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TEST REPORT 7LTC # 38.00 SMALL CASING PROTECTOR (FULL - PLASTIC) According to: API 5 CT 9-th Editions, Annex I; July 2011 / ISO 11960 * Note: if customer Specification values superior according to API, tests on product performed with values specified in customer Standard Specification. PTR 7.3.10 7" LTC Full Plastic Performance Test Report Issued by: Test Laboratory Effective Date: 11.10.2013 Rev. 1 Pg. 1 of 38 Approved: 11.10.2013 14:52 Voloșciuc Ion, SLI Approved: 11.10.2013 14:52 Tutunaru Iulian, MAC Approved: 11.10.2013 14:52 Frugoni Maurizio, DIG

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TEST REPORT 7” LTC # 38.00

SMALL CASING PROTECTOR

(FULL - PLASTIC)

According to:

API 5 CT 9-th Editions, Annex I; July 2011 / ISO 11960

* Note: if customer Specification values superior according to API, tests on product performed

with values specified in customer Standard Specification.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Issued by: Test Laboratory Effective Date: 11.10.2013 Rev. 1 Pg. 1 of 38 Approved: 11.10.2013 14:52Voloșciuc Ion, SLI

Approved: 11.10.2013 14:52Tutunaru Iulian, MAC

Approved: 11.10.2013 14:52Frugoni Maurizio, DIG

INDEX 1. PRODUCT GENERAL INFO 3

Drawing 0003 – BSC-T & C Tubing and Casing Full Plastic Protector 3

TABLE 1 - TEST SPECIFICATION 4

2. TEST REQUIREMENTS AND METHODOLOGY DESCRIPTION 5

2.1. AXIAL IMPACT TEST 5

2.2. ANGULAR IMPACT TEST 6

2.3. STRIPPING TEST 7

2.4. HOOKABILITY TEST 7

2.5. VIBRATION TEST 8

2.6. TORQUE TEST 9

2.7. CORROSION TEST 10

2.8. DIMENSIONAL STABILITY TEST 10

3. PRODUCT TEST RESULTS 12

3.1 AXIAL CRASH TEST 12

3.2 ANGULAR CRASH TEST 18

3.3. STRIPPING TEST 24

3.4. HOOKABILITY TEST 27

3.5. VIBRATION TEST 29

3.6. TORQUE TEST 30

3.7. CORROSION TEST 34

3.7. DIMENSIONAL STABILITY TEST 36

4. TESTS SUMMARY 38

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 2 of 38

Drawing 0003 – BSC-T & C Tubing and Casing Full Plastic Protector

1. PRODUCT GENERAL INFO

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 3 of 38

TABLE 1 - TEST SPECIFICATION

TEST T, °C TYPE

SPECIFIED TEST VALUE

UNIT TEST CONDITIONS ACCEPTANCE

CRITERIA

PRODUCT RANGE

≤3 ½ >3 ½ to

8 ¾ >8 ¾

AXIAL

IMPACT

+66 All

No damages and ovality

of the connection’s thread

and seal area after test

performance.

407 1627 2034

Jou

les

Minimum free fall of the hitter 0.3m

(12”) +21 All 407 1627 2034

-46 All 230 814 1085

ANGULAR

IMPACT (45°)

+66 All 203 814 1017 Place the protector and end size

piece at 45° from the horizontal. Minimum free fall of the hitter 0.3m

(12”)

+21 All 203 814 1017

-46 All 115 407 542

VIBRATION

TEST +21 All

Do not fall off or out

during a one-million-

cycle test

MIL STD 810G;

900 RPM Minimum;

- 0.33” Minimum vertical

displacement;

- Minimum acceleration of 4 time the

gravity during 1000 000 cycles;

STRIPPING

TEST

+66 PIN Protector threads may

signs of stress but shall

not be torn away Fax = 60 · W

LB

S - W – pipe mass;

- Apply storage or thread

compounds*, stabilize at given

temperatures and perform the test

+21 PIN

-46 PIN

HOOKABILITY

TEST +21 All

No damages on the

connections thread and/or

seal Lx = 45 · W · 1.5

LB

S - W – pipe mass;

- The protector manufacturer shall

demonstrate that the connections suffer no damage during handling

CORROSION

TEST +35 All

No corrosion on the

thread and seal areas.

