technical memorandum phase ii wetland …surrounding area. stakes marking the position of sd33, sw12...

EPA Region 5 Records Ctr.

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TECHNICAL MEMORANDUMPHASE II WETLAND INVESTIGATION

AMERICAN CHEMICAL SERVICE, INC.NPLSITE

GRIFFITH, INDIANA

FEBRUARY 1997

PREPARED FOR:

ACS RD/RA EXECUTIVE COMMITTEE« • •

PREPARED BY:

MONTGOMERY WATSONADD1SON, ILLINOIS

PROJECT NO. 1252042.0809.0076

MONTGOMERY WATSON


AMERICAN CHEMICAL SERVICE, INC.NPL SITE

GRIFFITH, INDIANA

FEBRUARY 1997

John A. Hurtenbach Michael W. Kierski, Ph.D.Environmental Scientist Senior Environmental Scientist

Peter J. Vagtf Ph.D.Project Manager

TABLE OF CONTENTS

INTRODUCTION.

BACKGROUND. .1

PHASE II SEDIMENT SAMPLING AND ANALYSIS 2Wetland Grid Sampling Locations 3Transect Sampling Locations 3Sampling Locations South of Culvert Outfall 4Sampling Location Survey ; 4Sediment Sampling Procedure 4Phased Analytical Program 5Data Validation and Reduction ; 6Discussion of PCS Results 7Extent of PCB Impacted Sediments 8Determination of a Threshold Area of PCB Affected Sediments 9Discussions of Mercury Results 10

CONCLUSIONS 11

LIST OF TABLES

Table 1 November 1996 Wetlands Sample Location CoordinatesTable 2 Summary of Wetlands Sediment Phased Sample AnalysisTable 3 Summary of Phased Analytical ApproachTable 4 Summary of Wetland Sediment Sample Analytical Results

LIST OF FIGURES

Figure 1 Wetland Sediment Sample Locations and PCB ConcentrationsFigure 2 Wetland Sediment PCB Isoconcentration Map (0-0.5 ft interval)Figure 3 Wetland Sediment PCB Isoconcentration Map (0.5-1.0 ft interval)Figure 4 Wetland Sediment PCB Isoconcentration Map (1.0-1.5 ft interval)Figure 5 Wetland Sample Locations and Mercury Concentrations

LIST OF APPENDICES

Appendix A Analytical ResultsAl PCB Analytical ResultsA2 Mercury Analytical Results

J:\ 12S2\M2\08\WP\RPT\Sed2-TOC.DOC


AMERICAN CHEMICAL SERVICE, INC.NPL SITE

GRIFFITH, INDIANA

INTRODUCTION

This Technical Memorandum presents the results and conclusions from the Phase IIWetland Investigation conducted at the ACS NPL Site in Griffith, Indiana on November 18through 21, 1996. The Phase II investigation was conducted in accordance with the U.S.EPA approved Phase II Wetlands Sampling Pre-design Work Plan Addendum(Montgomery Watson November 6,1996). The investigation consisted of the collection ofsediment samples at three depths from 66 predetermined locations. Selected samples wereanalyzed for PCB and mercury.

The purpose of the Phase II Wetland Investigation was to further define the extent of PCBand mercury contamination in the wetlands at the ACS Site identified in the report WetlandInvestigation Technical Memorandum (Montgomery Watson July 25, 1996); referred to inthis Report as the Phase I Wetland Investigation. The Phase II Wetland Investigation wasperformed to better determine the extent of PCB and/or mercury contamination within thewetlands west of the ACS Site. This information was gathered in order to decide whethertoxicity testing and/or bioaccumulation studies should be performed. In order to determinewhether such studier "•« necessary, surface area estimates of PCB affected sediments v, :recompared to the size of the home range of the receptor the U.S. EPA selected as ofpotential concern in the wetlands (i.e., the mink). The premise for further defining theextent of PCB contamination was mat it was considered reasonable to assume that below agiven threshold area of PCB impacted sediments, no toxicity testing or biological studieswould be necessary.

BACKGROUND

The Phase I sampling results indicated that PCBs had migrated into the wetland area westof the ACS Site. PCBs were detected in 19 of the 22 sediment samples collected in thePhase I Investigation. Except for the three locations discussed below (SD21, SD33, andSD3S), the total PCB concentrations ranged from less than 1 mg/kg to approximately 6

Phase 2 Wetland Investigation February 1997 ACS NPL Site RD/RA Pre-DcsignPagel

o

mg/kg. See the July 25, 1996 Wetland Investigation Technical Memorandum for moredetail regarding the results of the Phase I sampling.

The Phase II investigation was proposed to better define the extent of PCB affectedsediments along a drainage channel extending through the wetland from the westernboundary of the ACS facility. The three sediment samples (SD21, SD33, and SD35) withPCB concentrations above the 10 mg/kg cleanup objective for soils specified in the Recordof Decision (ROD) for the Site were located along this drainage channel. The PCB resultsfor these three sediment samples are summarized below.

Sample ID Total PCBsSD21 13.1 mg/kgSD35 17 mg/kgSD33 125 mg/kg

The distance from SD21 to SD33 is approximately 500 feet Three other samples, SD31,SD34, and SD18 were collected along the same general channel, but showed lower PCBconcentrations.

Sample ID Total PCBsSD31 0.9 mg/kgSD34 0.027 mg/kgSD18 below detection limit

An aerial photograph from 1980 indicated that the channel within the wetland cut from nearthe ACS facility fence (Sediment Sample Location SD22) west into the wetland to itsintersection with a north-south drainage ditch in the wetland in the vicinity of surface watersampling location SW12. The channel was identified in the field during the Phase Isampling at several locations. While PCBs are not currently handled or stored on site, itappears that in the past, surface water runoff from the Site flowed along this channel. Thiswater may have transported PCBs or sediments containing PCBs.

The Phase II Investigation was conducted to better define the extent of PCB and mercurycontaminated sediments within and along the drainage channel. The following sectiondescribes the sampling strategy and methods used during the Phase II Investigation.

PHASE II SEDIMENT SAMPLING AND ANALYSIS

Phase II wetland sediment sampling was performed between November 18 and November21, 1996. Site conditions at the time included temperatures of 15 to 45 °F, with rain andsnow. Surface water in the wetlands ranged from approximately 0 - 2 0 inches deep.Wetlands vegetation (i.e., grasses and cattails) was dormant and remained upright. Grassesranged from approximately 0.5 - 3 feet in height, while cattails ranged from approximately

Phase 2 Wetland Investigation February 1997 ACS NPL Site RD/RA Pre-DesienPage 2

4 - 7 feet in height. As such, the identification of the topographic expression of thedrainage ditch could not be made visually. An all terrain vehicle (ATV) was used to knockdown cattails in a grid pattern. These paths were then walked, and the channel identifiedby surface water depth. In general, the channel averaged approximately 1 ft deeper than thesurrounding area. Stakes marking the position of SD33, SW12 and SW13 from the Phase Isampling were located, confirming the identification of the channel.

Field procedures used to locate sampling points in the wetland, transects, and south of theculvert are discussed in this Section. Sampling locations are shown on Figure 1.

Wetland Grid Sampling LocationsFollowing identification of the channel, the grid system was established. Based on Figure2 of the Work Plan, grid lines were labeled with letters A through E running south to north,and numbers 1 through 11 running west to east The grid intersects were then markedbeginning with the known location of Phase 1 sediment sample SD33, corresponding toposition C9 in the grid. Using a measuring tape, 50 ft intervals were marked out along thechannel (positions Cl through Cll). Once the central axis of the grid was establishedalong the channel, points were measured out perpendicular to the channel at 50 ft intervals.Note that sample points were located to the side of the paths made by the ATV, to avoidsoils potentially disturbed by the wheels of the ATV.

Because the channel curves northwest at grid position C8, sampling points south of thechannel diverged, creating a gap between positions A7 and A8. An additional sample wascollected between these points, identified as position A8-1.

Transect Sampling LocationsFour transects were proposed. Three of the transects (Tl, T2, and T3) were selected to beperpendicular to the flow of the channel. Transect (T4) is arrayed around Phase I sedimentsample location SD21, which was incorrectly shown on figures in the Phase I TechnicalMemorandum and the Phase II Work Plan as north of the channel. During field activities,the position of SD21 was re-surveyeu and confirmed to be located in the channel based onthe presence of the original marker.

Because of clearing activities conducted in preparation of installing the perimetergroundwater containment system (PGCS) extraction trench in the vicinity of the transectsT2 and T3, these locations were confirmed by the survey team prior to sampling. It shouldbe noted that surface vegetation had been removed from the vicinity of the transects T2 andT3 and the surface soils in this area had been disturbed. Samples were then collected at 25foot intervals along each transect, identified from south to north as A through E.

Phase 2 Wetland Investigation February 1997 ACS NPL Site RD/RA Pre-DesignPage 3

Sampling Locations South of Culvert OutfallThree sampling locations were selected south of the culvert outfall at the far southwest sideof the sampling area. The sample location are as follows:

• "Culvert Outfall", was chosen in the vicinity of the culvert, to characterizesediment downstream from the outfall.

• "Culvert Downstream" was located 50 ft down-gradient (i.e., south) of the outfall,to characterize sediment transported from the vicinity of the outfall.

• "Culvert Upstream 1" was located 50 ft up-gradient (i.e., east) of the outfall, tocharacterize the contribution of the Griffith Landfill dewatering activities tosediment composition.

At the request of the U.S. EPA's representative, a fourth location was added 50 ft furtherup-gradient (i.e., east) of the outfall, identified as "Culvert Upstream T. The purpose ofadding mis fourth sampling point was to respond to the concern of the U.S. EPA oversightpersonnel mat "Culvert Upstream 1" might not have been located sufficiently up-gradientof the outfall pool, and thus would not clearly identify landfill contributions to the sedimentcomposition.

Sampling Location SurveyAfter sampling points were identified, the positions were surveyed within 0.1 foot of thehorizontal reference grid set up for the Site. A summary of the survey coordinates ispresented in Table 1.

Sediment Sampling ProcedureThe sediment samples were collected according to Montgomery Watson's sedimentsampling Standard Operation Procedure (SOP), which was approved by the U.S. EPA for

\ the Phase I sediment sampling in May 1996. The sampling device presented in the SOP (a^^ sample coring device with an opening running the length of the tube) proved ineffective in

the standing surface water of the wetland. The organic and sand sediments washed out ofthe open side of the sampling device when brought up through the standing surface water.This problem was resolved by using a standard 2 inch ID split-spoon sampler equippedwith a catcher to prevent loss of the sample. The split spoon was mounted on a 5 ft sectionof drill rod and driven into the sediments using a slam bar. This technique successfullyallowed a 2 ft core of sample to be removed in a single operation. The transect samples,located in areas without standing water, were collected without difficulty using the openside coring device.

At each intersection of the grid, each point on the transects, and at the locations south of theculvert, samples were collected from three depth intervals (0-6 inch, 6-12 inch, and 12 -18 inch). In the wetland grid sample locations, the surface (located up to 2 feet below thesurface water) was covered by successive layers of vegetation, representing each year'sgrowth of cattails. This layer varied in thickness from approximately 2 inches to 10 inches,


• and proved to be highly compressible, making accurate measurement difficult. Beneath theorganic layer was a layer of dark brown-gray to black, fine to medium sand approximately

~ 4 to 8 inches thick, underlain by a light brown fine to medium sand. These three layers(organic matter, dark colored sand, and light colored sand) were observed throughout the

_ wetland area. A sampling interval based strictly on depth would not account for theunpredictable thickness of the organic layer, resulting in samples containing parts of eachof these distinct layers. With concurrence of the U.S. EPA representative, it was decided

_, that the 0 - 6 inch sample (identified for convenience as 0.5 ft) would include the organiclayer, the 6 - 12 inch layer (identified for convenience as 1.0 ft) would include the dark

""" sand layer, and the 12 -18 inch layer (identified for convenience as 1.5 ft) would include~ the light colored sand. Samples from the transects composed of dark black silty sands,

were collected based strictly on depth from the ground surface. Culvert samples werecomposed primarily of gray-brown sands, without an organic layer, and were sampled

TS based strictly on depth interval.

/^*N Samples were placed in wide-mouth glass containers with Teflon lined lids, labeled,~'—/' tagged, and shipped on ice and under custody to IEA Laboratories for analysis.

Phased Analytical Program" A total of 231 sediment samples were collected, which included duplicate sediment- samples. The phased analytical program was designed to selectively analyze as many of

these samples as necessary to complete the identification of sediment areas with PCBi concentrations greater than 1 mg/kg. Table 2 presents a summary of all samples collected

- and the total PCB results for samples selected for analysis during each round.

The selection of the twenty-eight (28) Round 1 samples shown in Table 2 was determined~" in concurrence with the U.S. EPA prior to sampling activities. Round 1 samples were—( generally from the 0.5 ft layer, with the exception of samples at locations previously_ sampled in Phase I (i.e., SDC9, SDT3 (C), and SDT4 (C)), where the 1.0 ft interval was

**) selected. Each of the Round 1 samples was analyzed for PCBs, and at the request of theU.S. EPA, for mercury.

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PCB results for each sample, reported by the laboratory in ug/kg, were totaled andconverted to units of mg/kg or ppm (i.e., ug/kg x 1,000). If the total PCB concentration

w was greater man 1 mg/kg, the sample location in each direction and the interval directlybeneath that sample were selected for analysis. Table 3 lists the samples by round, and thelogic for the phased analytical approach.

It should be noted that, due to a laboratory oversight, samples from SDD5, intervals 0-0.5feet and 0.5-1 feet were extracted but not analyzed, although they should have been

~* because of SDC5. However, results from SDC4, SDD3, and SDD6, which are near SDD5,indicated no PCBs above 1 mg/kg.

Phase 2 Wetland Investigation. February 1997 ACS NPL Site RD/RA Pre-DesienPageS

Based on the Round 1 results, it was determined that an additional 119 sediment samplesmight need to be analyzed for PCBs of the total 231 samples collected. The Pesticide/PCBanalytical method technical hold time requires extraction within 14 days after sampling,and analysis of the extract within 40 days of completing the extraction procedure. In orderto meet extraction holding times while waiting for analytical results, it was decided toextract each of the additional sediment samples that could potentially require analysis basedon the Round 1 results. The extracts could then be held for 40 days prior to analysis.

As a result of the selection process, 37 of the 119 samples extracted were analyzed duringRound 2. Based on the Round 2 results, 14 additional samples were analyzed in Round 3.During Round 4, an additional 4 sediment samples were analyzed for PCBs. Including thefirst round, a total of eighty-three (83) sediment samples were analyzed for PCBs. Adiscussion of the analytical results from all four rounds is presented hi the followingsection.

Data Validation and ReductionPreliminary data results were faxed by IEA to Montgomery Watson and tabulated. Thesepreliminary results were used to identify samples for subsequent analytical rounds. (Copiesof the preliminary data for each of rounds 1,2, and 3 were faxed to the U.S. EPA as soon asthey were available from the laboratory). Final data packages were subsequently forwardedto Montgomery Watson for data validation and reduction.

The PCB laboratory analysis was performed according to the methodologies presented inthe CLP SOW. Data validation was performed in accordance with the National FunctionalGuidelines for Organic Data Review (February 1994). Based on the data validationprocedure, the results are acceptable for use in site evaluation with the followingcomments:

Holdtimes were met, with the exception of sample SDT4(A) 0.5 ft, which exceededthe extraction holdtime; and samples SDC5-1.5 ft, SDC7-1.5 ft, SDC11-1.5 ft andSDD11-1.0 ft, which exceeded analysis holdtimes. Results for these samples havebeen qualified as estimated (J or UJ). It should be noted that the technicalholdtimes are based on pesticides as well as PCBs, which are significantly morestable and resistant to degradation than the pesticide compounds. Although theresults for samples exceeding holdtimes have been qualified as estimated, it isunlikely significant degradation of the PCBs would have occurred.

Laboratory blanks were generally clean, without detects of PCBs at concentrationsgreater than the CRQL. Only one sample was affected by positive blank results,and in that sample the reported concentration exceeded the blank results by twomagnitudes, and did not require qualification.

Over all, the sample chromatography was acceptable, given the matrix interferencespresent in the samples. Matrix interferences resulted in many surrogate percentrecoveries being outside the QC limits. In addition, interferences may have masked

Phase 2 Wetland Investigation February 1997 ACS NPL Site RD/RA Pre-DcsignPage 6

primary identification peaks, resulting in a percent difference criteria between thetwo GC column quantitations exceeding 25% (laboratory qualifier P). As requiredby the method, the lower concentration (presumably not masked by interferences)was reported. In all cases reported detection limits were either less than 1 mg/kg, orthe sample concentration exceeded 1 mg/kg.

Mercury analysis was performed on all Round 1 samples by IEA Laboratories, andvalidated according to the National Functional Guidelines for Inorganic DataReview (February 1994). All mercury results are acceptable for use in siteevaluation. Some samples have been qualified as estimated (J or UJ) due to aslightly elevated spike recovery (130%, with QC limits of 75 -125%).

Results of all sample analyses are presented in Table 4. This table presents reporteddetection limits, concentrations, laboratory qualifiers and data validation qualifiers forsamples analyzed in the Phase II Investigation.

Discussion of PCB ResultsIn general, sediment samples with PCB concentrations exceeding 1 mg/kg in the wetlandgrid were limited to the immediate vicinity of the drainage channel:

SanmtelD Depth PCB»»g/kgAPD-SDC9 0.5 SD33-126 (Phase I sampling location)APD-SDC8 0.5 73APD-SDC7Dup 0.5 40APD-SDC7 1.0 30.3APO-SDB9 0.5 14.1APD-SDC5 1.0 3.6APD-SDC11 0.5 2.52APD-SDD11 0.5 2.16APD-SDC6 0.5 1.89APD-SDB5 0.5 1.51APD-SDCH 1.0 1.45APD-SDC5 0.5 1.42APD-SDC7 0.5 1.23APD-SDB10 0.5 1.2

Refer to Figure 2 for a graphical presentation of the total PCB results and Table 4 for atabular presentation. Results for Phase 1 samples matching grid locations are included forreference. Wetland grid samples with total PCB concentrations exceeding 1 mg/kg wereprimarily limited to the 0.5 ft interval. Recall that this interval was composed primarily oforganic material. At locations Cl 1, C7 and C5, near the upgradient end of the channel,total PCB concentrations exceeding 1 mg/kg were detected in the 1.0 ft interval. Recallthat this interval was composed of the dark colored, fine to medium sand. No samplesanalyzed from the 1.5 ft interval ( light brown, fine to medium sand) contained total PCBsat concentrations exceeding 1 mg/kg.


The following transect samples contained total PCBs at concentrations greater than1 mg/kg:

DklD

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APD-SD Tl(B)APD-SD T1(C)APD-SD T1(D)APD-SD T2 (B)APD-SD T2(C)APD-SD T2(C)APD-SD T2(C)APD-SD T2(D)APD-SD T2(D)APD-SD T3 (A)APD-SD T3(B)APD-SD T3(B)APD-SD f3(B)APD-SD T3(C)APD-SD T3(D)APD-SD T3(E)APD-SD T4(C)APD-SD T4(C)APD-SD T4(C)

0.50.50.50.50.51.01.50.51.00.50.51.01.50.50.50.50.51.01.5

sfa

14.45.21

7.233594.763.0229.19.4

11.6234274.0

SD35-1715.71.04

SD21-1360

24.5

(Phase I sampling location)

(Phase I sampling location)

Note that in transect Tl, PCBs appear to be limited to 0.5 ft interval, and in transect T4PCBs are limited to the center sample point (SDT4 (C)) in samples to depth. Tl is locatedin a grassy area and was not disturbed. T4 is located farthest upgradient in a confinedstream bed. By contrast, transects T2 and T3, located in areas of disturbed vegetation,exhibit more widely distributed PCB concentrations.

