teknokroma 2t Head Space Sampler
a. Insert the syringe holder into the heating block.b. Set the temperature and the equilibrium time with the keyboard.c. Press the start.
3
Insert the closed vials with the sample into the heating block.
2
Inject the sample into the GC.Repeat this sequence for the additional samples.
5
Put the syringe into the black holder.
1
After the equilibrium time is achieved, move the syringe holder intovial number 1, and aspirate the sample by moving the plunger upuntil the prefixed volume is reached.
4
85
Teknokroma 2t Head Space Sampler
Retention time (min.)Benzene 1.45Toulene 2.85
Chromatographic parametersChromatographic parametersChromatographic parametersChromatographic parametersChromatographic parametersColumn: TRB-1TRB-1TRB-1TRB-1TRB-1, P/N TR-113015Dimensions: 15m x 0,53mm x 3µmInjection: 0,7 ml, head space, (split 1:2), 150ºCCarrier gas: He, 4psi (27.6 kPa)Oven temperature: 60ºC (10 min.)Detector: FID, 250ºCSample: 5ml in 10ml vials (25ppm benzene/toulene in water)
Headspace condit ionsHeadspace condit ionsHeadspace condit ionsHeadspace condit ionsHeadspace condit ions10ml vials, P/N CC-10-CVCap with blue silicone/PTFE seal P/N CC-20-ST3Healting block temperature: 75ºCEquilibrium time: 30 minutesSampling time: 30 secondsSyringe used: 1ml (1001 LTN, pst 5, P/N HA-81343)Sampled volume: 0,7ml
Performance qualification
To check the Head Space sampler, proper performance, the followingreproductibility test is recommended. In this test, we check not only the equipmentperformance but we also evaluate:
• The vials are correctly sealed.• The sampling procedure followed by the analyst is correct• The Gas Chromatograph works properly• The data-aquisition system works properly
Sample preparation
Add 2.5 µl of benzene and 2.5 µl mof toulene to 100 ml of water (25ppm), stirup until it is completely dissolved.
Adjust headspace sample conditions and inject. Integrate the benzene and toluenepeacks of the 6 chromatograms obtained. The Relative Standard Deviation of thearea quotients must be lower than 5%.
Benzene areaBenzene areaBenzene areaBenzene areaBenzene area TTTTToulene areaoulene areaoulene areaoulene areaoulene area Area RatioArea RatioArea RatioArea RatioArea Ratio3418.4613418.4613418.4613418.4613418.461 5441.008 0.6283466.1253466.1253466.1253466.1253466.125 5449.905 0.6253359.1763359.1763359.1763359.1763359.176 5381.354 0.6243316.6463316.6463316.6463316.6463316.646 5374.388 0.6243782.4043782.4043782.4043782.4043782.404 6035.683 0.6273794.0263794.0263794.0263794.0263794.026 6063.646 0.626
Mean VMean VMean VMean VMean Valuealuealuealuealue 0.626Standard deviation (SD)Standard deviation (SD)Standard deviation (SD)Standard deviation (SD)Standard deviation (SD) 0.00163Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD)Relative standard deviation (RSD) 0.26%
ReferenceReferenceReferenceReferenceReference DescriptionDescriptionDescriptionDescriptionDescriptionTR-132110TR-132110TR-132110TR-132110TR-132110 2t Sampler for Static Head Space mod. 5060
(syringe not included)HA-81343HA-81343HA-81343HA-81343HA-81343 Syringe Hamilton 1 ml.1001 LTN point style 5HA-81443HA-81443HA-81443HA-81443HA-81443 Syringe Hamilton 2,5 ml. 1002 LTN point style 5
TTTTT e k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e re k n o k r o m a 2 t H e a d S p a c e S a m p l e r
8 6
Headspace Vials & AccesoriesHeadspace Vials• 20 mm crimp finish is beveled for a tigher seal.• Borosilicate glass• Flat bottom vials feature a slightly longer neck - custom fit for Carlo Erba
and Agilent.• Rounded bottom vials are specifically designed for Pekin-Elmer; also use with
Tekmar and Varian.
Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs VVVVVia lia lia lia lia l VVVVVolumeolumeolumeolumeolume DimmensionsDimmensionsDimmensionsDimmensionsDimmensionsCC-C4020-20/PCC-C4020-20/PCC-C4020-20/PCC-C4020-20/PCC-C4020-20/P CC-C4020-20CC-C4020-20CC-C4020-20CC-C4020-20CC-C4020-20 Flat Bottom 20 ml 23 x 75 mmCC-C4020-10/PCC-C4020-10/PCC-C4020-10/PCC-C4020-10/PCC-C4020-10/P CC-C4020-10CC-C4020-10CC-C4020-10CC-C4020-10CC-C4020-10 Flat Bottom 10 ml 23 x 46 mmCC-C4020-2/PCC-C4020-2/PCC-C4020-2/PCC-C4020-2/PCC-C4020-2/P CC-C4020-2CC-C4020-2CC-C4020-2CC-C4020-2CC-C4020-2 Rounded Bottom 20 ml 23 x 75 mmCC-C4020-210/PCC-C4020-210/PCC-C4020-210/PCC-C4020-210/PCC-C4020-210/P CC-C4020-210CC-C4020-210CC-C4020-210CC-C4020-210CC-C4020-210 Rounded Bottom 10 ml 23 x 46 mm
Headspace 20 mm Crimp Seals• Use with all Headspace vials
References 1000/csReferences 1000/csReferences 1000/csReferences 1000/csReferences 1000/cs Seal DescriptionSeal DescriptionSeal DescriptionSeal DescriptionSeal DescriptionCC-C4020-3ACC-C4020-3ACC-C4020-3ACC-C4020-3ACC-C4020-3A One-Piece unlined 20 mm aluminium crimp seals onlyCC-C4020-6ACC-C4020-6ACC-C4020-6ACC-C4020-6ACC-C4020-6A One-Piece pressure release unlined 20 mm crimp seals only. Pressure will vent
when a 3 bar +/- 0.5 rating is exceeded within the vial
Headspace 20 mm Crimp Seals with Septa• Pre-assembled 20 mm crimp seals with septa• Ready-to-use with any Headspace vials
Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs VVVVVia lia lia lia lia l VVVVVolumeolumeolumeolumeolume DimmensionsDimmensionsDimmensionsDimmensionsDimmensionsCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/PCC-C4020-32A/P CC-C4020-32ACC-C4020-32ACC-C4020-32ACC-C4020-32ACC-C4020-32A Tan PTFE/White Silicone Regular - 60 to 125ªCCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/PCC-C4020-32AP/P CC-C4020-32APCC-C4020-32APCC-C4020-32APCC-C4020-32APCC-C4020-32AP Tan PTFE/White Silicone Pressure Release - 60 to 125ªCCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/PCC-C4020-34A/P CC-C4020-34ACC-C4020-34ACC-C4020-34ACC-C4020-34ACC-C4020-34A Ivory PTFE/Red Rubber Regular - 40 to 100ªCCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/PCC-C4020-34AP/P CC-C4020-34APCC-C4020-34APCC-C4020-34APCC-C4020-34APCC-C4020-34AP Ivory PTFE/Red Rubber Pressure Release - 40 to 100ªCCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/PCC-C4020-36A/P CC-C4020-36ACC-C4020-36ACC-C4020-36ACC-C4020-36ACC-C4020-36A Gray PTFE/Black Butyl Molded Septa Regular - 40 to 125ªCCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/PCC-C4020-36AP/P CC-C4020-36APCC-C4020-36APCC-C4020-36APCC-C4020-36APCC-C4020-36AP Gray PTFE/Black Butyl Molded Septa Pressure Release - 40 to 125ªC
Headspace 20 mm Septa
Reference 100/pkReference 100/pkReference 100/pkReference 100/pkReference 100/pk Ref. 1000/csRef. 1000/csRef. 1000/csRef. 1000/csRef. 1000/cs SeptaSeptaSeptaSeptaSepta TTTTTemp. Rangeemp. Rangeemp. Rangeemp. Rangeemp. RangeCC-C4020-30/PCC-C4020-30/PCC-C4020-30/PCC-C4020-30/PCC-C4020-30/P CC-C4020-30CC-C4020-30CC-C4020-30CC-C4020-30CC-C4020-30 Gray Butyl Stopper -20 to 120ªCCC-C4020-32/PCC-C4020-32/PCC-C4020-32/PCC-C4020-32/PCC-C4020-32/P CC-C4020-32CC-C4020-32CC-C4020-32CC-C4020-32CC-C4020-32 Tan PTFE/White Silicone -60 to 125ªCCC-C4020-34/PCC-C4020-34/PCC-C4020-34/PCC-C4020-34/PCC-C4020-34/P CC-C4020-34CC-C4020-34CC-C4020-34CC-C4020-34CC-C4020-34 Ivory PTFE/Red Rubber -40 to 100ªCCC-C4020-36/PCC-C4020-36/PCC-C4020-36/PCC-C4020-36/PCC-C4020-36/P CC-C4020-36CC-C4020-36CC-C4020-36CC-C4020-36CC-C4020-36 Gray PTFE Black Butyl Molded Septa -40 to 125ªC
20 mm Crimping & Decapping Tools• For Headspace vials and any 20 mm crimp seals
ReferencesReferencesReferencesReferencesReferences DescriptionDescriptionDescriptionDescriptionDescription PkPkPkPkPkCC-C4020-100CC-C4020-100CC-C4020-100CC-C4020-100CC-C4020-100 Manual Crimper, 20 mm 1CC-C4020-101CC-C4020-101CC-C4020-101CC-C4020-101CC-C4020-101 Decapping Pliers, 20 mm 1CC-C4020-102CC-C4020-102CC-C4020-102CC-C4020-102CC-C4020-102 Manual Decrimper, 20 mm 1
CC-C4020-210 CC-C4020-2
H e a d S p a c e VH e a d S p a c e VH e a d S p a c e VH e a d S p a c e VH e a d S p a c e V i a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e si a l s & A c c e s o r i e s