Less than 10% corrosion

acceptable in the rest of

the connection

- According to ASTM B 117;

- Apply storage or thread

compounds˟, makeup at specified

torque, the other end shall be closed

with a ventilation hole.

- Perform the salt spray test for 1000 hours

TORQUE TEST

+66 All Meet the makeup and

brake out requirements.

Damages on seal, loosing

torque and disengagement

are considered as rejects.

- Apply storage of thread

compounds*, makeup the protector at specified torque and room

temperature, stabilize at each

temperature and brake out the protector. Record the result.

+21 All

-46 All

DIMENSIONAL

STABILITY

TEST

+66 All Variation in thread

diameter shall be less than

50% of the connection

thread height

- Measure the diameter at room

temperature;

- Stabilize at each test temperature

and record the diameter;

- Stabilize again at room temperature and record the diameter;

- Compare results.

+21 All

-46 All

* Used thread compound type: BESTOLIFE 2010 NM ULTRA.

˟ Used thread compound type: Kendex OCTG Orange 4421-608.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 4 of 38

2. TEST REQUIREMENTS AND METHODOLOGY DESCRIPTION

2.1.AXIAL IMPACT TEST

The primary function of a thread protector for the pipe ends is to protect the threads and

critical sealing areas from impact. This type of damage may occur at any point during the

transportation and handling process.

The tests must be performed at three

different environmental conditions -46°C,

+21°C and + 66°C (-50ºF, 70ºF, 150ºF),

that potentially could modify the

characteristics of the protectors. For the

tests it has been employed a guillotine that

reproduces the requested energy. The

sample shall be placed in a vertical

position, with the thread and the protector

in the upper part. The impact shall be

done in the middle of the protector.

The protector shall withstand an impact according to the energy value described in the table 2

below:

Table 2. Axial Impact Energy Values

Temperature 0C Minimum impact energy in Joules

≤ 3 ½” >3 ½” to 8 ¾” > 8 ¾”

66 407 1627 2034

21 407 1627 2034

-46 230 814 1085

The impact shall be given with a solid metal

bar 1 ½” (38 mm) wide and a minimum free

fall height of 12” (30 cm);

The impact should be performed at three

different temperatures:

+66⁰C;

+21⁰C;

- 46⁰C;

To ensure that the protectors and its end

size pieces have completely acquired the

temperature (externally but also internally)

the piece must have soaked at the required

temperature for at least 30 minutes.

To be considered as approved, the

connection must not present any damages

after the impact at any of the three test

temperatures, even if the protector is

completely destroyed (Fig.2).

Fig.2 a) NOK b) OK

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 5 of 38

2.2. ANGULAR IMPACT TEST

For angular impact it has been employed a

flat steel plate.

The sample shall be placed in a 45⁰ angle

position, with the protector in the upper part.

The impact shall be done in the face of the

protector.

The protectors shall withstand an impact

according to the energy value described in the

following table:

Table 3. Angular Impact Values

Temperature 0C Minimum impact energy in Joules

≤ 3 ½” >3 ½” to 8 ¾” > 8 ¾”

+66 203 814 1017

+21 203 814 1017

-46 115 407 542

The impact shall be performed with a flat

steel plate and a minimum free fall height of

12” (30 cm).The impact shall be given a

three different temperatures:

+66⁰C;

+21⁰C;

-46⁰C;

To ensure that the protectors and end size

pieces have completely acquired the

temperature the piece must have soaked at

the required temperature for at least 30

minutes.

To be considered as approved, the

connection must not present any damage

and ovality after the impact at any of the

three test temperatures, even if the protector

is destroyed.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 6 of 38

The stripping test is fundamental to evaluate the capacity of a pin protector to remain on

the pipe when an axial force is exerted on the inner edge. This force might be a result of a

relative motion between two adjacent joints during the transportation, or it might occur during

handling when a pipe is dragged along the ground up to the drill floor.

Here the formula applied:

Fax = 60 • w

Where:

Fax – axial force (pounds force);

60 – constant;

w - nominal weight. (pounds/feet)

This test applies only for the pin protector. The objective of this test is to validate the

protector resistance to striping while being pulled away from the connection.