Culvert samples from the 0.5 ft interval were analyzed for PCBs. Only the culvert outfall0.5 ft sample had total PCBs greater than 1 mg/kg (2.08 mg/kg). PCBs were not detectedin the sample location 50 feet downstream from the culvert. PCBs were not detected in thefourth Culvert location requested by the U.S. EPA oversight personnel.

Extent of Detected PCBs in SedimentsThe Phase I and Phase II sampling results were combined to develop a series ofisoconcentration maps delineating the horizontal and vertical extent of PCB concentrationsin sediments above specific limits. A map was developed for each of three sample depths:0 to 6 in, 6 to 12 in, and 12 to 18 in (refer to Figures 2, 3, and 4). Two isoconcentrationlines have been plotted on each map, a 1 mg/kg contour line and a 10 mg/kg contour line.The surface area associated with each contour was estimated by digitizing the area withineach contour. The following is a summary of the surface area estimates.

i IntervalPCB Limit1 mg/kg

10 mg/kg

Phase 2 Wetland Investigation

0-0.5 0.5 - 1.01.3 acres 0.3 acres0.5 acres 0.06 acres

February 1997

1.0-1.50.08 acres0.01 acres

ACS NPL Site REVRA Prc-DesignPageS

Figures 2, 3 and 4, along with the area estimates show that the PCBs are concentrated in anarrow zone along the drainage pathway west of the ACS facility. Within the surficialwetlands sediments, approximately 1.3 acres contains PCB concentrations above 1 ppm.Of that area, approximately 0.5 acre contains sediment with PCB concentrations above 10ppm. The highest PCB concentrations are located within the channel. The PCB affectedsediments primarily occur in the surficial sediment layer (0 to 6 in), with limited detectionsat the 12 to 18 in interval.

The surface area estimates from each depth interval were used to estimate the volume ofPCB affected sediments. The total volume of sediments with PCB concentrations above1 ppm is approximately 1,320 cubic yards. Of that volume, approximately 460 cubic yardscontains PCB concentrations above 10 ppm.

Determination of a Threshold Area of PCB Affected SedimentsOne objective of the Phase I and II wetlands investigation was to determine whether theextent of PCB impacted sediments was large enough to warrant performing ,toxicity/bioaccumulation studies. Based on this objective it was necessary to estimate whatwould be a biologically significant area of PCB affected sediments. The followingdiscusses the rationale for developing an estimate of this area.

The U.S. EPA considered the mink to be the receptor of concern within the ecological riskassessment for the Site, based on the potential for bioaccumulation to occur through itsfood chain within the wetland. Mink are carnivores which feed primarily on small animals,such as muskrats, waterfowl, voles and mice. Therefore, the primary concern is for theseprey species to become contaminated with PCBs, which could be passed on to the mink.The objective was to evaluate what percentage of the home range of a mink is affected byPCBs in the wetland in the vicinity of the ACS Site. The home range is considered the sizeof the area that a mink would need to roam and be able to acquire enough food to survive.It is worth noting that, to the best of our knowledge, mink have not been observed at ornear the Site.

Estimates for the home range size of the mink are provided in the Wildlife ExposureFactors Handbook (EPA 1993). Estimates of mink home ranges vary depending upon theparticular habitat where the mink reside. Within riverine environments the home range aremuch smaller than for wetland environments, because of the relative difference inabundance of food. For this reason, it was considered most accurate to select an estimate ofthe home range for mink at the Site that best corresponds to the wetland environment. Thesmallest home range estimate for the mink (i.e., 640 acres), for an environment similar tothe wetlands environment, was used as a conservative estimate of the home range for themink. This value corresponds to the lowest estimate of the mink home range in the PrairiePothole habitat of North Dakota developed by Eagle and cited in Allen (1986).

To estimate a biologically significant area of PCB affected sediment, a small fraction of theminks home range was selected. It was considered for purposes of this assessment that if1 percent or less of the mink's home range was contaminated above a selected PCB


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cleanup objective, that this could be considered an insignificant fraction of its home range.This is because the amount of prey potentially consumed from this area would be too smallto affect the health of the mink population. In other words, if the size of the PCB affectedarea was less than one percent of the mink home range, toxicity or bioaccumulation studieswould not need to be performed because significant health risks to the mink populationwould not be present One percent of the minks home range equates to 6.4 acres, orapproximately 280,000 ft2.

On the basis of the Phase I and II sediment sampling, 0.2 percent of the home range for amink is affected by PCBs at a level of 1 ppm or above. In addition, 0.08 percent of thehome range for a mink is affected by PCBs at a level of 10 ppm or above. Considering thatthese percentages are well below the threshold limit of 1 percent, there does not appear tobe a strong need to conduct toxicity testing, and/or bioaccumulation studies for the ACSSite.

Discussion of Mercury ResultsDuring the Phase II investigation each of the 28 Round 1 surficial sediment samples wereanalyzed for mercury as requested by the EPA (refer to Table 4). The following Round 1samples contained detects of mercury at concentrations greater man the reported instrumentdetection limit (IDL) of approximately 0.1 mg/kg:

Sample ID Depth Mercury me/kgAPD-SDB5 0.5 0.28APD-SDB9 0.5 0.28APD-SDC8 0.5 0.60APD-SDT1(B) 0.5 0.44APD-SDTKC) 0.5 1.4APD-SDT1(D) 0.5 2.6APD-SDT2(C) 03 6.1APD-SDT2(D) 0.5 1.6APD-SDT3(B) 0.5 1.2APD-SDT3(D) 0.5 2.5APD-SDT4(C) 0.5 0.28

Based on the mercury results, the extent of mercury affected sediments appears to be morelimited than the PCB affected sediments. Figure 5 provides an area! view of thedistribution of mercury sediment sample results. The distribution of the mercury resultsappeared to coincide with the PCB results, as mercury was detected only at locations wherePCBs were detected. The highest mercury concentrations coincided with the highest PCBconcentrations, which were located near the eastern end of the wetlands, close to the ACSfacility. In addition, with the exception of two sample locations, mercury was detectedsolely within the area where PCB concentrations were 10 mg/kg or more.


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CONCLUSIONS

The objective of the wetland investigation as stated in the Predesign Work Plan was todetermine if elevated PCB sediment concentrations are widespread within the wetlands inorder to decide whether toxicity testing and/or bioaccumulation studies should beperformed. The Phase I sampling event, reported in the Wetland Investigation TechnicalMemorandum (Montgomery Watson July 25, 1996) indicated that there were sediments onSite containing PCB concentrations above 10 ppm, in the wetland west of the ACS Site.However the spacing of the sampling results was not sufficiently close to accuratelydetermine the area or volume of affected sediments. A second phase of wetland samplingwas conducted in November 19% to provide a detailed delineation of the extent andconcentration of PCB impacts, so that this determination could be made.

The Phase I and Phase II sampling results have been combined in several maps to provide aseries of isoconcentration maps delineating the horizontal and vertical extent of PCBconcentrations in sediments. These maps show that the PCBs are concentrated along anarrow zone, parallel to the drainage pathway west of the ACS facility. Three maps havebeen developed, one for each of the three sample depths: 0 to 6 inches, 6 to 12 inches, and12 to 18 inches (refer to Figures 2, 3, and 4). Two isoconcentration lines have been plottedon each map, a 1 ppm contour line and a 10 ppm contour line.

•t

Approximately 1.3 acres are estimated to contain PCB concentrations above 1 ppm. Of.i that area, approximately 0.5 acres are estimated to contain sediment with PCB

concentrations above 10 ppm. The total volume of sediments with PCB concentrationsabove 1 ppm is approximately 1,320 cubic yards. Of that volume, approximately 460 cubicyards of sediment is estimated to contain PCB concentrations above 10 ppm. Based uponthese results, the surficial extent of PCB affected wetlands sediment does not appear to belarge enough to warrant toxicity or bioaccumulation studies. A discussion of the rationalefor this conclusion follows.

" The U.S. EPA considered the mink the receptor of concern within the ecological risk

; assessment for the Site, based on the potential for bioaccumulation to occur through itsfood chain within the wetland. Mink are carnivores which feed primarily on small animals,such as muskrats, waterfowl, voles and mice. Therefore, the primary concern is for theseprey species to become contaminated with PCBs, which could be passed on to the mink.The objective was to evaluate what percentage of the home range of a mink is affected byPCBs in the wetland in the vicinity of the ACS Site. The home range is considered the size

* of the area that a mink would need to roam to be able acquire enough food to survive.

Estimates for the home range size of the mink are provided in the Wildlife ExposureFactors Handbook (EPA 1993). The smallest home range estimate for the mink (i.e., 640acres), for an environment similar to the wetlands environment, was used as a conservativeestimate of the home range for the mink. It was considered for purposes of this assessmentthat if 1 percent or less of the mink's home range was contaminated above a selected PCBcleanup objective, that this could be considered an insignificant fraction of its home range,

Phase 2 Wetland Investigation February 1997 ACS NPL Site RD/RA Pre-DesienPage 11

which would not require toxicity or bioaccumulation studies to be performed. One percentof the minks home range equates to 6.4 acres, or approximately 280,000 ft2. On the basisof the Phase I and II sediment sampling, less than one percent of the typical home range fora mink is affected by PCBs at a level of 1 ppm or above. Therefore, there is no need toconduct toxicity testing, and/or bioaccumulation studies for the ACS Site.

JAH/djh/MWK/WVC:\COPY\WL-SED2-DOC

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Phase 2 Wetland Investigation February 1997Page 12

ACS NPL Site RP/RA Pre-Desigr

tAB

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Table 1November 1996 Wetlands Sample Location Coordinates

American Chemical Services Inc.

NPL Site

Griffith, Indiana

SamplingPointAlA2 jA3A4A5 iA6A7A8-1A8 jA9A10BlB2B3B4B5B6B7B8B9BIOBllClC2C3C4C5C6C7C8C9CIOCll

East412841744226427543204364441044554497454645844152419942484296433743894431449545444588464441774219426843154362440744524488454345954647

North730072797254723872197192716971577144712871137344732672997283726472367214718271787162

; 7165i 7386! 7363

734473277306728172607229722572117214

SamplingPointDl jD2 iD3D4D5D6D7 ;

D8D9D10DllE6E7E8 ;

T1(A)T1(B)Tl (C)T1(D) ;T1(E)T2(A)T2(B)T2(C)T2(D)T2(E) ,T3 (A)T3(B)T3(C)T3 (D)T3(E) ;T4(A)T4 (B)T4(C)T4(D)T4(E)

East4200423342804333437944234469450745604607465044444491452546964701470947134719484448404835483148254887489449004906491349945013502750405060

North: 7432j 7409i 7392' 7377

7354: 7327

73097275

i 7273i 7269

7265737373527322718872117237

; 7262728771347164

' 71901 7215| 7238i 7136! 7161

71867212

i 723671267145716271777192

SO-FINAL XLS/Coofdinatcs 2/13/97

Table 2Summary of Wetland Sediment Phased Sample Analysis

American Chemical Service, Inc. NPL SiteGriffith Indiana

SampleSample ID Deptk ! DateAPD-SD A 1 0.5 11/21/96APD-SD A 1 1.0

APD-SDA1 1.5 ;APD-SDA2 0.5 11/21/96APD-SDA2 1.0 'APD-SDA2 1.5APD-SDA3 0.5 11/21/96APD-SDA3 1.0APD-SDA3 1.5APD-SDA4 0.5 11/21/96APD-SDA4 1.0APD-SDA4 1.5APD-SDA5 0.5 11/21/96APD-SDA5 1.0

APD-SDA5 ' 1.5APD-SDA6 0.5 11/21/96APD-SDA6 1.0APD-SDA6 1.5APD-SDA7 0.5 11/21/96APD-SDA7 1.0APD-SDA7 1.5APD-SDA8 0.5 , 11/21/96APD-SDA8 1.0APD-SDA8 1.5APD-SDA8Dup 0.5 11/21/96APD-SDA8 Dup 1.0APD-SDA8Dup 1.5

APD-SDAS(l) 0.5 11/21/96APD-SDA8(1) 1.0 ;APD-SDA8(1) ' 1.5 iAPD-SDA9 0.5 • 11/21/96APD-SDA9 1.0 'APD-SDA9 1.5APD-SDA10 0.5 11/21/96APDrSDAlO 1.0 iAPD-SDA10 1.5APD-SDB1 0.5 11/20/96APD-SDB1 1.0 .APD-SDB1 1.5APD-SDBI Dup 0.5 11/21/96APD-SDB1 Dup 1.0APD-SDBI Dup 1.5

Total PCBs (mg/kj

Round 1

0.056

Round 2E

E ;EE 0.223E ;

EE ;E ;E !EEE 'E j 0.75E ! .E 0.007E ;EE 'EE :

EEE iEEE 'EE

E !E 'E 0.367

E 'EEEE ;

E ND

Round 3

ND

J

Round 4All

RoundsEEE

0.223EEEEE

I ^E

0.75E

0.007EEEEEEEEEEEEEEE

0.367EE

NDEE

0.056

ND

O

SD-FINAL XLS(Rounds) Page 1 of6 2/13/97

Table!Summary of Wetland Sediment PhasedSSrtfipks Analysis


SampleSample ID Depth DateAPD-SDB2 0.5 11/21/96APD-SDB2 1.0APD-SDB2 1.5APD-SDB3 0.5 1 1/21/96APD-SDB3 1.0APD-SDB3 1.5APD-SDB4 0.5 11/21/96APD-SDB4 1.0APD-SDB4 1.5APD-SDB5 0.5 11/20/96APD-SDB5 1.0APD-SDB5 1.5APD-SDB6 0.5 1 1/21/96APD-SDB6 1.0APD-SDB6 , 1. 5APD-SDB7 0.5 11/21/96APD-SDB7 1.0APD-SDB7 1.5APD-SDB8 0.5 11/21/96APD-SDB8 1.0APD-SDB8 1.5APO-SDB9 0.5 11/2096APD-SDB9 1.0APD-SDB9 1.5APD-SDB10 0.5 11/21/96APD-SDB10 1.0APD-SDB10 1.5APD-SDB11 0.5 11/21/96APD-SDBI 1 1.0 '•APD-SDBI 1 1.5APD-SDC1 0.5 ; 1 1/21/96APD-SDC1 1.0 iAPD-SDC1 1.5APD-SDC2 0.5 ii/2<V96APD-SDC2 1.0APD-SDC2 1.5APD-SDC3 0.5 11/21/96APD-SDC3 1.0APD-SDC3 1.5APD-SDC4 0.5 U/2ft-96APD-SDC4 1.0APD-SDC4 1.5

Total PCBs (mt/k|

Round 1

1.51

14.1

0.21

0.432

Round 2E ;EEE iEEE 0.106EE

E NDEE 0.72EEEEEE , 0.412EE

E 0.068EE UEEE ,E iE !

,

Round 3

0.9

0.18

0754

i

Round 4All

RoundsEEEEEE

0.106EE

1.51NDE

0.72EE

0.9EE

0.412EE

14.10.068

E13.

0.18E

0254EE

0.211

0.432

o

StXFINAL XLSdlounds) Page 2 of6 2/13

Table!Summary of Wetland Sediment Phased Sample Analysis


SampleSample ID Depth DateAPD-SDC5 0.5 11/21/96APD-SDC5 1.0APD-SDC5 1.5APD-SDC6 0.5 ; n/20/96APD-SDC6 1.0APD-SDC6 1.5APD-SDC7 0.5 H/21/96APD-SDC7 1.0APD-SDC7 1.5APD-SDC7Dup 0.5 11/21/96APD-SDC7Dup 1.0APD-SDC7Dup 1.5APD-SDC8 0.5 11/20/96APD-SDC8 1.0APD-SDC8 1.5APD-SDC9 0.5 11/20/96APD-SDC9 1.0APD-SDC9 1.5 'APD-SDC10 0.5 11/20/96APD-SDCIO 1.0APD-SDC10 1.5APD-SDC11 0.5 11/21/96APD-SDC11 1.0 'APD-SDC11 1.5APD-SDD1 0.5 11/20/96APD-SDDI 1.0APD-SDD1 1.5APD-SDDI Dup 0.5 11/20/96APD-SDDI Dup 1.0APD-SDDI Dup 1.5APD-SDD2 0.5 ; 11/20/96APD-SDD2 ' 1.0 iAPD-SDD2 1.5 'APD-SDD3 0.5 11/20/96APD-SDD3 1.0 !APD-SDD3 1.5APD-SDD4 0.5 11/20/96APD-SDD4 1.0APD-SDD4 1.5APD-SDD5 0.5 il/2(V96APD-SDD5 1.0APD-SDD5 1.5

Total PCBs (mg/kf

Round 1

1.89

73

SD33-1260.093

0.7

0.319

Round 2E 1.42E ,E

E NDEE 1.23EE iE , 40EE

E 0.12E

i

E ' 0.144EE ; 2.52EE

:it

EEE

Round 3

3.6

30.3

1.45

5)

Round 4

ND

ND

0.056

AllRauds

1.423.6ND1.89NDE

1.23303ND

? ^E73

0.12E

SD33-1260.093

0.70.144

E1521.4S0.056

x^>

0.319

EEE

SD-FINAL XLS(Rounds) Page 3 of6 2/13/97

Table 2Summary of Wetland Sediment Phased Simple Analysis


SampleSample ID Depth DateAPD-SDD6 0.5 1 1/20/96APD-SDD6 1.0APD-SDD6 1.5APD-SDD7 0.5 1 1/20/96APD-SDD7 1.0 :

APD-SDD7 1.5APD-SDD8 0.5 , ll/2(V96APD-SDD8 1.0APD-SDD8 1.5APD-SDD9 0.5 H/20/96APD-SDD9 1.0APD-SDD9 1.5APD-SDD10 05 11/21/96APD-SDD10 1.0APD-SDD10 1.5APD-SDDI 1 0.5 11/21/96APD-SDDI 1 1.0APD-SDDI 1 1JAPD-SDE6 , 0.5 11/21/96APD-SDE6 1.0APD-SDE6 1.5APD-SDE6Dup 0.5 it/21/96APD-SDE6Dup 1.0APD-SDE6Dup 1.5APD-SDE7 0.5 1 1/21/96APD-SDE7 1.0APD-SDE7 1.5APD-SDE8 0.5 1 1/21/96APD-SDE8 1.0APD-SDE8 1.5APD-SD Tl (A) •• 0.5 i 11/21/96APD-SD Tl (A) , 1.0 'APD-SD Tl (A) 1.5APD-SD Tl(B) 0.5 , 1 1/20/96APD-SD T1(B) 1.0APD-SD T1(B) 1.5APD-SD T1(C) 0.5 11/20/96APD-SD T1(C) 1.0APD-SD T1{C) 1.5APD-SD T1(D) 0.5 1 1/20/96APD-SD T1(D) 1.0APD-SD T1(D) 1.5

Total PCBs (mf/kg)

Round 1

0.65

0.021

10.2

14.4

5.21

Round 2E NDEE '

t

E 0.044EE

E 0.13E ;EEE 'E 'E ;EEEEE

EE 'EE i 0.81E IE i

E ! 0.063E

E 0.461E

E 0.198E

Round 3

2.16

Round 4

•

0.054

AllRoaads

NDEE

0.648

0.044EE

0.021

0.13EE

2.160.054

EEEEEEE

EEE

0.81EE

100.063

E14.4

0.461E

5.210.198

E

"•*

J

SO-FINAL XLS<Roundj) Page 4 of6 2/13

Table 2Summary of Wetland Sediment Phased Sample Analysis


SampleSample ID Depth DateAPD-SD T1(E) 0.5 11/21/96APD-SD T1(E) 1.0APD-SD T1(E) 1.5APD-SD T2 (A) 0.5 n/20/96APD-SD T2 (A) 1.0APD-SD T2( A) 1JAPD-SD T2(B) 0.5 • 11/21/96APD-SD T2(B) 1.0APD-SD T2(B) 1.5APD-SD T2(C) 0.5 1 1/20/96APD-SD T2(C) 1.0APD-SD T2(C) 1.5APD-SD T2(D) 0.5 1 1/20/96APD-SD T2(D) 1.0APD-SD T2(D) 1.5APD-SD T2 (D) Dup 0.5 1 1/21/96APD-SD T2(D) Dup 1.0APD-SD T2(D) Dup 1.5APD-SD T2(E) 0.5 n/20/96APD-SD T2(E) 1.0APD-SD T2(E) 1.5APD-SD T3 (A) 0.5 11/20/96APD-SD T3 (A) 1.0APD-SD T3( A)* 1.5APD-SD T3(B) 0.5 11/20/96APD-SD T3(B) 1.0APD-SD T3(B) 1.5APD-SD T3(C) 0.5 11/20/96APD-SD T3(C) 1.0APD-SD T3(C) 1.5APD-SD T3(D) 0.5 n/20/96APD-SD T3(D) 1.0 'APD-SD T3(D) 1.5APD-SD T3(E) 0.5 11/21/96APD-SD T3(E) 1.0APD-SD T3(E) 1.5APD-SD T4 (A) 0.5 11/21/96APD-SD T4( A) 1.0APD-SD T4( A) 1.5APD-SD T4(B) 0.5 ! 1/20/96APD-SD T4(B) 1.0APD-SD T4(B) 1.5

