supporting information for liu, okamoto, alexy, hong, tran...
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SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-67
1H NMR and 13C NMR Spectra of New Compounds
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 3aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-68
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 3aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-69
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 5aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-70
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-71
1 H N
MR
(500
MH
z, C
6D6)
of c
ompo
und 5ab.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-72
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ab.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-73
1 H N
MR
(500
MH
z, C
6D6)
of c
ompo
und 5ac.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-74
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ac.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-75
1 H N
MR
(500
MH
z, C
6D6)
of c
ompo
und 5ad.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-76
13C
NM
R (1
25 M
Hz,
C6D
6) o
f com
poun
d 5ad.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-77
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 5ae.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-78
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 3aa.
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ae.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-79
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 5af.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-80
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5af.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-81
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 5ag.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-82
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ag.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-83
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 5ba.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-84
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ba.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-85
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 5ca.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-86
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5ca.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-87
1 H
NM
R (5
00 M
Hz,
CD
Cl 3)
of c
ompo
und 5da.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-88
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 5da.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-89
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 5ea.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-90
13C
NM
R (1
00 M
Hz,
CD
Cl 3)
of c
ompo
und 5ea.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-91
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 5fa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-92
13C
NM
R (1
00 M
Hz,
CD
Cl 3)
of c
ompo
und 5fa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-93
1 H
NM
R (4
00 M
Hz,
CD
Cl 3)
of c
ompo
und 1a
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-94
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 1a
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-95
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 1d
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-96
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 1d
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-97
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 1e
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-98
13
C N
MR
(100
MH
z, C
DC
l 3) o
f com
poun
d 1e
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-99
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d 1f.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-100
13C
NM
R (1
00 M
Hz,
CD
Cl 3)
of c
ompo
und 1f
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-101
1 H N
MR
(400
MH
z, C
DC
l 3) o
f com
poun
d S5aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-102
13C
NM
R (1
00 M
Hz,
CD
Cl 3)
of c
ompo
und S5aa
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-103
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-104
13
C N
MR
(125
MH
z, C
DC
l 3) o
f com
poun
d 7aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-105
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7aa’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-106
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7aa’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-107
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ba.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-108
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ba.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-109
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ba’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-110
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ba’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-111
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ca.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-112
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ca.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-113
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ca’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-114
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ca’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-115
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7da.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-116
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7da.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-117
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7da’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-118
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7da’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-119
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ab.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-120
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ab.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-121
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ab’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-122
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ab’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-123
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ad.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-124
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ad.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-125
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ad’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-126
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ad’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-127
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ae.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-128
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ae.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-129
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7ae’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-130
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7ae’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-131
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7af.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-132
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7af.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-133
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 7af’.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-134
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 7af’
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-135
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d S2.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-136
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und S2
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-137
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 9aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-138
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 9aa.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-139
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 6b.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-140
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 6b
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-141
1 H N
MR
(500
MH
z, C
DC
l 3) o
f com
poun
d 6d.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-142
13C
NM
R (1
25 M
Hz,
CD
Cl 3)
of c
ompo
und 6d
.
SupportingInformationforLiu,Okamoto,Alexy,Hong,Tran,andStoltz
SI-143