For make a test:

- Apply the storage and/or thread

compound to the connection as required.

- Make up the protector as per

specification. Record the makeup torque.

- Stabilize the test piece sets at -46, +21

and +66⁰C.

- Perform the stripping test according to

IADC/SPE 11396 and the required

temperature and with an axial load equal

or greater than Fax.

- After the test, remove the protector and inspect for torn threads.

- Acceptance criteria is “Protector Thread may show sign of stress but shall not be torn away”.

2.4.HOOKABILITY TEST

For protectors designated as liftable, must be performed test to confirm the suitability of the

protector in lifting applications. Two separate test shall be performed using the same load, but at

different angles to represent different types of rigging set-ups.

For the first test load, the lifting wire shall apply the load in a direction approximately

perpendicular to the axis of the pipe sample.

For the second test load the lifting wire shall apply a load in a direction approximately 20°

from the axis of the pipe. The test load shall be calculated as follows:

L (load, lbs) = 1.5 • 45 (ft) • W (lbs/ft)

Make-up the test pieces at ambient temperature with storage compound using the

recommended force torque from table 4. Apply the load and hold for 5 minutes. Remove the

load and inspect the connection for damage. The type of hook, loads and test set-up shall be

documented.

2.3.STRIPPING TEST

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 7 of 38

2.5. VIBRATION TEST

During transportation pipes are carried by road on the back of a trailer, thread protectors are

submitted to vibration loading. Under these condition protectors must remain screwed to

continue to provide an optimum protection.

Make-up the test pieces at ambient temperature with storage compound using the

recommended installation torque force form Table 5.

Perform vibration testing as per MIL STD-810. Test shall be conducted at a minimum of

900 RPM (15 hertz) with a minimum of 0.33 inches vertical displacement.

The protector shall not fall off or out during a one-million-cycle test.

After the completion of the test measure and record the breakout torque for the protector.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 8 of 38

2.6. TORQUE TEST

The purpose of this test is to determine protector reacts to temperature changes and

excessive make-up torque. Protectors, which are damaged during make-up, will be more

susceptible to loosen or fall off during transportation and handling. Temperature changes can

affect the fit of the protector.

To evaluate the torque stripping resistance of the thread protector during make-up, an

attempt should be made to "strip-out" the pin and box protector.

The required "strip-out" torque must meet or exceed the over-torque limits specified below:

Table 5.

Diameter [ "inch]

INSTALLATION TORQUE OVERTORQUE

TEST

[ N.m ] [ Lb.ft ]

Min Max Min Max

[ N.m ]

2 3/8 35 51 26 37,6 154

2 7/8 43 62 31,8 45,5 186

3 1/2 52 76 38,3 55,6 227

4 60 86 44,1 63,6 260

4 1/2 68 97 49,9 71,6 293

5 76 108 55,6 79,5 325

5 1/2 83 119 60,7 87,5 357

5 3/4 86 124 63,6 91,1 372

6 90 130 66,5 95,4 390

6 5/8 99 143 73 104,8 428

7 105 151 77,3 111,3 455

7 5/8 114 164 83,9 120,7 493

7 3/4 117 167 86 122,9 502

8 5/8 130 186 95,4 136,7 558

9 5/8 138 197 101,2 144,6 590

9 7/8 158 199 116,4 146,1 597

10 158 199 116,4 146,1 597

10 3/4 161 203 118,6 148,9 608

11 1/2 164 205 120,7 151,1 617

11 3/4 165 208 121,5 152,6 623

12 3/4 169 211 124,4 155,5 635

13 3/8 171 214 125,8 157,6 644

13 3/4 173 216 127,3 159,1 650

13 5/8 172 215 126,5 158,4 647

14 173 217 127,3 159,8 652

16 181 227 133 167 682

16 1/8 181 227 133 167 682

17 185 231 135,9 169,9 694

17 7/8 188 235 138,1 172,8 706

18 189 236 138,8 173,5 708

18 5/8 191 239 140,3 175,7 717

>18 5 /8 200 250 150 180 750

To evaluate the effects of temperature, make-up the sample using storage compound and

manufacturer's recommended practice and torque.