Total PCBs (mg/kf

Round 1

7.23

359

29

234

SD35-170.22

15.7

-

0.15

Round 2E 0.237EEE 0.26EE

E : 0.48E

E ; 4.76E

E 9.4EE NDE NDE iE ; NDEEE : 11.60EE 0.132

E 27E

E 0.15E iE 1.04E ''E

Round 3

0.0222

3.02

0.96

0.08

4

ND

,)

Round 4All

Rounds0.237

EE

0.260.0222

E7.230.48

E

3.0229.19.40.96NDNDE

NDEE

11.60.080.132234274.0

SD35=170.223

15.70.15

E1.04

EE

ND

0.154

SD-FINAL XLS(RoundJ) Page 5 of6 2/13/97

Table 2Summary of Wetland Sediment Phased Silnple Analysis


"*%

*•»

•J*

1

-O~***

-•*»

^

SampleSample ID Depth DateAPD-SD T4(C) 0.5 It/2096APD-SD T4(C) 1.0APD-SD T4(Q 1.5APD-SD T4(D) 0.5 1 1/20/96APD-SD T4(D) 1.0APD-SD T4(D) 15APD-SD T4(E) i 05 it/21/96APD-SD T4(E) 1.0 ;APD-SD T4(E) 1.5APD-Culvert Outfall 05 lt/20/96APD-Culvert Outfall 1.0APD-Culvert Outfall 1.5ArL>-v.uiven Lwwnsircain u. 3 i i/jono

APD-Culvert Downstream 1.5APD-Culvert Upstream (1) 05 u/20/96APD-Culvert Upstream (I) 1.0APD-Culvert Upstream (1) 15APD-Culvert Upstream (2) 0.5 n/20/96APD-Culvert Upstream (2) 1 .0APD-Culvert Upstream (2) 1 5

Total PCBi (rag/In

Round 1SD21-13

60

0.74

2.08

0.29

0.099

036

Round 2

iE [ 245

i

!

i

E 0.028E •

i

'<

:

Round 3

5)

Round 4All

RoundsSD21-13

6024.50.742

2.080.028

E0.288

0.099

0.36

Onotes collected on November 20 and 21,1996fiom the ACS Site in Griffith Indiana. A subset of

Notes:This table is a sumnwry of all wetland sedimeall samples collected was selected for Round 1 analysis. On the basis of the Round 1 results, a second, third and fourth round of analyses wereperformed to define the extent of PCB affected sediments. This table presents the results of this decision making process.

Round 1- samples from 0.5' (or IJT ibr C9&T4(C))wu selected by the U.S. EPA and IDEM. Eariier sediment samples collected at grid pointsare also included for reference.Round 2 "Analyze all samples on each side and beneath any Round I sample > I ppm PCBs. Extract samples farther out to meet reasonable worstcase scenario.Round 3 - Analyze samples identified in Round 2 using same criteria as Round 2.Round 4 - Analyze samples identified in Round 3 using die same criteria as Round 2.

Total PCBs » sum of PCB results (generally Arochlors 1248,1254, and 1260), converted to mg/kg.E *> Extraction requested (samples have a holdtime of 14 days from collection to extraction, and extracts have a hokhime of 40 days after theextraction date).

Footnotes;a) Sample analyzed by 1EA in error.

SO-FINAL XLS(Rounds) Page 6 of6 2/13/97

Table 3

Summary Phased Analytical ApproachAmerican Chemical Service, Inc. NPL Site

Griffith Indiana

Round 1Sample mg/kg

SDB 1-0.5' ( 0.056i

SDB5-0.5' ; 1.51

iti

SDB9-0.51 14.1

i

!SDC2-O.S1 I 0.21

SDC4-OJ* 0.432i

SDC6-O.S* j 1.89

I

ii

SDC8-0.51 . 73

SDC9-1.01 0.093

SDC10-0.5' 0.7

SDD3-0.51 0.319

SDD7-0.51 0.65

SDD9-0.51 0.021

SDT1(B)-0.5' 10.2SDT1(C)-0.5' 14.4SDT1(D)-0.5' ' 5.21

SDT2(B)-0.5r 7.23SD T2 (C)-O.S' 359SD T2 (D)-0.5' 29

Round 2Sample mg/kg

NFA :

SDBS-1.0*SDB4-051

SDC5-0.31

SDB6-0.5'SDA5-0.51

SDB9-I.O*SDB8-05*SDBlO-0.51

SDA9-0.5'

ND0.111.42

0.720.75

0.0680.4113.

0367

NFA

NFA

SDC6-1.01

SDD6-0.5'SDC7-0.5'

SDC8-1.01

SDD8-0.5'

NDND1.23

, 0.120.044

!

NFA :

SDC10-1.0*SDD10-0.51

SDC11-0.51

• 0.14! 0.13

2.52

NFA

NFA

NFA

SOTHAJ-O-S1

SDT1(BHO*SDTHO-l-O*SDTlfD^l.O*SDT1(EH).5'

SDT2(AHI.5'SDT2(B)-1.0'SDT2(C)-1.0t

SDTaCD^I.O1

SD T2 (EyOS

; 0.81i 0.063! 0.46j 0.2| 0.241

; 0.260.484.76

: 9.4ND

Roaad3Sample : mg/kg

iNFANFA i

SDCS-LO* ! 3.6SDD5-051 ' NA

NFANFA

NFANFA

SDB10-1.01 0.18SDBI1-O.S' 0.25SDA 10-0.5* ND

NFA

NFANFA

SDC7-1.0T 30.3SDB7-0.51 0.90

NFANFA

NFANFA

SDCll-l.O- 1.45SDDI1-0.5' 2.16

NFANFANFANFANFA

1

NFANFA

SDT2(C)-I.5' . 3.02SDT2(D)-1.5' 0.%

NFA ;

Romd4Sample mg/kg

SDC5-I5' ND

NFANFANFA

SDC7-1.5* NDNFA

SDC11-1.5' 0.056SDDU-1.0 0.054

end of boringNFA

JAH^hMK Page 1 of 2 2/14/97

Table 3

Round 1Sample mg/kg

SDT3(BH>.5' 234

SD 13(0-1.0- 0.22SDT3(DH>.5' , 15.7

I

SDT4(BH>.5' i 0.15SDT4(C)-1.0' | 60SDT4(D)-0.5' j 0.74

I

Culvert Outfall-0.5' 2.08i

Culvert Downstream-0.5' 029

Culvert Upstream (D-0.5* 0.099

Culvert Upstream (2H>.5' 0.36

Round 2Sample mg/kg

SDT3(AH).5' 12

SD-n^H.o- ' 27SDTJPH.O1 | 0.15SOTS^HJ-S1 , 1.0

iNFA I

SDT4(Q-1.S' ' 24.5NFA i

(

Culvert Outfall-1.01 ; 0.03

NFAi

NFA

NFA i1

SDA2-0.5' i 0.223

Round 3Sample mg/kg

SDT3(A)-l.O> 0.08

SDTJfB)-!? i 4.0NFA jNFA

SDT4(AH).51 j NDend of boring !

iNFA ;

(

!

iNFA !

I

Round 4Sample mg/kg

NFAend of boring :

NFA j

(

ii

j

I

1

1

This table presents the process used to determine samples included m each successive round of PCB analysis for the ACS Phase 2Wetland Investigation. Round 1 samples were preselected for analysis before the fkld investigatioo began. Based on Round 1preliminary analytical results. Round 2 samples were selected for analysis. Round 3 samples were then selected based on Round 2, on soon until the samples analyzed had less man 1 mg/kg total PCBs, or die boring intervals were aO analyzed. Samples are included on thistable only one time, regardless of how often a location and interval may be selected by me decision process.

For example, SDB9-0.5' was analyzed in Round 1 with a total PCB result of 14 mg/kg. Five samples (the interval below plus die 0.5'sample from each cardinal direction) were selected for Round 2. Note that one of the five (SDCft-0.5*) was selected in Round 1 andtherefore is not re-selected in Round 2. Of these Round 2 samples, those with total PCBs less taaa 1 mg/kg do not trigger further analysis(Le., "NFA"). SDB10-0.5' had a concentration of 1.2 mg/kg, therefore Round 3 samples were selected from beneath and to the sideswhere previous analysis had not occurred. Of the Round 3 samples, all were less dun 1 mg/kg. therefore no Round 4 analyses wererequired.

Because preliminary results (as opposed to final validated results) were used to select the next round of analysis, some samples near the 1mg/kg cutoff appear to have been selected or missed in error. This problem could not be avoided without significantly missing analysishold-times.

Results are presented as mg/kg tool PCBs.NFA • No further analysis required.ND ** PCBs not detected in sample.Notes:1. Samples analyzed but not presented on this table include:

- SDA5-1.5' was analyzed by die laboratory in error.- SDT3(A)-1.5' was analyzed by die laboratory in error.- SDT2(A)-1.0' was analyzed based on draft results for the 0.5' interval, which were revised to less than 1 mg/kg in the final report.

2. Sample SDD5-0.5' was not analyzed, because SDC5 samples were initially missed by the lab and not completed until mid-January,after Round 4 had been scheduled.3. Sample SDA2-0.5', located in the channel upstream of the culvert, was selected in Round 2 to provide additional coverage within thatportion of the wetland.4. Sample SDC 10-0.5' had a draft total PCB concentration of 1.05 mg/kg, thus Round 2 samples were selected.5. Sample SDT4(A)-0.5' was added in Round 3 for additional coverage.

Page 2 of2 2/14/97

o' oTable 4

Summary of Wetland Sediment Sample Analytical ResultsAmerican Chemical Service, Inc. NPL Site

Griffith Indiana

SampleidAPD-SDA02APD-SDAOSAPD-SDA05APD-SDA09 "APD-SDAIOAPD-SDBOIAPD-SDB04APD-SDB05APD-SDB05APD-SDB06APD-SDB07APD-SDB08APD-SDB09APD-SDB09APD-SDBIOAPD-SDBI 6APD-SDBIIAPD-SDC02APD-SDC04APD-SDC05APD-SDC05APD-SDC05APD-SDC06APD-SDC06APD-SDC07APD-SDC07 DupAPD-SDC07APD-SDC07APD-SDC08APD-SDC08APD-SDC09APD-SDCIOAPD-SDCIOAPD-SDCI 1APD-SDCi IAPD-SDCI 1APD-SDD03

Dcplh0.50.51.56.50.50.50.50.51.00.50.50.50.51.00.51.0

"6.56.56.50.51.0J.5

1 6.5[ 1 . 6

0.50.51.01.50.51.01.00.51.00.51.01.50.5

AR-IOICtig/kg

60 Uf73 Uf42 IV59 IVSI V/94 VI19 IV100 IV42 U/230 IV53 IV97 IV

4,700 IV42 Uf310 IV44 U/

"57 tVUJ72 Uf52 W

270 W270 IV41 IVUJ220 W40 Uf57 U/490 W

4,700 IV40 WVI

7.200 IV43 IV41 IV19 U/44 W62 W45 W42 WVI57 Uf

AR-I22Itig/kg

120 U/150 U/15 IV120 * U/100 IV190 U/ISO W210 IV16 U/

460 VI110 U/200 IV

9,600 U/14 I)/

630 U/90 U/120 "~ U/UJ140 U/110 Uf540 U/550 U/41 U/UJ450 U/12 IV120 IV990 U/

9,600 IVII IVUJ

14.000 Uf17 IV13 U/ISO I/19 U/120 VI91 IV15 U/UJ120 IV

AR-1232Ug/kg

to tv73 IV42 IV59 IV51 IV94 IV19 IV100 IV42 IV230 IV53 IV97 IV

4,700 IV42 IV310 IV44 U/si" ~ unji72 IV52 IV270 IV270 IV41 IVU1220 IV40 IV57 IV490 IV

4,700 IV40 U/UJ

7.200 IV43 IV41 IV19 IV44 IV62 IV45 IV42 U/UJ57 IV

AR-1242utA|

60 U/73 tV42 tV»" ~" ut51 IV94 tV•9 IV100 IV42 Ut230 Uf53 IV97 IV

4,700 IV42 IV

3~IO U/44 IV

~57 IVUJ72 IV52 IV

270 IV270 IV41 IVUJ220 IV40 IV57 IV

490 VI4,700 IV

40 ivUJ7.200 IV

43 IV41 W19 IV44 IV62 Uf45 Uf42 IVUJ57 IV

AR-I24Iug/kf

100 P/160 P/4.2 JP/

~57~ "j/51 IV94 IV31 If250 /42 IV160 J/370 /79 If

2.100 V27 JP/

230 v36 If

" 57 tVUl"49 JP/72 P/

490 P/1,600 /41 IVUJ190 JP/40 IV400 lOfl

15.000 COP/11.000 91

40 U/UJ23,000 /

61 /21 JP/170 P/71 /

1.300 0730 /36 mi62 P/

AR-I2S4ug/kg

70 P/320 /2.1 JP/100 ' P/51 IV15 iff54 If130 142 IV*370 /310 P/250 /

7.100 /41 JP/670 /90 /

" (70 1'"' "a99 Pf230 /440 /1,000 P/41 U/UJ940 /40 IV520 10H

15.000 COP/6^00 P/

40 U/UJ35,000 P/

52 /49 P/360 P/73 P/•60 CP/440 P/20 - J/J170 /

AR-1260ug/kg

53 J/270 /42 IV

""210 ft51 IV41 If14 JP/'

430 P/42 IV190 It220 P/13 J>

4,900 P/42 IV300 Iff54 P/

"i4~ "" /i""63 JP/130 P/490 P/1.000 /41 IVUJ760 /40 IV310 JDP/

10.000 COP/13,000 P/

40 U/UJ15,000 P/

43 IV23 Iff170 P/44 IV360 P/2SO /42 U/UJ«7 P/

Total PCBfm|/kg0.2230.750.0070.367ND

0.0560.1061.5ND0.720.900.41214.1

0.0681.2

0.180.2540.210.4321.423.6ND1.89ND1.2340.030JND73

6.120.0930.7

0.1442^21.45

0.0560.319

Mercurymg/kg

n*M

niIW

na0.43 Uf

na0.28 /

nananaM

0.28 /nin»n*na

0.24 U/0.17 U/

nanana

O.I2U/nanananana

0.6 /na

O.I2U/O.I2UN/UJ

nananana

0.17 Uf

SO-FINAL XLS/Fhu) Tiblt Page I of3 C 2/13/97

' ' € 'Table 4

Summary of Wetland Sediment Sample Analytical ResultsAmerican Chemical Service, Inc. NPL She

Griffith Indiana

SampleidAPD-SDD06APD-SDD07APD-SDD08APD-SDD09APD-SDDIOAPD-SDDI 1APD-SDDI 1APD-SDTI (B)APD-SDT1 (C)APD-SDTI (D)APD-SDT2 (B)APD-SDT2(C)APD-SDT2 (D)APD-SDD (B)APD-SDT3 (C)APD-SDT3 (D)APD-SDT4 (B)APD-SDT4 (C)APD-SDT4 (D)APD-SDTI (A)APD-SD T1(B)APD-SDTMOAPD-SD fJ(D)APD-SD T1(E)APD-SD T2 (A)APD-SD T2 (A)APD-SD T2(B)APD-SDt2(C)APD-SD T2(C)APD-SD T2(D)APD-SD T2(D)APD-SD T2(E)APD-SbT3(A)APD-SDT3(A)APD-SD T3 (A)APD-SD T3(B)APD-SD T3(B)

Depth0.50.50.50.50.50.51.00.50.56.5"0.50.50.50.5i.o0.50.51.00.50.51.61.01.60.50.5.0.0.0.5.0

' '.'5 "

0.50.51.01.5.0

1.5

AR-IOI6ug/kg

12 VI160 IV

"46" ~U/~39 U/

~ ~75 " U/ "94 VI42 IVUJ

2.200 IV3.000 IVijzoo ' " ~ u/f.200 IV

15,000 Ut16,000 "' U/34,000 ' VI

41 ' VI3.600 IV

43 IV32,000 U/

•0 IV19 VI43 ~IV15 VIu DV72 VI59 U?42 IV52 IV

~4t " "U/410 VI51 VI

"52 ~ tV36 IV42 U/

"41 '" Vl"II " U/$30 " VI '46 VI

AR-IJ2IUg/kg

170 VI"340 IV

12 IVto vi

"J50 "U/"190 V16 ' /Vi

4,500 U/6.100 IV

2.400" IV"woo" u>170.000 IV'34",000" '" IV70,000 " VI

97 VI7400 IV

17 VI64,000 VI

160 IVISO U/97 IV170 IVlib "" u/ "140 VI120 IV16 VI100 IV91 VI970 VI100 IV

"106" uf74 IV•4 IV ~

"»4 " Vl'" J60 VI

1,100 VI'" 93 VI

AR-1232ug/kg

S2 IV160 " VI40 IV39 VI

• 73 ~ ~ ijr

94 IV42 IVUJ

2,200 IV3,000 U/1,200 VI1,200 IV

S5.000 IV16.000" "tV34JOOO IV

41 VI3.600 VI

43 VI32,000 VI

10 VI99 VI43 U/"15 tVtt tV "72 U/"59 IV42 IV52 IV41 " VI4t6 IV51 VI

'" si" u/36 IV

~ 42 " VI" 4 1 V I

SI VI530 " Ut46 VI

AR-1242Ug/kg

12 IV160 IV

"40" IV39 IV75 ~ ~Vt~~94 VI42 U/UJ

2.200 IV3.000 U/1.200 VIUOO" IV

15,000 IV16.000 ' VI34,000 IV4l" U/

3.600 IV43 IV

32.000 U/W IV•» U/

" 43" ~" IV15 IV

" a vi72 VI59 IV42 IV52 IV

""41"" "tv410 IV51 IV52 U/36 IV42 IV

" 4 1 VIII VI530 IV46 IV

AR-l24tuiAf

12 tV71 JP/40 IV "1.1 JP/

"75 u/6M> P/

16 JP/J

t.SOO JP/

2400 JP/

sib m930 V "

99,000 /6,700 JP7 "54,000 ft

SO ftzjoo nv

13 JP/10,000 JP/

22 mS9 IVii "" jp/120 ftW " " IV57 JP/59 VI5 J/

ISO P/1,100 CDF/1JOO /4400 civ510 " 7 "3« IV

5,6oo" " DP/14 JP/II U/

13,000 PD/2.200 PD>

AR-IU4ug/kg

12 U/320 " " /44 " >/12 JP/95 " P/ "~

940 /

31 J/J4.SOO P/9JOO P/

"3,500 >/3.400 P/

200,000 /"17,006 /150,000 /

100 /7.000 /

SO ft31,000 JP/

520 /570 /35 It250 /

" 160 " " / " "ISO P/260 P/10 V

200 P/* 2,000 CDP/

1.000 /3.400 CD/

" 3 1 0 " /36 VI

6j600 DP/52" /110 ft

14,000 . PD/""r.t6o PD/ "

AR-II60ug/kg

12 U/"250 T "

40 "" " U/"6.9 JP/35 " "JP/~540 /42 IVUJ

3.600 /2.MO J1 00 " /

"2,900 ft60,000 JP/5.400 JP/"30.000 JP/

43 JP/6400 P/

61 P/19.000 II200 /240 P/10 It91 P/S~ " "JP/ ""72 U/59 U/7.2 U100 /

"960 " DP/720 P/1,700 D/140" " >/36 IV

""«" "u/ "" 14 JP/

22 JP/530 IV

"46 V/~

Total PCBsmg/kgND0.656.0440.02101302.160.05410.214.45.27.23359292340.2216

0.1560

0.740.816.0630.4610~I980.2370.2600.0220.484.763M9.400.96ND11.60.080.132V4.0

Mercurymg/kg

na0.1 1U/

naO.IOU/

nana ,na '?

0.44 / t1.4 /2.6 /

0.15 U/6.1 /1.6 /1.2 /

0.13 Ut2.5/

O.I9UN/UJ0.28 N/J

0.12 UN/UJnana

« '*. "• 'rna <nanana

na

nana

na

na

na

na

na

na

na

"««e 2 of3 2/11/97

O:*)

Table 4Summary of Wetland Sediment Sample Analytical Results

American Chemkal Servke, Inc. NPL SiteGriffith Indiana

SampleidAPD-SD T3(D)APD-SD T3(E)APD-SD T4 (A)APD-SD T4(C)APD-Culvert DownstreamAPD-Culvert OutfallAPD-Culvert OutfallAPD-Culvert Upstream (1)APD-Culvert Upstream (2]

Depth1.00.50.5l.S0.50.51.00.50.5

AR-IOI6ug/kg

44 VI"320 "u/

41 U/UJ4JO IV41 VI

7t VI

51 VI77 VI

94 IV

AR-1221ug/kg

SI VI

660 ' VI94 U/UJ

"»40 " " IV97 IV160 IV100 n>

160 ','190 IV

AR-1232ug/kg

44 VI

320 VI

41 U/UJVlO IV41 IV71 U/51 VI

77 tV94 IV

AR-1142ug/kg

44 IV320" U/41 U/UJ410 IV "

_ 41 VI

n tv51 IV

77 IV94 tV

AR-1241ug/kg

61 P/320 /41 IVUJ

12,000 DC/"

51 /510 /51 IV29 1ft

110 /

AR-11S4ug/kg

19 P/

320 /41 IVUJ

7,700 DC/110 P/

110 fl

2*1 JP/43 JP/?40 /

AR-1260ug/kg

44 VI

"400 " "/41 IVUJ

"4.106" "bcprf20 /

760 flSI VI27 JP/

110 ft

Total PCBsmg/kg0.151.04ND24.50792.080.0280.100.36

Mercurying/kg

nanaM

naO.MUN/UJ0.16UN/UJ

naO.I7UNAJJO.I9UN/UJ

fc.-A .

FKneS,

This table presents final, validated results for sediment sample* collected M the ACS Site In Griffith, Indiana between November 20 and 22,1996. Samples were analyzed in rounds. Round I was determined by mutual agreementbetween all parlies Rounds 2.3, and 4 were selected to include intervals to the side and beneath any sample with a total PCB concentration greater than I ppm (based on preliminary results; final results may have been revised).

For each sample and analyte. this laMe presents the result (either the reported concentration or the reported sample quantitation limit) followed by the laboratory qualifier / data validation qualifier.

Laboratory Qualifiers:U - Undetected at the reported sample quanlilation limit (CRQL adjusted for dry weight, splits and any dilution factor).J - The associated numerical value is an estimated quantity, because the value was less than the sample quantitation limit (SQL).P - This qualifier is used for a pesticide/PCB target compound when there is greater than a 25% difference for the detected concentnC * Identification confirmed by CC/MS.D =• Result from secondary dilution analysis. In general, the result from the least dilute analysis that is also within the instrument liiN - Indicates spike sample recovery was not within contra) limits.na- Not analyzed.

> the two GC columns. The lower of the two values is reported.

nge is reported.

Data Validation Qualifiers:Where required, data validation qualifiers have been added after the lab qualifier and separated by a "/*.U - Result is qualified as undetected at the reported concentration (either Ihe sample result or oV SQL. which ever to greater) due to comaminationm an assJ - Result is estimated due to validation QC criteria (e.g. hokhimc exceedence).

SD-FINAL XLS/Fiml Table Page 3 of3 C 2/13/»7

O

Ti

\ *r**C .—.— -, » i'jntB*'?™ FwE.-au *

W Bitj TsP'-M

% i CrSO T3DJ c*3;-**5P •'B ^B1L7

AlTY TOC* T*W* r o-i*

Hf mK^rS LTM s7*s**-i>-;**** * > HEP / Xf Mk \ '-*v

liff Tf.*f"9%1.T2A Jb »•« § ,

o^T/IW"* ^•v^SJC^v »-'»r\., Ti. l^f"r>" T4C> ^> lnv

^ XT4ffl/ -MAn./y / Jf*• — / ' s

<\

•-^v'vj

"t-^ s,\

i£££HQ- - CHANNEL COURSE

SEDIMENT/SOIL SAMPLE LOCATION* AND NUMBER, FROM PHASE 1

WETLAND INVESTIGATION

.. - . - . TOTAL PCB CONCENTRATION.in mg/kg FROM PHASE 1WETLAND INVESTIGATION

_AI WETLAND SAMPLE LOCATIONWi AND NUMBER

SUMMARY OF TOTAL PCB RESULTS

2.52 - 0.5 ft]1.45 - 1.0 ft.(- ALL RESULTS IN mg/kg (ppm)

NO - 1.5 ft]

NO NOT DETECTED (DETECTION LIMITAPPROXIMATELY 0.05 mg/kg)

E EXTRACTED. NOT ANALYZEDNR ANALYSIS NOT REQUESTED

X"

T4Ew!ii$&&,'*Sj»wllrii m

Iff*s?

MOTES1. BASE MAP DEVELOPED FROM AN AERIAL

SURVEY MAP OF THE SITE FLOWN ONMARCH B, 1994 BY GEONEX CHICAGOAERIAL SURVEY, INC. . CONTOUR INTERVALIS TWO FEET.

2. SEDIMENT SAMPLES COLLECTED 3YMONTGOMERY WATSON FROM NOVEMBER 18TO NOVEMBER 21, 1996.

northO flQ 160aw iww

•*mt LHJ !•••••••••••

SCALE IN FEET

FlfillRF 1

a£

I 1

* *

11

si5

i !

e•9•«X3

23

j1

y5

**liLx

f tin

1252042 _.0809.0078 81

"'mffiir'0

(J o

PCBs IN SEDIMENTS 0-0.5 FEET DEEP

-- CHANNEL COURSE

1 SEDIMENT/SOIL SAMPLE LOCATIONAND NUMBER, FROM PHASE IWETLAND INVESTIGATION

•gjyffTlrTT"! I Tatll

:S2 - O.S ftl.45 - i.o ftk-ND - 1.5 ftj

f _D7 «T \<VL HSw I \ ) WisiT\ 8 M •<*«

In mg/kg FROM PHASE IWETLAND I

TOTAL PCB CONCENTRATION.* FROM PHASE

INVESTIGATION

WETLAND SAMPLE LOCATIONAND NUMBER

APPROXIMATE t mg/kg PCBISOCONCENTRATION CONTOUR

APPROXIMATE 10 mo/ko PCBISOCONCENTRATION CONTOUR

ALL RESULTS IN mg/kg (ppm)

NOT DETECTED (DETECTION LIMITAPPROXIMATELY 0.05 mg/kg)EXTRACTED, NOT ANALYZEDANALYSIS NOT REQUESTED

NOTESBASE MAP DEVELOPED FROM AN AERIALSURVEY MAP OF THE SITE FLOWN ONMARCH B, 1984 BY GEONEX CHICAGOAERIAL SURVEY, INC. CONTOUR INTERVALIS TWO FEET.

SEDIMENT SAMPLES COLLECTED BYMONTGOMERY WATSON FROM NOVEMBER 18TO NOVEMBER 21. 1996.

THE ISOCONCENTRATION CONTOURS WEREESTIMATED MANUALLY USING THEANALYTICAL DATA.

rioHh80

SCALE IN FEET

160

FIGURE 2

12520420009.0078

C)

PCBs IN SEDIMENTS 0.5-1 FEET DEEP

LEQENp— CHANNEL COURSE

W)V SEDIMENT/SOIL SAMPLE LOCATION* AND NUMBER, FROM PHASE 1

WETLAND INVESTIGATION

B .' . TOTAL PCB CONCENTRATION.In mg/kg FROM PHASE 1WETLAND INVESTIGATION

.^M WETLAND SAMPLE LOCATIONm AND NUMBER

. APPROXIMATE 1 mg/kg PCS* ISOCONCENTRATION CONTOUR

~ APPROXIMATE 10 mg/kg PCBw ISOCONCENTRATION CONTOUR

SUMMARY OF TOTAL PCB RESULTS

2.52 - 0.5 ft]1.45 - 1.0 ft,}— ALL RESULTS IN mg/kg (ppm)

"9C TOE / fi NO - 1 .5 fy

T JM\M NO NOT DETECTED (DETECTION LIMIT*8P TaoJTS APPROXIMATELY 0.05 mg/kg)^>» ' •,£, /--'' E EXTRACTED, NOT ANALYZEDT2CT3C/ "* ' NR ANALYSIS NOT REQUESTED

/ ^^*t ^ NOTES/ "* 1. BASE MAP DEVELOPED FROM AN AERIAL/ SURVEY MAP OF THE SITE FLOWN ON/ MARCH 8. 1994 BY GEONEX CHICAGO

AERIAL SURVEY, INC. CONTOUR INTERVALIS TWO FEET.

2. SEDIMENT SAMPLES COLLECTED BYMONTGOMERY WATSON FROM NOVEMBER 18TO NOVEMBER 21. 1998.

3. THE ISOCONCENTRATION CONTOURS WEREi ESTIMATED MANUALLY USING THEX. ANALYTICAL DATA.

-<XX>north0 80 160

SCALE IN FEET

FIGURE 3

-1aiii

1* *1!

|ti1

!i

\

i

!n

:-

=! .

AM

ER

ICA

N C

HEM

KN

PL

SI

TEG

RIF

FITH

. IN

DIA

N/

Onwing Numtar12520420809.0078 83

"i"

C

LEQEMD

CHANNEL COURSE

PCBa IN SEDIMENTS 1-15 FEET DEEP

SEDIMENT/SOIL SAMPLE LOCATIONAND NUMBER, FROM PHASE IWETLAND INVESTIGATION

TOTAL PCB CONCENTRATION.In mg/kg FROM PHASE IWETLAND INVESTIGATION

WETLAND SAMPLE LOCATIONAND NUMBER

. APPROXIMATE 1 mg/kg PCBN CONTOUR

RESULTS IN mg/kg (ppm).

APPROXIMATE 10ISOCONCENTRATION

NOT DETECTED (DETECTION LIMITAPPROXIMATELY O.O5 mg/kg)

YZEDEXTRACTED. NOT ANALANALYSIS NOT REQUESTED

M ^8 0.1

^upstream

r r an, H^

BASE MAP DEVELOPED FROM AN AERIALSURVEY MAP OF THE SITE aOWN ONMARCH B. 1994 BY GEONEX CHICAGOAERIAL SURVEY, INC. CONTOUR INTERVALIS TWO FEET.

SEDIMENT SAMPLES COLLECTED BYMONTGOMERY WATSON FROM NOVEMBER 18TO NOVEMBER 21. 1998.

THE ISOCONCENTRATION CONTOURS WEREESTIMATED MANUALLY USING THEANALYTICAL DATA.

north

FIGURE 4

a

*ii

* £

t

1

1

8

[

!

i!

Si

!iDmrinf Numtar12S20420809.0078 84

""ilwiiSr

C)

toutfall1

t~

IIJIifj

I

LEQEND

CHANNEL COURSE

_,B1 WETLAND SAMPLE LOCATIONSI AND NUMBER

2.5 TOTAL MERCURY CONCENTRATION,in mg/kg

ND NOT DETECTED (DETECTION LIMITAPPROXIMATELY 0.1 mg/kg)

MOTESt. BASE MAP DEVELOPED FROM AN AERIAL

SURVEY MAP OF THE SITE FLOWN ONMARCH 8. 1994 BY GEONEX CHICAGOAERIAL SURVEY, INC. CONTOUR INTERVALIS TWO FEET.

2. SEDIMENT SAMPLES COLLECTED BYMONTGOMERY WATSON FROM NOVEMBER 18TO NOVEMBER 21. 1996.

80

SCALE IN FEET

160

FIGURE 5

12520420809.0078 B6

C

AP

•ND

C

.•N.

ANALYTICAL RESULTS

Al PCB Analytical ResultsA2 Mercury Analytical Results

Al

PCB ANALYTICAL RESULTS

Summary of Wetland Sediment Sample AnalysesAmerican Chemical Service

Griffith Indiana

SampleidSDG 65603APD-SDB5APD-SDC6APD-SDC8APD-SDB9APD-CuNen OutfallAPD-SDD8APD-SDD6APD-SDCIOAPD-SD T1(E)APD-SD T2( A)APD-SD T2(E)APD-SD 13 (A)APD-SD T3(B)APD-SD T3(B)APD-SD T3(D)SDG 12560APD-SDC7APD-SDB7APD-SDDI 1APD-SDCSAPD-SDC11APD-SDCSAPD-SDT2(C)APD-SD T2(D)APD-SDA10SDG 1189APD-SD T4 (A)APD-SDB11SDG 1349APD-SDC11APD-SDC7APD-SDCSAPD-SDDI 1SDG 11589APD-SDC7APD-SD T2(B)APD-SD T2(QSDG 11591APD-SDC7 DupAPD-SDC11APD-SD T4(QAPD-SDA2APD-SDA9APD-SDA5SDG 11593APD-SDDIOAPD-SD Tl (A)

Depth

1.01.01.01.01.00.50.5IX)05050.50.514131.0

1.0030.5U)IJQ051.51505

0505

•1515151.0

0 51.01.0

050515050505

0505

Lab*IEA-NJ656030016560300365603005656030076560300965603012656030156560301765603023656030326560303465603036656030386560303965603040IEA-NC961256001961256002961256003961256004961256005961256006961256007961256008961256009IEA-NC970118901970111902IEA-NC970134901970134902970134903970134904IEA-NC9611599479611589-089611589-16IEA-NC

9611591-039611591-049611591-059611591-129611591-159611591-20IEA-NC9611593-019611593-17

SampleDate

11/20/9611/20/9611/20/9611/20/9611/30/9611/20/9611/20/9611/20/9611/21/96H/20/9611/20/9611/20/9611/20/9611/20/9611/20/96

11/210611/21/9611/21*611/21/9611721/96II/2I/M11/20/9611/20)9611/21/96

11/21/9611/21/96

11/21/9611/21/9611/21/9611/21/96

11/21/9611/21/9611/20/96

11/21/9611/21/9611/20/9611/21/9611/21/9611/21/96

11/21/9611/21/96

ExtractDace

12/2/9612/2/9612/2/9612/2/9612/20612/2/9612/2/9612/2/9612/2/9612/20612/2/9612/2/9612/2/9612/2/9612/2/96

12*0612/4*612*0612/40612/4/9612/3/9612*0612/40612/4/96

1/14071/1407

12/90612/30612/4/9612/406

12/30612/30612/306

12*0612/40612/40612/40612/40612*06

12/40612/406

121212121212121211121212121212

131313131312141413

5454

12121313

121213

131314131313

1313

RaoDate

12/140612/140612/150612/150612/150612/150612/140612/15/9612/150612/150612/150612/150612/W061/507

12/1506

1/12071/12071/10071/12/971/12071/12071/12071/10071/1007

1/21071/2107

1/21/971/28071/28071/2807

12/200612/200612/2006

12/190612/180612/190612/150612/140612/1406

12/130612/1406

121213131313121313131313133513

393937393940393737

77

49565555

171717

151415U1010

910

Pagel

Summary of Wetland Sediment Sample AnalysesAmerican Chemical Service

Griffith Indiana

SampleidSDG 11595APD-SD T2(D)SDG 2581AAPD-SDC2APD-SDD3APD-SDC4APD-SDB5APD-SDC6APD-SDD7APD-SDC8APD-SDB9APD-SDC9APD-SDD9APD-SDTI (B)APD-SDTI (QAPD-SDTI (D)APD-SDT2CB)APD-SDT2(OAPD-SDT2(D)APD-SDT3(B)APD-SDT3 (OAPD-SDT3CD)APD-SDBISDG 2581BAPD-Culvert OutfallAPD-Culvert DownstreamAPD-Culvert Upstream (1)APD-SDCIOAPD-SDT4(B)APD-SDT4(QAPD-SDT4(D)APD-Culvert Upstream (2)SDG2645AAPD-SDB6APD-SD T1(B)APD-SD T2 (A)APD-SD T3(E)APD-SD T1(D)APD-SD T3 (A)SDG2650AAPD-SDB10APD-SD A5APD-SDB4APD-SDB10APD-SDB8APD-SD T1(QAPD-SD T3 (A)

Depth

1.0

05050505050505051.00505050.50.50.505051.00.505

05050505051.00505

051.01.0051.015

05150.51.00.51.01.0

Lab#IEA-NC9611595-09IEA-CT962581A-01962581A-02962581A-03962581A-04962S81A-05962581A-06962581A-07962581A-08962581A-09962581A-10962581A-1196258IA-12962581A-13962S81A-14962581A-15962581A-16962S8IA-I7962581A-18962581A-19962581A.20IEA-CT962S81B-OI962S81B-02962S81B-03962581B-04962581B-05962S81B-06.9625818-07962581 B-08IEA-CT962645A-OS962645A-07962645A-10962645A-15962645A-16962645A-20IEA-CT962650A-01962650A-05962650A-07962650A-12962650A-13%2650A-179626SOA-18

SampleDate

11/2006

11/20/9611/200611/200611/200611/20/9611/200611/200611/200611/200611/200611/200611/200611/200611/200611/20/9611/200611/200611/200611/200611/2006

11/200611/200611/200611/200611/200611/200611/200611/2006

11/210611/200611/200611/210611/200611/2006

11/210611/210611/210611/21/9611/210611/21/9611/21/96

ExtracDate

12/406

11/210611/210611/210611/210611/210611/210611/210611/210611/210611/210611/210611/210611/210611/210611/21/9611/210611/210611/210611/210611/2106

11/210611/210611/210611/210611/210611/210611/210611/2106

12/30612/30612/30612/30612/30612/306

12/40612/40612/40612/4/9612/4/9612/4/9612/4/96

t

14

1111

121313121313

13131313131313

RunDate

12/1906

11/230611/230611/230611/230611/250611/240611/260611/260611/240611/250611/260611/260611/260611/260611/250611/250611/250611/250611/250611/2506

11/230611/230611/240611/240611/240611/28/9611/240611/2906

12/140612/14061/307

12/140612/170612/1406

12/140612/150612/15061/307

12/150612/15061/3/97

15

22224355345555444444

22

333738

111131111411

10U1130U1130

Page 2

IDPESTICID%ORGANICS ANALYSIS DATA SHEET

Lab Name: IEA-NJ Contract:

Code: IEANJ Case No.: SAS No.