Record the temperature and the torque used for make-up. Stabilize the samples at -50°F, 68°F

and 150°F and breakout the protector recording the torque.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 9 of 38

2.7. CORROSION TEST

A protector should be able to prevent water penetration along threaded area in order to

prevent potential corrosive attack of threads and seals.

Make-up the test pieces at ambient temperature with storage compound using the

recommended torque Table 5.

The cut-off end of the connector shall be sealed and protector vented to allow air flow

circulation.

A salt spray test per ASTM B117 shall be conducted for as minimum of 1000 hours at + 35°C

(95°F).

The test piece shall be oriented in the test chamber to simulate pipe rack storage.

At the completion of the test remove the sample and inspect for corrosion.

Seal surfaces shall have no corrosion damage. Other areas of the connection shall have less

than 10% damage on the external surfaces of pin connections and the internal surfaces of box

connections.

Record the storage compound used and provide photos of any corrosion areas.

2.8.DIMENSIONAL STABILITY TEST

Measure and record the thread diameters on the protector at 21°C (70°F).

Stabilize the samples at -46°C (-50°F), and 66°C (150°F) and immediately measure and

record the thread diameters.

Re-stabilize the samples at 21°C (70°F) measure and record dates again.

Changes in thread diameter resulting in thread engagement of less than one-half of the

specified thread height per side shall be unacceptable throughout the design temperature range.

In pictures below, special instruments used to measure samples diameters.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 10 of 38

Specialized certified Laboratory to perform all API 5CT 9-ed. Annex I Specification / ISO 11960 tests.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 11 of 38

3. PRODUCT TEST RESULTS

3.1 AXIAL CRASH TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 328,8 Sample code 290/13 Angle of impact, ⁰ 90 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +24,8 Test T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 52,5 E(ENERGY) ,Joule 1627 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 50,44 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 50,44 = 80,44 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and coupling thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 12 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 328,8 Sample code 289 /13 Angle of impact, ⁰ 90 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +24,8 Test T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 52,8 E(ENERGY) ,Joule 1627 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 50,44 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 50,44 = 80,44 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and coupling thread area.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 13 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 166,1 Sample code 291 /13 Angle of impact, ⁰ 90 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +25 Test T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 41 E(ENERGY) ,Joule 814 Steel bar Presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 =49,95 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 49,95 = 79,95 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and coupling thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 14 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 328,8 Sample code 281/13 Angle of impact, ⁰ 90 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +24,8 Test T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 52,5 E(ENERGY) ,Joule 1627 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 50,44 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 50,44 = 80,44 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 15 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 328,8 Sample code 283/13 Angle of impact, ⁰ 90 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +24,8 Test T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 52,5 E(ENERGY) ,Joule 1627 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 50,44 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 50,44 = 80,44 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 16 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Axial Crash Test W(WEIGHT), kg 166,1 Sample code 282/13 Angle of impact, ⁰ 90 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25 Test T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 41 E(ENERGY) ,Joule 814 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 49,59 cm

H(TOTAL HEIGHT), cm 30 (connection height) + 49,95 =79,95 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 17 of 38

3.2 ANGULAR CRASH TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 266,1 Sample code 293/13 Angle of impact, ⁰ 45 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C + 25,7 T(TEMPERATURE), ⁰C + 21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 64 E(ENERGY) ,Joule 814 Steel bar absence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 31,18 cm

H(TOTAL HEIGHT), cm 34,3 (connection height) + 31,18 = 65,48cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLES TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and coupling thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 18 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 266,1 Sample code 292/13 Angle of impact, ⁰ 45 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C + 25,7 T(TEMPERATURE), ⁰C + 66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 64 E(ENERGY) ,Joule 814 Steel bar absence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 31,18 cm

H(TOTAL HEIGHT), cm 34,3 (connection height) + 31,18 = 65,48 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLES TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and coupling thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 19 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 137,1 Sample code 294/13 Angle of impact, ⁰ 45 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +20 T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 64 E(ENERGY) ,Joule 407 Steel bar absence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 30,26 cm