Matrix: (soil/water)tSOlL

'Sample wt/vol: 30 (g/ml) g

Moisture: 22 decanted: N•»

Extraction: (SepF/Cont/Sonc) SONG

Concentrated Extract Volume:SOOO (uL)

Injection Volume: l.O (uL)

GPC Cleanup: (Y/N)Y_ pH:6.7

NO. COMPOUND

SDG No.:

Sample ID: 6,560.3001

Lab File ID: D4BCLP99I 024

Date Received: 11/25/96

Date Extracted: 12/02/96

Date Analyzed: 12/14/96

Dilution Factor: l.O

Sulfur Cleanup: Y

CONCENTRATION UNITS: Q(ug/L or ug/Kg)

12^74-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor-1016Aroclof-l!Arocior-iaAroclor-]Arocior-]

.2132

L242L248

ATOCJ.Or-1254Aroclor- 12 60

42864242424242

0ttuuutlu

FORM 1 PEST

VAU

OLM03

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

•-SDC6-1.0

Lab Name: IEA-NJ Contract: 68D50011

Lab Code: IEANJ Case No.: SAS No.: SDG No.:

Matrix: (soil/water):SOIL

Sample wt/vol: 30 (g/ml) cr_

Moisture: 19 decanted; N


Concentrated Extract Volume:5000 (uL)


_ GPC Cleanup: (Y/N)Y_ pH:6.8

NO. COMPOUND

Lab Sample ID: 65603003





Dilution Factor: J..O

Sulfur Cleanup: £_

CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-!Aroclor-:

.221L232

Aroclor- 1242Aroclor- 1248Aroclor- 1254Aroclor- 1260

40824040404040

UUUUUUU

FORM 1 PEST

VALIDATEDOLM03.0


O00051EPA SAMPLE NO.

-SDC8-U)'

Lab Name: IBA-NJ

~~Lab Code


Contract: 68D50Q11

IEANJ Case No.: SAS No.: SDG No.:


Sample wt/vol: 3_Q (g/ml) o

Moisture: 23 decanted: N_





NO. COMPOUND

Lab File ID: D4BCLP991_049

Date Received: n/25/96




Sulfur Cleanup; Y

CONCENTRATION UNITS:(ug/L or ug/Kg)

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Aroclor- 1232ATOClOr-1242ATOClOr-1248Aroclor- 1254Aroclor- 12 60

43tit434268£i4J

puuuu

u

FORM 1 PESTOLM03. C

VALIDATED


.si Lab Name: IEA-NJ Contract: 68D50011

- Lab Code: IEANJ Case No.: SAS No.: SDG No.


Sample wt/vol: 30 (g/ml) g

Moisture: 21 decanted: N


Concentrated Extract Volume;5000 (uL)


GPC Cleanup: (Y/N)Y_

NO. COMPOUND— '^Ar

Lab Sample ID: 656Q3007

Lab File ID: D4BCLP99I_047




Dilution Factor: 1.0 _

Sulfur Cleanup: Y

CONCENTRATION UNITS : Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016ATOClOr-1221Aroclor- 1232Aroclor- 1242Aroclor- 1248ATOClOr-1254Aroclor- 12 0

42844242274142

UUuuJPJPD

«..

FORM 1 PESTOLM03.0

VAL!


CULOUT-1'

Lab Name: IEA-NJ Contract: 68D5Q011

'Lab Code: IEANJ Case No.: SAS No.: SDG No.:

Matrix: (soil/water) -.SOIL

Sample wt/vol: 30 (o/ml) a



Concentrated Extract Volume:5QOQ (uL)


GPC Cleanup: (Y/N)Y_

NO. COMPOUND






Dilution Factor: 1.0

Sulfur Cleanup: Y

CONCENTRATION UNITS:(ug/L or ug/Kg) 2S/15S

12674-11-2111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016ATOCJArocJ

Lor- 1221LOr-1232

Aroclor- 1242Aroclor- 124 8

TGrbc.Aroc.

.or- 1254

.or- 12 60

511005151512851

UUUuuJi?u

FORM 1 PESTOLMO


NO

-SDD8-0.5'

Lab Name: IBA-NJ Contract: 68D50011

"Lab Code: IEANJ Case No.: SAS No.: SDG No.:

Matrix: (soil/water);SOIL

Sample wt/vol: 30 (g/ml) o



Concentrated Extract Volume:5OOP (uL)


.GPC Cleanup: (Y/N)Y__ pH:6.4

NO- COMPOUND







Sulfur Cleanup: Y


-

~' "•

12374 -i:11104-2111141- 1(

L-23-25-5

53469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Aroclor- 1232Aroclor- 12 42Aroclor- 1248Aroclor-]Aroclor-:

L254.260

4082464b40

-£*- 44JAtf 40

UUUUUPU

FORM 1 PEST

VAT! DATED

OLM03.0

IDPESTICIDE ORGANICS ANALYSIS DATA, SHEET

EPA

Lab Name: IEA-NJ Contract: 68D5QQ11


Lab Sample ID: 6S603Q15Matrix: (soil/water):SOIL

Sample wt/vol: 30 fg/mll o


Extraction: (SepF/Cont/Sonc) SONG.4

_ Concentrated Extract Volume:5000 (uL)


_GPC Cleanup: (Y/N)Y__ pH:6_JL-

NO. COMPOUND






Sulfur Cleanup: Y_


12*74-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016ATOClOr-1221ATOClOr-1232ATOClOr- 1242Aroclor- 124 eAroclor- 1254Aroclor- 1260

821708282826282

0uuuuuu

FORM 1 PEST

VALIDATED

OLM03.0


OOOOS.'JEPA SAMPLE NO

SDC10-1.0

>j





^ Moisture: 25 decanted: N

-^ Extraction: (SepF/Cont/Sonc) SONG

_ Concentrated Extract Volume:§000 (uL)

- Injection Volume: l.O (uL)

£? GPC Cleanup: (Y/N)Y_ pH:I

NO. COMPOUND

Lab Sample ID: 65603Q17






Sulfur Cleanup: Y


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 122!Aroclor- 1232Aroclor- 1242Aroclor- 124sAroclor- 1254Aroclor- 12 60

894444717344

UUUU

Pu

• • '.*

FORM 1 PEST

VALIDATEDOLM03.0


0000,%EPA SAMPLE'NO.

ftrt> SDT3/BV0.5'


Lab Code: IEANJ Case No.: SAS No.: _ SDG No.:

Matrix: (soil/water) .-SOIL

Sample wt/vol: 30 (g/mli a


j Extraction: (SepF/Cont/Sonc) SONG

^ Concentrated Extract Volume:5000 (uL)

,„ Injection Volume: l.O (uL)

GPC Cleanup: (Y/N)Y_ pH:

NO. COMPOUND







Sulfur Cleanup: Y_

CONCENTRATION UNITS: Q(ug/L or ug/Kg) Bfi/Kfi

12574-H-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016ATOClOr-1221Aroclor- 1232ATOClOr-1242ATOClOr-1248ATOCJLOr-1254Aroclor- 1260

7214072725718072

(JUUuJPPu

FORM 1 PESTOLM03.0

VALIDATED


EPA SAMPLE NO.

•SDT2fc>.5'




Sample wt/vol: 30 (g/mll g

Moisture: 44 decanted: N•>Extraction: (SepF/Cont/Sonc) SONG

Concentrated Extract Volume;5000 (uL)••» ^ •• •• • a—«««« i«»

.., Injection Volume: 1.0 (uL)

Cleanup: (Y/N)Y_ pH;6.2

COMPOUND


Lab File ID: D4BCLP99I_Q38





Sulfur Cleanup: Y

CONCENTRATION UNITS: Q(ug/L or ug/kg) UG/KG

12574-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor-:Aroclor-:Aroclor- 3

LOl*.221L232

Aroclor- 1242Aroclor- 1248Aroclor- 1254Aroclor- 12 60

5912059595926059

UUUUuPu

FORM 1 PESTOLM03.0

VALIDATED


O00115EPA SAMPLE NO.

-SDT2fe). 5'

Lab Name: IEA-NJ Contract: eapsooii

Lab Code: JEANJ Case No.: SAS No.: SDG No.:

- Matrix: (soil/water);SOIL

Sample wt/vol: 30 fg/mll a

- Moisture: 2 decanted: N

-- Extraction: (SepF/Cont/Sonc) SONC

~~ Concentrated Extract Volume:5000 (uL)


• GPC Cleanup: (Y/N)Y_ pH;5.3

NO. COMPOUND







Sulfur Cleanup: Y__


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1ll096-B2-5

Aroclor- 1016Aroclor- 1221ATOClOr-1232ATOClOr-1242Aroclor- 1248Aroc.ATOC.

.or-:

.or-:.254.260

36743636363636

TJUUuuuu

FORM 1 PESTOLM03

VAT! DATED


EPA SAMPLE NO.

SDT3A>Q5'


Lab Code: IEANJ Case No.: _ SAS No.: _ SDG No.:


Sample wt/vol: 30 (a/ml) a


Extraction: (SepF/Cont/Sonc) SONC


Injection Volume: 1.0 (uL)


CAS NO. COMPOUND


Lab File ID: D4BCLP99I040





Sulfur Cleanup: Y

CONCENTRATION UNITS:(ug/L or ug/Kg) OS/KG

12574-11-211104-28-211141-16-553469-21-912672-29-611097-69-1ll096-82-5

Aroclor- 1016Arocior-1221ATOClOr-1232ATOClOr-1242Aroclor- 1248Aroclor- 1254Aroclor- 1260

«844242

•S.tw 3900- .*,**>* 009"

42

"U"UUUBP»>EPPU

FORM 1 PESTOLM03.0

VALIDATED

I./*.


EPA SAMPL

SpT3A-.5'DL

Lab Name: IEA-NJ

Lab Code: IEANJ Case No.:

- Matrix: (soil/water) :SQIL_

Sample wt/vol: 30 (a/ml) o

- Moisture: 21 decanted: N

- Extraction: (SepF/Cont/Sonc) SONG

""• Concentrated Extract Volume:5000 (uL)


^ GPC Cleanup: (Y/N)Y_ pH:6.7

Contract: 6BD50011

SAS No.: SDG No.

•<_*as NO. COMPOUND

Lab Sample ID: 65603036DL

Lab File 3D: D4BCLP99AL013




Dilution Factor: IQ.Q

Sulfur Cleanup: Y_


12674-11-211104-28-211141-16-553469-21-912672-29-61]13L097-69-11096-82-5

Aroclor- 1016ATOClOr-1221ATOClOr-1232Arocior- 1242Aroclor- 1248Aroclor- 1254Arocior- 1260

42084042042050006600429

UDUUPDPDu

~O

FORM 1 PESTOLM03

VALIDATED


Contract: 6BD50011


O0013SEPA SAMPLE NO

•SDT3(B)-1.0'

Lab Name: IEA-NJ

Matrix: (soil/water) :SOIL

Sample wt/vol: 30 (o/ml) g



Concentrated Extract Volume: 5000 (uL)


_GPC Cleanup:

CAS NO.

(Y/N)Y_

COMPOUND

pH:6_JL_


Lab File ID: D4BCLP99I_042





Sulfur Cleanup: Y


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Arocior- 1232Arocior- 1242Arocior- 124 8.Aroclor -12 54Arocior-1260

5351100530530

13000/4*vro 13000-

530

uuuuE l>B 0U

FORM 1 PESTOLM03.0

VALIDATED


000145EPA SAMPLE NO

SDT3(B)-1.0'I




Sample wt/vol: 30 fg/ml) g





Cleanup: (Y/N)Y__

CAS NO. COMPOUND


Lab File ID: P4BCLP99I 041





Sulfur Cleanup: Y

CONCENTRATION UNITS: Q(ug/L or ug/Kg) UJJ/Efi

11104-28-211141-16-5

Arocior-1221Arocior-1232

110005300

UU

53469-21-9 Arocior-124212672-29-6 Arocior-124811097-69-1 Arocior-125411096-82-5 Aroclor-1260

530013000140005300

UPDPDU

FORM 1 PEST

VALIDATEDOLMO

~ Lab Name: IEA-NJ


Contract: 68D50011

SAS No.: SDG No.:

OOO15JJEPA SAMPLE NO.



Sample wt/vol: 30 (a/ml) a






CAS NO. COMPOUND

11104-28-211141-16-553469-21-912672-29-6J1097-69"=T11096-82-5

Aroclor- 1221Arocior- 1232Aroclor -1242Aroclor-1248Aroclor-1254Arocior- 1260


Lab File ID: D4BCLP99H 071





Sulfur Cleanup: Y


934646

2400"46

uuuEP?

u

"O

FORM 1 PESTOLM03.0

VALIDATED

-. Lab Name: IEA-NJ


Contract: 68D20022

SAS No.: SDG No.:

EPA

APD-SDT3B-1.



Sample wt/vol: UQ _ (g/ml) g



Concentrated Extract Volume: 5000 (uL)



NO. COMPOUND

Lab Sample ID: 656Q3Q39DL

Lab File ID: D4BCLP99J 022



Date Analyzed: Qi/07/97

Dilution Factor: J.O.0-

Sulfur Cleanup: Y_


12674-11-211104-26-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Arocior- 1232Arocior- 1242Arocior- 1248Aroclor- 1254Arocior- 1260

46093046046022dOiedo460

uuutfPDPDfttf

(

.J

FORM 1 PEST

VALIDATED


EPA SAMPLE NO


•Lab Code: IEANJ Case No.: SAS No.

Matrix: (soil/water):SQIL







SDG No.:

NO. COMPOUND


Lab File ID: D4BCLP99T_Q43





Sulfur Cleanup: Y


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Aroclor- 1232Aroclor- 1242Arocior- 1248Aroclor- 1254Arocior- 12 60

44884444618944

UU\]UPPU

FORM 1 PEST

VALIDATED

OLM03.0


Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

CLIENT SAMPLE NO.

/•W-SDA10-*.*'I H-Zi-*6>

Lab Code: IEA Case No.: 2240-016

Matrix: (soil/water) SOIL

Sample wt/vol: 30.1 (g/mL) G

% Moisture: 36 decanted: (Y/N) N


Concentrated Extract Volume: 5000(uL)

Injection Volume: 1.0(uL)

GPC Cleanup: (Y/N) Y pH: 7.0

CAS NO. COMPOUND

SDG No.: 12560


Lab File ID: P2010697_099.D


Date Extracted:12/04/96



Sulfur Cleanup: (Y/N) N

CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

11104-28-2 ATOClor-122111141-16-5 Aroclor-123253469-21-9 ATOClor-124212672-29-6 ATOClor-124811097-69-1 Aroclor-125411096-82-5 Aroclor-1260

ei3J,1005151515151

UUUUUU

J

FORM I PEST

3 008


CLIENT SAMPLE NO.








Injection Volume: l.O(uL)


-SDB7-CX5

SDG No.: 12560







Sulfur Cleanup: (Y/N) Y

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

1-11-2 Aroclor-101611104-28-2 Aroclor11141-16-5 Aroclor-]53469-21-9 Aroclor-]12672-29-6 Aroclor-1248~11097-69-1 ArocJ.or-1254"11096-82-5 Aroclor-1260"

310220

UUUU

PP

FORM I PESTVALIDATED

3/90

3 015


CLIENT SAMPLE NO.










CAS NO. COMPOUND

SDG No.: 12560









1 OCTA.I 1 _O______&^*w«l rw>_1 A1 C.

11104-28-2 ATOClor-122111141-16-5 Aroclor-123253469-21-9 Aroclor-124212672-29-6 Aroclor-124811097-69-1 Aroclor-125411096-82-5 Aroclor-1260

4C43

914545

730440280

UUU

P.

FORM I PESTVALIDATED


CLIENT SAMPLE NO



Matrix: (soil/water) SOIL»







SDG No.: 12560









11104-28-2—11141-16-5—53469-21-9—12672-29-6—11097-69-1—11096-82-5—

Aroclor-1221Aroclor-1232

— — Aroclor-1242Aroclor-1248Arocj.or-1254Arocior-1260

070540270270490440490

UUuPP

VAGDAltDFORM I PEST 3/90

032

10PESTICIDE ORGANICS ANALYSIS DATA-SHEET


CLIENT SAMPLE NO.

'-SDC5-XO









CAS NO. COMPOUND

SDG No.: 12560









11104-28-211141-16-553469-21-912672-29-611097-69-1—11096-82-5

ATOClor-1221Arocior-1232

— -Aroclor-1242— Aroclor-1248

Arocior-1254— -Aroclor-12 6 o

97O« / w550270270160010001000

UuuP

VAL1DAT!FORM I PEST

3 039



CLIENT SAMPLE NO.





Extraction: .(SepF/Cont/Sonc) SONC




CAS NO. COMPOUND

SDG No.: 12560







Sulfur Cleanup: (Y/N) Y


11104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

A_TwwX wf JL w «i» O— Aroclor-1221— Aroclor-1232—Aroclor-1242— Aroclor-1248— Arocior-1254— Aroclor-12 6 0

A"j(\n

96004700470011000630013000

UUUPPP

VALIDATEDFORM I PEST 3/90

3 048

10 • _PESTICIDE ORGANICS ANALYSIS DATA SHEET


CLIENT SAMPLE NO.





Extraction: .(SepF/Cont/Sonc) SONG




CAS NO. COMPOUND

SDG No.: 12560









11104-28-2—11141-16-5—53469-21-9—12672-29-6—11097-69-1—11096-82-5—

Aroclor-1221Arocior-1232Aroclor-124 2

— — Aroclor-1248ArocJLor-1254Aroclor-1260

QAy*1909494680940540

UUuP

J

VALIDATEDFORM I PEST 3/90

055



CLIENT SAMPLE NO.

>- SDT2fc) -/•*'





Extraction: .(SepF/Cont/Sonc) SONG




CAS NO. COMPOUND

SDG No.: 12560









1*5 C.1 A 1 1 _O__

11104-28-2 —11141-16-5 —53469-21-9 —12672-29-6 —11097-69-1 —11096-82-5 —

Aroclor-1221Aroclor-1232Arocior-1242Aroclor-1248Arocior-1254Aroclor-12 60

A O t\4oU97048048013001000720

UUU

P

FORM I PEST 3/90

064

.. IDPESTICIDE ORGANICS ANALYSIS DATA


CLIENT SAMPLE NO.

/9K>-SDT2&>)-/..T/

I tt-20-'tt>









CAS NO. COMPOUND

SDG No.: 12560


Lab File ID: P2010697J)98.I







11104-28-2 ATOClor-122111141-16-5 Aroclor-123253469-21-9 Aroclor- 124212672-29-6 Aroclor-124811097-69-1 Aroclor-125411096-82-5 Aroclor-1260

Kt9«1005252510310140

UUU

P

VALIDATEDFORM I PEST

3 07



CLIENT SAMPLE NO.



Sample wt/vol: 30.0 (g/mL) G*

% Moisture: 42 decanted: (Y/N) N•*.*.

Extraction: (SepF/Cont/Sonc) SONC-jConcentrated Extract Volume: SOOO(uL)



CAS NO. COMPOUND

SDG No.: 01189









1 O£*74_1 1 _•)__

11104-28-2—

53469-21-9 —12672-29-6—11097-69-1—11096-82-5 —

— — Aroclor-1221

Aroclor-1242Aroclor-1248

——Aroclor- 1254Arocior-1260

•

C7

120C7

575717084

U

UU

; i-

VALIDATED

FORM I PEST 3/90



CLIENT SAMPLE NO.

»l-:-I tt~3t-1i.

Lab code: IEA Case No.: 2240-017





__ Concentrated Extract Volume: 5000(uL)

. Injection Volume: 1.0(uL)

.,. GPC Cleanup: (Y/N) Y pH: 4.3

CAS NO. COMPOUND

SDG No.: 01189









1 *>£."! A ~ 1 1 _O______&Y->t<-O MV_I A1 £

11104-28-2 ATOClor-122111141-16-5 ATOClor-123253469-21-9 ATOClor-124212672-29-6 ATOClor-124811097-69-1 ATOClor-125411096-82-5 ATOClor-1260

t4-41

T- 218441414141

_ 41

UUUuuu

VALIDATED

FORM I PEST OLMO


CLIENT SAMPLE NO.


Lab Code: IEA -Case No.: 2240-018



% Moisture: 21 ./ decanted: (Y/N) N

^ Extraction: (SepF/Cont/Sonc) SONG

_ Concentrated Extract Volume: 5000(uL)


-* GPC Cleanup: (Y/N) Y pH: 6.5

- SDC5- I.S '-f 7

SDG No.: 01349




Date Extracted-.12/04/96





12674-11-2 -Aroclor-101611104-28-2 Aroclor-1221"11141-16-5 Aroclor-1232"53469-21-9 Aroclor-1242"12672-29-6 Aroclor-1248"11097-69-1 Aroclor-1254"11096-82-5 Aroclor-1260"

UT84

414141

UUUUUUU

VALIDATED

FORM I PEST 3/90



CLIENT SAMPLE NO.

fLab Code: IEA Case No.: 2240-018



t Moisture: 18 decanted: (Y/N) N

^ Extraction: (SepF/Cont/Sonc) SONC

... Concentrated Extract Volume: 5000 (uL)

- Injection Volume: l.O(uL)

-3 GPC Cleanup: (Y/N) Y pH: 7.6

CAS NO. COMPOUND

SDG NO.: 01349









11104-28-211141-16-553469-21-912672-29-611097-69-11109'6-82-5

"*^^J_i OCXO3.7 iU XOATOClOr-1221Aroclor-1232Aroclor-1242Aroclor-1248ATOClOr-1254Arocior-1260

**T" A.f\~f 4U814040404040

UUUUUU

VALIDATED• - ' —. !—<

FORM I PEST 3/ f



CLIENT SAMPLE NO.

fSDCll-l.*









SDG No.: 01349








CONCENTRATION UNITS:

. . . €>_.t

~*m

4

CAS NO.

11104-28-2

53469-21-9

COMPOUND (ug/L or ug/Kg) UG/KG Q

___&«-**** i /»-— i m £— — AiOCiOi XUiOAroclor-1221AiOCiOi ±£'34Aroclor-1242

_ _&v>««««1 «s*>_1 O AO— AT OC iOr— i « 4 o****^A-TOC JLWJt i* O^

AJLWWAWJb. «Lj£OU

U| 851 42t 42T 36T 20

U3~ 42

UUUuJu

VALIDATED

FORM I PEST 3/90



CLIENT SAMPLE NO.

/.U-SDD11-*.*'I //-2/-f*



„, Sample wt/vol: 30.0 (g/mL) G

_ % Moisture: 22 decanted: (Y/N) N

.-j Extraction: (SepF/Cont/Sonc) SONC

- Concentrated Extract Volume: 5000(uL)

- Injection Volume: 1.0(uL)

H GPC Cleanup: (Y/N) Y pH: 5.7

CAS NO. COMPOUND

SDG No.: 01349


Lab File ID: P1012597J)40.D







1 94C74.. 1 1 _O___

11104-28-211141-16-553469-21-91 O<;'73..OQ_<___

11097-69-111096-82-5

— AT oc JL or — i u i oAroclor-1221Aroclor-1232Aroclor-1242

___&v»#^*«l 4*^_1 A D— — ATOCJLOr— JL.24S— Aroclor-1254

Aroclor-1260

**T

11-L.TT

\JC5~

49H*

8642421 aID3842

UUU

TO•JcJU

VALIDATED

FORM I PEST 3/9C


CLIENT SAMPLE NO.

* Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

- Lab Code: IEA Case No.: 2240-011


~ Sample wt/vol: 30.1 (g/mL) G •


~ Extraction: (SepF/Cont/Sonc) SONG


- Injection Volume: l.O(uL)


SDC7-O.S

SDG No.: 11589







Sulfur Cleanup: (Y/N)- N


11104-28-21 1 1 A 1 — 1 £_R___

C 1 di af ft O 1 flD J*» Q57 -; J. 3712672-29-611097-69-111096-82-5

~~**Ai wCXOi* XUJLD

Aroclor-12 2 1— — — ArocjLor— u. j*

Aroclor-1248Aroclor-1254Aroclor-12 60

D1/120

C*7O /C "T3 /

-V^^ £5*fZO 4r€r&ste> 240

U

^ytoP3Tl>P3*1? P.

FORM I PEST 3/90



CLIENT SAMPLE NO.

SDC7DL

- Lab Code: IEA Case No.: 2240-011


— Sample wt/vol: 30.1 (g/mL) G

* Moisture: 42 decanted: (Y/N) N

~~ Extraction: (SepF/Cont/Sonc) SONC


""", Injection Volume: 1.0 (uL)


CAS NO. COMPOUND

SDG No.: 11589







Sulfur Cleanup: (Y/N> N


1 *>C*74_1 1 _O___

11104-28-2111 At _1 C_R___

53469-21-912672-29-611097-69-111096-82-5

— — — ATOCJLOr— iUJLOAroclor-1221

— — ATOCJLOr— JL« J*Aroclor-1242Aroclor-1248Arocior-1254Aroclor-12 60

e— A9 /U1200Kin9 /U

570400520310

U

UDJPDJPDJP

FORM I PEST \/ A \ \" 3/J



CLIENT SAMPLE NO

~ Lab Code: IEA Case No.: 2240-011







_ GPC Cleanup: (Y/N) Y pH: 7.0

CAS NO. COMPOUND

SDG No.: 11589


Lab File ID: P2121896__052.D







12674-11-2 Aroclor-101611104-28-2 Aroclor-1221"11141-16-5 Aroclor-1232"53469-21-9 ATOClor-1242"12672-29-6 Aroclor-1248"11097-69-1 Aroclor-1254"11096-82-5 Aroclor-12 60"

521005252180200100

UUUUPP

FORM I PEST

VALIDATED3/90


CLIENT SAMPLE NO.










SDG No.: 11589




Date Extracted .-12/03/96



Sulfur Cleanup: (Y/N).N


1 O£*7 A_1 1 _O___

11104-28-211141-16-553469-21-912672-29-611097-69-1*1 1 ft Q atT D *) ftAJLW3rO w «£ 3

— ATOCAOr— 1UJLOAroclor-1221Aroclor-12 3 2

— -Aroclor-1242Aroclor- 12 4 8Aroclor-1254

AQ«*O

984848

/t&&0 '1400si.s*** '1300

^ . . O O AT£*V v v v~

uuu

Jt>CP2> CP

,_ ^5i^ *

lu

FORM I PES.J


CLIENT SAMPLE NO.

J Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

— Lab Code: IEA Case No.: 2240-011



* Moisture: 32 decanted: (Y/N) N

"" Extraction: (SepF/Cont/Sonc) SONC•*«*

Concentrated Extract Volume: 5000(uL)] Injection Volume: 1.0(uL)

-,-'


SDT2CDL

SDG No.: 11589









11104-28-2

11097-69-111096-82-5

Aroclor-122 1— — — AiOCAOJt — x« J*

Aroclor-1254Aroclor-12 60

AOf\4oU980Ann•fOUAon1OU

i Q noJLOUU2000

960

U

^- r%Dt_UFCDP

DP

FORM I PEST 3/90

VALIDAit;


CLIENT SAMPLE NO.

' Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

-" Lab Code: IEA Case No.: 2240-012


~ Sample wt/vol: 30.1 (g/mL) G

*" % Moisture: 45 decanted: (Y/N) N

~* Extraction: (SepF/Cont/Sonc) SONG




SDA2-0.5

SDG No.: 11591









12674-11-2 Aroclor-1016111O4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

— Aroclor-1221— Aroclor-12 3 2— Aroclor-12 4 2— Aroclor-1248— Aroclor-12 54— Aroclor-12 60

6012060601007053

UUuuPPJ

J

VALIDATED

FORM I PES.T


CLIENT SAMPLE NO.

:j Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

— Lab Code: IEA Case No.: 2240-012


~ Sample wt/vol: 30.1 (g/mL) G •


""" Extraction: (SepF/Cont/Sonc) SONG•—» Concentrated Extract Volume: 5000(uL)

Injection Volume: 1.0(uL)f*


SDA5-0.5

SDG No.: 11591







Sulfur Cleanup: (Y/N> N


1 O«tTjl _1 1 •>

11104-28-21 1 1 A 1 _1 £_R___

53469-21-9- —12672-29-611097-69-111096-82-5

___H v»*s*«-1 **^*_1 fll C.— ATOCXOr— JLUlOAroclor-1221

___%*»-«>M-»l <^^-^T *> " •>— Arocxor— i2 j*Aroclor-12 4 2Aroclor-1248Aroclor-12 54

- — Aroclor-12 60

•7 *>/3150

*jt/ j73

160320270

U

U..JL

. .P,

VALIDATED

FORM I PEST 3/90



CLIENT SAMPLE NO.

SDA9-0.5



Sample wt/vol: - 30.1 (g/mL) G






SDG No.: 11591








CONCENTRATION UNITS:

-O•*

1

-• t

"•**

•1

UAS KU.

1 9£*74_1 1 _*)__

11104-28-2 —11141 _1 ct_R_

53469-21-9 —12672-29-6 —11097-69-1 —11096-82-5 —

tunfuuwu (ug/ii or ug>

____B\«>nsO / *-_1 m C

ATOClor-122 1

ATOClor-1242Arocior-1248Aroclor-1254ATOClor-1260

'fjqt uwr/J\(»

CQ39

120CO37

5957100210

U

U

UJP.P.

VALIDATED

FORM I PEST


CLIENT SAMPLE NO.

5 Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

" Lab Code: IEA Case No.: 2240-012



' % Moisture: 47 decanted: (Y/N) N





SDC11-0.5

SDG No.: 11591


Lab File ID: P1121296J)81.D







12674-11-2 Aroclor-101611104-28-2 Aroclor-1221"11141-16-5 Aroclor53469-21-9 Aroclor-]12672-29-6 Aroclor11097-69-1 Aroclor-1254"11096-82-5 Aroclor-12 60"

120

1300860360

1UUC

VALIDATED

FORM I PEST 3/90

IDPESTICIDE ORGANICS ANALYSIS DATA S£EET

; Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

CLIENT SAMPLE NO.

SDC7-0.5 T>u?









CAS NO. COMPOUND

SDG No.: 11591


Lab File ID: P1121296JJ96.D







1 9£*74_1 1 _1__111 A4_90_9___

11141-16-553469-21-912672-29-611097-69-111096-82-5

_ _&*»<**« i n*>_i ni a— — ATOCxOr— J.UJ.D___&^AI->1 /<V*-_1 991— ATOC JLOr— J.* * J.

Aroclor-12 3 2Aroclor-12 4 2Aroclor-1248

—Aroclor-1254—Aroclor-12 60

•« y \fQOA77W

490490

/5J/»o _66«015000

fWff^V ^TO^FW

Uu

j>cp^CP.J> CP



CLIENT SAMPLE NO.










SDC7-0.5DL

SDG No.: 11591









11104-28-2

12672-29-611097-69-111096-82-5

*"*"^*AJtwCJLOi JLUJLO

Aroclor-1221___>YT»r>l tir— 1 919

— AiOCiOi i*«t *Aroclor-12 4 8Aroclor-1254Aroclor-12 60

AQnnH J U U

9900AQnnA c*r\r\4SOU

150001500010000

U

CDPCDPCDP

VALIDATED

FORM I PEST 3/90


CLIENT SAMPLE NO.










SDT460-I.S

SDG No.: 11591









1-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

i-82-5

-Aroclor-1016-Aroclor-1221"-Aroclor-12 3 2"-Aroclor-12 4 2"-Aroclor-1248"-Aroclor-1254"

840410410

VALIDATED

FORM I PEST 3/9C


CLIENT SAMPLE NO.

j Lab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

~ Lab Code: IEA Case No.: 2240-012


~ Sample wt/vol: 30.0 (g/mL) G '

" % Moisture: 20 decanted: (Y/N) N

Extraction: (SepF/Cont/Sonc) SONG*-*W


Injection Volume: 1.0(uL)„>


SDT4DL

SDG No.: 11591









1 9£*74_1 1 _O___

11104-28-211141 _1 fi_R___

53469-21-91 9679_9Q_£___

11097-69-111096-82-5

___%>-n^O nv»_1 rtl cT— — — Arocxor— xuxoAroclor-1221

_•»•»!».¥• !-•*•* 1 i-k^--«1 ^O"""""•AiOCJLO-T^-L * -> -I

Arocior-1242___&V>/-|/^1 y"i>-— 1 *>AOAlt OCAOi — X&4O

Aroclor-1254Aroclor-12 60

A 1 f\f\4 XUU840041 Ort•• J.UU

4100i T> nrtnX & U U U

77004800

U

UC nuC DCD

_, i VALIDATED

FORM I PEST 3/90

Lab


Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

CLIENT SAMPLE NO.

Code: IEA Case No.: 2240-013


~3ample wt/vol: 30.0 (g/mL) G

> Moisture: 63 decanted: (Y/N) N



injection Volume: i.o(uL)

GPC Cleanup: (Y/N) Y

CAS NO.

pH: 7.0

COMPOUND

SDG No.: 11593









11104-28-211141-16-553469-21-912672-29-611097-69-111696-82-5

___fe«*j*\«O nv_1 A1 f.Arocxor— XUXDAroclor-1221Aroclor-1232Arocior-1242

— Aroclor-1248—Aroclor-1254—Aroclor-12 60

(to07180898989570240

UUUuP

VALIDATEDFORM I PEST 3/9<


CLIENT SAMPLE NO.

•JLab Name: INDUSTRIAL & ENVIRONMENTA Contract: SOW 1/91

—Lab Code: IEA Case No.: 2240-013


"-Sample wt/vol: 30.1 (g/mL) G

~% Moisture: 56 decanted: (Y/N) N


"concentrated Extract Volume: 5000(uL)

"injection Volume: 1.0(uL)


SDG No.: 11593


Lab File ID: P1121296__026.D







12674-11-2 Aroclor-101611104-28-2 Aroclor-1221"11141-16-5 ATOClor-1232"53469-21-9 Aroclor-124212672-29-6 Aroclor-1248~11097-69-1 ^Aroclor-1254"11096-82-5 Aroclor-12 60"

75150

7595

UUUUUP

VALIDATED

FORM I PEST 3/90



CLIENT SAMPLE NO







Injection Volume: l.O(uL)•


CAS NO. COMPOUND

SDG No.: 11595









1 9£*74_1 1 _9___

11104-28-211141 _1 C_R___

53469-21-912672-29-611097-69-111096-82-5

— — Arocxor —xuxo- — Aroclor-1221

ATOCXOlv X«J<>Aroclor-12 4 2Aroclor-1248

—Aroclor-1254Aroclor-1260

9X

100R13X51

>/j«-> 32003fro 2-iOOI7«»"O 1600

U

UC. P

C- o

FORM I PEST 3/90

VALIDATED



CLIENT SAMPLE NO.

SDT2DL









CAS NO. COMPOUND

SDG No.: 11595









11104-28-2

53469-21-912672-29-611097-69-111096-82-5

———Arocxor— xuxoAroclor-1221

___&v*n<->"l sw-_1 919— — — Aiocxor— J.* j«Aroclor-12 4 2Aroclor-1248Aroclor-1254Aroclor-1260

KinDJ.U

1000fil t\-JJ.\J

510430034001700

U

UDDD

FORM I PEST

VALIDATED

3/90

IDPESTICIDE ORGANICS ANALYSIS** DATA SHEET

UivEPA SAMPLE N

APD-SDC2-0.

Lab Name: IEA-CT Contract:

Lab Code: IEACT Case No. : 2581A SAS No. :


Sample wt/vol: 30 (g/ml) G

% Moisture: 54 decanted: (Y/N)N_


Concentrated Extract Volume .-5000 (uL)



SDG No.: A2581

Lab Sample ID: 962581A-01

Lab File ID: A1494CLP039




Dilution Factor: ^.Q

Sulfur Cleanup: (Y/N)N_

NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor- 1221Arocxor-1232Aroclor- 124 2Arocxor- 124 8Aroclor-1254Aroclor- 12 60

72140727249.99.63.

UtftJUJPPJP

VALIDATED

FORM I PEST3/90

Lab Name: IEA-CT


Contract:

026EPA SAMPLE NO

APD-SDD3-0.5

Lab Code: IE ACT Case No. : 2581A SAS No.


Sample wt/vol: 30 (a/ml) G



Concentrated Extract Volume;5OOP (uL)


GPC Cleanup: (Y/N)Y__ pH:6.6

SDG No.: A2581

.a CAS NO. COMPOUND






Dilution Factor: 1.0.



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor-1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Arocxor- 1260

57120575762.17087.

UUuuP

P


3/90

. Lab Name: IEA-CT

IDPESTICIDE ORGANICS ANALYSIS" DATA SHEET

Contract:

035EPA SAMPLE NO.

PAPD-S0C4-0.5

Lab Code: IE ACT Case No. : 2581A SAS No. :



* Moisture: .37 decanted: (Y/N)N_





SDG No.: A2581








NO. COMPOUND CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 10 16Aroclor-1221Aroclor-1232Arocxor-1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

52110525272.230130

UUUUP

P


3/90


EPA SAMPLE NO.

APD-SDB5-0.5


Lab Code: IEACT Case No.: 2581A SAS No. :


Sample wt/vol: 30 (Q/ml) G

% Moisture: £S decanted: (Y/N)N_





SDG No.: A2581

}CAS NO. COMPOUND







Sulfur Cleanup: (Y/N)N


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor-1016Aroclor-1221Aroclor- 1232Aroclor- 124 2Aroclor- 124 8Aroclor-1254Aroclor- 1260

100210100100250830430

UUUU

P


3/90

Lab Name: IEA-CT

*••,«*•'' ID ,,,.,-:.-^PESTICIDE ORGANICS ANALYSIS TOTA SHEET

Contract:

EPA SAMPLE NO

APD-SDC6-0.5




% Moisture: £g decanted: (Y/N)N_




GPC Cleanup: (Y/N)Y__ pH;5.9

SDG No.: A2581


Lab File ID: B5233CLP130




Dilution Factor: 5.0 .

Sulfur Cleanup: (Y/N)Y_

/CAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Arocxor-1242Arocior- 124 aAroclor-1254Aroclor- 12 6 6

220450220220190940760

UtfUuJP


3/90

Lab Name: IEA-CT


Contract:

SAS NO.:

' 063EPA SAMPLE NO.

APD-SDD7-0.5

Lab Code: IEACT Case No.:


Sample wt/vol: 30 (g/ml) G_






SDG No.: A2581

NO. COMPOUND


Lab File ID; A1494CLP079





Sulfur Cleanup: (Y/N)Y


12674-11-211104-28-211141-15-553469-21-912672-29-611097-69-111096-82-5

Aroclor-1016Aroclor-1221Aroclor- 12 3 2Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 12 60

16034016016078.320250

UUuuJP

•

VALIDATED

FORM I PEST3/90


" 07:EPA SAMPLE NO

APD-SDC8-0.5

— Lab Name: IEA-CT Contract:




% Moisture: 5J decanted: (Y/N)N_


Concentrated Extract Volume;5OOP (uL)


GPC Cleanup: (Y/N)Y__ pH;5.B

SDG No.: A2581


Lab File ID: BS233CLP157




Dilution Factor: 1PP. P


CAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Arocxor-1232Arocxor-1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

72001400072007200230003506615000

UUUU

PP

VALIDATED

FORM I PEST3/90


080EPA SAMPLE NO.

APD-SDB9-0.5

_ Lab Name: IEA-CT

Lab Code: IE ACT Case No.: 25811


Sample wt/vol: 30 (q/ml) G


Extraction: (SepF/font/Sonc) SONG




Contract:

SAS No.: SDG No.: A2581

CAS NO. COMPOUND









12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor-1016Aroclor-1221Arocxor-1232Aroclor- 124 2Aroclor- 1248Aroclor-1254Aroclor-1260

47PO96PO47004700210071004900

UUUUJ

P

\/VFORM I PEST

D

3/90

OttY

_ Lab Name: IEA-CT

ID ;,PESTICIDE ORGANICS ANALYSIS DATA SHEET

Contract:

EPA SAMPLE NO.

APD-SDC9-1.0

Lab Code: IEACT Case No.: 2581A SAS No.:








SDG No.: A2581

Lab Sample ID: 9625B1A-09





Dilution Factor: 1.0 •

Sulfur Cleanup: (Y/N)Y__

CAS NO. COMPOUND CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 10 16Arocxor-1221Aroclor- 1232Aroclor- 124 2Aroclor- 1248Aroclor-1254Aroclor- 1260

4183414121.49.23.

UUUuJP£JP

'O


3/90


096EPA SAMPLE NO.