H(TOTAL HEIGHT), cm 34,3 (connection height) + 30,26 = 64,56 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS Protector damaged but no damage or deformation of connection seal and

coupling thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 20 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 266,1 Sample code 284/13 Angle of impact, ⁰ 45 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25,7 T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 48,2 E(ENERGY) , Joule 814 Steel bar absence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 31,18 cm

H(TOTAL HEIGHT), cm 33,5 (connection height) + 31,18 = 64,68 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 21 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 266,1 Sample code 286/13 Angle of impact, ⁰ 45 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25,7 T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 48,2 E(ENERGY) ,Joule 814 Steel bar absence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 31,18 cm

H(TOTAL HEIGHT), cm 33,5 (connection height) + 31,18 = 64,68 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 22 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Angular Crash Test W(WEIGHT), kg 131,7 Sample code 285/13 Angle of impact, ⁰ 45 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25 Test T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 60 E(ENERGY) ,Joule 407 Steel bar presence

h(FREE FALL HEIGHT), cm

h(cm) =

• 100 ;

h(cm) =

• 100 = 31,50 cm

H(TOTAL HEIGHT), cm 33,5 (connection height) + 31,50 = 65,00 cm

IMAGES

SAMPLE BEFORE IMPACT CONNECTION BEFORE IMPACT

SAMPLE BEFORE IMPACT SAMPLE TEMPERATURE

IMPACT SAMPLE TESTED

SAMPLE AFTER IMPACT CONNECTION AFTER IMPACT

RESULTS No damage or deformation of connection seal and pipe thread area

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 23 of 38

3.3. STRIPPING TEST

TYPE OF

PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Stripping test W (Lb/Ft) 38,00 Sample code 302/13 Stripping angle, ⁰ 0 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25,4 T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 40

SF (stripping force) N

SF (N) =

SF (N) = = 10146 N

Sw (stripping weight) kg

Sw (kg) = SF (N) / 9,81

Sw (kg) = 10146 N / 9,81

= 1034,25 kg

IMAGES

SAMPLE BEFORE TEST THREAD OF PROTECTOR BEFORE TEST

TEST PREPARATION SAMPLE TEMPERATURE

TEST VALUE TEST SAMPLE

SAMPLE AFTER TEST CONNECTION AFTER TEST

RESULTS Protector withstands to 1358 kg/f. Not observed damage of protector thread.

PTR 7.3.10 7" LTC Full Plastic Performance Test Report Rev. 1 Pg. 24 of 38

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Stripping test W (Lb/Ft) 38,00 Sample code 288/13 Stripping angle, ⁰ 0 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25,4 T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 40

SF (stripping force) N

SF (N) =

SF (N) = = 10146 N

Sw (stripping weight) kg

Sw (kg) = SF (N) / 9,81

Sw (kg) = 10146 N / 9,81

= 1034,25 kg

IMAGES

SAMPLE BEFORE TEST THREAD OF PROTECTOR BEFORE TEST

TEST PREPARATION SAMPLE TEMPERATURE

TEST VALUE TEST SAMPLE

SAMPLE AFTER TEST THREAD OF PROTECTOR AFTER TEST

RESULTS Protector withstands to 1224 kg/f. Not observed damage of protector thread.

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Stripping test W (Lb/Ft) 38,00 Sample code 303/13 Stripping angle, ⁰ 0 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25 T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 41

SF (stripping force) N

SF (N) =

SF (N) = = 10146 N

Sw (stripping weight) kg

Sw (kg) = SF (N) / 9,81

Sw (kg) = 10146 N / 9,81

= 1034,25 kg

IMAGES

SAMPLE BEFORE TEST THREAD OF PROTECTOR BEFORE TEST

TEST PREPARATION SAMPLE TEMPERATURE

TEST VALUE TEST SAMPLE

THREAD OF PROTECTOR AFTER TEST CONNECTION AFTER TEST

RESULTS Protector withstands to 1300 kg/f. Not observed damage of protector thread.

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3.4. HOOKABILITY TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Hookability test W (Lb/Ft) 38,00 Sample code 296/13 Hanging angle, ⁰ 45 Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +24,9 T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 54

HF (hanging force) N

HF (N) =

HF (N) = = 11414,25 N

Hw (hanging weight) kg

Hw (kg) = HF (N) / 9,81

Hw (kg) = 11414,25 N / 9,81

= 1163,53 kg

IMAGES

SAMPLE BEFORE TEST CONNECTION BEFORE TEST

TEST PREPARATION SAMPLE TEMPERATURE

TEST VALUE TEST SAMPLE

SAMPLE AFTER TEST CONNECTION AFTER TEST

RESULTS The test has been performed with the appropriate range of hooks type UNI4395 and

DIN 15401. Not damaged coupling sealing face and internal thread of connection.

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Hookability test W (Lb/Ft) 38,00 Sample code 304/13 Hanging angle, ⁰ 45 Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +24,9 T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 54

HF (hanging force) N

HF (N) =

HF (N) = = 11414,25 N

Hw (hanging weight) kg

Hw (kg) = HF (N) / 9,81

Hw (kg) = 11414,25 N / 9,81

= 1163,53 kg

IMAGES

SAMPLE BEFORE TEST CONNECTION BEFORE TEST

TEST PREPARATION SAMPLE TEMPERATURE

TEST VALUE TEST SAMPLE

SAMPLE AFTER TEST CONNECTION AFTER TEST

RESULTS The test has been performed with the appropriate range of hooks type UNI4395

and DIN 15401. Not damaged pipe sealing face or connection thread.

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3.5. VIBRATION TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX & PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Vibration test Measured vertical displacement, mm 8,38

Sample(s) code 295/13 287/13

Measured Frequency (ν), (rot/min) 1076 Connection(s) code

T700P1 T700B1

Test Duration, h D =

=

= 15,48 h

Test T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) Number of cycles 1000 000 Min gravit. Acceleration, g 4 Min. Frequency, (rot/min) 900 LT (LAB. TEMPERATURE), ⁰C +23,4 Torque screwing force, Nm 150 LH (HUMIDITY IN THE LAB.) % 52

IMAGES

SAMPLES BEFORE TEST INITIAL POSITION

SAMPLE TEMPERATURE MEASURED FREQUENCY

DURING THE TEST TEST TIME

FINAL SAMPLES POSITION

RESULTS

Protectors do not fall out from pipe samples and did not move from its initial position. PIN protector was screwed with - 150 Nm and unscrewed with - 120 Nm force BOX protector was screwed with – 150 Nm and unscrewed with - 100 Nm force

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3.6. TORQUE TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 298/13 Usf (Range unscrewing), Nm NA Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +25,7 Test T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 48,2

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWED FORCE

RESULTS Protector was unscrewed with a force of 175 Nm at +24,5⁰C

TYPE OF

PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 297/13 Usf (Range unscrewing), Nm NA Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +25,7 Test T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 48,2

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWED FORCE

RESULTS Protector was unscrewed with a force of 130 Nm at +67⁰C

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TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 299/13 Usf (Range unscrewing), Nm NA Connection code T700B1 LT (LAB. TEMPERATURE), ⁰C +25 Test T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 41

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWING FORCE

RESULTS Protector was unscrewed with a force of 100 Nm at -50⁰C

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 293/13 Usf (Range unscrewing), Nm NA Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +25,7 Test T(TEMPERATURE), ⁰C +21 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 48,2

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWED FORCE

RESULTS Protector was unscrewed with a force of 175 Nm at +25⁰C

TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 292/13 Usf (Range unscrewing), Nm NA Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +24,8 Test T(TEMPERATURE), ⁰C +66 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 52,5

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWED FORCE

RESULTS Protector was unscrewed with a force of 100 Nm at +70⁰C

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Torque test Sf (Screwing force), Nm 150 Sample code 307/13 Usf (Range unscrewing), Nm NA Connection code T700P1 LT (LAB. TEMPERATURE), ⁰C +20 Test T(TEMPERATURE), ⁰C -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 70

IMAGES

SAMPLE BEFORE TEST TORQUE SCREWING FORCE

SAMPLE TEMPERATURE UNSCREWED FORCE

RESULTS Protector was unscrewed with a force of 175 Nm at -42,5 ⁰C

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3.7. CORROSION TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Corrosion test Conc of NaCl solution, % 5 Sample code 365/13 pH 6,5-7,2 Connection code 192 Mist concentration, 2 ml at 80 cm Test time, h 1000 LT (LAB. TEMPERATURE), ⁰C NA Test T(TEMPERATURE), ⁰C +35 LH (HUMIDITY IN THE LAB.) % NA

Pressure atomizer, atm min 2

IMAGES

SAMPLE BEFORE TEST CONNECTION BEFORE TEST

TEST PREPARATION DURING TEST

CONNECTION AFTER TEST CONNECTION AFTER TEST

SAMPLE AFTER TEST CONNECTION AFTER CLEANING

RESULTS No corrosion detected on sealing face and coupling / pipe threads.