APD-SDD9-0.5


Lab Code: IEACT Case No. : 25S1A SAS No. :



% Moisture: JL6 decanted: (Y/N)N_




GPC Cleanup: (Y/N)Y_ PH:5.8

SDG No.: A2581









12674-11-211104-28-211141-16-55^469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor -12 3 2Aroclor- 124 2Aroclor- 124 8Aroclor-1254Aroclor- 12 60

398039391.8

12.6.9

UUUuJPJPJP

V .Ti.il' i L~,

FORM I PEST3/90

— Lab Name: IEA-CT


Contract:

103EPA SAMPLE NC

-SDT1(B)-0.5

Lab Code : IEACT Case No . : 2581A SAS No . :



% Moisture: Tfi _ decanted: (Y/N)N_

(uL)

SDG No.: A2581

Extraction: (SepF/Cont/Sonc)

Concentrated Extract Volume: 50 OP


GPC Cleanup: (Y/N)Y__ oH;5.7

NO. COMPOUND






Dilution Factor: 20.0-



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Arocior- 124 2Aroclor- 124 8Arocior- 1254Arocxor-1260

2200450022002200180048003 00

UUuuJPP

VALID ATE!

FORM I PEST3/90

•* -* f\nO



Contract:

EPA SAMPLE NO.

-SDT1 (C) -0.5



Sample wt/vol: 30 (g/ml) G_

% Moisture: 1§ decanted: (Y/N)N_




GPC Cleanup: (Y/N)Y_ pH;5.8

SDG No.: A2581









12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Arocior- 1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

300P610030003000230093002800

UUuuJPPJ

VALIDATED

FORM I PEST3/90

«.. Lab Name: IEA-CT

-. . ID ,;-.PESTICIDE ORGANICS ANALYSIS DATA SHEET

Contract:

118EPA SAMPLE NO

-SDT1(D)-0.5





Extraction: (SepF/Cont/Sonc) S.ONC




SDG No.: A2581






Dilution Factor: 20.0-



12674-11-211104-26-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor-1016Aroclor-1221Aroclor -123 2Aroclor-1242Aroclor- 124 8Aroclor-1254Arocxor-1260

1200246o1200120051035001260

UUuuJPP

FORM I PEST

VALIDATED3/90

Lab Name: IEA-CT


Contract:

125EPA SAMPLE NO.

-SDT2(B)-0.5



Sample wt/vol: 30 (q/ml) G_






SDG NO.: A2581






Dilution Factor: 2P.O


-,_> CAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KQ

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1il09ol-82-5l

Aroclor- 1016Aroclor-1221Arocxor-1232Aroclor- 1242Arocior- 124 8Aroclor-1254Aroclor- 12 60

120P25001200120093034002900

UUUUJPP


3/90


13:?EPA SAMPLE NO

-SDT2(C}-0.5

Lab Name: TEA-CT Contract:

Lab Code: IEACT Case No.: 2581A SAS No.


Sample wt/vol: 30 (a/ml) G_



Concentrated Extract Volume;5OPO (uL)


GPC Cleanup: (Y/N)Y_ pH:6

SDG No.: A2581

CAS NO. COMPOUND


Lab File ID: B5233CLP11B




Dilution Factor: 1000-.0


CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocxor-l6l6Aroclor-1221Aroclor- 1232Aroclor- 124 2Arocxor-1248Aroclor-1254Aroexor-1260

8500017000085000850009900020000060000

Uuuu

JP

FORM I PEST

VALIDATED3/90

_ . Lab Name: IEA-CT


Contract:

139EPA SAMPLE NO.

-SDT2(D)-0.5

Lab Code: IEACT Case No. : 25B1A SAS No. :





Concentrated Extract Volume;50OP (uL)

Injection Volume: l.P (uL)

GPC Cleanup: (Y/N)Y__ pH;6.1

SDG No.: A2581






Dilution Factor: 20P/P



12674-11-211164-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1P16Arocior- 1221Aroclor-1232Aroclor- 124 2Aroclor -12 4 8Aroclor-1254Aroclor- 126P

16PPO340061600P1600P670P170005400

UUUUJP .

JP

VALIDATED

FORM I PEST3/90

73

Lab Name: IEA-CT

IDPESTICIDE ORGANICS ANALYSIS t*ATA SHEET

Contract:

146EPA SAMPLE NO.

-SDT3(B)-P.S



Sample wt/vol: 30 (q/ml) G



Concentrated Extract Volume;5POP (uL)



SDG No.: A2581








-WCAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 101 6Aroclor-1221Aroclor- 12 3 2Aroclor- 1242Aroclor -124 6Aroclor-1254Aroclor- 12 6 6

340007000034000340005400015000030600

UUuuP

JP

VALIDATE!

FORM I PEST3/90

Lab Name: IEA-CT


Contract:

153EPA SAMPLE NO.

-SDT3 (C) -1.0

Lab Code: IE ACT Case No. : 2581A SAS No. :


Sample wt/vol: 3J2 (g/ml) G_

V Moisture: 31 decanted: (Y/N)N_


Concentrated Extract Volume :5POP (uL)


G?C Cleanup: (Y/N)Y_ pH:6.5

SDG No.: A2581






Dilution Factor: l.O .



12674-11-2111P4-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

4897484880.10043.

UUUuP

JP

S I

FORM I PEST3/90

Lab Name: IEA-CT


Contract:

161EPA SAMPLE NO

-SDT3(D)-0.5




% Moisture: j»4 decanted: (Y/N)N_


Concentrated Extract Volume:50PP (uL)



SDG No.: A2581

NO. COMPOUND

Lab Sample ID: 962S81A-19





Dilution Factor: 50.P•


CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 124 2Aroclor- 124 8Aroclor-1254Aroclor- 1260

3600730036003600220070006500

UUUUJP

P


3/90

Lab Name: IEA-CT


Contract:

168EPA SAMPLE NO.

APD-SDB1-0.5



Sample wt/vol: 3P (g/ml) G






SDG No.: A2581

Lab Sample ID: 962581A-2P





Dilution Factor: l.O •


-i.- .'CAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 124 2Aroclor- 124 8Aroclor-1254Aroclor -12 60

9419094949415.41.

UUUUUJPJ


3/90

. ID - EPA SAMPLE SO.PESTICIDE ORGANICS ANALYSIS DATA SHEET I

flpfr-g.Ott.VERT OUTFALL-


Lab Code: IEACT Case No. : 2581B SAS No. :





Concentrated Extract Volume:5PPP (uL)



SDG No.: B2581

Lab Sample ID: 962581B-01

Lab File ID: A1494CLPP22







12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocior- 1016Aroclor-1221Aroclor- 1232Arocior- 1242Arocxor- 1248Aroclor-1254Aroclor- 1260

781607878510810760

UUuuPP


3/SO


u rOEPA SAMPLE NO.

ERT DOWN P. 5


Lab Code: IEACT Case No.: 2581B SAS No.:


Sample wt/vol: 30 (a/ml) G_

% Moisture: H decanted: (Y/N)N_





SDG No.: B2581

Lab Sample ID: 962581B-P2





Dilution Factor: l.P •



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Arocxor- 1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

4697484858.110120

UUUU

P

-o.S

FORM I PEST

VAL



Contract:

035EPA SAMPLE NO

ERT UP (DP. 5- o .X'




% Moisture: £7 decanted: (Y/N)N_





SDG No.: B2581






Dilution Factor: 1.0 :



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 123 2Aroclor- 1242Aroclor- 124 8Aroclor-1254Arocxor-1260

77160777729.43.27.

UUUUJPJPj£

VALIDATED

FORM I PEST3/9P

Lab Name: IEA-CT


Contract:

045EPA SAMPLE NO.

,9PD-SDC1P-0.5

Lab Code: IEACT Case No. : 2581B SAS No,








SDG No.: B2581

' CAS NO. COMPOUND


Lab File ID: A1494CLPP65




Dilution Factor: 2.P ..



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocior- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor-1248Arocxor- 1254Arocxor- 12 60

891808989170360170

UUUUPPP

VAT! DATEDFORM I PEST

3/90

_ Lab Name: IEA-CT


Contract:

053EPA SAMPLE NO

g>!>-SDT4(B)-P.5




% Moisture: 23 decanted: {Y/N)£_

Extraction: (SepF/Cont/Sonc) SQNC

Concentrated Extract Volume;50PO (uL)



SDG No.: B2581








NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-21 11104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 1248Aroclor-1254Aroclor- 12 60

4387434313.80.61.

UUUUJPPP

VALIDATED

FORM I PEST3/90


EPA SAMPLE NO.

*'O-SDT4 (C) -1.P


Lab Code: IE ACT Case No.: 2581B SAS No.:




Extraction: {SepF/Cont/Sonc) SONC




SDG No.: B2581

Lab Sample ID: 9625B1B-P6





Dilution Factor: SP'P.P



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Arocxor- 1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 1260

32000640PP3200032000100PP3100P19000

UUUUJJ?JPJ

VALIDATED

FORM I PEST3/9P

Lab Name: IEA-CT


Contract:

059EPA SAMPLE NO.

/»^>-SDT4(D}-0.5



Sample wt/vol: 3P (a/ml) G

* Moisture: 17 decanted: (Y/N)N_


Concentrated Extract Volume:SOPP (uL)

Injection Volume: 1-P (uL)


SDG No.: B2581

Lab Sample ID: 9625B1B-07








12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 1248Aroclor-1254Aroclor- 1260

80160808022.520200

UUuuJP

VALIDATED

FORM I PEST3/9P

••1


073EPA SAMPLE NO.

ERT UP(2)P.5

o Lab Name: IEA-CT Contract:




% Moisture: 65. decanted: (Y/N)N_


Concentrated Extract Volume:5POP (uL)


G?C Cleanup: (Y/N)Y_ PH:6.8

SDG No.: B2561






Dilution Factor: l.O •


-;--' CAS NO. COMPOUND CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocior-1016Arocxor- 1221Aroclor- 1232Aroclor -1242Arocxor- 124 8Aroclor-1254Arocxor-1260

941909494110140110

UUUU

P

VALIDATED

FORM I PEST3/90

- IDPESTICIDE ORGANJCS ANALYSIS DATA SHEET

0013EPA SAMPLE N

APD-SDB6-0.

— " • Lab Name: IEA-CT Contract:



Sample wt/vol: 3JJ (g/ml) G_






SDG No.: A2645

Lab Sample ID: 962645A-OS



Date Extracted: 12/P3/96


Dilution Factor: 5.P •



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocior- 1016Aroclor-1221Aroclor-1232Arocior- 1242Aroclor- 1248Aroclor-1254Aroclor- 1260

11'j

230460230230160370146

UUuuJ

•* •-

J

VALID A s ED

FORM I PEST3/9P


0022EPA SAMPLE NO.

ftp P-SDT1 (B) -1.P

— Lab Name: ISA-CT Contract:






Concentrated Extract Volume:500P (uL)


GPC Cleanup: (Y/N)Y__ pH:6

SDG NO.: A2645

CAS NO. COMPOUND






Dilution Factor: 1.0 '



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Arocior-i016Aroclor-1221Aroclor- 1232Aroclor- 1242Arocxor-1248Aroclor-1254Aroclor-1260

43874343

. 18.35.16.

UUUUJPJJ

S-/

FORM I PEST3/9P

- Lab Name: IEA-CT


Contract:

0030EPA SAMPLE NO.

**ElSDT2(A)-1.P





SONG

(uL)

SDG No.: A2645

Extraction: (SepF/Cont/Sonc)

Concentrated Extract Volume;5PPO

Injection Volume: J..P (uL)


CAS NO. COMPOUND





Date Analyzed: P1/P3/97

Dilution Factor: 3..P



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Aroclor-1221Aroclor -12 3 2Arocxor-1242Aroclor- 124 8Aroclor-1254Arocxor-1260

428642425.0

10.7.2

UUUUJJJ

VALI

FORM I PEST3/9P

0038ID

Lab Name: IEA-CT

PESTICIDE ORGANICS ANALYSIS DATA SHEET

Contract:

EPA SAMPLE NO,

> -SDT3 (E) -0.5- 2V-



Sample wt/vol: 3P (a/ml) G_



Concentrated Extract Volume:50PO (uL)



SDG No.: A2645






Dilution Factor: 5..0


f \CAS NO. COMPOUND CONCENTRATION UNITS: Q

(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

i 11096-82-5

Aroclor- 101 6Aroclor-1221Aroclor- 123 2Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 12 60

32066P32032032P32P4PO

UUUUU

V A I

FORM I PEST3/9P

004n

Lab Name: IEA-CT


Contract:

SAS No.:

EPA SAMPLE NO.

-SDT1(D)-1.0

Lab Code: IEACT Case No.: 264



% Moisture: 25 decanted: (Y/N)N__*-'*.


Concentrated Extract Volume:5P00 {uD

Injection Volume: 1.P (uL)

SDG No.: A2645

OGPC Cleanup: (Y/N)Y_ pH:6.3

CAS NO. COMPOUND






Dilution Factor: 2.P



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-11096-82-5

Aroclor-1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Arocior- 1260

8818088888816038.

UUuuuJP

VALIDATED

FORM I PEST3/9P


0052EPA SAMPLE NO.

>-SDT3(A) -1.5

- Lab Name: IEA-CT Contract:

Lab Code: IEACT Case No.:


JS45A SAS No.: SDG No.: A2645


Sample wt/vol: 30 (a/ml) G__




Injection Volume: 1.0 . (uL)

GPC Cleanup: (Y/N)Y_ pH:6

CAS NO. COMPOUND

Lab File ID:. B5234CLP279







12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

,1 11096-82-5

Arocxor-lOieAroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 12 60

8116081818111022.

UUUUUPJP

VALIDATED

FORM I PEST3/9P

0013ID

PESTICIDE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO.

flPD-SDB10-P.5


- Lab Code: IEACT Case No.: 265PA SAS No.:

•' Matrix: (soil/water) :SOIL

• Sample wt/vol: 30 (a/ml) G

* % Moisture: 12 decanted: (Y/N)N__

~" Extraction: (SepF/Cont/Sonc) SONG



Cleanup: (Y/N) Y_ pH:5.6

SDG No.: A265P









12674-11-211104-28-211141-16-553469-21-912672-29-6

. 11097-69-1|f 11096-82-5

Aroclor-1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Arocior- 12 60

310630310310230670300

uuuuJ

JP

VALIDATED

FORM I PEST3/9P


0020EPA SAMPLE NO.

APD-SDA5-1.5


Lab Code: IEACT Case No.: 2650A .SAS No.:





Concentrated Extract Volume:5POP (uL)


Cleanup: (Y/N)Y_ pH;6.1

SDG No.: A2650

Lab Sample ID: 96265PA-P5








12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

P 11096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Aroclor-1254Aroclor- 12 60

428542424.22.842

UUUuJPJPu


3/90

'.-4

Lab Name: IEA-CT


Contract:

0027.EPA SAMPLE NO.

APD-SDB4-P.5

Lab Code: IEACT Case No. : 265PA SAS No. :


_^ Sample wt/vol: 30 (a/ml) G

J % Moisture: £2 decanted: (Y/N)1L.

_, Extraction: (SepF/Cont/Sonc) SONG

« Concentrated Extract Volume;5OOP (uL)

-n Injection Volume: 1.0 (uL)

SDG No. : A2650

/*>*,GPC Cleanup: (Y/N)Y_ pH:j

CAS NO. COMPOUND

Lab Sample ID: 962650A-P7





Dilution Factor: 1.0 _

Sulfur Cleanup: (Y/N)li_

CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KQ

i

4•W

1

12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

i 11096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 124 8Arocior- 1254Arocior- 1266

8918089

i

89(B.54.14.

UUUUJJJP

VALIDATED

FORM I PEST3/90


0035EPA SAMPLE NO.

HPD-SDB10-1.0


- Lab Code: IEACT Case No.: 265PA SAS No. :

*J Matrix: (soil/water) :SOIL

- Sample wt/vol; 3P fa/ml) G_

** % Moisture: 2£ _ decanted: (Y/N)N_

•"! Extraction: { SepF/Cont/Sonc) SONG

~* Concentrated Extract Volume :5PPP (uL)



SDG No.: A265P

/~>-

Lab Sample ID: 96265PA-12

Lab File ID: B5239CLPP56




Dilution Factor: i.p



12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1P16Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor-1248Aroclor-1254Arocxor-1260

4490444436.90.54.

UUUUJ

P

VALIDATE!

FORM I PEST3/90

0044ID

PESTICIDE ORGANICS ANALYSIS DATA SHEETEPA SAMPLE NO.

APD-SDB8-P.5


Lab Code: IEACT Case No.: 265PA SAS No.:


Sample wt/vol: 3P (a/ml) G_


Extraction: (SepF/Cont/Sonc) SQNC



GPC Cleanup: (Y/N-)Y_ pH;5.7

SDG No.: A265P







Sulfur Cleanup: {Y/N)N_


12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-1

|i 11096-82-5

Aroclor- 1016Aroclor-1221Aroclor- 1232Aroclor- 1242Aroclor- 1248Aroclor-1254Aroclor-1260

97200979779.25083.

UUUUJ

J


3/90


0052EPA SAMPLE NO.

fit'/j-SDTl (C) -1.0





* Moisture: 22 decanted: (Y/N)N_


Concentrated Extract Volume:5P00 (uL)


GPC Cleanup: (Y/N)Y__ pH:6.2

SDG No.: A265P

CAS NO. COMPOUND









12674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

Aroclor- 1016Arocxor- 1221Aroclor- 1232Aroclor- 1242Aroclor- 1248Aroclor-1254Aroclor- 1260

8517P858512P25P91.

UUUuP

P


3/90


PLE NO,

»/>j>-SDT3(A)-l.P









Cleanup: (Y/N) Y_ pH:5.9

COMPOUND

SDG No.: A265P

Lab Sample ID: 96265PA-18







CAS NO. CONCENTRATION UNITS: Q(ug/L or ug/Kg) UG/KG

12674-11-211104-28-211141-16-553469-21-912672-29-6

( 11097-69-1li.096-82-5

Arocior- 1016Aroclor-1221Arocxor- 123 2Arocxor- 124 2Arocxor- 1248Arocior -1254Arocxor- 1260

4184414114.52.14.

UU0UJP

JP

VALIDATED

FORM I PEST3/9P

A2

MERCURY ANALYTICAL RESULTS

U.S. EPA - CLP

INORGANIC ANALYSES DATA SHEET

_db Name: ISA

Lab Code: IEA Case No.: 2581

Matrix (soil/water): SOIL

Level (low/roed): LOW

V Solids: 46.3

Contract:

SAS No.:

54C

EPA SAMPLE NO.

APD-CULVERT 010*$'

SDG No.: B25B1



Concentration Units (ug/L or tog/kg dry weight) : Mg/Kg

Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNidcelPotassiumseleniumSilversooiuraTnalliumvanadium£inccyanide

Concentration

U3" 0.16•

C

u

Q

N

M

MRMkMRMkMRMRMRMRMRMRMRMRMRMRcvJR1RJRIR9RJRJRJR4k

Clarity Before: OPAQUE

Clarity After: OPAQUE

Texture:

Artifacts

FORM I - INVALIDATED

ILM03. (

U.S. EPA - CLP


uab Name: IEA

Lab Code: ISA Case No.: 2581

Contract:

SAS No.:

541

EPA SAMPLE NO.

APD-CULVERT DOW

SDG No.: B2581


Level (low/med): LOW

% Solids: £7

Lab Sample ID: 9625B1B-02


Concentration Units (ug/L or mg/kg dry weight): Mg/Kg

Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperIronLeadMagnesiumManganeseMercuryNidceipotassiumseleniumSilversodiumThalliumVanadiumZinccyanide

Concentration

err 0.11

C

U

Q

•N

M

JkJkMkMkMkMkMkJkMkMkMkMkMkMkL'VMRMRMkMRMRMRMRMRMR



Texture:

Artifacts;


ILM03.0

Name: IEA_

Lab Code: IEA

U.S. EPA - CLP

INORGANIC ANALYSES DAT SHEET

Contract:

SAS No.:Case No.: 2581

54:EPA SAMPLE NO.

APD-CULVERT UP,fltS* //-2C-f^

SDG NO.: B2581



% Solids: 51.3

Lab Sample ID: 962SB1B-03


Concentration Units (ug/L or mg/kg dry weight) : Mg/Kg

CAS No.

7429-90-57440-36-07440-38-27440-39-3

Analyte

AluminumAntimonyArsenicBarium

Concentration

744O-41-77440-43 97440-70-27440-47-37440-48-47440-50-8

T=6~

caxciumChcobaltcopperiron

7439-96-5-y/-p

7440-OZ-C7440-09-77782-49-27440-22 47440-23-5

NicJceiircury

potassiumseleniumsilversodium

Ilium

7440-66-657-12-5 cyanide

u j

Color Before:

Color After:

Comments:

Clarity Before: OPAOUB

Clarity After:

SR

Texture:

Artifacts:

VALIDATE!FORM I - IN ILM03.0

«ctb Name: ISA




* Solids: 37.8

U.S. EPA - CLP

1INORGANIC ANALYSES DATA SHEET

Contract:

SAS NO.: .

547

EPA SAMPLE NO.

APD-CULVERT UP

SDG No.: B2581




Color Before:

Color After:

Comments;

CAS NO.

7429-90-574< 0-36-074< 0-38 -274< 0-39-3744C -41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97 -67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

Aluminum1AntimonyArsenicBariumBerylliumCaamiumCalciumciwonuumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilversodiumThalliumV&nadiumZincCyanide

Concentration

UT 0 . 19

C

U

Q

N

M

4kJkJkJkJkJkNkJkMkJkMkMkMkMRL'VMRMRMkMkMRMRMRMRMk



Texture:

Artifacts:

VALIDATEDFORM I - IN ILM03.0

U.S. EPA - CLP

INORGANIC ANALYSES DATASHEET

689EPA SAMPLE NO.

juab Name: IEA


Matrix (soil/water) : SjQIL_


% Solids: 21.1

Contract:

SAS No.:

APD-SDBI-0.5

SDG NO.: A2581




/*•>,

Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-3

Analyte


Concentration

7440-41-7*1 Beryllium I7440-43-57440-70-27440-47-37440-48-47*40-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-777B2-49-27440-22-4744O-23-57440-28-07440-62-27440-66-657-12-5

~T*iKPlTl7PcaxciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelpotassiumseleniumSilversodiumThalliumvanacL.umZinccyanide

0.43

C

U

Q M

JkJkMRMkJR&9±m&*&a±m&mIRIRIR2VIRJRmMRHRfitffRMRNR



Texture:

Artifacts:


U.S. EPA - CLP


673

EPA SAMPLE NO.

Name: IEA


Contract:

SAS No.:

APD-SDB5-0.5

SDG No.: A2581


Level (low/tned) : LQW

% Solids: 36.6




Color Before:

Color After:

Comments:

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-J50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumCalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilversodiumTnaiiiumvanadiumZincCyanide

Concentration

0.28*

C Q M

JkslkJkJkJkJkJkJkJRJkJRJRJRJRJVJRJRJRJRJRJRBTJRJR



Texture:

Artifacts:


U.S. EPA - CLP


677EPA SAMPLE NO.

Lab Name: IEA




% Solids: 69.2

Contract:

SAS No.:

APD-SDB9-0.5

SDG NO.: A2581

Lab Sample ID: 962581A-Q8



:>

/

Color Before:

Color After:

Comments :

CAS No.

7429-90-57444-36-07441-J8-27440- j 9-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1

Analyte


Concentration

CaSOiuincalciumcmroiHiuiftcobaltcopperironLeaa

£-W:E*I:«MM:»-t,fcM;T--MJi7439-97-67440-02-07440-09-77782-49-27446-22-47440-23-57440-«o 07440-62-27446-6 -657-12-5

MercuryNickelpotassiumseleniumSilversodiumTtxaiiiumvanacxLumzinccyanioe

Clarit

Clarit

0.28

C

4

Q

]

M

IRMRJRIRJR.JR&•'±m

H HMRP&pvHRfmMRJRIRIRJRJRJk

y Before: OPAQUE Texture:

y After: 3&&QQE. ArtifactS:

FORM I - IN

VALIDATEDILM03.0

U.S. EPA - CLP


670

EPA SAMPLE NO.

db Name: ISA




% Solids: 40.8

Contract:

SAS No.:

APD-SDC2-0.5H-1o~4 t,

SDG No.: A2581




Color Before:

Color After:

Comments;

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-0

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickel

Concent rat ion

0.24

Hr£ t V Q ' K° DT fl P *i " -" ' r * * ' ' " ti *" fg^fm^^^gmj^f7782-49-27440-22-47440-23-57440-28-07440-6--*7440-66-657-12-5

seleniumSilversodiumThalliumvanadiumZincCyanide

C

U

Q ' M

JRJkJRffRfURfroffRNRNREfttHRMRRRK1cvMRMRMRMRMRMRJRMRNRI



Texture:

Artifacts:


Lab Name: IEA

U.S. EPA - CLP


_ Lab Code: ISA Case No.: 2581

. Matrix (soil/water): SOIL

- Level (low/med) : LOW

•"• % Solids: 59.4

Contract:

SAS No.:

672EPA SAMPLE NO.

APD-SJ0C4-0.5

SDG No. : A2581




Color Before:

Color After:

Comments:

CAS No.

7429-90-5744O-36-07440-38-?744O-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-6

7435-95-47439-96-5

Analyte

AlviminwAntimonyArsenicBarium

Concentration

LumcalciumChromiumcobaltcopperironLeaaMagnesiumManganese

0.17

7440-09-77782-49-27440-22-4744O-23-57440-28 1)7440-62-27440-66-b57-12T-5

gptassiumseleniumSilverSodiumThalliumvanadiumZinccyanide

u



TO

Texture:

Artifacts:


.udb Name: IEA

Lab Code: IEA

U.S. EPA - CLP


Contract:

SAS No.:

674EPA SAMPLE NO.

APD-SDC6-0.5

Case No.: 2581 SDG No.: A2581

_ Matrix (soil/water): SOIL

-, Level (low/med) : LOW

~ % Solids: 77.9




Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AlunnnuffiAntimonyArsenicBariumBerylliumCadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelpotassiumseleniumSilversodiumThalliumVanarll urnZinccyanide

Concentration

0.12

C

U

Q M

JRJkJk*JkJkJkJkJkMkMkMkMRMRMRl!VMRMRMRMRMRMRMRMkMR



Texture:

Artifacts:

FORM I - INVALIDATE

ILM03.0

Name: IEA

Lab Code: IEA

U.S. EPA - CLP•.•* »" '•*•

''*. V -


Contract: .

SAS NO.:Case No.: 2581

676

EPA SAMPLE NO.

APD-SDC8-0.5

SDG NO.: A2581



% Solids: 74.3




CAS No.

7429-90-5

7441

Analyte

AntimonyArsenicBarium

7440-43-97440-70-2

Beryllium

calcium744O-47-3•t ll'BVB •

Chromium

iron

7439-95-T7439-96-57439-97-6

LeadMagnesiumManganeseMercury

7782-49-27440-22-47440-23-S

porassiumseleniumSilversooiunmaxxium

7440-66 657-12-5

ZincCyanide

Concentration

Color Before:

Color After:

Comments:

O.bO

Clarity Before: QEAOJQE

Clarity After:

M

BiKEIRTOTO

Texture:

Artifacts:


U.S. EPA - CLP


678EPA SAMPLE NO

Name: IEA


Contract:

SAS No.:

APD-SDC9-1.0

SDG No.: A2581

— Matrix (soil/water): SOIL

_ Level (low/med): I£W

>- % Solids: 79.9

Lab Sample ID: 9625S1A-09



Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-j 9-37440-41-77440-43-97440-70-27440-47-37440-48-47440-5O-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumrl»rtmil ttmcaxciumfip»'"om' umcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilversooiumThalliumvanadiumZinccyanide

Concentration

0 .12

C

U

Q M

MkMkMkMkMkMRMRMRMkMkMRMRMkMRcvMRMRMRMRMRMRMRMRMR



Texture:

Artifacts;


~ctb Name: IEA

Lab Code: IEA

U.S. EPA - CLP


Contract:

SAS No.:

EPA SAMPLE NO.

APD-SDCIO-0.5t,

Case No.: 2581 SDG No.: B2581



^ % Solids: 79.5




Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36MJ7440-38-274*0-39-3

Analyte

AntimonyArsenic

7440-41-77440-43-9440-70-27440-47-J7440-48-47440-50-87439-89-67439-92-17439-95-4^7439 96- 57439-97-b7440-02-07440-09-77782-49-27440-22-47440-23-5T7440-28-0

0-62-27447440-66-657-12-5

Barium

Lum

Concentration

calciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelpotassiumSeleniumSilverSoaiUmThallium

ZincCyanide

M

TOTO

TO

N

EOTSOT


Clarity After: OPAQUETexture:

Artifacts:

FORM I - IN ILM03 .0

U.S. EPA - CLP


671

EPA SAMPLE NO.

ab Name: IEA


Contract:

SAS No.:

APD-SDD3-0.5

SDG No. : A2581

Matrix (soil/water): SOIL.


% Solids: 51.9




Color Before:

Color After:

Comments:

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBanumBerylliumCatimiyiBcalciumcairofsiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilversodiumThalliumvanadiumZincCyanide

Concentration

0 .17

C

U

Q M

JkJkJkJRJkJkJkIRJRJkJRIRMRIRivIRIRMRMRMkJkMkMRMR



Texture:

Artifacts:


ILM03.0

Name: IEA

b/t)U.S. EPA - CLP

•*-.-;%. i • • <INORGANIC ANALYSES DA1 SHEET

EPA SAMPLE NO.




% Solids: 63.4

Contract:

SAS No. :

APD-SDD7-0.5

SDG No.: A2581




Color Before:

Color After:

Comments:

Concentration

0.11

M

SIRTOTO

TO

TO

TOT

TO

TO

SOTTO

EJRTOTOTO

Clarity Before:

Clarity After: OPAQUB

Texture:

Artifacts:


ILM03.0

xjab Name: IEA

Lab Code: IEA

U.S. EPA - CLP


Contract:

SAS NO.:

679

EPA SAMPLE NO.

APD-SDD9-0.5

Case No.: 2581 SDG NO. : A2581



% Solids: 81.4

Lab Sample ID: 9625B1A-10


Concentration Units (ug/L or rag/kg dry weight): Mg/Kg

Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-i;7440-39-:7440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-174: 9-95-47439-96-57439-97-67440-02-0

Analyte

Aluminum1AntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickel

Concentration

0.10

7440-09-7 I Potassium I7782-43-27440-22-47440-23-57440-28-07440-6.-27440-66-657-12-5

seleniumSilversodiumThalliumVanadiumZinccyanide

C

U

Q M

JkiJkJkTOJkJkJkJkJkJRJRMRMkMRL'VMRMRMkMRMRMkMkMRMR


Clarity After;

Texture:

Artifacts:


Name: IEA


.., Matrix (soil/water): SOIL

, Level (low/med): LOW

« V Solids: 47.3

U.S. EPA - CLP


Contract:

SAS No.:

680EPA SAMPLE NO.

APD-SDTI(B)-0.

SDG NO.: A2581




Color Before:

Color After:

Comments:

CAS NO

7429-90-57440-36-07440-38-27440-39-3

0-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-4^7439-96-57439-97-67440-02-0

Analyte


Concentration

calciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickel

0.4

7440-22-47440-23-57449-28-07440-62-2744O-66-657-12-5

silversodiumThalliumvanadiumZinccyanide

M

IR


Clarity After: QSWQB.

Texture;

Artifacts:


U.S. EPA - CLP


Name: IEA



Level (low/med): LQW

% Solids: 53.4

Contract:

SAS No.:

681

EPA SAMPLE NO.

APD-SDTI(C)-0./'-3Q-91,

SDG NO.: A2581



Concentration Units (ug/L or mg/kg dry weight) .- Mg/Kg

Color Before:

Color After:

Comments:

CAS NO.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelpotassiumseleniumSilversodiumThalliumVan fliumzinccyanide

Concentration

1.4»

C Q M

MkMkMkMkJkMRMkMkMRJRMkMRMRMRcvIRTOJRMRJRJRJRJRJR



Texture:

Artifacts


ILM03.0

Lab Name: IEA

Lab Code: IEA


Contrac&M

Case NO. : 2581 SAS No. :

682

EPA SAMPLE NO.

APD-SDTI (D)-0.

SDG NO. : A2581


Level (low/med): LOW.

% Solids: 40.4



-W

W


Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-8

Analyte


Concentration

caxciumiwn

cooaxtcopper7439-92 -1

7439-97-6

39-95-439-96-5

7440-09-740-Oi -0

82-49-240-22-4

7440-23-5

MagnesiumManganeseMercuryNickel

siumseleniumsilversodium

7440-66-657-12-5

Zinccyanide

2.6

M

Clarity Before: OPAQOR


Texture:

Artifacts:

VALIDATEFORM I - IN ILM03.0

U.S. EPA - CLP


683EPA SAMPLE NO.

i»ab Name: IEA


Contract:

SAS No.:

APD-SDT2(B)-0.

SDG No.: A2581

Matrix (soil/water) : SOIL

Level (low/tned) : LOW

% Solids: 52.9




'.-4 ••:

Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-3744O-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumsilversodiumThalliumvanadiumZinccyanide

Concentration

0.15

C

u

Q M

JRIRJRJkJkJkJRMRJRJRJRMRMkMRl!VMRMRMRMRIRMRMRMRIR



Texture:

Artifacts:


U.S. EPA -* CLP


684

EPA SAMPLE NO.

uab Name: IEA

Lab Code; IEA Case No.: 2581


- Level (low/med): LOW

- % Solids: 35.4

Contract

SAS No.:

APD-SDT2(C)-0.

SDG NO. : A2581




Color Before:

Color After:

Comments:

CAS No.

7429-90-5744O-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-3744O-48-4744O-5O-87439-89-67439-92-17439-95-47439-96-57439-97-6744(1-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte


Concentration

calciumChromiumcobaltTSopperironLeadMagnesiumManganeseMercuryNicxexpotassiumsexen: umSilversodiumT&aJLiiumvanadiumZinccyanide

6.1

M

v



Texture:

Artifacts:


\jab Name: IEA




% Solids: 43.4

U.S. EPA - CLP


Contract:

SAS No.:

685EPA SAMPLE NO.

APD-SDT2(D)-0.

SDG No.: A2581




Color Before:

Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumCalciumchromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumsexAn<iiimSilversodiumThalliumvanadiumZinccyanide

Concentration

1.6

C Q M

JRJkTOJkJkJkJkJkMR.MkMRMRMkMRcvMkMRMRMRMRMRMRMkMR



Texture:

Artifacts.-


uis1: EPA)-.CLP


Name: IEA

Lab Code: IRA Case No.: 2581

Matrix (soil/water): SOIL-


% Solids: 42.8

SAS No.:

686EPA SAMPLE NO.

APD-SDT3(B)-0.

SDG NO. : A2581




Color Before:

Color After:

Comments:

Concentration

7782-49-2

7440-23-50-ii2-4

/44U7440-62-27440-66-657-12-5

1.2

seleniumSilversodiumvanadiumZinccyanide

M

TOTOIK

IRIRIRIR

TO

TOTOIR

TO

TO

TOTOTO


Clarity After: OJ>A£QB

Texture:

Artifacts:


U.S. EPA - CLP

INORGANIC ANALYSES DATA SHEETEPA SAMPLE NO.

Lab Name: IEA



Level (low/med): LQH

* Solids: 70.7

Contract:

SAS No.:

APD-SDT3(C)-1.

SDG No.: A2581




Color Before:

Color After:

Comments:

CAS NO.

7429-90-57440-36-07440-38-27440-39-3744O-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-7 -07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilversodiumThalliumVanadiumZinccyanide

Concentration

0.13

-

C

U

Q M

JRMRJRMkMkMkMRMRMkMkMRMRMRMRcvMRMRMRMRMRIRMRMRMR



Texture:

Artifacts:

FORM I - IN VALIDATED ILM03.0

i.ab Name: IEA




% Solids: 30.8

U.S. EPA - CLP

* 1 *$*'


__, Contract:

SAS No.*f '

688

EPA SAMPLE NO.

APD-SDT3(D)-0.

SDG No.: A25B1




-J

-^-O''

.W

v

•-•-* ."""*.

•1

• Color Before:

-; Color After:

Comments :

CAS No. Analyte

7429-917441744<

3-31

Concentration'g-~m >;* rrrnt rrrrnr^ ^^^^^^^^^^^5-0 | AJitimony

3-38-2 i Arsenic7440-39-3 i Barium7440-41-7 1 Beryllium 1TTOfo^TCPS7440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-4744Or23-57440-28-07440-62-27446-66-657-12-5

fm^tai'caxc:cnroicobaJ

umLumliumLt

copperironLead •Magnesium IManganese

"H!M:

srcury.ckei

PotassiumseleniumsilversodiumThanavanaa

Lum.um

Zinccyanide

Clarit

Clarit

2.5

C

y Before: OPAQUE

y After: QPA.QUS

Q M

••••• inM ^^^^^H

g^^^ |NRMRIR

MRIR

MRIKI

t

MRMRMR

;•MkMRMRNR

Texture :

Artifacts :

— "


U.S. EPA - CLP


~ -ab Name: IEA

Lab Code: IEA Case No.; 2581



% Solids: 69.3

Contract:

SAS No.:

544EPA SAMPLE NO.

APD-SDT4(B)-0.//-•?*?-•* L

SDG No. : B2581




•-,- Color Before:

— Color After:

Comments:

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBariumBerylliumcadmiumcalciumChromiumcobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumseleniumSilverSodiumThalliumvanadiumzincCyanide

Concentration

UT 0 . 19

C

U

Q

' N

M

JkJkJkJkJkJRJkJkJkJkIRIRMRMRcvMRMRMRMRMRMRMRMRMR



Texture: .

Artifacts:


ILM03.0

- -ab Name: IEA

U.Sf EPA- - CLP


545

EPA SAMPLE NO.

Lab Code: ISA Case"No.: 2581



% Solids: 66.3

Contract:

SAS

APD-SDT4(C)-1.

SDG No.: B2581




CAS No.

7429"9q-5744O-36-0 Antimony

Analyte

Aluminum

Arsenic

Concentration M

TO

SIRTO

TOT

TOTOTO

TOSIR

TOTO

TOSIRSIRTOTO

Color Before:

-. Color After:

Comments:

Clarity Before: OPAQUB


Texture:

Artifacts:

FORM I - IN VALIDATEDILM03.0

U.S. EPA - CLP


«ab Name: IEA


Contract;

SAS No.:

546EPA SAMPLE NO.

APD-SDT4(D)-0.

SDG No.: B2581

Matrix (soil/water) :


% Solids: 73.5

Lab Sample ID: 962581B-Q7



Color Before:

~ Color After:

Comments;

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-657-12-5

Analyte

AluminumAntimonyArsenicBarium.Berylliumfjirtnri itmcalciumCtufomium

cobaltcopperironLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilversodiumThalliumvanadiumZinccyanide

Concentration

iff 0 . 12

C

U

Q

N

M

JkMkMkMRfciRMkMkMkMkMkMkMkMkMRcvMRMkMRMkMRMkMRMRMR



Texture:

Artifacts:

VALIDATE!FORM I - IN ILM03.0

,*. . - .. .*,,.,'• •.. .-• •>;.-.-.iwj* ;- . \ . "v --v*^*&S£n jBBEf)&P^*'-i?

t'*&''*i~ Z/"*''-* -JStftyrr- **''-"*' ~ '

T_"'-'*-Y'-^-'--*'-V'

:-':'---' • i- -'

J- J

.-- a», ''jMlt'-'vg '' ^ /L ' ^ i ^TTTTOTgBlgTHP^ " '

technical memorandum phase ii wetland …surrounding area. stakes marking the position of sd33, sw12...

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