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Corrosion test Conc of NaCl solution, % 5 Sample code 364/13 pH 6,5-7,2 Connection code 190 Mist concentration, 2 ml at 80 cm Test time, h 1000 LT (LAB. TEMPERATURE), ⁰C NA Test T(TEMPERATURE), ⁰C +35 LH (HUMIDITY IN THE LAB.) % NA

Pressure atomizer, atm min 2

IMAGES

SAMPLE BEFORE TEST CONNECTION BEFORE TEST

TEST PREPARATION DURING TEST

CONNECTION AFTER TEST CONNECTION AFTER TEST

SAMPLE AFTER TEST CONNECTION AFTER CLEANING

RESULTS No corrosion detected on sealing face and coupling / pipe threads.

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3.7. DIMENSIONAL STABILITY TEST

TYPE OF PROTECTOR 7” LTC - # 38.00 BOX CEL, (FULL PLASTIC)

CONDITIONS

Type of test Dimensional stability test Thread Height, mm 1,8 Sample code 300/13 Theoretical diameter, mm 176,24 Drawings code API specification Standard LT (LAB. TEMPERATURE), ⁰C +25 T(TEMPERATURE), ⁰C +21 & +66 & -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 55

Measuring point

DATA &

RESULTS

Temperature, ⁰C Thread Height, mm Theoretical diameter,

mm

Measured Diameter, mm

Measurement uncertainty,

mm Thread Engagement, %

+21

1,8 176,24

176,37 0,01 78,53

+66 177,07 0,01 98,00

+21 176,29 0,01 76,27

+21 176,29 0,01 76,27

-46 175,43 0,01 52,56

+21 176,32 0,02 77,26

IMAGES

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

GRAPHIC

CONCLUSION

Protector measured diameters did not exceeded permeated limits of engagement

(>=50% and <=100%) of thread height at all three extreme temperatures.

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TYPE OF PROTECTOR 7” LTC - # 38.00 PIN CEL, (FULL PLASTIC)

CONDITIONS

Type of test Dimensional stability test Thread Height, mm 1,8 Sample code 308/13 Theoretical diameter, mm 174,44 Drawings code API specification Standard LT (LAB. TEMPERATURE), ⁰C + T(TEMPERATURE), ⁰C +21 & +66 & -46 (+/- 6 ⁰C) LH (HUMIDITY IN THE LAB.) % 55

Measuring point

DATA &

RESULTS

Temperature, ⁰C Thread Height, mm Theoretical diameter,

mm

Measured Diameter, mm

Measurement uncertainty,

mm Thread Engagement, %

+21

1,8 174,44

174,59 0,02 70,78

+66 175,31 0,02 50,83

+21 174,68 0,03 68,44

+21 174,68 0,03 68,44

-46 173,68 0,05 96,11

+21 174,49 0,03 73,15

IMAGES

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

TEMPERATURE OF TEST GRAPHICAL ENGAGEMENT OF THREAD

GRAPHIC

CONCLUSION

Protector measured diameters did not exceeded permeated limits of engagement

(>=50% and <=100%) of thread height at all three extreme temperatures.

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TESTS SUMMARY

NR TYPE OF TEST TEMPERATURE / STATE

+21°C +66°C -46°C +35°C

1 AXIAL CRASH TEST OK OK OK NA

2 ANGULAR CRASH TEST OK OK OK NA

3 STRIPPING TEST OK OK OK NA

4 HOOKABILITIY TEST OK NA NA NA

5 VIBRATION TEST OK NA NA NA

6 TORQUE TEST OK OK OK NA

7 CORROSION TEST NA NA NA OK

8 DIMENSIONAL STABILITY TEST OK OK OK NA

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